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HomeMy WebLinkAboutWI0100106_Annual Report_20140613BUNNELL-LAMMONS ENGINEERING, INC. GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS REPORT OF ANNUAL GROUNDWATER AND SURFACE WATER SAMPLING AND ANALYSIS FOR 2013 FORMER ANDREX INDUSTRIES CORP. 180 DEAVERVIEW ROAD ASHEviLLE, NORTH CAROLINA BROWNFIELDS PROJECT NUMBER 07022-03-11 PREPARED FOR: ANDREX INDUSTRIES CORP. ASHEviLLE, NORTH CAROLINA PREPARED BY: BUNNELL-LAMMONS ENGINEERING, INC. GREENVILLE, SOUTH CAROLINA JUNE 13, 2014 BLE PROJECT NUMBER J13-1022-36 IHSB ID NUMBER NONCD0001271 GROUNDWATER INCIDENT NUMBER 6586 ttlltlllrlrri� CA i w 1 5 =7I rp 9 Car4t0.� #gyp`.; ,JJJJ1llttlllt1t ,1,A3 BUNNELL-LAMMONS ENGINEERING, INC. GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS June 13, 2014 Andrex Industries Corp. PO Box 648 Bondville, VT 05340 Attention: Mr. Stephen Gottdiener Subject: Report of Annual Groundwater and Surface Water Sampling and Analysis for 2013 Former Andrex Industries Corp. 180 Deaverview Road Asheville, North Carolina BLE Project Number J13-1022-36 Brownfields Project Number 07022-03-11 IHSB ID Number NONCD0001271 NCDENR Groundwater Incident Number 6586 Dear Mr. Gottdiener: As authorized by Andrex Industries Corp. acceptance of our proposal number P 13-0455 dated August 2, 2013, Bunnell-Lammons Engineering, Inc. (BLE) has performed required environmental services at the subject site. The purpose of this project was to collect and analyze groundwater and surface water samples as required by the North Carolina BrownBelds Program. The enclosed report describes the work performed and presents the results obtained. Project Information: Andrex formerly owned and operated an industrial textile production facility located at 180 Deaverview Road within the city limits of Asheville, North Carolina (Figure 1). The company operated a knitted fabric weaving and cutting business for women's and children's clothing at this location. In prior years, the facility was operated as a textile finishing business that conducted cutting, dry cleaning, shrinking and packaging of fabrics. The subject facility was in operation since the mid-1960s, although under various ownership. A two-story light manufacturing facility with approximately 77,000 square feet of office, manufacturing, warehouse, storage and utility space occupied the approximately nine -acre site. Two buildings were present at the site; a split level brick building and slab -on -grade metal building. No dry cleaning has been conducted on site since 1995. However, prior to 1995, dry cleaning operations were prevalent on site and the use of tetrachloroethylene (a.k.a. Perchloroethylene, PCE) was common. Virgin PCE was stored on site in a 6,000-gallon underground storage tank (UST). Prior to 1989, the use of the PCE UST was discontinued and the tank was filled with sand. The UST was replaced with a 6,000-gallon AST which was used until 1995. In 1995, dry cleaning processes and the use of PCE were discontinued. In 1991 concentrations of PCE were detected in the groundwater above the applicable North Carolina Title 15A Subchapter 2L (NC2L) groundwater standards' maximum level of 0.7 µg/1 and the NCDENR issued Groundwater Incident Number 6586 for the site. Concentrations of PCE were also 6004 PONDERS COURT PHONE (864)288-1265 GREENVILLE, SOUTH CAROLINA 29615 FAX (864) 288-4430 ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 documented in the soil near the PCE UST and at other subsurface facility locations. The NCDENR approved a comprehensive site assessment (CSA) and corrective action plan (CAP) for the site and remedial efforts were conducted from 1993 through 2005. Remedial efforts consisted of the installation and operation of two groundwater pump and treat (P&T) systems and one soil vapor extraction (SVE) system. The SVE and both groundwater P&T systems were operated and maintained by BLE for Andrex from May 2003 through August 2005. Treated groundwater effluent was discharged to the sanitary sewer under a MSD permit. BLE also performed annual site -wide groundwater and surface water sampling and analysis for Andrex to monitor the fate of the groundwater plume. BLE submitted quarterly reports of the remedial progress through August 2005 and annual groundwater monitoring reports through 2005 to the NCDENR to document site activities. The remediation system operations were suspended in August 2005 at the discretion of the property owner. Annual groundwater monitoring was also suspended at the discretion of the property owner, with the last sampling event conducted in November 2005. In early 2005, Andrex requested that BLE evaluate feasible remedial alternatives for the site. A preliminary review of alternate remedial technologies identified a unique opportunity to evaluate bioremediation at the site. Food -grade lactate containing byproducts (milk solution) from the neighboring Milkco, Inc. (Milkco) facility were being considered for use as a bio-enhancing remedial product for the former Andrex facility. The implementation of this type of remedial action was dependent upon the results of a feasibility study which includes bench- and field -scale testing studies of the lactate containing byproducts. In 2005, Andrex retained BLE to perform a pilot study of the milk solution. The study was to include two parts. The first part was a bench test which was to be followed by a field trial. BLE completed the bench study in early 2006. The results showed a net decrease in PCE concentration of 30% after 40 days in those microcosms containing the highest concentrations of milk solution. Significant concentrations of PCE daughter products were also produced in the bench study indicating successful de -chlorination of the parent product, as anticipated. The field trial portion of the pilot test was suspended by Andrex after the bench test results were obtained. In 2006, Milkco entered into a Brownfield's Agreement (Agreement) with the State of North Carolina as part of a potential purchase of the Andrex property. The property was sold in 2007 and as part of the plan (see below) for retrofit of the subject site; Milkco removed and/or demolished selected equipment and facility infrastructure. In August 2007, three underground storage tanks (one PCE and two heating oil) were removed and disposed by a contractor retained by Milkco on behalf of Andrex. The results of the activities were documented in a report titled Report of Limited Assessment for UST Closure dated November 26, 2007 (BLE Project No. J07-1022-20). As part of Milkco's redevelopment plans for the site, BLE issued a plan titled Work Plan for Redevelopment of the Andrex Brownfields Site (Milkco Cooler Expansion) dated June 13, 2008 (BLE Project No. J08-1022-23). The plan addressed the Program's requirements including excavation and disposal of contaminated soil (source area) and continued groundwater monitoring. The Program reviewed and approved (with modification) the plan in a letter to BLE dated July 7, 2008. The 2 ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 schedule for implementation of the redevelopment plan was changed on December 11, 2008 with concurrence of the Program. In July 2008, BLE abandoned selected groundwater monitoring and recovery wells in accordance with the approved redevelopment plan. The results of the well abandonment activities were documented in a report titled Report of Well Abandonment Services for the Milkco Cooler Expansion dated January 19, 2009 (BLE Project No. J08-1022-26). From July through September 2008, contaminated soils were removed and disposed by a contractor retained by Milkco in accordance with the approved redevelopment plan. The results of the remedial activities were documented in a report titled Report of Hotspot Soil Removal and Disposal for the Milkco Cooler Expansion dated June 3, 2009 (BLE Project No. J08-1022-25). By December 2008, the former Andrex brick building(s) and metal building had been demolished with only the building slabs remaining. Additionally, all groundwater and soil remediation systems had been dismantled, removed, and stored by Milkco. All work performed by Milkco (non - responsible party) is in compliance with the requirements of the NCDENR Brownfields Program (Program) and the Agreement. In February 2008, Andrex resumed annual groundwater monitoring at the site. BLE has performed the sampling services and prepared and submitted reports each calendar year since 2008. The approved redevelopment plan requires the continuation of annual groundwater monitoring and remedial activities at the site. In June 2010, BLE submitted a permit application to the NCDENR UIC program for a field -scale pilot test for remediation of the site's groundwater using milk solution. Subsequent information was requested by the DWQ and that information was prepared and/or collected, and submitted by BLE in August 2010 and December 2010. On December 22, 2010, the DWQ issued Injection Permit WI0100106 to Milkco. The permit requires special conditions and limitations including minor modifications to the injection monitoring plan. The permit effective dates were December 22, 2010 through November 20, 2013 with a renewal option if submitted 120 days prior to expiration of the permit. The permit was part of a green/sustainable enhanced bioremediation approach utilizing milk solution. The injection plan included an injection schedule over 5 years with semi-annual injections planned for the first two years. BLE proposed to conduct the project in phases with the first phase including two injection events (and monitoring) within a 12-month period (designated "Year One" in the plan). BLE was retained by Milkco to perform the injection and monitoring services for year one in 2011. Subsurface injections of milk solution into four former groundwater recovery wells were performed in May/June 2011 and September/October 2011 and monitoring was conducted as planned. The results showed that daughter products of PCE were being created as anticipated. Based on these data, injections during the first half of 2012 were suspended and monitoring was conducted to determine the long-term results of the 2011 injections. Sampling was conducted at a 60-day monitoring frequency through July 2012 and site -wide annual sampling conducted in September 2012. Based on the results obtained we recommended the performance of a third injection event in late September 2012 with a 60-day monitoring frequency through March 2013. These modifications were documented in a letter to the UIC Program titled Notice of Intent for Milk Solution Injection & Monitoring [3rd Injection Event and 3 ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 Monitoring Events (2012-2013)J dated September 12, 2012 (BLE Project No. J12-1022-35). The UIC approved the plan and the 3' injections were performed in September/October 2012 with subsequent monitoring conducted through March 2013. BLE issued an interim evaluation report documenting the performance of all 3 injection events and the 13 monitoring events performed to evaluate the results of the field -scale pilot test. The report titled Interim Evaluation Report -- Field -Scale Pilot Test UIC Permit No. WI0100106 dated July 30, 2013 (BLE Project No. J12-1022-35) which concluded that the pilot project was successful and full- scale injection should be performed as a viable groundwater remedial measure. At the request of Milkco, BLE prepared and submitted a permit renewal application dated July 30, 2013 and addendum dated November 19, 2013. The application included a plan for injection and monitoring over a 5 year permit term. The application et seq. and plan was approved (with modification) by the NCDENR in a letter to Milkco dated December 13, 2013. BLE has completed the required annual groundwater monitoring for the 2013 calendar year. The enclosed report describes the work performed and presents the results obtained as required in the approved redevelopment plan (et seq.). 11 ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 Scope of Services: On September 9, 2013, groundwater levels were measured and on September 10-13, 2013 samples were collected from the monitoring and recovery wells, as required. Groundwater sampling logs are included in Appendix A. Samples were collected from all wells except MW-1 through MW-4, MW-8, MW-8A, MW-19, MW-25, RW-2, and RW-4 as these wells were not present at the time of sampling (abandoned or destroyed). Samples were also collected from affected surface waters on September 13, 2013. The samples were analyzed at Pace Analytical Services, Inc. (Pace), in Huntersville, North Carolina by EPA Method 8260 MSV Low Level and for a subset of samples at Pace, in Asheville, North Carolina by SM 5310B (Appendix B). Water levels and groundwater elevations measured prior to sampling are shown on Table 1. A groundwater elevation contour map is included as Figure 2. Results of Groundwater Sampling: Chlorinated volatile organic compounds (VOCs) detected in the groundwater samples above the North Carolina standards (based on North Carolina's Class GA Groundwater Standards T15A Subchapter 2L) include but are not limited to: tetrachloroethene, trichloroethene, cis-1,2-dichloroethene, and vinyl chloride (Table 2). A historical contaminant concentration database and total chlorinated VOC data plots are presented in Appendix C. The data plots were visually evaluated and our interpretations of the overall contaminant trends from the initial sampling date of each well are presented below. Declining Stable Increasing Non -Detect MW-1 ** MW-9 MW-7 MW-20*** MW-2** MW-13 MW-15 MW-21 * * * MW-3** MW-14 MW-16 MW-22 MW-4** MW-18 MW-19* MW-5 MW-24 MW-25* MW-6 RW-1^^^^ MW-26 MW-8** RW-4** MW-8A** MW-10 MW-11 MW-12 MW-17 MW-23 RW-2** RW-3 RW-5 RW-6 RW-7**** * -- Well destroyed in 2003; not present at the time of the 2009 sampling event. ** -- Well abandoned after the 2008 sampling event (see subsequent sections of this report). Detected concentrations of chloroform are unrelated to the groundwater incident. **** -- Well is broken at depth and filled with roots as of September 2011. AAA -- Due to decreasing concentrations of PCE and increasing concentrations of daughter product. 5 ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 Sampling of groundwater for total organic carbon (TOC) began as part of the injection project in 2009 and is required for specific wells and surface water sampling points as part of the UIC permit. A historical summary table of TOC results was prepared as part of the aforementioned Interim Evaluation Report and has been updated to include data from this annual groundwater monitoring event (Table 3). The TOC results for the 2013 sampling event are similar to the historical results. Status of Well Conditions: Monitoring wells MW-19 and MW-25 were destroyed in 2003 and MW- 24 was damaged in late 2003 or early 2004. Recall that MW-19 was located on the Satterfield residential property and that MW-24 and MW-25 were located on the Milkco property (Figures 2 and 3). Sampling of monitoring wells MW-19 and MW-25 could not be performed in 2003 and beyond because the wells had been destroyed. Monitoring well MW-19 appears to have been destroyed by grading in 2003, presumably by the City of Asheville, who graded the area for routing of storm water. The well cap was found on the ground surface but no other parts of the well could be located. Monitoring well MW-25 was destroyed by grading by contractors working for Milkco. The work was part of a facility expansion at Milkco in the summer of 2003. No traces of the well could be located. Neither BLE nor Andrex was contacted prior the destruction of these wells. The well head of MW-24 was damaged by grading contractors working for Milkco. The work was part of a facility expansion at Milkco in late 2003 or early 2004. BLE personnel observed surface water leaking into the damaged well head and made temporary repairs to stop the infiltration of surface water in 2004. In 2005 the well head was permanently repaired however it appeared that the well riser pipe was bent at about five feet below ground surface at the time the well head was damaged. We were unable to lower a bailer or well pump into MW-24 due to the bent riser pipe. The well was not sampled in 2004 or 2005. We recommended permanent abandonment and replacement of MW-24 in 2005. After approval by the responsible party, BLE completed abandonment and reinstallation of MW-24 in 2007. In the summer of 2008 (after sampling was conducted in February 2008), several of the monitoring and recovery wells were abandoned as part of the property redevelopment plan approved by the Program. A report of well abandonment was submitted under separate cover. Monitoring well MW-6 and recovery well RW-1 were extended to the ground surface as part of the grading activities for the Milkco expansion (new roadway). The well heads were reconstructed and the well elevations were resurveyed by BLE. The water level and well construction data on Table 1 reflects the changes. Please note that the extension of MW-6 resulted in a deviation (bend) of the riser pipe below the ground surface. A bailer cannot be lowered down the well so sampling was performed using a check valve and poly tubing. Purge volumes are significantly reduced using this method compared to conventional bailing. 0 ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 Results of Surface Water Sampling: The laboratory results of the surface water sampling are consistent with previous sampling events. Chlorinated VOCs detected in the surface water samples above the North Carolina standards (based on North Carolina's Class WS Surface Water Standards T15A Subchapter 213) include tetrachloroethene and trichloroethene (Table 2). The former sample location Smith Mill 1 (SM-1) was collected from a small garden pond on the former Jehovah Witness property prior to 2005. The former pond was filled in by the new owners of the Jehovah Witness property sometime after November 2004. The SM-1 sample location was moved in 2009 to the location shown on Figure 3 based on the 2008 results. A surface water sample (JW-1) was collected from the former Jehovah Witness property in 2013 as in prior years (Figure 3). The sample was collected from a drainage feature in an area that appeared to be a spring. The results from this year and prior years (2002 through 2005) indicate that the drainage feature is a groundwater discharge point for northernmost contaminant plume. It is apparent from the data that the discharge at the former Jehovah Witness spring directly affects the surface water quality in Smith Mill Creek Tributary at down gradient sampling locations (SM-4 through SM-6) shown on Figure 3. The sampling locations (SM-1 through SM-6) in Smith Mill Creek Tributary will remain the same in 2014. Sampling of surface water for Total Organic Carbon was performed this year as required in the UIC Permit. These data cannot be compared to pre -injection values since no historical data exists. The laboratory data is included in Appendix B and are summarized on Table 3. Remediation Progress: A groundwater pump and treat system (upper system) and a SVE system were installed at the site in the mid 1990's. Groundwater was recovered from two recovery wells RW- 1 and RW-2 attached to the upper system. Upgrades to the groundwater recovery systems were completed in 2002. The upgrades included the addition of one recovery well (RW-3) to the upper system and construction of a new lower system and the installation of four new lower system recovery wells (RW-4 through RW-7). After 2002, contaminated groundwater was recovered by seven recovery wells RW-1 through RW-7. Groundwater recovery from RW-1 through RW-3 (upper system) was restarted on March 25, 2002. Groundwater recovery from RW-4 through RW-7 (lower system) began on May 23, 2002. The system upgrades were documented in a report titled As -Built Engineering Plans and Specification Groundwater Pump and Treat Systems (2002 Upgrade) dated February 5, 2003. Operation of both groundwater systems was discontinued on August 23, 2005 and the funds for operation of the systems were diverted to a laboratory -scale (bench) pilot test of an alternate remedial technology. The bench test was completed in 2006, however reporting of the results was suspended by Andrex while the Brownfields Agreement was in progress. As part of the site redevelopment plan, the results of the bench test and plans for future groundwater remediation were submitted to the Program. The SVE system has not been operational since November 2004 when a power surge (presumed lightning strike) damaged the system. Repairs were not made as Andrex had proposed a discontinuance of SVE remedial operations to the NCDENR at that time. Repairs were contingent on the initiation of the pilot test described above. Andrex opted to conduct the pilot test and therefore the SVE system was not repaired. In the summer of 2008, as part of the approved redevelopment plan, both groundwater systems and the SVE system we disassembled and the equipment was placed in storage by Milkco. Additionally, as part of the redevelopment plan, "hotspot" soils (contaminated soils with concentrations above a ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 specified limit) were removed and disposed by Milkco on behalf of Andrex. A report of soil removal and disposal was submitted under separate cover. An underground injection control permit was obtained from the NCDWQ on December 22, 2010. Subsurface injection of milk solution into former groundwater recovery wells were performed in [May to June 2011], [September to October 2011], and [September to October 2012] and monitoring was conducted as planned. The aforementioned Interim Evaluation Report was issued on July 30, 2013 (BLE Project No. J12-1022-35) which concluded that the pilot project was successful and full-scale injection should be performed as a viable groundwater remedial measure. At the request of Milkco, BLE prepared and submitted a permit renewal application dated July 30, 2013 and addendum dated November 19, 2013. The application et seq. and plan was approved (with modification) by the NCDENR in a letter to Milkco dated December 13, 2013. Full scale injection and monitoring is scheduled for the 2014 calendar year and the results will be reported under separate cover. The results of the field -scale pilot test including the results of the most recent 2013 annual monitoring event show that daughter products of PCE are being created as anticipated. In 2012 significant reductions in solvent concentrations were observed in the RW-5 injection area. As a result, the contour map of the total VOC plume was split into two discrete zones. The plume map contouring remains similar in 2013 however there has been some rebound in RW-5 and MW-10 as contaminated groundwater from upgradient locations migrates into the test area. In 2012 it was noted that a majority of the total VOCs in the RW-3 injection area (which includes MW- 12) had been transformed to daughter product (cis 1,2-DCE). In 2013 the remaining cis 1,2-DCE in RW-3 and MW-12 had been degraded and is below NC2L standards (Table 2). The RW-3 and MW- 12 area is now highlighted on the plume map (Figure 3) and noted as an area of very low concentrations as the result of groundwater remediation. Please note that several VOCs are produced as metabolic byproducts of the groundwater bioremediation. These metabolic byproducts are specified in bold text in the footnotes on Table 2 and are included on the laboratory results in Appendix B. It should be noted that milk solution migration and resultant remediation was not as prevalent in monitoring well MW-5 as the result of injection in the RW-3 well. The MW-5 area will be targeted in future remedial efforts. 0 ♦ILL Andrei Industries — 2013 Groundwater Monitoring June 13, 2014 Asheville, NC BLE Project Number J13-1022-36 Qualification of Report: The activities and evaluative approaches used in this assessment are consistent with those normally employed in hydrogeological assessments of this type. Our evaluation of site conditions has been based on our understanding of the site and project information and the data obtained during our annual sampling effort. This report has been prepared on behalf of and exclusively for the use of Andrex Industries Corp. This report and the findings contained herein shall not, in whole or in part, be disseminated or conveyed to any other party or used or relied upon by any other parry excluding NCDENR, without BLE's prior written consent. Closing: We appreciate the opportunity to serve as your environmental consultant on this project. Please contact us at (864) 288-1265 if you have any questions or comments regarding this report. Sincerely, BUNNELL-LAMMONS ENGINEERING, INC. Trevor J. Bento P. Andrew W. Ale nder, P.G., RSM Senior Hydrogeologist Senior Hydrogeologist Registered, North Carolina #2025 Registered, North Carolina #1475 cc: Ms. Tracy Wahl — DWM Brownfields Program Mr. Brett Laverty — DWR WQROS — Asheville Regional Office Mr. Michael Rogers — DWR WQROS UIC Program — Raleigh Office Mr. Keith Collins — Milkco, Inc. e: lawalactive projectslandrex mi1kco1phase36 gw samp 201311022-36 repor6andrex report of 2013 groundwater 1022-36 final.docx 9 TABLES Table 1 Well Construction and Groundwater Elevation Data Andrex Industries Asheville, North Carolina NCDENR Groundwater Incident Number 6586 BLE Project No. J13-1022-36 September 9, 2013 Well Well Location Latitude (North) Longitude (West) Meas. Pt. Elevation Gnd. Surface Elevation Depth to Water (bmp) Water Elevation *Total Borehole Depth (bgs) *Screen Depth (bgs) *Screen Elevation Well Type Well Monitors *Top of Rock Depth (bgs) *Top of Rock Elev. MW-1 On -Site 2222.34 2222.58 NP-A NP-A 46.2 31.2 - 46.2 2191.4 - 2176.4 Ills BR 35.0 2187.6 MW-2 On -Site 2222.28 2222.62 NP-A NP-A 45.0 28.0 - 43.0 2194.6 - 2179.6 Ills BR 29.0 2193.6 MW-3 On -Site 2210.40 2207.76 NP-A NP-A 55.0 40.0 - 55.0 2167.8 - 2152.8 II BR 36.5 2171.3 MW-4 On -Site 2206.87 2207.04 NP-A NP-A 86.7 51.7 - 86.7 2155.3 - 2120.3 HIS BR 26.0 2181.0 MW-5 On -Site 2216.75 2216.92 43.73 2173.02 53.0 43.0 - 53.0 2173.9 - 2163.9 HIS BR 37.0 2179.9 MW-6 On -Site 2218.43 2218.67 50.80 2167.63 71.9 50.4 - 70.4 2168.3 - 2148.3 II PWR 56.4 2162.3 MW-7 On -Site 35.580866 82.613866 2218.35 2218.60 26.12 2192.23 35.0 24.5 - 34.5 2194.1 - 2184.1 II BR 12.0 2206.6 MW-8 On -Site 2182.33 2182.63 NP-A NP-A 24.5 13.0 - 23.0 2169.6 - 2159.6 II PWR 22.0 2160.6 MW-8A On -Site 2182.52 2182.70 NP-A NP-A 35.0 30.0 - 35.0 2152.7 - 2147.7 Ills BR 15.5 2167.2 MW-9 On -Site 2175.57 2175.95 22.11 2153.46 60.0 44.0 - 54.0 2132.0 - 2122.0 II BR 34.0 2142.0 MW-10 On -Site 2159.92 2159.45 14.63 2145.29 39.0 29.0 - 39.0 2130.5 - 2120.5 II PWR 35.0 2124.5 MW-11 On -Site 2166.00 2166.39 23.68 2142.32 58.5 48.0 - 58.0 2118.4 - 2108.4 II SAP >80.0 <2086.4 MW-12 On -Site 2219.17 2219.49 46.75 2172.42 81.0 60.0 - 70.0 2159.5 - 2149.5 II PWR 71.0 2148.5 MW-13 Off -Site 2138.80 2138.96 0.75 2138.05 58.5 48.0 - 58.0 2091.0 - 2081.0 II SAP 58.5 2080.5 MW-14 Off -Site 2138.94 2139.20 Artesian >2138.94 75.0 65.0 - 75.0 2074.2 - 2064.2 Ills BR 59.0 2080.2 MW-15 Off -Site 2124.89 2125.18 10.31 2114.58 40.0 33.3 - 40.0 2091.9 - 2085.2 III0 BR 32.5 2092.7 MW-16 Off -Site 2124.59 2124.85 10.16 2114.43 33.5 23.5 - 33.5 2101.4 - 2091.4 II PWR 33.5 2091.4 MW-17 Off -Site 2094.64 2094.74 3.53 2091.11 14.2 4.0 - 14.0 2090.7 - 2080.7 II SAP 14.2 2080.5 MW-18 Off -Site 2101.81 2101.92 8.00 2093.81 59.0 49.0 - 59.0 2052.9 - 2042.9 II SAP 59.0 2042.9 MW-19 Off -Site 2127.61 2127.82 NP-D NP-D 58.0 48.0 - 58.0 2079.8 - 2069.8 II SAP 58.0 2069.8 MW-20 Off -Site 2180.55 2180.54 31.38 2149.17 77.0 67.0 - 77.0 2113.5 - 2103.5 II SAP 77.0 2103.5 MW-21 Off -Site 2091.17 2091.31 1.29 2089.88 36.5 26.5 - 36.5 2064.8 - 2054.8 II SAP 36.5 2054.8 MW-22 Off -Site 2090.71 2090.84 0.50 2090.21 57.0 47.0 - 57.0 2043.8 - 2033.8 IIIs BR 46.0 2044.8 MW-23 Off -Site 35.582017 82.611985 2145.05 2145.20 25.22 2119.83 41.5 31.0 - 41.5 2114.2 - 2103.7 IIIo BR 30.0 2115.2 MW-24 Off -Site 2225.37 2225.49 56.36 2169.01 110.0 70.0 - 80.0 2155.5 - 2145.5 II PWR 42.0 2183.5 MW-25 Off -Site 2207.91 2208.04 NP-D NP-D 106.0 96.0 - 106.0 2112.0 - 2102.0 II PWR 104.0 2104.0 MW-26 Off -Site 35.581075 82.616078 2207.46 2207.62 27.76 2179.70 51.5 41.0 - 51.0 2166.6 - 2156.6 II PWR/BR 42.0 2165.6 RW-1 On -Site 2218.19 2218.61 50.51 2167.68 84.4 42.4 - 82.4 2176.2 - 2136.2 II BR/PWR 72.4 2146.2 RW-2 On -Site 35.579993 82.613123 2182.46 2183.62 NP-A NP-A 78.0 35.0 - 75.0 2148.6 - 2108.6 II BR 31.0 2152.6 RW-3 On -Site 2217.58 2218.06 44.42 2173.16 76.0 54.0 - 64.0 2164.1 - 2154.1 II BR 36.0 2182.1 RW-4 On -Site 2160.78 2161.74 NP-A NP-A 60.0 19.6 - 59.6 2142.1 - 2102.1 II BR 20.0 2141.7 RW-5 On -Site 2159.48 2160.60 13.22 2146.26 66.0 20.2 - 60.2 2140.4 - 2100.4 II BR 16.0 2144.6 RW-6 On -Site 2160.44 2161.57 15.31 2145.13 67.0 20.0 - 60.0 2141.6 - 2101.6 II SAP/BR 36.0 2125.6 RW-7 On -Site 2164.57 2165.60 22.21 2142.36 67.0 13.0 - 53.0 2152.6 - 2112.6 II SAP/PWR 55.0 2110.6 Notes: *Values rounded to the nearest 0.1-ft. NM = Not measured NP-A = Not Present - Abandoned NP-D = Not Present - Destroyed by Grading bgs = below ground surface. bmp = below measuring point. Table 1 (2013) of 1022-36 Andrex 2013 Annual Tables 1 to 3.xlsx Water levels measured on 9/9/13. IIIo = Type III open bedrock well Measuring Point Elevation is top of casing. BR & PWR = Bedrock & Partially Weathered Rock MW-14 returned to artesian conditions as of 10/27/03. SAP = Saprolite 11= Type 11 well MW-24 was abandoned, redrilled and replaced in 2007 after the well head Ills = Type III screened well was damaged by Milkco contractors in 2003. The ground surface at RW-1 and MW-6 was raised 7.4 feet and the wells were extended. Both were resurveyed in November 2010. Prepared by: AWA Checked by: TJB Table 2 Laboratory Analytical Results of Groundwater & Surface Water Samples Selected Chlorinated VOCs Only Andrex Industries Asheville, North Carolina NCDENR Groundwater Incident Number 6586 BLE Project No. J13-1022-36 Ca .y V _ F^ O E- O U a� U I > o I o I I 1N L o U o 1F^ v ° N ar U r ID Q H w H W O FO NC 2L 0.7 3 70 1 0.03 1200 1 0.6 1 7 1 0.4 100 1 70 12,000. 0.6 50 6 0.2 NE Groundwater AB MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/12/2013 MW-5 5,250 305 0.89 69.8 ND ND 1.2 ND 5.2 505 ND ND 0.58 ND 1.4 6,139 9/13/2013 MW-6 1,260 228 ND 83.6 ND ND ND ND 6.1 709 ND ND ND 0.83 ND 2,288 9/11/2013 MW-7 152 ND 0.64 ND ND ND ND ND ND ND ND ND ND ND ND 153 AB MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-8A AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/11/2013 MW-9 1,260 90.4 ND 2.0 ND ND ND ND 1.5 352 ND ND 0.43 ND ND 1,706 9/12/2013 MW-10 157 17.7 ND 7.7 ND ND ND ND 0.76 56.0 ND ND 0.28 ND ND 239 9/12/2013 MW-11 1,050 65.7 ND 4.6 ND ND ND ND 1.6 203 ND ND 0.29 ND ND 1,325 9/12/2013 MW-12 3.9 ND ND 1.9 ND ND ND ND 8.3 13.3 ND ND ND ND ND 27 9/11/2013 MW-13 1,030 245 ND ND ND ND 0.91 ND 3.5 159 0.24 ND ND ND ND 1,439 9/11/2013 MW-14 774 322 ND ND ND ND 1.6 ND ND 167 ND ND ND ND ND 1,265 9/11/2013 MW-15 94.3 2.2 0.68 ND ND ND ND ND ND 3.9 0.63 ND ND ND ND 102 9/11/2013 MW-16 145 2.8 1.0 ND ND ND ND ND ND 5.7 0.96 ND ND ND ND 155 9/10/2013 MW-17 27.7 3.8 ND 1.8 ND ND ND ND ND 6.0 ND ND ND ND ND 39 9/10/2013 MW-18 ND ND 1.7 ND ND ND ND ND ND ND ND ND ND ND ND 1.7 NP** MW-19 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 9/10/2013 MW-20 ND ND 0.79 ND ND ND ND ND ND ND ND ND ND ND ND 0.79 9/10/2013 MW-21 ND ND 2.3 ND ND ND ND ND ND ND ND ND ND ND ND 2.3 9/10/2013 MW-22 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/11/2013 MW-23 39.0 1.5 ND ND ND ND ND ND ND 2.6 ND ND ND ND ND 43 9/10/2013 MW-24 406 2.9 0.65 ND ND ND ND ND ND 8.1 ND ND ND ND ND 418 NP** MW-25 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 9/10/2013 MW-26 ND ND 1.5 ND ND ND ND ND ND ND ND ND ND ND ND 1.5 9/13/2013 RW-1 22.5 58.4 0.73 14.8 ND ND 1.9 ND 6.3 1,740 ND ND ND ND ND 1,845 AB RW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/13/2013 RW-3 ND ND ND 1.2 ND ND ND 0.22 6.3 6.1 ND ND 0.40 ND ND 14 AB RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/13/2013 RW-5 34.6 ND ND ND ND ND ND ND ND 68.0 ND ND ND ND ND 103 9/13/2013 RW-6 27.8 20.1 ND 96 ND ND 3.2 ND 4.3 501 ND ND ND ND ND 652 9/13/2013 RW-7 57.3 17.8 ND 14.7 ND ND 1.2 ND ND 401 ND ND ND ND I ND 492 NC 2B 0.7 2.5 NE 0.025 NE NE NE NE NE I NE I NE I NE 1488 1488 1 NE I NE Surface Water 9/13/2013 Smith Mill Creek 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/13/2013 Smith Mill Creek 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/13/2013 Smith Mill Creek 3 0.53 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.53 9/13/2013 Smith Mill Creek 4 1.2 ND ND ND ND ND ND ND ND 0.34 ND ND ND ND ND 1.5 9/13/2013 Smith Mill Creek 5 1.2 ND ND ND ND ND ND ND ND 0.26 ND ND ND ND ND 1.5 9/13/2013 Smith Mill Creek 6 0.81 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.81 9/13/2013 Bear Creek 1 44.9 5.0 0.46 ND ND ND ND ND ND 15.8 ND ND ND ND ND 66 9/13/2013 Bear Creek 2 28.0 3.5 0.86 ND ND ND ND ND ND 10.7 ND ND ND ND ND 43 9/13/2013 Bear Creek 3 4.9 0.87 1.1 ND ND ND ND ND ND 3.1 ND ND ND ND ND 10 9/13/2013 Bear Creek 4 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/13/2013 Bear Creek 5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/13/2013 Jehovah Witness 1 12.2 1.2 ND ND ND ND ND ND ND 2.5 ND ND ND ND ND 16 9/13/2013 Cecil's Spring 1 17.6 2.1 ND ND ND ND ND ND ND 4.2 ND ND ND ND ND 24 9/13/2013 Cecil's Spring 2 5.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.1 Notes: Analyses performed by EPA Method 8260 MSV Low Level. J-flagged (estimated) results are included on this table but are not identified (see the lab report). Units in µg/l or parts per billion (ppb) Detected concentrations of petroleum hydrocarbon VOCs are NOT shown in this table (not part of the Andrex groundwater incident). Detected concentrations of acetone, chloromethane, and methylene chloride are NOT shown in this table (probable laboratory contaminants). Detected concentrations of 2-Butanone (MEK), Toluene, and 2-Hexanone are NOT shown in this table (metabolic products of bioremedation). NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in µg/l dated April 1, 2013. NC2B = North Carolina Surface Water Standards [WS - Water Supply Classification] under Title 15A Subchapter 2B in µg/1 dated May 1, 2007. ND = not detected at concentrations exceeding the laboratory reporting limit. NS = not sampled. NP = not present; monitoring well was abandoned or destroyed. AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008. * Compounds intermittently detected in the past. ** These wells were destroyed by grading during 2003. Recovery well samples are grab samples collected via bailer. Prepared by: AWA Table 2 (2013) of 1022-36 Andrex 2013 Annual Tables 1 to 3.xlsx Checked by: PJVH Table 3 TOC Historical Data Summary - Groundwater & Surface Water Samples Andrex Industries Asheville, North Carolina NCDENR Groundwater Incident Number 6586 BLE Project No. J13-1022-36 O Cl) W 3 o N > N W N Oi N y O ri s d U d a O N N G N 7 N N d 8 O s U O N O ° N cq N N N T N N V N M 0 O s M U d >> "z M N p U M Fw In Groundwater MW-1 AB All All All AB All All AB AB AB AB All AB AB AB All MW-2 AB AB All All All AB All All All All All All All All All All MW-3 All All All All All All All All All AB AB All AB AB AB AB MW-4 All All All AB All All All All All AB AB All AB AB AB All MW-5 2.1 1.2 18.5 5.2 2.9 ND 34.9 18.0 3.5 4.1 21.4 E 41.5 10.0 14.6 5.1 MW-6 5.9 NS 10.6 15.6 17.8 21.9 22.5 33.1 6.4 5.7 4.6 E 7.6 5.6 32.3 8.8 MW-7 ND ND NS ND ND NS 1.2 NS NS NS NS 8.0 C NS NS NS 1.2 MW-8 All All All All All All All All All All All All AB AB AB AB MW-8A All All AB All All AB All AB AB All All AB AB AB AB AB MW-9 4.7 25.9 NS 4.9 4.0 NS 4.0 NS NS NS NS 9.9 C NS NS 4.7 31.2 MW-10 5.8 ND 369 333 311 178 49.3 98 151 240 60 27 C 23.1 77.1 10.2 12.1 MW-11 4.0 ND 3.6 4.1 3.6 4.4 3.7 4.1 4.3 NS NS E NS NS 3.4 3.5 MW-12 1.3 ND 231 355 329 1,150 613 320 53 19.4 13.5 E 1,140 668 300 39.1 MW-13 3.8 ND NS 1.9 2.1 NS 2.6 NS 1.4 NS NS ND NS NS 2.2 2.7 MW-14 2.2 ND NS 1.5 1.6 NS 1.6 NS 1.5 NS NS E NS NS 2.0 2.1 MW-15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-16 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-17 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-18 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-19 NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** MW-20 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-21 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-22 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-23 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS MW-24 NS NS NS NS NS NS NS NS ND NS NS NS NS NS 1.8 2.2 MW-25 NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** NP** MW-26 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS RW-1 6.4 ND 1 363 720 4,590 1 6,400 4,480 5,300 4,460 2,660 1,600 1,244 C I 2,210 1,270 738 333 RW-2 All All All All All All All All AB All AB AB AB AB AB AB RW-3 3.4 ND 1 320 1,400 138 1 1,970 3,960 1,190 779 296 143 93 C I 2,730 274 18.3 175 RW-4 All All All All All AB All All AB All AB AB AB AB AB AB RW-5 5.4 19.2 I 438 518 462 1 3,630 268 31.8 970 263 550 292 C I 1,170 1,070 1,350 1,540 RW-6 4.3 13.4 NS 4.2 4.5 NS 6.0 NS 5.6 6.2 6.5 E 6.6 5.7 7.9 476 RW-7 4.3 13.7 I 2,560 3,520 3,010 I 4,030 4,230 3,720 3,020 NS NS 4,814 C NS NS 4,120 1,490 Surface Water Smith Mill Creek 1 NS NS NS NS 2.2 NS NS NS NS NS NS 1.6 NS NS NS 1.6 Smith Mill Creek 2 NS NS NS NS 1.7 NS NS NS NS NS NS 2.0 NS NS NS 5.5 Smith Mill Creek 3 NS NS NS NS 1.7 NS NS NS NS NS NS 2.2 NS NS NS 1.6 Smith Mill Creek 4 NS NS NS NS 1.4 NS NS NS NS NS NS 2.5 NS NS NS 1.7 Smith Mill Creek 5 NS NS NS NS 1.6 NS NS NS NS NS NS 2.5 NS NS NS 1.6 Smith Mill Creek 6 NS NS NS NS 1.6 NS NS NS NS NS NS 1.1 NS NS NS 1.6 Bear Creek 1 NS NS NS NS 1.2 NS NS NS NS NS NS ND NS NS NS 3.2 Bear Creek 2 NS NS NS NS 1.5 NS NS NS NS NS NS 6.4 NS NS NS 1.8 Bear Creek 3 NS NS NS NS 1.6 NS NS NS NS NS NS 1.7 NS NS NS 1.7 Bear Creek 4 NS NS NS NS 1.6 NS NS NS NS NS NS 1.5 NS NS NS 2.0 Bear Creek 5 NS NS NS NS 1.8 NS NS NS NS NS NS 1.2 NS NS NS 2.0 Jehovah Witness 1 NS NS NS NS 8.7 NS NS NS NS NS NS 1.7 NS NS NS 2.1 Cecil's Spring 1 NS NS NS NS 3.2 NS NS NS NS NS NS 5.2 NS NS NS 1.9 Cecil's Spring 2 NS NS NSJ NS 1.6 NS NS NS NS NS NS 1.6 NS NS NS 2A Notes: Analyses performed by SM 5310B. J-flagged (estimated) results if any are included on this table but are not identified (seethe lab report). Units in mg/l or parts per million (ppm) I = milk solution injected into this well. E - laboratory error due to contaminated containers, no data available. C = data has been corrected from a labortary error, result is an estimate only. ND - not detected at concentrations exceeding the laboratory reporting limit. NS = not sampled. Not on sampling matrix or sampling personnel oversight. NP - not present; monitoring well was abandoned or destroyed. AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008. ** These wells were destroyed by grading during 2003. Recovery well samples are grab samples collected via bailer. Prepared by: AWA Table 3 TOC of 1022-36 Andrex 2013 Annual Tables 1 to 3.xlsx Checked by: TJB FIGURES - al 0 0 0 �o a) o ,�K �y'` O N ti N CECIL'S OLLEGE 21114.436 � �'• ) W-15 ��` �'• �� 2114.58 � l s'� MW-18 RESIDENTIAL�� 2093.81 i �� RESIDENTIAL N / �� / TWENTIETH STREET RESIDENTIAL BEAR CREEK ROAD RESIDENTIAL �HAMILTON1 PROPERTY 1<0 McpADE STREET �M�=� �•• MALVERN HILLS I POOL-� �� � = ��.����^4-'_-•� ® PARK r TENNIS I COURTS I iw PLACE RESIDENTIAL RESIDENTIAL REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. REVISIONS No. DESCRIPTION BY O (1) O N DRAWN: ACE CHECKED: AWA APPROVED: BLNA ® ENS RESIDENTIAL RESIDENTI coo o N N � N o; MW-26 1 1 0 2179.70 O i cv z�8 : ,�20 RES'-x T ENTIAL m / III// // -.000 PERFEC MW-24 r MILKCO, INC. 2169.01 MW-1 MW-12 NP-A I2172.42 - RW-3 i 2173.16 MW-5� MW-25 2173.02 NP-D MW-6 2167.63 RW-1 216768 �iTI M l: HAINES ��M 9 .2$ I N MILK 0, INC. MW-3 I NP-A \• o TRW-2 II MW-8A* - NP-A NP-A RE INDUST IES, INC MW-4* NP-A MW-9 2153.46 II MW-8* GEAR, INC. RW-4 NP-A NP-A II RW-5 MW-10 II 2146.26 2145.29 RW-6 MW-11 \\ 2145.13 2142.32 ICE®�� VICE \\� STORE, - ** OTM O cm N vm N �:i�yll»illr_im DATE: 05-28-14 CAD FILE: ANDREX36-WTMO90913 JOB NO: J13-1022-36 M 4 SILVERS 2138 - RW-7 2142.36 w ---- PROPERTY MW-13 2138.05 W i ECHOLS PROPERTY NG \PROPERTY\ .Y M JUSTICE \ ' /i PROPERTY RESIDEN�IA� N �O MW-20 2149.17 n 4i ' RESIDENTIAL F L— J ROY D. ARMER PAR ••\ L---J W-23 I - - 2119.83 MW-21 I 2089.88 RASH RO \ I I ' •'�� _ _ MW-22 \\ I I •\ \ 2090.21 IMW-17 12091.11 ORMLx � NpRFpL� I�►• K SOU HOVA NESS� BIESTE F DL �s�o P PERTY • , PROPERTY .m RESIDENTIAL pqp RMER M 19 W ER WELL NP-D i RYDERMA OPERTY SATTERFIELD \ \ Rl OPERTY OUSE v -'-_,, 1p ffO O O � RESIDENTIAL (:0 O W NOTES: 1. THE GROUNDWATER PUMP AND TREAT SYSTEMS HAD BEEN REMOVED AND WERE NOT IN OPERATION AT THE TIME WATER LEVEL MEASUREMENTS WERE TAKEN. GROUNDWATER WAS NOT BEING PUMPED FROM RW-1 THROUGH RW-7 WHILE MEASUREMENTS WERE COLLECTED. 2. ** SKY LANES BOWLING CENTER NCDEH - PUBLIC WATER SYSTEM ID #10-11-025 WELL NAME: WELL #1 AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED "...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER." 1111UNNELL"II1100 MONEERNO, NC. NIL 6004 PONDERS COURT INC.TH CAROLINA 2961E PHONE: (864)288 i125 FAX: (864)28854430 N 1475 cr :op t�'FpL0a�5rP�a`; 2090 2080 Nk LEGEND APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR SHALLOW BEDROCK) GROUNDWATER MONITORING WELL ••� O APPROXIMATE LOCATION OF EXISTING (TYPE III -BEDROCK) ••� GROUNDWATER MONITORING WELL O RECOVERY WELL O WATER SUPPLY WELL BELOW GROUND STREAM SHOWING FLOW DIRECTION a • - • • �— ABOVE GROUND STREAM SHOWING FLOW DIRECTION - - PROPERTY LINE 2090.21 WATER LEVEL IN FEET ABOVE MEAN SEA LEVEL * GROUNDWATER ELEVATION IN WELL MW-14 IS TYPICALLY ARTESIAN AND REPRESENTS THE POTENTIOMETRIC SURFACE OF THE DEEPER ROCK AQUIFER AND WAS NOT CONSIDERED FOR CONTOURING PURPOSES. NP-A NOT PRESENT. WELL HAS BEEN ABANDONED. NP-D MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. MW-25 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY MILKO, INC. APPROXIMATE DIRECTION OF GROUNDWATER FLOW �MM APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE 2120 EQUIPOTENTIAL CONTOUR LINE 200 100 0 200 400 APPROXIMATE SCALE IN FEET GROUNDWATER ELEVATION CONTOUR MAP - SEPTEMBER 9, 2013 ANDREX INDUSTRIES DEAVERVIEW ROAD ASHEVILLE, NORTH CAROLINA FIGURE NO. 2 RESIDENTIAL )zz ".m ROAD �� ��� N C5.1 2 FO ER CECIL'S LEGE RESIDENTIAL _ � CS-1 10 ♦ �� , MW-16� MW-15 24 155 102 s0 MW-18 1.7 r00 a'^ ` MILKCO, INC. RESIDENTIAL o i TWEN r TH STREET r 00 o MW 418 \ m RW-3 14 RESIDENTIAL a RESIDENTIAL z � � _ _ OP � STREE — � Mc1 F_ P IC SERVIC CO. NC s RESIDE O � f0 \, 13LUUMINV "'y / _BC-2 RESIDENTI \ 43 i • .0. \ NOI 0000 0000 MALVERN HILLS P i BC-3 -� / 10 _ J BC-4 ND .._v__..� �• I TENNIS II _ND _ /•' I COURTS __3 *sawn MONO womm /•• � � RUMBOUGH PLACE /•• moonawasm 00,• Lu •• F�. Lu w RESIDENTIAL BC-5 /•' �000 V) z ND �•' Q o c co r ss iN-2 AB '6,139NP -, 1,845 MILKCO !a Fr I ` . PERFEAION GEAR, INC. MW-1 AB, MW-7 \ 153 MW-8A AB s0 MW-9 - - O RW-4 11786 AB ANDREX �� INDUSTRIES, INC.79 3 103 MW-10 239 MW-11 0 \ l 1,325 0 MW-26 1.5 (CHLOROFORM ONLY) HAYNES CORP. HAYNES CO �O 'jO s � o �® I � SM-1 ND L -- J RESIDENTIAL r---- i0 - o�� MW 917 I MW-23 - I 43 r - I v \ROY . FARMER BARK I SM-3 RASH F / •�''� •` rR�NCETp / LEGEND N ORI VE NOTES: RESIDENTIAL 1. LABORATORY ANALYSIS BY EPA METHOD 8260. APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR SHALLOW z 2. WELLS AND SURFACE WATER WAS SAMPLED ON SEPTEMBER 10-13, 2013. BEDROCK) GROUNDWATER MONITORING WELL J z 3. CONCENTRATIONS DETECTED IN MW-21 ARE PRIMARILY CHLOROFORM, APPROXIMATE LOCATION OF EXISTING TYPE III -BEDROCK PROBABLY RELATED TO LEAKING WATER SUPPLY LINES IN CLOSE 0 GROUNDWATER MONITORING WELL ( ) PROXIMITY TO THE WELLS. 4. SAMPLES FROM STREAMS DESIGNATED AS FOLLOWS: 0 RECOVERY WELL SM = SMITH MILL CREEK TRIBUTARY CS = CECIL'S SPRING APPROXIMATE LOCATION OF SURFACE WATER SAMPLES (SEE NOTE 4) BC = BEAR CREEK JW = FORMER JEHOVAH WITNESS PROPERTY (WATER SAMPLES COLLECTED 9-13-13). 5. NP = NOT PRESENT, WELL WAS NOT PRESENT AT TIME OF SAMPLING. 0 WATER SUPPLY WELL 6. ** SKY LANES BOWLING CENTER NCDEH - PUBLIC WATER SYSTEM ID #10-11-025 CONCENTRATION OF TOTAL DETECTED CHLORINATED VOLATILE ORGANIC WELL NAME: WELL #1 ++` � 162 COMPOUNDS IN PARTS PER BILLION (ppb). .'+ N CAR '�� AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED "...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER." BELOW GROUND STREAM SHOWING FLOW DIRECTION S _ 7. * THE WELLS MAY INTERCEPT FRACTURE SETS OR MAY BE SCREENED AT 1475 ELEVATIONS AT WHICH GROUNDWATER CONTAMINANT CONCENTRATIONS ARE-•• �— ABOVE GROUND STREAM SHOWING FLOW DIRECTION INCONSISTENT WITH THE ESTABLISHED PLUME. THE VALUES WERE IGNORED FOR Z CONTOURING PURPOSES. FOLOa�•• �`�•` - - PROPERTY LINE P,.� 8. THE FORMER WATER SUPPLY WELL ON THE CRYDERMAN PROPERTY APPEARED '�i,�r„W.T�#►��,+�' TO BE ABANDONED AND COULD NOT BE SAMPLED AS OF OCTOBER 2005. — APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE 9. MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. MW-25 WAS 100 TOTAL CHLORINATED CONCENTRATION CONTOUR IN PARTS PER BILLION NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY MILKO, INC. — —ND ESTIMATED LIMIT OF VOC'S 200 100 0 200 400 10. RECOVERY WELLS WERE NOT OPERATIONAL AT THE TIME OF SAMPLING. REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL &ASSOCIATES, EBENSBURG, PENNSYLVANIA VERY LOW CONCENTRATION AS THE RESULT OF GROUNDWATER FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. 11. AB = WELL ABANDONED IN 2008 PER APPROVED BROWNFIELD REDEVELOPMENT PLAN. REMEDIATION. IGNORED FOR CONTOURING PURPOSES. APPROXIMATE SCALE IN FEET REVISIONS No. DESCRIPTION BY DRAWN: ACE CHECKED: AWA APPROVED: DATE: 05-28-14 CAD FILE: ANDREX36-VOCSEPT13 JOB NO: J13-1022-36 MW-13 s520000 1,439 '000 SILVERS 5O0 BOWLING PROPERTY MW_14* '10O ' ALLEY 1 265 ` `.PROPER JUSTICE PROPERTY PROPERTY RESIDENTIAL MW-20 0.29 GR (CHLOROFORM ONLY) RESIDENTIAL / I I I 0.53 MW-21 \ I , 2.3 (CHLOROFORM ONLY) RW-7 492 M N022 JW-1•• •\ 16 ,' FORMER JEHOVA43 WITNESS PROPERTY ♦ `BIESTERFEDLT SEXTON 9 NORFp4k sou - \PERTY PROPERTY NP pTy 10 i � q��ROAO SM-5 L_ � - 0 FORMER 1.5 `.. SATTERFIELD - WATER WELL - CRYDERMAN SI PROPERTY —HOUSE ----PROPERTY a---ND—=-�- W RESIDENTIAL O Q 5 I VENHOE AVFnu PgTTp� AIiENpE / / RESIDENTIAL I a�. BUNNELL"MMON8 MONUM8, NC. 6004 PONDERS COURT INC. GREENVILLE, SOUTH CAROLINA 29615 PHONE: (864)288-1265 FAX: (864)288-4430 CONTOUR MAP OF TOTAL CHLORINATED VOLATILE ORGANIC COMPOUND ISOCONCENTRATIONS - SEPTEMBER 10-13, 2013 GROUNDWATER AND SURFACE WATER ANDREX INDUSTRIES ASHEVILLE, NORTH CAROLINA FIGURE NO. 3 APPENDICES APPENDIX A WELL SAMPLING LOGS BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 I Personnel: Name: Job #: I ID #: Conditions: Air Temperature: Total Well Depth in feet (TWD) Depth to Ground Water in feet (I: Length of Water Column (LWC) 1 Casing Volume in gallons (CV Standard Evacuation Volume (3 i Method of Well Evacuation: Method of Sample Collection: Total Volume of Water Removed Sep. 12, 2013 BPN Andrex J13-1022-36 MW-5 Clear 78OF = 53.00 )GW) = 43.73 = TWD - DGW = 9.27 i=LWCx0.17= 1.58 rasing volumes) = 4.73 Disp Bailer Disp Bailer (eallons): 6 eallons Casing Diameter: Casing Material: Measuring Point Elevation (ft Height of Riser (ft above land Land Surface Elevation (ft m, Screened Interval (ft bgs): Dedicated Pump or Bailer: Steel Guard Pine Around Cas Protective Post/Abutment: Well Integrity Satisfactory Well Yield (subjective): Samnle Date and Time: Remarks: TOCs + VOCs FIELD ANALYSIS 2 inches PVC 2216.75 flushmount 2216.92 43.0-53.0 no no low 9/12/2013 Cud 1045 Volume Purged (gallons) initial 2.0 4.0 6.0 Time (military) 1025 1030 1035 1040 pH (S.U.) 6.20 6.01 6.00 5.99 Sp. Cond. (umhos/cm) 90.9 75.3 75.6 75.8 Water Temp. (°C) 1 19.4 1 19.4 1 18 1 17.6 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.20 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 13, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2218.43 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-6 Land Surface Elevation (ft msl): 2218.67 Downgradient: yes Screened Interval (ft bgs): 50.4-70.4 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Partly Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 720F Locking Cap: yes Total Well Depth in feet (TWD) = 71.90 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 50.80 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 21.10 Well Yield (subjective): low 1 Casing Volume in gallons (CV) = LWC x 0.17 = 3.59 Sample Date and Time: 9/13/13 @ 1015 Standard Evacuation Volume (3 casing volumes) = 10.76 Remarks: Dry @ 1.5 gallons Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): 1.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1005 pH (S.U.) 5.32 Sp. Cond. (umhos/cm) 150.1 Water Temp. (°C) 18.7 Turbidity (subjective)* 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.62 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 I Personnel: Name: Job #: I ID #: Conditions: Air Temperature: Total Well Depth in feet (TWD) Depth to Ground Water in feet (I: Length of Water Column (LWC) 1 Casing Volume in gallons (CV Standard Evacuation Volume (3 i Method of Well Evacuation: Method of Sample Collection: Total Volume of Water Removed Sep. 11, 2013 BPN/TWL Andrex J13-1022-36 MW-7 Clear 790F = 35.00 )GW) = 26.12 = TWD - DGW = 8.88 i=LWCx0.17= 1.51 rasing volumes) = 4.53 Disp Bailer Disp Bailer (gallons): 4.5 gallons Casing Diameter: Casing Material: Measuring Point Elevation (ft Height of Riser (ft above land Land Surface Elevation (ft m, Screened Interval (ft bgs): Dedicated Pump or Bailer: Steel Guard Pine Around Cas Protective Post/Abutment: Well Integrity Satisfactory Well Yield (subjective): Samnle Date and Time: Remarks: TOCs + VOCs FIELD ANALYSIS 2 inches PVC 2218.35 flushmount 2218.60 24.5-34.5 no no low 9/11/2013 (a, 1120 Volume Purged (gallons) initial 1.5 3.0 4.5 Time (military) 1105 1107 1110 1115 pH (S.U.) 5.75 5.59 5.52 5.38 Sp. Cond. (umhos/cm) 56.5 46.2 44.7 43.8 Water Temp. (°C) 1 17.8 1 17.2 1 16.7 1 17.0 Turbidity (subjective)* 1 2 2 2 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.92 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 11, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2175.57 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-9 Land Surface Elevation (ft msl): 2175.95 Downgradient: yes Screened Interval (ft bgs): 44.0-54.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 820F Locking Cap: yes Total Well Depth in feet (TWD) = 54.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 22.11 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 32.09 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 5.46 Sample Date and Time: 9/11/2013 @ 1300 Standard Evacuation Volume (3 casing volumes) = 16.4 Remarks: TOC's + VOC's Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 16.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 5.5 11.0 16.5 Time (military) 1225 1233 1244 1255 pH (S.U.) 5.75 5.34 5.34 5.26 Sp. Cond. (umhos/cm) 83.4 98.5 100.3 101.6 Water Temp. (°C) 16.2 15.8 15.8 15.6 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.10 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 I Personnel: Name: Job #: I ID #: Conditions: Air Temperature: Total Well Depth in feet (TWD) Depth to Ground Water in feet (I: Length of Water Column (LWC) 1 Casing Volume in gallons (CV Standard Evacuation Volume (3 i Method of Well Evacuation: Method of Sample Collection: Total Volume of Water Removed Sep. 12, 2013 BPN/TWL Andrex J13-1022-36 MW-10 Clear 820F = 39.00 )GW) = 14.63 = TWD - DGW = 24.37 i=LWCx0.17= 4.14 rasing volumes) = 12.43 Disp Bailer Disp Bailer (eallons): 12.3 eallon� Casing Diameter: 2 inches Casing Material: PVC Measuring Point Elevation (ft msl): 2159.92 Height of Riser (ft above land surface): flushmount Land Surface Elevation (ft msl): 2159.45 Screened Interval (ft bgs): 29.0-39.0 Dedicated Pump or Bailer: no Steel Guard Pine Around Casine: no Protective Post/Abutment: no Well Integrity Satisfactory: ye: Well Yield (subjective): hil Samnle Date and Time: 9/12/2013 Cud 1245 Remarks: TOCs + VOCs FIELD ANALYSIS Volume Purged (gallons) initial 4.0 8.0 12.0 Time (military) 1220 1225 1232 1240 pH (S.U.) 5.78 6.01 6.05 6.18 Sp. Cond. (umhos/cm) 118.0 177.0 202.0 186.4 Water Temp. (°C) 1 18.0 1 15.9 1 16.4 1 16.1 Turbidity (subjective)* 1 2 2 2 2 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.54 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 12, 2013 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2166.00 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-11 Land Surface Elevation (ft msl): 2166.39 Downgradient: yes Screened Interval (ft bgs): 48.0-58.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy/Clear Steel Guard Pipe Around Casing: no Air Temperature: 840F Locking Cap: yes Total Well Depth in feet (TWD) = 58.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 23.68 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 34.82 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 5.92 Sample Date and Time: 9/12/2013 @ 1505 Standard Evacuation Volume (3 casing volumes) = 17.76 Remarks: TOCs + VOCs Method of Well Evacuation: Disp.Bailer Method of Sample Collection: Disp.Bailer Total Volume of Water Removed (gallons): 18 gallons Volume Purged (gallons) initial FIELD ANALYSIS 6.0 12.0 18.0 Time (military) 1330 1340 1350 1455 pH (S.U.) 5.90 5.60 5.54 5.45 Sp. Cond. (umhos/cm) 77.2 77.0 81.8 77.9 Water Temp. (°C) 17.2 16.6 16.5 17.1 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 6.25 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 12, 2013 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2219.17 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-12 Land Surface Elevation (ft msl): 2219.49 Downgradient: yes Screened Interval (ft bgs): 60.0-70.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 720F Locking Cap: yes Total Well Depth in feet (TWD) = 81.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 46.75 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 34.25 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 5.82 Sample Date and Time: 9/12/2013 @ 1000 Standard Evacuation Volume (3 casing volumes) = 17.47 Remarks: TOCs + VOCs Method of Well Evacuation: Disp Bailer Method of Sample Collection: Disp Bailer Total Volume of Water Removed (gallons): 18 gallons Volume Purged (gallons) initial FIELD ANALYSIS 6.0 12.0 18.0 Time (military) 905 920 935 950 pH (S.U.) 6.37 6.43 6.32 6.30 Sp. Cond. (umhos/cm) 464 365 335 314 Water Temp. (°C) 17.5 17.5 17.6 17.8 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 0.75 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 11, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2138.80 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-13 Land Surface Elevation (ft msl): 2138.96 Downgradient: yes Screened Interval (ft bgs): 48.0-58.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 850F Locking Cap: yes Total Well Depth in feet (TWD) = 58.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 0.75 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 57.75 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 9.82 Sample Date and Time: 9/11/2013 @ 1415 Standard Evacuation Volume (3 casing volumes) = 29.45 Remarks: TOCs + VOCs Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 30 gallons Volume Purged (gallons) initial FIELD ANALYSIS 10.0 20.0 30.0 Time (military) 1330 1345 1400 1412 pH (S.U.) 6.21 6.42 6.54 6.49 Sp. Cond. (umhos/cm) 109.2 113 108 112.2 Water Temp. (°C) 24.2 19.4 19.3 18.8 Turbidity (subjective)* 1 2 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 2.28 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 11, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2138.94 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-14 Land Surface Elevation (ft msl): 2139.2 Downgradient: yes Screened Interval (ft bgs): 65.0-75.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 860F Locking Cap: yes Total Well Depth in feet (TWD) = 75.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 0.00 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 75.00 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 12.75 Sample Date and Time: 9/11/2013 @ 1530 Standard Evacuation Volume (3 casing volumes) = 38.25 Remarks: TOC's + VOC's Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 38.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 12.75 25.5 38.25 Time (military) 1425 1440 1500 1520 pH (S.U.) 6.50 6.74 6.58 6.63 Sp. Cond. (umhos/cm) 108.7 112 111.4 109.5 Water Temp. (°C) 19.1 18.2 18.2 18.2 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 0.77 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 11, 2013 Casing Diameter: 6 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2124.89 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-15 Land Surface Elevation (ft msl): 2125.18 Downgradient: yes Screened Interval (ft bgs): 33.3-40.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) = 40.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 10.31 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 29.69 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 1.5 = 44.54 Sample Date and Time: 9/11/2013 @ 1045 Standard Evacuation Volume (3 casing volumes) = 133.61 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 135 gallons Volume Purged (gallons) initial FIELD ANALYSIS 45 90 135 Time (military) 1025 1030 1035 1040 pH (S.U.) 5.80 5.98 5.75 5.68 Sp. Cond. (umhos/cm) 50.1 50.1 48.6 49.9 Water Temp. (°C) 16.5 16.3 15.9 16.3 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.91 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 11, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2124.59 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-16 Land Surface Elevation (ft msl): 2124.85 Downgradient: yes Screened Interval (ft bgs): 23.5-33.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) = 33.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 10.16 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 23.34 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 3.97 Sample Date and Time: 9/11/2013 @ 1020 Standard Evacuation Volume (3 casing volumes) = 11.90 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 12 gallons Volume Purged (gallons) initial FIELD ANALYSIS 4.00 8.0 12.00 Time (military) 955 1000 1006 1012 pH (S.U.) 5.69 5.67 5.79 5.67 Sp. Cond. (umhos/cm) 57.5 53.7 52.7 53.1 Water Temp. (°C) 19.3 16.7 16.5 16.6 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.30 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 10, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2094.64 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-17 Land Surface Elevation (ft msl): 2094.74 Downgradient: yes Screened Interval (ft bgs): 4.0-14.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) = 14.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 3.53 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 10.67 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 1.81 Sample Date and Time: 9/10/2013 @ 1150 Standard Evacuation Volume (3 casing volumes) = 5.44 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 6.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 2.0 4.0 6.0 Time (military) 1128 1132 1135 1143 pH (S.U.) 5.65 5.67 5.72 5.64 Sp. Cond. (umhos/cm) 182.8 262 209 206 Water Temp. (°C) 24.3 22.5 21.5 21.7 Turbidity (subjective)* 2 2 2 2 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.64 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 10, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2101.81 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-18 Land Surface Elevation (ft msl): 2101.92 Downgradient: yes Screened Interval (ft bgs): 49.0-59.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 830F Locking Cap: yes Total Well Depth in feet (TWD) = 59.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 8.00 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 51.00 Well Yield (subjective): low 1 Casing Volume in gallons (CV) = LWC x 0.17 = 8.67 Sample Date and Time: 9/10/2013 @ 1430 Standard Evacuation Volume (3 casing volumes) = 26.01 Remarks: Dry @ 15 gallons Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 15 gallons Volume Purged (gallons) initial FIELD ANALYSIS 9.0 Time (military) 1345 1400 pH (S.U.) 5.94 6.29 Sp. Cond. (umhos/cm) 97.3 85.7 Water Temp. (°C) 20.3 16.3 Turbidity (subjective)* 2 2 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 3.90 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 10, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2180.55 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-20 Land Surface Elevation (ft msl): 2180.54 Downgradient: yes Screened Interval (ft bgs): 67.0-77.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 81OF Locking Cap: yes Total Well Depth in feet (TWD) = 77.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 31.38 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 45.62 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 7.76 Sample Date and Time: 9/10/2013 @ 1330 Standard Evacuation Volume (3 casing volumes) = 23.27 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 24 gallons Volume Purged (gallons) initial FIELD ANALYSIS 8.0 16.0 24.0 Time (military) 1222 1241 1303 1320 pH (S.U.) 5.95 6.12 5.96 6.00 Sp. Cond. (umhos/cm) 19.3 20.4 19.7 21.3 Water Temp. (°C) 18.3 17.6 18.3 18.4 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 7.30 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 10, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2091.17 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-21 Land Surface Elevation (ft msl): 2091.31 Downgradient: yes Screened Interval (ft bgs): 26.5-36.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) = 36.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 1.29 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 35.21 Well Yield (subjective): low 1 Casing Volume in gallons (CV) = LWC x 0.17 = 5.99 Sample Date and Time: 9/10/2013 @ 1005 Standard Evacuation Volume (3 casing volumes) = 17.96 Remarks: Dry @ 13 gallons Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 13 gallons Volume Purged (gallons) initial FIELD ANALYSIS 6.0 12.0 Time (military) 945 952 1002 pH (S.U.) 6.17 5.51 5.56 Sp. Cond. (umhos/cm) 78.9 84.8 85.0 Water Temp. (°C) 21.8 16.8 16.1 Turbidity (subjective)* 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 3.90 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 10, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2090.71 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-22 Land Surface Elevation (ft msl): 2090.84 Downgradient: yes Screened Interval (ft bgs): 47.0-57.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) = 57.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 0.50 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 56.50 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 9.61 Sample Date and Time: 9/10/2013 @ 1120 Standard Evacuation Volume (3 casing volumes) = 28.82 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 29.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 9.6 19.2 28.8 Time (military) 1015 1030 1050 1115 pH (S.U.) 6.1 6.28 6.02 6.12 Sp. Cond. (umhos/cm) 119.3 117.8 110.5 116.5 Water Temp. (°C) 21.1 16.2 16.3 16.9 Turbidity (subjective)* 2 2 2 2 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 2.56 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 11, 2013 Casing Diameter: 6 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2145.05 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-23 Land Surface Elevation (ft msl): 2145.20 Downgradient: yes Screened Interval (ft bgs): 31.0-41.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 720F Locking Cap: yes Total Well Depth in feet (TWD) = 41.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 25.22 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 16.28 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 1.5 = 24.42 Sample Date and Time: 9/11/2013 @ 940 Standard Evacuation Volume (3 casing volumes) = 73.26 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 75 gallons Volume Purged (gallons) initial FIELD ANALYSIS 25.0 50.0 75.0 Time (military) 923 925 928 931 pH (S.U.) 6.05 5.75 5.61 5.45 Sp. Cond. (umhos/cm) 176.0 198.1 197.0 207 Water Temp. (°C) 16.6 16.0 15.9 16.1 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 6.72 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 10, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2225.37 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-24 Land Surface Elevation (ft msl): 2225.49 Downgradient: yes Screened Interval (ft bgs): 70.0-80.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 840F Locking Cap: yes Total Well Depth in feet (TWD) = 80.10 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 56.36 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 23.74 Well Yield (subjective): low 1 Casing Volume in gallons (CV) = LWC x 0.17 = 4.04 Sample Date and Time: 9/10/2013 @ 1520 Standard Evacuation Volume (3 casing volumes) = 12.11 Remarks: TOC's + VOC's Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 12 gallons Volume Purged (gallons) initial FIELD ANALYSIS 4.0 8.0 12.0 Time (military) 1445 1455 1505 1517 pH (S.U.) 5.71 5.67 5.42 5.68 Sp. Cond. (umhos/cm) 95.6 118.8 115.0 115.0 Water Temp. (°C) 18.2 18.0 17.1 16.6 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 3.95 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 10, 2013 Casing Diameter: 2 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2207.46 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: MW-26 Land Surface Elevation (ft msl): 2207.62 Downgradient: yes Screened Interval (ft bgs): 41.0 - 51.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Clear Steel Guard Pipe Around Casing: no Air Temperature: 740F Locking Cap: yes Total Well Depth in feet (TWD) = 51.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 27.76 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 23.24 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.17 = 3.95 Sample Date and Time: 9/10/2013 @ 930 Standard Evacuation Volume (3 casing volumes) = 11.85 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 12 gallons Volume Purged (gallons) initial FIELD ANALYSIS 4.0 8.0 12.0 Time (military) 902 909 918 926 pH (S.U.) 8.02 5.7 5.61 5.59 Sp. Cond. (umhos/cm) 187.0 178.9 197.2 197.0 Water Temp. (°C) 16.9 16.8 16.3 16.1 Turbidity (subjective)* 1 1 1 1 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 3.46 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 13, 2013 Casing Diameter: 6 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2209.87 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: RW-1 Land Surface Elevation (ft msl): 2211.22 Downgradient: yes Screened Interval (ft bgs): 35.0-75.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Partly Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 660F Locking Cap: no Total Well Depth in feet (TWD) = 82.40 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 50.51 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 31.89 Well Yield (subjective): moderate 1 Casing Volume in gallons (CV) = LWC x 1.5 = 47.84 Sample Date and Time: 9/13/2013 @ 950 Standard Evacuation Volume (3 casing volumes) = 143.51 Remarks: Grab sample @ 62' btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 952 pH (S.U.) 5.06 Sp. Cond. (umhos/cm) 232 Water Temp. (°C) 19.1 Turbidity (subjective)* 2 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.20 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 13, 2013 Casing Diameter: 4 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2217.58 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: RW-3 Land Surface Elevation (ft msl): 2218.06 Downgradient: yes Screened Interval (ft bgs): 54.0 - 64.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 660F Locking Cap: yes Total Well Depth in feet (TWD) = 64.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 44.42 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 19.58 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 0.66 = 12.92 Sample Date and Time: 9/13/2013 @ 930 Standard Evacuation Volume (3 casing volumes) = 38.77 Remarks: Grab sample @ 59' btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 935 pH (S.U.) 6.3 Sp. Cond. (umhos/cm) 680 Water Temp. (°C) 19.1 Turbidity (subjective)* 3 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.65 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 13, 2013 Casing Diameter: 6 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2159.48 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: RW-5 Land Surface Elevation (ft msl): 2160.60 Downgradient: yes Screened Interval (ft bgs): 20.2 - 60.2 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Partly Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 70OF Locking Cap: yes Total Well Depth in feet (TWD) = 60.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 13.22 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 46.98 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 1.5 = 70.47 Sample Date and Time: 9/13/2013 @ 1030 Standard Evacuation Volume (3 casing volumes) = 211.41 Remarks: Grab sample @ 40' btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1035 pH (S.U.) 5.7 Sp. Cond. (umhos/cm) 1055 Water Temp. (°C) 18.4 Turbidity (subjective)* 3 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 0.74 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 13, 2013 Casing Diameter: 6 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2160.44 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: RW-6 Land Surface Elevation (ft msl): 2161.57 Downgradient: yes Screened Interval (ft bgs): 20.0 - 60.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Partly Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 70OF Locking Cap: yes Total Well Depth in feet (TWD) = 60.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 15.31 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 44.69 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 1.5 = 67.04 Sample Date and Time: 9/13/2013 @ 1550 Standard Evacuation Volume (3 casing volumes) = 201.11 Remarks: Grab sample @ 40' btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA (VOC Duplicate) Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1555 pH (S.U.) 6.05 Sp. Cond. (umhos/cm) 342.0 Water Temp. (°C) 18.1 Turbidity (subjective)* 3 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 2.01 BUNNELL-LAMMONS ENGINEERING, INC. FIELD DATA INFORMATION LOG FOR GRO UND WATER SAMPLING Page 1 of 1 Date: Sep. 13, 2013 Casing Diameter: 6 inches Field Personnel: BPN/TWL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2164.57 BLE Job #: J13-1022-36 Height of Riser (ft above land surface): flushmount Well ID #: RW-7 Land Surface Elevation (ft msl): 2165.60 Downgradient: yes Screened Interval (ft bgs): 13.0 - 53.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Partly Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 70OF Locking Cap: yes Total Well Depth in feet (TWD) = 53.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) = 22.21 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 30.79 Well Yield (subjective): high 1 Casing Volume in gallons (CV) = LWC x 1.5 = 46.19 Sample Date and Time: 9/13/2013 @ 1120 Standard Evacuation Volume (3 casing volumes) = 138.56 Remarks: Grab sample @ 33' btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1125 pH (S.U.) 5.29 Sp. Cond. (umhos/cm) 580 Water Temp. (°C) 16.8 Turbidity (subjective)* 3 * (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.08 APPENDIX B LABORATORY ANALYTICAL DATA SHEETS (Provided on Enclosed CD) qD aceAnalytical —pacelabs.com September 27, 2013 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 Eden, NC 27288 (336)623-8921 RE: Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Dear Mr. Alexander: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 16, 2013. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton for Tom Williams tom.williams@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE SUMMARY Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Lab ID Sample ID Matrix Date Collected Date Received 92172207001 MW-5 Water 09/12/13 10:45 09/16/13 09:00 92172207002 MW-6 Water 09/13/13 10:15 09/16/13 09:00 92172207003 MW-7 Water 09/11/13 11:20 09/16/13 09:00 92172207004 MW-9 Water 09/11/13 13:00 09/16/13 09:00 92172207005 MW-10 Water 09/12/13 12:45 09/16/13 09:00 92172207006 MW-11 Water 09/12/13 15:05 09/16/13 09:00 92172207007 MW-12 Water 09/12/13 10:00 09/16/13 09:00 92172207008 MW-13 Water 09/11/13 14:15 09/16/13 09:00 92172207009 MW-14 Water 09/11/13 15:30 09/16/13 09:00 92172207010 MW-15 Water 09/11/13 10:45 09/16/13 09:00 92172207011 MW-16 Water 09/11/13 10:20 09/16/13 09:00 92172207012 MW-17 Water 09/10/13 11:50 09/16/13 09:00 92172207013 MW-18 Water 09/10/13 14:30 09/16/13 09:00 92172207014 MW-20 Water 09/10/13 13:30 09/16/13 09:00 92172207015 MW-21 Water 09/10/13 10:05 09/16/13 09:00 92172207016 MW-22 Water 09/10/13 11:20 09/16/13 09:00 92172207017 MW-23 Water 09/11/13 09:40 09/16/13 09:00 92172207018 MW-24 Water 09/10/13 15:20 09/16/13 09:00 92172207019 MW-26 Water 09/10/13 09:30 09/16/13 09:00 92172207020 RW-1 Water 09/13/13 09:50 09/16/13 09:00 92172207021 RW-3 Water 09/13/13 09:30 09/16/13 09:00 92172207022 RW-5 Water 09/13/13 10:30 09/16/13 09:00 92172207023 RW-6 Water 09/13/13 15:50 09/16/13 09:00 92172207024 RW-7 Water 09/13/13 11:20 09/16/13 09:00 92172207026 FIELD BLANK 9/11 Water 09/11/13 08:30 09/16/13 09:00 92172207028 FIELD BLANK 9/13 Water 09/13/13 08:30 09/16/13 09:00 92172207029 DUPLICATE Water 09/13/13 00:00 09/16/13 09:00 92172207030 TRIP BLANK Water 09/13/13 00:00 09/16/13 09:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE ANALYTE COUNT Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92172207001 MW-5 EPA 8260 MCK 63 PASI-C 92172207002 MW-6 EPA 8260 MCK 63 PASI-C 92172207003 MW-7 EPA 8260 MCK 63 PASI-C 92172207004 MW-9 EPA 8260 MCK 63 PASI-C 92172207005 MW-10 EPA 8260 MCK 63 PASI-C 92172207006 MW-11 EPA 8260 MCK 63 PASI-C 92172207007 MW-12 EPA 8260 MCK 63 PASI-C 92172207008 MW-13 EPA 8260 MCK 63 PASI-C 92172207009 MW-14 EPA 8260 MCK 63 PASI-C 92172207010 MW-15 EPA 8260 MCK 63 PASI-C 92172207011 MW-16 EPA 8260 MCK 63 PASI-C 92172207012 MW-17 EPA 8260 MCK 63 PASI-C 92172207013 MW-18 EPA 8260 MCK 63 PASI-C 92172207014 MW-20 EPA 8260 MCK 63 PASI-C 92172207015 MW-21 EPA 8260 MCK 63 PASI-C 92172207016 MW-22 EPA 8260 MCK 63 PASI-C 92172207017 MW-23 EPA 8260 MCK 63 PASI-C 92172207018 MW-24 EPA 8260 MCK 63 PASI-C 92172207019 MW-26 EPA 8260 MCK 63 PASI-C 92172207020 RW-1 EPA 8260 MCK 63 PASI-C 92172207021 RW-3 EPA 8260 MCK 63 PASI-C 92172207022 RW-5 EPA 8260 MCK 63 PASI-C 92172207023 RW-6 EPA 8260 MCK 63 PASI-C 92172207024 RW-7 EPA 8260 MCK 63 PASI-C 92172207026 FIELD BLANK 9/11 EPA 8260 MCK 63 PASI-C 92172207028 FIELD BLANK 9/13 EPA 8260 MCK 63 PASI-C 92172207029 DUPLICATE EPA 8260 MCK 63 PASI-C 92172207030 TRIP BLANK EPA 8260 MCK 63 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-5 Lab ID: 92172207001 Collected: 09/12/13 10:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 50.0 20.0 2 09/23/13 08:36 67-64-1 Benzene ND ug/L 2.0 0.50 2 09/23/13 08:36 71-43-2 Bromobenzene ND ug/L 2.0 0.60 2 09/23/13 08:36 108-86-1 Bromochloromethane ND ug/L 2.0 0.34 2 09/23/13 08:36 74-97-5 Bromodichloromethane ND ug/L 2.0 0.36 2 09/23/13 08:36 75-27-4 Bromoform ND ug/L 2.0 0.52 2 09/23/13 08:36 75-25-2 Bromomethane ND ug/L 4.0 0.58 2 09/23/13 08:36 74-83-9 2-Butanone (MEK) ND ug/L 10.0 1.9 2 09/23/13 08:36 78-93-3 Carbon tetrachloride ND ug/L 2.0 0.50 2 09/23/13 08:36 56-23-5 Chlorobenzene 0.58J ug/L 2.0 0.46 2 09/23/13 08:36 108-90-7 Chloroethane ND ug/L 2.0 1.1 2 09/23/13 08:36 75-00-3 Chloroform 0.89J ug/L 2.0 0.28 2 09/23/13 08:36 67-66-3 Chloromethane ND ug/L 2.0 0.22 2 09/23/13 08:36 74-87-3 2-Chlorotoluene ND ug/L 2.0 0.70 2 09/23/13 08:36 95-49-8 4-Chlorotoluene ND ug/L 2.0 0.62 2 09/23/13 08:36 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 10.0 5.0 2 09/23/13 08:36 96-12-8 Dibromochloromethane ND ug/L 2.0 0.42 2 09/23/13 08:36 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 2.0 0.54 2 09/23/13 08:36 106-93-4 Dibromomethane ND ug/L 2.0 0.42 2 09/23/13 08:36 74-95-3 1,2-Dichlorobenzene ND ug/L 2.0 0.60 2 09/23/13 08:36 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 0.48 2 09/23/13 08:36 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 0.66 2 09/23/13 08:36 106-46-7 Dichlorodifluoromethane ND ug/L 2.0 0.42 2 09/23/13 08:36 75-71-8 1,1-Dichloroethane ND ug/L 2.0 0.64 2 09/23/13 08:36 75-34-3 1,2-Dichloroethane ND ug/L 2.0 0.24 2 09/23/13 08:36 107-06-2 1,1-Dichloroethene 1.2J ug/L 2.0 1.1 2 09/23/13 08:36 75-35-4 cis-1,2-Dichloroethene 505 ug/L 20.0 3.8 20 09/23/13 01:57 156-59-2 trans-1,2-Dichloroethene 5.2 ug/L 2.0 0.98 2 09/23/13 08:36 156-60-5 1,2-Dichloropropane ND ug/L 2.0 0.54 2 09/23/13 08:36 78-87-5 1,3-Dichloropropane ND ug/L 2.0 0.56 2 09/23/13 08:36 142-28-9 2,2-Dichloropropane ND ug/L 2.0 0.26 2 09/23/13 08:36 594-20-7 1,1-Dichloropropene ND ug/L 2.0 0.98 2 09/23/13 08:36 563-58-6 cis-1,3-Dichloropropene ND ug/L 2.0 0.26 2 09/23/13 08:36 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 2.0 0.52 2 09/23/13 08:36 10061-02-6 Diisopropyl ether ND ug/L 2.0 0.24 2 09/23/13 08:36 108-20-3 Ethylbenzene ND ug/L 2.0 0.60 2 09/23/13 08:36 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.4 2 09/23/13 08:36 87-68-3 2-Hexanone ND ug/L 10.0 0.92 2 09/23/13 08:36 591-78-6 p-Isopropyltoluene ND ug/L 2.0 0.62 2 09/23/13 08:36 99-87-6 Methylene Chloride 10.6 ug/L 4.0 1.9 2 09/23/13 08:36 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 10.0 0.66 2 09/23/13 08:36 108-10-1 Methyl-tert-butyl ether ND ug/L 2.0 0.42 2 09/23/13 08:36 1634-04-4 Naphthalene ND ug/L 2.0 0.48 2 09/23/13 08:36 91-20-3 Styrene ND ug/L 2.0 0.52 2 09/23/13 08:36 100-42-5 1,1,1,2-Tetrachloroethane 1.4J ug/L 2.0 0.66 2 09/23/13 08:36 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 2.0 0.80 2 09/23/13 08:36 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5 Lab ID: 92172207001 Collected: 09/12/13 10:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 5250 ug/L 100 46.0 100 09/23/13 21:50 127-18-4 Toluene 4.0 ug/L 2.0 0.52 2 09/23/13 08:36 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.66 2 09/23/13 08:36 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.70 2 09/23/13 08:36 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.96 2 09/23/13 08:36 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.58 2 09/23/13 08:36 79-00-5 Trichloroethene 305 ug/L 2.0 0.94 2 09/23/13 08:36 79-01-6 Trichlorofluoromethane ND ug/L 2.0 0.40 2 09/23/13 08:36 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.82 2 09/23/13 08:36 96-18-4 Vinyl acetate ND ug/L 4.0 0.70 2 09/23/13 08:36 108-05-4 Vinyl chloride 69.8 ug/L 2.0 1.2 2 09/23/13 08:36 75-01-4 Xylene (Total) ND ug/L 4.0 1.3 2 09/23/13 08:36 1330-20-7 m&p-Xylene ND ug/L 4.0 1.3 2 09/23/13 08:36 179601-23-1 o-Xylene ND ug/L 2.0 0.46 2 09/23/13 08:36 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 2 09/23/13 08:36 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 2 09/23/13 08:36 17060-07-0 Toluene-d8 (S) 100 % 70-130 2 09/23/13 08:36 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-6 Lab ID: 92172207002 Collected: 09/13/13 10:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 50.0 20.0 2 09/23/13 08:52 67-64-1 Benzene ND ug/L 2.0 0.50 2 09/23/13 08:52 71-43-2 Bromobenzene ND ug/L 2.0 0.60 2 09/23/13 08:52 108-86-1 Bromochloromethane ND ug/L 2.0 0.34 2 09/23/13 08:52 74-97-5 Bromodichloromethane ND ug/L 2.0 0.36 2 09/23/13 08:52 75-27-4 Bromoform ND ug/L 2.0 0.52 2 09/23/13 08:52 75-25-2 Bromomethane ND ug/L 4.0 0.58 2 09/23/13 08:52 74-83-9 2-Butanone (MEK) ND ug/L 10.0 1.9 2 09/23/13 08:52 78-93-3 Carbon tetrachloride ND ug/L 2.0 0.50 2 09/23/13 08:52 56-23-5 Chlorobenzene ND ug/L 2.0 0.46 2 09/23/13 08:52 108-90-7 Chloroethane ND ug/L 2.0 1.1 2 09/23/13 08:52 75-00-3 Chloroform ND ug/L 2.0 0.28 2 09/23/13 08:52 67-66-3 Chloromethane ND ug/L 2.0 0.22 2 09/23/13 08:52 74-87-3 2-Chlorotoluene ND ug/L 2.0 0.70 2 09/23/13 08:52 95-49-8 4-Chlorotoluene ND ug/L 2.0 0.62 2 09/23/13 08:52 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 10.0 5.0 2 09/23/13 08:52 96-12-8 Dibromochloromethane ND ug/L 2.0 0.42 2 09/23/13 08:52 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 2.0 0.54 2 09/23/13 08:52 106-93-4 Dibromomethane ND ug/L 2.0 0.42 2 09/23/13 08:52 74-95-3 1,2-Dichlorobenzene ND ug/L 2.0 0.60 2 09/23/13 08:52 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 0.48 2 09/23/13 08:52 541-73-1 1,4-Dichlorobenzene 0.83J ug/L 2.0 0.66 2 09/23/13 08:52 106-46-7 Dichlorodifluoromethane ND ug/L 2.0 0.42 2 09/23/13 08:52 75-71-8 1,1-Dichloroethane ND ug/L 2.0 0.64 2 09/23/13 08:52 75-34-3 1,2-Dichloroethane ND ug/L 2.0 0.24 2 09/23/13 08:52 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1.1 2 09/23/13 08:52 75-35-4 cis-1,2-Dichloroethene 709 ug/L 20.0 3.8 20 09/23/13 02:13 156-59-2 trans-1,2-Dichloroethene 6.1 ug/L 2.0 0.98 2 09/23/13 08:52 156-60-5 1,2-Dichloropropane ND ug/L 2.0 0.54 2 09/23/13 08:52 78-87-5 1,3-Dichloropropane ND ug/L 2.0 0.56 2 09/23/13 08:52 142-28-9 2,2-Dichloropropane ND ug/L 2.0 0.26 2 09/23/13 08:52 594-20-7 1,1-Dichloropropene ND ug/L 2.0 0.98 2 09/23/13 08:52 563-58-6 cis-1,3-Dichloropropene ND ug/L 2.0 0.26 2 09/23/13 08:52 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 2.0 0.52 2 09/23/13 08:52 10061-02-6 Diisopropyl ether ND ug/L 2.0 0.24 2 09/23/13 08:52 108-20-3 Ethylbenzene ND ug/L 2.0 0.60 2 09/23/13 08:52 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.4 2 09/23/13 08:52 87-68-3 2-Hexanone ND ug/L 10.0 0.92 2 09/23/13 08:52 591-78-6 p-Isopropyltoluene ND ug/L 2.0 0.62 2 09/23/13 08:52 99-87-6 Methylene Chloride 9.9 ug/L 4.0 1.9 2 09/23/13 08:52 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 10.0 0.66 2 09/23/13 08:52 108-10-1 Methyl-tert-butyl ether ND ug/L 2.0 0.42 2 09/23/13 08:52 1634-04-4 Naphthalene ND ug/L 2.0 0.48 2 09/23/13 08:52 91-20-3 Styrene ND ug/L 2.0 0.52 2 09/23/13 08:52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 2.0 0.66 2 09/23/13 08:52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 2.0 0.80 2 09/23/13 08:52 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 Lab ID: 92172207002 Collected: 09/13/13 10:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1260 ug/L 20.0 9.2 20 09/23/13 02:13 127-18-4 Toluene 1.4J ug/L 2.0 0.52 2 09/23/13 08:52 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.66 2 09/23/13 08:52 87-61-6 1,2,4-Trichlorobenzene 1.OJ ug/L 2.0 0.70 2 09/23/13 08:52 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.96 2 09/23/13 08:52 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.58 2 09/23/13 08:52 79-00-5 Trichloroethene 228 ug/L 2.0 0.94 2 09/23/13 08:52 79-01-6 Trichlorofluoromethane ND ug/L 2.0 0.40 2 09/23/13 08:52 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.82 2 09/23/13 08:52 96-18-4 Vinyl acetate ND ug/L 4.0 0.70 2 09/23/13 08:52 108-05-4 Vinyl chloride 83.6 ug/L 2.0 1.2 2 09/23/13 08:52 75-01-4 Xylene (Total) ND ug/L 4.0 1.3 2 09/23/13 08:52 1330-20-7 m&p-Xylene ND ug/L 4.0 1.3 2 09/23/13 08:52 179601-23-1 o-Xylene ND ug/L 2.0 0.46 2 09/23/13 08:52 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 2 09/23/13 08:52 460-00-4 1,2-Dichloroethane-d4 (S) 107 % 70-130 2 09/23/13 08:52 17060-07-0 Toluene-d8 (S) 96 % 70-130 2 09/23/13 08:52 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 Lab ID: 92172207003 Collected: 09/11/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 02:29 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 02:29 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 02:29 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 02:29 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 02:29 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 02:29 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 02:29 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 02:29 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 02:29 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 02:29 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 02:29 75-00-3 0.64J ug/L 1.0 0.14 1 09/23/13 02:29 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 02:29 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 02:29 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 02:29 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 02:29 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 02:29 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 02:29 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 02:29 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 02:29 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 02:29 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 02:29 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 02:29 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 02:29 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 02:29 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 02:29 75-35-4 ND ug/L 1.0 0.19 1 09/23/13 02:29 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 02:29 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 02:29 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 02:29 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 02:29 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 02:29 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 02:29 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 02:29 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 02:29 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 02:29 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 02:29 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 02:29 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 02:29 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 02:29 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 02:29 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 02:29 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 02:29 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 02:29 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 02:29 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 02:29 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 Lab ID: 92172207003 Collected: 09/11/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 152 ug/L 1.0 0.46 1 09/23/13 02:29 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 02:29 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 02:29 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 02:29 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 02:29 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 02:29 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 02:29 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 02:29 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 02:29 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 02:29 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 02:29 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 02:29 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 02:29 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 02:29 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 09/23/13 02:29 460-00-4 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 09/23/13 02:29 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/23/13 02:29 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Lab ID: 92172207004 Collected: 09/11/13 13:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 09:08 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 09:08 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 09:08 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 09:08 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 09:08 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 09:08 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 09:08 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 09:08 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 09:08 56-23-5 0.43J ug/L 1.0 0.23 1 09/23/13 09:08 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 09:08 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 09:08 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 09:08 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 09:08 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 09:08 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 09:08 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 09:08 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 09:08 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 09:08 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 09:08 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 09:08 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 09:08 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 09:08 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 09:08 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 09:08 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 09:08 75-35-4 352 ug/L 10.0 1.9 10 09/23/13 02:45 156-59-2 1.5 ug/L 1.0 0.49 1 09/23/13 09:08 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 09:08 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 09:08 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 09:08 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 09:08 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 09:08 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 09:08 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 09:08 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 09:08 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 09:08 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 09:08 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 09:08 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 09:08 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 09:08 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 09:08 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 09:08 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 09:08 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 09:08 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 09:08 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Lab ID: 92172207004 Collected: 09/11/13 13:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1260 ug/L 10.0 4.6 10 09/23/13 02:45 127-18-4 Toluene 0.28J ug/L 1.0 0.26 1 09/23/13 09:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 09:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 09:08 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 09:08 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 09:08 79-00-5 Trichloroethene 90.4 ug/L 1.0 0.47 1 09/23/13 09:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 09:08 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 09:08 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 09:08 108-05-4 Vinyl chloride 2.0 ug/L 1.0 0.62 1 09/23/13 09:08 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 09:08 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 09:08 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 09:08 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/23/13 09:08 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/23/13 09:08 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/23/13 09:08 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-10 Lab ID: 92172207005 Collected: 09/12/13 12:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 09:24 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 09:24 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 09:24 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 09:24 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 09:24 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 09:24 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 09:24 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 09:24 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 09:24 56-23-5 Chlorobenzene 0.28J ug/L 1.0 0.23 1 09/23/13 09:24 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 09:24 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/23/13 09:24 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 09:24 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 09:24 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 09:24 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 09:24 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 09:24 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 09:24 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 09:24 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 09:24 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 09:24 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 09:24 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 09:24 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 09:24 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 09:24 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 09:24 75-35-4 cis-1,2-Dichloroethene 56.0 ug/L 1.0 0.19 1 09/23/13 09:24 156-59-2 trans-1,2-Dichloroethene 0.76J ug/L 1.0 0.49 1 09/23/13 09:24 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 09:24 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 09:24 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 09:24 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 09:24 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 09:24 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 09:24 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 09:24 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 09:24 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 09:24 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 09:24 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 09:24 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 09:24 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 09:24 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 09:24 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 09:24 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 09:24 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 09:24 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 09:24 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-10 Lab ID: 92172207005 Collected: 09/12/13 12:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 157 ug/L 10.0 4.6 10 09/23/13 03:01 127-18-4 Toluene 67.1 ug/L 1.0 0.26 1 09/23/13 09:24 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 09:24 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 09:24 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 09:24 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 09:24 79-00-5 Trichloroethene 17.7 ug/L 1.0 0.47 1 09/23/13 09:24 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 09:24 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 09:24 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 09:24 108-05-4 Vinyl chloride 7.7 ug/L 1.0 0.62 1 09/23/13 09:24 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 09:24 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 09:24 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 09:24 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/23/13 09:24 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 09/23/13 09:24 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 09:24 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-11 Lab ID: 92172207006 Collected: 09/12/13 15:05 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 09:40 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 09:40 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 09:40 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 09:40 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 09:40 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 09:40 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 09:40 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 09:40 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 09:40 56-23-5 Chlorobenzene 0.29J ug/L 1.0 0.23 1 09/23/13 09:40 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 09:40 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/23/13 09:40 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 09:40 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 09:40 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 09:40 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 09:40 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 09:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 09:40 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 09:40 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 09:40 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 09:40 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 09:40 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 09:40 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 09:40 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 09:40 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 09:40 75-35-4 cis-1,2-Dichloroethene 203 ug/L 10.0 1.9 10 09/23/13 03:17 156-59-2 trans-1,2-Dichloroethene 1.6 ug/L 1.0 0.49 1 09/23/13 09:40 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 09:40 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 09:40 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 09:40 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 09:40 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 09:40 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 09:40 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 09:40 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 09:40 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 09:40 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 09:40 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 09:40 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 09:40 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 09:40 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 09:40 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 09:40 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 09:40 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 09:40 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 09:40 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11 Lab ID: 92172207006 Collected: 09/12/13 15:05 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1050 ug/L 10.0 4.6 10 09/23/13 03:17 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 09:40 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 09:40 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 09:40 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 09:40 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 09:40 79-00-5 Trichloroethene 65.7 ug/L 1.0 0.47 1 09/23/13 09:40 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 09:40 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 09:40 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 09:40 108-05-4 Vinyl chloride 4.6 ug/L 1.0 0.62 1 09/23/13 09:40 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 09:40 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 09:40 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 09:40 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/23/13 09:40 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/23/13 09:40 17060-07-0 Toluene-d8 (S) 94 % 70-130 1 09/23/13 09:40 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-12 Lab ID: 92172207007 Collected: 09/12/13 10:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 27.3J ug/L 50.0 20.0 2 09/23/13 09:56 67-64-1 Benzene ND ug/L 2.0 0.50 2 09/23/13 09:56 71-43-2 Bromobenzene ND ug/L 2.0 0.60 2 09/23/13 09:56 108-86-1 Bromochloromethane ND ug/L 2.0 0.34 2 09/23/13 09:56 74-97-5 Bromodichloromethane ND ug/L 2.0 0.36 2 09/23/13 09:56 75-27-4 Bromoform ND ug/L 2.0 0.52 2 09/23/13 09:56 75-25-2 Bromomethane ND ug/L 4.0 0.58 2 09/23/13 09:56 74-83-9 2-Butanone (MEK) 13.3 ug/L 10.0 1.9 2 09/23/13 09:56 78-93-3 Carbon tetrachloride ND ug/L 2.0 0.50 2 09/23/13 09:56 56-23-5 Chlorobenzene ND ug/L 2.0 0.46 2 09/23/13 09:56 108-90-7 Chloroethane ND ug/L 2.0 1.1 2 09/23/13 09:56 75-00-3 Chloroform ND ug/L 2.0 0.28 2 09/23/13 09:56 67-66-3 Chloromethane ND ug/L 2.0 0.22 2 09/23/13 09:56 74-87-3 2-Chlorotoluene ND ug/L 2.0 0.70 2 09/23/13 09:56 95-49-8 4-Chlorotoluene ND ug/L 2.0 0.62 2 09/23/13 09:56 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 10.0 5.0 2 09/23/13 09:56 96-12-8 Dibromochloromethane ND ug/L 2.0 0.42 2 09/23/13 09:56 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 2.0 0.54 2 09/23/13 09:56 106-93-4 Dibromomethane ND ug/L 2.0 0.42 2 09/23/13 09:56 74-95-3 1,2-Dichlorobenzene ND ug/L 2.0 0.60 2 09/23/13 09:56 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 0.48 2 09/23/13 09:56 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 0.66 2 09/23/13 09:56 106-46-7 Dichlorodifluoromethane ND ug/L 2.0 0.42 2 09/23/13 09:56 75-71-8 1,1-Dichloroethane ND ug/L 2.0 0.64 2 09/23/13 09:56 75-34-3 1,2-Dichloroethane ND ug/L 2.0 0.24 2 09/23/13 09:56 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1.1 2 09/23/13 09:56 75-35-4 cis-1,2-Dichloroethene 13.3 ug/L 2.0 0.38 2 09/23/13 09:56 156-59-2 trans-1,2-Dichloroethene 8.3 ug/L 2.0 0.98 2 09/23/13 09:56 156-60-5 1,2-Dichloropropane ND ug/L 2.0 0.54 2 09/23/13 09:56 78-87-5 1,3-Dichloropropane ND ug/L 2.0 0.56 2 09/23/13 09:56 142-28-9 2,2-Dichloropropane ND ug/L 2.0 0.26 2 09/23/13 09:56 594-20-7 1,1-Dichloropropene ND ug/L 2.0 0.98 2 09/23/13 09:56 563-58-6 cis-1,3-Dichloropropene ND ug/L 2.0 0.26 2 09/23/13 09:56 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 2.0 0.52 2 09/23/13 09:56 10061-02-6 Diisopropyl ether ND ug/L 2.0 0.24 2 09/23/13 09:56 108-20-3 Ethylbenzene ND ug/L 2.0 0.60 2 09/23/13 09:56 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.4 2 09/23/13 09:56 87-68-3 2-Hexanone ND ug/L 10.0 0.92 2 09/23/13 09:56 591-78-6 p-Isopropyltoluene ND ug/L 2.0 0.62 2 09/23/13 09:56 99-87-6 Methylene Chloride 9.8 ug/L 4.0 1.9 2 09/23/13 09:56 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 10.0 0.66 2 09/23/13 09:56 108-10-1 Methyl-tert-butyl ether ND ug/L 2.0 0.42 2 09/23/13 09:56 1634-04-4 Naphthalene ND ug/L 2.0 0.48 2 09/23/13 09:56 91-20-3 Styrene ND ug/L 2.0 0.52 2 09/23/13 09:56 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 2.0 0.66 2 09/23/13 09:56 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 2.0 0.80 2 09/23/13 09:56 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-12 Lab ID: 92172207007 Collected: 09/12/13 10:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 3.9 ug/L 2.0 0.92 2 09/23/13 09:56 127-18-4 Toluene 11000 ug/L 100 26.0 100 09/23/13 22:06 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.66 2 09/23/13 09:56 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.70 2 09/23/13 09:56 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.96 2 09/23/13 09:56 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.58 2 09/23/13 09:56 79-00-5 Trichloroethene ND ug/L 2.0 0.94 2 09/23/13 09:56 79-01-6 Trichlorofluoromethane ND ug/L 2.0 0.40 2 09/23/13 09:56 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.82 2 09/23/13 09:56 96-18-4 Vinyl acetate ND ug/L 4.0 0.70 2 09/23/13 09:56 108-05-4 Vinyl chloride 1.9J ug/L 2.0 1.2 2 09/23/13 09:56 75-01-4 Xylene (Total) ND ug/L 4.0 1.3 2 09/23/13 09:56 1330-20-7 m&p-Xylene ND ug/L 4.0 1.3 2 09/23/13 09:56 179601-23-1 o-Xylene ND ug/L 2.0 0.46 2 09/23/13 09:56 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 2 09/23/13 09:56 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 2 09/23/13 09:56 17060-07-0 Toluene-d8 (S) 99 % 70-130 2 09/23/13 09:56 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 Lab ID: 92172207008 Collected: 09/11/13 14:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 10:12 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 10:12 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 10:12 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 10:12 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 10:12 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 10:12 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 10:12 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 10:12 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 10:12 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 10:12 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 10:12 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 10:12 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 10:12 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 10:12 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 10:12 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 10:12 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 10:12 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 10:12 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 10:12 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 10:12 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 10:12 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 10:12 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 10:12 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 10:12 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 10:12 107-06-2 0.91J ug/L 1.0 0.56 1 09/23/13 10:12 75-35-4 159 ug/L 10.0 1.9 10 09/23/13 03:49 156-59-2 3.5 ug/L 1.0 0.49 1 09/23/13 10:12 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 10:12 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 10:12 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 10:12 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 10:12 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 10:12 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 10:12 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 10:12 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 10:12 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 10:12 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 10:12 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 10:12 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 10:12 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 10:12 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 10:12 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 10:12 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 10:12 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 10:12 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 10:12 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 19 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 Lab ID: 92172207008 Collected: 09/11/13 14:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1030 ug/L 10.0 4.6 10 09/23/13 03:49 127-18-4 Toluene 3.3 ug/L 1.0 0.26 1 09/23/13 10:12 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 10:12 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 10:12 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 10:12 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 10:12 79-00-5 Trichloroethene 245 ug/L 10.0 4.7 10 09/23/13 03:49 79-01-6 Trichlorofluoromethane 0.24J ug/L 1.0 0.20 1 09/23/13 10:12 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 10:12 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 10:12 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 10:12 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 10:12 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 10:12 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 10:12 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/23/13 10:12 460-00-4 1,2-Dichloroethane-d4 (S) 109 % 70-130 1 09/23/13 10:12 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/23/13 10:12 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 20 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 Lab ID: 92172207009 Collected: 09/11/13 15:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 10:28 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 10:28 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 10:28 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 10:28 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 10:28 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 10:28 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 10:28 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 10:28 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 10:28 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 10:28 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 10:28 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 10:28 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 10:28 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 10:28 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 10:28 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 10:28 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 10:28 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 10:28 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 10:28 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 10:28 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 10:28 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 10:28 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 10:28 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 10:28 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 10:28 107-06-2 1.6 ug/L 1.0 0.56 1 09/23/13 10:28 75-35-4 167 ug/L 1.0 0.19 1 09/23/13 10:28 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 10:28 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 10:28 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 10:28 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 10:28 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 10:28 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 10:28 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 10:28 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 10:28 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 10:28 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 10:28 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 10:28 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 10:28 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 10:28 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 10:28 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 10:28 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 10:28 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 10:28 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 10:28 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 10:28 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 21 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 Lab ID: 92172207009 Collected: 09/11/13 15:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 774 ug/L 5.0 2.3 5 09/23/13 04:05 127-18-4 Toluene 0.93J ug/L 1.0 0.26 1 09/23/13 10:28 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 10:28 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 10:28 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 10:28 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 10:28 79-00-5 Trichloroethene 322 ug/L 5.0 2.4 5 09/23/13 04:05 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 10:28 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 10:28 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 10:28 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 10:28 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 10:28 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 10:28 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 10:28 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/23/13 10:28 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 09/23/13 10:28 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/23/13 10:28 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 22 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-15 Lab ID: 92172207010 Collected: 09/11/13 10:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 04:20 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 04:20 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 04:20 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 04:20 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 04:20 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 04:20 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 04:20 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 04:20 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 04:20 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 04:20 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 04:20 75-00-3 0.68J ug/L 1.0 0.14 1 09/23/13 04:20 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 04:20 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 04:20 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 04:20 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 04:20 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 04:20 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 04:20 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 04:20 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 04:20 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 04:20 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 04:20 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 04:20 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 04:20 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 04:20 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 04:20 75-35-4 3.9 ug/L 1.0 0.19 1 09/23/13 04:20 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 04:20 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 04:20 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 04:20 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 04:20 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 04:20 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 04:20 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 04:20 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 04:20 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 04:20 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 04:20 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 04:20 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 04:20 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 04:20 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 04:20 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 04:20 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 04:20 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 04:20 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 04:20 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 04:20 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 23 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-15 Lab ID: 92172207010 Collected: 09/11/13 10:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 94.3 ug/L 1.0 0.46 1 09/23/13 04:20 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 04:20 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 04:20 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 04:20 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 04:20 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 04:20 79-00-5 Trichloroethene 2.2 ug/L 1.0 0.47 1 09/23/13 04:20 79-01-6 Trichlorofluoromethane 0.63J ug/L 1.0 0.20 1 09/23/13 04:20 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 04:20 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 04:20 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 04:20 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 04:20 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 04:20 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 04:20 95-47-6 Surrogates 4-Bromofluorobenzene (S) 102 % 70-130 1 09/23/13 04:20 460-00-4 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 09/23/13 04:20 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 04:20 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 Lab ID: 92172207011 Collected: 09/11/13 10:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 04:36 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 04:36 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 04:36 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 04:36 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 04:36 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 04:36 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 04:36 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 04:36 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 04:36 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 04:36 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 04:36 75-00-3 1.0 ug/L 1.0 0.14 1 09/23/13 04:36 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 04:36 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 04:36 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 04:36 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 04:36 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 04:36 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 04:36 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 04:36 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 04:36 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 04:36 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 04:36 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 04:36 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 04:36 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 04:36 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 04:36 75-35-4 5.7 ug/L 1.0 0.19 1 09/23/13 04:36 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 04:36 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 04:36 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 04:36 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 04:36 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 04:36 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 04:36 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 04:36 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 04:36 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 04:36 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 04:36 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 04:36 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 04:36 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 04:36 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 04:36 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 04:36 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 04:36 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 04:36 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 04:36 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 04:36 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 25 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 Lab ID: 92172207011 Collected: 09/11/13 10:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 145 ug/L 1.0 0.46 1 09/23/13 04:36 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 04:36 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 04:36 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 04:36 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 04:36 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 04:36 79-00-5 Trichloroethene 2.8 ug/L 1.0 0.47 1 09/23/13 04:36 79-01-6 Trichlorofluoromethane 0.96J ug/L 1.0 0.20 1 09/23/13 04:36 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 04:36 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 04:36 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 04:36 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 04:36 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 04:36 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 04:36 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/23/13 04:36 460-00-4 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 09/23/13 04:36 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 04:36 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-17 Lab ID: 92172207012 Collected: 09/10/13 11:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 04:52 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 04:52 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 04:52 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 04:52 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 04:52 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 04:52 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 04:52 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 04:52 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 04:52 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 04:52 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 04:52 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 04:52 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 04:52 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 04:52 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 04:52 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 04:52 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 04:52 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 04:52 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 04:52 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 04:52 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 04:52 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 04:52 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 04:52 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 04:52 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 04:52 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 04:52 75-35-4 6.0 ug/L 1.0 0.19 1 09/23/13 04:52 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 04:52 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 04:52 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 04:52 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 04:52 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 04:52 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 04:52 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 04:52 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 04:52 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 04:52 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 04:52 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 04:52 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 04:52 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 04:52 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 04:52 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 04:52 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 04:52 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 04:52 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 04:52 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 04:52 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 27 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-17 Lab ID: 92172207012 Collected: 09/10/13 11:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 27.7 ug/L 1.0 0.46 1 09/23/13 04:52 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 04:52 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 04:52 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 04:52 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 04:52 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 04:52 79-00-5 Trichloroethene 3.8 ug/L 1.0 0.47 1 09/23/13 04:52 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 04:52 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 04:52 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 04:52 108-05-4 Vinyl chloride 1.8 ug/L 1.0 0.62 1 09/23/13 04:52 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 04:52 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 04:52 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 04:52 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 09/23/13 04:52 460-00-4 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 09/23/13 04:52 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/23/13 04:52 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 28 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-18 Lab ID: 92172207013 Collected: 09/10/13 14:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 05:08 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 05:08 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 05:08 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 05:08 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 05:08 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 05:08 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 05:08 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 05:08 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 05:08 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 05:08 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 05:08 75-00-3 Chloroform 1.7 ug/L 1.0 0.14 1 09/23/13 05:08 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 05:08 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 05:08 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 05:08 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 05:08 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 05:08 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 05:08 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 05:08 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 05:08 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 05:08 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 05:08 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 05:08 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 05:08 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 05:08 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 05:08 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/23/13 05:08 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/23/13 05:08 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 05:08 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 05:08 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 05:08 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 05:08 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 05:08 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 05:08 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 05:08 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 05:08 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 05:08 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 05:08 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 05:08 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 05:08 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 05:08 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 05:08 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 05:08 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 05:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 05:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 05:08 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 29 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-18 Lab ID: 92172207013 Collected: 09/10/13 14:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 05:08 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 05:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 05:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 05:08 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 05:08 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 05:08 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 05:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 05:08 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 05:08 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 05:08 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 05:08 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 05:08 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 05:08 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 05:08 95-47-6 Surrogates 4-Bromofluorobenzene (S) 106 % 70-130 1 09/23/13 05:08 460-00-4 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 09/23/13 05:08 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 09/23/13 05:08 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 30 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-20 Lab ID: 92172207014 Collected: 09/10/13 13:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 05:24 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 05:24 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 05:24 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 05:24 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 05:24 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 05:24 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 05:24 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 05:24 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 05:24 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 05:24 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 05:24 75-00-3 Chloroform 0.79J ug/L 1.0 0.14 1 09/23/13 05:24 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 05:24 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 05:24 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 05:24 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 05:24 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 05:24 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 05:24 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 05:24 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 05:24 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 05:24 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 05:24 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 05:24 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 05:24 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 05:24 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 05:24 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/23/13 05:24 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/23/13 05:24 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 05:24 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 05:24 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 05:24 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 05:24 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 05:24 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 05:24 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 05:24 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 05:24 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 05:24 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 05:24 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 05:24 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 05:24 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 05:24 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 05:24 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 05:24 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 05:24 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 05:24 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 05:24 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 31 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-20 Lab ID: 92172207014 Collected: 09/10/13 13:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 05:24 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 05:24 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 05:24 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 05:24 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 05:24 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 05:24 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 05:24 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 05:24 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 05:24 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 05:24 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 05:24 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 05:24 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 05:24 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 05:24 95-47-6 Surrogates 4-Bromofluorobenzene (S) 104 % 70-130 1 09/23/13 05:24 460-00-4 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 09/23/13 05:24 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 05:24 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 32 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-21 Lab ID: 92172207015 Collected: 09/10/13 10:05 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 05:40 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 05:40 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 05:40 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 05:40 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 05:40 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 05:40 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 05:40 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 05:40 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 05:40 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 05:40 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 05:40 75-00-3 Chloroform 2.3 ug/L 1.0 0.14 1 09/23/13 05:40 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 05:40 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 05:40 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 05:40 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 05:40 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 05:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 05:40 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 05:40 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 05:40 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 05:40 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 05:40 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 05:40 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 05:40 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 05:40 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 05:40 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/23/13 05:40 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/23/13 05:40 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 05:40 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 05:40 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 05:40 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 05:40 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 05:40 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 05:40 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 05:40 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 05:40 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 05:40 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 05:40 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 05:40 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 05:40 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 05:40 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 05:40 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 05:40 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 05:40 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 05:40 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 05:40 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 33 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-21 Lab ID: 92172207015 Collected: 09/10/13 10:05 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 05:40 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 05:40 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 05:40 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 05:40 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 05:40 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 05:40 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 05:40 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 05:40 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 05:40 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 05:40 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 05:40 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 05:40 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 05:40 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 05:40 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 09/23/13 05:40 460-00-4 1,2-Dichloroethane-d4 (S) 113 % 70-130 1 09/23/13 05:40 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/23/13 05:40 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 34 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-22 Lab ID: 92172207016 Collected: 09/10/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 05:56 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 05:56 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 05:56 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 05:56 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 05:56 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 05:56 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 05:56 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 05:56 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 05:56 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 05:56 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 05:56 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 05:56 67-66-3 0.12J ug/L 1.0 0.11 1 09/23/13 05:56 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 05:56 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 05:56 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 05:56 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 05:56 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 05:56 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 05:56 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 05:56 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 05:56 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 05:56 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 05:56 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 05:56 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 05:56 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 05:56 75-35-4 ND ug/L 1.0 0.19 1 09/23/13 05:56 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 05:56 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 05:56 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 05:56 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 05:56 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 05:56 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 05:56 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 05:56 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 05:56 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 05:56 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 05:56 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 05:56 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 05:56 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 05:56 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 05:56 108-10-1 0.52J ug/L 1.0 0.21 1 09/23/13 05:56 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 05:56 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 05:56 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 05:56 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 05:56 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 35 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-22 Lab ID: 92172207016 Collected: 09/10/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 05:56 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 05:56 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 05:56 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 05:56 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 05:56 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 05:56 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 05:56 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 05:56 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 05:56 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 05:56 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 05:56 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 05:56 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 05:56 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 05:56 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/23/13 05:56 460-00-4 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 09/23/13 05:56 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 05:56 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 36 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-23 Lab ID: 92172207017 Collected: 09/11/13 09:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 06:12 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 06:12 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 06:12 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 06:12 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 06:12 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 06:12 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 06:12 74-83-9 ND ug/L 5.0 0.96 1 09/23/13 06:12 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 06:12 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 06:12 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 06:12 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 06:12 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 06:12 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 06:12 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 06:12 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 06:12 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 06:12 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 06:12 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 06:12 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 06:12 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 06:12 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 06:12 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 06:12 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 06:12 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 06:12 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 06:12 75-35-4 2.6 ug/L 1.0 0.19 1 09/23/13 06:12 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 06:12 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 06:12 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 06:12 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 06:12 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 06:12 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 06:12 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 06:12 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 06:12 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 06:12 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 06:12 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 06:12 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 06:12 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 06:12 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 06:12 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 06:12 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 06:12 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 06:12 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 06:12 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 06:12 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 37 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-23 Lab ID: 92172207017 Collected: 09/11/13 09:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 39.0 ug/L 1.0 0.46 1 09/23/13 06:12 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 06:12 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 06:12 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 06:12 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 06:12 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 06:12 79-00-5 Trichloroethene 1.5 ug/L 1.0 0.47 1 09/23/13 06:12 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 06:12 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 06:12 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 06:12 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 06:12 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 06:12 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 06:12 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 06:12 95-47-6 Surrogates 4-Bromofluorobenzene (S) 102 % 70-130 1 09/23/13 06:12 460-00-4 1,2-Dichloroethane-d4 (S) 114 % 70-130 1 09/23/13 06:12 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 06:12 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 38 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-24 Lab ID: 92172207018 Collected: 09/10/13 15:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 10:44 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 10:44 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 10:44 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 10:44 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 10:44 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 10:44 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 10:44 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 10:44 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 10:44 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 10:44 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 10:44 75-00-3 Chloroform 0.65J ug/L 1.0 0.14 1 09/23/13 10:44 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 10:44 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 10:44 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 10:44 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 10:44 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 10:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 10:44 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 10:44 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 10:44 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 10:44 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 10:44 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 10:44 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 10:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 10:44 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 10:44 75-35-4 cis-1,2-Dichloroethene 8.1 ug/L 1.0 0.19 1 09/23/13 10:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/23/13 10:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 10:44 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 10:44 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 10:44 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 10:44 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 10:44 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 10:44 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 10:44 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 10:44 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 10:44 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 10:44 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 10:44 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 10:44 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 10:44 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 10:44 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 10:44 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 10:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 10:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 10:44 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 39 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-24 Lab ID: 92172207018 Collected: 09/10/13 15:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 406 ug/L 10.0 4.6 10 09/23/13 06:28 127-18-4 Toluene 0.42J ug/L 1.0 0.26 1 09/23/13 10:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 10:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 10:44 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 10:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 10:44 79-00-5 Trichloroethene 2.9 ug/L 1.0 0.47 1 09/23/13 10:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 10:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 10:44 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 10:44 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 10:44 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 10:44 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 10:44 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 10:44 95-47-6 Surrogates 4-Bromofluorobenzene (S) 102 % 70-130 1 09/23/13 10:44 460-00-4 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 09/23/13 10:44 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 10:44 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 40 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: MW-26 Lab ID: 92172207019 Collected: 09/10/13 09:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 06:44 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 06:44 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 06:44 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 06:44 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 06:44 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 06:44 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 06:44 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 06:44 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 06:44 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 06:44 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 06:44 75-00-3 Chloroform 1.5 ug/L 1.0 0.14 1 09/23/13 06:44 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 06:44 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 06:44 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 06:44 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 06:44 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 06:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 06:44 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 06:44 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 06:44 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 06:44 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 06:44 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 06:44 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 06:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 06:44 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 06:44 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/23/13 06:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/23/13 06:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 06:44 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 06:44 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 06:44 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 06:44 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 06:44 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 06:44 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 06:44 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 06:44 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 06:44 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 06:44 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 06:44 99-87-6 Methylene Chloride 2.3 ug/L 2.0 0.97 1 09/23/13 06:44 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 06:44 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 06:44 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 06:44 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 06:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 06:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 06:44 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 41 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-26 Lab ID: 92172207019 Collected: 09/10/13 09:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 06:44 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 06:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 06:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 06:44 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 06:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 06:44 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 06:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 06:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 06:44 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 06:44 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 06:44 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 06:44 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 06:44 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 06:44 95-47-6 Surrogates 4-Bromofluorobenzene (S) 102 % 70-130 1 09/23/13 06:44 460-00-4 1,2-Dichloroethane-d4 (S) 113 % 70-130 1 09/23/13 06:44 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/23/13 06:44 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 42 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: RW-1 Lab ID: 92172207020 Collected: 09/13/13 09:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 29.1 ug/L 25.0 10.0 1 09/23/13 11:00 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 11:00 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 11:00 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 11:00 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 11:00 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 11:00 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 11:00 74-83-9 2-Butanone (MEK) 53.7 ug/L 5.0 0.96 1 09/23/13 11:00 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 11:00 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 11:00 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 11:00 75-00-3 Chloroform 0.73J ug/L 1.0 0.14 1 09/23/13 11:00 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 11:00 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 11:00 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 11:00 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 11:00 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 11:00 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 11:00 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 11:00 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 11:00 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 11:00 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 11:00 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 11:00 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 11:00 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 11:00 107-06-2 1,1-Dichloroethene 1.9 ug/L 1.0 0.56 1 09/23/13 11:00 75-35-4 cis-1,2-Dichloroethene 1740 ug/L 10.0 1.9 10 09/23/13 07:00 156-59-2 trans-1,2-Dichloroethene 6.3 ug/L 1.0 0.49 1 09/23/13 11:00 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 11:00 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 11:00 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 11:00 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 11:00 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 11:00 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 11:00 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 11:00 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 11:00 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 11:00 87-68-3 2-Hexanone 1.3J ug/L 5.0 0.46 1 09/23/13 11:00 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 11:00 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 11:00 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 11:00 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 11:00 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 11:00 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 11:00 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 11:00 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 11:00 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 43 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-1 Lab ID: 92172207020 Collected: 09/13/13 09:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 22.5 ug/L 1.0 0.46 1 09/23/13 11:00 127-18-4 Toluene 3.5 ug/L 1.0 0.26 1 09/23/13 11:00 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 11:00 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 11:00 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 11:00 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 11:00 79-00-5 Trichloroethene 58.4 ug/L 1.0 0.47 1 09/23/13 11:00 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 11:00 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 11:00 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 11:00 108-05-4 Vinyl chloride 14.8 ug/L 1.0 0.62 1 09/23/13 11:00 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 11:00 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 11:00 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 11:00 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/23/13 11:00 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/23/13 11:00 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 09/23/13 11:00 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 44 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: RW-3 Lab ID: 92172207021 Collected: 09/13/13 09:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 29.1 ug/L 25.0 10.0 1 09/23/13 07:16 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 07:16 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 07:16 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 07:16 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 07:16 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 07:16 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 07:16 74-83-9 2-Butanone (MEK) 16.6 ug/L 5.0 0.96 1 09/23/13 07:16 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 07:16 56-23-5 Chlorobenzene 0.40J ug/L 1.0 0.23 1 09/23/13 07:16 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 07:16 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/23/13 07:16 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 07:16 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 07:16 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 07:16 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 07:16 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 07:16 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 07:16 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 07:16 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 07:16 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 07:16 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 07:16 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 07:16 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 07:16 75-34-3 1,2-Dichloroethane 0.22J ug/L 1.0 0.12 1 09/23/13 07:16 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 07:16 75-35-4 cis-1,2-Dichloroethene 6.1 ug/L 1.0 0.19 1 09/23/13 07:16 156-59-2 trans-1,2-Dichloroethene 6.3 ug/L 1.0 0.49 1 09/23/13 07:16 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 07:16 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 07:16 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 07:16 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 07:16 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 07:16 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 07:16 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 07:16 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 07:16 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 07:16 87-68-3 2-Hexanone 3.4J ug/L 5.0 0.46 1 09/23/13 07:16 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 07:16 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 07:16 75-09-2 4-Methyl-2-pentanone (MIBK) 4.OJ ug/L 5.0 0.33 1 09/23/13 07:16 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 07:16 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 07:16 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 07:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 07:16 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 07:16 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 45 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-3 Lab ID: 92172207021 Collected: 09/13/13 09:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 07:16 127-18-4 Toluene 10300 ug/L 200 52.0 200 09/23/13 20:47 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 07:16 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 07:16 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 07:16 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 07:16 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 07:16 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 07:16 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 07:16 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 07:16 108-05-4 Vinyl chloride 1.2 ug/L 1.0 0.62 1 09/23/13 07:16 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 07:16 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 07:16 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 07:16 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 09/23/13 07:16 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/23/13 07:16 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 09/23/13 07:16 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 46 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: RW-5 Lab ID: 92172207022 Collected: 09/13/13 10:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 476J ug/L 500 200 20 09/23/13 11:16 67-64-1 Benzene ND ug/L 20.0 5.0 20 09/23/13 11:16 71-43-2 Bromobenzene ND ug/L 20.0 6.0 20 09/23/13 11:16 108-86-1 Bromochloromethane ND ug/L 20.0 3.4 20 09/23/13 11:16 74-97-5 Bromodichloromethane ND ug/L 20.0 3.6 20 09/23/13 11:16 75-27-4 Bromoform ND ug/L 20.0 5.2 20 09/23/13 11:16 75-25-2 Bromomethane ND ug/L 40.0 5.8 20 09/23/13 11:16 74-83-9 2-Butanone (MEK) 265 ug/L 100 19.2 20 09/23/13 11:16 78-93-3 Carbon tetrachloride ND ug/L 20.0 5.0 20 09/23/13 11:16 56-23-5 Chlorobenzene ND ug/L 20.0 4.6 20 09/23/13 11:16 108-90-7 Chloroethane ND ug/L 20.0 10.8 20 09/23/13 11:16 75-00-3 Chloroform ND ug/L 20.0 2.8 20 09/23/13 11:16 67-66-3 Chloromethane ND ug/L 20.0 2.2 20 09/23/13 11:16 74-87-3 2-Chlorotoluene ND ug/L 20.0 7.0 20 09/23/13 11:16 95-49-8 4-Chlorotoluene ND ug/L 20.0 6.2 20 09/23/13 11:16 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 100 50.4 20 09/23/13 11:16 96-12-8 Dibromochloromethane ND ug/L 20.0 4.2 20 09/23/13 11:16 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 20.0 5.4 20 09/23/13 11:16 106-93-4 Dibromomethane ND ug/L 20.0 4.2 20 09/23/13 11:16 74-95-3 1,2-Dichlorobenzene ND ug/L 20.0 6.0 20 09/23/13 11:16 95-50-1 1,3-Dichlorobenzene ND ug/L 20.0 4.8 20 09/23/13 11:16 541-73-1 1,4-Dichlorobenzene ND ug/L 20.0 6.6 20 09/23/13 11:16 106-46-7 Dichlorodifluoromethane ND ug/L 20.0 4.2 20 09/23/13 11:16 75-71-8 1,1-Dichloroethane ND ug/L 20.0 6.4 20 09/23/13 11:16 75-34-3 1,2-Dichloroethane ND ug/L 20.0 2.4 20 09/23/13 11:16 107-06-2 1,1-Dichloroethene ND ug/L 20.0 11.2 20 09/23/13 11:16 75-35-4 cis-1,2-Dichloroethene 68.0 ug/L 20.0 3.8 20 09/23/13 11:16 156-59-2 trans-1,2-Dichloroethene ND ug/L 20.0 9.8 20 09/23/13 11:16 156-60-5 1,2-Dichloropropane ND ug/L 20.0 5.4 20 09/23/13 11:16 78-87-5 1,3-Dichloropropane ND ug/L 20.0 5.6 20 09/23/13 11:16 142-28-9 2,2-Dichloropropane ND ug/L 20.0 2.6 20 09/23/13 11:16 594-20-7 1,1-Dichloropropene ND ug/L 20.0 9.8 20 09/23/13 11:16 563-58-6 cis-1,3-Dichloropropene ND ug/L 20.0 2.6 20 09/23/13 11:16 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 20.0 5.2 20 09/23/13 11:16 10061-02-6 Diisopropyl ether ND ug/L 20.0 2.4 20 09/23/13 11:16 108-20-3 Ethylbenzene ND ug/L 20.0 6.0 20 09/23/13 11:16 100-41-4 Hexachloro-1,3-butadiene ND ug/L 20.0 14.2 20 09/23/13 11:16 87-68-3 2-Hexanone ND ug/L 100 9.2 20 09/23/13 11:16 591-78-6 p-Isopropyltoluene ND ug/L 20.0 6.2 20 09/23/13 11:16 99-87-6 Methylene Chloride 168 ug/L 40.0 19.4 20 09/23/13 11:16 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100 6.6 20 09/23/13 11:16 108-10-1 Methyl-tert-butyl ether ND ug/L 20.0 4.2 20 09/23/13 11:16 1634-04-4 Naphthalene ND ug/L 20.0 4.8 20 09/23/13 11:16 91-20-3 Styrene ND ug/L 20.0 5.2 20 09/23/13 11:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 20.0 6.6 20 09/23/13 11:16 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 20.0 8.0 20 09/23/13 11:16 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 47 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-5 Lab ID: 92172207022 Collected: 09/13/13 10:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 34.6 ug/L 20.0 9.2 20 09/23/13 11:16 127-18-4 Toluene 34900 ug/L 200 52.0 200 09/23/13 07:32 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.6 20 09/23/13 11:16 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 7.0 20 09/23/13 11:16 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 9.6 20 09/23/13 11:16 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 5.8 20 09/23/13 11:16 79-00-5 Trichloroethene ND ug/L 20.0 9.4 20 09/23/13 11:16 79-01-6 Trichlorofluoromethane ND ug/L 20.0 4.0 20 09/23/13 11:16 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 8.2 20 09/23/13 11:16 96-18-4 Vinyl acetate ND ug/L 40.0 7.0 20 09/23/13 11:16 108-05-4 Vinyl chloride ND ug/L 20.0 12.4 20 09/23/13 11:16 75-01-4 Xylene (Total) ND ug/L 40.0 13.2 20 09/23/13 11:16 1330-20-7 m&p-Xylene ND ug/L 40.0 13.2 20 09/23/13 11:16 179601-23-1 o-Xylene ND ug/L 20.0 4.6 20 09/23/13 11:16 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 20 09/23/13 11:16 460-00-4 1,2-Dichloroethane-d4 (S) 103 % 70-130 20 09/23/13 11:16 17060-07-0 Toluene-d8 (S) 103 % 70-130 20 09/23/13 11:16 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 48 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: RW-6 Lab ID: 92172207023 Collected: 09/13/13 15:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 218 ug/L 25.0 10.0 1 09/23/13 21:34 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 21:34 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 21:34 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 21:34 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 21:34 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 21:34 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 21:34 74-83-9 2-Butanone (MEK) 34.3 ug/L 5.0 0.96 1 09/23/13 21:34 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 21:34 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 21:34 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 21:34 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/23/13 21:34 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 21:34 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 21:34 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 21:34 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 21:34 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 21:34 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 21:34 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 21:34 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 21:34 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 21:34 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 21:34 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 21:34 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 21:34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 21:34 107-06-2 1,1-Dichloroethene 3.2 ug/L 1.0 0.56 1 09/23/13 21:34 75-35-4 cis-1,2-Dichloroethene 501 ug/L 10.0 1.9 10 09/23/13 21:18 156-59-2 trans-1,2-Dichloroethene 4.3 ug/L 1.0 0.49 1 09/23/13 21:34 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 21:34 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 21:34 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 21:34 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 21:34 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 21:34 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 21:34 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 21:34 108-20-3 Ethylbenzene 0.91J ug/L 1.0 0.30 1 09/23/13 21:34 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 21:34 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 21:34 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 21:34 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 21:34 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 21:34 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 21:34 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 21:34 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 21:34 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 21:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 21:34 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 49 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 Lab ID: 92172207023 Collected: 09/13/13 15:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 27.8 ug/L 1.0 0.46 1 09/23/13 21:34 127-18-4 Toluene 5.7 ug/L 1.0 0.26 1 09/23/13 21:34 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 21:34 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 21:34 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 21:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 21:34 79-00-5 Trichloroethene 20.1 ug/L 1.0 0.47 1 09/23/13 21:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 21:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 21:34 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 21:34 108-05-4 Vinyl chloride 96.0 ug/L 1.0 0.62 1 09/23/13 21:34 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 21:34 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 21:34 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 21:34 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/23/13 21:34 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 09/23/13 21:34 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 09/23/13 21:34 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 50 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Lab ID: 92172207024 Collected: 09/13/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 254 ug/L 25.0 10.0 1 09/23/13 11:31 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 11:31 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 11:31 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 11:31 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 11:31 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 11:31 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 11:31 74-83-9 62.0 ug/L 5.0 0.96 1 09/23/13 11:31 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 11:31 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 11:31 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 11:31 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 11:31 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 11:31 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 11:31 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 11:31 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 11:31 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 11:31 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 11:31 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 11:31 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 11:31 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 11:31 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 11:31 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 11:31 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 11:31 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 11:31 107-06-2 1.2 ug/L 1.0 0.56 1 09/23/13 11:31 75-35-4 401 ug/L 10.0 1.9 10 09/23/13 08:04 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 11:31 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 11:31 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 11:31 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 11:31 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 11:31 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 11:31 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 11:31 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 11:31 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 11:31 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 11:31 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 11:31 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 11:31 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 11:31 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 11:31 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 11:31 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 11:31 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 11:31 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 11:31 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 11:31 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 51 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Lab ID: 92172207024 Collected: 09/13/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 57.3 ug/L 1.0 0.46 1 09/23/13 11:31 127-18-4 Toluene 2.9 ug/L 1.0 0.26 1 09/23/13 11:31 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 11:31 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 11:31 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 11:31 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 11:31 79-00-5 Trichloroethene 17.8 ug/L 1.0 0.47 1 09/23/13 11:31 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 11:31 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 11:31 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 11:31 108-05-4 Vinyl chloride 14.7 ug/L 1.0 0.62 1 09/23/13 11:31 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 11:31 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 11:31 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 11:31 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/23/13 11:31 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 09/23/13 11:31 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/23/13 11:31 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 52 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: FIELD BLANK 9/11 Lab ID: 92172207026 Collected: 09/11/13 08:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Date: 09/27/2013 09:01 AM Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/23/13 01:41 67-64-1 ND ug/L 1.0 0.25 1 09/23/13 01:41 71-43-2 ND ug/L 1.0 0.30 1 09/23/13 01:41 108-86-1 ND ug/L 1.0 0.17 1 09/23/13 01:41 74-97-5 ND ug/L 1.0 0.18 1 09/23/13 01:41 75-27-4 ND ug/L 1.0 0.26 1 09/23/13 01:41 75-25-2 ND ug/L 2.0 0.29 1 09/23/13 01:41 74-83-9 4.5J ug/L 5.0 0.96 1 09/23/13 01:41 78-93-3 ND ug/L 1.0 0.25 1 09/23/13 01:41 56-23-5 ND ug/L 1.0 0.23 1 09/23/13 01:41 108-90-7 ND ug/L 1.0 0.54 1 09/23/13 01:41 75-00-3 ND ug/L 1.0 0.14 1 09/23/13 01:41 67-66-3 ND ug/L 1.0 0.11 1 09/23/13 01:41 74-87-3 ND ug/L 1.0 0.35 1 09/23/13 01:41 95-49-8 ND ug/L 1.0 0.31 1 09/23/13 01:41 106-43-4 ND ug/L 5.0 2.5 1 09/23/13 01:41 96-12-8 ND ug/L 1.0 0.21 1 09/23/13 01:41 124-48-1 ND ug/L 1.0 0.27 1 09/23/13 01:41 106-93-4 ND ug/L 1.0 0.21 1 09/23/13 01:41 74-95-3 ND ug/L 1.0 0.30 1 09/23/13 01:41 95-50-1 ND ug/L 1.0 0.24 1 09/23/13 01:41 541-73-1 ND ug/L 1.0 0.33 1 09/23/13 01:41 106-46-7 ND ug/L 1.0 0.21 1 09/23/13 01:41 75-71-8 ND ug/L 1.0 0.32 1 09/23/13 01:41 75-34-3 ND ug/L 1.0 0.12 1 09/23/13 01:41 107-06-2 ND ug/L 1.0 0.56 1 09/23/13 01:41 75-35-4 ND ug/L 1.0 0.19 1 09/23/13 01:41 156-59-2 ND ug/L 1.0 0.49 1 09/23/13 01:41 156-60-5 ND ug/L 1.0 0.27 1 09/23/13 01:41 78-87-5 ND ug/L 1.0 0.28 1 09/23/13 01:41 142-28-9 ND ug/L 1.0 0.13 1 09/23/13 01:41 594-20-7 ND ug/L 1.0 0.49 1 09/23/13 01:41 563-58-6 ND ug/L 1.0 0.13 1 09/23/13 01:41 10061-01-5 ND ug/L 1.0 0.26 1 09/23/13 01:41 10061-02-6 ND ug/L 1.0 0.12 1 09/23/13 01:41 108-20-3 ND ug/L 1.0 0.30 1 09/23/13 01:41 100-41-4 ND ug/L 1.0 0.71 1 09/23/13 01:41 87-68-3 ND ug/L 5.0 0.46 1 09/23/13 01:41 591-78-6 ND ug/L 1.0 0.31 1 09/23/13 01:41 99-87-6 ND ug/L 2.0 0.97 1 09/23/13 01:41 75-09-2 ND ug/L 5.0 0.33 1 09/23/13 01:41 108-10-1 ND ug/L 1.0 0.21 1 09/23/13 01:41 1634-04-4 ND ug/L 1.0 0.24 1 09/23/13 01:41 91-20-3 ND ug/L 1.0 0.26 1 09/23/13 01:41 100-42-5 ND ug/L 1.0 0.33 1 09/23/13 01:41 630-20-6 ND ug/L 1.0 0.40 1 09/23/13 01:41 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 53 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: FIELD BLANK 9/11 Parameters Lab ID: 92172207026 Results Units Collected: Report Limit 09/11/13 08:30 MDL DF Received: 09/16/13 09:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 01:41 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 01:41 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 01:41 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 01:41 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 01:41 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 01:41 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 01:41 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 01:41 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 01:41 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 01:41 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 01:41 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 01:41 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 01:41 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 01:41 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/23/13 01:41 460-00-4 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 09/23/13 01:41 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/23/13 01:41 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 54 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: FIELD BLANK 9/13 Lab ID: 92172207028 Collected: 09/13/13 08:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 01:25 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 01:25 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 01:25 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 01:25 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 01:25 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 01:25 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 01:25 74-83-9 2-Butanone (MEK) 4AJ ug/L 5.0 0.96 1 09/23/13 01:25 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 01:25 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 01:25 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 01:25 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/23/13 01:25 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 01:25 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 01:25 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 01:25 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 01:25 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 01:25 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 01:25 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 01:25 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 01:25 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 01:25 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 01:25 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 01:25 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 01:25 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 01:25 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 01:25 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/23/13 01:25 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/23/13 01:25 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 01:25 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 01:25 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 01:25 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 01:25 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 01:25 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 01:25 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 01:25 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 01:25 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 01:25 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 01:25 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 01:25 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 01:25 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 01:25 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 01:25 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 01:25 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 01:25 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 01:25 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 01:25 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 55 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: FIELD BLANK 9/13 Parameters Lab ID: 92172207028 Results Units Collected: Report Limit 09/13/13 08:30 MDL DF Received: 09/16/13 09:00 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 01:25 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 01:25 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 01:25 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 01:25 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 01:25 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 01:25 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 01:25 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 01:25 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 01:25 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 01:25 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 01:25 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 01:25 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 01:25 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 01:25 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/23/13 01:25 460-00-4 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 09/23/13 01:25 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/23/13 01:25 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 56 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: DUPLICATE Lab ID: 92172207029 Collected: 09/13/13 00:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 295 ug/L 25.0 10.0 1 09/23/13 08:20 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 08:20 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 08:20 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 08:20 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 08:20 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 08:20 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 08:20 74-83-9 2-Butanone (MEK) 44.4 ug/L 5.0 0.96 1 09/23/13 08:20 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 08:20 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 08:20 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 08:20 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/23/13 08:20 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 08:20 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 08:20 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 08:20 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 08:20 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 08:20 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 08:20 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 08:20 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 08:20 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 08:20 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 08:20 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 08:20 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 08:20 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 08:20 107-06-2 1,1-Dichloroethene 3.2 ug/L 1.0 0.56 1 09/23/13 08:20 75-35-4 cis-1,2-Dichloroethene 509 ug/L 10.0 1.9 10 09/23/13 21:02 156-59-2 trans-1,2-Dichloroethene 4.5 ug/L 1.0 0.49 1 09/23/13 08:20 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 08:20 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 08:20 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 08:20 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 08:20 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 08:20 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 08:20 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 08:20 108-20-3 Ethylbenzene 1.2 ug/L 1.0 0.30 1 09/23/13 08:20 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 08:20 87-68-3 2-Hexanone 7.5 ug/L 5.0 0.46 1 09/23/13 08:20 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 08:20 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 08:20 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 08:20 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 08:20 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 08:20 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 08:20 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 08:20 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 08:20 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 57 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DUPLICATE Lab ID: 92172207029 Collected: 09/13/13 00:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 26.4 ug/L 1.0 0.46 1 09/23/13 08:20 127-18-4 Toluene 6.4 ug/L 1.0 0.26 1 09/23/13 08:20 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 08:20 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 08:20 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 08:20 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 08:20 79-00-5 Trichloroethene 19.9 ug/L 1.0 0.47 1 09/23/13 08:20 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 08:20 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 08:20 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 08:20 108-05-4 Vinyl chloride 94.8 ug/L 1.0 0.62 1 09/23/13 08:20 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 08:20 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 08:20 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 08:20 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/23/13 08:20 460-00-4 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 09/23/13 08:20 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 09/23/13 08:20 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 58 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Sample: TRIP BLANK Lab ID: 92172207030 Collected: 09/13/13 00:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/23/13 01:09 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/23/13 01:09 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/23/13 01:09 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/23/13 01:09 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/23/13 01:09 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/23/13 01:09 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/23/13 01:09 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/23/13 01:09 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/23/13 01:09 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/23/13 01:09 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/23/13 01:09 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/23/13 01:09 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/23/13 01:09 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/23/13 01:09 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/23/13 01:09 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/23/13 01:09 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/23/13 01:09 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/23/13 01:09 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/23/13 01:09 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/23/13 01:09 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/23/13 01:09 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 01:09 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/23/13 01:09 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/23/13 01:09 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/23/13 01:09 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/23/13 01:09 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/23/13 01:09 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/23/13 01:09 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/23/13 01:09 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/23/13 01:09 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/23/13 01:09 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/23/13 01:09 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/23/13 01:09 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/23/13 01:09 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/23/13 01:09 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/23/13 01:09 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/23/13 01:09 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/23/13 01:09 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/23/13 01:09 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/23/13 01:09 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/23/13 01:09 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/23/13 01:09 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/23/13 01:09 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/23/13 01:09 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/23/13 01:09 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/23/13 01:09 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 59 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK Lab ID: 92172207030 Collected: 09/13/13 00:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/23/13 01:09 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/23/13 01:09 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/23/13 01:09 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/23/13 01:09 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/23/13 01:09 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/23/13 01:09 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/23/13 01:09 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/23/13 01:09 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/23/13 01:09 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/23/13 01:09 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/23/13 01:09 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/23/13 01:09 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/23/13 01:09 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/23/13 01:09 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 09/23/13 01:09 460-00-4 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 09/23/13 01:09 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/23/13 01:09 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 60 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. acmnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 QC Batch: MSV/24317 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92172207001, 92172207002, 92172207003, 92172207004, 92172207005, 92172207006, 92172207007, 92172207008,92172207009,92172207010,92172207011,92172207012,92172207013,92172207014, 92172207015,92172207016,92172207017,92172207026,92172207028,92172207030 METHOD BLANK: 1051888 Matrix: Water Associated Lab Samples: 92172207001, 92172207002, 92172207003, 92172207004, 92172207005, 92172207006, 92172207007, 92172207008,92172207009,92172207010,92172207011,92172207012,92172207013,92172207014, 92172207015, 92172207016, 92172207017, 92172207026, 92172207028, 92172207030 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/23/13 00:37 1, 1, 1 -Trichloroethane ug/L ND 1.0 09/23/13 00:37 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/23/13 00:37 1,1,2-Trichloroethane ug/L ND 1.0 09/23/13 00:37 1,1-Dichloroethane ug/L ND 1.0 09/23/13 00:37 1,1-Dichloroethene ug/L ND 1.0 09/23/13 00:37 1,1-Dichloropropene ug/L ND 1.0 09/23/13 00:37 1,2,3-Trichlorobenzene ug/L ND 1.0 09/23/13 00:37 1,2,3-Trichloropropane ug/L ND 1.0 09/23/13 00:37 1,2,4-Trichlorobenzene ug/L ND 1.0 09/23/13 00:37 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/23/13 00:37 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/23/13 00:37 1,2-Dichlorobenzene ug/L ND 1.0 09/23/13 00:37 1,2-Dichloroethane ug/L ND 1.0 09/23/13 00:37 1,2-Dichloropropane ug/L ND 1.0 09/23/13 00:37 1,3-Dichlorobenzene ug/L ND 1.0 09/23/13 00:37 1,3-Dichloropropane ug/L ND 1.0 09/23/13 00:37 1,4-Dichlorobenzene ug/L ND 1.0 09/23/13 00:37 2,2-Dichloropropane ug/L ND 1.0 09/23/13 00:37 2-Butanone (MEK) ug/L ND 5.0 09/23/13 00:37 2-Chlorotoluene ug/L ND 1.0 09/23/13 00:37 2-Hexanone ug/L ND 5.0 09/23/13 00:37 4-Chlorotoluene ug/L ND 1.0 09/23/13 00:37 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/23/13 00:37 Acetone ug/L ND 25.0 09/23/13 00:37 Benzene ug/L ND 1.0 09/23/13 00:37 Bromobenzene ug/L ND 1.0 09/23/13 00:37 Bromochloromethane ug/L ND 1.0 09/23/13 00:37 Bromodichloromethane ug/L ND 1.0 09/23/13 00:37 Bromoform ug/L ND 1.0 09/23/13 00:37 Bromomethane ug/L ND 2.0 09/23/13 00:37 Carbon tetrachloride ug/L ND 1.0 09/23/13 00:37 Chlorobenzene ug/L ND 1.0 09/23/13 00:37 Chloroethane ug/L ND 1.0 09/23/13 00:37 Chloroform ug/L ND 1.0 09/23/13 00:37 Chloromethane ug/L ND 1.0 09/23/13 00:37 cis- 1,2-Dichloroethene ug/L ND 1.0 09/23/13 00:37 cis- 1,3-Dichloropropene ug/L ND 1.0 09/23/13 00:37 Dibromochloromethane ug/L ND 1.0 09/23/13 00:37 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 61 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 METHOD BLANK: 1051888 Matrix: Water Associated Lab Samples: 92172207001, 92172207002, 92172207003, 92172207004, 92172207005, 92172207006, 92172207007, 92172207008,92172207009,92172207010,92172207011,92172207012,92172207013,92172207014, 92172207015,92172207016,92172207017,92172207026,92172207028,92172207030 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dibromomethane ug/L ND 1.0 09/23/13 00:37 Dichlorodifluoromethane ug/L ND 1.0 09/23/13 00:37 Diisopropyl ether ug/L ND 1.0 09/23/13 00:37 Ethylbenzene ug/L ND 1.0 09/23/13 00:37 Hexachloro-1,3-butadiene ug/L ND 1.0 09/23/13 00:37 m&p-Xylene ug/L ND 2.0 09/23/13 00:37 Methyl-tert-butyl ether ug/L ND 1.0 09/23/13 00:37 Methylene Chloride ug/L ND 2.0 09/23/13 00:37 Naphthalene ug/L ND 1.0 09/23/13 00:37 o-Xylene ug/L ND 1.0 09/23/13 00:37 p-Isopropyltoluene ug/L ND 1.0 09/23/13 00:37 Styrene ug/L ND 1.0 09/23/13 00:37 Tetrachloroethene ug/L ND 1.0 09/23/13 00:37 Toluene ug/L ND 1.0 09/23/13 00:37 trans-1,2-Dichloroethene ug/L ND 1.0 09/23/13 00:37 trans- 1,3-Dichloropropene ug/L ND 1.0 09/23/13 00:37 Trichloroethene ug/L ND 1.0 09/23/13 00:37 Trichlorofluoromethane ug/L ND 1.0 09/23/13 00:37 Vinyl acetate ug/L ND 2.0 09/23/13 00:37 Vinyl chloride ug/L ND 1.0 09/23/13 00:37 Xylene (Total) ug/L ND 2.0 09/23/13 00:37 1,2-Dichloroethane-d4 (S) % 101 70-130 09/23/13 00:37 4-Bromofluorobenzene (S) % 99 70-130 09/23/13 00:37 Toluene-d8 (S) % 97 70-130 09/23/13 00:37 LABORATORY CONTROL SAMPLE: Parameter 1051889 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.1 108 70-130 1,1,1-Trichloroethane ug/L 50 54.0 108 70-130 1,1,2,2-Tetrachloroethane ug/L 50 52.0 104 70-130 1,1,2-Trichloroethane ug/L 50 53.7 107 70-130 1,1-Dichloroethane ug/L 50 53.3 107 70-130 1,1-Dichloroethene ug/L 50 59.9 120 70-132 1,1-Dichloropropene ug/L 50 55.5 111 70-130 1,2,3-Trichlorobenzene ug/L 50 54.3 109 70-135 1,2,3-Trichloropropane ug/L 50 56.1 112 70-130 1,2,4-Trichlorobenzene ug/L 50 55.7 111 70-134 1,2-Dibromo-3-chloropropane ug/L 50 52.5 105 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.5 109 70-130 1,2-Dichlorobenzene ug/L 50 55.1 110 70-130 1,2-Dichloroethane ug/L 50 52.4 105 70-130 1,2-Dichloropropane ug/L 50 59.4 119 70-130 1,3-Dichlorobenzene ug/L 50 54.0 108 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 62 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 LABORATORY CONTROL SAMPLE: Parameter 1051889 Units Spike Conc. LCS Result 1,3-Dichloropropane ug/L 50 57.0 1,4-Dichlorobenzene ug/L 50 53.9 2,2-Dichloropropane ug/L 50 44.8 2-Butanone (MEK) ug/L 100 120 2-Chlorotoluene ug/L 50 55.5 2-Hexanone ug/L 100 114 4-Chlorotoluene ug/L 50 57.0 4-Methyl-2-pentanone (MIBK) ug/L 100 116 Acetone ug/L 100 106 Benzene ug/L 50 56.3 Bromobenzene ug/L 50 54.4 Bromochloromethane ug/L 50 53.1 Bromodichloromethane ug/L 50 55.5 Bromoform ug/L 50 52.2 Bromomethane ug/L 50 50.1 Carbon tetrachloride ug/L 50 52.9 Chlorobenzene ug/L 50 52.7 Chloroethane ug/L 50 55.5 Chloroform ug/L 50 55.1 Chloromethane ug/L 50 49.2 cis-1,2-Dichloroethene ug/L 50 53.6 cis-1,3-Dichloropropene ug/L 50 57.9 Dibromochloromethane ug/L 50 52.2 Dibromomethane ug/L 50 52.8 Dichlorodifluoromethane ug/L 50 53.2 Diisopropyl ether ug/L 50 60.1 Ethylbenzene ug/L 50 50.6 Hexachloro-1,3-butadiene ug/L 50 49.2 m&p-Xylene ug/L 100 104 Methyl-tert-butyl ether ug/L 50 58.3 Methylene Chloride ug/L 50 54.5 Naphthalene ug/L 50 55.1 o-Xylene ug/L 50 56.2 p-Isopropyltoluene ug/L 50 55.9 Styrene ug/L 50 53.2 Tetrachloroethene ug/L 50 52.7 Toluene ug/L 50 54.3 trans-1,2-Dichloroethene ug/L 50 55.6 trans- 1,3-Dichloropropene ug/L 50 60.4 Trichloroethene ug/L 50 54.4 Trichlorofluoromethane ug/L 50 52.1 Vinyl acetate ug/L 100 111 Vinyl chloride ug/L 50 49.2 Xylene (Total) ug/L 150 160 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Date: 09/27/2013 09:01 AM LCS % Rec % Rec Limits 114 70-130 108 70-130 90 58-145 120 70-145 111 70-130 114 70-144 114 70-130 116 70-140 106 50-175 113 70-130 109 70-130 106 70-130 111 70-130 104 70-130 100 54-130 106 70-132 105 70-130 111 64-134 110 70-130 98 64-130 107 70-131 116 70-130 104 70-130 106 70-131 106 56-130 120 70-130 101 70-130 98 70-130 104 70-130 117 70-130 109 63-130 110 70-138 112 70-130 112 70-130 106 70-130 105 70-130 109 70-130 111 70-130 121 70-132 109 70-130 104 62-133 111 66-157 98 69-130 107 70-130 103 70-130 96 70-130 102 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 63 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052120 1052121 MS MSD 92172207013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 59.1 68.3 118 137 70-166 14 30 Benzene ug/L ND 50 50 55.2 63.1 110 126 70-148 13 30 Chlorobenzene ug/L ND 50 50 50.2 57.1 100 114 70-146 13 30 Toluene ug/L ND 50 50 49.6 57.2 99 114 70-155 14 30 Trichloroethene ug/L ND 50 50 54.7 64.0 109 127 69-151 16 30 1,2-Dichloroethane-d4(S) % 94 96 70-130 4-Bromofluorobenzene (S) % 99 99 70-130 Toluene-d8(S) % 97 98 70-130 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 64 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 QC Batch: MSV/24318 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92172207018, 92172207019, 92172207020, 92172207021, 92172207022, 92172207024, 92172207029 METHOD BLANK: 1051890 Matrix: Water Associated Lab Samples: 92172207018, 92172207019, 92172207020, 92172207021, 92172207022, 92172207024, 92172207029 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/23/13 00:53 1,1,1-Trichloroethane ug/L ND 1.0 09/23/13 00:53 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/23/13 00:53 1,1,2-Trichloroethane ug/L ND 1.0 09/23/13 00:53 1,1-Dichloroethane ug/L ND 1.0 09/23/13 00:53 1,1-Dichloroethene ug/L ND 1.0 09/23/13 00:53 1,1-Dichloropropene ug/L ND 1.0 09/23/13 00:53 1,2,3-Trichlorobenzene ug/L ND 1.0 09/23/13 00:53 1,2,3-Trichloropropane ug/L ND 1.0 09/23/13 00:53 1,2,4-Trichlorobenzene ug/L ND 1.0 09/23/13 00:53 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/23/13 00:53 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/23/13 00:53 1,2-Dichlorobenzene ug/L ND 1.0 09/23/13 00:53 1,2-Dichloroethane ug/L ND 1.0 09/23/13 00:53 1,2-Dichloropropane ug/L ND 1.0 09/23/13 00:53 1,3-Dichlorobenzene ug/L ND 1.0 09/23/13 00:53 1,3-Dichloropropane ug/L ND 1.0 09/23/13 00:53 1,4-Dichlorobenzene ug/L ND 1.0 09/23/13 00:53 2,2-Dichloropropane ug/L ND 1.0 09/23/13 00:53 2-Butanone (MEK) ug/L ND 5.0 09/23/13 00:53 2-Chlorotoluene ug/L ND 1.0 09/23/13 00:53 2-Hexanone ug/L ND 5.0 09/23/13 00:53 4-Chlorotoluene ug/L ND 1.0 09/23/13 00:53 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/23/13 00:53 Acetone ug/L ND 25.0 09/23/13 00:53 Benzene ug/L ND 1.0 09/23/13 00:53 Bromobenzene ug/L ND 1.0 09/23/13 00:53 Bromochloromethane ug/L ND 1.0 09/23/13 00:53 Bromodichloromethane ug/L ND 1.0 09/23/13 00:53 Bromoform ug/L ND 1.0 09/23/13 00:53 Bromomethane ug/L ND 2.0 09/23/13 00:53 Carbon tetrachloride ug/L ND 1.0 09/23/13 00:53 Chlorobenzene ug/L ND 1.0 09/23/13 00:53 Chloroethane ug/L ND 1.0 09/23/13 00:53 Chloroform ug/L ND 1.0 09/23/13 00:53 Chloromethane ug/L ND 1.0 09/23/13 00:53 cis-1,2-Dichloroethene ug/L ND 1.0 09/23/13 00:53 cis-1,3-Dichloropropene ug/L ND 1.0 09/23/13 00:53 Dibromochloromethane ug/L ND 1.0 09/23/13 00:53 Dibromomethane ug/L ND 1.0 09/23/13 00:53 Dichlorodifluoromethane ug/L ND 1.0 09/23/13 00:53 Diisopropyl ether ug/L ND 1.0 09/23/13 00:53 Ethylbenzene ug/L ND 1.0 09/23/13 00:53 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 65 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 METHOD BLANK: 1051890 Matrix: Water Associated Lab Samples: 92172207018, 92172207019, 92172207020, 92172207021, 92172207022, 92172207024, 92172207029 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0 09/23/13 00:53 m&p-Xylene ug/L ND 2.0 09/23/13 00:53 Methyl-tert-butyl ether ug/L ND 1.0 09/23/13 00:53 Methylene Chloride ug/L ND 2.0 09/23/13 00:53 Naphthalene ug/L ND 1.0 09/23/13 00:53 o-Xylene ug/L ND 1.0 09/23/13 00:53 p-Isopropyltoluene ug/L ND 1.0 09/23/13 00:53 Styrene ug/L ND 1.0 09/23/13 00:53 Tetrachloroethene ug/L ND 1.0 09/23/13 00:53 Toluene ug/L ND 1.0 09/23/13 00:53 trans-1,2-Dichloroethene ug/L ND 1.0 09/23/13 00:53 trans- 1,3-Dichloropropene ug/L ND 1.0 09/23/13 00:53 Trichloroethene ug/L ND 1.0 09/23/13 00:53 Trichlorofluoromethane ug/L ND 1.0 09/23/13 00:53 Vinyl acetate ug/L ND 2.0 09/23/13 00:53 Vinyl chloride ug/L ND 1.0 09/23/13 00:53 Xylene (Total) ug/L ND 2.0 09/23/13 00:53 1,2-Dichloroethane-d4 (S) % 103 70-130 09/23/13 00:53 4-Bromofluorobenzene (S) % 99 70-130 09/23/13 00:53 Toluene-d8 (S) % 97 70-130 09/23/13 00:53 LABORATORY CONTROL SAMPLE: 1051891 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.9 104 70-130 1,1,1-Trichloroethane ug/L 50 50.9 102 70-130 1,1,2,2-Tetrachloroethane ug/L 50 52.9 106 70-130 1,1,2-Trichloroethane ug/L 50 53.9 108 70-130 1,1-Dichloroethane ug/L 50 51.5 103 70-130 1,1-Dichloroethene ug/L 50 53.8 108 70-132 1,1-Dichloropropene ug/L 50 55.7 111 70-130 1,2,3-Trichlorobenzene ug/L 50 55.7 111 70-135 1,2,3-Trichloropropane ug/L 50 57.6 115 70-130 1,2,4-Trichlorobenzene ug/L 50 56.8 114 70-134 1,2-Dibromo-3-chloropropane ug/L 50 54.0 108 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.2 108 70-130 1,2-Dichlorobenzene ug/L 50 56.0 112 70-130 1,2-Dichloroethane ug/L 50 50.5 101 70-130 1,2-Dichloropropane ug/L 50 58.0 116 70-130 1,3-Dichlorobenzene ug/L 50 53.4 107 70-130 1,3-Dichloropropane ug/L 50 57.1 114 70-130 1,4-Dichlorobenzene ug/L 50 53.5 107 70-130 2,2-Dichloropropane ug/L 50 40.7 81 58-145 2-Butanone (MEK) ug/L 100 131 131 70-145 2-Chlorotoluene ug/L 50 53.9 108 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 66 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 LABORATORY CONTROL SAMPLE: Parameter 1051891 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2-Hexanone ug/L 100 119 119 70-144 4-Chlorotoluene ug/L 50 55.3 111 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 117 117 70-140 Acetone ug/L 100 108 108 50-175 Benzene ug/L 50 53.9 108 70-130 Bromobenzene ug/L 50 53.1 106 70-130 Bromochloromethane ug/L 50 52.3 105 70-130 Bromodichloromethane ug/L 50 52.0 104 70-130 Bromoform ug/L 50 52.4 105 70-130 Bromomethane ug/L 50 46.8 94 54-130 Carbon tetrachloride ug/L 50 47.9 96 70-132 Chlorobenzene ug/L 50 52.4 105 70-130 Chloroethane ug/L 50 47.2 94 64-134 Chloroform ug/L 50 53.3 107 70-130 Chloromethane ug/L 50 50.3 101 64-130 cis-1,2-Dichloroethene ug/L 50 53.1 106 70-131 cis-1,3-Dichloropropene ug/L 50 55.1 110 70-130 Dibromochloromethane ug/L 50 51.4 103 70-130 Dibromomethane ug/L 50 51.2 102 70-131 Dichlorodifluoromethane ug/L 50 42.3 85 56-130 Diisopropyl ether ug/L 50 60.1 120 70-130 Ethylbenzene ug/L 50 49.9 100 70-130 Hexachloro-1,3-butadiene ug/L 50 51.3 103 70-130 m&p-Xylene ug/L 100 104 104 70-130 Methyl-tert-butyl ether ug/L 50 56.5 113 70-130 Methylene Chloride ug/L 50 56.7 113 63-130 Naphthalene ug/L 50 57.1 114 70-138 o-Xylene ug/L 50 55.7 111 70-130 p-Isopropyltoluene ug/L 50 54.0 108 70-130 Styrene ug/L 50 53.0 106 70-130 Tetrachloroethene ug/L 50 52.1 104 70-130 Toluene ug/L 50 52.5 105 70-130 trans-1,2-Dichloroethene ug/L 50 53.3 107 70-130 trans- 1,3-Dichloropropene ug/L 50 57.9 116 70-132 Trichloroethene ug/L 50 51.3 103 70-130 Trichlorofluoromethane ug/L 50 44.0 88 62-133 Vinyl acetate ug/L 100 108 108 66-157 Vinyl chloride ug/L 50 45.1 90 69-130 Xylene (Total) ug/L 150 159 106 70-130 1,2-Dichloroethane-d4 (S) % 92 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8(S) % 101 70-130 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 67 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052113 1052114 MS MSD 92172207019 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 62.5 61.5 125 123 70-166 2 30 Benzene ug/L ND 50 50 59.5 59.5 119 119 70-148 0 30 Chlorobenzene ug/L ND 50 50 55.7 54.9 111 110 70-146 1 30 Toluene ug/L ND 50 50 53.7 53.6 107 107 70-155 0 30 Trichloroethene ug/L ND 50 50 59.8 59.6 120 119 69-151 0 30 1,2-Dichloroethane-d4(S) % 97 98 70-130 4-Bromofluorobenzene (S) % 100 99 70-130 Toluene-d8(S) % 97 99 70-130 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 68 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 QC Batch: MSV/24329 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92172207023 METHOD BLANK: 1052252 Matrix: Water Associated Lab Samples: 92172207023 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/23/13 14:42 1,1,1-Trichloroethane ug/L ND 1.0 09/23/13 14:42 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/23/13 14:42 1,1,2-Trichloroethane ug/L ND 1.0 09/23/13 14:42 1,1-Dichloroethane ug/L ND 1.0 09/23/13 14:42 1,1-Dichloroethene ug/L ND 1.0 09/23/13 14:42 1,1-Dichloropropene ug/L ND 1.0 09/23/13 14:42 1,2,3-Trichlorobenzene ug/L ND 1.0 09/23/13 14:42 1,2,3-Trichloropropane ug/L ND 1.0 09/23/13 14:42 1,2,4-Trichlorobenzene ug/L ND 1.0 09/23/13 14:42 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/23/13 14:42 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/23/13 14:42 1,2-Dichlorobenzene ug/L ND 1.0 09/23/13 14:42 1,2-Dichloroethane ug/L ND 1.0 09/23/13 14:42 1,2-Dichloropropane ug/L ND 1.0 09/23/13 14:42 1,3-Dichlorobenzene ug/L ND 1.0 09/23/13 14:42 1,3-Dichloropropane ug/L ND 1.0 09/23/13 14:42 1,4-Dichlorobenzene ug/L ND 1.0 09/23/13 14:42 2,2-Dichloropropane ug/L ND 1.0 09/23/13 14:42 2-Butanone (MEK) ug/L ND 5.0 09/23/13 14:42 2-Chlorotoluene ug/L ND 1.0 09/23/13 14:42 2-Hexanone ug/L ND 5.0 09/23/13 14:42 4-Chlorotoluene ug/L ND 1.0 09/23/13 14:42 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/23/13 14:42 Acetone ug/L ND 25.0 09/23/13 14:42 Benzene ug/L ND 1.0 09/23/13 14:42 Bromobenzene ug/L ND 1.0 09/23/13 14:42 Bromochloromethane ug/L ND 1.0 09/23/13 14:42 Bromodichloromethane ug/L ND 1.0 09/23/13 14:42 Bromoform ug/L ND 1.0 09/23/13 14:42 Bromomethane ug/L ND 2.0 09/23/13 14:42 Carbon tetrachloride ug/L ND 1.0 09/23/13 14:42 Chlorobenzene ug/L ND 1.0 09/23/13 14:42 Chloroethane ug/L ND 1.0 09/23/13 14:42 Chloroform ug/L ND 1.0 09/23/13 14:42 Chloromethane ug/L ND 1.0 09/23/13 14:42 cis-1,2-Dichloroethene ug/L ND 1.0 09/23/13 14:42 cis-1,3-Dichloropropene ug/L ND 1.0 09/23/13 14:42 Dibromochloromethane ug/L ND 1.0 09/23/13 14:42 Dibromomethane ug/L ND 1.0 09/23/13 14:42 Dichlorodifluoromethane ug/L ND 1.0 09/23/13 14:42 Diisopropyl ether ug/L ND 1.0 09/23/13 14:42 Ethylbenzene ug/L ND 1.0 09/23/13 14:42 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 69 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 METHOD BLANK: 1052252 Matrix: Water Associated Lab Samples: 92172207023 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0 09/23/13 14:42 m&p-Xylene ug/L ND 2.0 09/23/13 14:42 Methyl-tert-butyl ether ug/L ND 1.0 09/23/13 14:42 Methylene Chloride ug/L ND 2.0 09/23/13 14:42 Naphthalene ug/L ND 1.0 09/23/13 14:42 o-Xylene ug/L ND 1.0 09/23/13 14:42 p-Isopropyltoluene ug/L ND 1.0 09/23/13 14:42 Styrene ug/L ND 1.0 09/23/13 14:42 Tetrachloroethene ug/L ND 1.0 09/23/13 14:42 Toluene ug/L ND 1.0 09/23/13 14:42 trans-1,2-Dichloroethene ug/L ND 1.0 09/23/13 14:42 trans- 1,3-Dichloropropene ug/L ND 1.0 09/23/13 14:42 Trichloroethene ug/L ND 1.0 09/23/13 14:42 Trichlorofluoromethane ug/L ND 1.0 09/23/13 14:42 Vinyl acetate ug/L ND 2.0 09/23/13 14:42 Vinyl chloride ug/L ND 1.0 09/23/13 14:42 Xylene (Total) ug/L ND 2.0 09/23/13 14:42 1,2-Dichloroethane-d4 (S) % 86 70-130 09/23/13 14:42 4-Bromofluorobenzene (S) % 100 70-130 09/23/13 14:42 Toluene-d8 (S) % 99 70-130 09/23/13 14:42 LABORATORY CONTROL SAMPLE: 1052253 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.0 108 70-130 1,1,1-Trichloroethane ug/L 50 53.5 107 70-130 1,1,2,2-Tetrachloroethane ug/L 50 54.5 109 70-130 1,1,2-Trichloroethane ug/L 50 55.3 111 70-130 1,1-Dichloroethane ug/L 50 58.3 117 70-130 1,1-Dichloroethene ug/L 50 58.5 117 70-132 1,1-Dichloropropene ug/L 50 60.9 122 70-130 1,2,3-Trichlorobenzene ug/L 50 56.0 112 70-135 1,2,3-Trichloropropane ug/L 50 57.9 116 70-130 1,2,4-Trichlorobenzene ug/L 50 58.2 116 70-134 1,2-Dibromo-3-chloropropane ug/L 50 51.3 103 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.9 110 70-130 1,2-Dichlorobenzene ug/L 50 55.3 111 70-130 1,2-Dichloroethane ug/L 50 52.3 105 70-130 1,2-Dichloropropane ug/L 50 60.6 121 70-130 1,3-Dichlorobenzene ug/L 50 53.9 108 70-130 1,3-Dichloropropane ug/L 50 58.4 117 70-130 1,4-Dichlorobenzene ug/L 50 54.1 108 70-130 2,2-Dichloropropane ug/L 50 59.8 120 58-145 2-Butanone (MEK) ug/L 100 135 135 70-145 2-Chlorotoluene ug/L 50 54.4 109 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 70 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 LABORATORY CONTROL SAMPLE: Parameter 1052253 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2-Hexanone ug/L 100 123 123 70-144 4-Chlorotoluene ug/L 50 56.4 113 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 120 120 70-140 Acetone ug/L 100 114 114 50-175 Benzene ug/L 50 57.2 114 70-130 Bromobenzene ug/L 50 53.6 107 70-130 Bromochloromethane ug/L 50 53.8 108 70-130 Bromodichloromethane ug/L 50 53.8 108 70-130 Bromoform ug/L 50 53.6 107 70-130 Bromomethane ug/L 50 48.3 97 54-130 Carbon tetrachloride ug/L 50 50.1 100 70-132 Chlorobenzene ug/L 50 53.6 107 70-130 Chloroethane ug/L 50 52.5 105 64-134 Chloroform ug/L 50 55.8 112 70-130 Chloromethane ug/L 50 49.2 98 64-130 cis-1,2-Dichloroethene ug/L 50 56.8 114 70-131 cis-1,3-Dichloropropene ug/L 50 60.7 121 70-130 Dibromochloromethane ug/L 50 52.6 105 70-130 Dibromomethane ug/L 50 52.2 104 70-131 Dichlorodifluoromethane ug/L 50 53.5 107 56-130 Diisopropyl ether ug/L 50 63.6 127 70-130 Ethylbenzene ug/L 50 51.9 104 70-130 Hexachloro-1,3-butadiene ug/L 50 51.4 103 70-130 m&p-Xylene ug/L 100 108 108 70-130 Methyl-tert-butyl ether ug/L 50 59.6 119 70-130 Methylene Chloride ug/L 50 57.8 116 63-130 Naphthalene ug/L 50 55.4 111 70-138 o-Xylene ug/L 50 57.0 114 70-130 p-Isopropyltoluene ug/L 50 55.2 110 70-130 Styrene ug/L 50 55.4 111 70-130 Tetrachloroethene ug/L 50 54.8 110 70-130 Toluene ug/L 50 54.7 109 70-130 trans-1,2-Dichloroethene ug/L 50 57.5 115 70-130 trans- 1,3-Dichloropropene ug/L 50 63.2 126 70-132 Trichloroethene ug/L 50 54.0 108 70-130 Trichlorofluoromethane ug/L 50 47.9 96 62-133 Vinyl acetate ug/L 100 123 123 66-157 Vinyl chloride ug/L 50 52.6 105 69-130 Xylene (Total) ug/L 150 165 110 70-130 1,2-Dichloroethane-d4 (S) % 89 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 100 70-130 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 71 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052664 1052665 MS MSD 92172395042 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 68.6 75.7 137 151 70-166 10 30 Benzene ug/L ND 50 50 53.4 58.5 107 117 70-148 9 30 Chlorobenzene ug/L ND 50 50 51.8 56.0 104 112 70-146 8 30 Toluene ug/L ND 50 50 50.6 54.8 101 110 70-155 8 30 Trichloroethene ug/L ND 50 50 55.7 61.2 111 122 69-151 9 30 1,2-Dichloroethane-d4(S) % 97 98 70-130 4-Bromofluorobenzene (S) % 101 99 70-130 Toluene-d8(S) % 98 99 70-130 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 72 of 78 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 73 of 78 qD aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172207 Lab ID Sample ID QC Batch Method QC Batch 92172207001 MW-5 EPA 8260 MSV/24317 92172207002 MW-6 EPA 8260 MSV/24317 92172207003 MW-7 EPA 8260 MSV/24317 92172207004 MW-9 EPA 8260 MSV/24317 92172207005 MW-10 EPA 8260 MSV/24317 92172207006 MW-11 EPA 8260 MSV/24317 92172207007 MW-12 EPA 8260 MSV/24317 92172207008 MW-13 EPA 8260 MSV/24317 92172207009 MW-14 EPA 8260 MSV/24317 92172207010 MW-15 EPA 8260 MSV/24317 92172207011 MW-16 EPA 8260 MSV/24317 92172207012 MW-17 EPA 8260 MSV/24317 92172207013 MW-18 EPA 8260 MSV/24317 92172207014 MW-20 EPA 8260 MSV/24317 92172207015 MW-21 EPA 8260 MSV/24317 92172207016 MW-22 EPA 8260 MSV/24317 92172207017 MW-23 EPA 8260 MSV/24317 92172207018 MW-24 EPA 8260 MSV/24318 92172207019 MW-26 EPA 8260 MSV/24318 92172207020 RW-1 EPA 8260 MSV/24318 92172207021 RW-3 EPA 8260 MSV/24318 92172207022 RW-5 EPA 8260 MSV/24318 92172207023 RW-6 EPA 8260 MSV/24329 92172207024 RW-7 EPA 8260 MSV/24318 92172207026 FIELD BLANK 9/11 EPA 8260 MSV/24317 92172207028 FIELD BLANK 9/13 EPA 8260 MSV/24317 92172207029 DUPLICATE EPA 8260 MSV/24318 92172207030 TRIP BLANK EPA 8260 MSV/24317 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Page 74 of 78 F o V lOelul saldweS J N NN CD (D Z O Z O _ z z O �, (N/.� JaI000 paleaS 0 O •` a J 1polsn0 I y a ®. co w uo paAiaOab F (N/l.) auuoMO lenplsa�j \61 [—I m >- D ¢ J 0. ul dwal y Z uj fj O U C7 Z w J } c LLi ti wU. w Lu a 0 o (0 a O v M 0 CD Z J a: W � Z N N O H � cr Q nf 'L sf OPMU 6 q ^ R 3 m on t N /A t }sal SISAIeuV t �a41034w \� � \, loueufaw a l £OZSZeN HOeN 1 IOH Y, EONH o z # 'OSZH v c. 0 m 0 0 W > panjasajdufl S2i3NIV1N00 d0 # t2M r%A & m :y M avi o z N_¢ o U -ao ¢ " ` W j w w N0110311001V dN31 3ldNVS w t U .�..J ~ m N a (a Q 6 �i Q f `o z z d z w M C� N� p M N, M ene ❑ LLJ w ¢ o te1 r N N N e W Q �- Z z Z W Ni 4i S' S' Ct Qi s' O z a rn M J o E W 1 U LL a N oQ a F 0. m O ¢ W E �dN00=0 aVa0=0) 3d.11 3ldNVS d V _ oZ Ci Z U o J (gaj Ol sapOO pgeA aas) 3400 XIb1VW o _ —J :>>a��o>>�v w 0>> (n 0 F-- 0 oa r 3 0 T m z>�> N - N < O N ry W K X ®� " m Q Y O O V C c0 N L '- 0 O�� d U) 0 ¢ F O J U F Z D W 0 Z O U f 1 w Q W\ m J Z 0 �,\ a J �co O (L '= aC) o e 3 co j f7 w _ Pa e 75 of 78 # W31l N M V N t0 1 CO 01 fn Q' U ¢ w 6. cN- 4 y J CO 31 (N/A) joelul saldweS 1V Z CDO Z F- Y LU Z = y Z `o Q O ,a O O U Jaloo0 paIeaS Apoasn0 a w a) \ f� a �J (n (NA) aol co l w uo panlaoaa F- < (N/.l) OUPONO lenplsaa 3o ul dwal rn EL > U W� z 0 QQ U CD If y Z F F w w cn 2' C7 a lil._. v c .�. 3 Q J ' to O W 0 S a o 9 OO)Z$ 11 AWA s< x x X W m 1 N /A t ;sal SISAleuyt w V h �a4f0 loueyfan w a £OzSzeN a HOeN m IOH 4l DC oC X �d o i m �5/ , t £ONH I v l aim r� E° a d bOSzH U� o �o •o¢ Z m i 6a o a m mo w •:)3 pa/uasaadun Sb3NIV1N00 d0 #MC1 M M M 0 a 2 c� ¢ ab a Sn w NOIlO3ll001V dW313ldWVS H J w w afl z y 2 2 W o p p p N p fl O ee1 O � p¢ cVJ s Q E It W t= S`' M M P M M M M 0 ow o D r D O o !r O M M _n M Q z � z c� w fi fi" !T 16' 4r a w a rn M o U ~ J N - y O °� a oN m w O O Q W ELnn o O Z (dAOO=O 9VN9=`J) 3dA13ldWVS 2—d Z (gad oa sapoo pl�en aas) 3(]OO XRilVW +" m a o O E E —a 0 O= O T U N N W> a> Q N N N fn It Df O U 3 a 2a a N N •o o O U // p�� V _ L x C 'nO 9s (0 N - ¢Fw ` DoaO N F- z w w J p Z o U c V w o W; m J z Q �j �` c o aaj O � - Q U fl wA E o E a C~ �w a \5E P ge76of78 #W311 N w K 6 w Q ;oe;ul saldweS J N M M CD z 6 z Y z = � Z Q ~O o O 301000 paleas Rpo;sn0 o d w J (N/A) aol r-- ).._._ m a Q w y uo panlaoaa (N/A) auuolUO lenplsab � Oo ui dwal a Z LU L 0 of w i O c w — w c10i ti w Q v M U. 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V N � z s LLI D 0 LU E N z O .. , ..-z o W m Z "Y 0 c d V 0 �._ C w w fq # Mil N M v M w C) a W o_ P ge 77 of 78 Document Name: Sample Condition Upon Document Revised: June 4, 2013 . aeeAnalytical' 'Receipt (SCUR) Page 1 of 2 Document No.: Issuing Authorities: F-ASV-CS-003-rev.11 Pace Asheville Quality Office Client Name: Where Received: ❑ Huntersville Ashevillll�e Eden ❑ Raleigh Courier (Circle): Fed Ex UPS USPS Clierlt Commercial Pace Other Custody Seal on Cooler/Box Present: 7yes no Seals intact: yes Z no Packing Material: Bubble Wrap .7r Bubble Bags None Other Circle Thermometer Used: IR un#3 - � 265963 Type of Ice: W E Blue None Samples on ice, cooling process has begun IR Gun #`2-t 80344039 y Tmmn CnrrPrtinn Factor: Add / S�fbn r't act;l /( / C Corrected Cooler Temp.: ` C Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes No N/A Comments: Date and Ini ' f person ex? ng contents:' Chain of Custody Present: Yes I] No ❑N/A 1. Chain of Custody Filled Out: 9'Kes ❑No ❑N/A 2. Chain of Custody Relinquished: Gres ONo ❑N/A 3. Sampler Name & Signature on COC: LXes ❑No ❑N/A 4. Samples,Arrived within Hold Time: DKe. ON. ❑N/A 5. Short Hold Time Analysis (<72hr): ❑Yes Zo ❑N/A 6. Rush Turn Around Time Requested: ❑Yes -:;[No ❑N/A 7. Sufficient Volume: ZYes ❑No ❑WA 8. Correct Containers Used: -Pace Containers Used: JJYes 4E Yes []No ❑No ❑N/A ❑N/A 9. Containers Intact: C216s ❑No ❑N/A 10. Filtered volume received for Dissolved tests ❑Yes ❑No ❑NYA 11. Sample Labels match COO: -Includes date/time/ID/Analysis Matrix: _21es ❑No El N/A 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exception§r O boliform, TOC, O&G, WI-DRO (water) �' Af Yes -EJYes rUYes []No ❑No []No ❑N/A ❑N/A 13. Samples c ecked for dechlorination: ❑Yes ❑No rJN/A 14. Headspace in VOA Vials ( >6mm): ❑Yes Jo ❑N/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): &Yes ❑ ees ❑No ❑No ❑N/A ❑N/A 16. Client Notification/ Resolution: Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: / /i�_ Z% I Date: SRF Review:1 12 Z__ iDate: I IV & Note: Whenever there is a discrepancy affecting No h Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) Field Data Required? Y / N Page 78 of 78 qD aceAnalytical —pacelabs.com September 27, 2013 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 Eden, NC 27288 (336)623-8921 RE: Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Dear Mr. Alexander: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 16, 2013. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton for Tom Williams tom.williams@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE SUMMARY Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Lab ID Sample ID Matrix Date Collected Date Received 92172214001 MW-5 Water 09/12/13 10:45 09/16/13 09:00 92172214002 MW-6 Water 09/13/13 10:15 09/16/13 09:00 92172214003 MW-7 Water 09/11/13 11:20 09/16/13 09:00 92172214004 MW-9 Water 09/11/13 13:00 09/16/13 09:00 92172214005 MW-10 Water 09/12/13 12:45 09/16/13 09:00 92172214006 MW-11 Water 09/12/13 15:05 09/16/13 09:00 92172214007 MW-12 Water 09/12/13 10:00 09/16/13 09:00 92172214008 MW-13 Water 09/11/13 14:15 09/16/13 09:00 92172214009 MW-14 Water 09/11/13 15:30 09/16/13 09:00 92172214010 MW-24 Water 09/10/13 15:20 09/16/13 09:00 92172214011 RW-1 Water 09/13/13 09:50 09/16/13 09:00 92172214012 RW-3 Water 09/13/13 09:30 09/16/13 09:00 92172214013 RW-5 Water 09/13/13 10:30 09/16/13 09:00 92172214014 RW-6 Water 09/13/13 15:50 09/16/13 09:00 92172214015 RW-7 Water 09/13/13 11:20 09/16/13 09:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92172214001 MW-5 SM 5310B SAE 1 PASI-A 92172214002 MW-6 SM 5310B SAE 1 PASI-A 92172214003 MW-7 SM 5310B SAE 1 PASI-A 92172214004 MW-9 SM 5310B SAE 1 PASI-A 92172214005 MW-10 SM 5310B SAE 1 PASI-A 92172214006 MW-11 SM 5310B SAE 1 PASI-A 92172214007 MW-12 SM 5310B SAE 1 PASI-A 92172214008 MW-13 SM 5310B SAE 1 PASI-A 92172214009 MW-14 SM 5310B SAE 1 PASI-A 92172214010 MW-24 SM 5310B SAE 1 PASI-A 92172214011 RW-1 SM 5310B SAE 1 PASI-A 92172214012 RW-3 SM 5310B SAE 1 PASI-A 92172214013 RW-5 SM 5310B SAE 1 PASI-A 92172214014 RW-6 SM 5310B SAE 1 PASI-A 92172214015 RW-7 SM 5310B SAE 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5 Lab ID: 92172214001 Collected: 09/12/13 10:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 5.1 mg/L 1.0 1.0 1 09/25/13 21:40 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 Lab ID: 92172214002 Collected: 09/13/13 10:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 8.8 mg/L 1.0 1.0 1 09/25/13 21:51 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 Lab ID: 92172214003 Collected: 09/11/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.2 mg/L 1.0 1.0 1 09/25/13 22:07 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Lab ID: 92172214004 Collected: 09/11/13 13:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 31.2 mg/L 1.0 1.0 1 09/25/13 22:40 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-10 Lab ID: 92172214005 Collected: 09/12/13 12:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 12.1 mg/L 1.0 1.0 1 09/25/13 22:52 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11 Lab ID: 92172214006 Collected: 09/12/13 15:05 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.5 mg/L 1.0 1.0 1 09/25/13 23:05 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-12 Lab ID: 92172214007 Collected: 09/12/13 10:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 39.1 mg/L 2.0 2.0 2 09/26/13 11:43 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 Lab ID: 92172214008 Collected: 09/11/13 14:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.7 mg/L 1.0 1.0 1 09/26/13 00:19 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 Lab ID: 92172214009 Collected: 09/11/13 15:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.1 mg/L 1.0 1.0 1 09/26/13 00:32 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-24 Lab ID: 92172214010 Collected: 09/10/13 15:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.2 mg/L 1.0 1.0 1 09/26/13 00:47 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-1 Lab ID: 92172214011 Collected: 09/13/13 09:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 333 mg/L 20.0 20.0 20 09/26/13 01:00 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 15 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-3 Lab ID: 92172214012 Collected: 09/13/13 09:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 175 mg/L 20.0 20.0 20 09/26/13 01:12 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Sample: RW-5 Lab ID: 92172214013 Collected: 09/13/13 10:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1540 mg/L 50.0 50.0 50 09/26/13 02:33 7440-44-0 M6 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 17 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 Lab ID: 92172214014 Collected: 09/13/13 15:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 476 mg/L 50.0 50.0 50 09/26/13 03:05 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Lab ID: 92172214015 Collected: 09/13/13 11:20 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1490 mg/L 100 100 100 09/26/13 03:17 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 19 of 25 qD aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 QC Batch: WETA/16537 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92172214001, 92172214002, 92172214003, 92172214004, 92172214005, 92172214006, 92172214007, 92172214008,92172214009,92172214010,92172214011,92172214012 METHOD BLANK: 1052210 Matrix: Water Associated Lab Samples: 92172214001, 92172214002, 92172214003, 92172214004, 92172214005, 92172214006, 92172214007, 92172214008,92172214009,92172214010,92172214011,92172214012 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 10.0 09/25/13 18:25 LABORATORY CONTROL SAMPLE: 1052211 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 23.8 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052212 1052213 MS MSD 92172187001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 751 25 25 976 972 900 886 75-125 0 20 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052214 1052215 MS MSD 92172214003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 1.2 25 25 23.8 24.0 91 91 75-125 1 20 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 20 of 25 qD aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 QC Batch: WETA/16538 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92172214013, 92172214014, 92172214015 METHOD BLANK: 1052218 Matrix: Water Associated Lab Samples: 92172214013, 92172214014, 92172214015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 09/26/13 01:49 LABORATORY CONTROL SAMPLE: 1052219 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.2 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052220 1052221 MS MSD 92172214013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 1540 25 25 1520 1500 -114 -182 75-125 1 20 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052222 1052223 MS MSD 92172223008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 1.6 25 25 24.4 24.3 91 91 75-125 1 20 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 21 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 22 of 25 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172214 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92172214001 MW-5 SM 5310B WETA/16537 92172214002 MW-6 SM 5310B WETA/16537 92172214003 MW-7 SM 5310B WETA/16537 92172214004 MW-9 SM 5310B WETA/16537 92172214005 MW-10 SM 5310B WETA/16537 92172214006 MW-11 SM 5310B WETA/16537 92172214007 MW-12 SM 5310B WETA/16537 92172214008 MW-13 SM 5310B WETA/16537 92172214009 MW-14 SM 5310B WETA/16537 92172214010 MW-24 SM 5310B WETA/16537 92172214011 RW-1 SM 5310B WETA/16537 92172214012 RW-3 SM 5310B WETA/16537 92172214013 RW-5 SM 5310B WETA/16538 92172214014 RW-6 SM 5310B WETA/16538 92172214015 RW-7 SM 5310B WETA/16538 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Analytical Batch Page 23 of 25 N o m oo rn N A w ro ITEM # -o m a a o y (D a ;U (n y - O Cb o N o 3 i1 `tl 3 f� a' w ° z � � m p �' � � e`er m � n �. - - o z ❑ C 3� M m m N z ca l ow m c m m a m > l m oKo >o3i m ® co n 7 -b � n �IDm D0-1D Ocn�oN o 0 0 E.o Z f m m t 3 `0 �d p z m W NIN 3 1 MATRIX CODE (see valid codes to left) ►� t1 S® '� SAMPLE TYPE (G=GRAB C=COMP) A \, o c W m N j o rn m D m >& C < po N N m D D rn J m C) v m O r - r D r y ? 3 w W O _- N '- - z 0 �p D m a 3 D W w _ 1� w 4/ W W u1 w w .a o a Z W v` ^� .-y. rn z o N N N m m 0 N O 3 3 e^ 1 O O J� m 0 ii Z a v v D m SAMPLE TEMP AT COLLECTION o m m C r I — m C 'A — r N o_ n D -� N N N N N N# OF CONTAINERS v - v m ' o n 3 rn m o o O ' 3 o ❑ Unpreserved g c_ HzSO4 z p v c -< a HNO3 m m " HCI m z D 7 NaOH n a1 n NazS203 o, � ••h. m , M Methanol �` (� 0 )c h k m)f%X Other 17e, h v W N 3 CD jAnalysis Yest j v/ N j D OL s111 to = 3 y o m " D m CD 0 Co N v LP ii rr a z ❑ m O Q a D m 0 C O y n r' m :D en T ® 1 m m = (n 0 ° CD r m A m Z v Z D c 0 z .. y Tempin'C a Residual Chlorine (Y/N) D U) Received on D Ice (Y/N) o 6, o J Custody v r n � p O � (� 00 �n Sealed Cooler z tD .�'"d m Z 1 7 CO o o p Z N 0 r D J Samples Intact m (Y/N) ��° Pa e 24 of 25 Document Name: Sample Condition Upon Document Revised: June 4, 2013 Document No.: ' Issuing Authorities: www.ppcela4s. corm F-ASV-CS-003-rev.11 Pace Asheville Quality Office Client Name:' Where Received: ❑ Huntersville Asheville Eden Raleigh Courier (Circle): Fed Ex UPS USPS Clit Commercial Pace Other Custody Seal on Cooler/Box Present: M yes Let no Seals intact: yes 2/no Packing Material: Bubble Wrap Bubble Bags None Other Circle Thermometer Used: IR G -13 -65963 Type of Ice: V�Get Blue None Samples on ice, cooling process has begun IR Gun 2- 80344039 Temn Correction Factor: Add / Se�l , / C Corrected Cooler Temp.:_ C Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes No N/A 9 Comments: Date and Initial erson ex ' 1ng contents: Chain of Custody Present: es ❑No ❑N/A 1. Chain of Custody Filled Out: es ❑No ❑N/A 2. Chain of Custody Relinquished: _L�fres ❑No ❑N/A 3. Sampler Name & Signature on COC: es ❑No ❑N/A 4. Samples Arrived within Hold Time: lyres 1:1Noo ❑N/A 5. Short Hold Time Analysis (<72hr): ❑Yes 12110 ❑N/A 6. Rush Turn Around Time Requested: ❑Yes ,eNNo ❑N/A 7. Sufficient Volume: 2 es El No ❑N/A 8. Correct Containers Used: -Pace Containers Used: 0 res .�res ❑No El No ❑N/A ❑N/A 9. Containers Intact: -21 ,s ❑No El N/A 10. Filtered volume received for Dissolved tests ❑Yes ❑No ❑WX 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: s ❑No❑N/A 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: OA ' Worm, C O&G, WI-DRO (water) Yes pYes es ❑No ❑No ❑No ❑N/A ❑N!A 13. Samples checked for dechlonnation: ❑Yes ❑No Qr, (/A 14. Headspace in VOA Vials ( >6mm): ❑Yes LJNo ❑N/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): J2 es Ores [IN. ONo El N/A ❑N/A 16. Client Notification/ Resolution: Person Contacted: Comments/ Resolution: SCURF Review: Date: Date/Time: SRF Review: I i / Yl1L�._ _ Date: Note: Whenever there is a discrepancy affecting No h Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) Field Data Required? Y / N Page 25 of 25 qD aceAnalytical —pacelabs.com September 27, 2013 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 Eden, NC 27288 (336)623-8921 RE: Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Dear Mr. Alexander: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 16, 2013. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton for Tom Williams tom.williams@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE SUMMARY Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Lab ID Sample ID Matrix Date Collected Date Received 92172221001 BC-1 Water 09/13/13 13:50 09/16/13 09:00 92172221002 BC-2 Water 09/13/13 13:40 09/16/13 09:00 92172221003 BC-3 Water 09/13/13 13:30 09/16/13 09:00 92172221004 BC-4 Water 09/13/13 13:15 09/16/13 09:00 92172221005 BC-5 Water 09/13/13 13:00 09/16/13 09:00 92172221006 CS-1 Water 09/13/13 14:10 09/16/13 09:00 92172221007 CS-2 Water 09/13/13 14:00 09/16/13 09:00 92172221008 SM-1 Water 09/13/13 14:55 09/16/13 09:00 92172221009 SM-2 Water 09/13/13 14:50 09/16/13 09:00 92172221010 SM-3 Water 09/13/13 14:45 09/16/13 09:00 92172221011 SM-4 Water 09/13/13 14:40 09/16/13 09:00 92172221012 SM-5 Water 09/13/13 14:35 09/16/13 09:00 92172221013 SM-6 Water 09/13/13 14:30 09/16/13 09:00 92172221014 JW-1 Water 09/13/13 15:00 09/16/13 09:00 92172221015 TRIP BLANK Water 09/13/13 00:00 09/16/13 09:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92172221001 BC-1 EPA 8260 MCK 63 PASI-C 92172221002 BC-2 EPA 8260 MCK 63 PASI-C 92172221003 BC-3 EPA 8260 MCK 63 PASI-C 92172221004 BC-4 EPA 8260 MCK 63 PASI-C 92172221005 BC-5 EPA 8260 MCK 63 PASI-C 92172221006 CS-1 EPA 8260 MCK 63 PASI-C 92172221007 CS-2 EPA 8260 MCK 63 PASI-C 92172221008 SM-1 EPA 8260 MCK 63 PASI-C 92172221009 SM-2 EPA 8260 MCK 63 PASI-C 92172221010 SM-3 EPA 8260 MCK 63 PASI-C 92172221011 SM-4 EPA 8260 MCK 63 PASI-C 92172221012 SM-5 EPA 8260 MCK 63 PASI-C 92172221013 SM-6 EPA 8260 MCK 63 PASI-C 92172221014 JW-1 EPA 8260 MCK 63 PASI-C 92172221015 TRIP BLANK EPA 8260 MCK 63 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: BC-1 Lab ID: 92172221001 Collected: 09/13/13 13:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 19:19 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 19:19 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 19:19 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 19:19 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 19:19 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 19:19 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 19:19 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 19:19 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 19:19 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 19:19 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 19:19 75-00-3 Chloroform 0.46J ug/L 1.0 0.14 1 09/22/13 19:19 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 19:19 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 19:19 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 19:19 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 19:19 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 19:19 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 19:19 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 19:19 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 19:19 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 19:19 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 19:19 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 19:19 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 19:19 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 19:19 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 19:19 75-35-4 cis-1,2-Dichloroethene 15.8 ug/L 1.0 0.19 1 09/22/13 19:19 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 19:19 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 19:19 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 19:19 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 19:19 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 19:19 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 19:19 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 19:19 10061-02-6 Diisopropyl ether 0.33J ug/L 1.0 0.12 1 09/22/13 19:19 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 19:19 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 19:19 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 19:19 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 19:19 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 19:19 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 19:19 108-10-1 Methyl-tert-butyl ether 1.4 ug/L 1.0 0.21 1 09/22/13 19:19 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 19:19 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 19:19 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 19:19 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 19:19 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-1 Lab ID: 92172221001 Collected: 09/13/13 13:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 44.9 ug/L 1.0 0.46 1 09/22/13 19:19 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 19:19 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 19:19 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 19:19 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 19:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 19:19 79-00-5 Trichloroethene 5.0 ug/L 1.0 0.47 1 09/22/13 19:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 19:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 19:19 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 19:19 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 19:19 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 19:19 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 19:19 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 19:19 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/22/13 19:19 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 09/22/13 19:19 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/22/13 19:19 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: BC-2 Lab ID: 92172221002 Collected: 09/13/13 13:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 19:34 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 19:34 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 19:34 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 19:34 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 19:34 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 19:34 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 19:34 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 19:34 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 19:34 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 19:34 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 19:34 75-00-3 Chloroform 0.86J ug/L 1.0 0.14 1 09/22/13 19:34 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 19:34 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 19:34 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 19:34 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 19:34 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 19:34 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 19:34 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 19:34 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 19:34 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 19:34 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 19:34 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 19:34 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 19:34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 19:34 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 19:34 75-35-4 cis-1,2-Dichloroethene 10.7 ug/L 1.0 0.19 1 09/22/13 19:34 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 19:34 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 19:34 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 19:34 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 19:34 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 19:34 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 19:34 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 19:34 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 19:34 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 19:34 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 19:34 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 19:34 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 19:34 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 19:34 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 19:34 108-10-1 Methyl-tert-butyl ether 0.46J ug/L 1.0 0.21 1 09/22/13 19:34 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 19:34 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 19:34 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 19:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 19:34 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-2 Lab ID: 92172221002 Collected: 09/13/13 13:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 28.0 ug/L 1.0 0.46 1 09/22/13 19:34 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 19:34 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 19:34 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 19:34 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 19:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 19:34 79-00-5 Trichloroethene 3.5 ug/L 1.0 0.47 1 09/22/13 19:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 19:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 19:34 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 19:34 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 19:34 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 19:34 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 19:34 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 19:34 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 09/22/13 19:34 460-00-4 1,2-Dichloroethane-d4 (S) 112 % 70-130 1 09/22/13 19:34 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/22/13 19:34 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: BC-3 Lab ID: 92172221003 Collected: 09/13/13 13:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 19:50 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 19:50 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 19:50 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 19:50 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 19:50 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 19:50 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 19:50 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 19:50 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 19:50 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 19:50 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 19:50 75-00-3 Chloroform 1.1 ug/L 1.0 0.14 1 09/22/13 19:50 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 19:50 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 19:50 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 19:50 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 19:50 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 19:50 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 19:50 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 19:50 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 19:50 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 19:50 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 19:50 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 19:50 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 19:50 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 19:50 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 19:50 75-35-4 cis-1,2-Dichloroethene 3.1 ug/L 1.0 0.19 1 09/22/13 19:50 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 19:50 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 19:50 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 19:50 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 19:50 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 19:50 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 19:50 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 19:50 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 19:50 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 19:50 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 19:50 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 19:50 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 19:50 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 19:50 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 19:50 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/22/13 19:50 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 19:50 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 19:50 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 19:50 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 19:50 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-3 Lab ID: 92172221003 Collected: 09/13/13 13:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 4.9 ug/L 1.0 0.46 1 09/22/13 19:50 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 19:50 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 19:50 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 19:50 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 19:50 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 19:50 79-00-5 Trichloroethene 0.87J ug/L 1.0 0.47 1 09/22/13 19:50 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 19:50 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 19:50 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 19:50 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 19:50 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 19:50 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 19:50 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 19:50 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/22/13 19:50 460-00-4 1,2-Dichloroethane-d4 (S) 109 % 70-130 1 09/22/13 19:50 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/22/13 19:50 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: BC-4 Lab ID: 92172221004 Collected: 09/13/13 13:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 20:06 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 20:06 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 20:06 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 20:06 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 20:06 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 20:06 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 20:06 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 20:06 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 20:06 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 20:06 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 20:06 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 20:06 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 20:06 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 20:06 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 20:06 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 20:06 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 20:06 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 20:06 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 20:06 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 20:06 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 20:06 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:06 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 20:06 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 20:06 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 20:06 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 20:06 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 20:06 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 20:06 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 20:06 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 20:06 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 20:06 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 20:06 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 20:06 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 20:06 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 20:06 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 20:06 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 20:06 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 20:06 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 20:06 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 20:06 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 20:06 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/22/13 20:06 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 20:06 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 20:06 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 20:06 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 20:06 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-4 Lab ID: 92172221004 Collected: 09/13/13 13:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/22/13 20:06 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 20:06 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:06 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 20:06 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 20:06 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 20:06 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 20:06 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 20:06 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 20:06 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 20:06 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 20:06 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 20:06 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 20:06 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 20:06 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 09/22/13 20:06 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 09/22/13 20:06 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/22/13 20:06 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: BC-5 Lab ID: 92172221005 Collected: 09/13/13 13:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 20:22 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 20:22 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 20:22 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 20:22 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 20:22 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 20:22 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 20:22 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 20:22 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 20:22 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 20:22 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 20:22 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 20:22 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 20:22 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 20:22 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 20:22 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 20:22 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 20:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 20:22 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 20:22 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 20:22 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 20:22 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:22 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 20:22 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 20:22 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 20:22 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 20:22 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 20:22 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 20:22 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 20:22 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 20:22 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 20:22 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 20:22 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 20:22 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 20:22 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 20:22 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 20:22 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 20:22 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 20:22 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 20:22 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 20:22 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 20:22 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/22/13 20:22 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 20:22 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 20:22 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 20:22 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 20:22 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-5 Lab ID: 92172221005 Collected: 09/13/13 13:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/22/13 20:22 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 20:22 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:22 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 20:22 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 20:22 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 20:22 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 20:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 20:22 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 20:22 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 20:22 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 20:22 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 20:22 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 20:22 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 20:22 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/22/13 20:22 460-00-4 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 09/22/13 20:22 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/22/13 20:22 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: CS-1 Lab ID: 92172221006 Collected: 09/13/13 14:10 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 20:38 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 20:38 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 20:38 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 20:38 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 20:38 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 20:38 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 20:38 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 20:38 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 20:38 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 20:38 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 20:38 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 20:38 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 20:38 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 20:38 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 20:38 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 20:38 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 20:38 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 20:38 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 20:38 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 20:38 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 20:38 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:38 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 20:38 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 20:38 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 20:38 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 20:38 75-35-4 cis-1,2-Dichloroethene 4.2 ug/L 1.0 0.19 1 09/22/13 20:38 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 20:38 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 20:38 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 20:38 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 20:38 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 20:38 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 20:38 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 20:38 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 20:38 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 20:38 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 20:38 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 20:38 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 20:38 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 20:38 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 20:38 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/22/13 20:38 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 20:38 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 20:38 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 20:38 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 20:38 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 Lab ID: 92172221006 Collected: 09/13/13 14:10 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 17.6 ug/L 1.0 0.46 1 09/22/13 20:38 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 20:38 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:38 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 20:38 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 20:38 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 20:38 79-00-5 Trichloroethene 2.1 ug/L 1.0 0.47 1 09/22/13 20:38 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 20:38 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 20:38 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 20:38 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 20:38 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 20:38 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 20:38 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 20:38 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/22/13 20:38 460-00-4 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 09/22/13 20:38 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/22/13 20:38 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: CS-2 Lab ID: 92172221007 Collected: 09/13/13 14:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 20:54 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 20:54 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 20:54 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 20:54 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 20:54 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 20:54 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 20:54 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 20:54 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 20:54 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 20:54 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 20:54 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 20:54 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 20:54 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 20:54 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 20:54 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 20:54 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 20:54 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 20:54 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 20:54 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 20:54 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 20:54 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:54 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 20:54 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 20:54 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 20:54 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 20:54 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 20:54 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 20:54 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 20:54 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 20:54 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 20:54 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 20:54 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 20:54 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 20:54 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 20:54 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 20:54 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 20:54 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 20:54 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 20:54 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 20:54 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 20:54 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/22/13 20:54 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 20:54 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 20:54 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 20:54 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 20:54 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 Lab ID: 92172221007 Collected: 09/13/13 14:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 5.1 ug/L 1.0 0.46 1 09/22/13 20:54 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 20:54 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 20:54 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 20:54 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 20:54 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 20:54 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 20:54 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 20:54 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 20:54 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 20:54 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 20:54 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 20:54 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 20:54 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 20:54 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/22/13 20:54 460-00-4 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 09/22/13 20:54 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/22/13 20:54 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: SM-1 Lab ID: 92172221008 Collected: 09/13/13 14:55 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 21:10 67-64-1 Benzene 2.1 ug/L 1.0 0.25 1 09/22/13 21:10 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 21:10 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 21:10 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 21:10 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 21:10 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 21:10 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 21:10 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 21:10 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 21:10 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 21:10 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 21:10 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 21:10 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 21:10 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 21:10 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 21:10 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 21:10 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 21:10 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 21:10 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 21:10 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 21:10 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:10 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 21:10 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 21:10 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 21:10 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 21:10 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 21:10 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 21:10 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 21:10 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 21:10 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 21:10 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 21:10 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 21:10 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 21:10 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 21:10 108-20-3 Ethylbenzene 0.66J ug/L 1.0 0.30 1 09/22/13 21:10 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 21:10 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 21:10 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 21:10 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 21:10 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 21:10 108-10-1 Methyl-tert-butyl ether 10.6 ug/L 1.0 0.21 1 09/22/13 21:10 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 21:10 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 21:10 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 21:10 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 21:10 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-1 Lab ID: 92172221008 Collected: 09/13/13 14:55 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/22/13 21:10 127-18-4 Toluene 1.8 ug/L 1.0 0.26 1 09/22/13 21:10 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:10 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 21:10 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 21:10 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 21:10 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 21:10 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 21:10 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 21:10 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 21:10 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 21:10 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 21:10 1330-20-7 m&p-Xylene 1.9J ug/L 2.0 0.66 1 09/22/13 21:10 179601-23-1 o-Xylene 0.75J ug/L 1.0 0.23 1 09/22/13 21:10 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/22/13 21:10 460-00-4 1,2-Dichloroethane-d4 (S) 108 % 70-130 1 09/22/13 21:10 17060-07-0 Toluene-d8 (S) 96 % 70-130 1 09/22/13 21:10 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 20 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: SM-2 Lab ID: 92172221009 Collected: 09/13/13 14:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 21:26 67-64-1 Benzene 1.1 ug/L 1.0 0.25 1 09/22/13 21:26 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 21:26 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 21:26 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 21:26 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 21:26 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 21:26 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 21:26 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 21:26 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 21:26 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 21:26 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 21:26 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 21:26 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 21:26 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 21:26 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 21:26 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 21:26 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 21:26 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 21:26 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 21:26 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 21:26 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:26 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 21:26 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 21:26 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 21:26 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 21:26 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 21:26 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 21:26 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 21:26 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 21:26 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 21:26 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 21:26 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 21:26 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 21:26 10061-02-6 Diisopropyl ether 0.12J ug/L 1.0 0.12 1 09/22/13 21:26 108-20-3 Ethylbenzene 0.31J ug/L 1.0 0.30 1 09/22/13 21:26 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 21:26 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 21:26 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 21:26 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 21:26 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 21:26 108-10-1 Methyl-tert-butyl ether 8.5 ug/L 1.0 0.21 1 09/22/13 21:26 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 21:26 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 21:26 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 21:26 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 21:26 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-2 Lab ID: 92172221009 Collected: 09/13/13 14:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/22/13 21:26 127-18-4 Toluene 0.84J ug/L 1.0 0.26 1 09/22/13 21:26 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:26 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 21:26 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 21:26 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 21:26 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 21:26 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 21:26 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 21:26 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 21:26 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 21:26 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 21:26 1330-20-7 m&p-Xylene 0.94J ug/L 2.0 0.66 1 09/22/13 21:26 179601-23-1 o-Xylene 0.43J ug/L 1.0 0.23 1 09/22/13 21:26 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/22/13 21:26 460-00-4 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 09/22/13 21:26 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/22/13 21:26 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 22 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: SM-3 Lab ID: 92172221010 Collected: 09/13/13 14:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 21:42 67-64-1 Benzene 0.84J ug/L 1.0 0.25 1 09/22/13 21:42 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 21:42 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 21:42 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 21:42 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 21:42 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 21:42 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 21:42 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 21:42 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 21:42 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 21:42 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 21:42 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 21:42 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 21:42 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 21:42 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 21:42 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 21:42 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 21:42 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 21:42 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 21:42 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 21:42 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:42 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 21:42 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 21:42 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 21:42 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 21:42 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 21:42 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 21:42 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 21:42 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 21:42 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 21:42 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 21:42 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 21:42 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 21:42 10061-02-6 Diisopropyl ether 0.13J ug/L 1.0 0.12 1 09/22/13 21:42 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 21:42 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 21:42 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 21:42 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 21:42 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 21:42 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 21:42 108-10-1 Methyl-tert-butyl ether 8.0 ug/L 1.0 0.21 1 09/22/13 21:42 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 21:42 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 21:42 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 21:42 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 21:42 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-3 Lab ID: 92172221010 Collected: 09/13/13 14:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.53J ug/L 1.0 0.46 1 09/22/13 21:42 127-18-4 Toluene 0.66J ug/L 1.0 0.26 1 09/22/13 21:42 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:42 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 21:42 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 21:42 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 21:42 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 21:42 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 21:42 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 21:42 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 21:42 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 21:42 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 21:42 1330-20-7 m&p-Xylene 0.67J ug/L 2.0 0.66 1 09/22/13 21:42 179601-23-1 o-Xylene 0.31J ug/L 1.0 0.23 1 09/22/13 21:42 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/22/13 21:42 460-00-4 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 09/22/13 21:42 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 09/22/13 21:42 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: SM-4 Lab ID: 92172221011 Collected: 09/13/13 14:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 21:58 67-64-1 Benzene 0.32J ug/L 1.0 0.25 1 09/22/13 21:58 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 21:58 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 21:58 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 21:58 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 21:58 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 21:58 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 21:58 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 21:58 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 21:58 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 21:58 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 21:58 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 21:58 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 21:58 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 21:58 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 21:58 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 21:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 21:58 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 21:58 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 21:58 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 21:58 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:58 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 21:58 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 21:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 21:58 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 21:58 75-35-4 cis-1,2-Dichloroethene 0.34J ug/L 1.0 0.19 1 09/22/13 21:58 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 21:58 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 21:58 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 21:58 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 21:58 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 21:58 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 21:58 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 21:58 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 21:58 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 21:58 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 21:58 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 21:58 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 21:58 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 21:58 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 21:58 108-10-1 Methyl-tert-butyl ether 5.9 ug/L 1.0 0.21 1 09/22/13 21:58 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 21:58 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 21:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 21:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 21:58 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 25 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-4 Lab ID: 92172221011 Collected: 09/13/13 14:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.2 ug/L 1.0 0.46 1 09/22/13 21:58 127-18-4 Toluene 0.31J ug/L 1.0 0.26 1 09/22/13 21:58 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 21:58 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 21:58 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 21:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 21:58 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 21:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 21:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 21:58 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 21:58 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 21:58 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 21:58 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 21:58 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 21:58 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/22/13 21:58 460-00-4 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 09/22/13 21:58 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/22/13 21:58 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: SM-5 Lab ID: 92172221012 Collected: 09/13/13 14:35 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 22:14 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 22:14 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 22:14 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 22:14 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 22:14 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 22:14 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 22:14 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 22:14 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 22:14 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 22:14 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 22:14 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 22:14 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 22:14 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 22:14 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 22:14 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 22:14 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 22:14 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 22:14 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 22:14 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 22:14 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 22:14 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 22:14 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 22:14 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 22:14 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 22:14 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 22:14 75-35-4 cis-1,2-Dichloroethene 0.26J ug/L 1.0 0.19 1 09/22/13 22:14 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 22:14 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 22:14 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 22:14 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 22:14 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 22:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 22:14 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 22:14 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 22:14 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 22:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 22:14 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 22:14 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 22:14 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 22:14 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 22:14 108-10-1 Methyl-tert-butyl ether 5.4 ug/L 1.0 0.21 1 09/22/13 22:14 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 22:14 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 22:14 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 22:14 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 22:14 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 27 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-5 Lab ID: 92172221012 Collected: 09/13/13 14:35 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.2 ug/L 1.0 0.46 1 09/22/13 22:14 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 22:14 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 22:14 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 22:14 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 22:14 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 22:14 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 22:14 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 22:14 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 22:14 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 22:14 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 22:14 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 22:14 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 22:14 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 22:14 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/22/13 22:14 460-00-4 1,2-Dichloroethane-d4 (S) 116 % 70-130 1 09/22/13 22:14 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 09/22/13 22:14 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 28 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: SM-6 Lab ID: 92172221013 Collected: 09/13/13 14:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 22:30 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 22:30 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 22:30 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 22:30 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 22:30 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 22:30 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 22:30 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 22:30 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 22:30 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 22:30 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 22:30 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 22:30 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 22:30 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 22:30 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 22:30 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 22:30 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 22:30 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 22:30 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 22:30 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 22:30 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 22:30 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 22:30 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 22:30 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 22:30 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 22:30 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 22:30 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 22:30 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 22:30 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 22:30 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 22:30 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 22:30 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 22:30 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 22:30 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 22:30 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 22:30 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 22:30 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 22:30 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 22:30 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 22:30 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 22:30 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 22:30 108-10-1 Methyl-tert-butyl ether 4.1 ug/L 1.0 0.21 1 09/22/13 22:30 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 22:30 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 22:30 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 22:30 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 22:30 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 29 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-6 Lab ID: 92172221013 Collected: 09/13/13 14:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.81J ug/L 1.0 0.46 1 09/22/13 22:30 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 22:30 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 22:30 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 22:30 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 22:30 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 22:30 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 22:30 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 22:30 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 22:30 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 22:30 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 22:30 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 22:30 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 22:30 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 22:30 95-47-6 Surrogates 4-Bromofluorobenzene (S) 101 % 70-130 1 09/22/13 22:30 460-00-4 1,2-Dichloroethane-d4 (S) 109 % 70-130 1 09/22/13 22:30 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/22/13 22:30 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 30 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: JW-1 Lab ID: 92172221014 Collected: 09/13/13 15:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 22:46 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 22:46 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 22:46 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 22:46 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 22:46 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 22:46 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 22:46 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 22:46 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 22:46 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 22:46 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 22:46 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 22:46 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 22:46 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 22:46 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 22:46 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 22:46 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 22:46 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 22:46 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 22:46 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 22:46 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 22:46 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 22:46 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 22:46 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 22:46 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 22:46 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 22:46 75-35-4 cis-1,2-Dichloroethene 2.5 ug/L 1.0 0.19 1 09/22/13 22:46 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 22:46 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 22:46 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 22:46 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 22:46 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 22:46 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 22:46 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 22:46 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 22:46 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 22:46 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 22:46 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 22:46 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 22:46 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 22:46 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 22:46 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/22/13 22:46 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 22:46 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 22:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 22:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 22:46 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 31 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: JW-1 Lab ID: 92172221014 Collected: 09/13/13 15:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 12.2 ug/L 1.0 0.46 1 09/22/13 22:46 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 22:46 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 22:46 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 22:46 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 22:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 22:46 79-00-5 Trichloroethene 1.2 ug/L 1.0 0.47 1 09/22/13 22:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 22:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 22:46 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 22:46 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 22:46 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 22:46 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 22:46 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 22:46 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/22/13 22:46 460-00-4 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 09/22/13 22:46 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/22/13 22:46 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 32 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Sample: TRIP BLANK Lab ID: 92172221015 Collected: 09/13/13 00:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/22/13 23:01 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/22/13 23:01 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/22/13 23:01 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/22/13 23:01 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/22/13 23:01 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/22/13 23:01 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/22/13 23:01 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/22/13 23:01 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/22/13 23:01 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/22/13 23:01 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/22/13 23:01 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/22/13 23:01 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/22/13 23:01 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/22/13 23:01 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/22/13 23:01 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/22/13 23:01 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/22/13 23:01 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/22/13 23:01 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/22/13 23:01 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/22/13 23:01 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/22/13 23:01 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 23:01 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/22/13 23:01 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/22/13 23:01 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/22/13 23:01 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.56 1 09/22/13 23:01 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/22/13 23:01 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/22/13 23:01 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/22/13 23:01 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/22/13 23:01 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/22/13 23:01 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/22/13 23:01 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/22/13 23:01 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 0.26 1 09/22/13 23:01 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/22/13 23:01 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/22/13 23:01 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/22/13 23:01 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/22/13 23:01 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/22/13 23:01 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/22/13 23:01 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/22/13 23:01 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/22/13 23:01 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/22/13 23:01 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/22/13 23:01 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/22/13 23:01 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/22/13 23:01 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 33 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK Lab ID: 92172221015 Collected: 09/13/13 00:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/22/13 23:01 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/22/13 23:01 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/22/13 23:01 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/22/13 23:01 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/22/13 23:01 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/22/13 23:01 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/22/13 23:01 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/22/13 23:01 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/22/13 23:01 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/22/13 23:01 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/22/13 23:01 75-01-4 Xylene (Total) ND ug/L 2.0 0.66 1 09/22/13 23:01 1330-20-7 m&p-Xylene ND ug/L 2.0 0.66 1 09/22/13 23:01 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/22/13 23:01 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 09/22/13 23:01 460-00-4 1,2-Dichloroethane-d4 (S) 111 % 70-130 1 09/22/13 23:01 17060-07-0 Toluene-d8 (S) 97 % 70-130 1 09/22/13 23:01 2037-26-5 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 34 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 QC Batch: MSV/24325 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92172221001, 92172221002, 92172221003, 92172221004, 92172221005, 92172221006, 92172221007, 92172221008,92172221009,92172221010,92172221011,92172221012,92172221013,92172221014, 92172221015 METHOD BLANK: 1051937 Matrix: Water Associated Lab Samples: 92172221001, 92172221002, 92172221003, 92172221004, 92172221005, 92172221006, 92172221007, 92172221008,92172221009,92172221010,92172221011,92172221012,92172221013,92172221014, 92172221015 Parameter Units Blank Result Reporting Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/22/13 14:49 1,1,1-Trichloroethane ug/L ND 1.0 09/22/13 14:49 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/22/13 14:49 1,1,2-Trichloroethane ug/L ND 1.0 09/22/13 14:49 1,1-Dichloroethane ug/L ND 1.0 09/22/13 14:49 1,1-Dichloroethene ug/L ND 1.0 09/22/13 14:49 1,1-Dichloropropene ug/L ND 1.0 09/22/13 14:49 1,2,3-Trichlorobenzene ug/L ND 1.0 09/22/13 14:49 1,2,3-Trichloropropane ug/L ND 1.0 09/22/13 14:49 1,2,4-Trichlorobenzene ug/L ND 1.0 09/22/13 14:49 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/22/13 14:49 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/22/13 14:49 1,2-Dichlorobenzene ug/L ND 1.0 09/22/13 14:49 1,2-Dichloroethane ug/L ND 1.0 09/22/13 14:49 1,2-Dichloropropane ug/L ND 1.0 09/22/13 14:49 1,3-Dichlorobenzene ug/L ND 1.0 09/22/13 14:49 1,3-Dichloropropane ug/L ND 1.0 09/22/13 14:49 1,4-Dichlorobenzene ug/L ND 1.0 09/22/13 14:49 2,2-Dichloropropane ug/L ND 1.0 09/22/13 14:49 2-Butanone (MEK) ug/L ND 5.0 09/22/13 14:49 2-Chlorotoluene ug/L ND 1.0 09/22/13 14:49 2-Hexanone ug/L ND 5.0 09/22/13 14:49 4-Chlorotoluene ug/L ND 1.0 09/22/13 14:49 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/22/13 14:49 Acetone ug/L ND 25.0 09/22/13 14:49 Benzene ug/L ND 1.0 09/22/13 14:49 Bromobenzene ug/L ND 1.0 09/22/13 14:49 Bromochloromethane ug/L ND 1.0 09/22/13 14:49 Bromodichloromethane ug/L ND 1.0 09/22/13 14:49 Bromoform ug/L ND 1.0 09/22/13 14:49 Bromomethane ug/L ND 2.0 09/22/13 14:49 Carbon tetrachloride ug/L ND 1.0 09/22/13 14:49 Chlorobenzene ug/L ND 1.0 09/22/13 14:49 Chloroethane ug/L ND 1.0 09/22/13 14:49 Chloroform ug/L ND 1.0 09/22/13 14:49 Chloromethane ug/L ND 1.0 09/22/13 14:49 cis-1,2-Dichloroethene ug/L ND 1.0 09/22/13 14:49 cis-1,3-Dichloropropene ug/L ND 1.0 09/22/13 14:49 Dibromochloromethane ug/L ND 1.0 09/22/13 14:49 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 35 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 METHOD BLANK: 1051937 Matrix: Water Associated Lab Samples: 92172221001, 92172221002, 92172221003, 92172221004, 92172221005, 92172221006, 92172221007, 92172221008,92172221009,92172221010,92172221011,92172221012,92172221013,92172221014, 92172221015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dibromomethane ug/L ND 1.0 09/22/13 14:49 Dichlorodifluoromethane ug/L ND 1.0 09/22/13 14:49 Diisopropyl ether ug/L ND 1.0 09/22/13 14:49 Ethylbenzene ug/L ND 1.0 09/22/13 14:49 Hexachloro-1,3-butadiene ug/L ND 1.0 09/22/13 14:49 m&p-Xylene ug/L ND 2.0 09/22/13 14:49 Methyl-tert-butyl ether ug/L ND 1.0 09/22/13 14:49 Methylene Chloride ug/L ND 2.0 09/22/13 14:49 Naphthalene ug/L ND 1.0 09/22/13 14:49 o-Xylene ug/L ND 1.0 09/22/13 14:49 p-Isopropyltoluene ug/L ND 1.0 09/22/13 14:49 Styrene ug/L ND 1.0 09/22/13 14:49 Tetrachloroethene ug/L ND 1.0 09/22/13 14:49 Toluene ug/L ND 1.0 09/22/13 14:49 trans-1,2-Dichloroethene ug/L ND 1.0 09/22/13 14:49 trans- 1,3-Dichloropropene ug/L ND 1.0 09/22/13 14:49 Trichloroethene ug/L ND 1.0 09/22/13 14:49 Trichlorofluoromethane ug/L ND 1.0 09/22/13 14:49 Vinyl acetate ug/L ND 2.0 09/22/13 14:49 Vinyl chloride ug/L ND 1.0 09/22/13 14:49 Xylene (Total) ug/L ND 2.0 09/22/13 14:49 1,2-Dichloroethane-d4 (S) % 89 70-130 09/22/13 14:49 4-Bromofluorobenzene (S) % 100 70-130 09/22/13 14:49 Toluene-d8 (S) % 97 70-130 09/22/13 14:49 LABORATORY CONTROL SAMPLE: 1051938 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 52.7 105 70-130 1,1,1-Trichloroethane ug/L 50 48.2 96 70-130 1,1,2,2-Tetrachloroethane ug/L 50 55.6 111 70-130 1,1,2-Trichloroethane ug/L 50 54.8 110 70-130 1,1-Dichloroethane ug/L 50 51.5 103 70-130 1,1-Dichloroethene ug/L 50 52.3 105 70-132 1,1-Dichloropropene ug/L 50 56.9 114 70-130 1,2,3-Trichlorobenzene ug/L 50 58.7 117 70-135 1,2,3-Trichloropropane ug/L 50 54.5 109 70-130 1,2,4-Trichlorobenzene ug/L 50 58.6 117 70-134 1,2-Dibromo-3-chloropropane ug/L 50 51.6 103 70-130 1,2-Dibromoethane (EDB) ug/L 50 55.4 111 70-130 1,2-Dichlorobenzene ug/L 50 55.8 112 70-130 1,2-Dichloroethane ug/L 50 47.0 94 70-130 1,2-Dichloropropane ug/L 50 60.6 121 70-130 1,3-Dichlorobenzene ug/L 50 54.3 109 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 36 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 LABORATORY CONTROL SAMPLE: Parameter 1051938 Units Spike Conc. LCS Result 1,3-Dichloropropane ug/L 50 57.8 1,4-Dichlorobenzene ug/L 50 53.7 2,2-Dichloropropane ug/L 50 52.3 2-Butanone (MEK) ug/L 100 128 2-Chlorotoluene ug/L 50 53.6 2-Hexanone ug/L 100 121 4-Chlorotoluene ug/L 50 55.9 4-Methyl-2-pentanone (MIBK) ug/L 100 120 Acetone ug/L 100 101 Benzene ug/L 50 55.8 Bromobenzene ug/L 50 53.8 Bromochloromethane ug/L 50 47.0 Bromodichloromethane ug/L 50 49.6 Bromoform ug/L 50 50.6 Bromomethane ug/L 50 51.1 Carbon tetrachloride ug/L 50 44.5 Chlorobenzene ug/L 50 53.7 Chloroethane ug/L 50 45.1 Chloroform ug/L 50 51.7 Chloromethane ug/L 50 51.5 cis-1,2-Dichloroethene ug/L 50 52.7 cis-1,3-Dichloropropene ug/L 50 57.3 Dibromochloromethane ug/L 50 50.3 Dibromomethane ug/L 50 52.7 Dichlorodifluoromethane ug/L 50 49.1 Diisopropyl ether ug/L 50 61.8 Ethylbenzene ug/L 50 51.1 Hexachloro-1,3-butadiene ug/L 50 49.8 m&p-Xylene ug/L 100 103 Methyl-tert-butyl ether ug/L 50 54.3 Methylene Chloride ug/L 50 55.4 Naphthalene ug/L 50 58.5 o-Xylene ug/L 50 55.5 p-Isopropyltoluene ug/L 50 54.8 Styrene ug/L 50 54.4 Tetrachloroethene ug/L 50 53.9 Toluene ug/L 50 54.3 trans-1,2-Dichloroethene ug/L 50 53.1 trans- 1,3-Dichloropropene ug/L 50 59.4 Trichloroethene ug/L 50 52.3 Trichlorofluoromethane ug/L 50 42.4 Vinyl acetate ug/L 100 115 Vinyl chloride ug/L 50 52.1 Xylene (Total) ug/L 150 159 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Date: 09/27/2013 09:01 AM LCS % Rec % Rec Limits 116 70-130 107 70-130 105 58-145 128 70-145 107 70-130 121 70-144 112 70-130 120 70-140 101 50-175 112 70-130 108 70-130 94 70-130 99 70-130 101 70-130 102 54-130 89 70-132 107 70-130 90 64-134 103 70-130 103 64-130 105 70-131 115 70-130 101 70-130 105 70-131 98 56-130 124 70-130 102 70-130 100 70-130 103 70-130 109 70-130 111 63-130 117 70-138 111 70-130 110 70-130 109 70-130 108 70-130 109 70-130 106 70-130 119 70-132 105 70-130 85 62-133 115 66-157 104 69-130 106 70-130 84 70-130 98 70-130 102 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 37 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052122 1052123 MS MSD 92172221005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1-Dichloroethene ug/L ND 50 50 63.6 63.0 127 126 70-166 1 30 Benzene ug/L ND 50 50 59.1 61.8 118 124 70-148 4 30 Chlorobenzene ug/L ND 50 50 54.1 58.6 108 117 70-146 8 30 Toluene ug/L ND 50 50 53.5 56.3 107 113 70-155 5 30 Trichloroethene ug/L ND 50 50 59.3 61.9 119 124 69-151 4 30 1,2-Dichloroethane-d4(S) % 97 98 70-130 4-Bromofluorobenzene (S) % 98 98 70-130 Toluene-d8(S) % 98 96 70-130 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 38 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 39 of 43 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172221 Lab ID Sample ID QC Batch Method QC Batch 92172221001 BC-1 EPA 8260 MSV/24325 92172221002 BC-2 EPA 8260 MSV/24325 92172221003 BC-3 EPA 8260 MSV/24325 92172221004 BC-4 EPA 8260 MSV/24325 92172221005 BC-5 EPA 8260 MSV/24325 92172221006 CS-1 EPA 8260 MSV/24325 92172221007 CS-2 EPA 8260 MSV/24325 92172221008 SM-1 EPA 8260 MSV/24325 92172221009 SM-2 EPA 8260 MSV/24325 92172221010 SM-3 EPA 8260 MSV/24325 92172221011 SM-4 EPA 8260 MSV/24325 92172221012 SM-5 EPA 8260 MSV/24325 92172221013 SM-6 EPA 8260 MSV/24325 92172221014 JW-1 EPA 8260 MSV/24325 92172221015 TRIP BLANK EPA 8260 MSV/24325 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Page 40 of 43 W Q peaul saldwes \ z z Z +� Z z L) j m O (N/A) jaloo0 paleag O O �- 2 CL W Apo}sno C\j\V\ U EL i y � iN/.aal LO lY uo paAiaoaa � W F � �N/.l) auuoWO lenplsaa ice. Oa ul dwal Cm IL V Z uj z ❑ t�7 Z L.'Lu L d ~ - w 0 M Q aU) J y o N � N O Z a •• .d O Q J �0e N wul p 7 mamma- Q F- 7J� V I X m t N u t }sal SISAleuyt o � aau}O a w loueu}alN � U.e Q eOzS�eN HOeN m d IOH S� S( k V 9( S( k £ONH a `o "OSZH U c= o z .. o o o w `> panjasajdufl -� oa d C3 m a` & a`. H MJ3NIVINOO d0 # MLLI avi o m Q U Q a s a N0110311OO1V dW313ldWVS 0 w w w Q Q z a y a w Q 9 O fl Or+ M M M o N `o uai `o M M ao z w m z w w��M�MM�r_C"a__ `l �W U ° ¢ o M M C1 M C-' M ��' z0 Q Z a Z N W w J O w � Q d �n C) '� Q N °< o� w m O U Q W W E ' M N 4 (dWOO=O SVNJ=O) 3dAL3ldWVS r ',S It �5 � '5 �s E 0 i � o Z J ua o7 sapo� pl en aas) 3400 XIHiVW m a O m E Q!U)FCr CO �J �Y N N N O 0 a O a` O a` N p Prt m w of o C; mJ q U k x ° •� cr `l F- a � m m o cn0;- �¢i-0 U) z Z r S ,� LU O w 0 J,W J¢ o W m Z Q E d o? O_ E � S4 cc v O •- '9 d v d In W a m o a `"(� c v Pa e 41 of 43 o avi V7 w U Q �+ E w Q. R' # W311 r --- �p -- --- -- --- (NU.) w loelul seldwes CDC N O o oN \• z Z m Y W v Z O - i �y (N/A) J91000 paleaS Lo 0 O `a w /polsno r_ c C a I o ( aol o` co W uPOA o pania�aa o v C7 (N/l.) aulaol40 lenplsab oo ui dwal Q LL ci 0 a Z LU 0� L)Z O � Oco n LL � w R Q M U @ ll.l w {{ y C 2 Z V}i. C r a) D. E Ad O 0 H `� � C fn ❑ (Ji O / O� sT j Q ❑ ... Ilsaj_SISAIEUVi m a �a430 � c Joue4}aW V @ N �. V:S�eN Co U a _ HOeN - Qz w c In a 10H �( �i £ONH _ �-; o _ .� E e a i 7 Z OS H '.. 0 o o c o z o 0 `m o o _ panuasaadufl O Q _ o- n o L L S2j NIV1N00 JO # N w y .o z o _ N w w .. NOli33-nOO1VdW313�dWVS > w s Q a a O O ❑ N w U F .Q N O O Z m 4a Q E K o C ° W Z H = o Uz z Z z av L) F U 00 a N o w F w ' J J 0 W :EJ Q a m M U U- Q y `m 0 Q m RI E w p 0. p W L c E � Vol (dNOO=0 9ViJS=9) 3dkiA�dWVS 0 d Z 1i\ -j � U N(gal a as - osapoo pen aas2— ) 3400 njivN t LJu o"' H m a o C o U E @ Z E Z J w < C y 3 O T L N N > )%F>>aJJdof0I- (n 03: 0 fn K U C 0 D- 0� 0- a- o_ c - xX d ® @ m 1^ S q O O >@ 3: V __ .>_ �_ - 0 o moo. e e` aY7 , F Z W N V W U y . � m �@ WLUa _ W ; m Z m o .9 �� ` JCS E co o '= o Q E o. y" a C o _ IC ❑ Q N N Q o fQ) � /�/� ❑ � E Cc 1 N m Pa e 42 of 43 a W W # wall N M Document Name: Sample Condition Upon Document Revised: June 4, 2013 aliCal� Receip4 SCUR Page 1 of 2 ce-A RA�g�a°s �aM document No Issuing Authontie F-ASV-CS-003-rev.11 Pace Asheville Quality Office Client Name: Where Received: Huntersville Asheville' ` Eden Raleigh Courier (Circle): fed Ex UPS USPS CI t Commercial Pace Other Custody Seal on Cooler/Box Present: yes [2,"' no Seals intact: F-I yes 2-- -"'no Packing Material Bubble Wrap Bubble Bags. None _ Other Circle Thermometer Used. IR G 1302-65963 Type of lee: Ptt Blue None ZSamples on ice, cooling process has begun 1R Gun = 80344039 Tmmn t nrrncfinn Far -Mr Ar1A / S r Corrected Cooler Temp.: ] , C . --r Temp should be above freezing to 6°C Biological Tissue is Frozen: Yes No N/A Date and Initial of erson ez contents: Ue6 Comments: Chain of Custody Present: es ONO ❑N/A 1. Chain of Custody Filled Out: es ❑No ❑N/A 2. Chain of Custody Relinquished: ,Wes. []No ❑N/A 3. Sampler Name & Signature on COC: es ❑No ❑WA 4. Samples Arrived within Hold Time: J s ❑No ❑N/A 5. Short Hold Time Analysis (<72hr): ❑YesPWo ❑N/A 6. Rush Turn Around Time Requested: v ❑Yes AJNo ❑N/A 7. Sufficient Volume: <1'es ❑No ❑N/A 8. Correct Containers Used; -Pace Containers Used: 01es fires ❑No ONo ❑N/A ❑N/A 9. Containers Intact: Yes ONo ❑N/A 10. Filtered volume received for Dissolved tests ❑Yes ❑No QXrK 11. Sample Labels match COO: -Includes date/time/ID/Analysis Matrix: P<s ❑No* ❑N/A 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: 40oliform. C O&G, WI-DRO (water) Yes e. es ❑No ❑No [-]No ❑N/A ❑N/A 13. Sample checked for dechlonnation: ❑Yes ❑No EXIA 14. Headspace in VOA Vials ( >6mm): Dyes ®'No El N/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): Pfes [Yes ❑No ❑No ❑N/A ❑N/A 16. Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: Date: SRF Review: Date: Note: Whenever there is a discrepancy affecting No C rolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) Page 43 of 43 qD aceAnalytical —pacelabs.com September 27, 2013 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 Eden, NC 27288 (336)623-8921 RE: Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Dear Mr. Alexander: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 16, 2013. The results relate only to the samples included in this report. Results reported herein conform to the most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton for Tom Williams tom.williams@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE SUMMARY Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Lab ID Sample ID Matrix Date Collected Date Received 92172223001 BC-1 Water 09/13/13 13:50 09/16/13 09:00 92172223002 BC-2 Water 09/13/13 13:40 09/16/13 09:00 92172223003 BC-3 Water 09/13/13 13:30 09/16/13 09:00 92172223004 BC-4 Water 09/13/13 13:15 09/16/13 09:00 92172223005 BC-5 Water 09/13/13 13:00 09/16/13 09:00 92172223006 CS-1 Water 09/13/13 14:10 09/16/13 09:00 92172223007 CS-2 Water 09/13/13 14:00 09/16/13 09:00 92172223008 SM-1 Water 09/13/13 14:55 09/16/13 09:00 92172223009 SM-2 Water 09/13/13 14:50 09/16/13 09:00 92172223010 SM-3 Water 09/13/13 14:45 09/16/13 09:00 92172223011 SM-4 Water 09/13/13 14:40 09/16/13 09:00 92172223012 SM-5 Water 09/13/13 14:35 09/16/13 09:00 92172223013 SM-6 Water 09/13/13 14:30 09/16/13 09:00 92172223014 JW-1 Water 09/13/13 15:00 09/16/13 09:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92172223001 BC-1 SM 5310B SAE 1 PASI-A 92172223002 BC-2 SM 5310B SAE 1 PASI-A 92172223003 BC-3 SM 5310B SAE 1 PASI-A 92172223004 BC-4 SM 5310B SAE 1 PASI-A 92172223005 BC-5 SM 5310B SAE 1 PASI-A 92172223006 CS-1 SM 5310B SAE 1 PASI-A 92172223007 CS-2 SM 5310B SAE 1 PASI-A 92172223008 SM-1 SM 5310B SAE 1 PASI-A 92172223009 SM-2 SM 5310B SAE 1 PASI-A 92172223010 SM-3 SM 5310B SAE 1 PASI-A 92172223011 SM-4 SM 5310B SAE 1 PASI-A 92172223012 SM-5 SM 5310B SAE 1 PASI-A 92172223013 SM-6 SM 5310B SAE 1 PASI-A 92172223014 JW-1 SM 5310B SAE 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-1 Lab ID: 92172223001 Collected: 09/13/13 13:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.2 mg/L 1.0 1.0 1 09/26/13 03:28 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-2 Lab ID: 92172223002 Collected: 09/13/13 13:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.8 mg/L 1.0 1.0 1 09/26/13 03:40 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-3 Lab ID: 92172223003 Collected: 09/13/13 13:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.7 mg/L 1.0 1.0 1 09/26/13 03:52 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-4 Lab ID: 92172223004 Collected: 09/13/13 13:15 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.0 mg/L 1.0 1.0 1 09/26/13 04:46 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-5 Lab ID: 92172223005 Collected: 09/13/13 13:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.0 mg/L 1.0 1.0 1 09/26/13 05:00 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 Lab ID: 92172223006 Collected: 09/13/13 14:10 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.9 mg/L 1.0 1.0 1 09/26/13 05:12 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 Lab ID: 92172223007 Collected: 09/13/13 14:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.4 mg/L 1.0 1.0 1 09/26/13 05:25 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-1 Lab ID: 92172223008 Collected: 09/13/13 14:55 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 09/26/13 05:39 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-2 Lab ID: 92172223009 Collected: 09/13/13 14:50 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 5.5 mg/L 1.0 1.0 1 09/26/13 06:11 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-3 Lab ID: 92172223010 Collected: 09/13/13 14:45 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 09/26/13 06:25 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 14 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-4 Lab ID: 92172223011 Collected: 09/13/13 14:40 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.7 mg/L 1.0 1.0 1 09/26/13 06:37 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 15 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-5 Lab ID: 92172223012 Collected: 09/13/13 14:35 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 09/26/13 07:31 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-6 Lab ID: 92172223013 Collected: 09/13/13 14:30 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 09/26/13 07:43 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 17 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: JW-1 Lab ID: 92172223014 Collected: 09/13/13 15:00 Received: 09/16/13 09:00 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.1 mg/L 1.0 1.0 1 09/26/13 07:57 7440-44-0 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 24 qD aceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 QC Batch: WETA/16538 Analysis Method: SM 5310B QC Batch Method: SM 5310B Analysis Description: 5310E TOC Associated Lab Samples: 92172223001, 92172223002, 92172223003, 92172223004, 92172223005, 92172223006, 92172223007, 92172223008,92172223009,92172223010,92172223011,92172223012,92172223013,92172223014 METHOD BLANK: 1052218 Matrix: Water Associated Lab Samples: 92172223001, 92172223002, 92172223003, 92172223004, 92172223005, 92172223006, 92172223007, 92172223008,92172223009,92172223010,92172223011,92172223012,92172223013,92172223014 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 09/26/13 01:49 LABORATORY CONTROL SAMPLE: 1052219 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.2 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052220 1052221 MS MSD 92172214013 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 1540 25 25 1520 1500 -114 -182 75-125 1 20 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1052222 1052223 MS MSD 92172223008 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Total Organic Carbon mg/L 1.6 25 25 24.4 24.3 91 91 75-125 1 20 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 19 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/27/2013 09:01 AM without the written consent of Pace Analytical Services, Inc.. Page 20 of 24 ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalX cal 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: FormerAndrex Ind. J13-1022-36 Pace Project No.: 92172223 Lab ID Sample ID QC Batch Method QC Batch 92172223001 BC-1 SM 5310E WETA/16538 92172223002 BC-2 SM 5310E WETA/16538 92172223003 BC-3 SM 5310E WETA/16538 92172223004 BC-4 SM 5310E WETA/16538 92172223005 BC-5 SM 5310E WETA/16538 92172223006 CS-1 SM 5310E WETA/16538 92172223007 CS-2 SM 5310E WETA/16538 92172223008 SM-1 SM 5310B WETA/16538 92172223009 SM-2 SM 5310B WETA/16538 92172223010 SM-3 SM 5310B WETA/16538 92172223011 SM-4 SM 5310B WETA/16538 92172223012 SM-5 SM 5310B WETA/16538 92172223013 SM-6 SM 5310B WETA/16538 92172223014 JW-1 SM 5310B WETA/16538 Date: 09/27/2013 09:01 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Page 21 of 24 e;ul saldweS h �i z < co O Z K O Z O C co F=- O O J01000 paleas I o O O v w a < Rpo;sno r < E L..L N (N/A) ail uo paniaoaa � < .�CO w (N/J.) auuol40 lenplsa�j dwal 0, uI m V o Z Qy L 1___ u m Q l' LL w w� ++ T FO Cl) Gi J = a co Z D O -J y T r O O N r.+ U) U a rn o wCD a N E r fior£5 Sys' t N hk t ;sal sisAleuyt d �/ No m a ti �v �a410 �( k ca loueq;aw V v a £OZS�eN �+ ) > HOeN R ¢ z \ IOH Q Q , EONH ° a "OSzH O U o c E z o o o pa/uasaaduN OJ O Q o Cl) ai °> z n o m a (7 m m a = h !y S213NIV1NOO 30 # eA fJ [.1 Vi C4 tJ GJ lJ C4 Cl) M s Q U Q a a a � NOUDD- OO IV dA31 3]dWVS w a V m M .. a w a w a A F- W w Q z i F=— Z o M M T' 1 M M M a> a m W O w 1\ 4 w a s O LL LL N = °a a r oN w m .2 0 1 10 ` M 7 z B (dW00=0 8V2iO-t 3d).13ldWtlS r o ` d z ga o; Sep-pl en aas) AGOG XRilVW 3 $ 3 3 3 Ca a 0 c v a a o E E E _! �3a��a of U) �o o�� no�a�o U)W W c) a- 0 a 2 a` m o c U U « i x (� A '01 3:ain O�QFO N t _ (� Q w z z w Rs o N J Q z 0 ° V1 w w m ° z , o m ` Y'a F J rnH E oU) O f- cRTSo ca U ti O U Cl) a ! \ 1 1 ♦ ♦ ♦ 1 Q U a o m o < `� V 4 E a� Pa e 22 of 24 #W311 w r� v n o ti w rn c U) � c� Q w a � (N/A) w V ;se;ul sa(dweg z __ 11 CD 0 \v 00 Z w F Z O �. (N/A) 1a1000 paleas U O o W APolsnO O C\j J IL (._ i,.... N (N/A) a0I uo panl900a W F a (N/A) auuo14O lenplsay 3: 0. w dwal 0 E m a U UJ O _ Z �► c0 ,... Q w o ~ ui o ~ w a_ z J y N aw L L 0 Q Z m .� N O rn Q in 1 N /A t ISOL sisAleuyt W r JaylO w U louey)aw £OZSZeN a HOeN m I3H £ONH � '° a e bOSZH c= o R N o .o � o ,J panjasajdun p.if m a m m m a r w > z EC) o a Q ,� a K a `�' a S2J3NIVINOO JO # �� co Q W M r w a w a N0113317001V dA31 3ldWVS w ~ R r aye N O O F a K �i R� z N E W W Q A 7 U o Q w a Z Z O o Q-- zO a N W W O) M J O W Q J 1 U _ LL Q - Q V) W o a 0o N T R1 c o 3 j3 � ~ o O W E M (dW00=0 BVNJ=`J) 3lcva 3ldms V s o — z z J (gad o; sapoo pgen aas) 3400 XIb1VW o z Co a 0 O E E m m r-- 3: d. cr 0 wQ 0 �nO�QF0 Z c� Q n a a CT 0 y m O fn K U d 4. p U d xx g (n z�+ S �` 2 s O 0 O � 0 j WLLIJ o W m Q Z .g r Q J rn H E a o ? O t_ E $ N C N — G O ) Q U A (�v o�CO3 c d E o c m .. o °' u '6 U) n m ~ N N 3 N K Q E NN o E E m # W 311 w r� v in m ti ao rn o P ge 23 of 24 u7 n10 Q W a a Document Name: Sample Condition Upon Document Revised: June 4, 2013 aceAt7al tf ail Receipt" SOUR Page 1 of 2 Docu--ment No:: Is�air�A�throriti I F=ASV-CS-003-rev.11 Pace Asheville Quality Office Client Name: Where Received: F Huntersville Asheville' m Eden M Raleigh Courier (Circle): fed Ex UPS USPS CI'erht . Commercial Pace Other Custody Seal on Cooler/Box Present: fj yes L3no Seals intact: yes 21no Packing Material: El Bubble Wrap . Bubble Bags" None Other Circle Thermometer Used: IR G 3-13 55963 Type of Ice: VWt Blue None. 211Samples on ice, cooling process has begun IR =Gun2-7.80344039 Temp Correction Factor: Add / C Corrected Cooler Tem C . Biological Tissue is Frozen: Yes No N/A Date and Initial of son ex jng p' -�— contents: Temp should be above freezinq to 6°C Comments: Chain of Custody Present: es ❑No ❑N/A 1. Chain of Custody Filled Out: es. ❑No ❑N/A 2. Chain of Custody Relinquished: Pfes. ❑No ❑N/A 3. Sampler Name & Signature on COC: es ❑No ❑N/A 4. Samples Arrived within Hold Time: ,,) des ON. ❑N/A 5. Short Hold Time Analysis (<72hr): Dyes R<o ❑N/A 6. Rush Turn Around Time Requested: ❑Yes o ❑N/A 7. Sufficient Volume: <1'es"❑No ❑N/A 8. Correct Containers Used: -Pace Containers Used: ones 21.. ❑No ON. ON/A ❑N/A 9. Containers Intact: Yes ❑No ❑NIA 10. Filtered volume received for Dissolved tests ❑Yes ❑No PMK 11. Sample Labels match COO: -Includes date/time/ID/Analysis Matrix: -s ❑No❑N/A L9 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: 40olfform, C O&G, WI-DRO (water) Yes es ON. ❑No ON. ❑N/A ❑NIA 13. Sample checked for dechlorination: ❑Yes ❑No /A 14. Headspace in VOA Vials ( >6mm) Dyes 2 'N. ❑N/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): fifes Wes ❑No ❑No ❑N/A ❑N/A 16. Client Notification/ Resolution: Field Data Required? Y ! N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: SRF Review: I f o�llC � jDate:�1 / / Note: Whenever there is a discrepancy affecting No h Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) Page 24 of 24 APPENDIX C HISTORICAL LABORATORY ANALYSES RESULTS SUMMARY TABLES AND TIME VS. CONCENTRATION PLOTS Monitoring Well MW-1 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene 7,400 8,600 3,400 900 NS 860 3,600 3,500 880 NS 1,400 183 74 170 190 320 40 26 10 8.0 18 110 AB AB AB AB AB Trichloroethene 124 ND 21 2.6 NS ND 40 ND 3.7 NS ND ND 2.7 29 47 ND 1.0 1.2 ND ND ND 6.9 AB AB AB AB AB Chloroform 1.2 ND 1.7 9 NS 7 ND ND 17 NS ND ND 15 7 ND ND 1.1 ND 1.1 ND ND ND AB AB AB AB AB Vinyl Chloride ND ND ND I ND I NS I ND ND I ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1, 1 -Trichloroethane ND 340 ND IND INS ND ND I ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1 -Dichloroethene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloroethane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Trans 1,2-Dichloroethene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Cis 1,2-Dichloroethene NA NA NA NA NS INA NA NA NA NS NA NA NA 17 30 ND 0.82 ND ND ND ND 18.6 AB AB AB AB AB Trichlorofluoromethane ND ND ND NO NS ND NO NO ND NS ND NO ND ND ND ND ND ND ND NO ND NO AB AB AB AB AB 1,2-Dichloro ro ane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Chlorobenzene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,4-Dichlorobenzene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1, 1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA ND AB AB AB AB AB TOTAL CHLORINATEDS DETECTED 1 7,525 18,94013,4231 9121 NS 1867 13,64013,50019011 NS 11,4001 183 1 92 1 223 1 267 1 320 1 43 1 27 1 11 1 8.0 1 18 1 136 AB AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NS = Not Sampled; recovery system being monitored for aquifer modeling. The laboratory results from MW-1 were inadvertently labeled as MW-2 during the 2nd quarter 1994. The correction has been made on this spreadsheet. MW-1 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-2 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st I 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 640 81 76 NS 110 130 100 78 NS 66 69 28 76 41 31 19 17 12 13 19 6.9 AB AB AB AB AB Trichloroethene NP ND 1.7 7.3 NS 13 21 12 12 NS 13 ND ND 16 11 6.4 2.9 2.4 2.7 2.6 1.7 0.71 AB AB AB AB AB Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND 0.69 ND ND ND ND ND ND AB AB AB AB AB Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1, 1 -Trichloroethane NP 91 ND ND NS NDI ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND. AB AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND I ND ND ND ND AB AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 2.8 17 4.1 4.1 ND 1 1.8 0.83 1.2 ND AB AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloro ro ane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS I ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS I ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1, 1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA NS I NA NA NA NA NA NA NA NA NA NA NA ND AB AB AB AB AB TOTAL CHLORINATEDS DETECTED I NP 1 731 83 1 83 1 NS 123 151 1 112 90 1 NS 1 79 1 69 1 28 1 95 1 69 1 42 1 26 1 19 1 17 1 16 1 22 1 7.6 AB I AB AB I AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. The laboratory results from MW-2 were inadvertently labeled as MW-1 during the 2nd quarter 1994. The correction has been made on this spreadsheet. MW-2 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-3 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 18,000 350 140 NS 11 80 12 34 NS 9.2 623 600 38 160 91 89 29 39 55 45 820 AB AB AB AB AB Trichloroethene NP 700 26 21 NS 2.8 12 3.1 5 NS 1.7 149 430 13 95 20 3.7 3.2 3.9 5.0 3.6 26.6 AB AB AB AB AB Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND 1.1 ND ND ND ND ND ND ND AB AB AB AB AB Vinyl Chloride NP ND 34 49 1 NS 7.2 17 10 7.8 NS ND ND 59 3.5 11 ND ND ND 0.84 ND ND 2.6 AB AB AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS NDI ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND 1.1 ND ND ND ND ND ND ND AB AB AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND 1.30 ND ND ND ND ND ND ND ND ND 0.55 AB AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND I ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Trans 1,2-Dichloroethene NP ND 0.74 ND NS ND ND ND ND NS ND 1.57 ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA I NS INA NA NA NA NS NA NA NA 20 130 18 ND ND 2.3 0.53 1.2 40.9 AB AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloro ro ane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND AB AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND eNDND ND ND ND ND ND ND ND AB AB AB AB AB1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,1,2-Tetrachloroethene NA NA NA NA NS NA NA NA NA NS NA NA NA NA I NA NA NA NA ND AB AB AB AB AB TOTAL CHLORINATEDS DETECTED I NP 118,7001 4111 2101 NS 1 21 1 1091 25 1 47 INS 1 10.91 775 11,0891 75 1 398 1 129 1 93 1 32 1 46 1 61 1 50 1 891 AB I AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-3 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-4 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 2199h 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 1,100 630 510 NS 680 620 560 360 NS 250 363 410 840 630 180 560 170 200 200 150 230 AB AB AB AB AB Trichloroethene NP 620 230 220 NS 230 300 280 200 NS 180 248 240 430 410 160 500 140 170 170 180 275 AB AB AB AB AB Chloroform NP ND ND ND NS ND ND 22 ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND I ND AB AB AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS 2.5 ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND 3.4 ND AB AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 190 180 69 210 74 98 88 120 148 AB AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloro ro ane NP 4.5 3.3 ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND 0.75 0.78 AB AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1, 1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NAINSINA1 NA NA NA NA NA NA NA NA NA I NA ND AB AB AB AB AB TOTAL CHLORINATEDS DETECTED NP 1,725 863 1 730 1 NS 1 913 920 1 862 560 1 NS 430 1 611 1 650 1 1,460 1,220 409 1 1,270 384 1 468 1 458 1 454 1 654 AB AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-4 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-5 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 49,000 23,000 7,200 NS 9,200 7,800 7,600 9,000 NS 25,000 3,200 1,500 5,500 980 NS 25 d 120 150 610 106 2,160 3,750 2,340 4,940 5,250 Trichloroethene NP 300 470 ND NS ND 15 ND 23 NS ND ND ND ND ND NS 2.3 1.0 8.9 7.2 7.0 5.0 14.0 74.9 279 305 Chloroform NP ND 13 ND NS ND 20 ND 38 NS ND ND 14 ND ND NS ND d ND ND ND 0.61 1.2 4.2 ND ND 0.9 Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND 1.7 69.8 1, 1, 1 -Trichloroethane NP 530 8.9 ND NS ND 2.8 ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND ND 1, 1,2 -Trichloroethan e NP I ND 6.8 ND NS ND ND ND ND NS ND ND ND ND ND NS ND d ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND 1.5 1.2 1,2-Dichloroethane NP ND 1.2 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND 2.1 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND 3.2 5.2 Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 1 86 1 710 NS 1 13 1 dry 2.6 1 22 1 8 21 19 9.1 3,420 783 505 Trichlorofluoromethane NP ND ND ND NS ND 1.3 ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP ND ND ND NS NDgNDND ND NS ND ND ND ND ND NS ND d ND ND ND ND ND ND ND ND ND Chlorobenzene NP ND 130 ND NS NDD ND NS ND ND ND ND ND NS ND d ND ND ND ND ND ND ND 0.67 0.58 1,4-Dichlorobenzene NP ND ND ND NS NDD ND NS ND ND ND ND ND NS ND d ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NA NA NA NA NS NAA I NA NS NA NA NA NA NA NA NA d NA NA NA ND ND ND ND 1.6 1.4 TOTAL CHLORINATEDS DETECTED NP 49,830 23,632 1 7,200 1 NSI 9,200 1 7,839 1 7,600 1 9,061 INSI 25,000 13,200 1 1,514 15,586 1 1,690 1 NS 1 40 1 dry 1 124 1 181 1 625 135 21185 31777 51835 6.011 6111,139 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled, well dry or in use as pilot test recovery point. MW-5 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-6 Concentrations in Parts per Billion (µgll) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 40,000 37,000 7,600 NS 27,000 7,700 7,300 7,000 NS 3,500 3,270 3,300 12,000 4,700 5,100 7,800 5,900 3,200 1,000 5,000 3,050 3,580 270 2,160 2,550 1,260 Trichloroethene NP 1,600 6,500 290 NS 1,600 330 260 310 NS ND 162 160 2,700 1,500 1,200 1,800 860 390 110 150 251 267 58 110 52 228 Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP ND 280 47 NS ND 99 ND 84 NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 83.6 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP ND 1.7 ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP ND 17 ND NS ND ND ND ND NS ND 5.49 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP ND ND ND NS ND 1ND ND ND NS ND 1.32 ND ND I ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND 45 ND NS I ND ND ND ND NS ND 20.2 ND ND ND ND ND ND 4.5 ND 1.8 1.4 ND ND ND ND 6.1 Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 8,900 3,800 4,500 2,800 210 390 270 110 207 284 85 328 43 709 Trichlorofluoromethane NP ND 28 ND NS ND ND ND ND NS ND 2.82 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP ND 9.5 ND NS ND ND ND ND NS ND 2.17 ND NDMNDND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP ND L8 ND NS ND ND ND ND NS ND ND ND NDND ND ND ND ND 46 3.5 ND ND ND ND 0.83 1,1,1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA NS NA NA NA NANA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP 41,600 43,883 7,937 NS 28,600 8,129 7,560 7,394 NS 13,5001 3,4641 3,460 1 23,600 10,000 10,800 12,400 6,970 1 3,985 1 1,380 15,266 1 3,513 4,131 413 2,598 2,644 2,288 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-6 Prepared by: AWA 1022-36 Andres: Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-7 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 m3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 6.0 8.3 12 NS 76 46 27 13 NS 41 165 11 10 3.6 72 ND 1.9 1.4 1.4 1.3 ND 36 92 165 175 152 Trichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND 24 ND ND ND ND ND ND ND ND ND ND ND Chloroform NP ND ND ND NS 1.2 ND 1.1 ND NS 2.2 6.24 1.2 2 ND 0.62 ND ND 0.67 ND ND ND ND 0.6 0.51 ND 0.64 Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP ND ND ND NS IND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND I ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND I ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA ND ND 20 ND ND ND ND ND I ND ND ND ND ND ND Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND I ND ND ND ND ND ND 1,2-Dichloro ro ane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND I ND I ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND I ND ND I ND I ND I ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA NS I NA NA I NA NA I NA I NA I NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED NP 6.0 8.3 1 12 NS 77 1 46 1 28 1 13 NS 1 43 1 171 1 12 1 12 1 3.6 1 117 1 ND 1 1.9 1 2.1 1 1.4 1 1.3 1 ND 36 93 166 175 153 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-7 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-8 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 78 24 620 NS 20 950 900 1,500 NS 39 675 570 420 80 8.7 19 24 15 23 40 13 AB AB AB AB AB Trichloroethene NP 4.5 ND 68 NS ND 29 66 68 NS 1.1 53.4 58 14 8.4 1.8 ND ND ND ND 2.9 ND AB AB AB AB AB Chloroform NP ND I ND ND NS ND ND 8.5 ND NS ND I ND ND ND ND ND ND ND ND ND I ND ND AB AB AB I AB I AB Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,1-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane NP I ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA I NS NA NA NA 26 46 1.1 1 ND ND ND ND 3.9 ND AB AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloro ro ane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Chlorobenzene NP ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,4-Dichlorobenzene NP �ND g ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB1,1,1,2-Tetrachloroethane NA NA NS NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA ND AB AB AB AB AB TOTAL CHLORINATEDS DETECTED NP 1 83 1 24 688 NS 20 979 975 1,568 1 NS 1 40 1 728 628 460 1 134 1 12 1 19 1 24 1 15 23 47 13 1 AB I AB All I AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. NM-8 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-8A Concentrations in Parts per Billion (µg/l) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP 1,800 640 3,900 NS 970 3,400 3,700 6,300 NS 1,200 3,470 3,400 1,600 1,900 1,100 400 400 420 110 190 247 AB AB AB AB AB Trichloroethene NP 96 25 250 NS 39 190 240 270 NS ND 250 220 ND 410 95 79 47 42 10 20 16 AB AB AB AB AB Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Vinyl Chloride NP ND ND ND NS ND 2.8 ND ND NS ND 4.29 ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,1-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane NP I ND I ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND I ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND 1 1.9 ND ND NS ND 3.11 ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 120 430 160 150 83 80 17 40 28.4 AB AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND 0.92 ND ND NS ND 1.78 ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloro ro ane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS I ND I ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA NS I NA I NA NA NA NA NA NA NA NA NA NA ND AB AB AB AB AB TOTAL CHLORINATEDS DETECTED I NP 1,896 665 4,150 NS 1,009 3,596 3,940 6,570 NS 1,200 3,729 1 3,620 1 1,720 2,740 1 1,355 1 629 1 530 1 542 1 137 1 250 1 292 AB AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-8A Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-9 Concentrations in Parts per Billion (µgll) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 m1991i 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 1,900 4,550 3,800 3,600 3,600 1,100 270 2,200 1,700 1,000 680 4,730 4,840 5,080 4,180 2,000 1,260 Trichloroethene NP NP NP NP NP NP NP NP NP NP ND 608 620 570 970 270 66 250 140 92 98 341 234 145 107 99 90 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 4.4 ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND 9.42 ND ND ND ND 100 28 24 ND 10 2.5 ND ND ND ND 2 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND 0.74 ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 1.89 ND ND ND ND 0.5 ND ND ND 3.6 1.1 ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 8.81 ND ND ND ND 5.6 ND 2.6 ND 2.2 7 ND ND ND 1.9 1.5 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA 920 1,100 260 300 500 400 240 180 466 376 259 191 325 352 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 2.31 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND 6.29 ND ND ND ND 28 6.8 1.5 ND 2.2 1.6 ND ND ND 0.47 0.43 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 5.6 ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NA NP NP NP NP NP NP NP NP NP I NA NA NA NA NA NA NA NA NA NA NA 0.70 ND ND ND ND ND TOTAL CHLOMNATEDS DETECTED I NPI NPI NP I NPI NP INPI NP I NPI NP INPI 1,900 1 5,187 1 4,420 1 5,090 1 5,670 1 1,630 1 780 1 2,985 1 2,2681 1,332 1 976 5,551 5,450 5,484 1,178 2,426 1,706 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-9 Prepared by: AWA 1022-36 Andres: Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-10 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 4,700 4,920 5,400 9,900 4,200 4,500 3,500 900 800 590 1,200 3,360 1,910 3,160 182 5 157 Trichloroethene NP NP NP NP NP NP NP NP NP NP 400 484 480 920 400 450 440 120 74 54 120 180 76 127 75 ND 18 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND 3.07 ND ND ND ND ND ND ND ND 2.7 ND ND ND ND 1 5 7.7 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP I NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 2.00 ND ND ND ND ND ND ND ND 3.5 ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND NO 2.9 ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 7.69 ND ND ND ND ND ND 1.2 ND 1 2.6 5 ND ND 15.2 ND 0.76 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA 2,300 1,300 870 620 320 220 160 270 426 169 253 1,460 20 56 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 4.94 ND ND ND ND ND ND ND ND 2.9 ND ND ND ND ND ND 1,2-Dichloro ro ane I NP I NP I NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND NO ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND 2.51 ND ND ND ND ND ND ND ND ND 0.86 ND ND ND ND 0.28 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA I NA 1.2 1.2 ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP I NP I NP I NPI NP I NP I NP I NP I NP I NP 15,1001 5,424 1 5,880 113,1201 5,900 1 5,820 1 4,560 1 1,340 1 1,095 1 804 1 1,602 1 3,973 2,156 1 3,540 1 1,735 29 239 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NM-10 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-11 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 m3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 1,400 3,050 1,800 3,600 2,100 1,800 2,200 2,200 1,000 1,100 NS 975 791 2,400 2,130 1,940 1,050 Trichloroethene NP NP NP NP NP NP NP NP NP NP 190 370 240 410 280 300 110 330 230 180 NS 89 56 196 93 87 66 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 12 ND ND ND NS ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND ND 36 110 ND ND 22 ND 9.7 ND NS ND ND ND ND ND 4.6 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 1.74 ND ND ND ND 1.7 ND ND ND NS ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 5.95 ND ND ND ND 5.8 ND 2.2 ND NS 2.2 ND 5.2 ND 1.6 1.6 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA 1,000 770 530 980 480 490 380 NS 153 156 337 163 162 203 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 3.02 ND ND ND ND 1 ND ND ND NS ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND 9.77 ND ND ND ND 5.1 ND 2.2 ND NS ND ND ND ND 0.39 0.29 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND 2.08 ND ND ND ND 1.3 ND ND ND NS ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NPI NP I NP I NP INPI NA NA NA NA NA NA NA NA NA NA NS ND ND ND ND 0.51 ND TOTAL CHLORINATEDS DETECTED I NP I NP I NPI NP I NP I NPI NP I NP I NP I NPI 1,5901 3,443 1 2,076 1 5,1201 3,1501 2,630 1 3,339 1 3,0101 1,7341 1,6601 NS 1 1,2191 1,003 2,938 2,386 2,191 1,325 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-11 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-12 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 m3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 5,300 3,810 1,500 3,500 2,800 3,200 220 130 220 65 930 135 1,010 3,590 156 3 4 Trichloroethene NP NP NP NP NP NP NP NP NP NP ND 6.07 ND ND ND 550 3 ND ND ND 5 1.4 10 11 44 ND ND Chloroform NP NP NP NP NP NP NP NP NP NP ND 20.8 ND ND ND ND 1.3 ND ND ND ND 1.3 2.8 ND ND ND I ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 22.7 1.9 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11.3 ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 14.2 11.4 8.3 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA ND ND 750 2.8 ND ND ND 6.1 1.4 5 15 6,810 5,830 13 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP ND ND NO ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA NA ND 1.1 ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP I NP I NPI NP I NP I NPI NP I NP I NP I NP 15,3001 3,837 1 1,5001 3,500 1 2,8001 4,500 1 227 1 130 1 220 1 65 1 941 1 139 1,029 3,616 7,036 5,867 27 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-12 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-13 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 788 2,100 2,900 4,100 2,600 5,100 760 420 1,100 530 356 683 1,420 960 979 1,030 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 174 450 480 440 440 690 99 170 110 69 42 81 97 304 211 245 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 1.48 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 3.5 ND ND ND ND 0.88 0.91 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 1 ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 1.1 0.62 ND ND ND 0.79 3.5 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 990 1,300 1,000 1,500 230 130 300 200 121 256 241 158 196 159 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 2.7 ND ND 1.5 ND 0.45 0.24 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.24 ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA I NA NA I NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED NP NP NP NP NP NP NP NP NP NP I NP 1 963 2,550 4,370 1 5,840 4,040 1 7,290 1 1,089 720 1 1,510 807 1 519 1,0201 1.7591 1,4221 1,3881 1,439 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-13 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-14 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 231 280 1,100 650 570 510 250 440 320 340 375 377 867 997 968 774 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 74.9 110 220 160 190 180 120 220 130 170 196 174 396 331 362 322 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 1.76 ND ND ND ND ND ND ND ND 2.8 ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 3.8 0.79 ND 1.7 ND 1.5 1.6 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 140 110 100 90 64 95 77 120 123 91 206 136 158 167 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.25 ND 1,4-Dichlorobenzene NP I NP I NP 1 NP 1 NP jNP NP I NP I NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA I NA NA NA NA I NA I ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NPI 308 1 390 1 1,4601 920 1 860 1 780 1 434 1 755 1 527 1 637 1 695 642 1,471 1,464 1,490 1,265 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-14 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-15 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 71 45 92 70 71 110 110 90 100 130 171 197 704 194 176 94 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 2.59 2.4 4.6 2 2.4 2.7 ND ND ND 2.4 3.4 3.7 4.2 3.9 4.0 2.2 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.71 0.98 1.0 0.68 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND I ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 2.0 ND ND 5.7 ND 6 ND 4.5 6.3 6.6 8.0 9.4 7.3 3.9 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 11.25 1 ND 2.9 2 1.8 2.5 ND ND ND 3.1 1.3 1.1 1.6 1.2 1 0.63 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND 1.7 ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORWATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NPI NP I NP I NP 1 75 1 47 1 102 1 74 1 77 1 121 1 110 1 96 1 100 1 140 182 1 208 1 719 209 189 102 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-15 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-16 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 65.7 77 180 150 76 190 120 150 200 190 434 245 401 249 180 145 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 2.66 3.7 5.4 5 5.3 6.8 ND 2.6 ND 4.5 6.6 5.3 8.4 4.9 4.4 2.8 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND 0.8 ND 1.5 1.5 1 1.3 1 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene P NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene P NP NP NP NP NP NP NP NP NP NA NA 2.7 3.4 4.7 12 ND 8.4 5.1 8 13 9.3 16 11 9 6 Trichlorofluoromethane P NP NP NP NP NP NP NP NP NP 1.24 1.6 5.2 4.4 7.1 6.2 ND ND ND 4.1 3.6 ND 3.4 1.8 1.2 0.96 1,2-Dichloro ro ane 1p P NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP ND IN ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene P NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane P NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORWATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP 1 70 1 82 1 193 1 162 1 93 1 215 1 120 1 161 1 205 1 207 1 458 260 431 268 196 155 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-16 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-17 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 M19911993 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 320 410 430 82 78 29 52 82 54 100 17 24 18 7.5 1.0 27.7 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 36 86 54 35 27 13 14 20 11 13 8.2 7.2 4.3 3.4 1.0 3.8 Chloroform NP NP NP NP NP NP NP NP NP NP NP 0.36 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 5.68 12 12 17 14 10 8.6 5 1.6 3.2 2.7 5.9 7.9 7.6 7.3 1.8 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 150 64 41 47 43 37 23 33 33 39 18 16 12 6 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP I NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED NP NP NP I NP I NP I NPI NP I NP I NP INPI NPI 362 15081 646 1 198 1 160 1 99 1 118 1 144 1 90 1 149 62 76 48 34 22 39 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-17 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-18 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.7 1.1 0.7 ND ND 277 7.1 1.8 ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND 0.53 ND ND 0.9 ND 1.3 1.5 1.6 1.4 1.1 4.3 0.7 0.9 ND Chloroform NP NP NP NP NP NP NP NP NP NP NP 21.5 20 20 14 10 11 4.0 3.9 2.7 2 1.1 1.2 1.5 1.4 1 1.6 1.7 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene P NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene P NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND 0.98 ND ND ND Trichlorofluoromethane P NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane 1p P NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP ND IN ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene P NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane P NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORWATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP 1 22 1 20 1 21 1 14 1 10 1 12 1 4.0 1 5.9 1 5.3 1 4.3 1 2.5 2.3 284 9.2 4.3 1.7 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-18 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-19 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 8 5 13 16 7.7 16.0 19.0 NP NP NP NP NP NP NP NP NP Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND 1.1 2 0.58 1.10 1.60 NP NP NP NP NP NP NP NP NP Chloroform NP NP NP NP NP NP NP NP NP NP NP 1.51 1.1 3.3 4.1 3.3 6.8 5.9 NP NP NP NP NP NP NP NP NP Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND I ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 6 6.1 1.7 4.7 5.6 NP NP NP NP NP NP NP NP NP Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA I NA NA NP NP NP NP NP NP NP NP NP TOTAL CHLORWATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NPI NP I NP I NP 1 10 1 6 1 23 1 28 1 13 1 29 1 32 1 NP I NP I NP I NP NP NP NP NP NP Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-19 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-20 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.59 0.72 ND 0.79 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP I NP I NP I NP NP NP NP NP NP I NP NP ND I ND ND I ND I ND ND ND ND ND ND ND ND 0.59 0.72 ND 0.79 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-20 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-21 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd I 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND 1.5 0.64 ND 0.81 1.5 1.4 ND 1.1 0.81 ND 1.0 0.88 0.66 2.3 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP I NP I NPI NP NP I NP NP NP ND ND I ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane 1p NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP I ND I ND 1 1.5 1 0.6 1 ND 1 0.8 1 1.5 1 1.4 1 ND 1 1.1 1 0.8 ND 1.0 0.88 0.66 2.3 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-21 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-22 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd I 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND I ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP I NP I NPI NP NP I NP NP NP ND ND I ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane 1p NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP I NP NP I NP I NP I NPI NP I NP I NP I NP I NP I ND I ND I ND I ND I ND I ND I ND I ND I ND I ND I ND ND ND ND ND ND Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-22 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-23 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 M19911993 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 490 1,300 1,500 910 690 520 290 150 83 79 174 36 124 143 83 39 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 16.1 42 72 56 56 29 15 12 6.6 6.3 18.8 2.9 7.6 6.8 4.7 1.5 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 0.25 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 190 160 96 120 60 30 16 15 42 5.8 15 12 7 3 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED NP NP NP I NP I NP NP NP I NP I NP NP NP 506 1 1,352 1,762 1,126 842 1 669 1 365 1 192 1 106 1 100 1 234 45 147 162 95 43 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-23 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-24 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 930 550 360 230 120 120 54 17 NS NS 33 72 430 243 476 406 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 3.67 ND ND ND ND ND ND ND NS NS 0.82 1.1 2.7 6.2 3.0 2.9 Chloroform NP NP NP NP NP NP NP NP NP NP NP 6.07 ND ND ND ND ND ND ND NS NS ND ND ND ND ND 0.65 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS I ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND 7.1 ND ND ND ND NS NS 0.72 ND 2.0 1.4 6.8 8.1 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 13.84 1 ND ND I ND ND ND ND ND NS NS ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP I ND IND ND ND ND ND ND ND NS NS ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NS NS ND ND ND ND ND ND TOTAL CHLORWATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP 1944 15501 360 1 237 1 120 1 120 1 54 1 17 1 NS I NS 1 35 73 435 251 486 418 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; well was compromised, to be repaired in 2005. MW-24 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-25 Concentrations in Parts per Billion (µg/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 400 450 750 670 650 1,000 1,100 NP NP NP NP NP NP NP NP NP Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 80.6 88 130 170 140 190 270 NP NP NP NP NP NP NP NP NP Chloroform NP NP NP NP NP NP NP NP NP NP NP 0.43 ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND 11 ND ND NP NP NP NP NP NP NP NP NP 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 38 ND 38 100 71 NP NP NP NP NP NP NP NP NP Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP 2.14 5.8 ND ND ND ND ND NP NP NP NP NP NP NP NP NP Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP NP 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NP NP NP I NP NP NP NP NP NP TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NPI NP I NP I NP 1 483 15441 918 1 840 1 839 1 1,2901 1,441 1 NP I NP I NP I NP NP NP NP NP NP Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-25 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well MW-26 Concentrations in Parts per Billion (µgll) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.62 1.60 0.70 ND 0.51 ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP 12 9.9 7.6 7.7 4.8 4.3 2.7 ND 3.7 3.3 2.9 3.2 2.3 1.5 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP \D ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP INPI NP I NPI NP I NP I NP I NP I NP 1 12 1 10 1 7.6 1 7.7 1 4.8 1 4.3 1 2.7 1 ND 1 4.3 4.9 3.6 3.2 1 2.8 1.5 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-26 Prepared by: AWA 1022-36 Andres: Historical Well Tables 2013.xlsx Checked by: TJB Recovery Well RW-1 Concentrations in Parts per Billion (µg/l) Andres Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP 26,000 25,000 38,000 26,000 22,000 27,000 34,000 24,000 16,000 13,900 5,400 39,000 14,000 7,800 10,000 10,000 10,000 4,900 3,510 16,000 8,330 19,800 2,010 1,110 23 Trichloroethene NP NP 1,400 960 NO 700 920 870 1,200 1,400 1,200 924 1,400 7,100 1,100 640 530 NO 330 240 203 365 233 179 2,610 623 58 Chloroform NP NP ND ND NO 16 ND ND ND NO ND ND ND ND NO ND ND ND ND NO ND 1.1 ND ND NO ND 0.7 Vinyl Chloride NP NP ND 95 ND ND 38 49 ND ND ND ND ND 100 ND ND ND ND ND ND 3 ND ND ND ND 100 15 1, 1, 1 -Trichloroethane NP NP ND ND NO 12 ND ND ND NO ND ND ND ND NO ND ND ND ND NO ND ND ND ND NO ND ND 112-Trichloroethane NP NP NO ND NO ND ND 2.3 ND NO ND ND ND ND NO ND ND NO ND NO 2 ND ND ND NO ND ND 1,1-Dichloroethene NP NP ND ND ND ND ND 4.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9 2 1,2-Dichloroethane NP NP ND ND NO ND ND ND ND NO ND ND ND ND NO ND ND ND ND NO ND ND ND ND NO ND ND Trans 1,2-Dichloroethene NP NP ND ND ND 6 13 9 ND ND ND ND ND ND ND ND ND ND ND ND 3 3.3 ND ND 53 49 6 Cis 1,2-Dichloroethene NP NP NA NA NA NA NA NA NA NA NA NA NA 1 9,700 4,100 1,4001 1,400 1 810 1,300 1 590 594 417 293 168 7,610 15,200 1,740 Trichlorofluoromethane NP NP NO ND NO ND ND 12 ND NO ND ND NOrNDND ND ND NO ND NO ND ND NO ND NO ND ND 1,2-Dichloro ro ane NP NP ND ND ND ND ND ND ND ND ND ND NDND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP ND ND ND ND ND NO ND NO ND ND NDND ND ND ND ND 3 4.9 NO ND ND ND ND 1,4-Dichlorobenzene NP NP ND ND NO ND ND NO ND NO ND ND NOND ND NO ND NO ND 2.0 NO ND NO ND ND 1,1,1,2-Tetrachloroethane NP NP NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA 8.4 ND ND ND ND ND TOTAL CHLORINATEDS DETECTED NPI NP 1 27,400 1 26,055 1 38,000 1 26,734 1 22,971 1 27,947 135,200 1 25,400 1 17,200 1 14,8241 6,800 155,900 1 19,200 1 9,8401 11,9301 10,8101 11,6301 5,7301 4,318 116,802 8,856 20,147 12,283 17,0911 1,845 Quarterly groundwater sampling was initiated during the second quarter, 1993. NO = Not Detected at the method detection limit NA = Data not available. NP = Well not present at time of sampling RW-1 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.x1sx Checked by: TJB Recovery Well RW-2 Concentrations in Parts per Billion (µg/l) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP 1,400 2,800 740 1,800 900 1,990 2,500 930 2,000 1,700 1,700 1,200 260 99 110 76.7 AB AB AB AB AB Trichloroethene NP NP NP NP NP NP 91 290 330 95 ND 165 260 54 370 280 280 190 20 4.7 12 3.6 AB AB AB AB AB Chloroform NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Vinyl Chloride NP NP NP NP NP NP ND 9.2 ND ND ND ND ND 99 ND ND ND ND ND ND 3.1 ND AB AB AB AB AB 1,1,1-Trichloroethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1, 1 -Dichloroethene NP NP NP NP NP NP ND 0.73 ND ND ND ND ND ND ND ND ND ND ND ND 3.6 ND AB AB AB AB AB 1,2-Dichloroethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Trans 1,2-Dichloroethene NP NP NP NP NP NP ND 3.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Cis 1,2-Dichloroethene NP NP NP NP NP NP NA NA NA NA NA NA NA 420 480 210 230 140 42 44 210 5.9 AB AB AB AB AB Trichlorofluoromethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloro ro ane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB Chlorobenzene NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB AB 1,4-Dichlorobenzene NP NP NP NP I NP I NPI ND ND ND ND ND ND I ND ND ND I ND ND ND ND ND ND ND AB AB AB AB AB 1,1,1,2-Tetrachloroethane NP NP NP NP I NP I NP I NA NA NA NA NA NA I NA NA I NA I NA NA NA I NA NA NA ND AB AB AB AB AB TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NP I NP I NP 1,491 3,103 1,070 1,895 900 1 2,155 1 2,760 1 1,50312,8501 2,19012,2101 1,5301 322 1 148 1 339 1 86 AB AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit NA = Data not available. NP = Well not present at time of sampling RW-2 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well RW-3 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP 8,000 1,700 1,500 4,400 4,200 2,400 6,400 2,500 4,060 12,100 10,700 132 3 ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND 15 ND 8.2 ND ND 35 89 369 43.8 ND 71.3 1.4 ND Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP ND 3.7 ND 1.5 ND ND ND 1.3 1.3 ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND 40 11.9 1.2 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.79 ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 1.7 ND ND 14.7 0.87 ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 0.22 Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.97 ND ND ND 4.1 6.3 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND 18 ND 16 ND ND 51 120 992 59.8 ND 9,290 1,440 6 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.27 0.4 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP I NPINPI P NPI NP I NP NP I NP NP NA NA NA NA NA NA NA NA 1.2 ND#10,7001 ND ND ND TOTAL CHLOMNATEDS DETECTED NP NP NP NP NP NP NP NP NP NP NP NP NP 8,000 1,737 1,500 4,426 4,200 2,400 6,486 2,710 5,427 12,29,548 1 1.461 1 14 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-3 Prepared by: AWA 1022-36 Andres: Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well RW-4 Concentrations in Parts per Billion (µg/l) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 1st 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 4,000 1,000 1,200 3,000 1,900 640 610 3,050 AB AB AB AB AB Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 320 250 79 240 170 56 50 167 AB AB AB AB AB Chloroform NP NP NP NP NP NP NP NP NP NP NP I NP I NP NP I NP ND I ND ND ND ND ND I ND ND AB AB AB AB AB Vinyl Chloride NP NP NP NP NP NP NP I NP NP NP NP NP NP NP NP ND ND ND ND ND ND 22 ND AB AB AB AB AB 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 0.53 ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB AB Trans 1,2-Dichloroethene NP NP I NP I NP NP NP NP NP NP NP NP NP I NP NP NP ND 11 ND ND I ND ND 1.8 4.4 AB AB AB I AB AB Cis 1,2-Dichloroethene NP NP NP NP NP NP NP I NP NP NP NP NP NP NP NP 600 470 310 810 470 170 240 307 AB AB AB AB AB Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 1.1 ND ND ND ND ND ND AB AB AB AB AB 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB AB Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.79 AB AB AB AB AB 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB AB 1,1,1,2-Tetrachloroethane NP I NP I NP I NP NP NP NP I NP NP NP NP NP NP NP NP NA I NA NA I NA NA I NA NA 1.0 AB AB AB AB AB TOTAL CHLORINATEDS DETECTED NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 4,920 1,733 1,589 4,050 2,540 866 924 3,530 AB AB AB AB AB ND = Not Detected at the method detection limit. AB = Well abandoned. NP = Well not present at time of sampling. RW-4 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well RW-5 Concentrations in Parts per Billion (µg/l) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 1st 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 5,000 1,300 4,200 1,200 2,100 2,100 1,300 4,500 1,030 2,710 74 ND 35 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 560 410 430 82 170 160 130 240 58 140 70 ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP I NP I NP NP I NP ND I ND ND ND ND ND I ND 0.54 ND ND I ND ND ND Vinyl Chloride NP NP NP NP NP NP NP I NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 1.1 ND ND 14 ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 1.1 ND ND ND ND ND 0.5 ND ND 1.5 ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP I NP I NP NP NP NP NP NP NP NP NP I NP NP NP ND 12 ND ND I ND ND 2.6 7 ND ND 14.7 ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP I NP NP NP NP NP NP NP NP 770 850 1400 300 540 470 340 541 349 233 1,760 1 58 68 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 3.3 ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 1.2 ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND I ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA I NA 1 1.7 ND ND ND ND ND TOTAL CBLORINATEDS DETECTED I NPI NP I NP I NPI NP I NP I NP I NPI NPI NPI NP I NP I NP I NP I NP 1 6,330 1 2,576 16,030 1 1,582 1 2,810 1 2,730 1 1,773 1 5,293 1,437 1 3,083 1,934 1 58 103 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-5 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well RW-6 Concentrations in Parts per Billion (µg/l) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 1st 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 2,500 1,900 3,000 2,300 1,500 4,300 740 1,880 2,250 1,810 1,120 168 28 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 260 320 290 200 150 190 73 169 98 82 262 45 20 Chloroform NP NP NP NP NP NP NP NP NP NP NP I NP I NP NP I NP ND I ND ND ND ND ND I ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP I NP NP NP NP NP NP NP NP ND 1.8 ND ND ND ND ND ND ND ND ND 73.2 96 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND 1.4 3.2 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP I NP I NP NP NP NP NP NP NP NP NP I NP NP NP ND 3.5 ND ND I ND ND ND 4 ND ND 4.9 1 2.6 4.3 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP I NP NP NP NP NP NP NP NP 570 640 1,000 610 460 140 440 346 279 170 750 308 501 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.55 ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP I NP I NP I NP NP NP NP NP NP NP NP NP NP NP NP NA I NA I NA I NA NA NA NA 0.64 ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NP I NP I NPI NP I NP I NP I NPI NPI NPI NP I NP I NP I NP I NP 1 3,330 1 2,865 1 4,290 1 3,110 1 2,110 1 4,630 1 1,253 1 2,400 1 2,627 2,062 2,137 598 652 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-6 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB Monitoring Well RW-7 Concentrations in Parts per Billion (µg/l) Andrex Industries Asheville, North Carolina BLE Job Number J13-1022-36 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 2013 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 1st 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 2,300 1,300 2,200 2,300 2,100 1,700 700 855 2,090 2,880 107 41 57 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 250 220 400 300 280 200 98 95 104 158 10 8 18 Chloroform NP NP NP NP NP NP NP NP NP NP NP I NP I NP NP I NP ND I ND I ND ND ND ND I ND ND ND ND 11.1 1.2 ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 13 ND ND ND ND ND ND ND ND ND 12.6 14.7 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1.2 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 6.6 ND ND ND ND ND 2.3 ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 450 410 1,100 810 640 460 260 188 219 345 71.1 612 401 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloro ro ane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 4.2 ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP I NA NA NA NA NA NA NA ND ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NP I NP I NPI NP I NP I NP I NPI NP I NP I NP I NP I NP I NP I NP 1 3,000 1 1,954 1 3,700 1 3,410 1 3,020 1 2,360 1 1,058 1 1,141 2,413 3,383 1 200 1 675 492 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-7 Prepared by: AWA 1022-36 Andrex Historical Well Tables 2013.xlsx Checked by: TJB 10,000 111 7,000 bo 6,000 0 5,000 4,000 0 U 3,000 2,000 1,000 ,1 Total Chlorinated VOC Concentrations in MW-1 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 01 O — N M It kn 1�0 r- 00 01 O N M 't kn � r- 00 O N M 00 01 41 01 01 9 1 11 01 01 91 01 O O O O O O O O O O .--i •--� .--� --� U U U U U U U U U U U U U U U U U U U U U U U U U U N U N N N N N N U N N N 6> N N N N U N U N N N N N N Month -Year 800 700 600 500 0 400 c 300 W, 200 100 Total Chlorinated VOC Concentrations in MW-2 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 a1 O N M It N 00 01 O .--i N M It kf ) 00 01 O N M DD 01 01 D1 01 O O O O O O O O O O — — — — — U U U U U U U U U U U U U U U U U U U U U U U U U U Month -Year 20,000 18,000 16,000 14,000 12,000 0 10,000 8,000 0 L 6,000 4,000 2,000 1 Total Chlorinated VOC Concentrations in MW-3 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 01 O — N M It kn 00 01\ O .--i N M It kC) �O l� 00 01 O N M It 00 01 C�' C�' a1 a1 a, a1 a1 O O O O O O O O O O — — — — — U U U U U U U U U U U U U U U U U U U U U U U U U U =i=i=i==�=illlmillli=o=�=i=i=� Month -Year Total Chlorinated VOC Concentrations in MW-4 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 2,000 1,800 1,600 1,400 co EL 1,200 0 1,000 800 0 U 600 !III17 200 0 Ii i i i i i i i i i i i i i i i i i i i i i i i I M It W') t` 00 a1 O N M It N 1.0 � 00 a\ O -- N M U U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N N N N N N N N N N N N N Month -Year 60,000 50,000 tin 40,000 0 30,000 0 U 20,000 10,000 Total Chlorinated VOC Concentrations in MW-5 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 kn 00 C1 O — N M Zt kn `O l� 00 O - N M 00 O1 O O O O U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N U N U U N N N U N U U N N N U N U U N N N Month -Year Total Chlorinated VOC Concentrations in MW-6 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 50,000 45,000 40,000 35,000 co 30,000 0 0 25,000 0 20,000 0 L 15,000 10,000 5,000 0 i i i i i i i -ii i i i i :� i 01 O N M l� 00 D\ O -- N M It W) �10 l� 00 01 O -- N M N N N N N N N N N N N N N N N N N N N N N N N N N N A Q A Q A Q Q Q Q Q Q Q Q Q Q Q A A Q A A A A Q Q Q Month -Year 200 180 160 140 co 120 0 100 80 0 60 40 20 Total Chlorinated VOC Concentrations in MW-7 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 ^� N M It N \O r- 00 C1 O M 'IT k � 00 U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N U N N N U U U N N N U N N N Month -Year 1,800 1,600 1,400 1,200 cn c 1,000 800 0 0 U 600 m 200 Total Chlorinated VOC Concentrations in MW-8 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 M It ti) �10 l 00 d\ O .--i N M 4 to �10 l— 00 M U U U U U U U U U U U U U U U U U U U U U U U U U U Month -Year Total Chlorinated VOC Concentrations in MW-SA 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 7,000 CIO 5,000 co c 4,000 3,000 0 0 L 2,000 1,000 0! i i i i i i i i i i i i i i i i i i i i i i i Cl) O 1- N M It V) \C � 00 01 O N M It Ln l� 00 O\ O N M Co O1 91 91 91 91 91 a1 a1 U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N N N N N N N N N N N N N N Month -Year Total Chlorinated VOC Concentrations in MW-9 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 7,000 m 5,000 co 0 4,000 C c� 3,000 0 0 U 2,000 1,000 0 I i i i i i i i i i i i i i i i i i M V) l 00 O-1 O .--i N M 't kn �10 r- 00 M Month -Year f 12,000 10,000 8,000 6,000 0 4,000 2,000 Total Chlorinated VOC Concentrations in MW-10 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 M It kn 00 01 O N M kn �10 rl- 00 00 D1 01 01 D1 01 D1 01 O O O O O O U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N U N U N N N N N N U N N N Month -Year Total Chlorinated VOC Concentrations in MW-11 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 6,000 5,000 4,000 cn 0 3,000 0 U 2,000 1,000 0 I i i i i i i i i i i i i i i i i i M V) l 00 O-1 O .--i N M 't kn �10 l- 00 M U U U U U U U U U U U U U U U U U U U U U U U U U U Month -Year Total Chlorinated VOC Concentrations in MW-12 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 8,000 7,000 6,000 5,000 0 4,000 c 3,000 2,000 1,000 O 01 O N M It kf) C­ 00 0� O N M 't kn 110 00 M ON 1 1 1�1 a1 a1 O O O O O O O O O O — — — — — U U U U U U U U U U U U U U U U U U U U U U U U U U Month -Year Total Chlorinated VOC Concentrations in MW-13 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 8,000 7,000 6,000 5,000 0 4,000 c 3,000 A 2,000 1,000 0 m It kn � 00 O" O M � kn 110 � 00 ON O N M DD 01 01 a1 a1 41 a1 O� D\ Cn Cn O O O O O O O O O O -� U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N U U U U U U U U N N N N N N U Month -Year Total Chlorinated VOC Concentrations in MW-14 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 1,800 1,600 1,400 1,200 cn c 1,000 800 0 0 U 600 I11 200 0 I i i i i i i i i i i i i i i i i i M V) l 00 O-1 O .--i N M 't kn �10 l- 00 M U U U U U U U U U U U U U U U U U U U U U U U U U U Month -Year Total Chlorinated VOC Concentrations in MW-15 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 800 700 600 500 0 400 u c 300 U 200 100 0 M It kf) l� 00 01 O .--i N M It kn �O l� 00 41 O - N M DD 01 a1 a1 01 O O O O O O O O O O U U U U U U U U U U U U U U U U U U U U U U U U U U U N N U N N N U N N U N U U N N U N N U N N N U N N A Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q A Q Q A Q Q Q Q Q Q Month -Year Total Chlorinated VOC Concentrations in MW-16 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 500 450 L OIC 350 co 300 0 250 200 0 U 150 100 50 0 01 O - N M V') 00 01 O - (Iq M 't kr) \10 [__ 00 01 O O O O O O O O O O U U U U U U U U U U U U U U U U Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Month -Year 700 600 500 0 400 0 c� 300 0 0 200 100 Total Chlorinated VOC Concentrations in MW-17 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 + N M It kn 00 O\ O N M It kn \O l 00 a1 O N M O\ O\ O\ O\ O\ O\ O\ O\ O\ O O O O O O O O O O '--+ '--+ •--+ '--+ '--+ U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N N N N N N N N N N N N A A A A A A A A A A A A A A A A A A A A A A A A Month -Year Total Chlorinated VOC Concentrations in MW-18 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 300 250 200 co 0 150 Lj 100 50 0 I i i i i i i i i i i i i 11� -�i i • i T� O1 O '--+ N m It W) \O l� 00 01 O 00 O\ O N M Co a, 91 91 a, a1 91 a, U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N N N N N N N N N N N N N N Month -Year Total Chlorinated VOC Concentrations in MW-19 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 35 30 25 U 10 _5 0 01 O N M rl- 00 C� O -- N M kr) IC U U U U U U U U U U U U U U U U U U N N N N N U N N N N N N N N U N U N Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Month -Year r- 00 01 O -- N M U U U tj U U U U Q Q Q Q Q Q Q Q Total Chlorinated VOC Concentrations in MW-20 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 0.90 WE 0.70 0.60 0.50 0.40 t j 0.30 0.20 0.10 i i i i i i i L V 1 i I 0.00 Ti�i�����i T .�� (71\ O N M It kn O ---+ N M It W) 110 l� o0 01 O ' + N M 't O O O O O O O O O O ---+ ---+ ---+ •--+ ---+ U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N U N N N N N N U N N N N N N U N N N N N Month -Year A Total Chlorinated VOC Concentrations in MW-21 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 2.50 2.00 0.50 0.00 i s 1 i i i \0 i i i 1Ji i i i \✓ i i i i N cn 't kn �10 l� 00 01 O — N cn kn �10 l— 00 00 01 O� a1 a1 a1 a1 D1 a1 a1 a1 O O O O O O O O O O -� -� N N N N N N N N N N N N N N N N N N N N N N N N N N Q Q Q Q Q Q Q A Q Q Q A Q Q Q Q Q A Q Q Q A A Q Q Q Month -Year Total Chlorinated VOC Concentrations in MW-22 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 1.00 0.90 mm 0.70 0.60 0 0.50 0.40 0 L 0.30 0.20 0.10 0.00 N M lzt kr) 00 a1 O -- N M It kn r- M 00 O� a1 01 01 O� a1 01 01 O O O O U U U U U U U U U U U U U U U U U U U U U U U U U U N U N N N N U N N N N N N N U N N N N U N N N N U N =i=i===nEEL_W!�' Month -Year Total Chlorinated VOC Concentrations in MW-23 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 2,000 1,800 1,600 1,400 co 1,200 0 a 1,000 800 0 L M 200 0 I i i i i i i i i i i i ii i i -i M kn r­ 00 O*1 O N M lzt kn �10 t` 00 C1 O 00 01 O� 01 01 O� 01 01 ON O O O O O O O O O U U U U U U U U U U U U U U U U U U U U U U U U U U N N U N N N U N N N U N N N U N N N U N N N U N N N Month -Year Total Chlorinated VOC Concentrations in MW-24 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 1,000 900 800 700 co 600 0 500 400 0 A 300 200 100 0 kn `O r- 00 C1 O M It kn �10 � 00 M U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N U N N N N N N N N U N N N N N N U N U N N Month -Year 1,600 1,400 1,200 1,000 0 800 c 600 A 400 200 Total Chlorinated VOC Concentrations in MW-25 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 M tf) \�O 1` 00 a1 O N \C r- 00 U U U U U U U U U U U U U U U U U U U U U U U U U U U N N N U N N N N N N N U N N N U N N N N N N N N N Month -Year 14 12 10 4 2 Total Chlorinated VOC Concentrations in MW-26 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 N M V) l-- 00 01 O N M It tn �10 r- 00 d\ O N M O� O� O� 01 O� O� 01 O� 01 O O O O O O O O O O •--� --� --� •--� --� U U U U U U U U U U U U U U U U U U U U U U U U N U N N N U U U N U N N U U N N N U N N U U N N Q Q Q A Q Q Q Q Q Q Q A Q Q Q Q Q Q Q A Q Q Q Q Month -Year Total Chlorinated VOC Concentrations in RW-1 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 60,000 50,000 40,000 tin 0 30,000 0 U 20,000 10,000 01 ii i i i i i i i i i i i i i i i i i i i i 0� O N M 't tf) l- 00 01 O -- N M 't kn \O � 00 D\ O -- N M N N N N N N N N N N N N N N N N N N N N N N N N N N Month -Year Total Chlorinated VOC Concentrations in RW-2 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 3,500 3,000 2,500 co :~ 2,000 0 U 1,000 500 O to 11O l- 00 D\ O N M It N r- 00 N N N N N N N N N N N N N N N N N N N N N N N N N N Month -Year Total Chlorinated VOC Concentrations in RW-3 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 14,000 12,000 10,000 c 8,000 6,000 0 0 4,000 2,000 0 1 i i i i i i i i i i i i i i i i i i i i i i i ~Ti O N M 't W) r- 00 a1 O ^--+ N M It kn 110 l� 00 01 O + N M 00 01 a1 a1 a, a1 0, a1 a\ 01 a1 O O O O O O O O O O '--+ --+ •--+ '--+ •--+ U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N N N N N N N N N N N N N N Month -Year Total Chlorinated VOC Concentrations in RW-4 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 6,000 5,000 cn 4,000 0 3,000 0 U 2,000 1,000 0! i i i i i i i i i i i i i i i i i i i i i i i Q1 O — N M It W , `0 [— 00 01 O - N M It kn 110 r- 00 01 00 11 11 11 1 1 a1 11 11 11 Cn 01 O O O O O O O O O O U U U U U U U U U U U U U U U U U U U U U U U U U U N U N U N U U U U N N N U U U N N U U U U N N U U N Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Month -Year Total Chlorinated VOC Concentrations in RW-5 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 7,000 6,000 5,000 c 4,000 3,000 0 0 2,000 1,000 0 1i i i i i i i i i i i i i i i .! _�. O -- N M 't kn 00 01 C "t vn 110 l� 00 N N N N N N N N N N N N N N N N N N N N N N N N N N Q A Q Q A Q Q A Q A A Q A A Q Q Q Q Q A Q Q A Q Q A Month -Year Total Chlorinated VOC Concentrations in RW-6 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 5,000 4,500 111 3,500 co 3,000 0 2,500 2,000 0 L 1,500 1,000 500 0 N M It kf) �10 r­ 00 C� O -- N M It kf) r- 00 a1 O -- N M U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N N N N N N U N N N N N N N Month -Year Total Chlorinated VOC Concentrations in RW-7 3rd Quarter 1991- 3rd Quarter 2013 Andrex Industries, Asheville, NC BLE Job No. J13-1022-36 4,000 3,500 3,000 2,500 c 0 2,000 u c 1,500 L 1,000 500 0 I I I I I I I I I I I I I I I I I I i i i i i i I 01 O ---+ N M It V'1 \p ll- 00 01 O ^--+ N M It to \D r- 00 01 O N M 00 01 01 01 01 01 01 01 01 01 01 O O O O O O O O O O '--+ •--+ '--+ '--+ '--+ U U U U U U U U U U U U U U U U U U U U U U U U U U N N N N N N N N N N N N N N N N a> N N N N N N N N N Month -Year