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HomeMy WebLinkAboutWI0100106_Annual Report_20130717MIL13 BUNNELL-LAMMONS ENGINEERING, INC. GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS REPORT OF ANNUAL GROUNDWATER AND SURFACE WATER SAMPLING AND ANALYSIS FOR 2012 FORMER ANDREX INDUSTRIES CORP. 180 DEAVERVIEw ROAD ASHEVILLE, NORTH CAROLINA BROWNFIELDS PROJECT NUMBER 07022-03-11 PREPARED FOR: ANDREX INDUSTRIES CORP. ASHEVILLE, NORTH CAROLINA PREPARED BY: BUNNELL-LAMMONs ENGINEERING, INC. GREENVILLE, SOUTH CAROLINA JULY 17,2013 BLE PROJECT NUMBER J12-1022-34 IHSB ID NUMBER NONCDO001271 GROUNDWATER INCIDENT NUMBER 6586 CAR 1 5 TO LO w I fell 1001 NILE BUNNELL-LAMMONS ENGINEERING, INC. GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS July 17, 2013 Andrex Industries Corp. C/O The Van Winkle Law Firm 11 North Market Street Asheville, NC 28801 Attention: Mr. Mark Pinkston, PA Subject: Report of Annual Groundwater and Surface Water Sampling and Analysis for 2012 Former Andrex Industries Corp. 180 Deaverview Road Asheville, North Carolina BLE Project Number J12-1022-34 Brownfields Project Number 07022-03-11 11-ISB ID Number NONCDOOO 1271 NCDENR Groundwater Incident Number 6586 Dear Mr. Pinkston: As authorized by Andrex Industries Corp. acceptance of our proposal number P12-0459 dated July 31, 2012, Bunnell-Lammons Engineering, Inc. (BLE) has performed required environmental services at the subject site. The purpose of this project was to collect and analyze groundwater and surface water samples as required by the North Carolina Brownfields Program. The enclosed report describes the work performed and presents the results obtained. Project Information: The following information was obtained from our previous work at the Andrex site (1991 through present) and from our conversations and emails with Mr. Buddy Gaither and Mr. Jack Levins of Milkco, Inc., Mr. Drew Stahlman, Mr. Stephen Gilman, and Mr. Mark Davies of Stahlman Consulting, and Mr. Daniel Stiles of EAS Professionals, Inc. Andrex formerly owned and operated an industrial textile production facility located at 180 Deaverview Road within the city limits of Asheville, North Carolina (Figure 1). The company operated a knitted fabric weaving and cutting business for women's and children's clothing at this location. In prior years, the facility was operated as a textile finishing business that conducted cutting, dry cleaning, shrinking and packaging of fabrics. The subject facility was in operation since the mid 1960s, although under various ownership. A two-story light manufacturing facility with approximately 77,000 square feet of office, manufacturing, warehouse, storage and utility space occupied the approximately nine -acre site. Two buildings were present at the site; a split level brick building and slab -on -grade metal building. No dry cleaning has been conducted on site since 1995. However, prior to 1995, dry cleaning operations were prevalent on site and the use of tetrachloroethylene (a.k.a. Perchloroethylene, PCE) 6004 PONDERS COURT PHONE (864) 288-1265 GREENVILLE, SOUTH CAROLINA 29615 FAx (864) 288-4430 MILE Androc Industries — 2012 Groundwater Monitoring July 17, 2013 Asheville, NC BLE Project Number J12-1022-34 was common. Virgin PCE was stored on site in a 6,000-gallon underground storage tank (UST). Prior to 1989, the use of the PCE UST was discontinued and the tank was filled with sand. The UST was replaced with a 6,000-gallon AST which was used until 1995. In 1995, dry cleaning processes and the use of PCE were discontinued. In 1991 concentrations of PCE were detected in the groundwater above the applicable North Carolina Title 15A Subchapter 2L (NC2L) groundwater standards' maximum level of 0.7 gg/l and the NCDENR issued Groundwater Incident Number 6586 for the site. Concentrations of PCE were also documented in the soil near the PCE UST and at other subsurface facility locations. The NCDENR approved a comprehensive site assessment (CSA) and corrective action plan (CAP) for the site and remedial efforts were conducted from 1993 through 2005. Remedial efforts consisted of the installation and operation of two groundwater pump and treat (P&T) systems and one soil vapor extraction (SVE) system. The SVE and both groundwater P&T systems were operated and maintained by BLE for Andrex. from May 2003 through August 2005. Treated groundwater effluent was discharged to the sanitary sewer under a MSD permit. BLE also performed annual site -wide groundwater and surface water sampling and analysis for Andrex to monitor the fate of the groundwater plume. BLE submitted quarterly reports of the remedial progress through August 2005 and annual groundwater monitoring reports through 2005 to the NCDENR to document site activities. The remediation system operations were suspended in August 2005 at the discretion of the property owner. Annual groundwater monitoring was also suspended at the discretion of the property owner, with the last sampling event conducted in November 2005. In early 2005, Andrex requested that BLE evaluate feasible remedial alternatives for the site. A preliminary review of alternate remedial technologies identified a unique opportunity to evaluate bioremediation at the site. Food -grade lactate containing byproducts (milk solution) from the neighboring Milkco, Inc. (Milkco) facility were being considered for use as a bio-enhancing remedial product for the former Andrex. facility. The implementation of this type of remedial action is dependent upon the results of a feasibility study which includes bench and field testing studies of the lactate containing byproducts. In 2005, Andrex retained BLE to perform a pilot study of the milk byproducts. The study was to include two parts. The first part was a bench test which was to be followed by a field trial. BLE completed the bench study in early 2006. The results showed a net decrease in PCE concentration of 30% after 40 days in those microcosms containing the highest concentrations of milk solution. Significant concentrations of PCE daughter products were also produced in the bench study indicating successful de -chlorination of the parent product, as anticipated. The field trial portion of the pilot test was suspended by Andrex after the bench test results were obtained. In 2006, Milkco entered into a Brownfield's Agreement (Agreement) with the State of North Carolina as part of a potential purchase of the Andrex property. The property was sold in 2007 and as part of the plan (see below) for retrofit of the subject site; Milkco removed and/or demolished selected equipment and facility infrastructure. MILE Androc Industries — 2012 Groundwater Monitoring July 17, 2013 Asheville, NC BLE Project Number J12-1022-34 In August 2007, three underground storage tanks (one PCE and two heating oil) were removed and disposed by a contractor retained by Milkco on behalf of Andrex. The results of the activities were documented in a report titled Report of Limited Assessment for UST Closure dated November 26, 2007 (BLE Project No. J07-1022-20). As part of Milkco's redevelopment plans for the site, BLE issued a plan titled Work Plan for Redevelopment of the Andrex Brownfields Site (Milkco Cooler Expansion) dated June 13, 2008 (BLE Project No. J08-1022-23). The plan addressed the Program's requirements including excavation and disposal of contaminated soil (source area) and continued groundwater monitoring. The Program reviewed and approved (with modification) the plan in a letter to BLE dated July 7, 2008. The schedule for implementation of the redevelopment plan was changed on December 11, 2008 with concurrence of the Program. In July 2008, BLE abandoned selected groundwater monitoring and recovery wells in accordance with the approved redevelopment plan. The results of the well abandonment activities were documented in a report titled Report of Well Abandonment Services for the Milkco Cooler Expansion dated January 19, 2009 (BLE Project No. J08-1022-26). From July through September 2008, contaminated soils were removed and disposed by a contractor retained by Milkco in accordance with the approved redevelopment plan. The results of the remedial activities were documented in a report titled Report of Hotspot Soil Removal and Disposal for the Milkco Cooler Expansion dated June 3, 2009 (BLE Project No. J08-1022-25). By December 2008, the former Andrex brick building(s) and metal building had been demolished with only the building slabs remaining. Additionally, all groundwater and soil rernediation systems had been dismantled, removed, and stored by Milkco. All work performed by Milkco (non - responsible party) is in compliance with the requirements of the NCDENR Brownfields Program (Program) and the Agreement. In February 2008, Andrex resumed annual groundwater monitoring at the site. BLE has performed the sampling services and prepared and submitted reports each calendar year since 2008. The approved redevelopment plan requires the continuation of annual groundwater monitoring and remedial activities at the site. BLE has completed the required annual groundwater monitoring for the 2012 calendar year. The enclosed report describes the work performed and presents the results obtained as required in the approved redevelopment plan (et seq.). IBLIH Androc Industries — 2012 Groundwater Monitoring July 17, 2013 Asheville, NC BLE Project Number J12-1022-34 Scope of Services: On September 10, 2012, groundwater levels were measured and on September 10-13, 2012 samples were collected from the monitoring and recovery wells, as required. Groundwater sampling logs are included in Appendix A. Samples were collected from all wells except MW-1 through MW-4, MW-8, MW-8A, MW- 19, MW-25, RW-2, and RW-4 as these wells were not present at the time of sampling (abandoned or destroyed). Samples were also collected from affected surface waters on September 13, 2012. The samples were analyzed at Pace Analytical Services, hic. (Pace), in Huntersville, North Carolina by EPA Method 8260 MSV Low Level (Appendix B). Water levels and groundwater elevations measured prior to sampling are shown on Table 1. A groundwater elevation contour map is included as Figure 2. Results of Groundwater Sampling: Chlorinated volatile organic compounds (VOCs) detected in the groundwater samples above the North Carolina standards (based on North Carolina's Class GA Groundwater Standards T 1 5A Subchapter 2L) include but are not limited to: tetrachloroethene, trichloroethene, cis- 1,2-dichloroethene, and vinyl chloride (Table 2). A historical contaminant concentration database and total chlorinated VOC data plots are presented in Appendix C. The data plots were visually evaluated and our interpretations of the overall contaminant trends from the initial sampling date of each well are presented below. Declining Stable Increasing Non -Detect MW-l** MW-9 MW-7 MW-20*** MW-2** MW-13 MW-12 AAA MW-21 *** MW-3** MW-14 MW-15 MW-22 MW-4** MW-18 MW-16 MW-5 MW-24 MW-19* T%4W-6 MW-26 MW-25* MW-8** RW-1 MW-8A** RW-4** MW-10 MW-11 MW-17 MW-23 RW-2** Rw-3 RW-5 RW-6 RW-7**** Well destroyed in 2003; not present at the time of the 2009 sampling event. Well abandoned after the 2008 sampling event (see subsequent sections of this report). Detected concentrations of chloroform are unrelated to the groundwater incident. -- Well is broken and filled with roots and milk solution as of September 2011. Due to decreasing concentrations of PCE and increasing concentrations of daughter product. 11 IBLIH Androc Industries — 2012 Groundwater Monitoring July 17, 2013 Asheville, NC BLE Project Number J12-1022-34 Status of Well Conditions: Monitoring wells MW-19 and MW-25 were destroyed in 2003 and MW-24 was damaged in late 2003 or early 2004. Recall that MW-19 was located on the Satterfield residential property and that MW-24 and MW-25 were located on the Milkco property (Figures 2 and 3). Sampling of monitoring wells MW-19 and MW-25 could not be performed in 2003 and beyond because the wells had been destroyed. Monitoring well MW- 19 appears to have been destroyed by grading in 2003, presumably by the City of Asheville, who graded the area for routing of storm water. The well cap was found on the ground surface but no other parts of the well could be located. Monitoring well MW-25 was destroyed by grading by contractors working for Milkco. The work was part of a facility expansion at Milkco in the summer of 2003. No traces of the well could be located. Neither BLE nor Andrex. was contacted prior the destruction of these wells. The well head of MW-24 was damaged by grading contractors working for Milkco. The work was part of a facility expansion at Milkco in late 2003 or early 2004. BLE personnel observed surface water leaking into the damaged well head and made temporary repairs to stop the infiltration of surface water in 2004. In 2005 the well head was permanently repaired however it appeared that the well riser pipe was bent at about five feet below ground surface at the time the well head was damaged. We were unable to lower a bailer or well pump into MW-24 due to the bent riser pipe. The well was not sampled in 2004 or 2005. We recommended permanent abandonment and replacement of MW-24 in 2005. After approval by the responsible party, BLE completed abandonment and reinstallation of MW-24 in 2007. In the summer of 2008 (after sampling was conducted in February 2008), several of the monitoring and recovery wells were abandoned as part of the property redevelopment plan approved by the Program. A report of well abandontrient was submitted under separate cover. Monitoring well MW-6 and recovery well RW-1 were extended to the ground surface as part of the grading activities for the Milkco expansion (new roadway). The well heads were reconstructed and the well elevations were resurveyed by BLE. The water level and well construction data on Table I reflects the changes. Please note that the extension of MW-6 resulted in a deviation (bend) of the riser pipe below the ground surface. A bailer cannot be lowered down the well so sampling was performed using a check valve and poly tubing. Purge volumes are significantly reduced using this method compared to conventional bailing. Results of Surface Water Sampling: The laboratory results of the surface water sampling are consistent with previous sampling events. Chlorinated VOCs detected in the surface water samples above the North Carolina standards (based on North Carolina's Class WS Surface Water Standards T 1 5A Subchapter 213) include tetrachloroethene and trichloroethene (Table 2). The former sample location Smith Mill I (SM-1) was collected from a small garden pond on the former Jehovah Witness property prior to 2005. The former pond was filled in by the new owners of the Jehovah Witness property sometime after November 2004. The SM-1 sample location was moved in 2009 to the location shown on Figure 3 based on the 2008 results. 5 MILE Androc Industries — 2012 Groundwater Monitoring July 17, 2013 Asheville, NC BLE Project Number J12-1022-34 A surface water sample QW-1) was collected from the former Jehovah Witness property in 2010 as in prior years (Figure 3). The sample was collected from a drainage feature in an area that appeared to be a spring. The results from this year and prior years (2002 through 2005) indicate that the drainage feature is a groundwater discharge point for northernmost contaminant plume. It is apparent from the data that the discharge at the former Jehovah Witness spring directly affects the surface water quality in Smith Mill Creek Tributary at down gradient sampling locations (SM-4 through SM-6) shown on Figure 3. The sampling locations (SM-1 through SM-6) in Smith Mill Creek Tributary will remain the same in 2013. Sampling of surface water for Total Organic Carbon was performed this year as required in the UIC Permit. These data cannot be compared to pre - injection values since no historical data exists. The laboratory data is included in Appendix B. Remediation Progress: A groundwater pump and treat system (upper system) and a SVE system were installed at the site in the mid 1990's. Groundwater was recovered from two recovery wells RW- 1 and RW-2 attached to the upper system. Upgrades to the groundwater recovery systems were completed in 2002. The upgrades included the addition of one recovery well (RW-3) to the upper system and construction of a new lower system and the installation of four new lower system recovery wells (RW-4 through RW-7). After 2002, contaminated groundwater was recovered by seven recovery wells RW-1 through RW-7. Groundwater recovery from RW-1 through RW-3 (upper system) was restarted on March 25, 2002. Groundwater recovery from RW-4 through RW-7 (lower system) began on May 23, 2002. The system upgrades were documented in a report titled As -Built Engineering Plans and Specification Groundwater Pump and Treat Systems (2002 Upgrade) dated February 5, 2003. Operation of both groundwater systems was discontinued on August 23, 2005 and the funds for operation of the systems were diverted to a laboratory -scale (bench) pilot test of an alternate remedial technology. The bench test was completed in 2006, however reporting of the results was suspended by Andrex while the Brownfields Agreement was in progress. As part of the site redevelopment plan, the results of the bench test and plans for future groundwater remediation were submitted to the Program. The SVE system has not been operational since November 2004 when a power surge (presumed lightning strike) damaged the system. Repairs were not made as Andrex had proposed a discontinuance of SVE remedial operations to the NCDENR at that time. Repairs were contingent on the initiation of the pilot test described above. Andrex opted to conduct the pilot test and therefore the SVE system was not repaired. In the summer of 2008, as part of the approved redevelopment plan, both groundwater systems and the SVE system we disassembled and the equipment was placed in storage by Milkco. Additionally, as part of the redevelopment plan, "hotspot" soils (contaminated soils with concentrations above a specified limit) were removed and disposed by Milkco on behalf of Andrex. A report of soil removal and disposal was submitted under separate cover. An underground injection control permit was obtained from the NCDWQ on December 22, 2010. The permit was part of a green/sustainable enhanced bioremediation approach utilizing milk solution. M IBLIH Androc Industries - 2012 Groundwater Monitoring Asheville, NC July 17, 2013 BLE Project Number J12-1022-34 The injection plan included an injection schedule over 5 years with semi-annual injections planned for the first two years. We proposed to conduct the project in phases with the first phase including two injection events (and monitoring) within a 12-month period (designated "Year One" in the plan). BLE was retained by Milkco to perform the injection and monitoring services in 2011 through early 2013. Subsurface injection of m- ilk solution into former groundwater recovery wells were performed in [May to June 2011], [September to October 2011], and [September to October 2012] and monitoring was conducted as planned. The most recent monitoring event was conducted in March 2013. The results show that daughter products of PCE are being created as anticipated. Significant reduction in solvent concentrations has been observed in the RW-5 injection area. As a result, the contour map of the total VOC plume is now split into two discrete zones. Additionally, is should be noted that a majority of the total VOCs in the RW-3 injection area is now daughter product (cis 1,2- DCE). An injection project interim evaluation report is in progress and will be submitted under separate cover as required in the UIC permit. We anticipate submitting a permit renewal application and full-scale injection plan by July 30, 2013. Qualification of Report: The activities and evaluative approaches used in this assessment are consistent with those normally employed in hydrogeological assessments of this type. Our evaluation of site conditions has been based on our understanding of the site and project information and the data obtained during our annual sampling effort. This report has been prepared on behalf of and exclusively for the use of Andrex Industries Corp. This report and the findings contained herein shall not, in whole or in part, be disseminated or conveyed to any other party or used or relied upon by any other party excluding NCDENR, without BLE's prior written consent. Closing: We appreciate the opportunity to serve as your environmental consultant on this project. Please contact us at (864) 288-1265 if you have any questions or comments regarding this report. Sincerely, BuNNELL-LAMMONs ENGINEERING, INC. Senior Hydrogeologist Registered, North Carolina #2025 cc: Ms. Tracy Wahl - DWM Brownfields Program &ITC/ a16144w�� Andrew W. Alex9fider, P.G. Senior Hydrogeologist Registered, North Carolina #1475 c: lawalactive projects landrex milkcolphase34 gw samp 20121andrex report of 2012 groundwater 1022-34 draft.doc TABLES Table 1 Well Construction and Groundwater Elevation Data Andrex Industries Asheville, North Carolina NCDENR Groundwater Incident Number 6586 BLE Project No. J12-1022-34 September 10, 2012 Well Well Location Meas. Pt. Elevation Gnd. Surface Elevation Depth to Water (bmp) Water Elevation *Total Borehole Depth (bgs) *Screen Depth (bgs) *Screen Elevation Well Well *Top of Rock *Top of Type Monitors Depth(bgs) RockElev. MW-1 On -Site 2222.34 2222.58 NP-A NP-A 46.2 31.2 - 46.2 2191.4 - 2176.4 lIIs BR 35.0 2187.6 MW-2 On -Site 2222.28 2222.62 NP-A NP-A 45.0 28.0 - 43.0 2194.6 - 2179.6 HIS BR 29.0 2193.6 MW-3 On -Site 2210.40 2207.76 NP-A NP-A 55.0 40.0 - 55.0 2167.8 - 2152.8 11 BR 36.5 2171.3 MW-4 On -Site 2206.87 2207.04 NP-A NP-A 86.7 51.7 - 86.7 2155.3 - 2120.3 Ills BR 26.0 2181.0 MW-5 On -Site 2216.75 2216.92 46.30 2170.45 53.0 43.0 - 53.0 2173.9 - 2163.9 Ills BR 37.0 2179.9 MW-6 On -Site 2218.43 2218.67 53.64 2164.79 71.9 50.4 - 70.4 2168.3 - 2148.3 ILI PWR 56.4 2162.3 MW-7 On -Site 2218.35 2218.60 26.21 2192.14 35.0 24.5 - 34.5 2194.1 - 2184.1 H BR 12.0 2206.6 MW-8 On -Site 2182.33 2182.63 NP-A NP-A 24.5 13.0 - 23.0 2169.6 - 2159.6 H PWR 22.0 2160.6 MW-8A On -Site 2182.52 2182.70 NP-A NP-A 35.0 30.0 - 35.0 2152.7 - 2147.7 Ills BR 15.5 2167.2 MW_9 On -Site 2175.57 2175.95 25.72 2149.85 60.0 44.0 - 54.0 2132.0 - 2122.0 H BR 34.0 2142.0 MW-10 On -Site 2159.92 2159.45 16.21 2143.71 39.0 29.0 - 39.0 2130.5 - 2120.5 H PWR 35.0 2124.5 MW-1 1 On -Site 2166.00 2166.39 25.18 2140.82 58.5 48.0 - 58.0 2118.4 - 2108.4 11 SAP >80.0 <2086.4 MW-12 On -Site 2219.17 2219.49 49.28 2169.89 81.0 60.0 - 70.0 2159.5 - 2149.5 H PWR 71.0 2148.5 MW-13 Off -Site 2138.80 2138.96 2.50 2136.30 58.5 48.0 - 58.0 2091.0 - 2081.0 11 SAP 58.5 2080.5 MW-14 Off -Site 2138.94 2139.20 0.18 2138.76 75.0 65.0 - 75.0 2074.2 - 2064.2 Ills BR 59.0 2080.2 MW-15 Off -Site 2124.89 2125.18 11.63 2113.26 40.0 33.3 - 40.0 2091.9 - 2085.2 1110 BR 32.5 2092.7 MW-16 Off -Site 2124.59 2124.85 11.49 2113.10 33.5 23.5 - 33.5 2101.4 - 2091.4 H PWR 33.5 2091.4 MW-17 Off -Site 2094.64 2094.74 3.74 2090.90 14.2 4.0 - 14.0 2090.7 - 2080.7 H SAP 14.2 2080.5 MW-18 Off -Site 2101.81 2101.92 9.33 2092.48 59.0 49.0 - 59.0 2052.9 - 2042.9 H SAP 59.0 2042.9 MW-19 Off -Site 2127.61 2127.82 NP-D NP-D 58.0 48.0 - 58.0 2079.8 - 2069.8 11 SAP 58.0 2069.8 MW-20 Off -Site 2180.55 2180.54 36.32 2144.23 77.0 67.0 - 77.0 2113.5 - 2103.5 H SAP 77.0 2103.5 MW-21 Off -Site 2091.17 2091.31 1.59 2089.58 36.5 26.5 - 36.5 2064.8 - 2054.8 H SAP 36.5 2054.8 MW-22 Off -Site 2090.71 2090.84 0.75 2089.96 57.0 47.0 - 57.0 2043.8 - 2033.8 ]Ills BR 46.0 2044.8 MW-23 Off -Site 2145.05 2145.20 26.72 2118.33 41.5 31.0 - 41.5 2114.2 - 2103.7 HIO BR 30.0 2115.2 MW-24 Off -Site 2225.37 2225.49 61.72 2163.65 110.0 70.0 - 80.0 2155.5 - 2145.5 H PWR 42.0 2183.5 MW-25 Off -Site 2207.91 2208.04 NP-D NP-D 106.0 96.0 - 106.0 2112.0 - 2102.0 H PWR 104.0 2104.0 MW-26 Off -Site 2207.46 2207.62 30.12 2177.34 51.5 41.0 - 51.0 2166.6 - 2156.6 H PWR/BR 42.0 2165.6 RW-1 On -Site 2218.19 2218.61 53.16 2165.03 84.4 42.4 - 82.4 2176.2 - 2136.2 H BR/PWR 72.4 2146.2 RW-2 On -Site 2182.46 2183.62 NP-A NP-A 78.0 35.0 - 75.0 2148.6 - 2108.6 H BR 31.0 2152.6 RW-3 On -Site 2217.58 2218.06 47.60 2169.98 76.0 54.0 - 64.0 2164.1 - 2154.1 H BR 36.0 2182.1 RW-4 On -Site 2160.78 2161.74 NP-A NP-A 60.0 19.6 - 59.6 2142.1 - 2102.1 11 BR 20.0 2141.7 RW-5 On -Site 2159.48 2160.60 15.43 2144.05 66.0 20.2 - 60.2 2140.4 - 2100.4 H BR 16.0 2144.6 RW-6 On -Site 2160.44 2161.57 17.49 2142.95 67.0 20.0 - 60.0 2141.6 - 2101.6 H SAP/BR 36.0 2125.6 .RW-7 On -Site . 2164.57 2165.60 23.61 2140.96 67.0 13.0 - 53.0 1 2152.6 - 2112.6 11 SAP/PWR 55.0 2110.6 Notes: *Values rounded to the nearest 0. 1 -ft. NM = Not measured NP-A = Not Present - Abandoned NP-D = Not Present - Destroyed by Grading bgs = below ground surface. bmp = below measuring point. Water levels measured on 9/2 1 /11. Illo = Type III open bedrock well Measuring Point Elevation is top of casing. BR & PWR = Bedrock & Partially Weathered Rock MW-14 returned to artesian conditions as of 10/27/03. SAP = Saprolite II = Type Il well MW-24 was abandoned, redrilled and replaced in 2007 after the well head Ills = Type III screened well was damaged by Milkco contractors in 2003. The ground surface at RW- I and MW-6 was raised 7.4 feet and the wells were extended. Both were resurveyed in November 2010. Prepared by: AWA Table 1 (2012) of 1022-34 Andrex 2012 Annual Tables I & 2.xls Checked by: PJVH Table 2 Laboratory Analytical Results of Groundwater & Surface Water Samples Selected Chlorinated VOCs Only Andrex Industries Asheville, North Carolina NCDENR Groundwater Incident Number 6586 BLE Project No. J12-1022-34 U 0 U t 40. 0 -U U > 9 Ts 9 rs CA 0 0 0 0 0 N r. 0 d 0 cd E. CA U z W NC 2L 0.7 3 70 0.03 1200 1 NE 1 7 1 0.4 1 10T 1 70 1 2,0001 0.6 1 50 1 6 1 0.2 NE Groundwater AB MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/11/2012 MW-5 4,940 279 ND 1.7 ND ND 1.5 ND 3.2 783 ND ND 0.67 ND 1.6 6,011 9/11/2012 MW-6 2,550 51.5 ND ND ND ND ND ND ND 42.6 ND ND ND ND ND 2,644 9/11/2012 MW-7 175 ND ND ND ND ND ND ND ND ND ND ND ND. ND ND 175 AB MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-8A AB AB AB AB AB AB AB AB AB. AB AB AB AB AB. AB AB 9/11/2012 MW-9 2,000 98.6 ND ND ND ND ND ND 1.91 325 ND ND 0.47 ND ND 2,426 9/12/2012 MW-10 4.7 ND ND 5.0 ND ND ND ND ND 19.7 ND ND ND ND ND 29 9/12/2012 MW-11 1,940 86.6 ND ND ND ND ND ND 1.6 162 ND ND 0.39. ND 0.51 2,191 9/11/2012 MW-12 3.0 ND ND 22.7 ND ND ND ND 11.4 5,830 ND ND ND ND ND 5,867 9/11/2012 MW-13 979 211 ND ND ND ND 0.88. ND 0.79 196 0.45 ND 0.24 ND ND 1,388 9/11/2012 MW-14 968 362 ND ND ND ND 1.5 ND ND 158 ND ND 0.25 ND ND 1,490 9/12/2012 MW-15 176 4.0 1.0 ND ND ND ND ND ND 7.3 1.0 ND ND ND ND 189 9/12/2012 MW-16 180 4.4 1.3 ND ND ND ND ND ND 9.0 1.2 ND ND ND ND 196 9/10/2012 MW-17 1.0 0.96 ND 7.3 ND ND ND ND ND 12.3 ND ND ND ND ND 22 9/11/2012 MW-18 1.8 0.88 1.6 ND ND ND ND ND ND. ND ND ND ND ND. ND 4.3 NP** MW-19 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 9/11/2012 MW-20 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/10/2012 MW-21 ND ND 0.66 ND ND ND ND ND ND ND ND ND ND ND ND 0.66 9/10/2012 MW-22 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/12/2012 MW-23 83.3 4.7 ND ND ND ND ND, ND ND 7.1 ND ND ND. ND ND 95 9/11/2012 MW-24 476 3.0 ND ND ND ND ND ND ND 6.8 ND ND ND ND ND 486 NP** MW-25 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 9/10/2012 MW-26 0.51 ND 2.3 ND ND ND ND ND ND ND ND ND ND ND ND 2.8 9/12/2012 RW-1 1,110 623 ND 99.9 ND ND 9.3 ND 49 15,200 ND ND ND ND ND 17,091 AB RW-2 AB AB _AB AB AB AB AB AB AB AB AB AB AB. AB AB AB 9/12/2012 RW-3 2.5 1.4 ND 11.9 ND ND 0.87, ND 4.1 1,440 ND ND 0.27 ND ND 1,461 AB RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/12/2012 RW-5 ND ND ND ND ND ND ND ND ND 58.2 ND ND ND ND ND 58 9/12/2012 RW-6 168 45.1 ND 73.2 ND ND 1.4 ND 2.6 308 ND ND ND ND ND 598 9/12/2012 RW-7 41.1 8.0 1.2 12.6 ND ND ND ND ND 612 , ND ND ND. ND. ND 675 NC 2B 0.7 2.5 NE 0.025 NE NE I NE NE NE I NE I NE I NE 1488 1488 1 NE I NE Surface Water 9/13/2012 Smith Mill Creek 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/13/2012 Smith Mill Creek 2 0.88 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.88 9/13/2012 Smith Mill Creek 3 0.68 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.68 9/13/2012 Smith Mill Creek 4 2.1 ND ND ND ND ND ND ND ND 0.47 ND ND ND ND ND 2.6 9/13/2012 Smith Mill Creek 5 1.7 ND ND ND ND ND ND ND ND 0.28 ND ND ND ND ND 2.0 9/13/2012 Smith Mill Creek 6 1.3 ND ND ND ND ND ND ND ND ND ND ND ND. ND ND 1.3 9/13/2012 Bear Creek 1 28.4 2.9 0.82 ND ND ND ND ND ND 8.8 ND ND ND ND ND 41 9/13/2012 Bear Creek 2 23.0 3.2 0.99 ND ND ND ND ND ND 8.9 ND ND ND ND ND 36 9/13/2012 Bear Creek 3 6.9 1.2 1.4 ND ND ND ND ND ND 3.8 ND ND ND ND ND 13 9/13/2012 Bear Creek 4 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/13/2012 Bear Creek 5 0.51 ND ND ND ND ND ND. ND ND. ND ND ND ND ND. ND 0.51 9/13/2012 Jehovah Witness 1 25.8 2.5 ND ND ND ND ND ND ND 4.9 ND ND ND ND ND 33 9/13/2012 Cecil's Spring 1 18.5 1.3 ND ND ND ND ND ND 2.7 ND ND ND ND ND 23 9/13/2012 Cecil's Spring 2 5.9 ND ND ND ND ND ND ND ND 0.38 ND ND ND ND ND 6.3 Notes: Analyses performed by EPA Method 8260 MSV Low Level. J-flagged (estimated) results are included on this table but are not identified (see the lab report). Units in �tg/l or parts per billion (ppb) Detected concentrations of petroleum hydrocarbon VOCs are NOT shown in this table (not part of the Andrex groundwater incident). Detected concentrations of acetone, chloromethane, and methylene chloride are NOT shown in this table (probable laboratory contaminants). Detected concentrations of 2-Butanone (MEK) and 2-Hexanone are NOT shown in this table (metabolic products of bioremedation from milk solution injection). NC21, = North Carolina Groundwater Standards under Title 15A Subchapter 2L in [tg/l dated January 1, 2010. NC2B = North Carolina Surface Water Standards [WS - Water Supply Classification] under Title 15A Subchapter 2B in �tg/l dated May 1, 2007. ND not detected at concentrations exceeding the laboratory reporting limit. NS not sampled. NP = not present; monitoring well was abandoned or destroyed. AB = well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008. * Compounds intermittently detected in the past. ** These wells were destroyed by grading during 2003. Recovery well samples are grab samples collected via bailer. Prepared by: AWA Table 2 (2012) of 1022-34 Andrex 2012 Annual Tables I & 2.xls Checked by: PJVH ]FIGURES �'� �i ��Il; ��� ���� �� �� J.. �. ..,aril a RESIDENTIAL BEAR CREEK ROAD RESIDENTIAL 0 0 0 N N ry�0 �O ��ry � O 0 Mw-1 I CECIL'S OLLEGE 2113.10 ��'• W-15 2113.26 MW-18 2092.48 / � �/�� TWENTIETH STREET �HAMILTONI PROPERTY 0 STREET �M�=� McDADE ��/ i •�.. r ki •. MALVERN HILLS ►L _ POOL -� . ® PARK M-��,• �•• � TENNIS COURTS PLACE -- RESIDENTIAL G a if cn RESIDENTIAL REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. O Om O N BLNA ® ENS RESIDENTIAL RESIDENTIAL R O h0 O N N � ti / RESIDENTIAL 0 0 MW-24 MILKCO, INC. r 2163.65 MW-1 v MW-12 I 2169.89 MV RW-3 NF 2169.98 MW-5 2170.45 i MW-25 MW-6 NP—D 2164.79 RW-1 2165.03 MILKCO, INC. M MAI �f NP-A MW-26 0 2177.34 O 2 "_\I Tim a —L _A 0 Mw-7 cm 2192.14 1 x KW—[ MW-8A* A6R, \IDUST IES, INC. MW-4* MW-g NIP -A 2149.85 II MW-8* PERFECTIO GEAR, INC. TRW-4 NP-A \\ RW-5 MW-10 �� II 2144.15 2143.71 RW-6 MW-11 \\ I 2142.95 2140.82 O c ICE` MW-14* RW-7 w VICE® �\\,- SILVERS__ ---- 2138.7s 214o.ss w STORE- / MW-13 Q PROPERTY 2136.30 ILVS PROPERTY w i ECHOLS B ING 'G PROPERTY, LLEY M JUSTICE ' i PROPERTY O O \ ! C Alr N ey RESIDENTIAL DATE: 10-18-12 CAD FILE: ANDREX34-WTMO91012 JOB NO: J12-1022-34 .0 RE q Nf 0 MW-20 2144.23 SEXTON PROPERTY RESIDENTIAL � �•�• OJAe i l /• 040"" / H YNES Pn . L' �1 O AYN S C RP. N - F ROY D FARME O MW-23 — - 2118.33 I� MW I i 2089__ I ' kEHOVAN MW-22 2089.96 MW-12090.9R. NORFpoK TNER TNESS4\ BIESTE F DL �s�o N OPERTY • , PROPERTY ROgD - - FORMER 1 MW-19 WATER WELL NP-D - CRYDE AN - - PROPE Y SATTERFI PROPERTY HOUSj�_, 0 �j► O O jORESIDENTIALO O 00 /"y0F Al-. O NOTES: 1. THE GROUNDWATER PUMP AND TREAT SYSTEMS HAD BEEN REMOVED AND WERE NOT IN OPERATION AT THE TIME WATER LEVEL MEASUREMENTS WERE TAKEN. GROUNDWATER WAS NOT BEING PUMPED FROM RW-1 THROUGH RW-7 WHILE MEASUREMENTS WERE COLLECTED. 2. ** SKY LANES BOWLING CENTER NCDEH - PUBLIC WATER SYSTEM ID #10-11-025 WELL NAME: WELL #1 AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED "...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER." 2090 2080 LEGEND '•� APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR SHALLOW BEDROCK) GROUNDWATER MONITORING WELL ••� O APPROXIMATE LOCATION OF EXISTING (TYPE III -BEDROCK) ••\ GROUNDWATER MONITORING WELL O RECOVERY WELL O WATER SUPPLY WELL }--- BELOW GROUND STREAM SHOWING FLOW DIRECTION �•-•• �— ABOVE GROUND STREAM SHOWING FLOW DIRECTION PROPERTY LINE 2118.33 WATER LEVEL IN FEET ABOVE MEAN SEA LEVEL * GROUNDWATER ELEVATION IN WELL MW-14 IS TYPICALLY ARTESIAN AND REPRESENTS THE POTENT10METRIC SURFACE OF THE DEEPER ROCK AQUIFER AND WAS NOT CONSIDERED FOR CONTOURING PURPOSES. NP-A NOT PRESENT. WELL HAS BEEN ABANDONED. NP-D M W-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. M W-25 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY MILKO, INC. APPROXIMATE DIRECTION OF GROUNDWATER FLOW APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE 2120 EQUIPOTENTIAL CONTOUR LINE 200 100 0 200 400 APPROXIMATE SCALE IN FEET REVISIONS No. DESCRIPTION BY DRAWN: ACE CHECKED: AWA APPROVED: NIL BUNNELL-LAMMONS ENGNEERING, INC. 6004 PONDERS COURT GREENVILLE, SOUTH CAROLINA 29615 INC. PHONE: (864)288-1265 FAX: (864)288-4430 GROUNDWATER ELEVATION CONTOUR MAP - SEPTEMBER 10, 2012 ANDREX INDUSTRIES DEAVERVIEW ROAD ASHEVILLE, NORTH CAROLINA FIGURE NO. 2 RESIDENTIAL RESIDENTIAL BEAR CREEK ROAD RESIDENTIAL CS-2 \ 6.3 F RESIDENTIAL MW-26 /--�` 2.8 CECIL'S LEGE ER RESIDENTIAL _ 1 SPFMG� MW-16� MW-15 2310 / 196 1 189 S I MW s roo o 4.3 � 1 / � \all HAY ES CORP. MILK I HAY // STREET o MW-24 W-2 rO o v 486 AB RW-3 o 1,461 I ZZZZZII� - P N R � ZZZZ'''ZZZZ CO. NNC &0 17,091 M� HN NES CORP. ■ 090\ \ I4000, goopo opool 00-0 — McDADE 5aEE BLUUMINU " I � I � BC-2 RESIDENTI 36 - / goom •�,.i - *WOOD 0000 SNOOP SNOOP sopow � � MALVERN HILLS P i / 13 _ J BC-4 •r•• � ND Ole .� /•• t BC-5 /••�•• 100o F�' 0.51 /•' a c TENNIS ND spow" COURTS swoopwoo= �_ �__3 woom swoop woom � RUMBOUGH PLACE REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. RESIDENTIAL RESIDENTIAL ct#,O.Ti `B C1 1\ 2,426 AB S MW-8A o RW-4 AB PERFECTION GEAR, C. AB ANI X STRIES, I RW-5 ;00 58 MW-10 29 MW-11 0 2,191 RW-6 MW-13 598 1,388 9000 RW- \ \ _675 SILVERS Soo OBOWLING PROPER MW04* O SEXTON 1,490 9 PROP PROPERTYI , - i , AL y RESIDENTI-_coop _�, doom swoop 4000D MW p 20 RESIDENTIAL 0 L 1 I I I 1 1 I S CORP. �J may. r. 4 i \ � s2 SM-2 \ �� o.$$_ SM-1 ND RESIDENTIAL O I _ MW-17 MW-23 �G 22 95 \ � TROY D. FARMER BARK SM-3 RASH ROAD 0.68 MW-21 0.66 (CHLOROFORM ONLY) \\_ MW-22 � _ ® ND �33 / FORMER JEHOVAN l\ WITNESS PROPERTY `BIESTERFEDLT PROPERTY MW-19 � �pRFp�k S pUTN SM-4\, 10 _ I 14. pA0 2.6 \ BAKER DF SM-5 WC FORMER 2.0 �'`„ IYWATER WELL SATTERFIELD _ CRYDERMAN \SMI 6 ��• PROPERTY —HOUSE - - PROPERTY •�•.�• am* emposs r_ sommm Lu -now �.. _wooso �. z I PATTp� �lvuil/ / RESIDENTIAL I 200 100 0 200 400 APPROXIMATE SCALE IN FEET GAR �7 ' S = f 1475 Q 'w P�OLOp�S.• RESIDENTIAL Q A NOTES: 1. LABORATORY ANALYSIS BY EPA METHOD 8260. 2. WELLS AND SURFACE WATER WAS SAMPLED ON SEPTEMBER 10-13, 2012. 3. CONCENTRATIONS DETECTED IN MW-21 ARE PRIMARILY CHLOROFORM, PROBABLY RELATED TO LEAKING WATER SUPPLY LINES IN CLOSE PROXIMITY TO THE WELLS. 4. SAMPLES FROM STREAMS DESIGNATED AS FOLLOWS: SM = SMITH MILL CREEK TRIBUTARY CS = CECIL'S SPRING BC = BEAR CREEK JW = FORMER JEHOVAH WITNESS PROPERTY 5. NP = NOT PRESENT, WELL WAS NOT PRESENT AT TIME OF SAMPLING. 6. ** SKY LANES BOWLING CENTER NCDEH - PUBLIC WATER SYSTEM ID #10-11-025 WELL NAME: WELL #1 AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED "...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER." 7. * THE WELLS MAY INTERCEPT FRACTURE SETS OR MAY BE SCREENED AT ELEVATIONS AT WHICH GROUNDWATER CONTAMINANT CONCENTRATIONS ARE INCONSISTENT WITH THE ESTABLISHED PLUME. THE VALUES WERE IGNORED FOR CONTOURING PURPOSES. LEGEND APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR SHALLOW BEDROCK) GROUNDWATER MONITORING WELL O APPROXIMATE LOCATION OF EXISTING (TYPE III -BEDROCK) GROUNDWATER MONITORING WELL O RECOVERY WELL - APPROXIMATE LOCATION OF SURFACE WATER SAMPLES (SEE NOTE 4) (WATER SAMPLES COLLECTED 9-13-12). O WATER SUPPLY WELL 162 CONCENTRATION OF TOTAL DETECTED CHLORINATED VOLATILE ORGANIC COMPOUNDS IN PARTS PER BILLION (ppb). —�f-- �— BELOW GROUND STREAM SHOWING FLOW DIRECTION 8. THE FORMER WATER SUPPLY WELL ON THE CRYDERMAN PROPERTY APPEARED / — •• / — ABOVE GROUND STREAM SHOWING FLOW DIRECTION TO BE ABANDONED AND COULD NOT BE SAMPLED AS OF OCTOBER 2005. PROPERTY LINE 9. MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. MW-25 WAS APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY MILKO, INC. 100 TOTAL CHLORINATED CONCENTRATION CONTOUR IN PARTS PER BILLION 10. RECOVERY WELLS WERE NOT OPERATIONAL AT THE TIME OF SAMPLING. —ND-- ESTIMATED LIMIT OF VOC'S 11. AB = WELL ABANDONED IN 2008 PER APPROVED BROWNFIELD REDEVELOPMENT PLAN. REVISIONS No. DESCRIPTION BY DRAWN: ACE CHECKED: AWA APPROVED: DATE: 10-18-12 'AD FILE: ANDREX34-VOCSEPT12 JOB NO: J12-1022-34 NIL BUNNELL-LAMMONS MONEERNO, NC. 6004 PONDERS COURT GEENVILLEINC. PHONE: (64)288510265 UTH FAX: (864)28854430 CONTOUR MAP OF TOTAL CHLORINATED VOLATILE ORGANIC COMPOUND ISOCONCENTRATIONS - SEPTEMBER 10-13, 2012 GROUNDWATER AND SURFACE WATER ANDREX INDUSTRIES ASHEVILLE, NORTH CAROLINA FIGURE NO. 3 APPENDICES APPENDIX A WELL SAMPLING LOGS MILE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of I Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: RAD Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2216.75 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-5 Land Surface Elevation (ft msl): 2216.92 Downgradient: yes Screened Interval (ft bgs): 43.0-53.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Mostly cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 620F Locking Cap: yes Total Well Depth in feet (TWD) 53.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 46.80 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 6.20 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 1.05 Sample Date and Time: 9/11/2012 @ 1044 Standard Evacuation Volume (3 casing volumes) 3.16 Remarks: TOCs + VOCs Method of Well Evacuation: Disp Bailer Method of Sample Collection: Disp Bailer Total Volume of Water Removed (gallons): 3.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 1.0 2.0 3.0 Time (military) 1032 1035 1040 1044 pH (S.U.) 5.80 5.81 5.94 6.02 Sp. Cond. (umhos/cm) 85.7 91.7 95.4 97.9 Water Temp. ('C) 17.0 17 17 17 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 10.08 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2218.43 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-6 Land Surface Elevation (ft msl): 2218.67 Downgradient: yes Screened Interval (ft bgs): 50.4-70.4 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 790F Locking Cap: yes Total Well Depth in feet (TWD) 71.90 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 53.64 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 18.26 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 3.10 Sample Date and Time: 9/12/12 @ 1330 Standard Evacuation Volume (3 casing volumes) 9.31 Remarks: Dry@ 1. 5 gallons Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): 1.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1312 pH (S.U.) 5.34 Sp. Cond. (umhos/cm) 69.3 Water Temp. ('C) 18.0 Turbidity (subjective)* I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.64 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: RAD Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2218.35 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-7 Land Surface Elevation (ft msl): 2218.60 Downgradient: yes Screened Interval (ft bgs): 24.5-34.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Mostly Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 60OF Locking Cap: yes Total Well Depth in feet (TWD) 35.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 26.21 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 8.79 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 1.49 Sample Date and Time: 9/11/2012 @ 1012 Standard Evacuation Volume (3 casing volumes) 4.48 Remarks: TOCs + VOCs Method of Well Evacuation: Disp Bailer Method of Sample Collection: Disp Bailer Total Volume of Water Removed (gallons): 4.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 1.5 2.9 4.5 Time (military) 957 1002 1007 1012 pH (S.U.) 6.13 5.9 5.78 5.75 Sp. Cond. (umhos/cm) 76.4 53.3 48.2 44.6 Water Temp. ('C) 17 17.0 16.7 16.7 Turbidity (subjective)* 1 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 21.03 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2175.57 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-9 Land Surface Elevation (ft msl): 2175.95 Downgradient: yes Screened Interval (ft bgs): 44.0-54.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) 54.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 25.72 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 28.48 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 4.84 Sample Date and Time: 9/11/2012 @ 1245 Standard Evacuation Volume (3 casing volumes) 14.5 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 14.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 4.8 9.6 14.4 Time (military) 1213 1223 1233 1243 pH (S.U.) 5.94 6.04 5.6 5.65 Sp. Cond. (umhos/cm) 71.2 74.1 74.7 74.2 Water Temp. ('C) 16.2 15.1 14.9 15.0 Turbidity (subjective)* I 1 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 2.52 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 I Personnel: Name: Job #: I ID #: Conditions: Air Temperature: Total Well Depth in feet (TWD): Depth to Ground Water in feet (I Length of Water Column (LWC) I Casing Volume in gallons (CV Standard Evacuation Volume (3 Method of Well Evacuation: Method of Sample Collection: Total Volume of Water Removed Sep. 12, 2012 BPN Andrex J12-1022-34 MW-10 Clear 790F 39.00 )GW) 16.21 =TWD-DGW= 22.79 i = LWC x 0.17 = 3.87 -asing volumes) = 11.62 Disp Bailer Disp Bailer (eallons): 11.7 aallon� Casing Diameter: 2 inches Casing Material: PVC Measuring Point Elevation (ft msl): 2159.92 Height of Riser (ft above land surface): flushmount Land Surface Elevation (ft msl): 2159.45 Screened Interval (ft bgs): 29.0-39.0 Dedicated Pump or Bailer: no Steel Guard PiDe Around Casiniz: no Protective Post/Abutment: no Well Integrity Satisfactory: ye! Well Yield (subjective): hi� Samnle Date and Time: 9/12/2012 a, 1255 Remarks: TOCs + VOCs FIELD ANALYSIS Volume Purged (gallons) initial 3.9 7.8 11.7 Time (military) 1233 1239 1245 1250 pH (S.U.) 6.16 6.00 6.27 6.30 Sp. Cond. (umhos/cm) 95.0 133.2 119.3 106.2 Water Temp. ('C) 1 17.2 1 15.9 1 15.6 1 15.1 1 Turbidity (subjective)* 1 2 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.59 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 2 inches Field Personnel: RAD Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2166.00 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-1 I Land Surface Elevation (ft msl): 2166.39 Downgradient: yes Screened Interval (ft bgs): 48.0-58.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: no Air Temperature: 730F Locking Cap: yes Total Well Depth in feet (TWD) 58.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 25.18 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 33.32 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 5.66 Sample Date and Time: 9/12/2012 @ 1307 Standard Evacuation Volume (3 casing volumes) 16.99 Remarks: TOCs + VOCs Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 17.1 gallons Volume Purged (gallons) initial FIELD ANALYSIS 5.7 11.4 17.1 Time (military) 1241 1250 1258 1307 pH (S.U.) 5.75 5.81 5.54 5.61 Sp. Cond. (umhos/cm) 111.4 98.0 95.7 93.8 Water Temp. ('C) 17.6 16.0 16.0 15.9 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 14.04 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: RAD Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2219.17 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-12 Land Surface Elevation (ft msl): 2219.49 Downgradient: yes Screened Interval (ft bgs): 60.0-70.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Mostly Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 630F Locking Cap: yes Total Well Depth in feet (TWD) 81.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 49.28 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 31.72 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 5.39 Sample Date and Time: 9/11/2012 @ 1155 Standard Evacuation Volume (3 casing volumes) 16.18 Remarks: TOCs + VOCs Method of Well Evacuation: Disp Bailer Method of Sample Collection: Disp Bailer Total Volume of Water Removed (gallons): 16.2 gallons Volume Purged (gallons) initial FIELD ANALYSIS 5.4 10.8 16.2 Time (military) 1104 1124 1138 1155 pH (S.U.) 6.31 6.53 6.53 6.52 Sp. Cond. (umhos/cm) 684 722 698 660 Water Temp. ('C) 17.6 17.0 16.9 17.0 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 9.83 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2138.80 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-13 Land Surface Elevation (ft msl): 2138.96 Downgradient: yes Screened Interval (ft bgs): 48.0-58.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 81OF Locking Cap: yes Total Well Depth in feet (TWD) 58.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 2.50 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 56.00 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 9.52 Sample Date and Time: 9/11/2012 @ 1430 Standard Evacuation Volume (3 casing volumes) 28.56 Remarks: TOCs + VOCs Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 28.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 9.5 19.0 28.5 Time (military) 1410 1415 1420 1425 pH (S.U.) 6.64 6.6 6.51 6.49 Sp. Cond. (umhos/cm) 51.2 55.8 54.7 55.8 Water Temp. ('C) 18.2 18.3 17.0 18.2 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 3.99 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2138.94 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-14 Land Surface Elevation (ft msl): 2139.2 Downgradient: yes Screened Interval (ft bgs): 65.0-75.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 80OF Locking Cap: yes Total Well Depth in feet (TWD) 75.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 0.18 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 74.82 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 12.72 Sample Date and Time: 9/11/2012 @ 1405 Standard Evacuation Volume (3 casing volumes) 38.16 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 39.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 12.7 25.4 38.1 Time (military) 1332 1342 1351 1400 pH (S.U.) 6.30 6.57 6.73 6.75 Sp. Cond. (umhos/cm) 57.0 54.4 55.4 55.8 Water Temp. ('C) 18.1 17.2 18.3 17.7 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.97 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 6 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2124.89 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-15 Land Surface Elevation (ft msl): 2125.18 Downgradient: yes Screened Interval (ft bgs): 33.3-40.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 720F Locking Cap: yes Total Well Depth in feet (TWD) 40.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 11.63 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 28.37 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 42.56 Sample Date and Time: 9/12/2012 @ 1030 Standard Evacuation Volume (3 casing volumes) = 127.67 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 130 gallons Volume Purged (gallons) initial FIELD ANALYSIS 43 86 129 Time (military) 1014 1017 1021 1026 pH (S.U.) 6.75 6.50 6.40 6.22 Sp. Cond. (umhos/cm) 42.7 39.4 38.5 39.5 Water Temp. ('C) 16.3 16.1 16.1 16.1 Turbidity (subjective)* 2 1 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 6.65 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2124.59 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-16 Land Surface Elevation (ft msl): 2124.85 Downgradient: yes Screened Interval (ft bgs): 23.5-33.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 720F Locking Cap: yes Total Well Depth in feet (TWD) 33.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 11.49 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 22.01 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 3.74 Sample Date and Time: 9/12/2012 @ 1100 Standard Evacuation Volume (3 casing volumes) 11.23 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 11.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 3.75 7.5 11.25 Time (military) 1043 1048 1054 1058 pH (S.U.) 6.01 6.00 5.99 5.99 Sp. Cond. (umhos/cm) 39.2 41.3 40.4 41.3 Water Temp. ('C) 19.1 16.9 17.0 16.4 Turbidity (subjective)* 1 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.87 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 10, 2012 Casing Diameter: 2 inches Field Personnel: DRM Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2094.64 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-17 Land Surface Elevation (ft msl): 2094.74 Downgradient: yes Screened Interval (ft bgs): 4.0-14.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 790F Locking Cap: yes Total Well Depth in feet (TWD) 14.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 3.74 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 10.46 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 1.78 Sample Date and Time: 9/10/2012 @ 1305 Standard Evacuation Volume (3 casing volumes) 5.33 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 6.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 2.0 4.0 6.0 Time (military) 1250 1255 1300 1305 pH (S.U.) 6.11 6.03 6.04 6.03 Sp. Cond. (umhos/cm) 300 482 449 450 Water Temp. ('C) 26.0 23.3 21.9 22.0 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 10.96 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2101.81 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-18 Land Surface Elevation (ft msl): 2101.92 Downgradient: yes Screened Interval (ft bgs): 49.0-59.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 80OF Locking Cap: yes Total Well Depth in feet (TWD) 59.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 9.33 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 49.67 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 8.44 Sample Date and Time: 9/11/2012 @ 1515 Standard Evacuation Volume (3 casing volumes) 25.33 Remarks: Dry@ 10 gallons Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 10.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 8.4 Time (military) 1455 1505 pH (S.U.) 6.93 6.70 Sp. Cond. (umhos/cm) 48 47.6 Water Temp. ('C) 17.4 16.3 Turbidity (subjective)* I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.83 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2180.55 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-20 Land Surface Elevation (ft msl): 2180.54 Downgradient: yes Screened Interval (ft bgs): 67.0-77.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 70OF Locking Cap: yes Total Well Depth in feet (TWD) 77.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 36.32 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 40.68 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 6.92 Sample Date and Time: 9/11/2012 @ 1045 Standard Evacuation Volume (3 casing volumes) 20.75 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 20.7 gallons Volume Purged (gallons) initial FIELD ANALYSIS 6.9 13.8 20.7 Time (military) 956 1010 1024 1038 pH (S.U.) 7.85 7.65 7.00 7.09 Sp. Cond. (umhos/cm) 21.5 19.9 19.4 19.4 Water Temp. ('C) 16.3 16.1 16.5 16.0 Turbidity (subjective)* 1 2 3 3 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 8.30 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 10, 2012 Casing Diameter: 2 inches Field Personnel: DRM Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2091.17 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-21 Land Surface Elevation (ft msl): 2091.31 Downgradient: yes Screened Interval (ft bgs): 26.5-36.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 790F Locking Cap: yes Total Well Depth in feet (TWD) 36.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 1.59 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 34.91 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 5.93 Sample Date and Time: 9/10/2012 @ 1525 Standard Evacuation Volume (3 casing volumes) 17.80 Remarks: Dry @ 12 gallons Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 12.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 6.0 12.0 Time (military) 1450 1510 1525 pH (S.U.) 6.37 5.97 6.04 Sp. Cond. (umhos/cm) 94 91.7 91.3 Water Temp. ('C) 22.5 19.7 15.8 Turbidity (subjective)* I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 11.16 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 10, 2012 Casing Diameter: 2 inches Field Personnel: DRM Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2090.71 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-22 Land Surface Elevation (ft msl): 2090.84 Downgradient: yes Screened Interval (ft bgs): 47.0-57.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 790F Locking Cap: yes Total Well Depth in feet (TWD) 57.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 0.75 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 56.25 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 9.56 Sample Date and Time: 9/10/2012 @ 1445 Standard Evacuation Volume (3 casing volumes) 28.69 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 29.0 gallons Volume Purged (gallons) initial FIELD ANALYSIS 9.6 19.2 29.0 Time (military) 1330 1345 1415 1445 pH (S.U.) 6.16 6.21 6.30 6.80 Sp. Cond. (umhos/cm) 124.5 124.4 134.4 138.1 Water Temp. ('C) 22.8 19.7 15.9 15.9 Turbidity (subjective)* 1 1 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 15.07 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 6 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2145.05 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-23 Land Surface Elevation (ft msl): 2145.20 Downgradient: yes Screened Interval (ft bgs): 31.0-41.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 71OF Locking Cap: yes Total Well Depth in feet (TWD) 41.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 26.72 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 14.78 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 22.17 Sample Date and Time: 9/12/2012 @ 1000 Standard Evacuation Volume (3 casing volumes) = 66.51 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 70 gallons Volume Purged (gallons) initial FIELD ANALYSIS 22.2 44.4 66.6 Time (military) 952 954 956 958 pH (S.U.) 6.92 6.93 6.62 6.25 Sp. Cond. (umhos/cm) 83 109.3 116.8 123.2 Water Temp. ('C) 16.2 16.1 16.2 16.2 Turbidity (subjective)* 2 2 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 8.05 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 11, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2225.37 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-24 Land Surface Elevation (ft msl): 2225.49 Downgradient: yes Screened Interval (ft bgs): 70.0-80.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 720F Locking Cap: yes Total Well Depth in feet (TWD) 80.10 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 61.72 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 18.38 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 3.12 Sample Date and Time: 9/11/2012 @ 1130 Standard Evacuation Volume (3 casing volumes) 9.37 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 9.3 gallons Volume Purged (gallons) initial FIELD ANALYSIS 3.1 6.2 9.3 Time (military) 1058 1106 1115 1124 pH (S.U.) 6.34 5.94 6.15 6.01 Sp. Cond. (umhos/cm) 65.0 67.5 55.0 56.2 Water Temp. ('C) 16.1 15.2 15.6 15.6 Turbidity (subjective)* 1 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 4.52 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 10, 2012 Casing Diameter: 2 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2207.46 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: MW-26 Land Surface Elevation (ft msl): 2207.62 Downgradient: yes Screened Interval (ft bgs): 41.0-51.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Clear Steel Guard Pipe Around Casing: no Air Temperature: 790F Locking Cap: yes Total Well Depth in feet (TWD) 51.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 30.12 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 20.88 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 3.55 Sample Date and Time: 9/10/2012 @ 1350 Standard Evacuation Volume (3 casing volumes) 10.65 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 10.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 3.5 7.0 10.5 Time (military) 1312 1325 1333 1340 pH (S.U.) 6.88 6.43 6.16 5.97 Sp. Cond. (umhos/cm) 262.0 267.0 236.0 265.0 Water Temp. ('C) 17.7 16.7 16.5 16.5 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.20 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 6 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2209.87 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: RW- 1 Land Surface Elevation (ft msl): 2211.22 Downgradient: yes Screened Interval (ft bgs): 35.0-75.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 790F Locking Cap: no Total Well Depth in feet (TWD) 82.40 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 53.16 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 29.24 Well Yield (subjective): moderate I Casing Volume in gallons (CV) = LWC x 1.5 = 43.86 Sample Date and Time: 9/12/2012 @ 1345 Standard Evacuation Volume (3 casing volumes) = 131.58 Remarks: Grab sample @ 68'btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1350 pH (S.U.) 5.17 Sp. Cond. (umhos/cm) 300 Water Temp. ('C) 19.0 Turbidity (subjective)* 3 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.18 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 4 inches Field Personnel: BPN Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2217.58 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: RW-3 Land Surface Elevation (ft msl): 2218.06 Downgradient: yes Screened Interval (ft bgs): 54.0-64.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Clear Steel Guard Pipe Around Casing: yes Air Temperature: 80OF Locking Cap: yes Total Well Depth in feet (TWD) 64.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 47.60 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 16.40 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0.66 10.82 Sample Date and Time: 9/12/2012 @ 1405 Standard Evacuation Volume (3 casing volumes) 32.47 Remarks: Grab sample @ 59'btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1410 pH (S.U.) 5.95 Sp. Cond. (umhos/cm) 137.7 Water Temp. ('C) 20.5 Turbidity (subjective)* 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.58 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 6 inches Field Personnel: RAD Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2159.48 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: RW-5 Land Surface Elevation (ft msl): 2160.60 Downgradient: yes Screened Interval (ft bgs): 20.2-60.2 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 730F Locking Cap: yes Total Well Depth in feet (TWD) 60.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 15.43 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 44.77 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 67.16 Sample Date and Time: 9/12/2012 @ 1405 Standard Evacuation Volume (3 casing volumes) = 201.47 Remarks: Grab sample @ 40'btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1405 pH (S.U.) 6.18 Sp. Cond. (umhos/cm) 792 Water Temp. ('C) 17.2 Turbidity (subjective)* I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 10.23 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 6 inches Field Personnel: RAD Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2160.44 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: RW-6 Land Surface Elevation (ft msl): 2161.57 Downgradient: yes Screened Interval (ft bgs): 20.0-60.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 730F Locking Cap: yes Total Well Depth in feet (TWD) 60.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 17.49 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 42.51 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 63.77 Sample Date and Time: 9/12/2012 @ 1340 Standard Evacuation Volume (3 casing volumes) = 191.30 Remarks: Grab sample @ 40'btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1340 pH (S.U.) 5.94 Sp. Cond. (umhos/cm) 275.0 Water Temp. ('C) 15.5 Turbidity (subjective)* I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 11.41 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 12, 2012 Casing Diameter: 6 inches Field Personnel: RAD Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2164.57 BLE Job #: J12-1022-34 Height of Riser (ft above land surface): flushmount Well ID #: RW-7 Land Surface Elevation (ft msl): 2165.60 Downgradient: yes Screened Interval (ft bgs): 13.0-53.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 730F Locking Cap: yes Total Well Depth in feet (TWD) 53.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 23.61 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 29.39 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 44.09 Sample Date and Time: 9/12/2012 @ 1320 Standard Evacuation Volume (3 casing volumes) = 132.26 Remarks: Grab sample @ 38'btoc Method of Well Evacuation: Method of Sample Collection: Disp. Bailer TOCs + VOCs Total Volume of Water Removed (gallons): NA Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1320 pH (S.U.) 5.73 Sp. Cond. (umhos/cm) 4.91 Water Temp. ('C) 16.6 Turbidity (subjective)* I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 16.19 APPENDIX B LABORATORY ANALYTICAL DATA SHEETS (Provided on Enclosed CD) qD ceAnalytical —pacelabs.com October 02, 2012 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 Eden, NC 27288 (336)623-8921 RE: Project: Annual Andrex J12-1022-34 Pace Project No.: 92131396 Dear Mr. Alexander: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 13, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TN I standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tom Williams tom.williams@pacelabs.com Project Manager Enclosures PIC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 67 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 67 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE SUMMARY Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Lab ID Sample ID Matrix Date Collected Date Received 92131396001 MW-5 Water 09/11/12 10:44 09/13/12 14:15 92131396002 MW-6 Water 09/11/12 13:30 09/13/12 14:15 92131396003 MW-7 Water 09/11/12 10:12 09/13/12 14:15 92131396004 MW-9 Water 09/11/12 12:45 09/13/12 14:15 92131396005 MW-10 Water 09/12/12 12:55 09/13/12 14:15 92131396006 MW-1 1 Water 09/12/12 13:07 09/13/12 14:15 92131396007 MW-12 Water 09/11/12 11:55 09/13/12 14:15 92131396008 MW-13 Water 09/11/12 14:30 09/13/12 14:15 92131396009 MW-14 Water 09/11/12 14:05 09/13/12 14:15 92131396010 MW-15 Water 09/12/12 10:30 09/13/12 14:15 92131396011 MW-16 Water 09/12/12 11:00 09/13/12 14:15 92131396012 MW-17 Water 09/10/12 13:05 09/13/12 14:15 92131396013 MW-1 8 Water 09/11/12 15:15 09/13/12 14:15 92131396014 MW-20 Water 09/11/12 10:45 09/13/12 14:15 92131396015 MW-21 Water 09/10/12 15:25 09/13/12 14:15 92131396016 MW-22 Water 09/10/12 14:45 09/13/12 14:15 92131396017 MW-23 Water 09/12/12 10:00 09/13/12 14:15 92131396018 MW-24 Water 09/11/12 11:30 09/13/12 14:15 92131396019 MW-26 Water 09/10/12 13:50 09/13/12 14:15 92131396020 RW-1 Water 09/12/12 13:45 09/13/12 14:15 92131396021 RW-3 Water 09/12/12 14:05 09/13/12 14:15 92131396022 RW-5 Water 09/12/12 14:05 09/13/12 14:15 92131396023 RW-6 Water 09/12/12 13:40 09/13/12 14:15 92131396024 RW-7 Water 09/12/12 13:20 09/13/12 14:15 92131396025 TRIP BLANK Water 09/12/12 00:00 09/13/12 14:15 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 REPORT OF LABORATORY ANALYSIS Page 3 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE ANALYTE COUNT Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92131396001 MW-5 EPA 8260 KJIVI 63 PASI-C 92131396002 MW-6 EPA 8260 KJIM 63 PASI-C 92131396003 MW-7 EPA 8260 KJIM 63 PASI-C 92131396004 MW-9 EPA 8260 KJIM 63 PASI-C 92131396005 MW-10 EPA 8260 KJIM 63 PASI-C 92131396006 MW-11 EPA 8260 KJIM 63 PASI-C 92131396007 MW-12 EPA 8260 KJIM 63 PASI-C 92131396008 MW-13 EPA 8260 KJIM 63 PASI-C 92131396009 MW-14 EPA 8260 KJIM 63 PASI-C 92131396010 MW-15 EPA 8260 KJIM 63 PASI-C 92131396011 MW-16 EPA 8260 KJIVI 63 PASI-C 92131396012 MW-17 EPA 8260 KJIVI 63 PASI-C 92131396013 MW-18 EPA 8260 KJIM 63 PASI-C 92131396014 MW-20 EPA 8260 KJIM 63 PASI-C 92131396015 MW-21 EPA 8260 KJIM 63 PASI-C 92131396016 MW-22 EPA 8260 KJIM 63 PASI-C 92131396017 MW-23 EPA 8260 KJIM 63 PASI-C 92131396018 MW-24 EPA 8260 KJIM 63 PASI-C 92131396019 MW-26 EPA 8260 KJIM 63 PASI-C 92131396020 RW-1 EPA 8260 KJIM 63 PASI-C 92131396021 RW-3 EPA 8260 KJIM 63 PASI-C 92131396022 RW-5 EPA 8260 KJIM 63 PASI-C 92131396023 RW-6 EPA 8260 KJIM 63 PASI-C 92131396024 RW-7 EPA 8260 KJIM 63 PASI-C 92131396025 TRIP BLANK EPA 8260 KJIM 63 PASI-C REPORT OF LABORATORY ANALYSIS Page 4 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5 LabID: 92131396001 Collected: 09/11/12 10:44 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 62.5 25.0 2.5 09/25/12 19:11 67-64-1 ND ug/L 2.5 0.62 2.5 09/25/12 19:11 71-43-2 ND ug/L 2.5 0.75 2.5 09/25/12 19:11 108-86-1 ND ug/L 2.5 0.42 2.5 09/25/12 19:11 74-97-5 ND ug/L 2.5 0.45 2.5 09/25/12 19:11 75-27-4 ND ug/L 2.5 0.65 2.5 09/25/12 19:11 75-25-2 ND ug/L 5.0 0.72 2.5 09/25/12 19:11 74-83-9 ND ug/L 12.5 2.4 2.5 09/25/12 19:11 78-93-3 ND ug/L 2.5 0.62 2.5 09/25/12 19:11 56-23-5 0.67J ug/L 2.5 0.58 2.5 09/25/12 19:11 108-90-7 ND ug/L 2.5 1.4 2.5 09/25/12 19:11 75-00-3 ND ug/L 2.5 0.35 2.5 09/25/12 19:11 67-66-3 ND ug/L 2.5 0.28 2.5 09/25/12 19:11 74-87-3 ND ug/L 2.5 0.88 2.5 09/25/12 19:11 95-49-8 ND ug/L 2.5 0.78 2.5 09/25/12 19:11 106-43-4 ND ug/L 12.5 6.3 2.5 09/25/12 19:11 96-12-8 ND ug/L 2.5 0.52 2.5 09/25/12 19:11 124-48-1 ND ug/L 2.5 0.68 2.5 09/25/12 19:11 106-93-4 ND ug/L 2.5 0.52 2.5 09/25/12 19:11 74-95-3 ND ug/L 2.5 0.75 2.5 09/25/12 19:11 95-50-1 ND ug/L 2.5 0.60 2.5 09/25/12 19:11 541-73-1 ND ug/L 2.5 0.82 2.5 09/25/12 19:11 106-46-7 ND ug/L 2.5 0.52 2.5 09/25/12 19:11 75-71-8 ND ug/L 2.5 0.80 2.5 09/25/12 19:11 75-34-3 ND ug/L 2.5 0.30 2.5 09/25/12 19:11 107-06-2 1.5J ug/L 2.5 1.4 2.5 09/25/12 19:11 75-35-4 783 ug/L 25.0 4.8 25 09/14/12 20:12 156-59-2 3.2 ug/L 2.5 1.2 2.5 09/25/12 19:11 156-60-5 ND ug/L 2.5 0.68 2.5 09/25/12 19:11 78-87-5 ND ug/L 2.5 0.70 2.5 09/25/12 19:11 142-28-9 ND ug/L 2.5 0.32 2.5 09/25/12 19:11 594-20-7 ND ug/L 2.5 1.2 2.5 09/25/12 19:11 563-58-6 ND ug/L 2.5 0.32 2.5 09/25/12 19:11 10061-01-5 ND ug/L 2.5 0.65 2.5 09/25/12 19:11 10061-02-6 ND ug/L 2.5 0.30 2.5 09/25/12 19:11 108-20-3 ND ug/L 2.5 0.75 2.5 09/25/12 19:11 100-41-4 ND ug/L 2.5 1.8 2.5 09/25/12 19:11 87-68-3 ND ug/L 12.5 1.2 2.5 09/25/12 19:11 591-78-6 ND ug/L 2.5 0.78 2.5 09/25/12 19:11 99-87-6 ND ug/L 5.0 2.4 2.5 09/25/12 19:11 75-09-2 ND ug/L 12.5 0.82 2.5 09/25/12 19:11 108-10-1 ND ug/L 2.5 0.52 2.5 09/25/12 19:11 1634-04-4 ND ug/L 2.5 0.60 2.5 09/25/12 19:11 91-20-3 ND ug/L 2.5 0.65 2.5 09/25/12 19:11 100-42-5 1.6J ug/L 2.5 0.82 2.5 09/25/12 19:11 630-20-6 ND ug/L 2.5 1.0 2.5 09/25/12 19:11 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 5 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5 LabID: 92131396001 Collected: 09/11/12 10:44 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 4940 ug/L 25.0 11.5 25 09/14/12 20:12 127-18-4 Toluene ND ug/L 2.5 0.65 2.5 09/25/12 19:11 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.5 0.82 2.5 09/25/12 19:11 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.5 0.88 2.5 09/25/12 19:11 120-82-1 1,1,1-Trichloroethane ND ug/L 2.5 1.2 2.5 09/25/12 19:11 71-55-6 1,1,2-Trichloroethane ND ug/L 2.5 0.72 2.5 09/25/12 19:11 79-00-5 Trichloroethene 279 ug/L 2.5 1.2 2.5 09/25/12 19:11 79-01-6 Trichlorofluoromethane ND ug/L 2.5 0.50 2.5 09/25/12 19:11 75-69-4 1,2,3-Trichloropropane ND ug/L 2.5 1.0 2.5 09/25/12 19:11 96-18-4 Vinyl acetate ND ug/L 5.0 0.88 2.5 09/25/12 19:11 108-05-4 Vinyl chloride 1.7J ug/L 2.5 1.6 2.5 09/25/12 19:11 75-01-4 m&p-Xylene ND ug/L 5.0 1.6 2.5 09/25/12 19:11 179601-23-1 o-Xylene ND ug/L 2.5 0.58 2.5 09/25/12 19:11 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 2.5 09/25/12 19:11 460-00-4 Dibromofluoromethane (S) 100 % 70-130 2.5 09/25/12 19:11 1868-53-7 1,2-Dichloroethane-d4 (S) 99 % 70-130 2.5 09/25/12 19:11 17060-07-0 Tbluene-d8 (S) 96 % 70-130 2.5 09/25/12 19:11 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 6 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 LabID: 92131396002 Collected: 09/11/12 13:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 250 21.7 10 09/14/12 20:28 67-64-1 ND ug/L 10.0 2.5 10 09/14/12 20:28 71-43-2 ND ug/L 10.0 3.0 10 09/14/12 20:28 108-86-1 ND ug/L 10.0 1.7 10 09/14/12 20:28 74-97-5 ND ug/L 10.0 1.8 10 09/14/12 20:28 75-27-4 ND ug/L 10.0 2.6 10 09/14/12 20:28 75-25-2 ND ug/L 20.0 2.9 10 09/14/12 20:28 74-83-9 ND ug/L 50.0 9.6 10 09/14/12 20:28 78-93-3 ND ug/L 10.0 2.5 10 09/14/12 20:28 56-23-5 ND ug/L 10.0 2.3 10 09/14/12 20:28 108-90-7 ND ug/L 10.0 5.4 10 09/14/12 20:28 75-00-3 ND ug/L 10.0 1.4 10 09/14/12 20:28 67-66-3 ND ug/L 10.0 1.1 10 09/14/12 20:28 74-87-3 ND ug/L 10.0 3.5 10 09/14/12 20:28 95-49-8 ND ug/L 10.0 3.1 10 09/14/12 20:28 106-43-4 ND ug/L 50.0 25.2 10 09/14/12 20:28 96-12-8 ND ug/L 10.0 2.1 10 09/14/12 20:28 124-48-1 ND ug/L 10.0 2.7 10 09/14/12 20:28 106-93-4 ND ug/L 10.0 2.1 10 09/14/12 20:28 74-95-3 ND ug/L 10.0 3.0 10 09/14/12 20:28 95-50-1 ND ug/L 10.0 2.4 10 09/14/12 20:28 541-73-1 ND ug/L 10.0 3.3 10 09/14/12 20:28 106-46-7 ND ug/L 10.0 2.1 10 09/14/12 20:28 75-71-8 ND ug/L 10.0 3.2 10 09/14/12 20:28 75-34-3 ND ug/L 10.0 1.2 10 09/14/12 20:28 107-06-2 ND ug/L 10.0 5.6 10 09/14/12 20:28 75-35-4 42.6 ug/L 10.0 1.9 10 09/14/12 20:28 156-59-2 ND ug/L 10.0 4.9 10 09/14/12 20:28 156-60-5 ND ug/L 10.0 2.7 10 09/14/12 20:28 78-87-5 ND ug/L 10.0 2.8 10 09/14/12 20:28 142-28-9 ND ug/L 10.0 1.3 10 09/14/12 20:28 594-20-7 ND ug/L 10.0 4.9 10 09/14/12 20:28 563-58-6 ND ug/L 10.0 1.3 10 09/14/12 20:28 10061-01-5 ND ug/L 10.0 2.6 10 09/14/12 20:28 10061-02-6 ND ug/L 10.0 1.2 10 09/14/12 20:28 108-20-3 ND ug/L 10.0 3.0 10 09/14/12 20:28 100-41-4 ND ug/L 10.0 7.1 10 09/14/12 20:28 87-68-3 ND ug/L 50.0 4.6 10 09/14/12 20:28 591-78-6 ND ug/L 10.0 3.1 10 09/14/12 20:28 99-87-6 ND ug/L 20.0 9.7 10 09/14/12 20:28 75-09-2 ND ug/L 50.0 3.3 10 09/14/12 20:28 108-10-1 ND ug/L 10.0 2.1 10 09/14/12 20:28 1634-04-4 ND ug/L 10.0 2.4 10 09/14/12 20:28 91-20-3 ND ug/L 10.0 2.6 10 09/14/12 20:28 100-42-5 ND ug/L 10.0 3.3 10 09/14/12 20:28 630-20-6 ND ug/L 10.0 4.0 10 09/14/12 20:28 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 7 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 LabID: 92131396002 Collected: 09/11/12 13:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2550 ug/L 20.0 9.2 20 09/17/12 14:47 127-18-4 Toluene ND ug/L 10.0 2.6 10 09/14/12 20:28 108-88-3 1,2,3-Trichlorobenzene ND ug/L 10.0 3.3 10 09/14/12 20:28 87-61-6 1,2,4-Trichlorobenzene ND ug/L 10.0 3.5 10 09/14/12 20:28 120-82-1 1,1,1-Trichloroethane ND ug/L 10.0 4.8 10 09/14/12 20:28 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 2.9 10 09/14/12 20:28 79-00-5 Trichloroethene 51.5 ug/L 10.0 4.7 10 09/14/12 20:28 79-01-6 Trichlorofluoromethane ND ug/L 10.0 2.0 10 09/14/12 20:28 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.1 10 09/14/12 20:28 96-18-4 Vinyl acetate ND ug/L 20.0 3.5 10 09/14/12 20:28 108-05-4 Vinyl chloride ND ug/L 10.0 6.2 10 09/14/12 20:28 75-01-4 m&p-Xylene ND ug/L 20.0 6.6 10 09/14/12 20:28 179601-23-1 o-Xylene ND ug/L 10.0 2.3 10 09/14/12 20:28 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 10 09/14/12 20:28 460-00-4 Dibromofluoromethane (S) 105 % 70-130 10 09/14/12 20:28 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 10 09/14/12 20:28 17060-07-0 Tbluene-d8 (S) 95 % 70-130 10 09/14/12 20:28 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 8 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 LabID: 92131396003 Collected: 09/11/12 10:12 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/14/12 19:25 67-64-1 ND ug/L 1.0 0.25 1 09/14/12 19:25 71-43-2 ND ug/L 1.0 0.30 1 09/14/12 19:25 108-86-1 ND ug/L 1.0 0.17 1 09/14/12 19:25 74-97-5 ND ug/L 1.0 0.18 1 09/14/12 19:25 75-27-4 ND ug/L 1.0 0.26 1 09/14/12 19:25 75-25-2 ND ug/L 2.0 0.29 1 09/14/12 19:25 74-83-9 ND ug/L 5.0 0.96 1 09/14/12 19:25 78-93-3 ND ug/L 1.0 0.25 1 09/14/12 19:25 56-23-5 ND ug/L 1.0 0.23 1 09/14/12 19:25 108-90-7 ND ug/L 1.0 0.54 1 09/14/12 19:25 75-00-3 ND ug/L 1.0 0.14 1 09/14/12 19:25 67-66-3 ND ug/L 1.0 0.11 1 09/14/12 19:25 74-87-3 ND ug/L 1.0 0.35 1 09/14/12 19:25 95-49-8 ND ug/L 1.0 0.31 1 09/14/12 19:25 106-43-4 ND ug/L 5.0 2.5 1 09/14/12 19:25 96-12-8 ND ug/L 1.0 0.21 1 09/14/12 19:25 124-48-1 ND ug/L 1.0 0.27 1 09/14/12 19:25 106-93-4 ND ug/L 1.0 0.21 1 09/14/12 19:25 74-95-3 ND ug/L 1.0 0.30 1 09/14/12 19:25 95-50-1 ND ug/L 1.0 0.24 1 09/14/12 19:25 541-73-1 ND ug/L 1.0 0.33 1 09/14/12 19:25 106-46-7 ND ug/L 1.0 0.21 1 09/14/12 19:25 75-71-8 ND ug/L 1.0 0.32 1 09/14/12 19:25 75-34-3 ND ug/L 1.0 0.12 1 09/14/12 19:25 107-06-2 ND ug/L 1.0 0.56 1 09/14/12 19:25 75-35-4 ND ug/L 1.0 0.19 1 09/14/12 19:25 156-59-2 ND ug/L 1.0 0.49 1 09/14/12 19:25 156-60-5 ND ug/L 1.0 0.27 1 09/14/12 19:25 78-87-5 ND ug/L 1.0 0.28 1 09/14/12 19:25 142-28-9 ND ug/L 1.0 0.13 1 09/14/12 19:25 594-20-7 ND ug/L 1.0 0.49 1 09/14/12 19:25 563-58-6 ND ug/L 1.0 0.13 1 09/14/12 19:25 10061-01-5 ND ug/L 1.0 0.26 1 09/14/12 19:25 10061-02-6 ND ug/L 1.0 0.12 1 09/14/12 19:25 108-20-3 ND ug/L 1.0 0.30 1 09/14/12 19:25 100-41-4 ND ug/L 1.0 0.71 1 09/14/12 19:25 87-68-3 ND ug/L 5.0 0.46 1 09/14/12 19:25 591-78-6 ND ug/L 1.0 0.31 1 09/14/12 19:25 99-87-6 ND ug/L 2.0 0.97 1 09/14/12 19:25 75-09-2 ND ug/L 5.0 0.33 1 09/14/12 19:25 108-10-1 ND ug/L 1.0 0.21 1 09/14/12 19:25 1634-04-4 ND ug/L 1.0 0.24 1 09/14/12 19:25 91-20-3 ND ug/L 1.0 0.26 1 09/14/12 19:25 100-42-5 ND ug/L 1.0 0.33 1 09/14/12 19:25 630-20-6 ND ug/L 1.0 0.40 1 09/14/12 19:25 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 9 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 LabID: 92131396003 Collected: 09/11/12 10:12 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 175 ug/L 1.0 0.46 1 09/14/12 19:25 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/14/12 19:25 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/14/12 19:25 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/14/12 19:25 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/14/12 19:25 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/14/12 19:25 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/14/12 19:25 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/14/12 19:25 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/14/12 19:25 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/14/12 19:25 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/14/12 19:25 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/14/12 19:25 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/14/12 19:25 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/14/12 19:25 460-00-4 Dibromofluoromethane (S) 103 % 70-130 1 09/14/12 19:25 1868-53-7 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 09/14/12 19:25 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/14/12 19:25 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 10 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 LabID: 92131396004 Collected: 09/11/12 12:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 50.0 20.0 2 09/25/12 19:42 67-64-1 ND ug/L 2.0 0.50 2 09/25/12 19:42 71-43-2 ND ug/L 2.0 0.60 2 09/25/12 19:42 108-86-1 ND ug/L 2.0 0.34 2 09/25/12 19:42 74-97-5 ND ug/L 2.0 0.36 2 09/25/12 19:42 75-27-4 ND ug/L 2.0 0.52 2 09/25/12 19:42 75-25-2 ND ug/L 4.0 0.58 2 09/25/12 19:42 74-83-9 ND ug/L 10.0 1.9 2 09/25/12 19:42 78-93-3 ND ug/L 2.0 0.50 2 09/25/12 19:42 56-23-5 0.47J ug/L 2.0 0.46 2 09/25/12 19:42 108-90-7 ND ug/L 2.0 1.1 2 09/25/12 19:42 75-00-3 ND ug/L 2.0 0.28 2 09/25/12 19:42 67-66-3 ND ug/L 2.0 0.22 2 09/25/12 19:42 74-87-3 ND ug/L 2.0 0.70 2 09/25/12 19:42 95-49-8 ND ug/L 2.0 0.62 2 09/25/12 19:42 106-43-4 ND ug/L 10.0 5.0 2 09/25/12 19:42 96-12-8 ND ug/L 2.0 0.42 2 09/25/12 19:42 124-48-1 ND ug/L 2.0 0.54 2 09/25/12 19:42 106-93-4 ND ug/L 2.0 0.42 2 09/25/12 19:42 74-95-3 ND ug/L 2.0 0.60 2 09/25/12 19:42 95-50-1 ND ug/L 2.0 0.48 2 09/25/12 19:42 541-73-1 ND ug/L 2.0 0.66 2 09/25/12 19:42 106-46-7 ND ug/L 2.0 0.42 2 09/25/12 19:42 75-71-8 ND ug/L 2.0 0.64 2 09/25/12 19:42 75-34-3 ND ug/L 2.0 0.24 2 09/25/12 19:42 107-06-2 ND ug/L 2.0 1.1 2 09/25/12 19:42 75-35-4 325 ug/L 2.0 0.38 2 09/25/12 19:42 156-59-2 1.9J ug/L 2.0 0.98 2 09/25/12 19:42 156-60-5 ND ug/L 2.0 0.54 2 09/25/12 19:42 78-87-5 ND ug/L 2.0 0.56 2 09/25/12 19:42 142-28-9 ND ug/L 2.0 0.26 2 09/25/12 19:42 594-20-7 ND ug/L 2.0 0.98 2 09/25/12 19:42 563-58-6 ND ug/L 2.0 0.26 2 09/25/12 19:42 10061-01-5 ND ug/L 2.0 0.52 2 09/25/12 19:42 10061-02-6 ND ug/L 2.0 0.24 2 09/25/12 19:42 108-20-3 ND ug/L 2.0 0.60 2 09/25/12 19:42 100-41-4 ND ug/L 2.0 1.4 2 09/25/12 19:42 87-68-3 ND ug/L 10.0 0.92 2 09/25/12 19:42 591-78-6 ND ug/L 2.0 0.62 2 09/25/12 19:42 99-87-6 ND ug/L 4.0 1.9 2 09/25/12 19:42 75-09-2 ND ug/L 10.0 0.66 2 09/25/12 19:42 108-10-1 ND ug/L 2.0 0.42 2 09/25/12 19:42 1634-04-4 ND ug/L 2.0 0.48 2 09/25/12 19:42 91-20-3 ND ug/L 2.0 0.52 2 09/25/12 19:42 100-42-5 ND ug/L 2.0 0.66 2 09/25/12 19:42 630-20-6 ND ug/L 2.0 0.80 2 09/25/12 19:42 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 11 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 LabID: 92131396004 Collected: 09/11/12 12:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2000 ug/L 20.0 9.2 20 09/14/12 20:44 127-18-4 Toluene ND ug/L 2.0 0.52 2 09/25/12 19:42 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.66 2 09/25/12 19:42 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.70 2 09/25/12 19:42 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.96 2 09/25/12 19:42 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.58 2 09/25/12 19:42 79-00-5 Trichloroethene 98.6 ug/L 2.0 0.94 2 09/25/12 19:42 79-01-6 Trichlorofluoromethane ND ug/L 2.0 0.40 2 09/25/12 19:42 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.82 2 09/25/12 19:42 96-18-4 Vinyl acetate ND ug/L 4.0 0.70 2 09/25/12 19:42 108-05-4 Vinyl chloride ND ug/L 2.0 1.2 2 09/25/12 19:42 75-01-4 m&p-Xylene ND ug/L 4.0 1.3 2 09/25/12 19:42 179601-23-1 o-Xylene ND ug/L 2.0 0.46 2 09/25/12 19:42 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 2 09/25/12 19:42 460-00-4 Dibromofluoromethane (S) 104 % 70-130 2 09/25/12 19:42 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 2 09/25/12 19:42 17060-07-0 Tbluene-d8 (S) 93 % 70-130 2 09/25/12 19:42 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 12 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-10 LabID: 92131396005 Collected: 09/12/1212:55 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 59.1 J ug/L 125 50.0 5 09/25/12 20:14 67-64-1 Benzene ND ug/L 5.0 1.2 5 09/25/12 20:14 71-43-2 Bromobenzene ND ug/L 5.0 1.5 5 09/25/12 20:14 108-86-1 Bromochloromethane ND ug/L 5.0 0.85 5 09/25/12 20:14 74-97-5 Bromodichloromethane ND ug/L 5.0 0.90 5 09/25/12 20:14 75-27-4 Bromoform ND ug/L 5.0 1.3 5 09/25/12 20:14 75-25-2 Bromomethane N D ug/L 10.0 1.4 5 09/25/12 20:14 74-83-9 2-Butanone (MEK) 128 ug/L 25.0 4.8 5 09/25/12 20:14 78-93-3 Carbon tetrachloride ND ug/L 5.0 1.2 5 09/25/12 20:14 56-23-5 Chlorobenzene ND ug/L 5.0 1.2 5 09/25/12 20:14 108-90-7 Chloroethane ND ug/L 5.0 2.7 5 09/25/12 20:14 75-00-3 Chloroform ND ug/L 5.0 0.70 5 09/25/12 20:14 67-66-3 Chloromethane ND ug/L 5.0 0.55 5 09/25/12 20:14 74-87-3 2-Chlorotoluene ND ug/L 5.0 1.8 5 09/25/12 20:14 95-49-8 4-Chlorotoluene ND ug/L 5.0 1.6 5 09/25/12 20:14 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 25.0 12.6 5 09/25/12 20:14 96-12-8 Dibromochloromethane ND ug/L 5.0 1.0 5 09/25/12 20:14 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 1.4 5 09/25/12 20:14 106-93-4 Dibromomethane ND ug/L 5.0 1.0 5 09/25/12 20:14 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 1.5 5 09/25/12 20:14 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 1.2 5 09/25/12 20:14 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 1.6 5 09/25/12 20:14 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 1.0 5 09/25/12 20:14 75-71-8 1,1-Dichloroethane ND ug/L 5.0 1.6 5 09/25/12 20:14 75-34-3 1,2-Dichloroethane ND ug/L 5.0 0.60 5 09/25/12 20:14 107-06-2 M-Dichloroethene ND ug/L 5.0 2.8 5 09/25/12 20:14 75-35-4 cis-1,2-Dichloroethene 19.7 ug/L 5.0 0.95 5 09/25/12 20:14 156-59-2 trans- 1,2-Dichloroethene ND ug/L 5.0 2.4 5 09/25/12 20:14 156-60-5 1,2-Dichloropropane ND ug/L 5.0 1.4 5 09/25/12 20:14 78-87-5 1,3-Dichloropropane ND ug/L 5.0 1.4 5 09/25/12 20:14 142-28-9 2,2-Dichloropropane ND ug/L 5.0 0.65 5 09/25/12 20:14 594-20-7 1,1-Dichloropropene ND ug/L 5.0 2.4 5 09/25/12 20:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 0.65 5 09/25/12 20:14 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 5.0 1.3 5 09/25/12 20:14 10061-02-6 Diisopropyl ether ND ug/L 5.0 0.60 5 09/25/12 20:14 108-20-3 Ethylbenzene ND ug/L 5.0 1.5 5 09/25/12 20:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 3.6 5 09/25/12 20:14 87-68-3 2-Hexanone ND ug/L 25.0 2.3 5 09/25/12 20:14 591-78-6 p-Isopropyltoluene ND ug/L 5.0 1.6 5 09/25/12 20:14 99-87-6 Methylene Chloride ND ug/L 10.0 4.8 5 09/25/12 20:14 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 25.0 1.6 5 09/25/12 20:14 108-10-1 Methyl-tert-butyl ether ND ug/L 5.0 1.0 5 09/25/12 20:14 1634-04-4 Naphthalene ND ug/L 5.0 1.2 5 09/25/12 20:14 91-20-3 Styrene ND ug/L 5.0 1.3 5 09/25/12 20:14 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 1.6 5 09/25/12 20:14 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 5.0 2.0 5 09/25/12 20:14 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 13 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-10 LabID: 92131396005 Collected: 09/12/1212:55 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 4.7J ug/L 5.0 2.3 5 09/25/12 20:14 127-18-4 Toluene 8800 ug/L 50.0 13.0 50 09/14/12 20:59 108-88-3 1,2,3-Trichlorobenzene ND ug/L 5.0 1.6 5 09/25/12 20:14 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 1.8 5 09/25/12 20:14 120-82-1 1,1,1-Trichloroethane ND ug/L 5.0 2.4 5 09/25/12 20:14 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 1.4 5 09/25/12 20:14 79-00-5 Trichloroethene ND ug/L 5.0 2.4 5 09/25/12 20:14 79-01-6 Trichlorofluoromethane ND ug/L 5.0 1.0 5 09/25/12 20:14 75-69-4 1,2,3-Trichloropropane ND ug/L 5.0 2.0 5 09/25/12 20:14 96-18-4 Vinyl acetate ND ug/L 10.0 1.8 5 09/25/12 20:14 108-05-4 Vinyl chloride 5.OJ ug/L 5.0 3.1 5 09/25/12 20:14 75-01-4 m&p-Xylene ND ug/L 10.0 3.3 5 09/25/12 20:14 179601-23-1 o-Xylene ND ug/L 5.0 1.2 5 09/25/12 20:14 95-47-6 Surrogates 4-Bromofluorobenzene (S) 93 % 70-130 5 09/25/12 20:14 460-00-4 Dibromofluoromethane (S) 92 % 70-130 5 09/25/12 20:14 1868-53-7 1,2-Dichloroethane-d4 (S) 99 % 70-130 5 09/25/12 20:14 17060-07-0 Tbluene-d8 (S) 98 % 70-130 5 09/25/12 20:14 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 14 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-11 LabID: 92131396006 Collected: 09/12/12 13:07 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/25/12 16:03 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/25/12 16:03 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/25/12 16:03 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/25/12 16:03 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/25/12 16:03 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/25/12 16:03 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/25/12 16:03 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/25/12 16:03 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/25/12 16:03 56-23-5 Chlorobenzene 0.39J ug/L 1.0 0.23 1 09/25/12 16:03 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/25/12 16:03 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/25/12 16:03 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/25/12 16:03 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/25/12 16:03 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/25/12 16:03 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/25/12 16:03 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/25/12 16:03 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/25/12 16:03 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/25/12 16:03 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/25/12 16:03 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/25/12 16:03 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 16:03 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/25/12 16:03 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/25/12 16:03 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/25/12 16:03 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/25/12 16:03 75-35-4 cis-1,2-Dichloroethene 162 ug/L 1.0 0.19 1 09/25/12 16:03 156-59-2 trans- 1,2-Dichloroethene 1.6 ug/L 1.0 0.49 1 09/25/12 16:03 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/25/12 16:03 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/25/12 16:03 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/25/12 16:03 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/25/12 16:03 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/25/12 16:03 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/25/12 16:03 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/25/12 16:03 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/25/12 16:03 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/25/12 16:03 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/25/12 16:03 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/25/12 16:03 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/25/12 16:03 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/25/12 16:03 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/25/12 16:03 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/25/12 16:03 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/25/12 16:03 100-42-5 1,1,1,2-Tetrachloroethane 0.51J ug/L 1.0 0.33 1 09/25/12 16:03 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/25/12 16:03 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 15 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11 LabID: 92131396006 Collected: 09/12/12 13:07 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1940 ug/L 10.0 4.6 10 09/14/12 21:15 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/25/12 16:03 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 16:03 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/25/12 16:03 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/25/12 16:03 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/25/12 16:03 79-00-5 Trichloroethene 86.6 ug/L 1.0 0.47 1 09/25/12 16:03 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/25/12 16:03 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/25/12 16:03 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/25/12 16:03 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/25/12 16:03 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/25/12 16:03 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/25/12 16:03 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 09/25/12 16:03 460-00-4 Dibromofluoromethane (S) 102 % 70-130 1 09/25/12 16:03 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 09/25/12 16:03 17060-07-0 Tbluene-d8 (S) 96 % 70-130 1 09/25/12 16:03 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 16 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-12 LabID: 92131396007 Collected: 09/11/12 11:55 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 125 50.0 5 09/25/12 20:45 67-64-1 ND ug/L 5.0 1.2 5 09/25/12 20:45 71-43-2 ND ug/L 5.0 1.5 5 09/25/12 20:45 108-86-1 ND ug/L 5.0 0.85 5 09/25/12 20:45 74-97-5 ND ug/L 5.0 0.90 5 09/25/12 20:45 75-27-4 ND ug/L 5.0 1.3 5 09/25/12 20:45 75-25-2 ND ug/L 10.0 1.4 5 09/25/12 20:45 74-83-9 ND ug/L 25.0 4.8 5 09/25/12 20:45 78-93-3 ND ug/L 5.0 1.2 5 09/25/12 20:45 56-23-5 ND ug/L 5.0 1.2 5 09/25/12 20:45 108-90-7 ND ug/L 5.0 2.7 5 09/25/12 20:45 75-00-3 ND ug/L 5.0 0.70 5 09/25/12 20:45 67-66-3 ND ug/L 5.0 0.55 5 09/25/12 20:45 74-87-3 ND ug/L 5.0 1.8 5 09/25/12 20:45 95-49-8 ND ug/L 5.0 1.6 5 09/25/12 20:45 106-43-4 ND ug/L 25.0 12.6 5 09/25/12 20:45 96-12-8 ND ug/L 5.0 1.0 5 09/25/12 20:45 124-48-1 ND ug/L 5.0 1.4 5 09/25/12 20:45 106-93-4 ND ug/L 5.0 1.0 5 09/25/12 20:45 74-95-3 ND ug/L 5.0 1.5 5 09/25/12 20:45 95-50-1 ND ug/L 5.0 1.2 5 09/25/12 20:45 541-73-1 ND ug/L 5.0 1.6 5 09/25/12 20:45 106-46-7 ND ug/L 5.0 1.0 5 09/25/12 20:45 75-71-8 ND ug/L 5.0 1.6 5 09/25/12 20:45 75-34-3 ND ug/L 5.0 0.60 5 09/25/12 20:45 107-06-2 ND ug/L 5.0 2.8 5 09/25/12 20:45 75-35-4 5830 ug/L 50.0 9.5 50 09/14/12 21:31 156-59-2 11.4 ug/L 5.0 2.4 5 09/25/12 20:45 156-60-5 ND ug/L 5.0 1.4 5 09/25/12 20:45 78-87-5 ND ug/L 5.0 1.4 5 09/25/12 20:45 142-28-9 ND ug/L 5.0 0.65 5 09/25/12 20:45 594-20-7 ND ug/L 5.0 2.4 5 09/25/12 20:45 563-58-6 ND ug/L 5.0 0.65 5 09/25/12 20:45 10061-01-5 ND ug/L 5.0 1.3 5 09/25/12 20:45 10061-02-6 ND ug/L 5.0 0.60 5 09/25/12 20:45 108-20-3 ND ug/L 5.0 1.5 5 09/25/12 20:45 100-41-4 ND ug/L 5.0 3.6 5 09/25/12 20:45 87-68-3 ND ug/L 25.0 2.3 5 09/25/12 20:45 591-78-6 ND ug/L 5.0 1.6 5 09/25/12 20:45 99-87-6 ND ug/L 10.0 4.8 5 09/25/12 20:45 75-09-2 ND ug/L 25.0 1.6 5 09/25/12 20:45 108-10-1 ND ug/L 5.0 1.0 5 09/25/12 20:45 1634-04-4 ND ug/L 5.0 1.2 5 09/25/12 20:45 91-20-3 ND ug/L 5.0 1.3 5 09/25/12 20:45 100-42-5 ND ug/L 5.0 1.6 5 09/25/12 20:45 630-20-6 ND ug/L 5.0 2.0 5 09/25/12 20:45 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 17 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-12 LabID: 92131396007 Collected: 09/11/12 11:55 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 3.OJ ug/L 5.0 2.3 5 09/25/12 20:45 127-18-4 Toluene 2.9J ug/L 5.0 1.3 5 09/25/12 20:45 108-88-3 1,2,3-Trichlorobenzene ND ug/L 5.0 1.6 5 09/25/12 20:45 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 1.8 5 09/25/12 20:45 120-82-1 1,1,1-Trichloroethane ND ug/L 5.0 2.4 5 09/25/12 20:45 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 1.4 5 09/25/12 20:45 79-00-5 Trichloroethene ND ug/L 5.0 2.4 5 09/25/12 20:45 79-01-6 Trichlorofluoromethane ND ug/L 5.0 1.0 5 09/25/12 20:45 75-69-4 1,2,3-Trichloropropane ND ug/L 5.0 2.0 5 09/25/12 20:45 96-18-4 Vinyl acetate ND ug/L 10.0 1.8 5 09/25/12 20:45 108-05-4 Vinyl chloride 22.7 ug/L 5.0 3.1 5 09/25/12 20:45 75-01-4 m&p-Xylene ND ug/L 10.0 3.3 5 09/25/12 20:45 179601-23-1 o-Xylene ND ug/L 5.0 1.2 5 09/25/12 20:45 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 5 09/25/12 20:45 460-00-4 Dibromofluoromethane (S) 105 % 70-130 5 09/25/12 20:45 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 5 09/25/12 20:45 17060-07-0 Tbluene-d8 (S) 100 % 70-130 5 09/25/12 20:45 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 18 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 LabID: 92131396008 Collected: 09/11/1214:30 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/14/12 19:41 67-64-1 ND ug/L 1.0 0.25 1 09/14/12 19:41 71-43-2 ND ug/L 1.0 0.30 1 09/14/12 19:41 108-86-1 ND ug/L 1.0 0.17 1 09/14/12 19:41 74-97-5 ND ug/L 1.0 0.18 1 09/14/12 19:41 75-27-4 ND ug/L 1.0 0.26 1 09/14/12 19:41 75-25-2 ND ug/L 2.0 0.29 1 09/14/12 19:41 74-83-9 ND ug/L 5.0 0.96 1 09/14/12 19:41 78-93-3 ND ug/L 1.0 0.25 1 09/14/12 19:41 56-23-5 0.24J ug/L 1.0 0.23 1 09/14/12 19:41 108-90-7 ND ug/L 1.0 0.54 1 09/14/12 19:41 75-00-3 ND ug/L 1.0 0.14 1 09/14/12 19:41 67-66-3 ND ug/L 1.0 0.11 1 09/14/12 19:41 74-87-3 ND ug/L 1.0 0.35 1 09/14/12 19:41 95-49-8 ND ug/L 1.0 0.31 1 09/14/12 19:41 106-43-4 ND ug/L 5.0 2.5 1 09/14/12 19:41 96-12-8 ND ug/L 1.0 0.21 1 09/14/12 19:41 124-48-1 ND ug/L 1.0 0.27 1 09/14/12 19:41 106-93-4 ND ug/L 1.0 0.21 1 09/14/12 19:41 74-95-3 ND ug/L 1.0 0.30 1 09/14/12 19:41 95-50-1 ND ug/L 1.0 0.24 1 09/14/12 19:41 541-73-1 ND ug/L 1.0 0.33 1 09/14/12 19:41 106-46-7 ND ug/L 1.0 0.21 1 09/14/12 19:41 75-71-8 ND ug/L 1.0 0.32 1 09/14/12 19:41 75-34-3 ND ug/L 1.0 0.12 1 09/14/12 19:41 107-06-2 0.88J ug/L 1.0 0.56 1 09/14/12 19:41 75-35-4 196 ug/L 1.0 0.19 1 09/14/12 19:41 156-59-2 0.79J ug/L 1.0 0.49 1 09/14/12 19:41 156-60-5 ND ug/L 1.0 0.27 1 09/14/12 19:41 78-87-5 ND ug/L 1.0 0.28 1 09/14/12 19:41 142-28-9 ND ug/L 1.0 0.13 1 09/14/12 19:41 594-20-7 ND ug/L 1.0 0.49 1 09/14/12 19:41 563-58-6 ND ug/L 1.0 0.13 1 09/14/12 19:41 10061-01-5 ND ug/L 1.0 0.26 1 09/14/12 19:41 10061-02-6 ND ug/L 1.0 0.12 1 09/14/12 19:41 108-20-3 ND ug/L 1.0 0.30 1 09/14/12 19:41 100-41-4 ND ug/L 1.0 0.71 1 09/14/12 19:41 87-68-3 ND ug/L 5.0 0.46 1 09/14/12 19:41 591-78-6 ND ug/L 1.0 0.31 1 09/14/12 19:41 99-87-6 ND ug/L 2.0 0.97 1 09/14/12 19:41 75-09-2 ND ug/L 5.0 0.33 1 09/14/12 19:41 108-10-1 ND ug/L 1.0 0.21 1 09/14/12 19:41 1634-04-4 ND ug/L 1.0 0.24 1 09/14/12 19:41 91-20-3 ND ug/L 1.0 0.26 1 09/14/12 19:41 100-42-5 ND ug/L 1.0 0.33 1 09/14/12 19:41 630-20-6 ND ug/L 1.0 0.40 1 09/14/12 19:41 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 19 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 LabID: 92131396008 Collected: 09/11/1214:30 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 979 ug/L 20.0 9.2 20 09/17/12 15:03 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/14/12 19:41 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/14/12 19:41 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/14/12 19:41 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/14/12 19:41 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/14/12 19:41 79-00-5 Trichloroethene 211 ug/L 20.0 9.4 20 09/17/12 15:03 79-01-6 Trichlorofluoromethane 0.45J ug/L 1.0 0.20 1 09/14/12 19:41 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/14/12 19:41 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/14/12 19:41 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/14/12 19:41 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/14/12 19:41 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/14/12 19:41 95-47-6 Surrogates 4-Bromofluorobenzene (S) 92 % 70-130 1 09/14/12 19:41 460-00-4 Dibromofluoromethane (S) 101 % 70-130 1 09/14/12 19:41 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 09/14/12 19:41 17060-07-0 Tbluene-d8 (S) 92 % 70-130 1 09/14/12 19:41 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 20 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 LabID: 92131396009 Collected: 09/11/12 14:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/25/12 16:34 67-64-1 ND ug/L 1.0 0.25 1 09/25/12 16:34 71-43-2 ND ug/L 1.0 0.30 1 09/25/12 16:34 108-86-1 ND ug/L 1.0 0.17 1 09/25/12 16:34 74-97-5 ND ug/L 1.0 0.18 1 09/25/12 16:34 75-27-4 ND ug/L 1.0 0.26 1 09/25/12 16:34 75-25-2 ND ug/L 2.0 0.29 1 09/25/12 16:34 74-83-9 ND ug/L 5.0 0.96 1 09/25/12 16:34 78-93-3 ND ug/L 1.0 0.25 1 09/25/12 16:34 56-23-5 0.25J ug/L 1.0 0.23 1 09/25/12 16:34 108-90-7 ND ug/L 1.0 0.54 1 09/25/12 16:34 75-00-3 ND ug/L 1.0 0.14 1 09/25/12 16:34 67-66-3 ND ug/L 1.0 0.11 1 09/25/12 16:34 74-87-3 ND ug/L 1.0 0.35 1 09/25/12 16:34 95-49-8 ND ug/L 1.0 0.31 1 09/25/12 16:34 106-43-4 ND ug/L 5.0 2.5 1 09/25/12 16:34 96-12-8 ND ug/L 1.0 0.21 1 09/25/12 16:34 124-48-1 ND ug/L 1.0 0.27 1 09/25/12 16:34 106-93-4 ND ug/L 1.0 0.21 1 09/25/12 16:34 74-95-3 ND ug/L 1.0 0.30 1 09/25/12 16:34 95-50-1 ND ug/L 1.0 0.24 1 09/25/12 16:34 541-73-1 ND ug/L 1.0 0.33 1 09/25/12 16:34 106-46-7 ND ug/L 1.0 0.21 1 09/25/12 16:34 75-71-8 ND ug/L 1.0 0.32 1 09/25/12 16:34 75-34-3 ND ug/L 1.0 0.12 1 09/25/12 16:34 107-06-2 1.5 ug/L 1.0 0.56 1 09/25/12 16:34 75-35-4 158 ug/L 1.0 0.19 1 09/25/12 16:34 156-59-2 ND ug/L 1.0 0.49 1 09/25/12 16:34 156-60-5 ND ug/L 1.0 0.27 1 09/25/12 16:34 78-87-5 ND ug/L 1.0 0.28 1 09/25/12 16:34 142-28-9 ND ug/L 1.0 0.13 1 09/25/12 16:34 594-20-7 ND ug/L 1.0 0.49 1 09/25/12 16:34 563-58-6 ND ug/L 1.0 0.13 1 09/25/12 16:34 10061-01-5 ND ug/L 1.0 0.26 1 09/25/12 16:34 10061-02-6 ND ug/L 1.0 0.12 1 09/25/12 16:34 108-20-3 ND ug/L 1.0 0.30 1 09/25/12 16:34 100-41-4 ND ug/L 1.0 0.71 1 09/25/12 16:34 87-68-3 ND ug/L 5.0 0.46 1 09/25/12 16:34 591-78-6 ND ug/L 1.0 0.31 1 09/25/12 16:34 99-87-6 ND ug/L 2.0 0.97 1 09/25/12 16:34 75-09-2 ND ug/L 5.0 0.33 1 09/25/12 16:34 108-10-1 ND ug/L 1.0 0.21 1 09/25/12 16:34 1634-04-4 ND ug/L 1.0 0.24 1 09/25/12 16:34 91-20-3 ND ug/L 1.0 0.26 1 09/25/12 16:34 100-42-5 ND ug/L 1.0 0.33 1 09/25/12 16:34 630-20-6 ND ug/L 1.0 0.40 1 09/25/12 16:34 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 21 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 LabID: 92131396009 Collected: 09/11/12 14:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 968 ug/L 5.0 2.3 5 09/14/12 21:46 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/25/12 16:34 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 16:34 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/25/12 16:34 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/25/12 16:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/25/12 16:34 79-00-5 Trichloroethene 362 ug/L 5.0 2.4 5 09/14/12 21:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/25/12 16:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/25/12 16:34 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/25/12 16:34 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/25/12 16:34 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/25/12 16:34 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/25/12 16:34 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/25/12 16:34 460-00-4 Dibromofluoromethane (S) 102 % 70-130 1 09/25/12 16:34 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 09/25/12 16:34 17060-07-0 Tbluene-d8 (S) 93 % 70-130 1 09/25/12 16:34 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 22 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-15 LabID: 92131396010 Collected: 09/12/1210:30 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/14/12 19:57 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/14/12 19:57 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/14/12 19:57 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/14/12 19:57 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/14/12 19:57 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/14/12 19:57 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/14/12 19:57 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/14/12 19:57 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/14/12 19:57 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/14/12 19:57 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/14/12 19:57 75-00-3 Chloroform 1.0 ug/L 1.0 0.14 1 09/14/12 19:57 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/14/12 19:57 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/14/12 19:57 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/14/12 19:57 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/14/12 19:57 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/14/12 19:57 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/14/12 19:57 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/14/12 19:57 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/14/12 19:57 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/14/12 19:57 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/14/12 19:57 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/14/12 19:57 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/14/12 19:57 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/14/12 19:57 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/14/12 19:57 75-35-4 cis-1,2-Dichloroethene 7.3 ug/L 1.0 0.19 1 09/14/12 19:57 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/14/12 19:57 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/14/12 19:57 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/14/12 19:57 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/14/12 19:57 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/14/12 19:57 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/14/12 19:57 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/14/12 19:57 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/14/12 19:57 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/14/12 19:57 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/14/12 19:57 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/14/12 19:57 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/14/12 19:57 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/14/12 19:57 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/14/12 19:57 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/14/12 19:57 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/14/12 19:57 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/14/12 19:57 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/14/12 19:57 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/14/12 19:57 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 23 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-15 LabID: 92131396010 Collected: 09/12/1210:30 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 176 ug/L 1.0 0.46 1 09/14/12 19:57 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/14/12 19:57 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/14/12 19:57 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/14/12 19:57 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/14/12 19:57 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/14/12 19:57 79-00-5 Trichloroethene 4.0 ug/L 1.0 0.47 1 09/14/12 19:57 79-01-6 Trichlorofluoromethane 1.OJ ug/L 1.0 0.20 1 09/14/12 19:57 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/14/12 19:57 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/14/12 19:57 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/14/12 19:57 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/14/12 19:57 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/14/12 19:57 95-47-6 Surrogates 4-Bromofluorobenzene (S) 92 % 70-130 1 09/14/12 19:57 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/14/12 19:57 1868-53-7 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 09/14/12 19:57 17060-07-0 Tbluene-d8 (S) 96 % 70-130 1 09/14/12 19:57 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 24 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 LabID: 92131396011 Collected: 09/12/1211:00 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 10.0 1 09/25/12 15:32 67-64-1 ND ug/L 1.0 0.25 1 09/25/12 15:32 71-43-2 ND ug/L 1.0 0.30 1 09/25/12 15:32 108-86-1 ND ug/L 1.0 0.17 1 09/25/12 15:32 74-97-5 ND ug/L 1.0 0.18 1 09/25/12 15:32 75-27-4 ND ug/L 1.0 0.26 1 09/25/12 15:32 75-25-2 ND ug/L 2.0 0.29 1 09/25/12 15:32 74-83-9 ND ug/L 5.0 0.96 1 09/25/12 15:32 78-93-3 ND ug/L 1.0 0.25 1 09/25/12 15:32 56-23-5 ND ug/L 1.0 0.23 1 09/25/12 15:32 108-90-7 ND ug/L 1.0 0.54 1 09/25/12 15:32 75-00-3 1.3 ug/L 1.0 0.14 1 09/25/12 15:32 67-66-3 ND ug/L 1.0 0.11 1 09/25/12 15:32 74-87-3 ND ug/L 1.0 0.35 1 09/25/12 15:32 95-49-8 ND ug/L 1.0 0.31 1 09/25/12 15:32 106-43-4 ND ug/L 5.0 2.5 1 09/25/12 15:32 96-12-8 ND ug/L 1.0 0.21 1 09/25/12 15:32 124-48-1 ND ug/L 1.0 0.27 1 09/25/12 15:32 106-93-4 ND ug/L 1.0 0.21 1 09/25/12 15:32 74-95-3 ND ug/L 1.0 0.30 1 09/25/12 15:32 95-50-1 ND ug/L 1.0 0.24 1 09/25/12 15:32 541-73-1 ND ug/L 1.0 0.33 1 09/25/12 15:32 106-46-7 ND ug/L 1.0 0.21 1 09/25/12 15:32 75-71-8 ND ug/L 1.0 0.32 1 09/25/12 15:32 75-34-3 ND ug/L 1.0 0.12 1 09/25/12 15:32 107-06-2 ND ug/L 1.0 0.56 1 09/25/12 15:32 75-35-4 9.0 ug/L 1.0 0.19 1 09/25/12 15:32 156-59-2 ND ug/L 1.0 0.49 1 09/25/12 15:32 156-60-5 ND ug/L 1.0 0.27 1 09/25/12 15:32 78-87-5 ND ug/L 1.0 0.28 1 09/25/12 15:32 142-28-9 ND ug/L 1.0 0.13 1 09/25/12 15:32 594-20-7 ND ug/L 1.0 0.49 1 09/25/12 15:32 563-58-6 ND ug/L 1.0 0.13 1 09/25/12 15:32 10061-01-5 ND ug/L 1.0 0.26 1 09/25/12 15:32 10061-02-6 ND ug/L 1.0 0.12 1 09/25/12 15:32 108-20-3 ND ug/L 1.0 0.30 1 09/25/12 15:32 100-41-4 ND ug/L 1.0 0.71 1 09/25/12 15:32 87-68-3 ND ug/L 5.0 0.46 1 09/25/12 15:32 591-78-6 ND ug/L 1.0 0.31 1 09/25/12 15:32 99-87-6 ND ug/L 2.0 0.97 1 09/25/12 15:32 75-09-2 ND ug/L 5.0 0.33 1 09/25/12 15:32 108-10-1 ND ug/L 1.0 0.21 1 09/25/12 15:32 1634-04-4 ND ug/L 1.0 0.24 1 09/25/12 15:32 91-20-3 ND ug/L 1.0 0.26 1 09/25/12 15:32 100-42-5 ND ug/L 1.0 0.33 1 09/25/12 15:32 630-20-6 ND ug/L 1.0 0.40 1 09/25/12 15:32 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 25 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 LabID: 92131396011 Collected: 09/12/1211:00 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 180 ug/L 2.0 0.92 2 09/15/12 10:04 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/25/12 15:32 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 15:32 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/25/12 15:32 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/25/12 15:32 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/25/12 15:32 79-00-5 Trichloroethene 4.4 ug/L 1.0 0.47 1 09/25/12 15:32 79-01-6 Trichlorofluoromethane 1.2 ug/L 1.0 0.20 1 09/25/12 15:32 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/25/12 15:32 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/25/12 15:32 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/25/12 15:32 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/25/12 15:32 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/25/12 15:32 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/25/12 15:32 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/25/12 15:32 1868-53-7 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 09/25/12 15:32 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/25/12 15:32 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 26 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-17 LabID: 92131396012 Collected: 09/10/1213:05 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 4.5J ug/L 25.0 2.2 1 09/15/12 04:18 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 04:18 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 04:18 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 04:18 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 04:18 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 04:18 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 04:18 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 04:18 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 04:18 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 04:18 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 04:18 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 04:18 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 04:18 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 04:18 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 04:18 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 04:18 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 04:18 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 04:18 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 04:18 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 04:18 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 04:18 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 04:18 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 04:18 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 04:18 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 04:18 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 04:18 75-35-4 cis-1,2-Dichloroethene 12.3 ug/L 1.0 0.19 1 09/15/12 04:18 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 04:18 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 04:18 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 04:18 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 04:18 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 04:18 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 04:18 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 04:18 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 04:18 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 04:18 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 04:18 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 04:18 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 04:18 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 04:18 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 04:18 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 04:18 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 04:18 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 04:18 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 04:18 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 04:18 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 27 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-17 LabID: 92131396012 Collected: 09/10/1213:05 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.0 ug/L 1.0 0.46 1 09/15/12 04:18 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 04:18 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 04:18 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 04:18 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 04:18 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 04:18 79-00-5 Trichloroethene 0.96J ug/L 1.0 0.47 1 09/15/12 04:18 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 04:18 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 04:18 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 04:18 108-05-4 Vinyl chloride 7.3 ug/L 1.0 0.62 1 09/15/12 04:18 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 04:18 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 04:18 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 09/15/12 04:18 460-00-4 Dibromofluoromethane (S) 109 % 70-130 1 09/15/12 04:18 1868-53-7 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 09/15/12 04:18 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 09/15/12 04:18 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 28 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-18 LabID: 92131396013 Collected: 09/11/1215:15 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/15/12 04:34 67-64-1 ND ug/L 1.0 0.25 1 09/15/12 04:34 71-43-2 ND ug/L 1.0 0.30 1 09/15/12 04:34 108-86-1 ND ug/L 1.0 0.17 1 09/15/12 04:34 74-97-5 ND ug/L 1.0 0.18 1 09/15/12 04:34 75-27-4 ND ug/L 1.0 0.26 1 09/15/12 04:34 75-25-2 ND ug/L 2.0 0.29 1 09/15/12 04:34 74-83-9 ND ug/L 5.0 0.96 1 09/15/12 04:34 78-93-3 ND ug/L 1.0 0.25 1 09/15/12 04:34 56-23-5 ND ug/L 1.0 0.23 1 09/15/12 04:34 108-90-7 ND ug/L 1.0 0.54 1 09/15/12 04:34 75-00-3 1.6 ug/L 1.0 0.14 1 09/15/12 04:34 67-66-3 ND ug/L 1.0 0.11 1 09/15/12 04:34 74-87-3 ND ug/L 1.0 0.35 1 09/15/12 04:34 95-49-8 ND ug/L 1.0 0.31 1 09/15/12 04:34 106-43-4 ND ug/L 5.0 2.5 1 09/15/12 04:34 96-12-8 ND ug/L 1.0 0.21 1 09/15/12 04:34 124-48-1 ND ug/L 1.0 0.27 1 09/15/12 04:34 106-93-4 ND ug/L 1.0 0.21 1 09/15/12 04:34 74-95-3 ND ug/L 1.0 0.30 1 09/15/12 04:34 95-50-1 ND ug/L 1.0 0.24 1 09/15/12 04:34 541-73-1 ND ug/L 1.0 0.33 1 09/15/12 04:34 106-46-7 ND ug/L 1.0 0.21 1 09/15/12 04:34 75-71-8 ND ug/L 1.0 0.32 1 09/15/12 04:34 75-34-3 ND ug/L 1.0 0.12 1 09/15/12 04:34 107-06-2 ND ug/L 1.0 0.56 1 09/15/12 04:34 75-35-4 ND ug/L 1.0 0.19 1 09/15/12 04:34 156-59-2 ND ug/L 1.0 0.49 1 09/15/12 04:34 156-60-5 ND ug/L 1.0 0.27 1 09/15/12 04:34 78-87-5 ND ug/L 1.0 0.28 1 09/15/12 04:34 142-28-9 ND ug/L 1.0 0.13 1 09/15/12 04:34 594-20-7 ND ug/L 1.0 0.49 1 09/15/12 04:34 563-58-6 ND ug/L 1.0 0.13 1 09/15/12 04:34 10061-01-5 ND ug/L 1.0 0.26 1 09/15/12 04:34 10061-02-6 ND ug/L 1.0 0.12 1 09/15/12 04:34 108-20-3 ND ug/L 1.0 0.30 1 09/15/12 04:34 100-41-4 ND ug/L 1.0 0.71 1 09/15/12 04:34 87-68-3 ND ug/L 5.0 0.46 1 09/15/12 04:34 591-78-6 ND ug/L 1.0 0.31 1 09/15/12 04:34 99-87-6 ND ug/L 2.0 0.97 1 09/15/12 04:34 75-09-2 ND ug/L 5.0 0.33 1 09/15/12 04:34 108-10-1 ND ug/L 1.0 0.21 1 09/15/12 04:34 1634-04-4 ND ug/L 1.0 0.24 1 09/15/12 04:34 91-20-3 ND ug/L 1.0 0.26 1 09/15/12 04:34 100-42-5 ND ug/L 1.0 0.33 1 09/15/12 04:34 630-20-6 ND ug/L 1.0 0.40 1 09/15/12 04:34 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 29 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-18 LabID: 92131396013 Collected: 09/11/1215:15 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.8 ug/L 1.0 0.46 1 09/15/12 04:34 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 04:34 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 04:34 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 04:34 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 04:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 04:34 79-00-5 Trichloroethene 0.88J ug/L 1.0 0.47 1 09/15/12 04:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 04:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 04:34 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 04:34 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 04:34 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 04:34 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 04:34 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 09/15/12 04:34 460-00-4 Dibromofluoromethane (S) 104 % 70-130 1 09/15/12 04:34 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 09/15/12 04:34 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/15/12 04:34 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 30 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-20 LabID: 92131396014 Collected: 09/11/12 10:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/15/12 04:50 67-64-1 ND ug/L 1.0 0.25 1 09/15/12 04:50 71-43-2 ND ug/L 1.0 0.30 1 09/15/12 04:50 108-86-1 ND ug/L 1.0 0.17 1 09/15/12 04:50 74-97-5 ND ug/L 1.0 0.18 1 09/15/12 04:50 75-27-4 ND ug/L 1.0 0.26 1 09/15/12 04:50 75-25-2 ND ug/L 2.0 0.29 1 09/15/12 04:50 74-83-9 ND ug/L 5.0 0.96 1 09/15/12 04:50 78-93-3 ND ug/L 1.0 0.25 1 09/15/12 04:50 56-23-5 ND ug/L 1.0 0.23 1 09/15/12 04:50 108-90-7 ND ug/L 1.0 0.54 1 09/15/12 04:50 75-00-3 ND ug/L 1.0 0.14 1 09/15/12 04:50 67-66-3 ND ug/L 1.0 0.11 1 09/15/12 04:50 74-87-3 ND ug/L 1.0 0.35 1 09/15/12 04:50 95-49-8 ND ug/L 1.0 0.31 1 09/15/12 04:50 106-43-4 ND ug/L 5.0 2.5 1 09/15/12 04:50 96-12-8 ND ug/L 1.0 0.21 1 09/15/12 04:50 124-48-1 ND ug/L 1.0 0.27 1 09/15/12 04:50 106-93-4 ND ug/L 1.0 0.21 1 09/15/12 04:50 74-95-3 ND ug/L 1.0 0.30 1 09/15/12 04:50 95-50-1 ND ug/L 1.0 0.24 1 09/15/12 04:50 541-73-1 ND ug/L 1.0 0.33 1 09/15/12 04:50 106-46-7 ND ug/L 1.0 0.21 1 09/15/12 04:50 75-71-8 ND ug/L 1.0 0.32 1 09/15/12 04:50 75-34-3 ND ug/L 1.0 0.12 1 09/15/12 04:50 107-06-2 ND ug/L 1.0 0.56 1 09/15/12 04:50 75-35-4 ND ug/L 1.0 0.19 1 09/15/12 04:50 156-59-2 ND ug/L 1.0 0.49 1 09/15/12 04:50 156-60-5 ND ug/L 1.0 0.27 1 09/15/12 04:50 78-87-5 ND ug/L 1.0 0.28 1 09/15/12 04:50 142-28-9 ND ug/L 1.0 0.13 1 09/15/12 04:50 594-20-7 ND ug/L 1.0 0.49 1 09/15/12 04:50 563-58-6 ND ug/L 1.0 0.13 1 09/15/12 04:50 10061-01-5 ND ug/L 1.0 0.26 1 09/15/12 04:50 10061-02-6 ND ug/L 1.0 0.12 1 09/15/12 04:50 108-20-3 ND ug/L 1.0 0.30 1 09/15/12 04:50 100-41-4 ND ug/L 1.0 0.71 1 09/15/12 04:50 87-68-3 ND ug/L 5.0 0.46 1 09/15/12 04:50 591-78-6 ND ug/L 1.0 0.31 1 09/15/12 04:50 99-87-6 ND ug/L 2.0 0.97 1 09/15/12 04:50 75-09-2 ND ug/L 5.0 0.33 1 09/15/12 04:50 108-10-1 ND ug/L 1.0 0.21 1 09/15/12 04:50 1634-04-4 ND ug/L 1.0 0.24 1 09/15/12 04:50 91-20-3 ND ug/L 1.0 0.26 1 09/15/12 04:50 100-42-5 ND ug/L 1.0 0.33 1 09/15/12 04:50 630-20-6 ND ug/L 1.0 0.40 1 09/15/12 04:50 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 31 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-20 LabID: 92131396014 Collected: 09/11/12 10:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/15/12 04:50 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 04:50 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 04:50 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 04:50 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 04:50 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 04:50 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 04:50 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 04:50 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 04:50 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 04:50 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 04:50 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 04:50 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 04:50 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/15/12 04:50 460-00-4 Dibromofluoromethane (S) 106 % 70-130 1 09/15/12 04:50 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/15/12 04:50 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/15/12 04:50 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 32 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-21 LabID: 92131396015 Collected: 09/10/12 15:25 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 05:05 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 05:05 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 05:05 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 05:05 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 05:05 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 05:05 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 05:05 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 05:05 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 05:05 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 05:05 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 05:05 75-00-3 Chloroform 0.66J ug/L 1.0 0.14 1 09/15/12 05:05 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 05:05 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 05:05 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 05:05 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 05:05 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 05:05 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 05:05 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 05:05 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 05:05 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 05:05 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 05:05 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 05:05 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 05:05 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 05:05 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 05:05 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 05:05 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 05:05 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 05:05 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 05:05 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 05:05 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 05:05 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 05:05 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 05:05 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 05:05 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 05:05 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 05:05 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 05:05 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 05:05 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 05:05 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 05:05 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 05:05 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 05:05 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 05:05 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 05:05 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 05:05 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 33 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-21 LabID: 92131396015 Collected: 09/10/12 15:25 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/15/12 05:05 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 05:05 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 05:05 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 05:05 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 05:05 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 05:05 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 05:05 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 05:05 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 05:05 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 05:05 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 05:05 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 05:05 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 05:05 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 05:05 460-00-4 Dibromofluoromethane (S) 104 % 70-130 1 09/15/12 05:05 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 09/15/12 05:05 17060-07-0 Tbluene-d8 (S) 97 % 70-130 1 09/15/12 05:05 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 34 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-22 LabID: 92131396016 Collected: 09/10/12 14:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 05:21 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 05:21 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 05:21 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 05:21 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 05:21 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 05:21 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 05:21 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 05:21 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 05:21 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 05:21 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 05:21 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 05:21 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 05:21 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 05:21 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 05:21 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 05:21 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 05:21 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 05:21 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 05:21 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 05:21 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 05:21 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 05:21 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 05:21 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 05:21 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 05:21 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 05:21 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 05:21 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 05:21 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 05:21 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 05:21 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 05:21 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 05:21 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 05:21 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 05:21 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 05:21 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 05:21 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 05:21 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 05:21 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 05:21 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 05:21 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 05:21 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 05:21 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 05:21 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 05:21 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 05:21 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 05:21 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 35 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-22 LabID: 92131396016 Collected: 09/10/12 14:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/15/12 05:21 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 05:21 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 05:21 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 05:21 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 05:21 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 05:21 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 05:21 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 05:21 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 05:21 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 05:21 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 05:21 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 05:21 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 05:21 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 05:21 460-00-4 Dibromofluoromethane (S) 104 % 70-130 1 09/15/12 05:21 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 09/15/12 05:21 17060-07-0 Tbluene-d8 (S) 101 % 70-130 1 09/15/12 05:21 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 36 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-23 LabID: 92131396017 Collected: 09/12/12 10:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 05:37 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 05:37 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 05:37 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 05:37 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 05:37 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 05:37 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 05:37 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 05:37 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 05:37 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 05:37 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 05:37 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 05:37 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 05:37 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 05:37 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 05:37 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 05:37 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 05:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 05:37 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 05:37 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 05:37 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 05:37 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 05:37 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 05:37 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 05:37 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 05:37 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 05:37 75-35-4 cis-1,2-Dichloroethene 7.1 ug/L 1.0 0.19 1 09/15/12 05:37 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 05:37 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 05:37 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 05:37 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 05:37 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 05:37 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 05:37 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 05:37 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 05:37 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 05:37 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 05:37 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 05:37 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 05:37 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 05:37 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 05:37 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 05:37 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 05:37 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 05:37 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 05:37 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 05:37 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 37 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-23 LabID: 92131396017 Collected: 09/12/12 10:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 83.3 ug/L 1.0 0.46 1 09/15/12 05:37 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 05:37 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 05:37 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 05:37 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 05:37 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 05:37 79-00-5 Trichloroethene 4.7 ug/L 1.0 0.47 1 09/15/12 05:37 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 05:37 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 05:37 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 05:37 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 05:37 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 05:37 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 05:37 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/15/12 05:37 460-00-4 Dibromofluoromethane (S) 108 % 70-130 1 09/15/12 05:37 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/15/12 05:37 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/15/12 05:37 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 38 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-24 LabID: 92131396018 Collected: 09/11/12 11:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/15/12 05:52 67-64-1 ND ug/L 1.0 0.25 1 09/15/12 05:52 71-43-2 ND ug/L 1.0 0.30 1 09/15/12 05:52 108-86-1 ND ug/L 1.0 0.17 1 09/15/12 05:52 74-97-5 ND ug/L 1.0 0.18 1 09/15/12 05:52 75-27-4 ND ug/L 1.0 0.26 1 09/15/12 05:52 75-25-2 ND ug/L 2.0 0.29 1 09/15/12 05:52 74-83-9 ND ug/L 5.0 0.96 1 09/15/12 05:52 78-93-3 ND ug/L 1.0 0.25 1 09/15/12 05:52 56-23-5 ND ug/L 1.0 0.23 1 09/15/12 05:52 108-90-7 ND ug/L 1.0 0.54 1 09/15/12 05:52 75-00-3 ND ug/L 1.0 0.14 1 09/15/12 05:52 67-66-3 ND ug/L 1.0 0.11 1 09/15/12 05:52 74-87-3 ND ug/L 1.0 0.35 1 09/15/12 05:52 95-49-8 ND ug/L 1.0 0.31 1 09/15/12 05:52 106-43-4 ND ug/L 5.0 2.5 1 09/15/12 05:52 96-12-8 ND ug/L 1.0 0.21 1 09/15/12 05:52 124-48-1 ND ug/L 1.0 0.27 1 09/15/12 05:52 106-93-4 ND ug/L 1.0 0.21 1 09/15/12 05:52 74-95-3 ND ug/L 1.0 0.30 1 09/15/12 05:52 95-50-1 ND ug/L 1.0 0.24 1 09/15/12 05:52 541-73-1 ND ug/L 1.0 0.33 1 09/15/12 05:52 106-46-7 ND ug/L 1.0 0.21 1 09/15/12 05:52 75-71-8 ND ug/L 1.0 0.32 1 09/15/12 05:52 75-34-3 ND ug/L 1.0 0.12 1 09/15/12 05:52 107-06-2 ND ug/L 1.0 0.56 1 09/15/12 05:52 75-35-4 6.8 ug/L 1.0 0.19 1 09/15/12 05:52 156-59-2 ND ug/L 1.0 0.49 1 09/15/12 05:52 156-60-5 ND ug/L 1.0 0.27 1 09/15/12 05:52 78-87-5 ND ug/L 1.0 0.28 1 09/15/12 05:52 142-28-9 ND ug/L 1.0 0.13 1 09/15/12 05:52 594-20-7 ND ug/L 1.0 0.49 1 09/15/12 05:52 563-58-6 ND ug/L 1.0 0.13 1 09/15/12 05:52 10061-01-5 ND ug/L 1.0 0.26 1 09/15/12 05:52 10061-02-6 ND ug/L 1.0 0.12 1 09/15/12 05:52 108-20-3 ND ug/L 1.0 0.30 1 09/15/12 05:52 100-41-4 ND ug/L 1.0 0.71 1 09/15/12 05:52 87-68-3 ND ug/L 5.0 0.46 1 09/15/12 05:52 591-78-6 ND ug/L 1.0 0.31 1 09/15/12 05:52 99-87-6 ND ug/L 2.0 0.97 1 09/15/12 05:52 75-09-2 ND ug/L 5.0 0.33 1 09/15/12 05:52 108-10-1 ND ug/L 1.0 0.21 1 09/15/12 05:52 1634-04-4 ND ug/L 1.0 0.24 1 09/15/12 05:52 91-20-3 ND ug/L 1.0 0.26 1 09/15/12 05:52 100-42-5 ND ug/L 1.0 0.33 1 09/15/12 05:52 630-20-6 ND ug/L 1.0 0.40 1 09/15/12 05:52 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 39 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-24 LabID: 92131396018 Collected: 09/11/12 11:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 476 ug/L 5.0 2.3 5 09/17/12 15:18 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 05:52 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 05:52 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 05:52 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 05:52 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 05:52 79-00-5 Trichloroethene 3.0 ug/L 1.0 0.47 1 09/15/12 05:52 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 05:52 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 05:52 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 05:52 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 05:52 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 05:52 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 05:52 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/15/12 05:52 460-00-4 Dibromofluoromethane (S) 103 % 70-130 1 09/15/12 05:52 1868-53-7 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 09/15/12 05:52 17060-07-0 Tbluene-d8 (S) 94 % 70-130 1 09/15/12 05:52 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 40 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: MW-26 LabID: 92131396019 Collected: 09/10/12 13:50 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 06:08 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 06:08 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 06:08 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 06:08 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 06:08 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 06:08 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 06:08 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 06:08 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 06:08 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 06:08 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 06:08 75-00-3 Chloroform 2.3 ug/L 1.0 0.14 1 09/15/12 06:08 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 06:08 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 06:08 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 06:08 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 06:08 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 06:08 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 06:08 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 06:08 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 06:08 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 06:08 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:08 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 06:08 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 06:08 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 06:08 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 06:08 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 06:08 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 06:08 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 06:08 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 06:08 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 06:08 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 06:08 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 06:08 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 06:08 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 06:08 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 06:08 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 06:08 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 06:08 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 06:08 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 06:08 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 06:08 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 06:08 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 06:08 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 06:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 06:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 06:08 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 41 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-26 LabID: 92131396019 Collected: 09/10/12 13:50 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.51J ug/L 1.0 0.46 1 09/15/12 06:08 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 06:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 06:08 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 06:08 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 06:08 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 06:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 06:08 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 06:08 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 06:08 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 06:08 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 06:08 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 06:08 95-47-6 Surrogates 4-Bromofluorobenzene (S) 93 % 70-130 1 09/15/12 06:08 460-00-4 Dibromofluoromethane (S) 109 % 70-130 1 09/15/12 06:08 1868-53-7 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 09/15/12 06:08 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/15/12 06:08 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 42 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: RW-1 LabID: 92131396020 Collected: 09/12/12 13:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 180J ug/L 250 100 10 09/25/12 18:08 67-64-1 Benzene ND ug/L 10.0 2.5 10 09/25/12 18:08 71-43-2 Bromobenzene ND ug/L 10.0 3.0 10 09/25/12 18:08 108-86-1 Bromochloromethane ND ug/L 10.0 1.7 10 09/25/12 18:08 74-97-5 Bromodichloromethane ND ug/L 10.0 1.8 10 09/25/12 18:08 75-27-4 Bromoform ND ug/L 10.0 2.6 10 09/25/12 18:08 75-25-2 Bromomethane ND ug/L 20.0 2.9 10 09/25/12 18:08 74-83-9 2-Butanone (MEK) 216 ug/L 50.0 9.6 10 09/25/12 18:08 78-93-3 Carbon tetrachloride ND ug/L 10.0 2.5 10 09/25/12 18:08 56-23-5 Chlorobenzene ND ug/L 10.0 2.3 10 09/25/12 18:08 108-90-7 Chloroethane ND ug/L 10.0 5.4 10 09/25/12 18:08 75-00-3 Chloroform ND ug/L 10.0 1.4 10 09/25/12 18:08 67-66-3 Chloromethane ND ug/L 10.0 1.1 10 09/25/12 18:08 74-87-3 2-Chlorotoluene ND ug/L 10.0 3.5 10 09/25/12 18:08 95-49-8 4-Chlorotoluene ND ug/L 10.0 3.1 10 09/25/12 18:08 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 50.0 25.2 10 09/25/12 18:08 96-12-8 Dibromochloromethane ND ug/L 10.0 2.1 10 09/25/12 18:08 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 10.0 2.7 10 09/25/12 18:08 106-93-4 Dibromomethane ND ug/L 10.0 2.1 10 09/25/12 18:08 74-95-3 1,2-Dichlorobenzene ND ug/L 10.0 3.0 10 09/25/12 18:08 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 2.4 10 09/25/12 18:08 541-73-1 1,4-Dichlorobenzene ND ug/L 10.0 3.3 10 09/25/12 18:08 106-46-7 Dichlorodifluoromethane ND ug/L 10.0 2.1 10 09/25/12 18:08 75-71-8 1,1-Dichloroethane ND ug/L 10.0 3.2 10 09/25/12 18:08 75-34-3 1,2-Dichloroethane ND ug/L 10.0 1.2 10 09/25/12 18:08 107-06-2 M-Dichloroethene 9.3J ug/L 10.0 5.6 10 09/25/12 18:08 75-35-4 cis-1,2-Dichloroethene 15200 ug/L 100 19.0 100 09/15/12 10:20 156-59-2 trans- 1,2-Dichloroethene 49.0 ug/L 10.0 4.9 10 09/25/12 18:08 156-60-5 1,2-Dichloropropane ND ug/L 10.0 2.7 10 09/25/12 18:08 78-87-5 1,3-Dichloropropane ND ug/L 10.0 2.8 10 09/25/12 18:08 142-28-9 2,2-Dichloropropane ND ug/L 10.0 1.3 10 09/25/12 18:08 594-20-7 1,1-Dichloropropene ND ug/L 10.0 4.9 10 09/25/12 18:08 563-58-6 cis-1,3-Dichloropropene ND ug/L 10.0 1.3 10 09/25/12 18:08 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 10.0 2.6 10 09/25/12 18:08 10061-02-6 Diisopropyl ether ND ug/L 10.0 1.2 10 09/25/12 18:08 108-20-3 Ethylbenzene ND ug/L 10.0 3.0 10 09/25/12 18:08 100-41-4 Hexachloro-1,3-butadiene ND ug/L 10.0 7.1 10 09/25/12 18:08 87-68-3 2-Hexanone ND ug/L 50.0 4.6 10 09/25/12 18:08 591-78-6 p-Isopropyltoluene ND ug/L 10.0 3.1 10 09/25/12 18:08 99-87-6 Methylene Chloride ND ug/L 20.0 9.7 10 09/25/12 18:08 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 50.0 3.3 10 09/25/12 18:08 108-10-1 Methyl-tert-butyl ether ND ug/L 10.0 2.1 10 09/25/12 18:08 1634-04-4 Naphthalene ND ug/L 10.0 2.4 10 09/25/12 18:08 91-20-3 Styrene ND ug/L 10.0 2.6 10 09/25/12 18:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 10.0 3.3 10 09/25/12 18:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 10.0 4.0 10 09/25/12 18:08 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 43 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-1 LabID: 92131396020 Collected: 09/12/12 13:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1110 ug/L 10.0 4.6 10 09/25/12 18:08 127-18-4 Toluene 3.2J ug/L 10.0 2.6 10 09/25/12 18:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 10.0 3.3 10 09/25/12 18:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 10.0 3.5 10 09/25/12 18:08 120-82-1 1,1,1-Trichloroethane ND ug/L 10.0 4.8 10 09/25/12 18:08 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 2.9 10 09/25/12 18:08 79-00-5 Trichloroethene 623 ug/L 10.0 4.7 10 09/25/12 18:08 79-01-6 Trichlorofluoromethane ND ug/L 10.0 2.0 10 09/25/12 18:08 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.1 10 09/25/12 18:08 96-18-4 Vinyl acetate ND ug/L 20.0 3.5 10 09/25/12 18:08 108-05-4 Vinyl chloride 99.9 ug/L 10.0 6.2 10 09/25/12 18:08 75-01-4 m&p-Xylene ND ug/L 20.0 6.6 10 09/25/12 18:08 179601-23-1 o-Xylene ND ug/L 10.0 2.3 10 09/25/12 18:08 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 10 09/25/12 18:08 460-00-4 Dibromofluoromethane (S) 109 % 70-130 10 09/25/12 18:08 1868-53-7 1,2-Dichloroethane-d4 (S) 106 % 70-130 10 09/25/12 18:08 17060-07-0 Tbluene-d8 (S) 101 % 70-130 10 09/25/12 18:08 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 44 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: IRW-3 LabID: 92131396021 Collected: 09/12/12 14:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 123 ug/L 25.0 10.0 1 09/25/12 17:05 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/25/12 17:05 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/25/12 17:05 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/25/12 17:05 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/25/12 17:05 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/25/12 17:05 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/25/12 17:05 74-83-9 2-Butanone (MEK) 17.4 ug/L 5.0 0.96 1 09/25/12 17:05 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/25/12 17:05 56-23-5 Chlorobenzene 0.27J ug/L 1.0 0.23 1 09/25/12 17:05 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/25/12 17:05 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/25/12 17:05 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/25/12 17:05 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/25/12 17:05 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/25/12 17:05 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/25/12 17:05 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/25/12 17:05 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/25/12 17:05 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/25/12 17:05 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/25/12 17:05 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/25/12 17:05 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 17:05 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/25/12 17:05 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/25/12 17:05 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/25/12 17:05 107-06-2 M-Dichloroethene 0.87J ug/L 1.0 0.56 1 09/25/12 17:05 75-35-4 cis-1,2-Dichloroethene 1440 ug/L 10.0 1.9 10 09/15/12 10:35 156-59-2 trans- 1,2-Dichloroethene 4.1 ug/L 1.0 0.49 1 09/25/12 17:05 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/25/12 17:05 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/25/12 17:05 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/25/12 17:05 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/25/12 17:05 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/25/12 17:05 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/25/12 17:05 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/25/12 17:05 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/25/12 17:05 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/25/12 17:05 87-68-3 2-Hexanone 0.79J ug/L 5.0 0.46 1 09/25/12 17:05 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/25/12 17:05 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/25/12 17:05 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/25/12 17:05 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/25/12 17:05 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/25/12 17:05 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/25/12 17:05 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/25/12 17:05 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/25/12 17:05 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 45 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: IRW-3 LabID: 92131396021 Collected: 09/12/12 14:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2.5 ug/L 1.0 0.46 1 09/25/12 17:05 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/25/12 17:05 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 17:05 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/25/12 17:05 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/25/12 17:05 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/25/12 17:05 79-00-5 Trichloroethene 1.4 ug/L 1.0 0.47 1 09/25/12 17:05 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/25/12 17:05 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/25/12 17:05 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/25/12 17:05 108-05-4 Vinyl chloride 11.9 ug/L 1.0 0.62 1 09/25/12 17:05 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/25/12 17:05 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/25/12 17:05 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/25/12 17:05 460-00-4 Dibromofluoromethane (S) 110 % 70-130 1 09/25/12 17:05 1868-53-7 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 09/25/12 17:05 17060-07-0 Tbluene-d8 (S) 102 % 70-130 1 09/25/12 17:05 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 46 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: IRW-5 LabID: 92131396022 Collected: 09/12/12 14:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 132J ug/L 250 100 10 09/25/12 18:39 67-64-1 Benzene ND ug/L 10.0 2.5 10 09/25/12 18:39 71-43-2 Bromobenzene ND ug/L 10.0 3.0 10 09/25/12 18:39 108-86-1 Bromochloromethane ND ug/L 10.0 1.7 10 09/25/12 18:39 74-97-5 Bromodichloromethane ND ug/L 10.0 1.8 10 09/25/12 18:39 75-27-4 Bromoform ND ug/L 10.0 2.6 10 09/25/12 18:39 75-25-2 Bromomethane ND ug/L 20.0 2.9 10 09/25/12 18:39 74-83-9 2-Butanone (MEK) 65.1 ug/L 50.0 9.6 10 09/25/12 18:39 78-93-3 Carbon tetrachloride ND ug/L 10.0 2.5 10 09/25/12 18:39 56-23-5 Chlorobenzene ND ug/L 10.0 2.3 10 09/25/12 18:39 108-90-7 Chloroethane ND ug/L 10.0 5.4 10 09/25/12 18:39 75-00-3 Chloroform ND ug/L 10.0 1.4 10 09/25/12 18:39 67-66-3 Chloromethane ND ug/L 10.0 1.1 10 09/25/12 18:39 74-87-3 2-Chlorotoluene ND ug/L 10.0 3.5 10 09/25/12 18:39 95-49-8 4-Chlorotoluene ND ug/L 10.0 3.1 10 09/25/12 18:39 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 50.0 25.2 10 09/25/12 18:39 96-12-8 Dibromochloromethane ND ug/L 10.0 2.1 10 09/25/12 18:39 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 10.0 2.7 10 09/25/12 18:39 106-93-4 Dibromomethane ND ug/L 10.0 2.1 10 09/25/12 18:39 74-95-3 1,2-Dichlorobenzene ND ug/L 10.0 3.0 10 09/25/12 18:39 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 2.4 10 09/25/12 18:39 541-73-1 1,4-Dichlorobenzene ND ug/L 10.0 3.3 10 09/25/12 18:39 106-46-7 Dichlorodifluoromethane ND ug/L 10.0 2.1 10 09/25/12 18:39 75-71-8 1,1-Dichloroethane ND ug/L 10.0 3.2 10 09/25/12 18:39 75-34-3 1,2-Dichloroethane ND ug/L 10.0 1.2 10 09/25/12 18:39 107-06-2 M-Dichloroethene ND ug/L 10.0 5.6 10 09/25/12 18:39 75-35-4 cis-1,2-Dichloroethene 58.2 ug/L 10.0 1.9 10 09/25/12 18:39 156-59-2 trans- 1,2-Dichloroethene ND ug/L 10.0 4.9 10 09/25/12 18:39 156-60-5 1,2-Dichloropropane ND ug/L 10.0 2.7 10 09/25/12 18:39 78-87-5 1,3-Dichloropropane ND ug/L 10.0 2.8 10 09/25/12 18:39 142-28-9 2,2-Dichloropropane ND ug/L 10.0 1.3 10 09/25/12 18:39 594-20-7 1,1-Dichloropropene ND ug/L 10.0 4.9 10 09/25/12 18:39 563-58-6 cis-1,3-Dichloropropene ND ug/L 10.0 1.3 10 09/25/12 18:39 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 10.0 2.6 10 09/25/12 18:39 10061-02-6 Diisopropyl ether ND ug/L 10.0 1.2 10 09/25/12 18:39 108-20-3 Ethylbenzene ND ug/L 10.0 3.0 10 09/25/12 18:39 100-41-4 Hexachloro-1,3-butadiene ND ug/L 10.0 7.1 10 09/25/12 18:39 87-68-3 2-Hexanone ND ug/L 50.0 4.6 10 09/25/12 18:39 591-78-6 p-Isopropyltoluene ND ug/L 10.0 3.1 10 09/25/12 18:39 99-87-6 Methylene Chloride ND ug/L 20.0 9.7 10 09/25/12 18:39 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 50.0 3.3 10 09/25/12 18:39 108-10-1 Methyl-tert-butyl ether ND ug/L 10.0 2.1 10 09/25/12 18:39 1634-04-4 Naphthalene ND ug/L 10.0 2.4 10 09/25/12 18:39 91-20-3 Styrene ND ug/L 10.0 2.6 10 09/25/12 18:39 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 10.0 3.3 10 09/25/12 18:39 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 10.0 4.0 10 09/25/12 18:39 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 47 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: IRW-5 LabID: 92131396022 Collected: 09/12/12 14:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 10.0 4.6 10 09/25/12 18:39 127-18-4 Toluene 11200 ug/L 100 26.0 100 09/15/12 10:51 108-88-3 1,2,3-Trichlorobenzene ND ug/L 10.0 3.3 10 09/25/12 18:39 87-61-6 1,2,4-Trichlorobenzene ND ug/L 10.0 3.5 10 09/25/12 18:39 120-82-1 1,1,1-Trichloroethane ND ug/L 10.0 4.8 10 09/25/12 18:39 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 2.9 10 09/25/12 18:39 79-00-5 Trichloroethene ND ug/L 10.0 4.7 10 09/25/12 18:39 79-01-6 Trichlorofluoromethane ND ug/L 10.0 2.0 10 09/25/12 18:39 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.1 10 09/25/12 18:39 96-18-4 Vinyl acetate ND ug/L 20.0 3.5 10 09/25/12 18:39 108-05-4 Vinyl chloride ND ug/L 10.0 6.2 10 09/25/12 18:39 75-01-4 m&p-Xylene ND ug/L 20.0 6.6 10 09/25/12 18:39 179601-23-1 o-Xylene ND ug/L 10.0 2.3 10 09/25/12 18:39 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 10 09/25/12 18:39 460-00-4 Dibromofluoromethane (S) 103 % 70-130 10 09/25/12 18:39 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 10 09/25/12 18:39 17060-07-0 Tbluene-d8 (S) 98 % 70-130 10 09/25/12 18:39 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 48 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: IRW-6 LabID: 92131396023 Collected: 09/12/12 13:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 10.0 1 09/25/12 17:37 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/25/12 17:37 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/25/12 17:37 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/25/12 17:37 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/25/12 17:37 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/25/12 17:37 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/25/12 17:37 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/25/12 17:37 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/25/12 17:37 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/25/12 17:37 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/25/12 17:37 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/25/12 17:37 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/25/12 17:37 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/25/12 17:37 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/25/12 17:37 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/25/12 17:37 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/25/12 17:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/25/12 17:37 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/25/12 17:37 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/25/12 17:37 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/25/12 17:37 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 17:37 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/25/12 17:37 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/25/12 17:37 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/25/12 17:37 107-06-2 M-Dichloroethene 1.4 ug/L 1.0 0.56 1 09/25/12 17:37 75-35-4 cis-1,2-Dichloroethene 308 ug/L 2.5 0.48 2.5 09/15/12 11:07 156-59-2 trans- 1,2-Dichloroethene 2.6 ug/L 1.0 0.49 1 09/25/12 17:37 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/25/12 17:37 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/25/12 17:37 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/25/12 17:37 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/25/12 17:37 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/25/12 17:37 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/25/12 17:37 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/25/12 17:37 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/25/12 17:37 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/25/12 17:37 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/25/12 17:37 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/25/12 17:37 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/25/12 17:37 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/25/12 17:37 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/25/12 17:37 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/25/12 17:37 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/25/12 17:37 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/25/12 17:37 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/25/12 17:37 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 49 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: IRW-6 LabID: 92131396023 Collected: 09/12/12 13:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 168 ug/L 1.0 0.46 1 09/25/12 17:37 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/25/12 17:37 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/25/12 17:37 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/25/12 17:37 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/25/12 17:37 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/25/12 17:37 79-00-5 Trichloroethene 45.1 ug/L 1.0 0.47 1 09/25/12 17:37 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/25/12 17:37 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/25/12 17:37 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/25/12 17:37 108-05-4 Vinyl chloride 73.2 ug/L 1.0 0.62 1 09/25/12 17:37 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/25/12 17:37 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/25/12 17:37 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/25/12 17:37 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 09/25/12 17:37 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 09/25/12 17:37 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/25/12 17:37 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 50 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: IRW-7 LabID: 92131396024 Collected: 09/12/12 13:20 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 2160 ug/L 250 21.7 10 09/17/12 14:31 67-64-1 Benzene ND ug/L 2.0 0.50 2 09/15/12 11:23 71-43-2 Bromobenzene ND ug/L 2.0 0.60 2 09/15/12 11:23 108-86-1 Bromochloromethane ND ug/L 2.0 0.34 2 09/15/12 11:23 74-97-5 Bromodichloromethane ND ug/L 2.0 0.36 2 09/15/12 11:23 75-27-4 Bromoform ND ug/L 2.0 0.52 2 09/15/12 11:23 75-25-2 Bromomethane ND ug/L 4.0 0.58 2 09/15/12 11:23 74-83-9 2-Butanone (MEK) 259 ug/L 10.0 1.9 2 09/15/12 11:23 78-93-3 Carbon tetrachloride ND ug/L 2.0 0.50 2 09/15/12 11:23 56-23-5 Chlorobenzene ND ug/L 2.0 0.46 2 09/15/12 11:23 108-90-7 Chloroethane ND ug/L 2.0 1.1 2 09/15/12 11:23 75-00-3 Chloroform 1.2J ug/L 2.0 0.28 2 09/15/12 11:23 67-66-3 Chloromethane ND ug/L 2.0 0.22 2 09/15/12 11:23 74-87-3 2-Chlorotoluene ND ug/L 2.0 0.70 2 09/15/12 11:23 95-49-8 4-Chlorotoluene ND ug/L 2.0 0.62 2 09/15/12 11:23 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 10.0 5.0 2 09/15/12 11:23 96-12-8 Dibromochloromethane ND ug/L 2.0 0.42 2 09/15/12 11:23 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 2.0 0.54 2 09/15/12 11:23 106-93-4 Dibromomethane ND ug/L 2.0 0.42 2 09/15/12 11:23 74-95-3 1,2-Dichlorobenzene ND ug/L 2.0 0.60 2 09/15/12 11:23 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 0.48 2 09/15/12 11:23 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 0.66 2 09/15/12 11:23 106-46-7 Dichlorodifluoromethane ND ug/L 2.0 0.42 2 09/15/12 11:23 75-71-8 1,1-Dichloroethane ND ug/L 2.0 0.64 2 09/15/12 11:23 75-34-3 1,2-Dichloroethane ND ug/L 2.0 0.24 2 09/15/12 11:23 107-06-2 M-Dichloroethene ND ug/L 2.0 1.1 2 09/15/12 11:23 75-35-4 cis-1,2-Dichloroethene 612 ug/L 10.0 1.9 10 09/17/12 14:31 156-59-2 trans- 1,2-Dichloroethene ND ug/L 2.0 0.98 2 09/15/12 11:23 156-60-5 1,2-Dichloropropane ND ug/L 2.0 0.54 2 09/15/12 11:23 78-87-5 1,3-Dichloropropane ND ug/L 2.0 0.56 2 09/15/12 11:23 142-28-9 2,2-Dichloropropane ND ug/L 2.0 0.26 2 09/15/12 11:23 594-20-7 1,1-Dichloropropene ND ug/L 2.0 0.98 2 09/15/12 11:23 563-58-6 cis-1,3-Dichloropropene ND ug/L 2.0 0.26 2 09/15/12 11:23 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 2.0 0.52 2 09/15/12 11:23 10061-02-6 Diisopropyl ether ND ug/L 2.0 0.24 2 09/15/12 11:23 108-20-3 Ethylbenzene ND ug/L 2.0 0.60 2 09/15/12 11:23 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1.4 2 09/15/12 11:23 87-68-3 2-Hexanone ND ug/L 10.0 0.92 2 09/15/12 11:23 591-78-6 p-Isopropyltoluene ND ug/L 2.0 0.62 2 09/15/12 11:23 99-87-6 Methylene Chloride 2.OJ ug/L 4.0 1.9 2 09/15/12 11:23 75-09-2 4-Methyl-2-pentanone (MIBK) 5.OJ ug/L 10.0 0.66 2 09/15/12 11:23 108-10-1 Methyl-tert-butyl ether 1.3J ug/L 2.0 0.42 2 09/15/12 11:23 1634-04-4 Naphthalene ND ug/L 2.0 0.48 2 09/15/12 11:23 91-20-3 Styrene ND ug/L 2.0 0.52 2 09/15/12 11:23 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 2.0 0.66 2 09/15/12 11:23 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 2.0 0.80 2 09/15/12 11:23 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 51 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: IRW-7 LabID: 92131396024 Collected: 09/12/12 13:20 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 41.1 ug/L 2.0 0.92 2 09/15/12 11:23 127-18-4 Toluene 1.7J ug/L 2.0 0.52 2 09/15/12 11:23 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.66 2 09/15/12 11:23 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.70 2 09/15/12 11:23 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.96 2 09/15/12 11:23 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.58 2 09/15/12 11:23 79-00-5 Trichloroethene 8.0 ug/L 2.0 0.94 2 09/15/12 11:23 79-01-6 Trichlorofluoromethane ND ug/L 2.0 0.40 2 09/15/12 11:23 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.82 2 09/15/12 11:23 96-18-4 Vinyl acetate ND ug/L 4.0 0.70 2 09/15/12 11:23 108-05-4 Vinyl chloride 12.6 ug/L 2.0 1.2 2 09/15/12 11:23 75-01-4 m&p-Xylene ND ug/L 4.0 1.3 2 09/15/12 11:23 179601-23-1 o-Xylene ND ug/L 2.0 0.46 2 09/15/12 11:23 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 2 09/15/12 11:23 460-00-4 Dibromofluoromethane (S) 106 % 70-130 2 09/15/12 11:23 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 2 09/15/12 11:23 17060-07-0 Tbluene-d8 (S) 104 % 70-130 2 09/15/12 11:23 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 52 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Sample: TRIP BLANK LabID: 92131396025 Collected: 09/12/12 00:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Analytical Method: EPA 8260 Acetone 6.5J ug/L 25.0 2.2 1 09/15/12 02:44 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 02:44 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 02:44 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 02:44 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 02:44 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 02:44 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 02:44 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 02:44 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 02:44 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 02:44 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 02:44 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 02:44 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 02:44 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 02:44 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 02:44 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 02:44 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 02:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 02:44 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 02:44 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 02:44 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 02:44 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 02:44 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 02:44 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 02:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 02:44 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 02:44 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 02:44 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 02:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 02:44 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 02:44 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 02:44 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 02:44 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 02:44 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 02:44 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 02:44 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 02:44 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 02:44 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 02:44 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 02:44 99-87-6 Methylene Chloride 1.9J ug/L 2.0 0.97 1 09/15/12 02:44 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 02:44 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 02:44 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 02:44 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 02:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 02:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 02:44 79-34-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 53 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK LabID: 92131396025 Collected: 09/12/12 00:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/15/12 02:44 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 02:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 02:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 02:44 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 02:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 02:44 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 02:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 02:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 02:44 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 02:44 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 02:44 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 02:44 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 02:44 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 02:44 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/15/12 02:44 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/15/12 02:44 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/15/12 02:44 2037-26-5 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 54 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 QC Batch: MSV/20383 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92131396002,92131396003,92131396008,92131396010 METHOD BLANK: 833655 Matrix: Water Associated Lab Samples: 92131396002,92131396003,92131396008,92131396010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/14/12 13:56 1,1,1-Trichloroethane ug/L ND 1.0 09/14/12 13:56 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/14/12 13:56 1,1,2-Trichloroethane ug/L ND 1.0 09/14/12 13:56 1,1-Dichloroethane ug/L ND 1.0 09/14/12 13:56 1,1-Dichloroethene ug/L ND 1.0 09/14/12 13:56 1,1-Dichloropropene ug/L ND 1.0 09/14/12 13:56 1,2,3-Trichlorobenzene ug/L ND 1.0 09/14/12 13:56 1,2,3-Trichloropropane ug/L ND 1.0 09/14/12 13:56 1,2,4-Trichlorobenzene ug/L ND 1.0 09/14/12 13:56 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/14/12 13:56 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/14/12 13:56 1,2-Dichlorobenzene ug/L ND 1.0 09/14/12 13:56 1,2-Dichloroethane ug/L ND 1.0 09/14/12 13:56 1,2-Dichloropropane ug/L ND 1.0 09/14/12 13:56 1,3-Dichlorobenzene ug/L ND 1.0 09/14/12 13:56 1,3-Dichloropropane ug/L ND 1.0 09/14/12 13:56 1,4-Dichlorobenzene ug/L ND 1.0 09/14/12 13:56 2,2-Dichloropropane ug/L ND 1.0 09/14/12 13:56 2-Butanone (MEK) ug/L ND 5.0 09/14/12 13:56 2-Chlorotoluene ug/L ND 1.0 09/14/12 13:56 2-Hexanone ug/L ND 5.0 09/14/12 13:56 4-Chlorotoluene ug/L ND 1.0 09/14/12 13:56 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/14/12 13:56 Acetone ug/L ND 25.0 09/14/12 13:56 Benzene ug/L ND 1.0 09/14/12 13:56 Bromobenzene ug/L ND 1.0 09/14/12 13:56 Bromochloromethane ug/L ND 1.0 09/14/12 13:56 Bromodichloromethane ug/L ND 1.0 09/14/12 13:56 Bromoform ug/L ND 1.0 09/14/12 13:56 Bromomethane ug/L ND 2.0 09/14/12 13:56 Carbon tetrachloride ug/L ND 1.0 09/14/12 13:56 Chlorobenzene ug/L ND 1.0 09/14/12 13:56 Chloroethane ug/L ND 1.0 09/14/12 13:56 Chloroform ug/L ND 1.0 09/14/12 13:56 Chloromethane ug/L ND 1.0 09/14/12 13:56 cis-1,2-Dichloroethene ug/L ND 1.0 09/14/12 13:56 cis-1,3-Dichloropropene ug/L ND 1.0 09/14/12 13:56 Dibromochloromethane ug/L ND 1.0 09/14/12 13:56 Dibromomethane ug/L ND 1.0 09/14/12 13:56 Dichlorodifluoromethane ug/L ND 1.0 09/14/12 13:56 Diisopropyl ether ug/L ND 1.0 09/14/12 13:56 Ethylbenzene ug/L ND 1.0 09/14/12 13:56 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 55 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 METHOD BLANK: 833655 Matrix: Water Associated Lab Samples: 92131396002,92131396003,92131396008,92131396010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0 09/14/12 13:56 m&p-Xylene ug/L ND 2.0 09/14/12 13:56 Methyl-tert-butyl ether ug/L ND 1.0 09/14/12 13:56 Methylene Chloride ug/L ND 2.0 09/14/12 13:56 Naphthalene ug/L ND 1.0 09/14/12 13:56 o-Xylene ug/L ND 1.0 09/14/12 13:56 p-Isopropyltoluene ug/L ND 1.0 09/14/12 13:56 Styrene ug/L ND 1.0 09/14/12 13:56 Tetrachloroethene ug/L ND 1.0 09/14/12 13:56 Toluene ug/L ND 1.0 09/14/12 13:56 trans- 1,2-Dichloroethene ug/L ND 1.0 09/14/12 13:56 trans- 1, 3-Dichloropropene ug/L ND 1.0 09/14/12 13:56 Trichloroethene ug/L ND 1.0 09/14/12 13:56 Trichlorofluoromethane ug/L ND 1.0 09/14/12 13:56 Vinyl acetate ug/L ND 2.0 09/14/12 13:56 Vinyl chloride ug/L ND 1.0 09/14/12 13:56 1,2-Dichloroethane-d4 (S) % 101 70-130 09/14/12 13:56 4-Bromofluorobenzene (S) % 97 70-130 09/14/12 13:56 Dibromofluoromethane (S) % 106 70-130 09/14/12 13:56 Tbluene-d8 (S) % 101 70-130 09/14/12 13:56 LABORATORY CONTROL SAMPLE: 833656 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 46.3 93 70-130 1,1,1-Trichloroethane ug/L 50 45.6 91 70-130 1,1,2,2-Tetrachloroethane ug/L 50 45.4 91 70-130 1,1,2-Trichloroethane ug/L 50 47.0 94 70-130 1,1-Dichloroethane ug/L 50 45.2 90 70-130 1,1-Dichloroethene ug/L 50 48.0 96 70-132 1,1-Dichloropropene ug/L 50 42.5 85 70-130 1,2,3-Trichlorobenzene ug/L 50 47.2 94 70-135 1,2,3-Trichloropropane ug/L 50 46.1 92 70-130 1,2,4-Trichlorobenzene ug/L 50 47.7 95 70-134 1,2-Dibromo-3-chloropropane ug/L 50 50.1 100 70-130 1,2-Dibromoethane (EDB) ug/L 50 49.8 100 70-130 1,2-Dichlorobenzene ug/L 50 47.7 95 70-130 1,2-Dichloroethane ug/L 50 43.4 87 70-130 1,2-Dichloropropane ug/L 50 44.2 88 70-130 1,3-Dichlorobenzene ug/L 50 46.2 92 70-130 1,3-Dichloropropane ug/L 50 46.9 94 70-130 1,4-Dichlorobenzene ug/L 50 46.8 94 70-130 2,2-Dichloropropane ug/L 50 45.6 91 58-145 2-Butanone (MEK) ug/L 100 91.1 91 70-145 2-Chlorotoluene ug/L 50 44.1 88 70-130 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 56 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 LABORATORY CONTROL SAMPLE: Parameter 833656 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2-Hexanone ug/L 100 103 103 70-144 4-Chlorotoluene ug/L 50 48.8 98 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 99.6 100 70-140 Acetone ug/L 100 96.1 96 50-175 Benzene ug/L 50 45.0 90 70-130 Bromobenzene ug/L 50 49.2 98 70-130 Bromochloromethane ug/L 50 44.1 88 70-130 Bromodichloromethane ug/L 50 45.4 91 70-130 Bromoform ug/L 50 48.3 97 70-130 Bromomethane ug/L 50 39.3 79 54-130 Carbon tetrachloride ug/L 50 42.6 85 70-132 Chlorobenzene ug/L 50 46.6 93 70-130 Chloroethane ug/L 50 55.3 ill 64-134 Chloroform ug/L 50 45.0 90 70-130 Chloromethane ug/L 50 44.2 88 64-130 cis-1,2-Dichloroethene ug/L 50 42.8 86 70-131 cis-1,3-Dichloropropene ug/L 50 45.6 91 70-130 Dibromochloromethane ug/L 50 49.4 99 70-130 Dibromomethane ug/L 50 44.1 88 70-131 Dichlorodifluoromethane ug/L 50 41.9 84 56-130 Diisopropyl ether ug/L 50 44.8 90 70-130 Ethylbenzene ug/L 50 45.6 91 70-130 Hexachloro-1,3-butadiene ug/L 50 43.6 87 70-130 m&p-Xylene ug/L 100 94.3 94 70-130 Methyl-tert-butyl ether ug/L 50 45.7 91 70-130 Methylene Chloride ug/L 50 46.9 94 63-130 Naphthalene ug/L 50 48.9 98 70-138 o-Xylene ug/L 50 45.9 92 70-130 p-Isopropyltoluene ug/L 50 47.0 94 70-130 Styrene ug/L 50 47.2 94 70-130 Tetrachloroethene ug/L 50 47.2 94 70-130 Toluene ug/L 50 44.4 89 70-130 trans- 1,2-Dichloroethene ug/L 50 42.2 84 70-130 trans- 1, 3-Dichloropropene ug/L 50 48.3 97 70-132 Trichloroethene ug/L 50 46.7 93 70-130 Trichlorofluoromethane ug/L 50 43.9 88 62-133 Vinyl acetate ug/L 100 108 108 66-157 Vinyl chloride ug/L 50 42.8 86 69-130 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 98 70-130 Dibromofluoromethane (S) % 96 70-130 Tbluene-d8 (S) % 97 70-130 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 57 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 833657 833658 IVIS MSD 92131396003 Spike Spike IVIS MSD IVIS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual M-Dichloroethene ug/L ND 50 50 51.3 47.0 103 94 70-166 9 30 Benzene ug/L ND 50 50 46.0 47.2 92 94 70-148 3 30 Chlorobenzene ug/L ND 50 50 53.8 56.8 108 114 70-146 5 30 Toluene ug/L ND 50 50 53.2 55.8 106 112 70-155 5 30 Trichloroethene ug/L ND 50 50 57.8 58.1 115 116 69-151 1 30 1,2-Dichloroethane-d4 (S) % 97 100 70-130 4-Bromofluorobenzene (S) % 95 95 70-130 Dibromofluoromethane (S) % 98 102 70-130 Tbluene-d8 (S) % 94 96 70-130 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 58 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 QC Batch: MSV/20385 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92131396012,92131396013,92131396014,92131396015,92131396016,92131396017,92131396018, 92131396019,92131396024,92131396025 METHOD BLANK: 833666 Matrix: Water Associated Lab Samples: 92131396012,92131396013,92131396014,92131396015,92131396016,92131396017,92131396018, 92131396019,92131396024,92131396025 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/15/12 01:10 1,1,1-Trichloroethane ug/L ND 1.0 09/15/12 01:10 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/15/12 01:10 1,1,2-Trichloroethane ug/L ND 1.0 09/15/12 01:10 1,1-Dichloroethane ug/L ND 1.0 09/15/12 01:10 1,1-Dichloroethene ug/L ND 1.0 09/15/12 01:10 1,1-Dichloropropene ug/L ND 1.0 09/15/12 01:10 1,2,3-Trichlorobenzene ug/L ND 1.0 09/15/12 01:10 1,2,3-Trichloropropane ug/L ND 1.0 09/15/12 01:10 1,2,4-Trichlorobenzene ug/L ND 1.0 09/15/12 01:10 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/15/12 01:10 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/15/12 01:10 1,2-Dichlorobenzene ug/L ND 1.0 09/15/12 01:10 1,2-Dichloroethane ug/L ND 1.0 09/15/12 01:10 1,2-Dichloropropane ug/L ND 1.0 09/15/12 01:10 1,3-Dichlorobenzene ug/L ND 1.0 09/15/12 01:10 1,3-Dichloropropane ug/L ND 1.0 09/15/12 01:10 1,4-Dichlorobenzene ug/L ND 1.0 09/15/12 01:10 2,2-Dichloropropane ug/L ND 1.0 09/15/12 01:10 2-Butanone (MEK) ug/L ND 5.0 09/15/12 01:10 2-Chlorotoluene ug/L ND 1.0 09/15/12 01:10 2-Hexanone ug/L ND 5.0 09/15/12 01:10 4-Chlorotoluene ug/L ND 1.0 09/15/12 01:10 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/15/12 01:10 Acetone ug/L ND 25.0 09/15/12 01:10 Benzene ug/L ND 1.0 09/15/12 01:10 Bromobenzene ug/L ND 1.0 09/15/12 01:10 Bromochloromethane ug/L ND 1.0 09/15/12 01:10 Bromodichloromethane ug/L ND 1.0 09/15/12 01:10 Bromoform ug/L ND 1.0 09/15/12 01:10 Bromomethane ug/L ND 2.0 09/15/12 01:10 Carbon tetrachloride ug/L ND 1.0 09/15/12 01:10 Chlorobenzene ug/L ND 1.0 09/15/12 01:10 Chloroethane ug/L ND 1.0 09/15/12 01:10 Chloroform ug/L ND 1.0 09/15/12 01:10 Chloromethane ug/L ND 1.0 09/15/12 01:10 cis-1,2-Dichloroethene ug/L ND 1.0 09/15/12 01:10 cis-1,3-Dichloropropene ug/L ND 1.0 09/15/12 01:10 Dibromochloromethane ug/L ND 1.0 09/15/12 01:10 Dibromomethane ug/L ND 1.0 09/15/12 01:10 Dichlorodifluoromethane ug/L ND 1.0 09/15/12 01:10 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 59 of 67 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 METHOD BLANK: 833666 Matrix: Water Associated Lab Samples: 92131396012,92131396013,92131396014,92131396015,92131396016,92131396017,92131396018, 92131396019,92131396024,92131396025 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diisopropyl ether ug/L ND 1.0 09/15/12 01:10 Ethylbenzene ug/L ND 1.0 09/15/12 01:10 Hexachloro-1,3-butadiene ug/L ND 1.0 09/15/12 01:10 m&p-Xylene ug/L ND 2.0 09/15/12 01:10 Methyl-tert-butyl ether ug/L ND 1.0 09/15/12 01:10 Methylene Chloride ug/L ND 2.0 09/15/12 01:10 Naphthalene ug/L ND 1.0 09/15/12 01:10 o-Xylene ug/L ND 1.0 09/15/12 01:10 p-Isopropyltoluene ug/L ND 1.0 09/15/12 01:10 Styrene ug/L ND 1.0 09/15/12 01:10 Tetrachloroethene ug/L ND 1.0 09/15/12 01:10 Toluene ug/L ND 1.0 09/15/12 01:10 trans- 1,2-Dichloroethene ug/L ND 1.0 09/15/12 01:10 trans- 1, 3-Dichloropropene ug/L ND 1.0 09/15/12 01:10 Trichloroethene ug/L ND 1.0 09/15/12 01:10 Trichlorofluoromethane ug/L ND 1.0 09/15/12 01:10 Vinyl acetate ug/L ND 2.0 09/15/12 01:10 Vinyl chloride ug/L ND 1.0 09/15/12 01:10 1,2-Dichloroethane-d4 (S) % 100 70-130 09/15/12 01:10 4-Bromofluorobenzene (S) % 101 70-130 09/15/12 01:10 Dibromofluoromethane (S) % 103 70-130 09/15/12 01:10 Tbluene-d8 (S) % 101 70-130 09/15/12 01:10 LABORATORY CONTROL SAMPLE: 833667 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 50.6 101 70-130 1,1,1-Trichloroethane ug/L 50 47.4 95 70-130 1,1,2,2-Tetrachloroethane ug/L 50 46.2 92 70-130 1,1,2-Trichloroethane ug/L 50 49.2 98 70-130 M-Dichloroethane ug/L 50 47.6 95 70-130 M-Dichloroethene ug/L 50 44.0 88 70-132 1,1-Dichloropropene ug/L 50 43.7 87 70-130 1,2,3-Trichlorobenzene ug/L 50 46.3 93 70-135 1,2,3-Trichloropropane ug/L 50 47.5 95 70-130 1,2,4-Trichlorobenzene ug/L 50 47.2 94 70-134 1,2-Dibromo-3-chloropropane ug/L 50 47.6 95 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.0 104 70-130 1,2-Dichlorobenzene ug/L 50 47.6 95 70-130 1,2-Dichloroethane ug/L 50 45.3 91 70-130 1,2-Dichloropropane ug/L 50 47.5 95 70-130 1,3-Dichlorobenzene ug/L 50 47.1 94 70-130 1,3-Dichloropropane ug/L 50 48.2 96 70-130 1,4-Dichlorobenzene ug/L 50 47.5 95 70-130 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 60 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 LABORATORY CONTROL SAMPLE: Parameter 833667 Units Spike Conc. LCS Result 2,2-Dichloropropane ug/L 50 36.8 2-Butanone (MEK) ug/L 100 91.5 2-Chlorotoluene ug/L 50 50.2 2-Hexanone ug/L 100 106 4-Chlorotoluene ug/L 50 47.6 4-Methyl-2-pentanone (MIBK) ug/L 100 104 Acetone ug/L 100 98.3 Benzene ug/L 50 48.2 Bromobenzene ug/L 50 48.9 Bromochloromethane ug/L 50 46.4 Bromodichloromethane ug/L 50 49.0 Bromoform ug/L 50 50.4 Bromomethane ug/L 50 46.5 Carbon tetrachloride ug/L 50 47.2 Chlorobenzene ug/L 50 49.8 Chloroethane ug/L 50 54.2 Chloroform ug/L 50 47.1 Chloromethane ug/L 50 49.9 cis-1,2-Dichloroethene ug/L 50 47.4 cis-1,3-Dichloropropene ug/L 50 47.1 Dibromochloromethane ug/L 50 52.2 Dibromomethane ug/L 50 47.3 Dichlorodifluoromethane ug/L 50 44.4 Diisopropyl ether ug/L 50 46.3 Ethylbenzene ug/L 50 49.3 Hexachloro-1,3-butadiene ug/L 50 42.9 m&p-Xylene ug/L 100 103 Methyl-tert-butyl ether ug/L 50 46.0 Methylene Chloride ug/L 50 46.4 Naphthalene ug/L 50 47.6 o-Xylene ug/L 50 48.8 p-Isopropyltoluene ug/L 50 48.4 Styrene ug/L 50 50.0 Tetrachloroethene ug/L 50 49.7 Toluene ug/L 50 47.6 trans- 1,2-Dichloroethene ug/L 50 43.1 trans- 1, 3-Dichloropropene ug/L 50 48.9 Trichloroethene ug/L 50 49.8 Trichlorofluoromethane ug/L 50 46.4 Vinyl acetate ug/L 100 103 Vinyl chloride ug/L 50 46.2 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Tbluene-d8 (S) % LCS % Rec % Rec Limits 74 58-145 92 70-145 100 70-130 106 70-144 95 70-130 104 70-140 98 50-175 96 70-130 98 70-130 93 70-130 98 70-130 101 70-130 93 54-130 94 70-132 100 70-130 108 64-134 94 70-130 100 64-130 95 70-131 94 70-130 104 70-130 95 70-131 89 56-130 93 70-130 99 70-130 86 70-130 103 70-130 92 70-130 93 63-130 95 70-138 98 70-130 97 70-130 100 70-130 99 70-130 95 70-130 86 70-130 98 70-132 100 70-130 93 62-133 103 66-157 92 69-130 87 70-130 100 70-130 94 70-130 97 70-130 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 61 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 833668 833669 IVIS MSD 92131396015 Spike Spike IVIS MSD IVIS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual M-Dichloroethene ug/L ND 50 50 47.1 46.7 94 93 70-166 1 30 Benzene ug/L ND 50 50 47.7 46.6 95 93 70-148 2 30 Chlorobenzene ug/L ND 50 50 56.2 54.2 112 108 70-146 4 30 Toluene ug/L ND 50 50 54.0 54.6 108 109 70-155 1 30 Trichloroethene ug/L ND 50 50 57.6 56.6 115 113 69-151 2 30 1,2-Dichloroethane-d4 (S) % 102 102 70-130 4-Bromofluorobenzene (S) % 94 99 70-130 Dibromofluoromethane (S) % 104 106 70-130 Tbluene-d8 (S) % 96 100 70-130 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 62 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 QC Batch: MSV/20483 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92131396001,92131396004,92131396005,92131396006,92131396007,92131396009,92131396011, 92131396020,92131396021,92131396022,92131396023 METHOD BLANK: 839776 Matrix: Water Associated Lab Samples: 92131396001,92131396004,92131396005,92131396006,92131396007,92131396009,92131396011, 92131396020,92131396021,92131396022,92131396023 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/25/12 15:00 1,1,1-Trichloroethane ug/L ND 1.0 09/25/12 15:00 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/25/12 15:00 1,1,2-Trichloroethane ug/L ND 1.0 09/25/12 15:00 1,1-Dichloroethane ug/L ND 1.0 09/25/12 15:00 1,1-Dichloroethene ug/L ND 1.0 09/25/12 15:00 1,1-Dichloropropene ug/L ND 1.0 09/25/12 15:00 1,2,3-Trichlorobenzene ug/L ND 1.0 09/25/12 15:00 1,2,3-Trichloropropane ug/L ND 1.0 09/25/12 15:00 1,2,4-Trichlorobenzene ug/L ND 1.0 09/25/12 15:00 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/25/12 15:00 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/25/12 15:00 1,2-Dichlorobenzene ug/L ND 1.0 09/25/12 15:00 1,2-Dichloroethane ug/L ND 1.0 09/25/12 15:00 1,2-Dichloropropane ug/L ND 1.0 09/25/12 15:00 1,3-Dichlorobenzene ug/L ND 1.0 09/25/12 15:00 1,3-Dichloropropane ug/L ND 1.0 09/25/12 15:00 1,4-Dichlorobenzene ug/L ND 1.0 09/25/12 15:00 2,2-Dichloropropane ug/L ND 1.0 09/25/12 15:00 2-Butanone (MEK) ug/L ND 5.0 09/25/12 15:00 2-Chlorotoluene ug/L ND 1.0 09/25/12 15:00 2-Hexanone ug/L ND 5.0 09/25/12 15:00 4-Chlorotoluene ug/L ND 1.0 09/25/12 15:00 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/25/12 15:00 Acetone ug/L ND 25.0 09/25/12 15:00 Benzene ug/L ND 1.0 09/25/12 15:00 Bromobenzene ug/L ND 1.0 09/25/12 15:00 Bromochloromethane ug/L ND 1.0 09/25/12 15:00 Bromodichloromethane ug/L ND 1.0 09/25/12 15:00 Bromoform ug/L ND 1.0 09/25/12 15:00 Bromomethane ug/L ND 2.0 09/25/12 15:00 Carbon tetrachloride ug/L ND 1.0 09/25/12 15:00 Chlorobenzene ug/L ND 1.0 09/25/12 15:00 Chloroethane ug/L ND 1.0 09/25/12 15:00 Chloroform ug/L ND 1.0 09/25/12 15:00 Chloromethane ug/L ND 1.0 09/25/12 15:00 cis-1,2-Dichloroethene ug/L ND 1.0 09/25/12 15:00 cis-1,3-Dichloropropene ug/L ND 1.0 09/25/12 15:00 Dibromochloromethane ug/L ND 1.0 09/25/12 15:00 Dibromomethane ug/L ND 1.0 09/25/12 15:00 Dichlorodifluoromethane ug/L ND 1.0 09/25/12 15:00 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 63 of 67 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 METHOD BLANK: 839776 Matrix: Water Associated Lab Samples: 92131396001,92131396004,92131396005,92131396006,92131396007,92131396009,92131396011, 92131396020,92131396021,92131396022,92131396023 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diisopropyl ether ug/L ND 1.0 09/25/12 15:00 Ethylbenzene ug/L ND 1.0 09/25/12 15:00 Hexachloro-1,3-butadiene ug/L ND 1.0 09/25/12 15:00 m&p-Xylene ug/L ND 2.0 09/25/12 15:00 Methyl-tert-butyl ether ug/L ND 1.0 09/25/12 15:00 Methylene Chloride ug/L ND 2.0 09/25/12 15:00 Naphthalene ug/L ND 1.0 09/25/12 15:00 o-Xylene ug/L ND 1.0 09/25/12 15:00 p-Isopropyltoluene ug/L ND 1.0 09/25/12 15:00 Styrene ug/L ND 1.0 09/25/12 15:00 Tetrachloroethene ug/L ND 1.0 09/25/12 15:00 Toluene ug/L ND 1.0 09/25/12 15:00 trans- 1,2-Dichloroethene ug/L ND 1.0 09/25/12 15:00 trans- 1, 3-Dichloropropene ug/L ND 1.0 09/25/12 15:00 Trichloroethene ug/L ND 1.0 09/25/12 15:00 Trichlorofluoromethane ug/L ND 1.0 09/25/12 15:00 Vinyl acetate ug/L ND 2.0 09/25/12 15:00 Vinyl chloride ug/L ND 1.0 09/25/12 15:00 1,2-Dichloroethane-d4 (S) % 103 70-130 09/25/12 15:00 4-Bromofluorobenzene (S) % 96 70-130 09/25/12 15:00 Dibromofluoromethane (S) % 106 70-130 09/25/12 15:00 Tbluene-d8 (S) % 103 70-130 09/25/12 15:00 LABORATORY CONTROL SAMPLE: 839777 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 48.8 98 70-130 1,1,1-Trichloroethane ug/L 50 52.0 104 70-130 1,1,2,2-Tetrachloroethane ug/L 50 47.8 96 70-130 1,1,2-Trichloroethane ug/L 50 51.6 103 70-130 M-Dichloroethane ug/L 50 49.3 99 70-130 M-Dichloroethene ug/L 50 43.7 87 70-132 1,1-Dichloropropene ug/L 50 51.1 102 70-130 1,2,3-Trichlorobenzene ug/L 50 53.3 107 70-135 1,2,3-Trichloropropane ug/L 50 49.8 100 70-130 1,2,4-Trichlorobenzene ug/L 50 53.7 107 70-134 1,2-Dibromo-3-chloropropane ug/L 50 51.7 103 70-130 1,2-Dibromoethane (EDB) ug/L 50 50.5 101 70-130 1,2-Dichlorobenzene ug/L 50 51.0 102 70-130 1,2-Dichloroethane ug/L 50 48.1 96 70-130 1,2-Dichloropropane ug/L 50 48.1 96 70-130 1,3-Dichlorobenzene ug/L 50 49.9 100 70-130 1,3-Dichloropropane ug/L 50 50.3 101 70-130 1,4-Dichlorobenzene ug/L 50 50.0 100 70-130 Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 64 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 LABORATORY CONTROL SAMPLE: Parameter 839777 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2,2-Dichloropropane ug/L 50 48.1 96 58-145 2-Butanone (MEK) ug/L 100 99.8 100 70-145 2-Chlorotoluene ug/L 50 52.8 106 70-130 2-Hexanone ug/L 100 107 107 70-144 4-Chlorotoluene ug/L 50 52.8 106 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 106 106 70-140 Acetone ug/L 100 88.6 89 50-175 Benzene ug/L 50 48.9 98 70-130 Bromobenzene ug/L 50 51.1 102 70-130 Bromochloromethane ug/L 50 46.3 93 70-130 Bromodichloromethane ug/L 50 48.3 97 70-130 Bromoform ug/L 50 51.1 102 70-130 Bromomethane ug/L 50 47.9 96 54-130 Carbon tetrachloride ug/L 50 46.0 92 70-132 Chlorobenzene ug/L 50 49.5 99 70-130 Chloroethane ug/L 50 48.8 98 64-134 Chloroform ug/L 50 48.0 96 70-130 Chloromethane ug/L 50 40.8 82 64-130 cis-1,2-Dichloroethene ug/L 50 48.6 97 70-131 cis-1,3-Dichloropropene ug/L 50 49.4 99 70-130 Dibromochloromethane ug/L 50 49.9 100 70-130 Dibromomethane ug/L 50 47.9 96 70-131 Dichlorodifluoromethane ug/L 50 36.4 73 56-130 Diisopropyl ether ug/L 50 52.4 105 70-130 Ethylbenzene ug/L 50 48.8 98 70-130 Hexachloro-1,3-butadiene ug/L 50 55.6 ill 70-130 m&p-Xylene ug/L 100 100 100 70-130 Methyl-tert-butyl ether ug/L 50 54.5 109 70-130 Methylene Chloride ug/L 50 48.8 98 63-130 Naphthalene ug/L 50 55.5 ill 70-138 o-Xylene ug/L 50 48.2 96 70-130 p-Isopropyltoluene ug/L 50 53.3 107 70-130 Styrene ug/L 50 50.8 102 70-130 Tetrachloroethene ug/L 50 48.7 97 70-130 Toluene ug/L 50 48.9 98 70-130 trans- 1,2-Dichloroethene ug/L 50 46.7 93 70-130 trans- 1, 3-Dichloropropene ug/L 50 50.4 101 70-132 Trichloroethene ug/L 50 46.4 93 70-130 Trichlorofluoromethane ug/L 50 38.8 78 62-133 Vinyl acetate ug/L 100 112 112 66-157 Vinyl chloride ug/L 50 41.3 83 69-130 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 98 70-130 Dibromofluoromethane (S) % 99 70-130 Tbluene-d8 (S) % 98 70-130 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 65 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRIL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 66 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD ceAnalytical —paoelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Annual Andrex J 12-1022-34 Pace Project No.: 92131396 Lab ID Sample ID QC Batch Method QC Batch 92131396001 MW-5 EPA 8260 IVISV/20483 92131396002 MW-6 EPA 8260 IVISV/20383 92131396003 MW-7 EPA 8260 IVISV/20383 92131396004 MW-9 EPA 8260 IVISV/20483 92131396005 MW-10 EPA 8260 IVISV/20483 92131396006 MW-11 EPA 8260 IVISV/20483 92131396007 MW-12 EPA 8260 IVISV/20483 92131396008 MW-13 EPA 8260 IVISV/20383 92131396009 MW-14 EPA 8260 IVISV/20483 92131396010 MW-15 EPA 8260 IVISV/20383 92131396011 MW-16 EPA 8260 IVISV/20483 92131396012 MW-17 EPA 8260 IVISV/20385 92131396013 MW-1 8 EPA 8260 IVISV/20385 92131396014 MW-20 EPA 8260 IVISV/20385 92131396015 MW-21 EPA 8260 IVISV/20385 92131396016 MW-22 EPA 8260 IVISV/20385 92131396017 MW-23 EPA 8260 IVISV/20385 92131396018 MW-24 EPA 8260 IVISV/20385 92131396019 MW-26 EPA 8260 IVISV/20385 92131396020 RW-1 EPA 8260 IVISV/20483 92131396021 RW-3 EPA 8260 IVISV/20483 92131396022 RW-5 EPA 8260 IVISV/20483 92131396023 RW-6 EPA 8260 IVISV/20483 92131396024 RW-7 EPA 8260 IVISV/20385 92131396025 TRIP BLANK EPA 8260 IVISV/20385 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Date: 10/02/2012 09:50 AM REPORT OF LABORATORY ANALYSIS Page 67 of 67 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. w z w 3: 0 a 0 L L co w tm z D w 0 L L co w CD z Z) C.) (D _a E U) 0 4) cr V5 44k loueqlevq 0 co EOZSZB N U.- HOBN z I OH >e ONH D 0 c 10- H E C 0 L: tbSZH pemesaidun < .2 cu w r a. 0 a. co W -j 5 > (D E 0 -a < 0- W4) ca r a. 2 Co a SU3NIViNOO JO M M V) FN(011031100 IV dV431 3ldNVS U. w "M 0 z cc W ca CO 0 CL 2 w T4 v "4 N ftj A �4 .r- 0 MWAP LLJ z 0 w C) v UNDO t4 -mo a �w %map .0mm F- LU ui 0 a. � C0 LLJ 0 0 m 1.0- C 6 (dV400=0 8VlJE)=E)) 3dAI3-ldV4VS oz L: 01 S9POO P118A Ges) 3000 XW UVV4 0 E m E :3 !77� c ',Ov 0 J= 0 ii (D U) cc 7- *6 CD z *6 4) z: �— il -j -j 0- Lu 0 3: 4) CL a) a 0 07 .00 a. d- a. 00 X X ca 0 0 (D a) (N./,k) joelul a dweS cu Jold peleas L6 3 � T— AP , sno (N Ol u p C)a 04 o �tl 0 Oo Ul dwa_L U- UJ co S ca .10 8 a w LU -i -i \ IL IL L CL Lo 0 LU E W Z z z IL 0 z 0 a: 0 I\A z . . ....... . z z 0 . . . . . . . . . . . . LU L L LO . .... CL (N/A) GuIJO140 jenppa�j D M.i L L 0 CU c a. co M. Z : � '�:�; : �:­ � : i: 77, cr _sj I 5k . .. ... fy, 1081ul I es cc Jol glees LO p Ap s no 2- ool uo p oq-�:l 6 0. Ul dwe U- LU _S\N1 � d' CD S CL 0 r_ co *01 1 01 M M I —c: w LU '01 -1 —1 \w IL IL L- 4) CL 0 4- 0 w E W m M z M z z CL z (D T- o LLI . . . . . . . . 0 z Z,. a uj o 0 Lo LLJ L (v 9L i 0 dirp. w L L RAW. 4) CL U) 0: z D 0 E 0 4) (D m cr E (D 0 z AD 0 (L I NIX (N/A) 9uliolqo jenppe�j Jqqjo loueqlavy > Q) HOBN IOH CD hi 'bNH 0 1.0- a G E t'OS3H r -j 0 0 r- 0 CL (1) a) 0 CY :0, L: a. 0) CL peAjesejdun SU3NIViNOO -40 # w > J) E 00 V(D ac" w 8 CCU if M(U CLu CD NOUO3-1-100 IV dIA131 3-ldV4VS w LL 0 0 z w 0 w cc R r- Q a w (L 2 z 0 LIJ w 0 0 w L 0 a. 0 U) w Waco Q 10- 0 (dV400=0 8VH0=E)) 3dU 3-IdINVS z (:UGI 01 SOPOO PIJBA Gas) MOO XIU.LVV4 0 E m E m �: � �: a. -J 0- w a) 0 F- M 0 t: 0 >10 (D 7- 46 z 4) cr CL a) a o a. id. Q T f E -00 0 0 X X 0 0 CL r co cc - 0 MI) r- a �: �: cl, (D 0 0 LU D LL LU CD 0 <1 m I LU co m J 0 F- C� < I CD 0 5 40- L.0- M^ AV M o 2 o E = m 0 0 cr 0) E -5 cu E CS rr 0 I Iw 13- 12 #w3.LI 0) z 0 z 0 0 LU -j TrE M!IE F M. I 161 108jul Splatues 04 I/ N cu WNW 2 Jai Glees L6 kk� T- Aploisno (N u pft 1 0, 0. Ul dwejL U- 1� w 0 fc-L a LU ui -i -i a. CL Lo 0 0 16 0 LU E m LIM- Z m Z Z 0 z 0 cr 0 -V Document Name: Sampl.e Condition Upon Document Revised: October 19, 2011 AaceAnalXical Receipt (SCUR) Page 1 of 2 Document No.: Issuing Authorities: .4- -J.,.ibr- com F-ASV-CS-003-rev.07 Pace Asheville Quality Office Project 31 Client Name: Asheville Where Rece.ived: Huntersville Eden Pace Other Courier (Circle): Fed Ex UPS USPS C, Win t Commercial i fig Custody Seal on Cooler/Box Present: El yes no seals intact: yes 10006 no Packing Material: Bubble Wrap Bubble Bags oz<one Other 0"' Circle Thermometer Used: IR 2-8 4039 Type of Ice: W Blue None 00Samples on ice, cooling process has begun I un ack -11.1-565135 Corrected Cooler Ternp 43�, �D C Temp should be above freezing to 60C Biological Tissue is Frozen:. Yes No N/A . Comments: Date and Initit6person exa I on S: . � ' r c -tent Chain of Custody Present: FYes E]No nN/A 1. Chain of. Custody Filled Out: 4!fYes' ONo 0 N/A 2. Chain of.Custody Relinquished: Oyes ONo ON/A 3 Sa rpler Name & Signature on COC: e" �_es ElNo ON/A 4. Samples Arrived within Hold Time: 27'Y'es 0 No ON/A 5. Short Hold Time Analysis (<72hr): ElYes ?1`N`o ON/A 6 Rush Turn Around Time Requested: OYes P11o' [1 N/A 7. Sufficient Vol ume: 9 es ONo ON/A 8. Correct Containers Used: -Pace Containers Used: ElYes .2<es []No E]No EIN/A EIN/A 9. Containers Intact: QY'es ONo EIN/A 10. Filtered volume received for Dissolved tests DYes -.0No 21� r1A 11. sample Labels match COC: -includes date/time/ID/Analysis Matrix: ElTe—s" 0 No EIN/A 12.' All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. _VColiform, TOC, O&G, WI-DRO (wa , ter) exceptionr(�9 ;[Y-t�.s 9Y.as 0Yes ONo []No []No ON/A 0N/A 13. D/Z Initial when completed Samples checked for dechlorination: DYes 0NO 0</A 14. Headspace in VOA Vials >6mm): OYesXNo ON/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): - gTY"es 04's ONo DNo EIN/A EIN/A 16. Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: Field.Data Required? Y / N - Date: SCURF Review:1 _]Date: SRF Review: 12_')��. compliance samples, a copy of this form will be sent to the North C6r'o'lina DEHNR Note: Whenever there is a discrepancy affecting North Ca olina Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers) //,q50 qD ceAnalytical —pacelabs.com September 18, 2012 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 Eden, NC 27288 (336)623-8921 RE: Project: AndrexAnnuaIJ12-1022-34 Pace Project No.: 92131386 Dear Mr. Alexander: Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 13, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TN I standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tom Williams tom.williams@pacelabs.com Project Manager Enclosures PIC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 39 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 39 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE SUMMARY Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Lab ID Sample ID Matrix Date Collected Date Received 92131386001 BC-1 Water 09/13/12 10:50 09/13/12 14:15 92131386002 BC-2 Water 09/13/12 10:40 09/13/12 14:15 92131386003 BC-3 Water 09/13/12 10:30 09/13/12 14:15 92131386004 BC-4 Water 09/13/12 10:15 09/13/12 14:15 92131386005 BC-5 Water 09/13/12 10:05 09/13/12 14:15 92131386006 SM-1 Water 09/13/12 13:00 09/13/12 14:15 92131386007 SM-2 Water 09/13/12 12:40 09/13/12 14:15 92131386008 SM-3 Water 09/13/12 12:30 09/13/12 14:15 92131386009 SM-4 Water 09/13/12 12:20 09/13/12 14:15 92131386010 SM-5 Water 09/13/12 12:15 09/13/12 14:15 92131386011 SM-6 Water 09/13/12 12:05 09/13/12 14:15 92131386012 JW-1 Water 09/13/12 12:45 09/13/12 14:15 92131386013 CS-1 Water 09/13/12 11:15 09/13/12 14:15 92131386014 CS-2 Water 09/13/12 11:00 09/13/12 14:15 92131386015 TRIP BLANK Water 09/13/12 00:00 09/13/12 14:15 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 REPORT OF LABORATORY ANALYSIS Page 3 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92131386001 BC-1 EPA 8260 KJIVI 63 PASI-C 92131386002 BC-2 EPA 8260 KJIM 63 PASI-C 92131386003 BC-3 EPA 8260 KJIM 63 PASI-C 92131386004 BC-4 EPA 8260 KJIM 63 PASI-C 92131386005 BC-5 EPA 8260 KJIM 63 PASI-C 92131386006 SM-1 EPA 8260 KJIM 63 PASI-C 92131386007 SM-2 EPA 8260 KJIM 63 PASI-C 92131386008 SM-3 EPA 8260 KJIM 63 PASI-C 92131386009 SM-4 EPA 8260 KJIM 63 PASI-C 92131386010 SM-5 EPA 8260 KJIM 63 PASI-C 92131386011 SM-6 EPA 8260 KJIVI 63 PASI-C 92131386012 JW-11 EPA 8260 KJIVI 63 PASI-C 92131386013 CS-1 EPA 8260 KJIM 63 PASI-C 92131386014 CS-2 EPA 8260 KJIM 63 PASI-C 92131386015 TRIP BLANK EPA 8260 KJIM 63 PASI-C REPORT OF LABORATORY ANALYSIS Page 4 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: BC-1 LabID: 92131386001 Collected: 09/13/12 10:50 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 06:24 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 06:24 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 06:24 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 06:24 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 06:24 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 06:24 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 06:24 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 06:24 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 06:24 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 06:24 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 06:24 75-00-3 Chloroform 0.82J ug/L 1.0 0.14 1 09/15/12 06:24 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 06:24 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 06:24 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 06:24 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 06:24 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 06:24 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 06:24 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 06:24 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 06:24 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 06:24 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:24 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 06:24 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 06:24 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 06:24 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 06:24 75-35-4 cis-1,2-Dichloroethene 8.8 ug/L 1.0 0.19 1 09/15/12 06:24 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 06:24 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 06:24 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 06:24 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 06:24 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 06:24 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 06:24 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 06:24 10061-02-6 Diisopropyl ether 0.26J ug/L 1.0 0.12 1 09/15/12 06:24 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 06:24 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 06:24 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 06:24 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 06:24 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 06:24 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 06:24 108-10-1 Methyl-tert-butyl ether 0.57J ug/L 1.0 0.21 1 09/15/12 06:24 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 06:24 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 06:24 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 06:24 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 06:24 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 5 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-1 LabID: 92131386001 Collected: 09/13/12 10:50 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 28.4 ug/L 1.0 0.46 1 09/15/12 06:24 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 06:24 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:24 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 06:24 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 06:24 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 06:24 79-00-5 Trichloroethene 2.9 ug/L 1.0 0.47 1 09/15/12 06:24 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 06:24 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 06:24 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 06:24 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 06:24 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 06:24 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 06:24 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 06:24 460-00-4 Dibromofluoromethane (S) 99 % 70-130 1 09/15/12 06:24 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/15/12 06:24 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 09/15/12 06:24 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 6 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: BC-2 LabID: 92131386002 Collected: 09/13/12 10:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 06:39 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 06:39 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 06:39 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 06:39 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 06:39 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 06:39 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 06:39 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 06:39 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 06:39 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 06:39 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 06:39 75-00-3 Chloroform 0.99J ug/L 1.0 0.14 1 09/15/12 06:39 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 06:39 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 06:39 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 06:39 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 06:39 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 06:39 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 06:39 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 06:39 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 06:39 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 06:39 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:39 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 06:39 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 06:39 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 06:39 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 06:39 75-35-4 cis-1,2-Dichloroethene 8.9 ug/L 1.0 0.19 1 09/15/12 06:39 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 06:39 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 06:39 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 06:39 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 06:39 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 06:39 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 06:39 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 06:39 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 06:39 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 06:39 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 06:39 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 06:39 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 06:39 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 06:39 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 06:39 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 06:39 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 06:39 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 06:39 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 06:39 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 06:39 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 7 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-2 LabID: 92131386002 Collected: 09/13/12 10:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 23.0 ug/L 1.0 0.46 1 09/15/12 06:39 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 06:39 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:39 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 06:39 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 06:39 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 06:39 79-00-5 Trichloroethene 3.2 ug/L 1.0 0.47 1 09/15/12 06:39 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 06:39 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 06:39 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 06:39 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 06:39 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 06:39 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 06:39 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 09/15/12 06:39 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/15/12 06:39 1868-53-7 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 09/15/12 06:39 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/15/12 06:39 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 8 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: BC-3 LabID: 92131386003 Collected: 09/13/12 10:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 06:55 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 06:55 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 06:55 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 06:55 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 06:55 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 06:55 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 06:55 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 06:55 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 06:55 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 06:55 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 06:55 75-00-3 Chloroform 1.4 ug/L 1.0 0.14 1 09/15/12 06:55 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 06:55 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 06:55 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 06:55 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 06:55 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 06:55 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 06:55 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 06:55 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 06:55 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 06:55 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:55 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 06:55 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 06:55 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 06:55 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 06:55 75-35-4 cis-1,2-Dichloroethene 3.8 ug/L 1.0 0.19 1 09/15/12 06:55 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 06:55 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 06:55 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 06:55 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 06:55 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 06:55 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 06:55 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 06:55 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 06:55 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 06:55 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 06:55 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 06:55 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 06:55 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 06:55 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 06:55 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 06:55 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 06:55 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 06:55 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 06:55 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 06:55 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 9 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-3 LabID: 92131386003 Collected: 09/13/12 10:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 6.9 ug/L 1.0 0.46 1 09/15/12 06:55 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 06:55 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 06:55 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 06:55 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 06:55 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 06:55 79-00-5 Trichloroethene 1.2 ug/L 1.0 0.47 1 09/15/12 06:55 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 06:55 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 06:55 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 06:55 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 06:55 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 06:55 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 06:55 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/15/12 06:55 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 09/15/12 06:55 1868-53-7 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 09/15/12 06:55 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/15/12 06:55 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 10 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: BC-4 LabID: 92131386004 Collected: 09/13/12 10:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 07:11 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 07:11 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 07:11 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 07:11 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 07:11 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 07:11 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 07:11 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 07:11 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 07:11 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 07:11 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 07:11 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 07:11 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 07:11 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 07:11 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 07:11 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 07:11 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 07:11 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 07:11 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 07:11 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 07:11 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 07:11 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:11 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 07:11 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 07:11 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 07:11 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 07:11 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 07:11 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 07:11 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 07:11 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 07:11 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 07:11 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 07:11 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 07:11 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 07:11 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 07:11 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 07:11 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 07:11 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 07:11 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 07:11 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 07:11 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 07:11 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 07:11 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 07:11 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 07:11 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 07:11 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 07:11 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 11 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-4 LabID: 92131386004 Collected: 09/13/12 10:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/15/12 07:11 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 07:11 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:11 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 07:11 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 07:11 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 07:11 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 07:11 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 07:11 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 07:11 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 07:11 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 07:11 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 07:11 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 07:11 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 07:11 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 09/15/12 07:11 1868-53-7 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 09/15/12 07:11 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 09/15/12 07:11 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 12 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: BC-5 LabID: 92131386005 Collected: 09/13/12 10:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 2.8J ug/L 25.0 2.2 1 09/15/12 07:26 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 07:26 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 07:26 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 07:26 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 07:26 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 07:26 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 07:26 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 07:26 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 07:26 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 07:26 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 07:26 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 07:26 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 07:26 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 07:26 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 07:26 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 07:26 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 07:26 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 07:26 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 07:26 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 07:26 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 07:26 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:26 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 07:26 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 07:26 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 07:26 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 07:26 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 07:26 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 07:26 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 07:26 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 07:26 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 07:26 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 07:26 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 07:26 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 07:26 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 07:26 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 07:26 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 07:26 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 07:26 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 07:26 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 07:26 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 07:26 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 07:26 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 07:26 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 07:26 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 07:26 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 07:26 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 13 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-5 LabID: 92131386005 Collected: 09/13/12 10:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.51J ug/L 1.0 0.46 1 09/15/12 07:26 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 07:26 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:26 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 07:26 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 07:26 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 07:26 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 07:26 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 07:26 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 07:26 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 07:26 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 07:26 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 07:26 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 07:26 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/15/12 07:26 460-00-4 Dibromofluoromethane (S) 104 % 70-130 1 09/15/12 07:26 1868-53-7 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 09/15/12 07:26 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/15/12 07:26 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 14 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: SM-1 LabID: 92131386006 Collected: 09/13/12 13:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 2.6J ug/L 25.0 2.2 1 09/15/12 07:42 67-64-1 Benzene 2.0 ug/L 1.0 0.25 1 09/15/12 07:42 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 07:42 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 07:42 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 07:42 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 07:42 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 07:42 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 07:42 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 07:42 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 07:42 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 07:42 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 07:42 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 07:42 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 07:42 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 07:42 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 07:42 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 07:42 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 07:42 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 07:42 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 07:42 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 07:42 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:42 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 07:42 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 07:42 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 07:42 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 07:42 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 07:42 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 07:42 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 07:42 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 07:42 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 07:42 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 07:42 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 07:42 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 07:42 10061-02-6 Diisopropyl ether 0.23J ug/L 1.0 0.12 1 09/15/12 07:42 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 07:42 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 07:42 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 07:42 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 07:42 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 07:42 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 07:42 108-10-1 Methyl-tert-butyl ether 17.2 ug/L 1.0 0.21 1 09/15/12 07:42 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 07:42 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 07:42 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 07:42 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 07:42 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 15 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-1 LabID: 92131386006 Collected: 09/13/12 13:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/15/12 07:42 127-18-4 Toluene 1.0 ug/L 1.0 0.26 1 09/15/12 07:42 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:42 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 07:42 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 07:42 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 07:42 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 07:42 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 07:42 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 07:42 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 07:42 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 07:42 75-01-4 m&p-Xylene 0.75J ug/L 2.0 0.66 1 09/15/12 07:42 179601-23-1 o-Xylene 0.39J ug/L 1.0 0.23 1 09/15/12 07:42 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 07:42 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 09/15/12 07:42 1868-53-7 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 09/15/12 07:42 17060-07-0 Tbluene-d8 (S) 101 % 70-130 1 09/15/12 07:42 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 16 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: SM-2 LabID: 92131386007 Collected: 09/13/12 12:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 07:58 67-64-1 Benzene 0.73J ug/L 1.0 0.25 1 09/15/12 07:58 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 07:58 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 07:58 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 07:58 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 07:58 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 07:58 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 07:58 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 07:58 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 07:58 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 07:58 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 07:58 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 07:58 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 07:58 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 07:58 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 07:58 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 07:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 07:58 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 07:58 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 07:58 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 07:58 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:58 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 07:58 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 07:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 07:58 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 07:58 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 07:58 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 07:58 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 07:58 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 07:58 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 07:58 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 07:58 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 07:58 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 07:58 10061-02-6 Diisopropyl ether 0.21J ug/L 1.0 0.12 1 09/15/12 07:58 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 07:58 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 07:58 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 07:58 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 07:58 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 07:58 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 07:58 108-10-1 Methyl-tert-butyl ether 12.8 ug/L 1.0 0.21 1 09/15/12 07:58 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 07:58 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 07:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 07:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 07:58 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 17 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-2 LabID: 92131386007 Collected: 09/13/12 12:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.88J ug/L 1.0 0.46 1 09/15/12 07:58 127-18-4 Toluene 0.34J ug/L 1.0 0.26 1 09/15/12 07:58 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 07:58 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 07:58 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 07:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 07:58 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 07:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 07:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 07:58 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 07:58 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 07:58 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 07:58 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 07:58 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 07:58 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/15/12 07:58 1868-53-7 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 09/15/12 07:58 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 09/15/12 07:58 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 18 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: SM-3 LabID: 92131386008 Collected: 09/13/12 12:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 08:14 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 08:14 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 08:14 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 08:14 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 08:14 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 08:14 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 08:14 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 08:14 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 08:14 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 08:14 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 08:14 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 08:14 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 08:14 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 08:14 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 08:14 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 08:14 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 08:14 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 08:14 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 08:14 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 08:14 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 08:14 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 08:14 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 08:14 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 08:14 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 08:14 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 08:14 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 08:14 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 08:14 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 08:14 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 08:14 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 08:14 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 08:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 08:14 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 08:14 10061-02-6 Diisopropyl ether 0.17J ug/L 1.0 0.12 1 09/15/12 08:14 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 08:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 08:14 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 08:14 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 08:14 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 08:14 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 08:14 108-10-1 Methyl-tert-butyl ether 11.1 ug/L 1.0 0.21 1 09/15/12 08:14 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 08:14 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 08:14 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 08:14 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 08:14 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 19 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-3 LabID: 92131386008 Collected: 09/13/12 12:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.68J ug/L 1.0 0.46 1 09/15/12 08:14 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 08:14 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 08:14 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 08:14 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 08:14 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 08:14 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 08:14 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 08:14 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 08:14 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 08:14 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 08:14 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 08:14 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 08:14 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 09/15/12 08:14 460-00-4 Dibromofluoromethane (S) 108 % 70-130 1 09/15/12 08:14 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 09/15/12 08:14 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 09/15/12 08:14 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 20 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: SM-4 LabID: 92131386009 Collected: 09/13/12 12:20 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 08:29 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 08:29 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 08:29 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 08:29 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 08:29 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 08:29 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 08:29 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 08:29 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 08:29 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 08:29 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 08:29 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 08:29 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 08:29 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 08:29 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 08:29 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 08:29 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 08:29 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 08:29 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 08:29 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 08:29 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 08:29 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 08:29 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 08:29 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 08:29 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 08:29 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 08:29 75-35-4 cis-1,2-Dichloroethene 0.47J ug/L 1.0 0.19 1 09/15/12 08:29 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 08:29 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 08:29 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 08:29 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 08:29 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 08:29 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 08:29 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 08:29 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 08:29 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 08:29 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 08:29 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 08:29 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 08:29 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 08:29 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 08:29 108-10-1 Methyl-tert-butyl ether 7.7 ug/L 1.0 0.21 1 09/15/12 08:29 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 08:29 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 08:29 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 08:29 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 08:29 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 21 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-4 LabID: 92131386009 Collected: 09/13/12 12:20 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2.1 ug/L 1.0 0.46 1 09/15/12 08:29 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 08:29 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 08:29 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 08:29 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 08:29 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 08:29 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 08:29 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 08:29 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 08:29 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 08:29 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 08:29 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 08:29 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 08:29 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 09/15/12 08:29 460-00-4 Dibromofluoromethane (S) 104 % 70-130 1 09/15/12 08:29 1868-53-7 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 09/15/12 08:29 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/15/12 08:29 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 22 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: SM-5 LabID: 92131386010 Collected: 09/13/12 12:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 08:45 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 08:45 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 08:45 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 08:45 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 08:45 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 08:45 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 08:45 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 08:45 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 08:45 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 08:45 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 08:45 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 08:45 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 08:45 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 08:45 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 08:45 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 08:45 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 08:45 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 08:45 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 08:45 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 08:45 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 08:45 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 08:45 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 08:45 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 08:45 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 08:45 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 08:45 75-35-4 cis-1,2-Dichloroethene 0.28J ug/L 1.0 0.19 1 09/15/12 08:45 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 08:45 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 08:45 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 08:45 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 08:45 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 08:45 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 08:45 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 08:45 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 08:45 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 08:45 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 08:45 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 08:45 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 08:45 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 08:45 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 08:45 108-10-1 Methyl-tert-butyl ether 6.0 ug/L 1.0 0.21 1 09/15/12 08:45 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 08:45 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 08:45 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 08:45 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 08:45 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 23 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-5 LabID: 92131386010 Collected: 09/13/12 12:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.7 ug/L 1.0 0.46 1 09/15/12 08:45 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 08:45 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 08:45 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 08:45 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 08:45 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 08:45 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 08:45 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 08:45 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 08:45 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 08:45 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 08:45 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 08:45 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 08:45 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/15/12 08:45 460-00-4 Dibromofluoromethane (S) 103 % 70-130 1 09/15/12 08:45 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 09/15/12 08:45 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/15/12 08:45 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 24 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: SM-6 LabID: 92131386011 Collected: 09/13/12 12:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone 5.8J ug/L 25.0 2.2 1 09/15/12 09:01 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 09:01 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 09:01 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 09:01 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 09:01 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 09:01 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 09:01 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 09:01 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 09:01 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 09:01 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 09:01 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 09:01 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 09:01 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 09:01 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 09:01 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 09:01 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 09:01 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 09:01 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 09:01 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 09:01 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 09:01 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 09:01 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 09:01 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 09:01 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 09:01 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 09:01 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 09:01 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 09:01 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 09:01 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 09:01 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 09:01 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 09:01 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 09:01 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 09:01 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 09:01 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 09:01 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 09:01 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 09:01 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 09:01 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 09:01 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 09:01 108-10-1 Methyl-tert-butyl ether 4.7 ug/L 1.0 0.21 1 09/15/12 09:01 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 09:01 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 09:01 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 09:01 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 09:01 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 25 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-6 LabID: 92131386011 Collected: 09/13/12 12:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.3 ug/L 1.0 0.46 1 09/15/12 09:01 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 09:01 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 09:01 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 09:01 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 09:01 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 09:01 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 09:01 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 09:01 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 09:01 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 09:01 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 09:01 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 09:01 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 09:01 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 09/15/12 09:01 460-00-4 Dibromofluoromethane (S) 103 % 70-130 1 09/15/12 09:01 1868-53-7 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 09/15/12 09:01 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/15/12 09:01 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 26 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: JW-1 LabID: 92131386012 Collected: 09/13/12 12:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 2.2 1 09/15/12 09:16 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 09:16 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 09:16 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 09:16 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 09:16 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 09:16 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 09:16 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 09:16 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 09:16 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 09:16 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 09:16 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 09:16 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 09:16 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 09:16 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 09:16 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 09:16 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 09:16 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 09:16 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 09:16 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 09:16 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 09:16 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 09:16 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 09:16 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 09:16 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 09:16 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 09:16 75-35-4 cis-1,2-Dichloroethene 4.9 ug/L 1.0 0.19 1 09/15/12 09:16 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 09:16 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 09:16 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 09:16 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 09:16 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 09:16 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 09:16 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 09:16 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 09:16 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 09:16 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 09:16 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 09:16 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 09:16 99-87-6 Methylene Chloride ND ug/L 2.0 0.97 1 09/15/12 09:16 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 09:16 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 09:16 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 09:16 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 09:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 09:16 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 09:16 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 27 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: JW-1 LabID: 92131386012 Collected: 09/13/12 12:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 25.8 ug/L 1.0 0.46 1 09/15/12 09:16 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 09:16 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 09:16 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 09:16 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 09:16 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 09:16 79-00-5 Trichloroethene 2.5 ug/L 1.0 0.47 1 09/15/12 09:16 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 09:16 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 09:16 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 09:16 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 09:16 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 09:16 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 09:16 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/15/12 09:16 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 09/15/12 09:16 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 09/15/12 09:16 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 09/15/12 09:16 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 28 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 LabID: 92131386013 Collected: 09/13/12 11:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/15/12 09:32 67-64-1 ND ug/L 1.0 0.25 1 09/15/12 09:32 71-43-2 ND ug/L 1.0 0.30 1 09/15/12 09:32 108-86-1 ND ug/L 1.0 0.17 1 09/15/12 09:32 74-97-5 ND ug/L 1.0 0.18 1 09/15/12 09:32 75-27-4 ND ug/L 1.0 0.26 1 09/15/12 09:32 75-25-2 ND ug/L 2.0 0.29 1 09/15/12 09:32 74-83-9 ND ug/L 5.0 0.96 1 09/15/12 09:32 78-93-3 ND ug/L 1.0 0.25 1 09/15/12 09:32 56-23-5 ND ug/L 1.0 0.23 1 09/15/12 09:32 108-90-7 ND ug/L 1.0 0.54 1 09/15/12 09:32 75-00-3 ND ug/L 1.0 0.14 1 09/15/12 09:32 67-66-3 ND ug/L 1.0 0.11 1 09/15/12 09:32 74-87-3 ND ug/L 1.0 0.35 1 09/15/12 09:32 95-49-8 ND ug/L 1.0 0.31 1 09/15/12 09:32 106-43-4 ND ug/L 5.0 2.5 1 09/15/12 09:32 96-12-8 ND ug/L 1.0 0.21 1 09/15/12 09:32 124-48-1 ND ug/L 1.0 0.27 1 09/15/12 09:32 106-93-4 ND ug/L 1.0 0.21 1 09/15/12 09:32 74-95-3 ND ug/L 1.0 0.30 1 09/15/12 09:32 95-50-1 ND ug/L 1.0 0.24 1 09/15/12 09:32 541-73-1 ND ug/L 1.0 0.33 1 09/15/12 09:32 106-46-7 ND ug/L 1.0 0.21 1 09/15/12 09:32 75-71-8 ND ug/L 1.0 0.32 1 09/15/12 09:32 75-34-3 ND ug/L 1.0 0.12 1 09/15/12 09:32 107-06-2 ND ug/L 1.0 0.56 1 09/15/12 09:32 75-35-4 2.7 ug/L 1.0 0.19 1 09/15/12 09:32 156-59-2 ND ug/L 1.0 0.49 1 09/15/12 09:32 156-60-5 ND ug/L 1.0 0.27 1 09/15/12 09:32 78-87-5 ND ug/L 1.0 0.28 1 09/15/12 09:32 142-28-9 ND ug/L 1.0 0.13 1 09/15/12 09:32 594-20-7 ND ug/L 1.0 0.49 1 09/15/12 09:32 563-58-6 ND ug/L 1.0 0.13 1 09/15/12 09:32 10061-01-5 ND ug/L 1.0 0.26 1 09/15/12 09:32 10061-02-6 ND ug/L 1.0 0.12 1 09/15/12 09:32 108-20-3 ND ug/L 1.0 0.30 1 09/15/12 09:32 100-41-4 ND ug/L 1.0 0.71 1 09/15/12 09:32 87-68-3 ND ug/L 5.0 0.46 1 09/15/12 09:32 591-78-6 ND ug/L 1.0 0.31 1 09/15/12 09:32 99-87-6 ND ug/L 2.0 0.97 1 09/15/12 09:32 75-09-2 ND ug/L 5.0 0.33 1 09/15/12 09:32 108-10-1 ND ug/L 1.0 0.21 1 09/15/12 09:32 1634-04-4 ND ug/L 1.0 0.24 1 09/15/12 09:32 91-20-3 ND ug/L 1.0 0.26 1 09/15/12 09:32 100-42-5 ND ug/L 1.0 0.33 1 09/15/12 09:32 630-20-6 ND ug/L 1.0 0.40 1 09/15/12 09:32 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 29 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 LabID: 92131386013 Collected: 09/13/12 11:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 18.5 ug/L 1.0 0.46 1 09/15/12 09:32 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 09:32 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 09:32 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 09:32 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 09:32 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 09:32 79-00-5 Trichloroethene 1.3 ug/L 1.0 0.47 1 09/15/12 09:32 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 09:32 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 09:32 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 09:32 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 09:32 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 09:32 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 09:32 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 09/15/12 09:32 460-00-4 Dibromofluoromethane (S) 106 % 70-130 1 09/15/12 09:32 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 09/15/12 09:32 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/15/12 09:32 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 30 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 LabID: 92131386014 Collected: 09/13/12 11:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/15/12 09:48 67-64-1 ND ug/L 1.0 0.25 1 09/15/12 09:48 71-43-2 ND ug/L 1.0 0.30 1 09/15/12 09:48 108-86-1 ND ug/L 1.0 0.17 1 09/15/12 09:48 74-97-5 ND ug/L 1.0 0.18 1 09/15/12 09:48 75-27-4 ND ug/L 1.0 0.26 1 09/15/12 09:48 75-25-2 ND ug/L 2.0 0.29 1 09/15/12 09:48 74-83-9 ND ug/L 5.0 0.96 1 09/15/12 09:48 78-93-3 ND ug/L 1.0 0.25 1 09/15/12 09:48 56-23-5 ND ug/L 1.0 0.23 1 09/15/12 09:48 108-90-7 ND ug/L 1.0 0.54 1 09/15/12 09:48 75-00-3 ND ug/L 1.0 0.14 1 09/15/12 09:48 67-66-3 ND ug/L 1.0 0.11 1 09/15/12 09:48 74-87-3 ND ug/L 1.0 0.35 1 09/15/12 09:48 95-49-8 ND ug/L 1.0 0.31 1 09/15/12 09:48 106-43-4 ND ug/L 5.0 2.5 1 09/15/12 09:48 96-12-8 ND ug/L 1.0 0.21 1 09/15/12 09:48 124-48-1 ND ug/L 1.0 0.27 1 09/15/12 09:48 106-93-4 ND ug/L 1.0 0.21 1 09/15/12 09:48 74-95-3 ND ug/L 1.0 0.30 1 09/15/12 09:48 95-50-1 ND ug/L 1.0 0.24 1 09/15/12 09:48 541-73-1 ND ug/L 1.0 0.33 1 09/15/12 09:48 106-46-7 ND ug/L 1.0 0.21 1 09/15/12 09:48 75-71-8 ND ug/L 1.0 0.32 1 09/15/12 09:48 75-34-3 ND ug/L 1.0 0.12 1 09/15/12 09:48 107-06-2 ND ug/L 1.0 0.56 1 09/15/12 09:48 75-35-4 0.38J ug/L 1.0 0.19 1 09/15/12 09:48 156-59-2 ND ug/L 1.0 0.49 1 09/15/12 09:48 156-60-5 ND ug/L 1.0 0.27 1 09/15/12 09:48 78-87-5 ND ug/L 1.0 0.28 1 09/15/12 09:48 142-28-9 ND ug/L 1.0 0.13 1 09/15/12 09:48 594-20-7 ND ug/L 1.0 0.49 1 09/15/12 09:48 563-58-6 ND ug/L 1.0 0.13 1 09/15/12 09:48 10061-01-5 ND ug/L 1.0 0.26 1 09/15/12 09:48 10061-02-6 ND ug/L 1.0 0.12 1 09/15/12 09:48 108-20-3 ND ug/L 1.0 0.30 1 09/15/12 09:48 100-41-4 ND ug/L 1.0 0.71 1 09/15/12 09:48 87-68-3 ND ug/L 5.0 0.46 1 09/15/12 09:48 591-78-6 ND ug/L 1.0 0.31 1 09/15/12 09:48 99-87-6 ND ug/L 2.0 0.97 1 09/15/12 09:48 75-09-2 ND ug/L 5.0 0.33 1 09/15/12 09:48 108-10-1 ND ug/L 1.0 0.21 1 09/15/12 09:48 1634-04-4 ND ug/L 1.0 0.24 1 09/15/12 09:48 91-20-3 ND ug/L 1.0 0.26 1 09/15/12 09:48 100-42-5 ND ug/L 1.0 0.33 1 09/15/12 09:48 630-20-6 ND ug/L 1.0 0.40 1 09/15/12 09:48 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 31 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 LabID: 92131386014 Collected: 09/13/12 11:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 5.9 ug/L 1.0 0.46 1 09/15/12 09:48 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 09:48 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 09:48 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 09:48 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 09:48 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 09:48 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 09:48 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 09:48 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 09:48 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 09:48 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 09:48 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 09:48 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 09:48 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 09/15/12 09:48 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 09/15/12 09:48 1868-53-7 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 09/15/12 09:48 17060-07-0 Tbluene-d8 (S) 102 % 70-130 1 09/15/12 09:48 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 32 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Sample: TRIP BLANK LabID: 92131386015 Collected: 09/13/12 00:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Analytical Method: EPA 8260 Acetone 5.5J ug/L 25.0 2.2 1 09/15/12 03:00 67-64-1 Benzene ND ug/L 1.0 0.25 1 09/15/12 03:00 71-43-2 Bromobenzene ND ug/L 1.0 0.30 1 09/15/12 03:00 108-86-1 Bromochloromethane ND ug/L 1.0 0.17 1 09/15/12 03:00 74-97-5 Bromodichloromethane ND ug/L 1.0 0.18 1 09/15/12 03:00 75-27-4 Bromoform ND ug/L 1.0 0.26 1 09/15/12 03:00 75-25-2 Bromomethane ND ug/L 2.0 0.29 1 09/15/12 03:00 74-83-9 2-Butanone (MEK) ND ug/L 5.0 0.96 1 09/15/12 03:00 78-93-3 Carbon tetrachloride ND ug/L 1.0 0.25 1 09/15/12 03:00 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 09/15/12 03:00 108-90-7 Chloroethane ND ug/L 1.0 0.54 1 09/15/12 03:00 75-00-3 Chloroform ND ug/L 1.0 0.14 1 09/15/12 03:00 67-66-3 Chloromethane ND ug/L 1.0 0.11 1 09/15/12 03:00 74-87-3 2-Chlorotoluene ND ug/L 1.0 0.35 1 09/15/12 03:00 95-49-8 4-Chlorotoluene ND ug/L 1.0 0.31 1 09/15/12 03:00 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 2.5 1 09/15/12 03:00 96-12-8 Dibromochloromethane ND ug/L 1.0 0.21 1 09/15/12 03:00 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.27 1 09/15/12 03:00 106-93-4 Dibromomethane ND ug/L 1.0 0.21 1 09/15/12 03:00 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.30 1 09/15/12 03:00 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 0.24 1 09/15/12 03:00 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 03:00 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 0.21 1 09/15/12 03:00 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.32 1 09/15/12 03:00 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.12 1 09/15/12 03:00 107-06-2 M-Dichloroethene ND ug/L 1.0 0.56 1 09/15/12 03:00 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.19 1 09/15/12 03:00 156-59-2 trans- 1,2-Dichloroethene ND ug/L 1.0 0.49 1 09/15/12 03:00 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.27 1 09/15/12 03:00 78-87-5 1,3-Dichloropropane ND ug/L 1.0 0.28 1 09/15/12 03:00 142-28-9 2,2-Dichloropropane ND ug/L 1.0 0.13 1 09/15/12 03:00 594-20-7 1,1-Dichloropropene ND ug/L 1.0 0.49 1 09/15/12 03:00 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 0.13 1 09/15/12 03:00 10061-01-5 trans- 1, 3-Dichloropropene ND ug/L 1.0 0.26 1 09/15/12 03:00 10061-02-6 Diisopropyl ether ND ug/L 1.0 0.12 1 09/15/12 03:00 108-20-3 Ethylbenzene ND ug/L 1.0 0.30 1 09/15/12 03:00 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 0.71 1 09/15/12 03:00 87-68-3 2-Hexanone ND ug/L 5.0 0.46 1 09/15/12 03:00 591-78-6 p-Isopropyltoluene ND ug/L 1.0 0.31 1 09/15/12 03:00 99-87-6 Methylene Chloride 1.4J ug/L 2.0 0.97 1 09/15/12 03:00 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 0.33 1 09/15/12 03:00 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 0.21 1 09/15/12 03:00 1634-04-4 Naphthalene ND ug/L 1.0 0.24 1 09/15/12 03:00 91-20-3 Styrene ND ug/L 1.0 0.26 1 09/15/12 03:00 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 0.33 1 09/15/12 03:00 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 0.40 1 09/15/12 03:00 79-34-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 33 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK LabID: 92131386015 Collected: 09/13/12 00:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/15/12 03:00 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/15/12 03:00 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/15/12 03:00 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/15/12 03:00 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/15/12 03:00 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/15/12 03:00 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/15/12 03:00 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/15/12 03:00 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/15/12 03:00 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/15/12 03:00 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/15/12 03:00 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/15/12 03:00 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/15/12 03:00 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 09/15/12 03:00 460-00-4 Dibromofluoromethane (S) 104 % 70-130 1 09/15/12 03:00 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 09/15/12 03:00 17060-07-0 Tbluene-d8 (S) 101 % 70-130 1 09/15/12 03:00 2037-26-5 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 34 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 QC Batch: MSV/20387 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92131386001,92131386002,92131386003,92131386004,92131386005,92131386006,92131386007, 92131386008,92131386009,92131386010,92131386011,92131386012,92131386013,92131386014, 92131386015 METHOD BLANK: 833712 Matrix: Water Associated Lab Samples: 92131386001,92131386002,92131386003,92131386004,92131386005,92131386006,92131386007, 92131386008,92131386009,92131386010,92131386011,92131386012,92131386013,92131386014, 92131386015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1, 1, 1,2-Tetrachloroethane ug/L ND 1.0 09/15/12 00:54 1, 1, 1 -Trichloroethane ug/L ND 1.0 09/15/12 00:54 1, 1,2,2-Tetrachloroethane ug/L ND 1.0 09/15/12 00:54 1, 1,2-Trichloroethane ug/L ND 1.0 09/15/12 00:54 1,1-Dichloroethane ug/L ND 1.0 09/15/12 00:54 1,1-Dichloroethene ug/L ND 1.0 09/15/12 00:54 1,1-Dichloropropene ug/L ND 1.0 09/15/12 00:54 1,2,3-Trichlorobenzene ug/L ND 1.0 09/15/12 00:54 1,2,3-Trichloropropane ug/L ND 1.0 09/15/12 00:54 1,2,4-Trichlorobenzene ug/L ND 1.0 09/15/12 00:54 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/15/12 00:54 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/15/12 00:54 1,2-Dichlorobenzene ug/L ND 1.0 09/15/12 00:54 1,2-Dichloroethane ug/L ND 1.0 09/15/12 00:54 1,2-Dichloropropane ug/L ND 1.0 09/15/12 00:54 1,3-Dichlorobenzene ug/L ND 1.0 09/15/12 00:54 1,3-Dichloropropane ug/L ND 1.0 09/15/12 00:54 1,4-Dichlorobenzene ug/L ND 1.0 09/15/12 00:54 2,2-Dichloropropane ug/L ND 1.0 09/15/12 00:54 2-Butanone (MEK) ug/L ND 5.0 09/15/12 00:54 2-Chlorotoluene ug/L ND 1.0 09/15/12 00:54 2-Hexanone ug/L ND 5.0 09/15/12 00:54 4-Chlorotoluene ug/L ND 1.0 09/15/12 00:54 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/15/12 00:54 Acetone ug/L ND 25.0 09/15/12 00:54 Benzene ug/L ND 1.0 09/15/12 00:54 Bromobenzene ug/L ND 1.0 09/15/12 00:54 Bromochloromethane ug/L ND 1.0 09/15/12 00:54 Bromodichloromethane ug/L ND 1.0 09/15/12 00:54 Bromoform ug/L ND 1.0 09/15/12 00:54 Bromomethane ug/L ND 2.0 09/15/12 00:54 Carbon tetrachloride ug/L ND 1.0 09/15/12 00:54 Chlorobenzene ug/L ND 1.0 09/15/12 00:54 Chloroethane ug/L ND 1.0 09/15/12 00:54 Chloroform ug/L ND 1.0 09/15/12 00:54 Chloromethane ug/L ND 1.0 09/15/12 00:54 cis-1,2-Dichloroethene ug/L ND 1.0 09/15/12 00:54 cis-1,3-Dichloropropene ug/L ND 1.0 09/15/12 00:54 Dibromochloromethane ug/L ND 1.0 09/15/12 00:54 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 35 of 39 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 METHOD BLANK: 833712 Matrix: Water Associated Lab Samples: 92131386001,92131386002,92131386003,92131386004,92131386005,92131386006,92131386007, 92131386008,92131386009,92131386010,92131386011,92131386012,92131386013,92131386014, 92131386015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dibromomethane ug/L ND 1.0 09/15/12 00:54 Dichlorodifluoromethane ug/L ND 1.0 09/15/12 00:54 Diisopropyl ether ug/L ND 1.0 09/15/12 00:54 Ethylbenzene ug/L ND 1.0 09/15/12 00:54 Hexachloro-1,3-butadiene ug/L ND 1.0 09/15/12 00:54 m&p-Xylene ug/L ND 2.0 09/15/12 00:54 Methyl-tert-butyl ether ug/L ND 1.0 09/15/12 00:54 Methylene Chloride ug/L ND 2.0 09/15/12 00:54 Naphthalene ug/L ND 1.0 09/15/12 00:54 o-Xylene ug/L ND 1.0 09/15/12 00:54 p-Isopropyltoluene ug/L ND 1.0 09/15/12 00:54 Styrene ug/L ND 1.0 09/15/12 00:54 Tetrachloroethene ug/L ND 1.0 09/15/12 00:54 Toluene ug/L ND 1.0 09/15/12 00:54 trans- 1,2-Dichloroethene ug/L ND 1.0 09/15/12 00:54 trans- 1, 3-Dichloropropene ug/L ND 1.0 09/15/12 00:54 Trichloroethene ug/L ND 1.0 09/15/12 00:54 Trichlorofluoromethane ug/L ND 1.0 09/15/12 00:54 Vinyl acetate ug/L ND 2.0 09/15/12 00:54 Vinyl chloride ug/L ND 1.0 09/15/12 00:54 1,2-Dichloroethane-d4 (S) % 104 70-130 09/15/12 00:54 4-Bromofluorobenzene (S) % 94 70-130 09/15/12 00:54 Dibromofluoromethane (S) % 104 70-130 09/15/12 00:54 Tbluene-d8 (S) % 100 70-130 09/15/12 00:54 LABORATORY CONTROL SAMPLE: 833713 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 50.8 102 70-130 1,1,1-Trichloroethane ug/L 50 49.7 99 70-130 1,1,2,2-Tetrachloroethane ug/L 50 47.4 95 70-130 1,1,2-Trichloroethane ug/L 50 49.6 99 70-130 1,1-Dichloroethane ug/L 50 48.7 97 70-130 1,1-Dichloroethene ug/L 50 47.4 95 70-132 1,1-Dichloropropene ug/L 50 45.4 91 70-130 1,2,3-Trichlorobenzene ug/L 50 47.7 95 70-135 1,2,3-Trichloropropane ug/L 50 46.1 92 70-130 1,2,4-Trichlorobenzene ug/L 50 48.4 97 70-134 1,2-Dibromo-3-chloropropane ug/L 50 50.1 100 70-130 1,2-Dibromoethane (EDB) ug/L 50 51.7 103 70-130 1,2-Dichlorobenzene ug/L 50 50.3 101 70-130 1,2-Dichloroethane ug/L 50 45.1 90 70-130 1,2-Dichloropropane ug/L 50 48.0 96 70-130 1,3-Dichlorobenzene ug/L 50 47.6 95 70-130 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 36 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 LABORATORY CONTROL SAMPLE: Parameter 833713 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichloropropane ug/L 50 49.4 99 70-130 1,4-Dichlorobenzene ug/L 50 48.2 96 70-130 2,2-Dichloropropane ug/L 50 34.4 69 58-145 2-Butanone (MEK) ug/L 100 96.5 97 70-145 2-Chlorotoluene ug/L 50 52.7 105 70-130 2-Hexanone ug/L 100 108 108 70-144 4-Chlorotoluene ug/L 50 50.6 101 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 103 103 70-140 Acetone ug/L 100 102 102 50-175 Benzene ug/L 50 48.2 96 70-130 Bromobenzene ug/L 50 49.5 99 70-130 Bromochloromethane ug/L 50 47.1 94 70-130 Bromodichloromethane ug/L 50 50.5 101 70-130 Bromoform ug/L 50 51.4 103 70-130 Bromomethane ug/L 50 42.6 85 54-130 Carbon tetrachloride ug/L 50 49.1 98 70-132 Chlorobenzene ug/L 50 50.2 100 70-130 Chloroethane ug/L 50 63.3 127 64-134 Chloroform ug/L 50 47.4 95 70-130 Chloromethane ug/L 50 55.7 ill 64-130 cis-1,2-Dichloroethene ug/L 50 48.0 96 70-131 cis-1,3-Dichloropropene ug/L 50 47.2 94 70-130 Dibromochloromethane ug/L 50 52.3 105 70-130 Dibromomethane ug/L 50 47.7 95 70-131 Dichlorodifluoromethane ug/L 50 46.4 93 56-130 Diisopropyl ether ug/L 50 46.2 92 70-130 Ethylbenzene ug/L 50 49.5 99 70-130 Hexachloro-1,3-butadiene ug/L 50 43.8 88 70-130 m&p-Xylene ug/L 100 98.9 99 70-130 Methyl-tert-butyl ether ug/L 50 46.6 93 70-130 Methylene Chloride ug/L 50 47.7 95 63-130 Naphthalene ug/L 50 48.6 97 70-138 o-Xylene ug/L 50 49.1 98 70-130 p-Isopropyltoluene ug/L 50 49.1 98 70-130 Styrene ug/L 50 50.1 100 70-130 Tetrachloroethene ug/L 50 49.6 99 70-130 Toluene ug/L 50 48.0 96 70-130 trans- 1,2-Dichloroethene ug/L 50 45.1 90 70-130 trans- 1, 3-Dichloropropene ug/L 50 48.5 97 70-132 Trichloroethene ug/L 50 48.9 98 70-130 Trichlorofluoromethane ug/L 50 47.4 95 62-133 Vinyl acetate ug/L 100 108 108 66-157 Vinyl chloride ug/L 50 48.4 97 69-130 1,2-Dichloroethane-d4 (S) % 89 70-130 4-Bromofluorobenzene (S) % 98 70-130 Dibromofluoromethane (S) % 94 70-130 Tbluene-d8 (S) % 96 70-130 Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 37 of 39 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRIL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 38 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Andrex Annual J12-1022-34 Pace Project No.: 92131386 Lab ID Sample ID QC Batch Method QC Batch 92131386001 BC-1 EPA 8260 MSV/20387 92131386002 BC-2 EPA 8260 MSV/20387 92131386003 BC-3 EPA 8260 MSV/20387 92131386004 BC-4 EPA 8260 MSV/20387 92131386005 BC-5 EPA 8260 MSV/20387 92131386006 SM-1 EPA 8260 MSV/20387 92131386007 SM-2 EPA 8260 MSV/20387 92131386008 SM-3 EPA 8260 MSV/20387 92131386009 SM-4 EPA 8260 MSV/20387 92131386010 SM-5 EPA 8260 MSV/20387 92131386011 SM-6 EPA 8260 MSV/20387 92131386012 JW-11 EPA 8260 MSV/20387 92131386013 CS-1 EPA 8260 MSV/20387 92131386014 CS-2 EPA 8260 MSV/20387 92131386015 TRIP BLANK EPA 8260 MSV/20387 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Date: 09/18/2012 11:53 AM REPORT OF LABORATORY ANALYSIS Page 39 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. uj . . ....... 0 00 (Y) z z 0 Lu 0 L L LO F- z 0 L fy- L tu vi LLJ F- F�:V.��..':.,..1144 T z c/) aj� cu E Aw 0 U) Cr :3 E CD aci 0 (N/A) euuolqo jenpse�j I I OOIF ME JqqjO 0 > jOu8qjqvq OzSzeN HOIRN z IOH �4 4)1 so NH III 0 2 "OSZH >D M . c) EE cc 0 10- z >% a 0 L: 2 :7 pejuesaidun 0 0 0 0 cc CL E w (.D a r '0 0 CL 0- cm MEINIVINOO :30 # C" ro uj e > J) aca. 12 cul CU ca m a. NOUO3-1100 JLV dIN31 3'ldV4VS co LL 0 (1) W 2 a 0 - 0 C) z w m F- u 00 "O.V46 'i 0 a. cu C) uj a 2 z 0 UJ W. F- (0) z 0 z .0 0 LU -j IL CO) N) C) w V) JL 0 0 w 0 OU) ix 0 CM." a (dVVOO=O SVUE)=E)) 3dUg-ldVVVS 0 z -a 0 u (:gel 01 SOPOO PjleA 89S) 3CIOO.XNiVIN 0 0 cr Mg 0 a 0 ca -C 2= E E M :D z z a. -J -j w Cl Cf) 0 F- (no 4) -00 U) iL O'L) x cu 4) C.) 0 a) :3 Cf) a) 4) c 0. Ch -r cu ca — 0 0 0 a 9w" LU D rg Cc, OW cc 2 z too) U- 0 W m C� 0 cc E JOR + Qj 14N 4 cc ca 9 JOR J C) D 14 2 (D r ?3 0 42. E cu _n C V 0 POW zo = cr cn col %n sn \nl;, 0 g r CL 0 (1) q4) I! E F., # WaLl ui Wes cu A) 2 J810 peleas :V) LO V- A no (N 01 C) UO pie 38�j cq 0 6 00 Ul IdwajL < L.L 2 1 1 V Im Fa w S; 0 a ca 8 zS C Ilk w LU -i -i E CL IL Q CL U� 4- 6 w E w m M z z z z 0 cc 0 .......... uj J2 F- j o z z CD z 4) F- 0 a 0 4) L L LO co ui (N/A) 9uliol4o jenp!se�j z D Ix L L & 4-j jqqj o loueqlevy cc > HOBN ':ONH 0 cu E E cu "OS2�H 0 0 'o c G 0 H 2 Z >% w ca 0 CD :3 U 0 r- - :07 L: 0- 4) CL pe/uesejdun SU3NIVINOO :10 o LU > -j U) CL E 0 Q 2 a) w co M W CD a) co w cu 0- M cu iL N011031100 IV dIA131 3-ldV\lVS co ..s C4 CO) � 7� w :3 (.) . . 9 ~ %� 4-L (? r- CL 20 Z CO) w w Zap F- U.1 M 0 w w (0) F- 0 a. 0 w F--; 0 Z b < co 4`3 (dV400=0 GVHE)=E)) 3dU 31dlNVS 0 0 z (:4Gj 01 SOPOO P!IBA 99s) 3(300,XRJ.LVN (D .2 a) .0 a. 0 E cu E �: � I a. -i -i (L of F- co 0 3: < 0 0 14-) 12 V- z "U z *6 cr 4) 4) o CL (1) a 0 LU 4) '08 U) w w C) m a. CL 0 LC x co 4) L. E o :3 Cf) , 0) 4 a) 4) r 4Z U) -8;� CL co .r Cc M 0 La - OLL U) 0 0 w c z c) cc —CD LL w 0 W CA 0 ZP CML co cz E co 0) U) .0 JOR co C cl S? 0 a r CL o E = z cc U) C 0 U) cr 0 CL E o co E w cr # W311 U) z 0 P FS z 0 w -j IL CO "r1hL Em � joelul svAam les 0 0 CN cc Jai peleas to o1sno ID I- (N ol 0 I clq UO P 1 391:1 C) 0. ui dwejL < U- 111Qh.- Lu A ow cc %so 0 co w lz N ui ui -i _j a. a. (D -eo 0 46 0 ui E W m D Z z z CL M 0 z (D cr 0 Document Name: Sample Condition- Upon Document Revised: October 19, 2011 "jceAnal jdical Receipt (SCUR) . Page 1 of 2 Document No.: Issuing Authorities: corn- F-ASV-CS-003-rev.07 Pace Asheville Quality Office Client Name: Project Where Received: Huntersville sheville L1 Eden Courier (Circle): Fed Ex UPS USPS nt Commercial Pace Other SE D ye s n o seals intact: yes no Custody Seal. on Cooler/Box Present: F C M M 5e-!.1 Packing Material: F] Bubble Wrap ubble Bags None Other Circle Thermometer Used: IR_I�n#244039 Type of Ice: Blue None Samples on ice, cooling process has begun IR Gun Ba.c 111565135 -A Corrected Cooler Temp.:. C Temp should be above.freezing to 60C Biological Tissue is Frozen:. Yes No N/A Comments: Date and Initia.1 of person * . I I , ell contents : IT V: Chain of Custody Present: POKe E]No EIN/A 1 Chain of Custody Filled Out: J;?<, El No ON/A 2. Chain of Custody Relinq uished: 04es DNo ON/A 3. Sampler.Nam'e & Signature on COC: �<s ONo ON/A 4. Samples Arrived within Hold Time: �Wes D.No ON/A 5. Short Hold Time Analysis (<72hr): Dyes faVo ON/A 6. Rush Turn Around Time Requested: OYes F=�o ON/A 7.* Sufficient Volume: ET�es ONo EIN/A 8. Correct Containers Used: -Pace 'Containers Used: Pies []No Xes DNo EIN/A ON/A 9. containers Intact, El'Yes ONo ON/A 10. Filtered volume received for Dissolved tests DYes 0 No L361A 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: Ak)boliform, TOC, O&G, WI-DRO (water) �ElYes Eluo eflYes E]No 6Yes El No E]Yes 0No ON/A EIN/A ON/A ----Initial 12.' 13. when completed Samples checked for dechlorination: DYes ONO 14. Headspace in VOA Vials >6mm): ElYes 217o ON/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): ��es DNo D-Nile's' E]No ON/A ON/A 16. Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: Field.Data Required? Y / N SCURF Review: Date: SRF Review: D ate: Note: Whenever there is a crepancyy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers) qD ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (336)623-8921 October 10, 2012 Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 RE: Project: AndrexAnnual Sampling Pace Project No.: 92134321 (828)254-7176 (704)875-9092 Dear Mr. Alexander: Enclosed are the analytical results for sample(s) received by the laboratory on September 13, 2012. The results relate only to the samples included in this report. Results reported herein conform to the most current TN I standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tom Williams tom.williams@pacelabs.com Project Manager Enclosures PIC REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 22 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: Andrex Annual Sampling Pace Project No.: 92134321 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification E87648 Massachusetts Certification M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 22 qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 SAMPLE SUMMARY Project: Andrex Annual Sampling Pace Project No.: 92134321 Lab ID Sample ID Matrix Date Collected Date Received 92134321001 MW-13 Water 09/11/12 14:30 09/13/12 14:15 92134321002 BC-1 Water 09/13/12 10:50 09/13/12 14:15 92134321003 BC-2 Water 09/13/12 10:40 09/13/12 14:15 92134321004 BC-3 Water 09/13/12 10:30 09/13/12 14:15 92134321005 BC-4 Water 09/13/12 10:15 09/13/12 14:15 92134321006 BC-5 Water 09/13/12 10:05 09/13/12 14:15 92134321007 SM-1 Water 09/13/12 13:00 09/13/12 14:15 92134321008 SM-2 Water 09/13/12 12:40 09/13/12 14:15 92134321009 SM-3 Water 09/13/12 12:30 09/13/12 14:15 92134321010 SM-4 Water 09/13/12 12:20 09/13/12 14:15 92134321011 SM-5 Water 09/13/12 12:15 09/13/12 14:15 92134321012 SM-6 Water 09/13/12 12:05 09/13/12 14:15 92134321013 CS-1 Water 09/13/12 11:15 09/13/12 14:15 92134321014 CS-2 Water 09/13/12 11:00 09/13/12 14:15 92134321015 JW-1 Water 09/13/12 12:45 09/13/12 14:15 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 REPORT OF LABORATORY ANALYSIS Page 3 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project: Andrex Annual Sampling Pace Project No.: 92134321 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92134321001 MW-13 SM 5310B EWS 1 PASI-A 92134321002 BC-1 SM 5310B EWS 1 PASI-A 92134321003 BC-2 SM 5310B EWS 1 PASI-A 92134321004 BC-3 SM 5310B EWS 1 PASI-A 92134321005 BC-4 SM 5310B EWS 1 PASI-A 92134321006 BC-5 SM 5310B EWS 1 PASI-A 92134321007 SM-1 SM 5310B EWS 1 PASI-A 92134321008 SM-2 SM 5310B EWS 1 PASI-A 92134321009 SM-3 SM 5310B EWS 1 PASI-A 92134321010 SM-4 SM 5310B EWS 1 PASI-A 92134321011 SM-5 SM 5310B EWS 1 PASI-A 92134321012 SM-6 SM 5310B EWS 1 PASI-A 92134321013 CS-1 SM 5310B EWS 1 PASI-A 92134321014 CS-2 SM 5310B EWS 1 PASI-A 92134321015 JW-1 SM 5310B EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS Page 4 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 LabID: 92134321001 Collected: 09/11/1214:30 Received: 09/13/1214:15 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon ND mg/L 1.0 1.0 1 10/08/12 16:28 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 5 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-1 LabID: 92134321002 Collected: 09/13/12 10:50 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon ND mg/L 1.0 1.0 1 10/08/12 16:49 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 6 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-2 LabID: 92134321003 Collected: 09/13/12 10:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 6.4 mg/L 1.0 1.0 1 10/08/12 17:05 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 7 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-3 LabID: 92134321004 Collected: 09/13/12 10:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.7 mg/L 1.0 1.0 1 10/08/12 17:17 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 8 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-4 LabID: 92134321005 Collected: 09/13/12 10:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.5 mg/L 1.0 1.0 1 10/08/12 17:27 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 9 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-5 LabID: 92134321006 Collected: 09/13/12 10:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.2 mg/L 1.0 1.0 1 10/08/12 17:41 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 10 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-1 LabID: 92134321007 Collected: 09/13/12 13:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/08/12 18:33 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 11 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-2 LabID: 92134321008 Collected: 09/13/12 12:40 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.0 mg/L 1.0 1.0 1 10/08/12 18:43 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 12 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-3 LabID: 92134321009 Collected: 09/13/12 12:30 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.2 mg/L 1.0 1.0 1 10/08/12 18:55 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 13 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-4 LabID: 92134321010 Collected: 09/13/12 12:20 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.5 mg/L 1.0 1.0 1 10/08/12 19:05 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 14 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-5 LabID: 92134321011 Collected: 09/13/12 12:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.5 mg/L 1.0 1.0 1 10/08/12 19:15 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 15 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-6 LabID: 92134321012 Collected: 09/13/12 12:05 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.1 mg/L 1.0 1.0 1 10/08/12 19:38 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 16 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 LabID: 92134321013 Collected: 09/13/12 11:15 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 5.2 mg/L 1.0 1.0 1 10/08/12 19:54 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 17 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 LabID: 92134321014 Collected: 09/13/12 11:00 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/08/12 20:04 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 18 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Andrex Annual Sampling Pace Project No.: 92134321 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: JW-1 LabID: 92134321015 Collected: 09/13/12 12:45 Received: 09/13/12 14:15 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.7 mg/L 1.0 1.0 1 10/08/12 20:54 7440-44-0 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 19 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Andrex Annual Sampling Pace Project No.: 92134321 QC Batch: WETA/13421 Analysis Method: SM 531 OB QC Batch Method: SM 5310B Analysis Description: 531 OB TOC Associated Lab Samples: 92134321001,92134321002,92134321003,92134321004,92134321005,92134321006,92134321007, 92134321008,92134321009,92134321010,92134321011,92134321012,92134321013,92134321014, 92134321015 METHOD BLANK: 848795 Matrix: Water Associated Lab Samples: 92134321001,92134321002,92134321003,92134321004,92134321005,92134321006,92134321007, 92134321008,92134321009,92134321010,92134321011,92134321012,92134321013,92134321014, 92134321015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 10/08/12 15:51 LABORATORY CONTROL SAMPLE: 848796 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.0 96 90-110 MATRIX SPIKE SAMPLE: 848797 92134321001 Spike VIS VIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L ND 25 25.4 99 75-125 MATRIX SPIKE SAMPLE: 848799 92134321011 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 2.5 25 26.3 95 75-125 SAMPLE DUPLICATE: 848798 92134321002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L ND ND 20 SAMPLE DUPLICATE: 848800 92134321012 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 1.1 1.1 2 20 Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 20 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: Andrex Annual Sampling Pace Project No.: 92134321 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRIL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville Date: 10/10/2012 12:49 PM REPORT OF LABORATORY ANALYSIS Page 21 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. qD Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Andrex Annual Sampling Pace Project No.: 92134321 Lab ID Sample ID QC Batch Method QC Batch 92134321001 MW-13 SIM 531 OB WETA/1 3421 92134321002 BC-1 SIM 531 OB WETA/1 3421 92134321003 BC-2 SIM 531 OB WETA/1 3421 92134321004 BC-3 SIM 531 OB WETA/1 3421 92134321005 BC-4 SIM 531 OB WETA/1 3421 92134321006 BC-5 SIM 531 OB WETA/1 3421 92134321007 SM-1 SIM 531 OB WETA/1 3421 92134321008 SM-2 SIM 531 OB WETA/1 3421 92134321009 SM-3 SIM 531 OB WETA/1 3421 92134321010 SM-4 SIM 531 OB WETA/1 3421 92134321011 SM-5 SIM 531 OB WETA/1 3421 92134321012 SM-6 SIM 531 OB WETA/1 3421 92134321013 CS-1 SIM 531 OB WETA/1 3421 92134321014 CS-2 SIM 531 OB WETA/1 3421 92134321015 JW-11 SIM 531 OB WETA/1 3421 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Date: 10/10/2012 12:49 PIVI REPORT OF LABORATORY ANALYSIS Page 22 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. it LU On Joel uj a. 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CONCENTRATION PLOTS Monitoring Well MW-1 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 US 2nd I 3rd — 4th lst 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene 7,400 8,600 3,400 900 NS 860 3,600 3,500 880 NS 1,400 183 74 170 190 320 40 26 10 8.0 18 110 AB AB AB AB Trichloroethene 124 ND 21 2.6 NS ND 40 ND 3.7 NS ND ND 2.7 29 47 ND 1.0 1.2 ND ND ND 6.9 AB AB AB AB Chloroform 1.2 ND 1.7 9 NS 7 ND ND 17 NS ND ND 15 7 ND ND 1.1 ND 1.1 ND ND ND AB AB AB AB Vinyl Chloride ND I ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1, 1 -Trichloroethane ND 340 ND ND NS ND ND ND ND NS ND MND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1,2-Trichloroethane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1 -Dichloroethene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloroethane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB_ Trans 1,2-Dichloroethene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Cis 1,2-Dichloroethene NA NA NA NA NS NA NA NA NA NS NA NA NA 17 30 ND 0.82 ND ND ND ND 18.6 AB AB AB AB Trichlorofluoromethane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloropropane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Chlorobenzene ND ND NO ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB A-13 AB 1,4-Dichlorobenzene ND ND ND ND NS ND ND ND ND NS ND— ND ND ND ND ND ND ND_ ND ND ND ND AB AB AB AB 1,1,1,2-Tetrachloroethane NA NA NA NA NS INA NA NA NA NS NA NA NA NA NA NA NA , NA NA NA NA ND AB AB AB AB TOTAL CHLORINATEDS DETECTED 17,52518,94013,4231 9121 NS 1867 13,64013,50019011 NS 11,4001 183 1 92 1 223 1 267 1 320 1 43 1 27 1 11 1 8.0 1 18 136 AB AR AR AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NS = Not Sampled; recovery system being monitored for aquifer modeling. The laboratory results from MW-1 were inadvertently labeled as MW-2 during the 2nd quarter 1994. The correction has been made on this spreadsheet. Mw-1 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-2 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 0i 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP 640 81 76 NS 110 130 100 78 NS 66 69 28 76 41 31 19 17 12 13 19 6.9 AB AB AB AB Trichloroethene NP ND 1.7 7.3 NS 13 21 12 12 NS 13 ND ND 16 11 6.4 2.9 2.4 2.7 2.6 1.7 0.71 AB AB AB AB_ Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND 0.69 ND ND ND ND ND ND AB AB AB AB Vinyl Chloride NP ND ND ND I NS IND ND I ND I ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB I AB AB AB 1, 1, 1 -Trichloroethane NP 91 ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND- ND ND ND AB AB AB AB 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,1-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND. AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND I ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB I AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 2.8 17 4.1 4.1 ND 1 1.8_ 0.83 1.2 ND AB A-13 A-13 AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS �jS�NDA -ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND AB AB AB t,1,1,2-Tetrachloroethane NA NA NA NA NS N I NA , N NS NA NA NA NA NA NA +� NA NA NA NA NA ND AB AB AB AB TOTAL CHLORINATEDS DETECTED I NP 731 83 1 83 1 NS 11231 151 1 1121 90 1 NS 1 79 1 69 1 28 1 95 1 69 1 42 1 26 1 19 1 17 1 16 1 22 1 7.6 i AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. The laboratory results from MW-2 were inadvertently labeled as MW- I during the 2nd quarter 1994. The correction has been made on this spreadsheet. MW-2 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TR3 Monitoring Well MW-3 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1 95 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3�d 4th 2nd 3rd 4th Ist 2nd 3rd 4th Ist 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP 18,000 350 140 NS 11 80 12 34 NS 9.2 623 600 38 160 91 89 29 39 55 45 820 AB AB AB AB_ Trichloroethene NP 700 26 21 NS 2.8 12 3.1 5 NS 1.7 149 430 13 95 20 3.7 3.2 3.9 5.0 3.6 26.6 AB AB AB AB_ Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND 1.1 ND ND ND ND ND ND ND AB AB AB AB Vinyl Chloride NP ND 34 49 NS 7.21 17 1 10 7.8 1 NS I ND ND 59 3.5 11 ND ND ND 0.84 ND ND 2.6 AB AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND 1.1 ND ND ND ND ND ND ND AB AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND 1.30 ND ND ND ND ND ND ND ND ND 0.55 AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB_ Trans 1,2-Dichloroethene NP ND 0.74 ND NS ND ND ND ND NS ND 1.57 ND ND ND ND ND ND ND ND ND ND AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 20 130 18 ND ND 2.3 0.53 1.2 40.9 AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,4-Dichlorobenzene NP I ND ND NDINSIND ND ND ND NS ND ND I ND ND ND ND ND I ND ND ND ND ND AB AB AB AB 1,1,1,2-Tetrachloroethane NA I NA NA NAINSINA1 NA I NA NA NS NA NA I NA NA NA NA NA I NA NA I NA NA ND AB AB AB AB_ TOTAL CHLORINATEDS DETECTED I NP 118,7001 411 12101 NS 121 1 109 1 25 1 47 1 NS 1 10.91 775 1 1,0891 75 1 398 1 129 1 93 1 32 1 46 61 50 1 891 AB --A—� AB B AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-3 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TR3 Monitoring Well MW-4 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd F�t 4 th 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant I Tetrachloroethene NP 1,100 630 510 NS 680 620 560 360 NS 250 363 410 840 630 180 560 170 200 200 150 230 AB AB AB AB Trichloroethene NP 620 230 220 NS 230 300 280 200 NS 180 248 240 430 410 160 500 140 170 170 180 275 AB AB AB AB Chloroform NP ND ND ND NS ND ND 22 ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Vinyl Chloride NP -ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS 2.5 ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1,2-Trichloroethane NP I ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND 3.4 ND AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND —ND ND AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND_ ND ND ND ND AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 190 180 69 210 74 98 88 120 148 AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloropropane NP 4.5 3.3 ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND 0.75 0.78 AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,1,1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA NS NA. NA NA NA NA NA NA NA NA NA NA ND AB AB AB AB TOTAL CHLORINATEDS DETECTED I NPI 1,7251 863 1 7301 NSI 9131 920 1 8621 560 1 NS 1 430 1 611 1 650 1 1,4601 1,2201 409 1 1,2701 384 1 468 1 458 454 654 1 AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-4 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-5 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP 49,000 23,000 7,200 NS 9,200 7,800 7,600 9,000 NS 25,000 3,200 1,500 5,500 980 NS 25 dy 120 150 610 106 2,160 3,750 2,340 4,940 Trichloroethene NP 300 470 ND NS ND 15 ND 23 NS ND ND ND ND ND NS 2.3 d 1.0 8.9 7.2 7.0 5.0 14.0 74.9 279.0 Chloroform NP ND 13 ND NS ND 20 ND 38 NS ND ND 14 ND ND NS ND dry NE) ND ND 0.61 1.2 4.2 ND ND Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS . ND dry ND ND ND ND ND ND ND 1.7 1,1,1-Trichloroethane NP 530 8.9 ND NS ND 2.8 ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND NDJ 1, 1,2-Trichloroethane NP ND 6.8 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS ND �g ND ND ND ND ND ND ND 2 1,2-Dichloroethane NP ND 1.2 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND 2.1 ND NS ND ND ND ND NS. ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND 3 Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 86 710 NS 13 dry 2.6 22 8 21 19 3,420 783 Trichlorolluoromethane NP ND ND ND NS ND 1.3 ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND Chlorobenzene NP ND 130 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND I- 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NA NA NA NA NS NA NA I NA I NA INS, NA NA NA NA NA NA NA dry NA NA NA ND ND ND ND 2 TOTAL CHLORINATEDS DETECTED NP 49,830 23,632 1 7,200 1 NSI 9,200 1 7,8391 7,600 1 9,061 1 NS 1 25,000 1 3,200 1 1,5141 5,5861 1,6901 NS 1 40 1 dr-y 1 124 1 181 1 625 1 135 12,18513,7771 5,835 6.011 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled, well dry or in use as pilot test recovery point. MW-5 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-6 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2001; 2008 2009 2010 2011 2012 3rdF4th 2nd 3rd 4th 1st 2nd 3rd 4th Ist 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP 40,000 37,000 7,600 NS 27,000 7,700 7,300 7,000 NS 3,500 3,270 3,300 12,000 4,700 5,100 7,800 5,900 3,200 1,000 5,000 3,050 3,580 270 2,160 2,550 Trichloroethene NP 1,600 6,500 290 NS 1,600 330 260 310 NS ND 162 160 2,700 1,500 1,200 1,800 860 390 110 150 251 267 58 110 52 Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP ND 280 47 NS ND 99 ND 84 NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP ND 1.7 ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP ND 17 ND NS ND ND ND ND NS ND 5.49 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND 1.32 ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND 45 ND NS ND ND ND ND NS ND 20.2 ND ND ND ND ND ND 4.5 ND 1.8 1.4 ND ND ND ND Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 1 8,900 3,800 1 4,500 2,8001 210 390 270 110 207 284 85 328 43 Trichlorofluoromethane NP ND 28 ND NS ND ND ND ND NS ND 2.82 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP ND 9.5 ND NS ND ND ND ND NS ND 2.17 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP ND 1.8 ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND 4.6 3.5 ND ND ND ND 11,1,1,2-Tetrachloroethme NA NA NA NA NS NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA ND ND ND NU NU TOTAL CHLORINATEDS DETECTED I NP 141,600143,88317,9371 NS 128,60018,12917,56017,3941 NS 13,5001 3,464 1 3,460 1 23,600110,000110,800112,4001 6,970 1 3,9851 1,3801 5,266 1 3,5131 4,1311 413 1 2,5981 2,644 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. NM-6 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-7 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd I 4th 2.d 3rd 4th lst 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP 6.0 8.3 12 NS 76 46 27 13 NS 41 165 11 10 3.6 72 ND 1.9 1.4 1.4 1.3 ND 36 92 165 175 Trichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND 24 ND ND ND ND ND ND ND ND ND ND Chloroform NP ND ND ND NS 1.2 ND 1.1 ND NS 2.2 6.24 1.2 2 ND 0.62 ND ND 0.67 ND ND ND ND 0.6 0.51 ND Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND lj-Dichloroethenc NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA ND ND 20 ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP ND ND ND NS IND ND ND ND NS ND ND ND ND I ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP ND ND ND NS I ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NA NAINAINAINS1— NA NA NAINSINA1 NA I NA I NA I NA I NA I NA I NA NA I NA I ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I I NP 16.01 8.3 1 12 1 NS 177 1 46 1 28 1 13 INS 1 43 1 171 1 12 1 12 1 3.6 1 117 1 ND 1 1.9 1 2.1 1 1.4 1 1.3 1 ND 1 36 93 166 175 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-7 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-8 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1 95 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP 78 24 620 NS 20 950 900 1,500 NS 39 675 570 420_ 80 8.7 19 24 15 23 40 13 AB AB AB AB Trichloroethene NP 4.5 ND 68 NS ND 29 66 68 NS 1.1 53.4 58 14 8.4 1.8 ND ND ND ND 2.9 ND AB AB AB AB Chloroform NP ND ND ND NS ND ND 8.5 ND NS ND ND ND ND ND I ND ND I ND ND ND ND ND AB AB I AB AB Vinyl Chloride NP ND ND. ND. NS ND. ND ND ND NS. ND. ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND ND ND NS ND I ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB ],I-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Cis 1,2-Dichloroethene NP NA I NA NA NS NA NA NA NA NS NA NA NA 26 46 1.1 ND ND ND ND 3.9 ND AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB31 AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB 3 AB AB AB 1, 1, 1,2-Tetrachloroethane NA NA NA NA NS INA NA NA NA NS NA I NA NA NA NA NA NA NA NA NA NA ND AB A133 AB B TOTAL CHLORINATEDS DETECTED �NI? F83 1 24 1 6881 NS 1 201 979 1 975 1 1,568 INSI 40 1 728 1 628 1 460 1 134 1 12 1 19 1 24 1 15 1 23 1 47 1 13 AB AB I AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. Mw-8 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-8A Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1 91 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2.d 3rd 4th lst 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP 1,800 640 3,900 NS 970 3,400 3,700 6,300 NS 1,200 3,470 3,400 1,600 1,900 1,100 400 400 420 110 190 247 AB AB AB AB Trichloroethene NP 96 25 250 NS 39 190 240 270 NS ND 250 220 ND 410 95 79 47 42 10 20 16 AB AB AB AB Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND I ND ND ND ND ND ND ND ND ND AB AB AB AB Vinyl Chloride NP ND ND ND NS ND 2.8 1 ND ND NS I ND 4.29 ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND 1.9 ND ND NS ND 3.11 ND ND ND ND ND ND ND ND ND ND AB AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS I NA NA NA 120 430 160 1 150 83 80 17 40 28.4 AB AB AB AB Trichlorofluoromethane NP ND ND ND NS ND 0.92 ND ND NS ND 1.78 ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,2-Dichloropropane NP I ND I ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND NT) NT) D AB AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND D AB AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND N— --- - -- D AB AB AB AB 1, 1, 1,2-Tetrachloroethane NA I NA I NA NA NS NA NA NA NA -A -A D AB AB AB AB TOTAL CHLORMATEDS DETECTED I NP 11,8961 665 14,1501 NS 11,00913,59613,94016,5701 NS 11,2001 3,729 13,620 1 1,720 12,740 1 1,355 1 629 1 530 1 542 1 137 1 250 1 292 AB AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-8A Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-9 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 rd R3�1 4th 2nd 3rd 4th Ist 2nd 3rd 4th Ist 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd Contaminant I --- Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 1,900 4,550 3,800 3,600 3,600 1,100 270 2,200 1,700 1,000 680 4,730 4,840 5,080 4,180 2,000 Trichloroethene NP NP NP NP NP NP NP NP NP NP ND 608 620 570 970 270 66 250 140 92 98 341 234 145 107 99 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 4.4 ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND 9.42 ND ND ND ND 100 28 24 ND 1 10 2.5 ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NE) 0.74 ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 1.89 ND ND ND ND 0.5 ND ND ND 3.6 1.1 ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NE) ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 8.81 ND ND ND ND 5.6 ND 2.6 1 ND 2.2 7 ND ND ND 1.9 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA 920 1,100 260 300 500 400 240 180 466 376 259 191 325 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 2.31 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP, N NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP I NP NP NP NP NP NP NP NP ND 6.29 ND ND ND ND 28 6.8 1.5 ND 2.2 1.6 ND ND ND 0.47 1,4-Dichlorobenzene tNPNP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 5.6 ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA I NA NA 0.70 ND ND ND ND TOTAL CHLORINATEDS DETECTED NPI NPI NP I NPI NP I NP I NP I NP I NP I NPI 1,9001 5,187 1 4,420 1 5,090 1 5,670 1 1,6301 780 1 2,985 1 2,2681 1,332 1 976 1 5,551 5,450 1 5,484 4,478 2426 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NM-9 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-10 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1 95 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2.d 3rd 4th lst_ 2nd 3rd 4th 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant -Ist Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 4,700 4,920 5,400 9,900 4,200 4,500 3,500 900 800 590 1,200 3,360 1,910 3,160 182 5 Trichloroethene NP NP NP NP NP NP NP NP NP NP 400 484 480 920 400 450 440 120 74 54 120 180 76 127 75 ND Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND 1 3.07 ND ND ND ND ND ND ND ND 2.7 ND ND ND ND 5 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 2.00 ND ND ND ND ND ND ND ND 3.5 ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.9 ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 7.69 ND ND ND ND ND ND 1.2 ND 2.6 5 ND ND 15.2 ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA I NA NA 2,300 1,300 870 620 320 220 160 270 426 169 253 1,460 20 Trichlorofluoromethane NP NP NP NP, NP, NP NP NP NP NP ND 4.94 ND ND ND ND ND ND_ ND ND 2.9 ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene I NP NP NP NP NP NP NP NP NP_ NP ND 2.51 ND ND ND ND ND ND ND ND ND 0.86 ND ND ND ND — 1,4-Dichlorobenzene I NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane I NP NP N- NP NP NP NP NP NP I NP NA NA I NA NA NA I NA NA NA NA 1.2 1.2 ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NP I NP I NPI NP I NP I NP I NPI NPI NP 15,10015,424 1 5,880 113,1201 5,900 1 5,820 1 4,560 1 1,340 1 1,095 1 804 1 1,602 3,973 2,156 3,540 1,73: Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NM-10 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-11 Concentrations in Parts per Billion (jig/]) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 1,400 3,050 1,800 3,600 2,100 1,800 2,200 2,200 1,000 1,100 NS 975 791 2,400 2,130 1,940 Trichloroethene NP NP NP NP NP NP NP NP NP NP 190 370 240 410 280 300 110 330 230 180 NS 89 56 196 93 87 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND I ND ND ND 12 ND ND ND NS I ND ND ND ND ND Vinyl Chloride NP NP NP I NP NP NP NP I NP NP NP ND ND 36 110 ND ND 22 ND 9.7 ND NS ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND ND Ij-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 1.74 ND ND ND ND 1.7 ND ND ND NS ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND —ND ND ND ND ND ND ND NS ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 5.95 ND ND ND ND 5.8 ND 2.2 ND NS 2.2 ND 5.2 ND 1. Cis 1,2-Dichloroethene NP NP NP I NP NP NP NP I NP NP NP NA NA NA 1,000 770 530 980 480 490 380 NS 153 156 337 163 162 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 3.02 ND ND ND ND I ND ND ND NS ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND 9.77 ND ND ND ND 5.1 ND 2.2 ND NS ND ND ND ND 0.39 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND 2.08 ND ND ND ND 1.3 ND ND ND NS ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NA NA NA NA I NA NA NA NA NA NA NS ND ND ND ND 0.51 TOTAL CHLORMATEDS DETECTED I I NP NP NP I NP I NP I NPI NP I NP I NPINPI 1,5901 3,443 1 2,076 1 5,1201 3,1501 2,630 1 3,339 1 3,0101 1,7341 1,6601 NS 1 1,2191 1,0031 2,938 2,386 2,191 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-11 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJ13 Monitoring Well MW-12 Concentrations in Parts per Billion (jig/]) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2ml 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 5,300 3,810 1,500 3,500 2,800 3,200 220 130 220 65 930 135 1,010 3,590 156 3 Trichloroethene NP NP NP NP NP NP NP NP NP NP ND 6.07 ND ND ND 550 3 ND ND ND 5— 1.4 10 11 44 ND Chloroform NP NP NP NP NP NP NP NP NP NP ND 20.8 ND I ND ND ND 1.3 ND ND ND ND 1.3 2.8 ND ND ND Vinyl Chloride NP NP NP I NP NP NP NP I NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 22.7 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Ij-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11.3 ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND —ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 14.2 11.4 Cis 1,2-Dichloroethene NP NP NP I NP NP NP NP I NP NP NP NA NA NA ND ND 750 2.8 ND ND ND 6.1 1.4 5 15 1 6,810 5,830 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA I NA ND 1.1 ND ND ND TOTAL CHLORMATEDS DETECTED I I NP NP NP I NP I NP I NPI NP I NP I NP I NP 1 5,300 1 3,8371 1,5001 3,500 1 2,8001 4,500 1 227 1 130 1 220 1 65 1 941 1 139 1,0291 3,616 7,036 5,867 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-12 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJ13 Monitoring Well MW-13 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1 97 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 m3rd4th 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 788 2,100 2,900 4,100 2,600 5,100 760 420 1,100 530 356 683 1,420 960 979 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 174 450 480 440 440 690 99 170 110 69 42 81 97 304 211 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP I NP I NP NPI NP I NP I NP NP NP 1.48 1 ND ND ND ND ND ND ND ND ND ND I ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND I ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 3.5 ND ND ND 0.88 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP I ND ND ND ND I ND I ND ND I ND ND 1 —ND ND ND ND ND I ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 1.1 0.62 ND I ND ND 0.79 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 990 1,300 1,000 1,500 230 130 300 200 121 256 241 158 196 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 2.7 ND ND 1.5 ND 0.45 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND I ND ND ND ND ND ND ND ND 0.24 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND I ND I ND ND I ND I ND I ND I ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP I NP I NP NA NA NA NA I NA I NA NA I NA I NA I NA I ND ND I ND ND ND TOTAL CHLORINATEDS IDETECTED NP NP I NP I NP I NPINPI NP I NP I NPINPI NPI 963 1 2,5501 4,370 1 5,8401 4,040 1 7,290 1 1,0891 720 1 1,5101 807 1 — 1,0201 1,7591 1,4221 1,388 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-13 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-14 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2.d 3rd 4th lst 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 231 280 1,100 650 570 510 250 440 320 340 375 377 867 997 968 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 74.9 110 220 160 190 180 120 220 130 170 196 174 396 331 362 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 1.76 ND ND ND ND ND ND ND ND 2.8 ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 3.8 0.79 ND 1.7 ND 1.5 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 140 110 100 90 64 95 77 120 123 91 206 136 158 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.25 1,4-Dichlorobenzene NP NP NP NPTNP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP I NP-1 ]�Tj ;P-1 NPFNP 17P I NP I NA NA I NA I NA I NA I NA I NA I NA NA NA I ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NPI 308 1 390 1 1,4601 920 1 860 1 780 1 434 1 755 1 527 1 637 1 os 642 1 1,471 1 A64 1490 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-14 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-15 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1995 199 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2.d 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 71 45 92 70 71 110 110 90 100 130 171 197 704 194 176 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 2.59 2.4 4.6 2 2.4 2.7 ND ND ND 2.4 3.4 3.7 4.2 3.9 4.0 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.71 0.98 1 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND- ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 2.0 ND ND 5.7 ND 6 ND 4.5 6.3 6.6 8.0 9.4 7.3 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 1.25 ND 2.9 2 1.8 2.5 ND ND ND 3.1 1.3 1.1 1.6 1.2 1 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP ND ND ND ND 1.7 ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND_ ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP Np T NP NP ND ND ND ND ND ND ND ND ND - ND ND ND ND ND ND 11 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA I NA -FNA NA NA NA ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP INPI NP I NPI NP I NP I NP 1 75 1 47 1 102 1 74 1 77 1 121 1 110 1 96 1 100 1 140 182 208 719 209 189 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-15 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-16 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1 95 199 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 65.7 77 180 150 76 190 120 150 200 190 434 245 401 249 180 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 2.66 3.7 5.4 5 5.3 6.8 ND 2.6 ND 4.5 6.6 5.3 8.4 4.9 4.4 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND 0.8 ND 1.5 1.5 1.3 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND -ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 2.7 3.4 4.7 12 ND 8.4 5.1 8 13 9.3 16 11 9 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 1.24 1.6 5.2 4.4 7.1 6.2 ND ND ND 4.1 3.6 ND 3.4 1.8 1.2 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP _NP I NP NP NP N NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP Np NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP _LNPL�Ny NP I NP NP NP NA NA NA NA I NA I NA NA NA I NA NA ND ND ND ND TOTAL CHLOMNATEDS DETECTED I NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP 1 70 1 82 1 193 1 162 1 93 1 215 1 120 1 161 1 205 207 45's 260 431 268 196 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-16 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-17 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 19 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 m3rd4th 2nd 3rd 4th Ist 2nd 3rd 4th 1st 2.d 2.d 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 320 410 430 82 78 29 52 82 54 100 17 24 18 7.5 1.0 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 36 86 54 35 27 13 14 20 11 13 8.2 7.2 4.3 3.4 1.0 Chloroform NP NP NP NP NP NP NP NP NP NP NP 0.36 ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 5.68 12 12 17 14 to 8.6 5 1.6 3.2 2.7 5.9 7.9 7.6 7.3 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NPI NP ND ND I ND ND ND ND ND ND ND ND ND ND I ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 150 64 41 47 43 37 23 33 33 39 18 16 12 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NPI NP I NP NP NP NP ND ND ND ND ND ND ND I ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP I NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP I NP NA NA I NA NA NA NA NA NA NA NA ND ND ND ND I ND TOTAL CHLORINATEDS DETECTED I NP NP NP NP NP NP NP NP I NP I NP I NPI 362 15081 646 1 198 1 160 1 99 1 118 1 144 1 90 1 149 1 62 48 34 1 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-17 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-18 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1995 1 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2.d 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.7 1.1 0.7 ND ND 277 7.1 1.8 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND 0.53 ND ND 0.9 ND 1.3 1.5 1.6 1.4 1.1 4.3 0.7 0.9 Chloroform NP NP NP NP NP NP NP NP NP NP NP 21.5 20 20 14 10 11 4.0 3.9 2.7 2 1.1 1.2 1.5 1.4 1.6 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND 0.98 ND ND Trichlorofluoromethane NP, NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP Np NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND D ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP !N" NP rN" NP NP ND ND ND ND ND ND D ND ND ND ND 1,1,1,2-Tetrachloroetbone NP NP -1-113 NP NIP NP NP P P NP NW VA I 1� D ND ND ND ND TOTAL CHLOMNATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NP I NP I NP I NP 1 22 1 20 1 21 1 14 1 10 1 12 1 4.0 1 5.9 1 5.3 1 4.3 1 2.5 2.3 284 9.2 4.3 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-18 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-19 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1995 1 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2.d 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 8 5 13 16 7.7 16.0 19.0 NP NP NP NP NP NP NP NP Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND 1.1 2 0.58 1.10 1.60 NP NP NP NP NP NP NP NP Chloroform NP NP NP NP NP NP NP NP NP NP NP 1.51 1.1 3.3 4.1 3.3 6.8 5.9 NP NP NP NP NP NP NP NP Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND —ND ND ND NP NP NP NP NP NP NP NP 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 6 6.1 1.7 4.7 5.6 NP NP NP NP NP NP NP NP Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,2-Dichloropropane NP NP NP NP NP Np NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP P 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NP NP NP NP NP NP NP NP TOTAL CHLOMNATEDS DETECTED I NP NP NP I NP I NP INPI NP I NP I NP I NP I NP 1 10 1 6 1 23 1 28 1 13 1 29 1 32 1 NP I NP I NP I NP NP NP NP NP Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-19 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-20 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1 95 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2.d 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.59 0.72 ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA I ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP_ NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA, NA NA NA NA NA NA NA ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP NP NP I NP I NP I NPI NP I NP I NP I NPI NP I ND IND I ND I ND I ND I ND I ND I ND I ND I ND ND ND 0.59 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-20 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-21 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1995 199 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2.d 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND 1.5 0.64 ND 0.81 1.5 1 1.4 ND 1.1 0.81 ND 1.0 0.88 — 0.66 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND_ ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP- NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND D ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP �NPtNP NP NP NP ND ND ND I�D ND ND xTn I xTr-% D ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NA -A -A XT A D ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP NP I NP NP NP NP NP NP I NP NP I NP I ND IND 1 1.5 1 0.6 1 ND 0.9 1.5 1 1.4 ND 1.1 0.8 ND Lo 0.88 0.66 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-21 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-22 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1995 199 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2.d 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND — ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND_ ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND_ ND ND ND I ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND— ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP N"P NP JINP NP NP NP NP NP NP ND ND ND ND ND �11)1 ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP_ NP NP ND ND ND ND_ ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLOMNATEDS DETECTED I NP NP NP I NP I NP I NPI NP I NP I NP I NPI NP I ND I NDI ND I ND I ND I ND I ND I ND I ND I ND I ND ND ND_ ND ND Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-22 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-23 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1995 1 97 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 m3rd4th 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 490 1,300 1,500 910 690 520 290 150 83 79 174 36 124 143 83 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 16.1 42 72 56 56 29 15 12 6.6 6.3 18.8 2.9 7.6 6.8 4.7 Chloroform NP NP NP NP NP- NP NP -NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP I NP I NP NPI NP I NP I NP NP I NP 0.25 1 ND ND ND ND ND ND ND ND ND ND I ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP I NP I NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND I ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND 10 ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 190 160 96 120 60 30 16 15 42 5.8 15 12 7 Trichlorofluoromethane NP NP NP I NP I NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP I NP I NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND _ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NPINPINPINPINP NP NPI NP I NA NA NA+NA I NA NA NA I NA � NDA I NA ND I ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP NP NP I NP I NP I NPI NP I NP I NPINPI NPI 506 1 1,3521 1,7621 1,1261 842 1 669 1 365 1 192 1 106 1 100 1 234 1 45 147 162 95 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-23 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-24 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1 95 199 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2.d 3rd 4th Ist 2.d 3rd 4th Ist 2nd 2nd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant .3rd Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 930 550 360 230 120 120 54 17 NS NS 33 72 430 243 476 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 3.67 ND ND ND ND ND ND ND NS NS 0.82 1.1 2.7 6.2 3.0— Chloroform NP NP NP NP NP NP NP NP NP NP NP 6.07 ND ND ND ND ND ND ND NS NS ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND I ND ND ND_ ND ND ND ND NS NS ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND_ ND ND ND ND NS NS ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND -ND ND ND ND ND ND ND NS NS ND ND ND_ ND ND Cis 1,2-Dichloroethene NP NP NP P NP NP NP NP I NP NP NP NP NP NA NA ND 7.1 ND ND ND ND NS NS 0.72 ND 2.0 1.4 6.8 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 3.84 ND ND ND ND ND ND ND NS NS ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND ND Chlorobenzene NP NP NP N"P NP JINP NP NP NP NP NP NP ND ND ND ND ND D ND ND NS NS ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP_ NP NP ND ND ND ND ND :L �ND ND ND NS NS ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NA I NA NA NA NA I NA NA NA NS NS ND ND ND ND ND TOTAL CHLOMNATEDS DETECTED I NPI NPI NP I NPI NP INPI NP I NP I NP I NP I NP 1 944 1 550 1 360 1 237 1 120 1 120 1 54 1 17 1 NS I NS 1 35 73 435 251 486 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; well was compromised, to be repaired in 2005. MW-24 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-25 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 993 1994 1 95 199 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 400 450 750 670 650 1,000 1,100 NP NP NP NP NP NP NP NP Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 80.6 88 130 170 140 190 270 NP NP NP NP NP NP NP NP Chloroform NP NP NP NP NP NP NP NP NP NP NP 0.43 ND ND ND ND ND ND NP NP NP I NP NP NP NP NP Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND 11 ND ND NP NP NP NP NP NP NP NP 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND NDJ NP NP NP NP NP NP NP NP Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 38 ND 38 100 71 NP NP NP NP NP NP NP NP Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND, ND ND ND ND ND NP NP NP NP NP NP NP NP_ 1,2-Dichloropropane NP NP NP NP NP Np NP NP NP NP 2.14 5.8 ND ND ND ND ND NP NP NP NP NP NP NP NP Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP NP 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NP NP N- NP NP NP NP NP TOTAL CHLOMNATEDS DETECTED I NP I NPI NP I NP I NP INPI NP I NP I NP I NP I NP 1 483 15441 918 1 840 1 839 1 1,2901 1,441 1 NP I NP I NP I NP NP NP NP NP Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-25 Prepared by: AWA 1022-34 Andres: Historical Well Tables 2012.xls Checked by: TJB Monitoring Well MW-26 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.62 1.60 0.70 ND 0.51 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP 12 9.9 7.6 7.7 4.8 4.3 2.7 ND 3.7 3.3 2.9 3.2 2.3 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP N ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropanc P NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND _ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA ND ND ND ND ND TOTAL CHLOFINATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NPI NP I NP I NP I NP I NP 1 12 1 10 1 7.6 1 7.7 1 4.8 1 4.3 1 2.7 1 ND 1 4.3 4.9 3.6 3.2 2.8 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NM-26 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Recovery Well RW-I Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1 91 1993 1994 1 95 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th Ist 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP 26,000 25,000 38,000 26,000 22,000 27,000 34,000 24,000 16,000 13,900 5,400 39,000 14,000 7,800 10,000 10,000 10,000 4,900 3,510 16,000 8,330 19,800 2,010 1,110 Trichloroethene NP NP 1,400 960 ND 700 920 870 1,200 1,400 1,200 924 1,400 7,100 1,100 640 530 ND 330 240 203 365 233 179 2,610 623 Chloroform NP NP ND ND ND 16 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.1 ND ND ND ND Vinyl Chloride NP NP ND 95 ND ND 38 49 ND ND ND ND ND 100 ND ND ND ND ND ND 3 ND ND ND ND 100 1, 1, 1 -Trichloroethane NP NP ND ND ND 12 ND NE) ND ND ND ND ND ND I ND NE) I ND I NE) ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND ND ND ND I ND 2 ND ND ND ND ND I,I-Dichloroethene NP NP ND ND ND ND ND 4.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9 1,2-Dichloroethane NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP ND ND ND 6 13 9 ND ND ND ND ND ND ND ND ND ND ND ND 3 3.3 ND ND 53 49 Cis 1,2-Dichloroethene NP NP NA NA NA NA NA NA NA NA NA NA NA 9,700 4,100 1,400 1,400 810 1,300 590 1 594 417 293 1 168 7,610 15,2001 Trichlorofluoromethane NP NP ND ND ND ND ND 12 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NPINPI -ND ND ND I ND ND ND NE) ND ND ND ND ND ND ND LD LD NE) ND 3 4.9 ND ND ND ND 1,4-Dichlorobenzene NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.0 ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP I NP I NA NA NA NA NA NA NA NA NA XTA NA ND ND ND ND TOTAL CHLORINATEDS IDETECTED NPI NP 127,400 126,055 138,000 126,734 122,971 127,947 135,200 125,400 1 17,200 1 14,8241 6,800 155,900 1 19,200 1 9,840 1 11,930 1 10,810 1 11,630 15,730 14,318 116,8021 8,856 120,147112,283117,0911 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit NA - Data not available. NP = Well not present at time of sampling RW-1 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.yJs Checked by: TJB Recovery Well RW-2 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 1993 1994 1 5 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 M 2.d 3rd 4th Ist 2.d 3rd 4th lst 2nd 3rd 3rd 4th 4th' 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP 1,400 2,800 740 1,800 900 1,990 2,500 930 2,000 1,700 1,700 1,200 260 99 110 76.7 AB AB AB AB Trichloroethene — NP NP NP NP NP NP 91 290 330 95 ND 165 260 54 370 280 280 190 20 4.7 12 3.6 AB AB AB AB Chloroform NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB — AB Vinyl Chloride NPI NP NP NPI NP NPI ND 1 9.2 1 ND ND I ND I ND ND 99 ND ND I ND ND ND ND 3.1 ND AB AB AB AB 1, 1, 1 -Trichloroethane NP NP NP NP NP NP ND ND ND ND ND ND NO ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1,2-Trichloroethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND— ND NO ND ND ND ND AB AB AB AB 1, 1 -Dichloroethene NP NP NP NP NP NP ND 0.73 ND ND ND ND ND ND ND ND ND ND ND ND 3.6 ND AB AB AB AB 1,2-Dichloroethane NP NP- NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB Trans 1,2-Dichloroethene NP NP NP NP NP NP ND 3.3 ND I ND ND ND ND ND ND ND ND I ND ND ND ND ND AB AB AB AB Cis 1,2-Dichloroethene NP NP NP NP I NP NPI NA I NA NA NA NA NA NA 420 480 210 230 140 42 44 210 5.9 AB AB AB AB Trichlornfluoromethane NPI NP_. NP NP NP NP NO ND ND ND ND I ND NO NO ND ND NO NO ND NO ND NO AB AB AB AB 1,2-Dichloropropane NP NP NP NP NP NP ND ND ND ND ND ND I ND ND ND ND ND ND ND ND ND ND AB AB AB AB Chlorobenzene NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB AB 1,4-Dichlorobenzene NP NP NP NP NP NP ND ND ND ND ND ND NO ND ND ND ND ND ND ND ND ND AB AB AB AB 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NA NA I NA NA NA NA NA NA NA NA I NA NA NA NA NA ND AB AB AB AB TOTAL CHLORINATEDS DETECTED I NP I NP I NP I NPI NP I NP 11,49113,10311,07011,8951 900 12,155 12,760 1 1,503 12,850 1 2,19012,2101 1,5301 322 1 148 1 339 1 86 AB AB AB AB_ Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit NA = Data not available. NP = Well not present at time of sampling RW-2 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well RW-3 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 1991 993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 1 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP 8,000 1,700 1,500 4,400 4,200 2,400 6,400 2,500 4,060 12,100 10,700 132 3 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND 15 ND 8.2 ND ND 35 89 369 43.8 ND 71.3 1.4 Chlorofmm NP NP NP NP NP NP NP NP NP NP NP NP NP ND 3.7 ND 1.5 ND ND ND 1.3 1.3 ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND 40 11.9 1,1,1-Trichloroethane NP NP _NP NP NP NP NP NP NP NP NP NP NP N ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP I NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.79 ND ND ND ND 1, 1 -Dichloroethene, NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 1.7 ND ND 14.7 0.87 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.97 ND ND ND 4.1 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND 18 ND 16 ND ND 51 120 992 59.8 1 ND 9,290 1,440 Trichloroflumomethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropanc NP NP P NP NP NP NP NP NP NP NP NP N ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.27 1,4-Dichlorobenzene NP NP NP NP NP NP NP *NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tefxachloroethane NP NP NP NP NP NP NP NP NP NP NP NP NA XT A NA NA NA — N� NA 1.2 ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NP I NP I NPI NP I NPI NP I NP I NP I NP I NP 1 8,0001 1,7371 1,500 1 4,426 1 4,200 1 2,400 1 6,486 1 2,710 1 5,427 1 12,2041 10,7001 9,548 1 1,461 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-3 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well RW-4 Concentrations in Parts per Billion (lAg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 1993 1994 1 5 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th lst 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 4,000 1,000 1,200 3,000 1,900 640 610 3,050 AB AB AB AB_ Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 320 250 79 240 170 56 50 167 AB AB AB AB Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 22 ND AB AB AB AB 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 0.53 ND ND ND ND ND ND AB AB AB AB 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB Trans 1,2-Dichloroethene NP NP NP NP NP NP. NP NP NP NP NP NP NP NP NP ND 11 ND ND ND ND 1.8 4.4 AB AB AB AB Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 600 470 310 810 470 170 240 307 AB AB AB AB Trichlorofluoromethane NP NP NP NP NP NP- NP NP NP NP NP NP NP NP NP ND 1.1 ND ND ND ND ND ND AB AB AB AB 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.79 AB AB AB AB_ 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND AB AB AB AB ,1,1,1,2-Tetrachloro d NP NP NP NP NP NP NP NP NP NP NP NP NP NA NA NA , NA NA NA NA 1.0 AB AB AB AB TOTAL CHLORINATEDS i DETECTED I NP I NP I NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 4,920 1 1,733 1 1,5891 4,050 1 2,540 1 866 1 924 1 3,530 AB I AB I AB A ND = Not Detected at the method detection limit. AB = Well abandoned. NP = Well not present at time of sampling. RW-4 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well RW-5 Concentrations in Parts per Billion (lAg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 1993 1994 1 5 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th lst 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 5,000 1,300 4,200 1,200 2,100 2,100 1,300 4,500 1,030 2,710 74 ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 560 410 430 82 170 160 130 240 58 140 70 ND Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.54 ND ND I ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 1.1 ND ND 14 ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 1.1 ND ND ND ND ND 0.5 ND ND 1.5 ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 12 ND ND ND ND 2.6 7 ND ND 14.7 ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 770 850 1400 300 540 470 340 541 349 233 1,760 58 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 3.3 ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 1.2 ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroed NP NP NP NP NP NP, NP NP NP NP NP NP NP NP NP NA NA NA NA NA NA NA 1.7 ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 6,330 1 2,576 1 6,030 1 1,582 1 2,810 1 2,730 1 1,773 1 5,293 1,437 3,083 1,934 59 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-5 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well RW-6 Concentrations in Parts per Billion (lAg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 1993 1994 1 5 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th lst 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 2,500 1,900 3,000 2,300 1,500 4,300 740 1,880 2,250 1,810 1,120 168 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 260 320 290 200 150 190 73 169 98 82 262 45 Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 1.8 ND ND ND ND ND ND ND ND ND 73.2 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND 1.4 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP. NP NP NP NP NP NP NP NP NP ND 3.5 ND ND ND ND ND 4 ND ND 4.9 2.6 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 570 640 1,000 610 460 140 440 346 279 170 750 308 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.55 ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroetba-- NP NP NP NP NP NP, NP NP NP NP, NP NP NP NP NP NA , NA NA NA I NA NA NA ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 3,330 1 2,865 1 4,290 1 3,110 1 2,110 1 4,630 1 1,253 1 2,400 1 2,627 1 2,062 2,137—r598 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-6 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Monitoring Well RW-7 Concentrations in Parts per Billion (lAg/1) Andrex Industries Asheville, North Carolina BLE Job Number J12-1022-34 Yearly Quarter 19 1 1993 1994 1 5 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2012 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th lst 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 2,300 1,300 2,200 2,300 2,100 1,700 700 855 2,090 2,880 107 41 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 250 220 400 300 280 200 98 95 104 158 10 8 Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND 11.1 1.2 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 13 1 ND ND ND ND ND ND ND ND ND 12.6 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP. NP NP NP NP NP NP NP NP NP ND 6.6 ND ND ND ND ND 2.3 ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 450 410 1,100 810 640 460 260 188 219 345 71.1 612 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 4.2 ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroeth... NP NP NP NP NP NP, NP NP NP NP, NP NP NP NP NP NA NA NA NA NA NA NA ND ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 3,000 1 1,954 1 3,700 1 3,410 1 3,020 1 2,360 1 1,058 1 1,141 2,413 3,383#200 675 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-7 Prepared by: AWA 1022-34 Andrex Historical Well Tables 2012.xls Checked by: TJB Hm 9,000 8,000 7,000 6,000 5,000 4,000 3,000 2,000 1,000 Total Chlorinated VOC Concentrations in MW-1 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 m It kf) 00 01� C) — (14 M It kn �O r­ 00 cl� C) M 1:? 91 1:? 1� C: C C i , Month -Year 111 OEEMOWY Lai Total Chlorinated VOC Concentrations in MW-2 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 EM 700 ME 500 400 300 200 100 0 ! i i i i i i i i i i i i - i -i - i i i i i i i 01� C) rq m 't W) 110 1­ 00 011 C) — rq m It kn 110 rl- 00 C� �!9111F'1]111i' I 1111mdll Month -Year 20,000 18,000 16,000 14,000 12,000 10,000 8,000 6,000 2,000 0 � — 1- Total Chlorinated VOC Concentrations in MW-3 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 ,It W) �10 r__ 00 01� C) m 't �10 I­ C� a) a) a� a� a) a) C� C� a) a) C� C� a) a) Month -Year Total Chlorinated VOC Concentrations in MW-4 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 1,800 1,600 1,400 1,200 1,000 800 600 400 200 C" C) m It kn 00 C� C) m IZI- W') r--- 00 m 0? 1�1 1�1 1�1 1�1 1�1 1�1 1�1 1�1 1�1 1�1 1:? 91 1 11, 111 ��h_ �99=� Month -Year 60,000 50,000 40,000 30,000 C-) 20,000 10,000 0 0? Total Chlorinated VOC Concentrations in MW-5 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 C14 rn It kn 17- 00 C� C) — N M 1�t V) 1�0 1:? 91 1:? 91 1�1 1� 1:? I 111 1; 1111 1 11 11111111 Month -Year 17— 00 cl� 1:? 91 ��_ �_ �'d 50,000 45,000 FA[l](1111111 35,000 30,000 25,000 cd 20,000 (-) 15,000 10,000 5,000 lel�g Total Chlorinated VOC Concentrations in MW-6 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 It rl- 00 (71, C) N m It W) 110 rl- Month-Year 200 180 160 K"It, 120 100 80 60 Ell] Total Chlorinated VOC Concentrations in MW-7 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 rq m It —5 1 � 1 1 1 � I � I NINE 1 1 1 1 � 1 1 NINE I I I � I I � I I IN! I � I 110111i, I 1111mdll Month -Year mm 1,600 1,400 1,200 1,000 800 600 ROTOR K11111 0 4- m Total Chlorinated VOC Concentrations in MW-8 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 rq m It Ln 00 CIA m 't V) 110 Month -Year 7,000 6,000 5,000 4,000 ZE 3,000 Lail 2,000 1,000 01� C� Total Chlorinated VOC Concentrations in MW-8A 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 m kn 00 C) — C14 m :I- kr) 1�0 r­ 00 C� C) m 1:? 9, 91 91 91 91 91 91 91 1:? Month -Year Lei, 7,000 6,000 5,000 4,000 3,000 2,000 1,000 N!WNWNWNWI� Total Chlorinated VOC Concentrations in MW-9 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 It W) 110 r- 00 01� C) CIA fn 't W) 110 Month -Year I!!q Lail 14,000 12,000 10,000 8,000 6,000 4,000 2,000 a,\ 0? Total Chlorinated VOC Concentrations in MW-10 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 C14 rn It kn 00 C� C) — N rn Zt kn 1�0 r­ 00 C" 1:? 91 91 91 91 1� 91 91 1:? 91 Month -Year 6,000 5,000 4,000 3,000 2,000 1,000 0 4- m Total Chlorinated VOC Concentrations in MW-11 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 Month -Year Lei, Total Chlorinated VOC Concentrations in MW-12 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 8,000 7,000 6,000 5,000 4,000 .3 UUU 2,000 1,000 0 C� C) (14 't kf) �10 rl- 00 C� C) Cq m 't W') 10 r- 00 (71, C) Month -Year 8,000 7,000 6,000 5,000 4,000 3,000 2,000 1,000 0 4- cl� C� Total Chlorinated VOC Concentrations in MW-13 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 m kn 00 0� C) — C14 m I- kr) ��O C�' 91 C? 1:? 1:? 91 91 1:? Month -Year r­ 00 m M 1,600 1,400 1,200 1,000 800 600 Hirt, KBE 0 m Total Chlorinated VOC Concentrations in MW-14 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 't V) 110 rl- Month-Year Lail Total Chlorinated VOC Concentrations in MW-15 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 EM F11111 R11111 500 400 300 200 0 ! i i i i i i i i i i i i i i i i i i i i i i i 01� C) m It kr) 00 0� C) — C14 m IZI- kn 1�0 r--- 00 C� m 1:? 91 1:? 1:? 91 91 91 91 91 91 Month -Year Total Chlorinated VOC Concentrations in MW-16 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 500 450 400 350 300 250 200 (_� 150 �111j' 50 0 01� C) N fn It W) �10 1­ 00 (71, a) (14 m 't kn 110 rl- Month-Year Total Chlorinated VOC Concentrations in MW-17 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 700 600 500 9 400 Lail 300 200 [till] 0 C" C) C14 rn I:t kn 00 m kr) 00 00 C� C" C" C� C� C� cl� C" C) C) C) C) C) C) C) C) C) I Month -Year Total Chlorinated VOC Concentrations in MW-18 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 300 250 200 150 100 50 0 ! i i i i i i i i i i i i 2R7_= ; - I I I i i �� i C� C) N m I:t W') 110 r­ 00 (7\ C) N rn It kn 110 r- 00 m 1:? 91 91 91 91 91 91 91 91 Month -Year 35 30 25 20 15 to 5 Total Chlorinated VOC Concentrations in MW-19 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 't r__ 00 01� C) N rl- Month-Year Total Chlorinated VOC Concentrations in MW-20 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 0.80 0.70 0.60 0.50 0.40 0.30 0.20 0.10 0.00 i i i i i i * * i 0 V V *i 01 4 4 i i * i 0 01� C14 rn It W') 110 r­ 00 0� C) — (14 rn �t kn 1,0 00 Cl� 91 91 91 91 91 1:? 1� 1:? 1:? Month -Year Total Chlorinated VOC Concentrations in MW-21 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 1.60 11 U11111 1.20 1.00 0.80 0.60 =DA 0.20 0.00 i i i ! *6 ! i i 4! w i i i i \4( i i m It W) �10 1­ 00 �10 r__ Oc C7*) m Imal Month -Year Total Chlorinated VOC Concentrations in MW-22 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 1.00 0.90 0.80 0.70 0.60 0.50 0.40 0.30 0.20 0.10 0.00 Month -Year 2,000 1,800 1,600 1,400 1,200 1,000 800 600 L"I 200 0 19 Total Chlorinated VOC Concentrations in MW-23 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 't tn 110 r__ 00 C� C) CIA m It V) 110 rl- Month -Year 00 CIA Total Chlorinated VOC Concentrations in MW-24 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 1,000 900 800 700 600 500 400 300 200 100 0 01� C) C14 m 't W) 110 1­ 00 01� C) C14 m 00 Month -Year Lail 1,600 1,400 1,200 1,000 800 600 400 200 0 4- Total Chlorinated VOC Concentrations in MW-25 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 W) 110 r__ 00 C� a) CIA M It kn 110 rl- Month-Year 14 12 to 8 6 4 2 Total Chlorinated VOC Concentrations in MW-26 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 N It tn 110 rl- 00 01� C) rq m 't V) 110 1­ 91 91 91 91 91 91 1�1 91 91 91 91 1�1 91 91 91 Month -Year 60,000 50,000 40,000 30,000 20,000 10,000 0 Total Chlorinated VOC Concentrations in RW-1 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 C) 't W) Month -Year Lail 3,500 3,000 2,500 2,000 1,500 1,000 500 0 m Total Chlorinated VOC Concentrations in RW-2 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 W) 110 r__ 00 C� C) M 't kn 110 rl- 00 Month -Year A 14,000 12,000 10,000 8,000 6,000 4,000 MILO 0 cl� C� Total Chlorinated VOC Concentrations in RW-3 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 m kn 1�0 r­ 00 C� C) — m I- kn 1�0 r­ 00 C� C) m C�' C? 91 91 91 91 91 91 91 91 1:? Month -Year 6,000 5,000 4,000 3,000 C-) 2,000 1,000 0 Total Chlorinated VOC Concentrations in RW-4 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 r­ 00 C� C) — C14 1�1 91 91 1:? Month -Year m kn r- 00 01� m 1:? 91 7,000 6,000 5,000 4,000 3,000 2,000 1,000 0 Total Chlorinated VOC Concentrations in RW-5 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 C� a) C� Month -Year - - - - - - - - - - �g 5,000 4,500 Om 3,500 3,000 2,500 2,000 1,500 1,000 500 0 Total Chlorinated VOC Concentrations in RW-6 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 C) rq fn 't tn 110 r__ 00 01� C) — CIA fn It kn 110 r__ 00 CIA Month -Year Le 4,000 3,500 3,000 2,500 2,000 1,500 1,000 500 0 i i i i i _+_ C" C) C14 ""', 0? Total Chlorinated VOC Concentrations in RW-7 3rd Quarter 1991 - 3rd Quarter 2012 Andrex Industries, Asheville, NC BLE Job No. J12-1022-34 r­ 00 0� C) — N rn I:t 1:? 91 91 91 91 Month -Year kf) 00 m