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WI0100106_Annual Report_20120220
MIL13 BUNNELL-LAMMONS ENGINEERING, INC. GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS REPORT OF ANNUAL GROUNDWATER AND SURFACE WATER SAMPLING AND ANALYSIS FOR 2011 FORMER ANDREX INDUSTRIES CORP. 180 DEAVERVIEw ROAD ASHEVILLE, NORTH CAROLINA BROWNFIELDS PROJECT NUMBER 07022-03-11 PREPARED FOR: ANDREX INDUSTRIES CORP. ASHEVILLE, NORTH CAROLINA 0 I�A CA% Z,/, PREPARED BY: th 41- BUNNELL-LAMMONs ENGINEERING, INC. �%SaL I all 0 0 2134 !-T GREENVILLE, SOUTH CAROLINA % OLOG X-0% % z FEBRUARY 20,2012 BLE PROJECT NUMBER Jl 1-1022-32 IHSB ID NUMBER NONCDO001271 GROUNDWATER INCIDENT NUMBER 6586 CAR 1 5 TO a- LO w 11P6111100 NILE BUNNELL-LAMMONS ENGINEERING, INC. GEOTECHNICAL, ENVIRONMENTAL AND CONSTRUCTION MATERIALS CONSULTANTS February 20, 2012 Andrex Industries Corp. C/O The Van Winkle Law Firm 11 North Market Street Asheville, NC 28801 Attention: Mr. Mark Pinkston, PA Subject: Report of Annual Groundwater and Surface Water Sampling and Analysis for 2011 Former Andrex Industries Corp. 180 Deaverview Road Asheville, North Carolina BLE Project Number J1 1-1022-32 Brownfields Project Number 07022-03-11 11-ISB ID Number NONCDOOO 1271 NCDENR Groundwater Incident Number 6586 Dear Mr. Pinkston: As authorized by Andrex Industries Corp. acceptance of our proposal number P1 1-0453 dated August 9, 2011, Bunnell-Lammons Engineering, Inc. (BLE) has performed required envirom-nental services at the subject site. The purpose of this project was to collect and analyze groundwater and surface water samples as required by the North Carolina Brownfields Program. The enclosed report describes the work performed and presents the results obtained. Project Information: The following information was obtained from our previous work at the Andrex site (1991 through present) and from our conversations and emails with Mr. Buddy Gaither and Mr. Jack Levins of Milkco, Inc., Mr. Drew Stahlman, Mr. Stephen Gilman, and Mr. Mark Davies of Stahlman Consulting, and Mr. Daniel Stiles of EAS Professionals, Inc. Andrex formerly owned and operated an industrial textile production facility located at 180 Deaverview Road within the city limits of Asheville, North Carolina (Figure 1). The company operated a knitted fabric weaving and cutting business for women's and children's clothing at this location. In prior years, the facility was operated as a textile finishing business that conducted cutting, dry cleaning, shrinking and packaging of fabrics. The subject facility was in operation since the mid 1960s, although under various ownership. A two-story light manufacturing facility with approximately 77,000 square feet of office, manufacturing, warehouse, storage and utility space occupied the approximately nine -acre site. Two buildings were present at the site; a split level brick building and slab -on -grade metal building. No dry cleaning has been conducted on site since 1995. However, prior to 1995, dry cleaning operations were prevalent on site and the use of tetrachloroethylene (a.k.a. Perchloroethylene, PCE) 6004 PONDERS COURT PHONE (864) 288-1265 GREENVILLE, SOUTH CAROLINA 29615 FAx (864) 288-4430 MILE Androc Industries — 2011 Groundwater Monitoring February 20, 2012 Asheville, NC BLE Project Number J11-1022-32 was common. Virgin PCE was stored on site in a 6,000-gallon underground storage tank (UST). Prior to 1989, the use of the PCE UST was discontinued and the tank was filled with sand. The UST was replaced with a 6,000-gallon AST which was used until 1995. In 1995, dry cleaning processes and the use of PCE were discontinued. In 1991 concentrations of PCE were detected in the groundwater above the applicable North Carolina Title 15A Subchapter 2L (NC2L) groundwater standards' maximum level of 0.7 gg/l and the NCDENR issued Groundwater Incident Number 6586 for the site. Concentrations of PCE were also documented in the soil near the PCE UST and at other subsurface facility locations. The NCDENR approved a comprehensive site assessment (CSA) and corrective action plan (CAP) for the site and remedial efforts were conducted from 1993 through 2005. Remedial efforts consisted of the installation and operation of two groundwater pump and treat (P&T) systems and one soil vapor extraction (SVE) system. The SVE and both groundwater P&T systems were operated and maintained by BLE for Andrex. from May 2003 through August 2005. Treated groundwater effluent was discharged to the sanitary sewer under a MSD permit. BLE also performed annual site -wide groundwater and surface water sampling and analysis for Andrex to monitor the fate of the groundwater plume. BLE submitted quarterly reports of the remedial progress through August 2005 and annual groundwater monitoring reports through 2005 to the NCDENR to document site activities. The remediation system operations were suspended in August 2005 at the discretion of the property owner. Annual groundwater monitoring was also suspended at the discretion of the property owner, with the last sampling event conducted in November 2005. In early 2005, Andrex requested that BLE evaluate feasible remedial alternatives for the site. A preliminary review of alternate remedial technologies identified a unique opportunity to evaluate bioremediation at the site. Food -grade lactate containing byproducts (milk solution) from the neighboring Milkco, Inc. (Milkco) facility were being considered for use as a bio-enhancing remedial product for the former Andrex. facility. The implementation of this type of remedial action is dependent upon the results of a feasibility study which includes bench and field testing studies of the lactate containing byproducts. In 2005, Andrex retained BLE to perform a pilot study of the milk byproducts. The study was to include two parts. The first part was a bench test which was to be followed by a field trial. BLE completed the bench study in early 2006. The results showed a net decrease in PCE concentration of 30% after 40 days in those microcosms containing the highest concentrations of milk solution. Significant concentrations of PCE daughter products were also produced in the bench study indicating successful de -chlorination of the parent product, as anticipated. The field trial portion of the pilot test was suspended by Andrex after the bench test results were obtained. In 2006, Milkco entered into a Brownfield's Agreement (Agreement) with the State of North Carolina as part of a potential purchase of the Andrex property. The property was sold in 2007 and as part of the plan (see below) for retrofit of the subject site; Milkco removed and/or demolished selected equipment and facility infrastructure. MILE Androc Industries — 2011 Groundwater Monitoring February 20, 2012 Asheville, NC BLE Project Number J11-1022-32 In August 2007, three underground storage tanks (one PCE and two heating oil) were removed and disposed by a contractor retained by Milkco on behalf of Andrex. The results of the activities were documented in a report titled Report of Limited Assessment for UST Closure dated November 26, 2007 (BLE Project No. J07-1022-20). As part of Milkco's redevelopment plans for the site, BLE issued a plan titled Work Plan for Redevelopment of the Andrex Brownfields Site (Milkco Cooler Expansion) dated June 13, 2008 (BLE Project No. J08-1022-23). The plan addressed the Program's requirements including excavation and disposal of contaminated soil (source area) and continued groundwater monitoring. The Program reviewed and approved (with modification) the plan in a letter to BLE dated July 7, 2008. The schedule for implementation of the redevelopment plan was changed on December 11, 2008 with concurrence of the Program. In July 2008, BLE abandoned selected groundwater monitoring and recovery wells in accordance with the approved redevelopment plan. The results of the well abandonment activities were documented in a report titled Report of Well Abandonment Services for the Milkco Cooler Expansion dated January 19, 2009 (BLE Project No. J08-1022-26). From July through September 2008, contaminated soils were removed and disposed by a contractor retained by Milkco in accordance with the approved redevelopment plan. The results of the remedial activities were documented in a report titled Report of Hotspot Soil Removal and Disposal for the Milkco Cooler Expansion dated June 3, 2009 (BLE Project No. J08-1022-25). By December 2008, the former Andrex brick building(s) and metal building had been demolished with only the building slabs remaining. Additionally, all groundwater and soil rernediation systems had been dismantled, removed, and stored by Milkco. All work performed by Milkco (non - responsible party) is in compliance with the requirements of the NCDENR Brownfields Program (Program) and the Agreement. In February 2008, Andrex resumed annual groundwater monitoring at the site. BLE has performed the sampling services and prepared and submitted reports each calendar year since 2008. The approved redevelopment plan requires the continuation of annual groundwater monitoring and remedial activities at the site. BLE has completed the required annual groundwater monitoring for the 2011 calendar year. The enclosed report describes the work performed and presents the results obtained as required in the approved redevelopment plan (et seq.). IBLIH Androc Industries — 2011 Groundwater Monitoring February 20, 2012 Asheville, NC BLE Project Number J11-1022-32 Scope of Services: On September 21, 2011, groundwater levels were measured and on September 21-23, 2011 samples were collected from the monitoring and recovery wells, as required. Groundwater sampling logs are included in Appendix A. Samples were collected from all wells except MW-1 through MW-4, MW-8, MW-8A, MW- 19, MW-25, RW-2, and RW-4 as these wells were not present at the time of sampling (abandoned or destroyed). Samples were also collected from affected surface waters on September 28, 2011. The samples were analyzed at Pace Analytical Services, hic. (Pace), in Huntersville, North Carolina by EPA Method 8260 MSV Low Level (Appendix B). Water levels and groundwater elevations measured prior to sampling are shown on Table 1. A groundwater elevation contour map is included as Figure 2. Results of Groundwater Sampling: Chlorinated volatile organic compounds (VOCs) detected in the groundwater samples above the North Carolina standards (based on North Carolina's Class GA Groundwater Standards T15A Subchapter 2L) include: tetrachloroethene, trichloroethene, cis- 1,2-dichloroethene, and vinyl chloride (Table 2). A historical contaminant concentration database and total chlorinated VOC data plots are presented in Appendix C. The data plots were visually evaluated and our interpretations of the overall contaminant trends from the initial sampling date of each well are presented below. Declining Stable Increasing Non -Detect MW-l** MW-9 MW-7 MW-20*** MW-2** MW-10 MW-12 MW-21 *** MW-3** MW-11 MW-15 MW-22 MW-4** MW-12 MW-16 MW-5 MW-13 MW-19* T%4W-6 MW-14 MW-25* MW-8** MW-18 RW-3 MW-8A** MW-24 MW-17 MW-26 MW-23 RW-1 R)AT-2** RW-4** RW-5 RW-6 RW-7**** Well destroyed in 2003; not present at the time of the 2009 sampling event. Well abandoned after the 2008 sampling event (see subsequent sections of this report). Detected concentrations of chloroform are unrelated to the groundwater incident. -- Well is broken and filled with roots and milk solution as of September 2011. 11 IBLIH Androc Industries — 2011 Groundwater Monitoring February 20, 2012 Asheville, NC BLE Project Number J11-1022-32 Status of Well Conditions: Monitoring wells MW-19 and MW-25 were destroyed in 2003 and MW-24 was damaged in late 2003 or early 2004. Recall that MW-19 was located on the Satterfield residential property and that MW-24 and MW-25 were located on the Milkco property (Figures 2 and 3). Sampling of monitoring wells MW-19 and MW-25 could not be performed in 2003 and beyond because the wells had been destroyed. Monitoring well MW- 19 appears to have been destroyed by grading in 2003, presumably by the City of Asheville, who graded the area for routing of storm water. The well cap was found on the ground surface but no other parts of the well could be located. Monitoring well MW-25 was destroyed by grading by contractors working for Milkco. The work was part of a facility expansion at Milkco in the summer of 2003. No traces of the well could be located. Neither BLE nor Andrex. was contacted prior the destruction of these wells. The well head of MW-24 was damaged by grading contractors working for Milkco. The work was part of a facility expansion at Milkco in late 2003 or early 2004. BLE personnel observed surface water leaking into the damaged well head and made temporary repairs to stop the infiltration of surface water in 2004. In 2005 the well head was permanently repaired however it appeared that the well riser pipe was bent at about five feet below ground surface at the time the well head was damaged. We were unable to lower a bailer or well pump into MW-24 due to the bent riser pipe. The well was not sampled in 2004 or 2005. We recommended permanent abandonment and replacement of MW-24 in 2005. After approval by the responsible party, BLE completed abandonment and reinstallation of MW-24 in 2007. In the summer of 2008 (after sampling was conducted in February 2008), several of the monitoring and recovery wells were abandoned as part of the property redevelopment plan approved by the Program. A report of well abandom-nent was submitted under separate cover. Monitoring well MW-6 and recovery well RW-1 were extended to the ground surface as part of the grading activities for the Milkco expansion (new roadway). The well heads were reconstructed and the well elevations were resurveyed by BLE. The water level and well construction data on Table I reflects the changes. Please note that the extension of MW-6 resulted in a deviation (bend) of the riser pipe below the ground surface. A bailer cannot be lowered down the well so sampling was performed using a check valve and poly tubing. Purge volumes are significantly reduced using this method compared to conventional bailing. Results of Surface Water Sampling: The laboratory results of the surface water sampling are consistent with previous sampling events. Chlorinated VOCs detected in the surface water samples above the North Carolina standards (based on North Carolina's Class WS Surface Water Standards T 1 5A Subchapter 213) include tetrachloroethene and trichloroethene (Table 2). The former sample location Smith Mill I (SM-1) was collected from a small garden pond on the former Jehovah Witness property prior to 2005. The former pond was filled in by the new owners of the Jehovah Witness property sometime after November 2004. The SM-1 sample location was moved in 2009 to the location shown on Figure 3 based on the 2008 results. 5 MILE Androc Industries — 2011 Groundwater Monitoring February 20, 2012 Asheville, NC BLE Project Number J11-1022-32 A surface water sample QW-1) was collected from the former Jehovah Witness property in 2010 as in prior years (Figure 3). The sample was collected from a drainage feature in an area that appeared to be a spring. The results from this year and prior years (2002 through 2005) indicate that the drainage feature is a groundwater discharge point for northernmost contaminant plume. It is apparent from the data that the discharge at the former Jehovah Witness spring directly affects the surface water quality in Smith Mill Creek Tributary at down gradient sampling locations (SM-4 through SM-6) shown on Figure 3. The sampling locations (SM-1 through SM-6) in Smith Mill Creek Tributary will remain the same in 2012. Sampling of surface water for Total Organic Carbon was performed this year as required in the UIC Permit. These data cannot be compared to pre - injection values since no historical data exists. The laboratory data is included in Appendix B. Remediation Progress: A groundwater pump and treat system (upper system) and a SVE system were installed at the site in the mid 1990's. Groundwater was recovered from two recovery wells RW- 1 and RW-2 attached to the upper system. Upgrades to the groundwater recovery systems were completed in 2002. The upgrades included the addition of one recovery well (RW-3) to the upper system and construction of a new lower system and the installation of four new lower system recovery wells (RW-4 through RW-7). After 2002, contaminated groundwater was recovered by seven recovery wells RW-1 through RW-7. Groundwater recovery from RW-1 through RW-3 (upper system) was restarted on March 25, 2002. Groundwater recovery from RW-4 through RW-7 (lower system) began on May 23, 2002. The system upgrades were documented in a report titled As -Built Engineering Plans and Specification Groundwater Pump and Treat Systems (2002 Upgrade) dated February 5, 2003. Operation of both groundwater systems was discontinued on August 23, 2005 and the funds for operation of the systems were diverted to a laboratory -scale (bench) pilot test of an alternate remedial technology. The bench test was completed in 2006, however reporting of the results was suspended by Andrex while the Brownfields Agreement was in progress. As part of the site redevelopment plan, the results of the bench test and plans for future groundwater remediation were submitted to the Program. The SVE system has not been operational since November 2004 when a power surge (presumed lightning strike) damaged the system. Repairs were not made as Andrex. had proposed a discontinuance of SVE remedial operations to the NCDENR at that time. Repairs were contingent on the initiation of the pilot test described above. Andrex opted to conduct the pilot test and therefore the SVE system was not repaired. In the summer of 2008, as part of the approved redevelopment plan, both groundwater systems and the SVE system we disassembled and the equipment was placed in storage by Milkco. Additionally, as part of the redevelopment plan, "hotspot" soils (contaminated soils with concentrations above a specified limit) were removed and disposed by Milkco on behalf of Andrex. A report of soil removal and disposal was submitted under separate cover. An underground injection control permit was obtained from the NCDWQ on December 22, 2010. The permit was part of a green/sustainable enhanced bioremediation approach utilizing milk solution. M MILE Androc Industries — 2011 Groundwater Monitoring Asheville, NC February 20, 2012 BLE Project Number J11-1022-32 The injection plan included an injection schedule over 5 years with semi-annual injections planned for the first two years. We proposed to conduct the project in phases with the first phase including two injection events (and monitoring) within a 12-month period (designated "Year One" in the plan). BLE was retained by Milkco to perform the injection and monitoring services for year one in 2011. Subsurface injection of milk solution into four former groundwater recovery wells were performed in June 2011 and September 2011 and monitoring was conducted as planned. The results show that daughter products of PCE are being created as anticipated. Based on these data we propose to suspend injections during the first half of 2012 and conduct monitoring to determine the long-term results of the 2011 injections. The first monitoring event is scheduled to be performed in March 2012. An injection project interim evaluation report will be prepared and submitted under separate cover as required in the UIC permit. Qualification of Report: The activities and evaluative approaches used in this assessment are consistent with those normally employed in hydrogeological assessments of this type. Our evaluation of site conditions has been based on our understanding of the site and project information and the data obtained during our annual sampling effort. This report has been prepared on behalf of and exclusively for the use of Andrex Industries Corp. This report and the findings contained herein shall not, in whole or in part, be disseminated or conveyed to any other party or used or relied upon by any other party excluding NCDENR, without BLE's prior written consent. Closing: We appreciate the opportunity to serve as your environtriental. consultant on this project. Please contact us at (864) 288-1265 if you have any questions or comments regarding this report. Sincerely, BuNNELL-LAMMONs ENGINEERING, INC. Benjamin A"PNisbleth, P. G. Staff Geologist Registered, North Carolina #2134 cc: Ms. Tracy Wahl — DWM Brownfields Program Andrew W. 4A1ex/der, P. G. Senior Hydrogeologist Registered, North Carolina #1475 c: lawalactive projects landrex milkcolphase32 gw samp 2011 landrex report of 2011 groundwater 1022-32final.doc 7 TABLES Table 1 Well Construction and Groundwater Elevation Data Andrex Industries Asheville, North Carolina NCDENR Groundwater Incident Number 6586 BLE Project No. Jll-1022-32 September 21, 2011 Well Well Location Meas. Pt. Elevation Gnd. Surface Elevation Depth to Water (bmp) Water Elevation *Total Borehole Depth (bgs) *Screen Depth (bgs) *Screen Elevation Well Well *Top of Rock *Top of Type Monitors Depth(bgs) RockElev. MW-1 On -Site 2222.34 2222.58 NP-A NP-A 46.2 31.2 - 46.2 2191.4 - 2176.4 lIIs BR 35.0 2187.6 MW-2 On -Site 2222.28 2222.62 NP-A NP-A 45.0 28.0 - 43.0 2194.6 - 2179.6 HIS BR 29.0 2193.6 MW-3 On -Site 2210.40 2207.76 NP-A NP-A 55.0 40.0 - 55.0 2167.8 - 2152.8 11 BR 36.5 2171.3 MW-4 On -Site 2206.87 2207.04 NP-A NP-A 86.7 51.7 - 86.7 2155.3 - 2120.3 Ills BR 26.0 2181.0 MW-5 On -Site 2216.75 2216.92 47.30 2169.45 53.0 43.0 - 53.0 2173.9 - 2163.9 Ills BR 37.0 2179.9 MW-6 On -Site 2218.43 2218.67 54.31 2164.12 71.9 50.4 - 70.4 2168.3 - 2148.3 ILI PWR 56.4 2162.3 MW-7 On -Site 2218.35 2218.60 26.43 2191.92 35.0 24.5 - 34.5 2194.1 - 2184.1 H BR 12.0 2206.6 MW-8 On -Site 2182.33 2182.63 NP-A NP-A 24.5 13.0 - 23.0 2169.6 - 2159.6 H PWR 22.0 2160.6 MW-8A On -Site 2182.52 2182.70 NP-A NP-A 35.0 30.0 - 35.0 2152.7 - 2147.7 Ills BR 15.5 2167.2 MW_9 On -Site 2175.57 2175.95 27.08 2148.49 60.0 44.0 - 54.0 2132.0 - 2122.0 H BR 34.0 2142.0 MW-10 On -Site 2159.92 2159.45 17.39 2142.53 39.0 29.0 - 39.0 2130.5 - 2120.5 H PWR 35.0 2124.5 MW-1 1 On -Site 2166.00 2166.39 25.80 2140.20 58.5 48.0 - 58.0 2118.4 - 2108.4 11 SAP >80.0 <2086.4 MW-12 On -Site 2219.17 2219.49 49.74 2169.43 81.0 60.0 - 70.0 2159.5 - 2149.5 H PWR 71.0 2148.5 MW-13 Off -Site 2138.80 2138.96 3.31 2135.49 58.5 48.0 - 58.0 2091.0 - 2081.0 11 SAP 58.5 2080.5 MW-14 Off -Site 2138.94 2139.20 Artesian >2138.94 75.0 65.0 - 75.0 2074.2 - 2064.2 Ills BR 59.0 2080.2 MW-15 Off -Site 2124.89 2125.18 12.09 2112.80 40.0 33.3 - 40.0 2091.9 - 2085.2 1110 BR 32.5 2092.7 MW-16 Off -Site 2124.59 2124.85 12.95 2111.64 33.5 23.5 - 33.5 2101.4 - 2091.4 H PWR 33.5 2091.4 MW-17 Off -Site 2094.64 2094.74 4.25 2090.39 14.2 4.0 - 14.0 2090.7 - 2080.7 H SAP 14.2 2080.5 MW-18 Off -Site 2101.81 2101.92 8.71 2093.10 59.0 49.0 - 59.0 2052.9 - 2042.9 H SAP 59.0 2042.9 MW-19 Off -Site 2127.61 2127.82 NP-D NP-D 58.0 48.0 - 58.0 2079.8 - 2069.8 11 SAP 58.0 2069.8 MW-20 Off -Site 2180.55 2180.54 37.29 2143.26 77.0 67.0 - 77.0 2113.5 - 2103.5 H SAP 77.0 2103.5 MW-21 Off -Site 2091.17 2091.31 2.31 2088.86 36.5 26.5 - 36.5 2064.8 - 2054.8 H SAP 36.5 2054.8 MW-22 Off -Site 2090.71 2090.84 1.56 2089.15 57.0 47.0 - 57.0 2043.8 - 2033.8 ]Ills BR 46.0 2044.8 MW-23 Off -Site 2145.05 2145.20 28.72 2116.33 41.5 31.0 - 41.5 2114.2 - 2103.7 HIO BR 30.0 2115.2 MW-24 Off -Site 2225.37 2225.49 63.21 2162.16 110.0 70.0 - 80.0 2155.5 - 2145.5 H PWR 42.0 2183.5 MW-25 Off -Site 2207.91 2208.04 NP-D NP-D 106.0 96.0 - 106.0 2112.0 - 2102.0 H PWR 104.0 2104.0 MW-26 Off -Site 2207.46 2207.62 30.69 2176.77 51.5 41.0 - 51.0 2166.6 - 2156.6 H PWR/BR 42.0 2165.6 RW-1 On -Site 2218.19 2218.61 53.59 2164.60 84.4 42.4 - 82.4 2176.2 - 2136.2 H BR/PWR 72.4 2146.2 RW-2 On -Site 2182.46 2183.62 NP-A NP-A 78.0 35.0 - 75.0 2148.6 - 2108.6 H BR 31.0 2152.6 RW-3 On -Site 2217.58 2218.06 48.10 2169.48 76.0 54.0 - 64.0 2164.1 - 2154.1 H BR 36.0 2182.1 RW-4 On -Site 2160.78 2161.74 NP-A NP-A 60.0 19.6 - 59.6 2142.1 - 2102.1 11 BR 20.0 2141.7 RW-5 On -Site 2159.48 2160.60 16.35 2143.13 66.0 20.2 - 60.2 2140.4 - 2100.4 H BR 16.0 2144.6 RW-6 On -Site 2160.44 2161.57 18.36 2142.08 67.0 20.0 - 60.0 2141.6 - 2101.6 H SAP/BR 36.0 2125.6 .RW-7 On -Site . 2164.57 2165.60 24.10 2140.47 67.0 13.0 - 53.0 1 2152.6 - 2112.6 11 SAP/PWR 55.0 2110.6 Notes: *Values rounded to the nearest 0. 1 -ft. NM = Not measured NP-A = Not Present - Abandoned NP-D = Not Present - Destroyed by Grading bgs = below ground surface. bmp = below measuring point. Water levels measured on 9/2 1 /11. Illo = Type III open bedrock well Measuring Point Elevation is top of casing. BR & PWR = Bedrock & Partially Weathered Rock MW-14 returned to artesian conditions as of 10/27/03. SAP = Saprolite II = Type Il well MW-24 was abandoned, redrilled and replaced in 2007 after the well head Ills = Type III screened well was damaged by Milkco contractors in 2003. The ground surface at RW- I and MW-6 was raised 7.4 feet and the wells were extended. Both were resurveyed in November 2010. Prepared by: AWA Table 1 (2011) of 1022-32 Andrex 2011 Annual Tables I & 2.xls Checked by: BDS Table 2 Laboratory Analytical Results of Groundwater & Surface Water Samples Selected Chlorinated VOCs Only Andrex Industries Asheville, North Carolina NCDENR Groundwater Incident Number 6586 BLE Project No. Jll-1022-32 U 40, 0 U 0 Q 0 U 7Slu N 0 N U NC 2L 0.:7 3 70 0.03 2 0=0 NE 7 0.4 100 70 2,000 0.6 50 6 0.2 NE Groundwater AB MW-1 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-3 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/23/2011 MW-5 2,340 75 ND ND ND ND ND ND ND 3,420 ND ND ND. ND ND 5,835 9/23/2011 MW-6 2,160 110 ND ND ND ND ND ND ND 328 ND ND ND ND ND 2,598 9/23/2011 MW-7 165 ND 0.51 ND ND ND ND ND ND ND ND ND ND ND ND 166 AB MW-8 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB MW-8A AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB_ 9/23/2011 MW-9 4,180 107 ND ND ND ND ND ND ND 191 ND ND ND. ND ND 4,478 9/23/2011 MW-10 182 75 ND ND ND ND ND 2.9 15 1,460 ND ND ND ND ND 1,735 9/23/2011 MW-11 2,130 93 ND ND ND ND ND ND ND 163 ND ND ND ND ND 2,386 9/23/2011 MW-12 156 44 ND ND ND ND 11 ND 14 6,810 ND ND ND ND ND 7,036 9/22/2011 MW-13 960 304 ND ND ND ND ND ND ND 158 ND ND ND ND ND 1,422 9/22/2011 MW-14 997 331 ND ND ND ND ND ND ND 136 ND ND ND ND ND 1,464 9/22/2011 MW-15 194 3.9 0.98 ND ND ND ND ND ND 9.4 1.2 ND ND. ND ND 209 9/22/2011 MW-16 249 4.9 1.5 ND ND ND ND ND ND 11 1.8 ND ND ND ND 268 9/22/2011 MW-17 7.5 3.4 ND 7.6 ND ND ND ND ND 16 ND ND ND ND ND 34 9/22/2011 MW-18 7.1 0.72 1.4 ND ND ND ND ND- ND ND ND ND ND ND ND 9.2 NP** MW-19 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 9/22/2011 MW-20 ND ND 0.72 ND ND ND ND ND ND, ND ND ND ND. ND ND 0.72 9/21/2011 MW-21 ND ND 0.88 ND ND ND ND ND ND ND ND ND ND ND ND 0.88 9/21/2011 MW-22 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/23/2011 MW-23 143 6.8 ND ND ND ND ND ND ND 12 ND ND ND ND ND 162 9/22/2011 MW-24 243 6.2 ND ND ND ND ND ND ND 1.4 ND ND ND ND ND 251 NP** MW-25 NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 9/21/2011 MW-26 ND ND 3.2 ND ND ND ND ND ND ND ND ND ND ND ND 3.2 9/23/2011 RW-1 2,010 2,610 ND ND ND ND ND ND 53 7,610 ND ND ND ND ND 12,283 AB RW-2 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/23/2011 RW-3 132 71 ND 40 ND ND 15 ND ND 9,290 ND ND ND. ND ND 9,548 AB RW-4 AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB AB 9/23/2011 RW-5 74 70 ND 14 ND ND 1.5 ND 15 1,760 ND ND ND 1,934 9/23/2011 RW-6 1,120 262 ND ND ND ND ND ND 4.9 750 ND ND ND 2,137 9/23/2011 RW-7 107 10 11 ND ND ND ND ND ND 71 ND ND ND 200 NC 2B 0.7 2.5 NE 0.025 NE NE NE NE NE NE I NE I NE 1488 1488 1 NE I NE Surface Water 9/28/2011 Smith Mill Creek 1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/28/2011 Smith Mill Creek 2 0.68 ND 0.31 ND ND ND ND ND ND ND ND ND ND ND ND 0.99 9/28/2011 Smith Mill Creek 3 0.61 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.61 9/28/2011 Smith Mill Creek 4 2.1 ND ND ND ND ND ND ND ND 0.58 ND ND ND ND ND 2.7 9/28/2011 Smith Mill Creek 5 1.7 ND ND ND ND ND ND ND ND. 0.39 ND ND ND ND ND 2.1 9/28/2011 Smith Mill Creek 6 1.3 ND ND ND ND ND N ND ND 0.24 ND ND ND ND ND 1.5 9/28/2011 Bear Creek 1 3.4 ND ND ND ND ND ND ND ND 2.0 ND ND ND. ND ND 5.4 9/28/2011 Bear Creek 2 14 2.1 0.95 ND ND ND ND ND ND 6.4 ND ND ND ND ND 24 9/28/2011 Bear Creek 3 6.8 1.5 1.6 ND ND ND ND ND ND 5.2 ND ND ND ND ND 15 9/28/2011 Bear Creek 4 ND ND ND ND ND ND ND ND ND. ND ND ND ND ND ND ND 9/28/2011 Bear Creek 5 0.58 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.58 9/28/2011 Jehovah Witness 1 17 2.1 0.41 ND ND ND ND ND ND 3.7 ND ND ND. ND ND 23 9/28/2011 Cecil's Spring 1 18 1.6 ND ND ND ND ND ND ND 3.3 ND ND ND ND ND 22 9/28/2011 Cecil's Spring 2 1 7.3 0.84 ND ND ND ND ND ND ND 0.81 ND ND ND I ND ND 9.0 Notes. Analyses performed by EPA Method 8260 MSV Low Level. J-flagged (estimated) results are included on this table but are not identified (see the lab report). Units in gg/l or parts per billion (ppb) Detected concentrations of petroleum hydrocarbon VOCs are NOT shown in this table (not part of the Andrex groundwater incident). Detected concentrations of acetone, chloromethane, and methylene chloride are NOT shown in this table (probable laboratory contaminants). NC2L = North Carolina Groundwater Standards under Title 15A Subchapter 2L in Vg/l dated January 1, 2010. NC2B = North Carolina Surface Water Standards [WS - Water Supply Classification] under Title 15A Subchapter 2B in pg/l dated May 1, 2007. ND not detected at concentrations exceeding the laboratory reporting limit. NS not sampled. NP not present; monitoring well was abandoned or destroyed. AB well was abandoned as part of the approved Brownfield Redevelopment Plan in 2008. Compounds intermittently detected in the past. ** These wells were destroyed by grading during 2003. Recovery wells were sampled by purging with downbole pumps. Prepared by: AWA Table 2 (2011) of1022-32 Andrex 2011 AnnualTables I &2.xls Checked by: BDS ]FIGURES �'� �i ��Il; ��� ���� �� �� J.. �. ..,aril 0 0 0 N N ry�0 �O ��ry � O 0 R p O �Z ty cy N MW-16 CECIL'S OLLEGE 2111.64 1`S• SFRNrG _ � �'• � W-15 v ��` �'• �� 2112.80 / o J o � 9 MW-18 RESIDENTIAL G�G�, 2093.10/_ _ J/ m �� RESIDENTIAL N �/ TWENTIETH SHEET a RESIDENTIAL BEAR CREEK ROAD RESIDENTIAL �HAMILTONI PROPERTY 0 STREET McDADE ��/ i •�.. r ki •. MALVERN HILLS ►L _ POOL -� . ® PARK M-��,• �•• � TENNIS COURTS PLACE -- RESIDENTIAL G a if cn RESIDENTIAL REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA FROM PHOTOGRAPHY DATED MARCH-APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. BLNA ® ENS RESIDENTIAL RESIDENTIAL O O N r RESIDENTIAL MW-24 MILKCO, INC. 2162.16 MW-1 MW-12 NP-A \ 2169.43 MV I RW-3 NF 2169.48 — IMW-5 2169.45 i W-25 MW-6 NP-D 2164.12 RW-1 2164.60 MILKCO, INC. M MW-3 �f NP-A MW-26 0 2176.77 O 2 "_\I Tim a —L _A 0 Mw-7 cm 2191.92 1 x KW—[ MW-8A* A6R, \IDUST IES, INC. MW-4* MW-9 NIP -A 2148.49 II MW-8* NP-A PERFECTIO GEAR, INC. TRW-4 NP-A RW-5 MW-10 \ II 2143.13 2142.53 RW-6 MW-11 \\ 2142.08 2140.20 O � a Lu c ICE �� / M -14 138.94 2140.47 VICE® \\,- SILVERS_ w STORE- / MW-13 Q PROPERTY 2135.49 SILVERS PROPERTYw i ECHOLS B ING \PROPERTY\ LLEY M JUSTICE ' i PROPERTY ^M ' O O ! C Alr �N N ey RESIDENTIAL DATE: 02-10-12 CAD FILE: ANDREX32-WTMO92111 JOB NO: J11-1022-32 .0 RE q Nf 0 MW-20 2143.26 SEXTON PROPERTY RESIDENTIAL H YNES Pn . 2 L' l� �1 O AYN S C RP. N - - F ROY D FARME O MW-23 — - 2116.33 I� MW I i 2088_-- I ' •'�• MW-22 - - 2089.15 BMW-17 •�• 2090.39 DRMls\�.\ NORFpLEHOVAN K TNER TNESS4\ BIESTE F DL �s�o N Rq��ROgD OPERTY • , PROPERTY - - FORMER 1 MW-19 WATER WELL NP-D - CRYDE AN - - PROPE Y SATTERFI PROPERTY HOUS-_, 0 j► O O jOREENTIAL�O O 00 /"y0F Al-. O NOTES: 1. THE GROUNDWATER PUMP AND TREAT SYSTEMS HAD BEEN REMOVED AND WERE NOT IN OPERATION AT THE TIME WATER LEVEL MEASUREMENTS WERE TAKEN. GROUNDWATER WAS NOT BEING PUMPED FROM RW-1 THROUGH RW-7 WHILE MEASUREMENTS WERE COLLECTED. 2. ** SKY LANES BOWLING CENTER NCDEH - PUBLIC WATER SYSTEM ID #10-11-025 WELL NAME: WELL #1 AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED "...THE ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER." 2090 2080 LEGEND ••� Q5 APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR ••� SHALLOW BEDROCK) GROUNDWATER MONITORING WELL O APPROXIMATE LOCATION OF EXISTING (TYPE III -BEDROCK) •�, GROUNDWATER MONITORING WELL O RECOVERY WELL O WATER SUPPLY WELL }--- BELOW GROUND STREAM SHOWING FLOW DIRECTION �•-•• �— ABOVE GROUND STREAM SHOWING FLOW DIRECTION PROPERTY LINE 2116.33 WATER LEVEL IN FEET ABOVE MEAN SEA LEVEL * GROUNDWATER ELEVATION IN WELL MW-14 (ARTESIAN) MAY REPRESENT THE POTENTIOMETRIC SURFACE OF THE DEEPER ROCK AQUIFER AND WAS NOT CONSIDERED FOR CONTOURING PURPOSES. NP-A NOT PRESENT. WELL HAS BEEN ABANDONED. NP-D MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. MW-25 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY MILKO, INC. APPROXIMATE DIRECTION OF GROUNDWATER FLOW APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE 2120 EQUIPOTENTIAL CONTOUR LINE 200 100 0 200 400 APPROXIMATE SCALE IN FEET REVISIONS No. DESCRIPTION BY DRAWN: ACE CHECKED: AWA APPROVED: NIL BUNNELL-LAMMONS ENGNNEERING, INC. 6004 PONDERS COURT GREENVILLE, SOUTH CAROLINA 29615 INC. PHONE: (864)288-1265 FAX: (864)288-4430 GROUNDWATER ELEVATION CONTOUR MAP - SEPTEMBER 21, 2011 ANDREX INDUSTRIES DEAVERVIEW ROAD ASHEVILLE, NORTH CAROLINA FIGURE NO. 2 RESIDENTIAL RESIDENTIAL BEAR CREEK ROAD RESIDENTIAL CS-2 �` 90 -----\FO ER CECIL'S LEG RESIDENTIAL Cs—, .. ._ MW-16 MW-1\5 22 268 209 MW-18 J 9.2 1 TWEN TH STREET 100_ I — 00000 rl STREE IC SERVICES � 0.INC \\ RESID `SO r0 13LUUMINU "' wool 0000 � _BC-2 RESIDENTI 24 swoop woom 00-W __Ilvl swoop MO-00 MALVERN HILLS P 15 — J BC-4 ND _ •1�'� _ r — /.• _ M—` I TENNIS �1 _ND /•' I COURTS swoop swoop OWN= /•• � � __3RUswoop MBOUGH PLACE BC-5 /••�•• 100o F�' V Z 0.58 /•' Q o Q Q REFERENCE: ORTHOPHOTO MAP OF BUNCOMBE COUNTY, N.C. PREPARED BY L. ROBERT KIMBALL & ASSOCIATES, EBENSBURG, PENNSYLVANIA FROM PHOTOGRAPHY DATED MARCH—APRIL 1985 IN ACCORDANCE WITH NATIONAL MAP ACCURACY STANDARDS. RESIDENTIAL RESIDENTIAL J ICE Dr i�.T/ 'BC-1� — 5.4 1 1 I I I 1 H _ MW-26 am� swoop 4=� swoop Gomm" RESIDENTIAL O 2 (CHLOROFORM ONLY) I 1 10 ,•,; r s 00 � ° �•• HAJES CORP. MILK I HAYNES CORP. �-/.• MW-24 W-2/ . lill M 251 RW-3 AB J' / ,r^ 9,548 I A / T MW-12 — MW-1 / 5,835 5 7,036 AB /' MW-6* ` r'• W-25 O 2,598 MW— NP RW-1 166 ` y 12,283 �� 3 H ONES CORP. •� MILKCO, `` INC. O O 0,000 z. �Q 1 AB ' MW-9 MWB 8 �0 I 114,478 — 0 'MW B 8A — — — F-- FECTION AR, INC IRW -4 �► ---1 1 �\ s ANDREX AB M II O L_-- INDUSTRIES, I D O 1 SM-2 \ IRW-5 � •. � 0.99_ J Z ` SILVERS .0I BOWLING \PROPER AI I CV RESIDENTIAL \\ I1I 1,934 � ----- lO —23, MW-10 RW-6 MW-11 D I\1 162 r 1,735 0 2,386 o OY D. FARMER BARK 2,137 MW-13 1,422 RW-7 200 0 \ NoomIi MW-14* -A RESIDENTIAL swoop mosop MW-20 GR (CHLOROFORM2ONLY) 200 100 0 200 400 APPROXIMATE SCALE IN FEET RESIDENTIAL SM-1 ND MW-17 �G 34 I SM-3 RASH ROAD I I 0.61 MW-21 I i 0.88 (CHLOROFORM ONLY) I MW-22 �_ ® ND 23 �' FORMER JEHOVAN l\ WITNESS PROPERTY `BIESTERFEDLT At PROPERTY mw— 9 �� T ��k Soul SM-4\ , 10 Ak'%4D 2.7 SM-5 \ BAKER DF i 7wc MER 2.1ATER WELL SATTERFIELD J_ _ _ _ CRYDERMAN SM1. 6 ��• swoop swoop PROPERTY —HOUSE - - —.PROPERTY •�•.�• "swoop owwwwo ND am* ouna—m—summ —I r_ Lu -now �� _� �. z RESIDENTIAL \ GAR �7 S = f 1475 Q 'w P�OLOp�S.• Q RESIDENTIAL A NOTES: 1. LABORATORY ANALYSIS BY EPA METHOD 8260. 2. WELLS AND SURFACE WATER WAS SAMPLED ON SEPTEMBER 22-28, 2011. MW-6 WAS SAMPLED ON NOVEMBER 9, 2010. 3. CONCENTRATIONS DETECTED IN MW-21 AND MW-26 ARE PRIMARILY CHLOROFORM, PROBABLY RELATED TO LEAKING WATER SUPPLY LINES IN CLOSE PROXIMITY TO THE WELLS. 4. SAMPLES FROM STREAMS DESIGNATED AS FOLLOWS: SM = SMITH MILL CREEK TRIBUTARY CS = CECIL'S SPRING BC = BEAR CREEK JW = FORMER JEHOVAH WITNESS PROPERTY 5. NP = NOT PRESENT, WELL WAS NOT PRESENT AT TIME OF SAMPLING. 6. ** SKY LANES BOWLING CENTER NCDEH — PUBLIC WATER SYSTEM ID #10-11-025 WELL NAME: WELL #1 AS OF 5-19-2009, MR. MARC FOWLER OF BUNCOMBE COUNTY HAS STATED 'I ESTABLISHMENT HAS BEEN RESTORED TO CITY WATER." 7. * THE WELLS MAY INTERCEPT FRACTURE SETS OR MAY BE SCREENED AT ELEVATIONS AT WHICH GROUNDWATER CONTAMINANT CONCENTRATIONS ARE INCONSISTENT WITH THE ESTABLISHED PLUME. THE VALUES WERE IGNORED FOR CONTOURING PURPOSES. 8. THE FORMER WATER SUPPLY WELL ON THE CRYDERMAN PROPERTY APPEARED TO BE ABANDONED AND COULD NOT BE SAMPLED AS OF OCTOBER 2005. 9. MW-19 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY THE CITY OF ASHEVILLE. MW-25 WAS NOT PRESENT IN OCTOBER 2003 AND WAS PRESUMED TO BE DESTROYED BY GRADING PERFORMED BY MILKO, INC. 10. RECOVERY WELLS WERE NOT OPERATIONAL AT THE TIME OF SAMPLING. 11. AB = WELL ABANDONED IN 2008 PER APPROVED BROWNFIELD REDEVELOPMENT PLAN. LEGEND APPROXIMATE LOCATION OF EXISTING (SAPROLITE OR SHALLOW BEDROCK) GROUNDWATER MONITORING WELL 0 APPROXIMATE LOCATION OF EXISTING (TYPE III —BEDROCK) GROUNDWATER MONITORING WELL 0 RECOVERY WELL - APPROXIMATE LOCATION OF SURFACE WATER SAMPLES (SEE NOTE 4) (WATER SAMPLES COLLECTED 9-28-11). O WATER SUPPLY WELL 162 CONCENTRATION OF TOTAL DETECTED CHLORINATED VOLATILE ORGANIC COMPOUNDS IN PARTS PER BILLION (ppb). —�f-- �— BELOW GROUND STREAM SHOWING FLOW DIRECTION —"— ABOVE GROUND STREAM SHOWING FLOW DIRECTION PROPERTY LINE APPROXIMATE LOCATION OF SANITARY SEWER MANHOLE WITH SEWER LINE 100 TOTAL CHLORINATED CONCENTRATION CONTOUR IN PARTS PER BILLION ND-- ESTIMATED LIMIT OF VOC'S REVISIONS No. DESCRIPTION BY DRAWN: ACE CHECKED: AWA APPROVED: DATE: 02-10-12 CAD FILE: ANDREX32—VOCSEPT1I JOB No: J11-1022-32 NIL BUNNELL-LAMMONS ENONEERNO, NC. 6004 PONDERS COURT INC. PHONE: (64)288510265 FAX: (864)288UTH CAROLINA 54430 CONTOUR MAP OF TOTAL CHLORINATED VOLATILE ORGANIC COMPOUND ISOCONCENTRATIONS — SEPTEMBER 22-28, 2011 GROUNDWATER AND SURFACE WATER ANDREX INDUSTRIES ASHEVILLE, NORTH CAROLINA FIGURE NO. 3 APPENDICES APPENDIX A WELL SAMPLING LOGS MILE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of I Date: Sep.23,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2216.75 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-5 Land Surface Elevation (ft msl): 2216.92 Downgradient: yes Screened Interval (ft bgs): 43.0-53.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudv Steel Guard PiDe Around Casiniz: ves Air Temperature: 68OF Locking Cap: yes Total Well Depth in feet (TWD) 53.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 47.30 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 5.70 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 0.97 Sample Date and Time: 9/23/2011 @ 950 Standard Evacuation Volume (3 casing volumes) 2.91 Remarks: Slight sour milk odor. Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump ITotal Volume of Water Removed (eallons): 3 izallons I FIELD ANALYSIS Volume Purged (gallons) initial 1.0 1.9 2.9 Time (military) 941 944 946 948 pH (S.U.) 6 6 6 6 Sp. Cond. (umhos/cm) 67.7 59.4 57 57 Water Temp. ('C) 1 17.6 1 17.5 1 17.6 1 17.5 1 Turbidity (subjective)* 1 2 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. — 1.60 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2218.43 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-6 Land Surface Elevation (ft msl): 2218.67 Downgradient: yes Screened Interval (ft bgs): 50.4-70.4 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 70OF Locking Cap: yes Total Well Depth in feet (TWD) 71.90 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 54.31 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 17.59 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 2.99 Sample Date and Time: 9/23/2011 @ 1840 Standard Evacuation Volume (3 casing volumes) 8.97 Remarks: Well Damaged -- Could not get sampling equipment (pump or std. disp. Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer bailer) downhole. Additional blockage at undetermined depth. Total Volume of Water Removed (gallons): 1.5 gallons Sampled and purged with small diameter bailer. Volume Purged (gallons) initial FIELD ANALYSIS Time (military) 1822 pH (S.U.) 5.5 Sp. Cond. (umhos/cm) 140.7 Water Temp. ('C) 16.9 Turbidity (subjective)* 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 13.1 (from purged sample, not downhole DO measurement) IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2218.35 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-7 Land Surface Elevation (ft msl): 2218.60 Downgradient: yes Screened Interval (ft bgs): 24.5-34.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 670F Locking Cap: yes Total Well Depth in feet (TWD) 35.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 26.43 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 8.57 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 1.46 Sample Date and Time: 9/23/2011 @ 925 Standard Evacuation Volume (3 casing volumes) 4.37 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 4.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 1.5 2.9 4.4 Time (military) 916 919 921 923 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 43.5 41.8 36.9 34.8 Water Temp. ('C) 17.2 16.9 16.8 16.8 Turbidity (subjective)* 3 2 2 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 7.64 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2175.57 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-9 Land Surface Elevation (ft msl): 2175.95 Downgradient: yes Screened Interval (ft bgs): 44.0-54.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) 54.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 27.08 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 27.12 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 4.61 Sample Date and Time: 9/23/2011 @ 1435 Standard Evacuation Volume (3 casing volumes) 13.8 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 14 gallons Volume Purged (gallons) initial FIELD ANALYSIS 4.6 9.2 13.8 Time (military) 1408 1415 1422 1433 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 81.6 72.0 68.3 67.1 Water Temp. ('C) 16.0 15.1 14.9 15.0 Turbidity (subjective)* 2 1 1 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.62 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2159.92 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-10 Land Surface Elevation (ft msl): 2159.45 Downgradient: yes Screened Interval (ft bgs): 29.0-39.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: no Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) 39.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 17.39 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 21.61 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 3.67 Sample Date and Time: 9/23/2011 @ 1350 Standard Evacuation Volume (3 casing volumes) 11.02 Remarks: Duplicate A collected 9-23-11 @ 1350 Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump ITotal Volume of Water Removed (eallons): 11.02 aallons FIELD ANALYSIS Volume Purged (gallons) initial 3.7 7.3 11.0 Time (military) 1327 1333 1339 1346 pH (S.U.) 6 6 6 6 Sp. Cond. (umhos/cm) 118.2 115.7 176.5 222.7 Water Temp. ('C) 1 18.0 1 15.9 1 15.7 1 15.7 1 Turbidity (subjective)* 1 4 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 0.75 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2166.00 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-1 I Land Surface Elevation (ft msl): 2166.39 Downgradient: yes Screened Interval (ft bgs): 48.0-58.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Sunny Steel Guard Pipe Around Casing: no Air Temperature: 730F Locking Cap: yes Total Well Depth in feet (TWD) 58.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 25.80 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 32.70 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 5.56 Sample Date and Time: 9/23/2011 @ 1305 Standard Evacuation Volume (3 casing volumes) 16.68 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 17 gallons Volume Purged (gallons) initial FIELD ANALYSIS 5.6 11.1 16.7 Time (military) 1241 1247 1256 1305 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 81.6 68.4 63.9 59.8 Water Temp. ('C) 18.2 18.2 16.9 16.7 Turbidity (subjective)* 3 2 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.32 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2219.17 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-12 Land Surface Elevation (ft msl): 2219.49 Downgradient: yes Screened Interval (ft bgs): 60.0-70.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 70OF Locking Cap: yes Total Well Depth in feet (TWD) 81.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 49.74 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 31.26 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 5.31 Sample Date and Time: 9/23/2011 @ 1020 Standard Evacuation Volume (3 casing volumes) 15.94 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 16 gallons Volume Purged (gallons) initial FIELD ANALYSIS 5.3 10.6 15.9 Time (military) 1000 1006 1012 1018 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 216.4 232.4 230.9 222.5 Water Temp. ('C) 17.1 17.1 17.2 17.3 Turbidity (subjective)* 2 1 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.80 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2138.80 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-13 Land Surface Elevation (ft msl): 2138.96 Downgradient: yes Screened Interval (ft bgs): 48.0-58.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) 58.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 3.31 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 55.19 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 9.38 Sample Date and Time: 9/22/2011 @ 1500 Standard Evacuation Volume (3 casing volumes) 28.15 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 28.15 gallons Volume Purged (gallons) initial FIELD ANALYSIS 9.4 18.8 28.2 Time (military) 1418 1426 1446 1455 pH (S.U.) 6 6 6 6 Sp. Cond. (umhos/cm) 55.7 57.6 55.7 57.4 Water Temp. ('C) 17.5 17.0 17.5 17.8 Turbidity (subjective)* 3 1 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.80 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2138.94 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-14 Land Surface Elevation (ft msl): 2139.2 Downgradient: yes Screened Interval (ft bgs): 65.0-75.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) 75.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) Artesian Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 75.00 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 12.75 Sample Date and Time: 9/22/2011 @ 1415 Standard Evacuation Volume (3 casing volumes) 38.25 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 38.25 gallons Volume Purged (gallons) initial FIELD ANALYSIS 12.8 25.5 38.3 Time (military) 1326 1338 1354 1410 pH (S.U.) 6 6 6 6 Sp. Cond. (umhos/cm) 25.7 55.4 56.8 60.6 Water Temp. ('C) 18.1 17.1 16.8 16.6 Turbidity (subjective)* 2 1 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.94 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 6 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2124.89 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-15 Land Surface Elevation (ft msl): 2125.18 Downgradient: yes Screened Interval (ft bgs): 33.3-40.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 670F Locking Cap: yes Total Well Depth in feet (TWD) 40.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 12.09 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 27.91 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 41.87 Sample Date and Time: 9/22/2011 @ 1000 Standard Evacuation Volume (3 casing volumes) = 125.60 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 126 gallons Volume Purged (gallons) initial FIELD ANALYSIS 42 84 126 Time (military) 944 948 952 956 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 39.5 38.8 38.6 38.4 Water Temp. ('C) 15.7 15.2 15.0 15.1 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 8.45 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2124.59 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-16 Land Surface Elevation (ft msl): 2124.85 Downgradient: yes Screened Interval (ft bgs): 23.5-33.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 660F Locking Cap: yes Total Well Depth in feet (TWD) 33.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 12.95 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 20.55 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 3.49 Sample Date and Time: 9/22/2011 @ 0940 Standard Evacuation Volume (3 casing volumes) 10.48 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 10.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 3.5 7.0 10.5 Time (military) 918 923 927 936 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 50.2 45.1 43.4 42.3 Water Temp. ('C) 17.0 15.9 15.9 15.9 Turbidity (subjective)* 3 2 2 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.82 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2094.64 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-17 Land Surface Elevation (ft msl): 2094.74 Downgradient: yes Screened Interval (ft bgs): 4.0-14.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 630F Locking Cap: yes Total Well Depth in feet (TWD) 14.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 4.25 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 9.95 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 1.69 Sample Date and Time: 9/22/2011 @ 0900 Standard Evacuation Volume (3 casing volumes) 5.07 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 5.07 gallons Volume Purged (gallons) initial FIELD ANALYSIS 1.7 3.4 5.1 Time (military) 842 845 851 857 pH (S.U.) 6 6 6 6 Sp. Cond. (umhos/cm) 169.8 168.9 166.6 154.3 Water Temp. ('C) 19.8 19.1 22.1 21.7 Turbidity (subjective)* 2 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.45 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2101.81 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-18 Land Surface Elevation (ft msl): 2101.92 Downgradient: yes Screened Interval (ft bgs): 49.0-59.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 70OF Locking Cap: yes Total Well Depth in feet (TWD) 59.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 8.71 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 50.29 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 8.55 Sample Date and Time: 9/22/2011 @ 113 0 Standard Evacuation Volume (3 casing volumes) 25.65 Remarks: Dry @ 18 gallons Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 18 gallons Volume Purged (gallons) initial FIELD ANALYSIS 8.6 17.1 Time (military) 1024 1051 1116 pH (S.U.) 6 6 6 Sp. Cond. (umhos/cm) 49.3 47.1 46.1 Water Temp. ('C) 15.9 16.6 17.0 Turbidity (subjective)* 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.35 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2180.55 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-20 Land Surface Elevation (ft msl): 2180.54 Downgradient: yes Screened Interval (ft bgs): 67.0-77.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 71OF Locking Cap: yes Total Well Depth in feet (TWD) 77.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 37.29 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 39.71 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 6.75 Sample Date and Time: 9/22/2011 @ 1305 Standard Evacuation Volume (3 casing volumes) 20.25 Remarks: Method of Well Evacuation: Disp. Bailer Method of Sample Collection: Disp. Bailer Total Volume of Water Removed (gallons): 20.25 gallons Volume Purged (gallons) initial FIELD ANALYSIS 6.8 13.5 20.3 Time (military) 1215 1228 1243 1303 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 20.5 19.3 18.4 17.6 Water Temp. ('C) 17.0 16.1 16.6 16.7 Turbidity (subjective)* 1 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 7.01 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 21, 2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2091.17 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-21 Land Surface Elevation (ft msl): 2091.31 Downgradient: yes Screened Interval (ft bgs): 26.5-36.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) 36.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 2.31 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 34.19 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 5.81 Sample Date and Time: 9/21/2011 @ 1600 Standard Evacuation Volume (3 casing volumes) 17.44 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 17.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 5.8 11.5 17.4 Time (military) 1502 1512 1535 1552 pH (S.U.) 5.5 5.5 5.5 5.5 Sp. Cond. (umhos/cm) 52.6 51.3 52.2 49.5 Water Temp. ('C) 16.9 17.0 17.2 17.1 Turbidity (subjective)* 2 2 2 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 3.38 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 21, 2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2090.71 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-22 Land Surface Elevation (ft msl): 2090.84 Downgradient: yes Screened Interval (ft bgs): 47.0-57.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) 57.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 1.56 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 55.44 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 9.42 Sample Date and Time: 9/21/2011 @ 1500 Standard Evacuation Volume (3 casing volumes) 28.27 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 28.3 gallons Volume Purged (gallons) initial FIELD ANALYSIS 9.4 18.8 28.3 Time (military) 1357 1412 1433 1454 pH (S.U.) 5.5 5.5 5.5 5.5 Sp. Cond. (umhos/cm) 87.6 66.2 63.0 61.7 Water Temp. ('C) 17.4 17.1 16.6 16.9 Turbidity (subjective)* 2 1 1 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.80 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 6 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2145.05 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-23 Land Surface Elevation (ft msl): 2145.20 Downgradient: yes Screened Interval (ft bgs): 31.0-41.5 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) 41.50 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 28.72 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 12.78 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 19.17 Sample Date and Time: 9/23/2011 @ 1505 Standard Evacuation Volume (3 casing volumes) = 57.51 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 58 gallons Volume Purged (gallons) initial FIELD ANALYSIS 19.2 39.3 57.5 Time (military) 1053 1055 1057 1059 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 144.1 142.4 117.8 128.1 Water Temp. ('C) 17.9 15.9 16.7 15.9 Turbidity (subjective)* I I I I (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 5.85 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.22,2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2225.37 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-24 Land Surface Elevation (ft msl): 2225.49 Downgradient: yes Screened Interval (ft bgs): 70.0-80.0 Upgradient: Dedicated Pump or Bailer: no Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) 80.10 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 63.21 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 16.89 Well Yield (subjective): low I Casing Volume in gallons (CV) = LWC x 0. 17 2.87 Sample Date and Time: 9/22/2011 @ 1545 Standard Evacuation Volume (3 casing volumes) 8.61 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 8.6 gallons Volume Purged (gallons) initial FIELD ANALYSIS 2.9 5.7 8.6 Time (military) 1519 1524 1531 1540 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 60.8 54.4 51.6 50.4 Water Temp. ('C) 19.1 16.8 16.9 16.9 Turbidity (subjective)* 3 2 2 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.73 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep. 21, 2011 Casing Diameter: 2 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2207.46 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: MW-26 Land Surface Elevation (ft msl): 2207.62 Downgradient: yes Screened Interval (ft bgs): 41.0-51.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Cloudy/Rain Steel Guard Pipe Around Casing: no Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) 51.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 30.69 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 20.31 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0. 17 3.45 Sample Date and Time: 9/21/2011 @ 1336 Standard Evacuation Volume (3 casing volumes) 10.36 Remarks: Method of Well Evacuation: Monsoon Pump Method of Sample Collection: Monsoon Pump Total Volume of Water Removed (gallons): 10.4 gallons Volume Purged (gallons) initial FIELD ANALYSIS 3.5 6.9 10.4 Time (military) 1319 1324 1329 1333 pH (S.U.) 6 6 6 6 Sp. Cond. (umhos/cm) 84.0 95.2 104.8 104.1 Water Temp. ('C) 18.2 17.0 16.6 16.7 Turbidity (subjective)* 3 2 1 1 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 3.05 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 6 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2209.87 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: RW- 1 Land Surface Elevation (ft msl): 2211.22 Downgradient: yes Screened Interval (ft bgs): 35.0-75.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 71OF Locking Cap: no Total Well Depth in feet (TWD) 82.40 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 53.59 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 28.81 Well Yield (subjective): moderate I Casing Volume in gallons (CV) = LWC x 1.5 = 43.22 Sample Date and Time: 9/23/2011 @ 1805 Standard Evacuation Volume (3 casing volumes) = 129.65 Remarks: Pump clogged @ 55 gallons Method of Well Evacuation: Sub Pump Method of Sample Collection: Disp. Bailer Duplicate B collected at 1805 Total Volume of Water Removed (gallons): 55 gallons Volume Purged (gallons) initial FIELD ANALYSIS 44 Time (military) 1744 1752 pH (S.U.) 5 5 Sp. Cond. (umhos/cm) 290.7 446.5 Water Temp. ('C) 17.1 17.2 Turbidity (subjective)* 4 4 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.16 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 4 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2217.58 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: RW-3 Land Surface Elevation (ft msl): 2218.06 Downgradient: yes Screened Interval (ft bgs): 54.0-64.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: P. Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 68OF Locking Cap: yes Total Well Depth in feet (TWD) 64.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 48.10 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW 15.90 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 0.66 10.49 Sample Date and Time: 9/23/2011 @ 1935 Standard Evacuation Volume (3 casing volumes) 31.48 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 31.5 gallons Volume Purged (gallons) initial FIELD ANALYSIS 10.5 21.0 31.5 Time (military) 1905 1915 1924 1932 pH (S.U.) 4.5 4.5 4.5 4.5 Sp. Cond. (umhos/cm) 3124 601 315.7 218.9 Water Temp. ('C) 18.8 18.2 17.7 17.4 Turbidity (subjective)* 4 3 3 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 0.64 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 6 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2159.48 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: RW-5 Land Surface Elevation (ft msl): 2160.60 Downgradient: yes Screened Interval (ft bgs): 20.2-60.2 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 740F Locking Cap: yes Total Well Depth in feet (TWD) 60.20 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 16.35 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 43.85 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 65.78 Sample Date and Time: 9/23/2011 @ 1720 Standard Evacuation Volume (3 casing volumes) = 197.33 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 200 gallons Volume Purged (gallons) initial FIELD ANALYSIS 66 132 198 Time (military) 1659 1705 1712 1718 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 609 365.2 309.2 333.1 Water Temp. ('C) 15.9 15.0 15.1 15.2 Turbidity (subjective)* 4 3 3 3 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 2.65 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 6 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2160.44 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: RW-6 Land Surface Elevation (ft msl): 2161.57 Downgradient: yes Screened Interval (ft bgs): 20.0-60.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Sunny Steel Guard Pipe Around Casing: yes Air Temperature: 760F Locking Cap: yes Total Well Depth in feet (TWD) 60.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 18.36 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 41.64 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 62.46 Sample Date and Time: 9/23/2011 @ 1640 Standard Evacuation Volume (3 casing volumes) = 187.38 Remarks: Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 190 gallons Volume Purged (gallons) initial FIELD ANALYSIS 62 124 188 Time (military) 1620 1626 1633 1639 pH (S.U.) 5 5 5 5 Sp. Cond. (umhos/cm) 155.5 98.0 81.1 74.9 Water Temp. ('C) 15.8 15.3 15.3 15.9 Turbidity (subjective)* 2 2 2 2 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 1.66 IBLE BUNNELL-LAMMONS ENGINEERING, INC. FIELD DA TA INFORMA TION L 0 G FOR GR 0 UND KA TER SAMPLING Page I of 1 Date: Sep.23,2011 Casing Diameter: 6 inches Field Personnel: BPN/BAL Casing Material: PVC Site Name: Andrex Measuring Point Elevation (ft msl): 2164.57 BLE Job #: 1022-32 Height of Riser (ft above land surface): flushmount Well ID #: RW-7 Land Surface Elevation (ft msl): 2165.60 Downgradient: yes Screened Interval (ft bgs): 13.0-53.0 Upgradient: Dedicated Pump or Bailer: yes Weather Conditions: Cloudy Steel Guard Pipe Around Casing: yes Air Temperature: 750F Locking Cap: yes Total Well Depth in feet (TWD) 53.00 Protective Post/Abutment: no Depth to Ground Water in feet (DGW) 24.10 Well Integrity Satisfactory: yes Length of Water Column (LWC) = TWD - DGW = 28.90 Well Yield (subjective): high I Casing Volume in gallons (CV) = LWC x 1.5 = 43.35 Sample Date and Time: 9/23/2011 @ 1550 Standard Evacuation Volume (3 casing volumes) = 130.05 Remarks: Pumped clogged by roots. Method of Well Evacuation: Sub. Pump Method of Sample Collection: Sub. Pump Total Volume of Water Removed (gallons): 60 gallons Volume Purged (gallons) initial FIELD ANALYSIS 48.4 Time (military) 1525 1545 pH (S.U.) 4 4 Sp. Cond. (umhos/cm) 484.2 674 Water Temp. ('C) 17.2 17.2 Turbidity (subjective)* 4 4 (1) Clear (2) Slight (3) Moderate (4) High COMMENTS/OBSERVATIONS: D.O. = 2.60 APPENDIX B LABORATORY ANALYTICAL DATA SHEETS (Provided on Enclosed CD) ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27288 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (336)623-8921 October 05, 2011 Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 RE: Project: FORMERANDREX INDUSTRIES Pace Project No.: 92103091 (828)254-7176 Dear Mr. Alexander: Enclosed are the analytical results for sample(s) received by the laboratory on September 26, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures PIC, R�b REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (704)875-9092 Page 1 of 81 Pace Analytical Services, Inc. Pace Analytical Services, Inc. acmnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.p,?celabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: FORMERANDREX INDUSTRIES Pace Project No.: 92103091 Charlotte Certification III)s 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. M 99006003 Virginia Drinking Water Certification #: 00213 Connecticut Certification#: PH-01 04 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DHH Drinking Water # LA 100031 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460144 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 81 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. I ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE SUMMARY Project: Pace Project No.: Lab ID FORMER ANDREX INDUSTRIES 92103091 Sample ID Matrix Date Collected Date Received 92103091001 MW-5 Water 09/23/11 09:50 09/26/11 11:30 92103091002 MW-6 Water 09/23/11 18:40 09/26/11 11:30 92103091003 MW-7 Water 09/23/11 09:25 09/26/11 11:30 92103091004 MW-9 Water 09/23/11 14:35 09/26/11 11:30 92103091005 MW-10 Water 09/23/11 13:50 09/26/11 11:30 92103091006 MW-11 1 Water 09/23/11 13:05 09/26/11 11:30 92103091007 MW-12 Water 09/23/11 10:20 09/26/11 11:30 92103091008 MW-13 Water 09/22/11 15:00 09/26/11 11:30 92103091009 MW-14 Water 09/22/11 14:15 09/26/11 11:30 92103091010 MW-15 Water 09/22/11 10:00 09/26/11 11:30 92103091011 MW-16 Water 09/22/11 09:40 09/26/11 11:30 92103091012 MW-17 Water 09/22/11 09:00 09/26/11 11:30 92103091013 MW-1 8 Water 09/22/11 11:30 09/26/11 11:30 92103091014 MW-20 Water 09/22/11 13:05 09/26/11 11:30 92103091015 MW-21 Water 09/21/11 16:00 09/26/11 11:30 92103091016 MW-22 Water 09/21/11 15:00 09/26/11 11:30 92103091017 MW-23 Water 09/23/11 15:05 09/26/11 11:30 92103091018 MW-24 Water 09/22/11 15:45 09/26/11 11:30 92103091019 MW-26 Water 09/21/11 13:36 09/26/11 11:30 92103091020 RW-1 Water 09/23/11 18:05 09/26/11 11:30 92103091021 RW-3 Water 09/23/11 19:35 09/26/11 11:30 92103091022 RW-5 Water 09/23/11 17:20 09/26/11 11:30 92103091023 RW-6 Water 09/23/11 16:40 09/26/11 11:30 92103091024 RW-7 Water 09/23/11 15:50 09/26/11 11:30 92103091025 RINSATE A Water 09/23/11 00:00 09/26/11 11:30 92103091026 RINSATE B Water 09/23/11 00:00 09/26/11 11:30 92103091027 DUPLICATE A Water 09/23/11 00:00 09/26/11 11:30 92103091028 DUPLICATE B Water 09/23/11 00:00 09/26/11 11:30 92103091029 DUPLICATE C Water 09/23/11 00:00 09/26/11 11:30 92103091030 TRIP BLANK Water 09/22/11 00:00 09/26/11 11:30 REPORT OF LABORATORY ANALYSIS Page 3 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 SAMPLE ANALYTE COUNT Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92103091001 MW-5 EPA 8260 AW 63 PASI-C 92103091002 MW-6 EPA 8260 AW 63 PASI-C 92103091003 MW-7 EPA 8260 AW 63 PASI-C 92103091004 MW-9 EPA 8260 AW 63 PASI-C 92103091005 MW-10 EPA 8260 AW 63 PASI-C 92103091006 MW-11 EPA 8260 AW 63 PASI-C 92103091007 MW-12 EPA 8260 AW 63 PASI-C 92103091008 MW-13 EPA 8260 AW 63 PASI-C 92103091009 MW-14 EPA 8260 AW 63 PASI-C 92103091010 MW-15 EPA 8260 MCK 63 PASI-C 92103091011 MW-16 EPA 8260 AW 63 PASI-C 92103091012 MW-17 EPA 8260 AW 63 PASI-C 92103091013 MW-18 EPA 8260 MCK 63 PASI-C 92103091014 MW-20 EPA 8260 AW 63 PASI-C 92103091015 MW-21 EPA 8260 AW 63 PASI-C 92103091016 MW-22 EPA 8260 AW 63 PASI-C 92103091017 MW-23 EPA 8260 AW 63 PASI-C 92103091018 MW-24 EPA 8260 AW 63 PASI-C 92103091019 MW-26 EPA 8260 AW 63 PASI-C 92103091020 RW-1 EPA 8260 MCK 63 PASI-C 92103091021 RW-3 EPA 8260 AW 63 PASI-C 92103091022 IRW-5 EPA 8260 AW 63 PASI-C 92103091023 RW-6 EPA 8260 MCK 63 PASI-C 92103091024 RW-7 EPA 8260 AW 63 PASI-C 92103091025 RINSATE A EPA 8260 AW 63 PASI-C 92103091026 RINSATE B EPA 8260 AW 63 PASI-C 92103091027 DUPLICATE A EPA 8260 AW 63 PASI-C 92103091028 DUPLICATE B EPA 8260 MCK 63 PASI-C 92103091029 DUPLICATE C EPA 8260 MCK 63 PASI-C 92103091030 TRIP BLANK EPA 8260 AW 63 PASI-C REPORT OF LABORATORY ANALYSIS Page 4 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5 Labll): 92103091001 Collected: 09/23/11 09:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 500 43.4 20 09/28/11 20:24 67-64-1 ND ug/L 20.0 5.0 20 09/28/11 20:24 71-43-2 ND ug/L 20.0 6.0 20 09/28/11 20:24 108-86-1 ND ug/L 20.0 3.4 20 09/28/11 20:24 74-97-5 ND ug/L 20.0 3.6 20 09/28/11 20:24 75-27-4 ND ug/L 20.0 5.2 20 09/28/11 20:24 75-25-2 ND ug/L 40.0 5.8 20 09/28/11 20:24 74-83-9 ND ug/L 100 19.2 20 09/28/11 20:24 78-93-3 ND ug/L 20.0 5.0 20 09/28/11 20:24 56-23-5 ND ug/L 20.0 4.6 20 09/28/11 20:24 108-90-7 ND ug/L 20.0 10.8 20 09/28/11 20:24 75-00-3 ND ug/L 20.0 2.8 20 09/28/11 20:24 67-66-3 ND ug/L 20.0 2.2 20 09/28/11 20:24 74-87-3 ND ug/L 20.0 7.0 20 09/28/11 20:24 95-49-8 ND ug/L 20.0 6.2 20 09/28/11 20:24 106-43-4 ND ug/L 100 50.4 20 09/28/11 20:24 96-12-8 ND ug/L 20.0 4.2 20 09/28/11 20:24 124-48-1 ND ug/L 20.0 5.4 20 09/28/11 20:24 106-93-4 ND ug/L 20.0 4.2 20 09/28/11 20:24 74-95-3 ND ug/L 20.0 6.0 20 09/28/11 20:24 95-50-1 ND ug/L 20.0 4.8 20 09/28/11 20:24 541-73-1 ND ug/L 20.0 6.6 20 09/28/11 20:24 106-46-7 ND ug/L 20.0 4.2 20 09/28/11 20:24 75-71-8 ND ug/L 20.0 6.4 20 09/28/11 20:24 75-34-3 ND ug/L 20.0 2.4 20 09/28/11 20:24 107-06-2 ND ug/L 20.0 11.2 20 09/28/11 20:24 75-35-4 3420 ug/L 20.0 3.8 20 09/28/11 20:24 156-59-2 ND ug/L 20.0 9.8 20 09/28/11 20:24 156-60-5 ND ug/L 20.0 5.4 20 09/28/11 20:24 78-87-5 ND ug/L 20.0 5.6 20 09/28/11 20:24 142-28-9 ND ug/L 20.0 2.6 20 09/28/11 20:24 594-20-7 ND ug/L 20.0 9.8 20 09/28/11 20:24 563-58-6 ND ug/L 20.0 2.6 20 09/28/11 20:24 10061-01-5 ND ug/L 20.0 5.2 20 09/28/11 20:24 10061-02-6 ND ug/L 20.0 2.4 20 09/28/11 20:24 108-20-3 ND ug/L 20.0 6.0 20 09/28/11 20:24 100-41-4 ND ug/L 20.0 14.2 20 09/28/11 20:24 87-68-3 ND ug/L 100 9.2 20 09/28/11 20:24 591-78-6 ND ug/L 20.0 6.2 20 09/28/11 20:24 99-87-6 ND ug/L 40.0 19.4 20 09/28/11 20:24 75-09-2 ND ug/L 100 6.6 20 09/28/11 20:24 108-10-1 ND ug/L 20.0 4.2 20 09/28/11 20:24 1634-04-4 ND ug/L 20.0 4.8 20 09/28/11 20:24 91-20-3 ND ug/L 20.0 5.2 20 09/28/11 20:24 100-42-5 ND ug/L 20.0 6.6 20 09/28/11 20:24 630-20-6 ND ug/L 20.0 8.0 20 09/28/11 20:24 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 5 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5 Labll): 92103091001 Collected: 09/23/11 09:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2340 ug/L 20.0 9.2 20 09/28/11 20:24 127-18-4 Toluene ND ug/L 20.0 5.2 20 09/28/11 20:24 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.6 20 09/28/11 20:24 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 7.0 20 09/28/11 20:24 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 9.6 20 09/28/11 20:24 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 5.8 20 09/28/11 20:24 79-00-5 Trichloroethene 74.9 ug/L 20.0 9.4 20 09/28/11 20:24 79-01-6 Trichlorofluoromethane ND ug/L 20.0 4.0 20 09/28/11 20:24 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 8.2 20 09/28/11 20:24 96-18-4 Vinyl acetate ND ug/L 40.0 7.0 20 09/28/11 20:24 108-05-4 Vinyl chloride ND ug/L 20.0 12.4 20 09/28/11 20:24 75-01-4 m&p-Xylene ND ug/L 40.0 13.2 20 09/28/11 20:24 179601-23-1 o-Xylene ND ug/L 20.0 4.6 20 09/28/11 20:24 95-47-6 4-Bromofluorobenzene (S) 90 % 70-130 20 09/28/11 20:24 460-00-4 Dibromofluoromethane (S) 108 % 70-130 20 09/28/11 20:24 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 20 09/28/11 20:24 17060-07-0 Tbluene-d8 (S) 92 % 70-130 20 09/28/11 20:24 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 6 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 Labll): 92103091002 Collected: 09/23/11 18:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 500 43.4 20 09/28/11 20:47 67-64-1 ND ug/L 20.0 5.0 20 09/28/11 20:47 71-43-2 ND ug/L 20.0 6.0 20 09/28/11 20:47 108-86-1 ND ug/L 20.0 3.4 20 09/28/11 20:47 74-97-5 ND ug/L 20.0 3.6 20 09/28/11 20:47 75-27-4 ND ug/L 20.0 5.2 20 09/28/11 20:47 75-25-2 ND ug/L 40.0 5.8 20 09/28/11 20:47 74-83-9 ND ug/L 100 19.2 20 09/28/11 20:47 78-93-3 ND ug/L 20.0 5.0 20 09/28/11 20:47 56-23-5 ND ug/L 20.0 4.6 20 09/28/11 20:47 108-90-7 ND ug/L 20.0 10.8 20 09/28/11 20:47 75-00-3 ND ug/L 20.0 2.8 20 09/28/11 20:47 67-66-3 ND ug/L 20.0 2.2 20 09/28/11 20:47 74-87-3 ND ug/L 20.0 7.0 20 09/28/11 20:47 95-49-8 ND ug/L 20.0 6.2 20 09/28/11 20:47 106-43-4 ND ug/L 100 50.4 20 09/28/11 20:47 96-12-8 ND ug/L 20.0 4.2 20 09/28/11 20:47 124-48-1 ND ug/L 20.0 5.4 20 09/28/11 20:47 106-93-4 ND ug/L 20.0 4.2 20 09/28/11 20:47 74-95-3 ND ug/L 20.0 6.0 20 09/28/11 20:47 95-50-1 ND ug/L 20.0 4.8 20 09/28/11 20:47 541-73-1 ND ug/L 20.0 6.6 20 09/28/11 20:47 106-46-7 ND ug/L 20.0 4.2 20 09/28/11 20:47 75-71-8 ND ug/L 20.0 6.4 20 09/28/11 20:47 75-34-3 ND ug/L 20.0 2.4 20 09/28/11 20:47 107-06-2 ND ug/L 20.0 11.2 20 09/28/11 20:47 75-35-4 328 ug/L 20.0 3.8 20 09/28/11 20:47 156-59-2 ND ug/L 20.0 9.8 20 09/28/11 20:47 156-60-5 ND ug/L 20.0 5.4 20 09/28/11 20:47 78-87-5 ND ug/L 20.0 5.6 20 09/28/11 20:47 142-28-9 ND ug/L 20.0 2.6 20 09/28/11 20:47 594-20-7 ND ug/L 20.0 9.8 20 09/28/11 20:47 563-58-6 ND ug/L 20.0 2.6 20 09/28/11 20:47 10061-01-5 ND ug/L 20.0 5.2 20 09/28/11 20:47 10061-02-6 ND ug/L 20.0 2.4 20 09/28/11 20:47 108-20-3 ND ug/L 20.0 6.0 20 09/28/11 20:47 100-41-4 ND ug/L 20.0 14.2 20 09/28/11 20:47 87-68-3 ND ug/L 100 9.2 20 09/28/11 20:47 591-78-6 ND ug/L 20.0 6.2 20 09/28/11 20:47 99-87-6 ND ug/L 40.0 19.4 20 09/28/11 20:47 75-09-2 ND ug/L 100 6.6 20 09/28/11 20:47 108-10-1 ND ug/L 20.0 4.2 20 09/28/11 20:47 1634-04-4 ND ug/L 20.0 4.8 20 09/28/11 20:47 91-20-3 ND ug/L 20.0 5.2 20 09/28/11 20:47 100-42-5 ND ug/L 20.0 6.6 20 09/28/11 20:47 630-20-6 ND ug/L 20.0 8.0 20 09/28/11 20:47 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 7 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 Labll): 92103091002 Collected: 09/23/11 18:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2160 ug/L 20.0 9.2 20 09/28/11 20:47 127-18-4 Toluene ND ug/L 20.0 5.2 20 09/28/11 20:47 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.6 20 09/28/11 20:47 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 7.0 20 09/28/11 20:47 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 9.6 20 09/28/11 20:47 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 5.8 20 09/28/11 20:47 79-00-5 Trichloroethene 110 ug/L 20.0 9.4 20 09/28/11 20:47 79-01-6 Trichlorofluoromethane ND ug/L 20.0 4.0 20 09/28/11 20:47 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 8.2 20 09/28/11 20:47 96-18-4 Vinyl acetate ND ug/L 40.0 7.0 20 09/28/11 20:47 108-05-4 Vinyl chloride ND ug/L 20.0 12.4 20 09/28/11 20:47 75-01-4 m&p-Xylene ND ug/L 40.0 13.2 20 09/28/11 20:47 179601-23-1 o-Xylene ND ug/L 20.0 4.6 20 09/28/11 20:47 95-47-6 4-Bromofluorobenzene (S) 90 % 70-130 20 09/28/11 20:47 460-00-4 Dibromofluoromethane (S) 105 % 70-130 20 09/28/11 20:47 1868-53-7 1,2-Dichloroethane-d4 (S) 114 % 70-130 20 09/28/11 20:47 17060-07-0 Tbluene-d8 (S) 90 % 70-130 20 09/28/11 20:47 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 8 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 Labll): 92103091003 Collected: 09/23/11 09:25 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/28/11 19:15 67-64-1 ND ug/L 1.0 0.25 1 09/28/11 19:15 71-43-2 ND ug/L 1.0 0.30 1 09/28/11 19:15 108-86-1 ND ug/L 1.0 0.17 1 09/28/11 19:15 74-97-5 ND ug/L 1.0 0.18 1 09/28/11 19:15 75-27-4 ND ug/L 1.0 0.26 1 09/28/11 19:15 75-25-2 ND ug/L 2.0 0.29 1 09/28/11 19:15 74-83-9 ND ug/L 5.0 0.96 1 09/28/11 19:15 78-93-3 ND ug/L 1.0 0.25 1 09/28/11 19:15 56-23-5 ND ug/L 1.0 0.23 1 09/28/11 19:15 108-90-7 ND ug/L 1.0 0.54 1 09/28/11 19:15 75-00-3 0.51J ug/L 1.0 0.14 1 09/28/11 19:15 67-66-3 ND ug/L 1.0 0.11 1 09/28/11 19:15 74-87-3 ND ug/L 1.0 0.35 1 09/28/11 19:15 95-49-8 ND ug/L 1.0 0.31 1 09/28/11 19:15 106-43-4 ND ug/L 5.0 2.5 1 09/28/11 19:15 96-12-8 ND ug/L 1.0 0.21 1 09/28/11 19:15 124-48-1 ND ug/L 1.0 0.27 1 09/28/11 19:15 106-93-4 ND ug/L 1.0 0.21 1 09/28/11 19:15 74-95-3 ND ug/L 1.0 0.30 1 09/28/11 19:15 95-50-1 ND ug/L 1.0 0.24 1 09/28/11 19:15 541-73-1 ND ug/L 1.0 0.33 1 09/28/11 19:15 106-46-7 ND ug/L 1.0 0.21 1 09/28/11 19:15 75-71-8 ND ug/L 1.0 0.32 1 09/28/11 19:15 75-34-3 ND ug/L 1.0 0.12 1 09/28/11 19:15 107-06-2 ND ug/L 1.0 0.56 1 09/28/11 19:15 75-35-4 ND ug/L 1.0 0.19 1 09/28/11 19:15 156-59-2 ND ug/L 1.0 0.49 1 09/28/11 19:15 156-60-5 ND ug/L 1.0 0.27 1 09/28/11 19:15 78-87-5 ND ug/L 1.0 0.28 1 09/28/11 19:15 142-28-9 ND ug/L 1.0 0.13 1 09/28/11 19:15 594-20-7 ND ug/L 1.0 0.49 1 09/28/11 19:15 563-58-6 ND ug/L 1.0 0.13 1 09/28/11 19:15 10061-01-5 ND ug/L 1.0 0.26 1 09/28/11 19:15 10061-02-6 ND ug/L 1.0 0.12 1 09/28/11 19:15 108-20-3 ND ug/L 1.0 0.30 1 09/28/11 19:15 100-41-4 ND ug/L 1.0 0.71 1 09/28/11 19:15 87-68-3 ND ug/L 5.0 0.46 1 09/28/11 19:15 591-78-6 ND ug/L 1.0 0.31 1 09/28/11 19:15 99-87-6 ND ug/L 2.0 0.97 1 09/28/11 19:15 75-09-2 ND ug/L 5.0 0.33 1 09/28/11 19:15 108-10-1 ND ug/L 1.0 0.21 1 09/28/11 19:15 1634-04-4 ND ug/L 1.0 0.24 1 09/28/11 19:15 91-20-3 ND ug/L 1.0 0.26 1 09/28/11 19:15 100-42-5 ND ug/L 1.0 0.33 1 09/28/11 19:15 630-20-6 ND ug/L 1.0 0.40 1 09/28/11 19:15 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 9 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 Labll): 92103091003 Collected: 09/23/11 09:25 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 165 ug/L 1.0 0.46 1 09/28/11 19:15 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/28/11 19:15 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/28/11 19:15 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/28/11 19:15 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/28/11 19:15 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/28/11 19:15 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/28/11 19:15 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/28/11 19:15 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/28/11 19:15 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/28/11 19:15 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/28/11 19:15 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/28/11 19:15 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/28/11 19:15 95-47-6 4-Bromofluorobenzene (S) 90 % 70-130 1 09/28/11 19:15 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/28/11 19:15 1868-53-7 1,2-Dichloroethane-d4 (S) 114 % 70-130 1 09/28/11 19:15 17060-07-0 Tbluene-d8 (S) 90 % 70-130 1 09/28/11 19:15 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 10 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Labll): 92103091004 Collected: 09/23/11 14:35 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 625 54.2 25 09/28/11 21:09 67-64-1 ND ug/L 25.0 6.2 25 09/28/11 21:09 71-43-2 ND ug/L 25.0 7.5 25 09/28/11 21:09 108-86-1 ND ug/L 25.0 4.2 25 09/28/11 21:09 74-97-5 ND ug/L 25.0 4.5 25 09/28/11 21:09 75-27-4 ND ug/L 25.0 6.5 25 09/28/11 21:09 75-25-2 ND ug/L 50.0 7.2 25 09/28/11 21:09 74-83-9 ND ug/L 125 24.0 25 09/28/11 21:09 78-93-3 ND ug/L 25.0 6.2 25 09/28/11 21:09 56-23-5 ND ug/L 25.0 5.8 25 09/28/11 21:09 108-90-7 ND ug/L 25.0 13.5 25 09/28/11 21:09 75-00-3 ND ug/L 25.0 3.5 25 09/28/11 21:09 67-66-3 ND ug/L 25.0 2.8 25 09/28/11 21:09 74-87-3 ND ug/L 25.0 8.8 25 09/28/11 21:09 95-49-8 ND ug/L 25.0 7.8 25 09/28/11 21:09 106-43-4 ND ug/L 125 63.0 25 09/28/11 21:09 96-12-8 ND ug/L 25.0 5.2 25 09/28/11 21:09 124-48-1 ND ug/L 25.0 6.8 25 09/28/11 21:09 106-93-4 ND ug/L 25.0 5.2 25 09/28/11 21:09 74-95-3 ND ug/L 25.0 7.5 25 09/28/11 21:09 95-50-1 ND ug/L 25.0 6.0 25 09/28/11 21:09 541-73-1 ND ug/L 25.0 8.2 25 09/28/11 21:09 106-46-7 ND ug/L 25.0 5.2 25 09/28/11 21:09 75-71-8 ND ug/L 25.0 8.0 25 09/28/11 21:09 75-34-3 ND ug/L 25.0 3.0 25 09/28/11 21:09 107-06-2 ND ug/L 25.0 14.0 25 09/28/11 21:09 75-35-4 191 ug/L 25.0 4.8 25 09/28/11 21:09 156-59-2 ND ug/L 25.0 12.2 25 09/28/11 21:09 156-60-5 ND ug/L 25.0 6.8 25 09/28/11 21:09 78-87-5 ND ug/L 25.0 7.0 25 09/28/11 21:09 142-28-9 ND ug/L 25.0 3.2 25 09/28/11 21:09 594-20-7 ND ug/L 25.0 12.2 25 09/28/11 21:09 563-58-6 ND ug/L 25.0 3.2 25 09/28/11 21:09 10061-01-5 ND ug/L 25.0 6.5 25 09/28/11 21:09 10061-02-6 ND ug/L 25.0 3.0 25 09/28/11 21:09 108-20-3 ND ug/L 25.0 7.5 25 09/28/11 21:09 100-41-4 ND ug/L 25.0 17.8 25 09/28/11 21:09 87-68-3 ND ug/L 125 11.5 25 09/28/11 21:09 591-78-6 ND ug/L 25.0 7.8 25 09/28/11 21:09 99-87-6 ND ug/L 50.0 24.2 25 09/28/11 21:09 75-09-2 ND ug/L 125 8.2 25 09/28/11 21:09 108-10-1 ND ug/L 25.0 5.2 25 09/28/11 21:09 1634-04-4 ND ug/L 25.0 6.0 25 09/28/11 21:09 91-20-3 ND ug/L 25.0 6.5 25 09/28/11 21:09 100-42-5 ND ug/L 25.0 8.2 25 09/28/11 21:09 630-20-6 ND ug/L 25.0 10.0 25 09/28/11 21:09 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 11 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Labll): 92103091004 Collected: 09/23/11 14:35 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 4180 ug/L 25.0 11.5 25 09/28/11 21:09 127-18-4 Toluene ND ug/L 25.0 6.5 25 09/28/11 21:09 108-88-3 1,2,3-Trichlorobenzene ND ug/L 25.0 8.2 25 09/28/11 21:09 87-61-6 1,2,4-Trichlorobenzene ND ug/L 25.0 8.8 25 09/28/11 21:09 120-82-1 1,1,1-Trichloroethane ND ug/L 25.0 12.0 25 09/28/11 21:09 71-55-6 1,1,2-Trichloroethane ND ug/L 25.0 7.2 25 09/28/11 21:09 79-00-5 Trichloroethene 107 ug/L 25.0 11.8 25 09/28/11 21:09 79-01-6 Trichlorofluoromethane ND ug/L 25.0 5.0 25 09/28/11 21:09 75-69-4 1,2,3-Trichloropropane ND ug/L 25.0 10.2 25 09/28/11 21:09 96-18-4 Vinyl acetate ND ug/L 50.0 8.8 25 09/28/11 21:09 108-05-4 Vinyl chloride ND ug/L 25.0 15.5 25 09/28/11 21:09 75-01-4 m&p-Xylene ND ug/L 50.0 16.5 25 09/28/11 21:09 179601-23-1 o-Xylene ND ug/L 25.0 5.8 25 09/28/11 21:09 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 25 09/28/11 21:09 460-00-4 Dibromofluoromethane (S) 105 % 70-130 25 09/28/11 21:09 1868-53-7 1,2-Dichloroethane-d4 (S) 116 % 70-130 25 09/28/11 21:09 17060-07-0 Tbluene-d8 (S) 90 % 70-130 25 09/28/11 21:09 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 12 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-10 Labll): 92103091005 Collected: 09/23/11 13:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 500 43.4 20 09/28/11 21:32 67-64-1 ND ug/L 20.0 5.0 20 09/28/11 21:32 71-43-2 ND ug/L 20.0 6.0 20 09/28/11 21:32 108-86-1 ND ug/L 20.0 3.4 20 09/28/11 21:32 74-97-5 ND ug/L 20.0 3.6 20 09/28/11 21:32 75-27-4 ND ug/L 20.0 5.2 20 09/28/11 21:32 75-25-2 ND ug/L 40.0 5.8 20 09/28/11 21:32 74-83-9 ND ug/L 100 19.2 20 09/28/11 21:32 78-93-3 ND ug/L 20.0 5.0 20 09/28/11 21:32 56-23-5 ND ug/L 20.0 4.6 20 09/28/11 21:32 108-90-7 ND ug/L 20.0 10.8 20 09/28/11 21:32 75-00-3 ND ug/L 20.0 2.8 20 09/28/11 21:32 67-66-3 6.OJ ug/L 20.0 2.2 20 09/28/11 21:32 74-87-3 ND ug/L 20.0 7.0 20 09/28/11 21:32 95-49-8 ND ug/L 20.0 6.2 20 09/28/11 21:32 106-43-4 ND ug/L 100 50.4 20 09/28/11 21:32 96-12-8 ND ug/L 20.0 4.2 20 09/28/11 21:32 124-48-1 ND ug/L 20.0 5.4 20 09/28/11 21:32 106-93-4 ND ug/L 20.0 4.2 20 09/28/11 21:32 74-95-3 ND ug/L 20.0 6.0 20 09/28/11 21:32 95-50-1 ND ug/L 20.0 4.8 20 09/28/11 21:32 541-73-1 ND ug/L 20.0 6.6 20 09/28/11 21:32 106-46-7 ND ug/L 20.0 4.2 20 09/28/11 21:32 75-71-8 ND ug/L 20.0 6.4 20 09/28/11 21:32 75-34-3 2.9J ug/L 20.0 2.4 20 09/28/11 21:32 107-06-2 ND ug/L 20.0 11.2 20 09/28/11 21:32 75-35-4 1460 ug/L 20.0 3.8 20 09/28/11 21:32 156-59-2 1 5.2J ug/L 20.0 9.8 20 09/28/11 21:32 156-60-5 N D ug/L 20.0 5.4 20 09/28/11 21:32 78-87-5 N D ug/L 20.0 5.6 20 09/28/11 21:32 142-28-9 N D ug/L 20.0 2.6 20 09/28/11 21:32 594-20-7 N D ug/L 20.0 9.8 20 09/28/11 21:32 563-58-6 N D ug/L 20.0 2.6 20 09/28/11 21:32 10061-01-5 N D ug/L 20.0 5.2 20 09/28/11 21:32 10061-02-6 N D ug/L 20.0 2.4 20 09/28/11 21:32 108-20-3 N D ug/L 20.0 6.0 20 09/28/11 21:32 100-41-4 N D ug/L 20.0 14.2 20 09/28/11 21:32 87-68-3 N D ug/L 100 9.2 20 09/28/11 21:32 591-78-6 N D ug/L 20.0 6.2 20 09/28/11 21:32 99-87-6 N D ug/L 40.0 19.4 20 09/28/11 21:32 75-09-2 N D ug/L 100 6.6 20 09/28/11 21:32 108-10-1 N D ug/L 20.0 4.2 20 09/28/11 21:32 1634-04-4 N D ug/L 20.0 4.8 20 09/28/11 21:32 91-20-3 N D ug/L 20.0 5.2 20 09/28/11 21:32 100-42-5 N D ug/L 20.0 6.6 20 09/28/11 21:32 630-20-6 N D ug/L 20.0 8.0 20 09/28/11 21:32 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 13 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-10 Labll): 92103091005 Collected: 09/23/11 13:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 182 ug/L 20.0 9.2 20 09/28/11 21:32 127-18-4 Toluene ND ug/L 20.0 5.2 20 09/28/11 21:32 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.6 20 09/28/11 21:32 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 7.0 20 09/28/11 21:32 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 9.6 20 09/28/11 21:32 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 5.8 20 09/28/11 21:32 79-00-5 Trichloroethene 74.8 ug/L 20.0 9.4 20 09/28/11 21:32 79-01-6 Trichlorofluoromethane ND ug/L 20.0 4.0 20 09/28/11 21:32 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 8.2 20 09/28/11 21:32 96-18-4 Vinyl acetate ND ug/L 40.0 7.0 20 09/28/11 21:32 108-05-4 Vinyl chloride ND ug/L 20.0 12.4 20 09/28/11 21:32 75-01-4 m&p-Xylene ND ug/L 40.0 13.2 20 09/28/11 21:32 179601-23-1 o-Xylene ND ug/L 20.0 4.6 20 09/28/11 21:32 95-47-6 4-Bromofluorobenzene (S) 93 % 70-130 20 09/28/11 21:32 460-00-4 Dibromofluoromethane (S) 105 % 70-130 20 09/28/11 21:32 1868-53-7 1,2-Dichloroethane-d4 (S) 114 % 70-130 20 09/28/11 21:32 17060-07-0 Tbluene-d8 (S) 97 % 70-130 20 09/28/11 21:32 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 14 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11 Labll): 92103091006 Collected: 09/23/11 13:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 250 21.7 10 09/28/11 21:55 67-64-1 ND ug/L 10.0 2.5 10 09/28/11 21:55 71-43-2 ND ug/L 10.0 3.0 10 09/28/11 21:55 108-86-1 ND ug/L 10.0 1.7 10 09/28/11 21:55 74-97-5 ND ug/L 10.0 1.8 10 09/28/11 21:55 75-27-4 ND ug/L 10.0 2.6 10 09/28/11 21:55 75-25-2 ND ug/L 20.0 2.9 10 09/28/11 21:55 74-83-9 ND ug/L 50.0 9.6 10 09/28/11 21:55 78-93-3 ND ug/L 10.0 2.5 10 09/28/11 21:55 56-23-5 ND ug/L 10.0 2.3 10 09/28/11 21:55 108-90-7 ND ug/L 10.0 5.4 10 09/28/11 21:55 75-00-3 ND ug/L 10.0 1.4 10 09/28/11 21:55 67-66-3 ND ug/L 10.0 1.1 10 09/28/11 21:55 74-87-3 ND ug/L 10.0 3.5 10 09/28/11 21:55 95-49-8 ND ug/L 10.0 3.1 10 09/28/11 21:55 106-43-4 ND ug/L 50.0 25.2 10 09/28/11 21:55 96-12-8 ND ug/L 10.0 2.1 10 09/28/11 21:55 124-48-1 ND ug/L 10.0 2.7 10 09/28/11 21:55 106-93-4 ND ug/L 10.0 2.1 10 09/28/11 21:55 74-95-3 ND ug/L 10.0 3.0 10 09/28/11 21:55 95-50-1 ND ug/L 10.0 2.4 10 09/28/11 21:55 541-73-1 ND ug/L 10.0 3.3 10 09/28/11 21:55 106-46-7 ND ug/L 10.0 2.1 10 09/28/11 21:55 75-71-8 ND ug/L 10.0 3.2 10 09/28/11 21:55 75-34-3 ND ug/L 10.0 1.2 10 09/28/11 21:55 107-06-2 ND ug/L 10.0 5.6 10 09/28/11 21:55 75-35-4 163 ug/L 10.0 1.9 10 09/28/11 21:55 156-59-2 ND ug/L 10.0 4.9 10 09/28/11 21:55 156-60-5 ND ug/L 10.0 2.7 10 09/28/11 21:55 78-87-5 ND ug/L 10.0 2.8 10 09/28/11 21:55 142-28-9 ND ug/L 10.0 1.3 10 09/28/11 21:55 594-20-7 ND ug/L 10.0 4.9 10 09/28/11 21:55 563-58-6 ND ug/L 10.0 1.3 10 09/28/11 21:55 10061-01-5 ND ug/L 10.0 2.6 10 09/28/11 21:55 10061-02-6 ND ug/L 10.0 1.2 10 09/28/11 21:55 108-20-3 ND ug/L 10.0 3.0 10 09/28/11 21:55 100-41-4 ND ug/L 10.0 7.1 10 09/28/11 21:55 87-68-3 ND ug/L 50.0 4.6 10 09/28/11 21:55 591-78-6 ND ug/L 10.0 3.1 10 09/28/11 21:55 99-87-6 ND ug/L 20.0 9.7 10 09/28/11 21:55 75-09-2 ND ug/L 50.0 3.3 10 09/28/11 21:55 108-10-1 ND ug/L 10.0 2.1 10 09/28/11 21:55 1634-04-4 ND ug/L 10.0 2.4 10 09/28/11 21:55 91-20-3 ND ug/L 10.0 2.6 10 09/28/11 21:55 100-42-5 ND ug/L 10.0 3.3 10 09/28/11 21:55 630-20-6 ND ug/L 10.0 4.0 10 09/28/11 21:55 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 15 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11 Labll): 92103091006 Collected: 09/23/11 13:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2130 ug/L 25.0 11.5 25 09/29/11 16:46 127-18-4 Toluene ND ug/L 10.0 2.6 10 09/28/11 21:55 108-88-3 1,2,3-Trichlorobenzene ND ug/L 10.0 3.3 10 09/28/11 21:55 87-61-6 1,2,4-Trichlorobenzene ND ug/L 10.0 3.5 10 09/28/11 21:55 120-82-1 1,1,1-Trichloroethane ND ug/L 10.0 4.8 10 09/28/11 21:55 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 2.9 10 09/28/11 21:55 79-00-5 Trichloroethene 92.5 ug/L 10.0 4.7 10 09/28/11 21:55 79-01-6 Trichlorofluoromethane ND ug/L 10.0 2.0 10 09/28/11 21:55 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.1 10 09/28/11 21:55 96-18-4 Vinyl acetate ND ug/L 20.0 3.5 10 09/28/11 21:55 108-05-4 Vinyl chloride ND ug/L 10.0 6.2 10 09/28/11 21:55 75-01-4 m&p-Xylene ND ug/L 20.0 6.6 10 09/28/11 21:55 179601-23-1 o-Xylene ND ug/L 10.0 2.3 10 09/28/11 21:55 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 10 09/28/11 21:55 460-00-4 Dibromofluoromethane (S) 106 % 70-130 10 09/28/11 21:55 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 10 09/28/11 21:55 17060-07-0 Tbluene-d8 (S) 90 % 70-130 10 09/28/11 21:55 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 16 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-12 Labll): 92103091007 Collected: 09/23/11 10:20 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 500 43.4 20 09/28/11 22:18 67-64-1 ND ug/L 20.0 5.0 20 09/28/11 22:18 71-43-2 ND ug/L 20.0 6.0 20 09/28/11 22:18 108-86-1 ND ug/L 20.0 3.4 20 09/28/11 22:18 74-97-5 ND ug/L 20.0 3.6 20 09/28/11 22:18 75-27-4 ND ug/L 20.0 5.2 20 09/28/11 22:18 75-25-2 ND ug/L 40.0 5.8 20 09/28/11 22:18 74-83-9 ND ug/L 100 19.2 20 09/28/11 22:18 78-93-3 ND ug/L 20.0 5.0 20 09/28/11 22:18 56-23-5 ND ug/L 20.0 4.6 20 09/28/11 22:18 108-90-7 ND ug/L 20.0 10.8 20 09/28/11 22:18 75-00-3 ND ug/L 20.0 2.8 20 09/28/11 22:18 67-66-3 4.6J ug/L 20.0 2.2 20 09/28/11 22:18 74-87-3 ND ug/L 20.0 7.0 20 09/28/11 22:18 95-49-8 ND ug/L 20.0 6.2 20 09/28/11 22:18 106-43-4 ND ug/L 100 50.4 20 09/28/11 22:18 96-12-8 ND ug/L 20.0 4.2 20 09/28/11 22:18 124-48-1 ND ug/L 20.0 5.4 20 09/28/11 22:18 106-93-4 ND ug/L 20.0 4.2 20 09/28/11 22:18 74-95-3 ND ug/L 20.0 6.0 20 09/28/11 22:18 95-50-1 ND ug/L 20.0 4.8 20 09/28/11 22:18 541-73-1 ND ug/L 20.0 6.6 20 09/28/11 22:18 106-46-7 ND ug/L 20.0 4.2 20 09/28/11 22:18 75-71-8 ND ug/L 20.0 6.4 20 09/28/11 22:18 75-34-3 ND ug/L 20.0 2.4 20 09/28/11 22:18 107-06-2 11.3J ug/L 20.0 11.2 20 09/28/11 22:18 75-35-4 6810 ug/L 100 19.0 100 09/29/11 17:09 156-59-2 14.2J ug/L 20.0 9.8 20 09/28/11 22:18 156-60-5 ND ug/L 20.0 5.4 20 09/28/11 22:18 78-87-5 ND ug/L 20.0 5.6 20 09/28/11 22:18 142-28-9 ND ug/L 20.0 2.6 20 09/28/11 22:18 594-20-7 ND ug/L 20.0 9.8 20 09/28/11 22:18 563-58-6 ND ug/L 20.0 2.6 20 09/28/11 22:18 10061-01-5 ND ug/L 20.0 5.2 20 09/28/11 22:18 10061-02-6 ND ug/L 20.0 2.4 20 09/28/11 22:18 108-20-3 ND ug/L 20.0 6.0 20 09/28/11 22:18 100-41-4 ND ug/L 20.0 14.2 20 09/28/11 22:18 87-68-3 ND ug/L 100 9.2 20 09/28/11 22:18 591-78-6 ND ug/L 20.0 6.2 20 09/28/11 22:18 99-87-6 ND ug/L 40.0 19.4 20 09/28/11 22:18 75-09-2 ND ug/L 100 6.6 20 09/28/11 22:18 108-10-1 ND ug/L 20.0 4.2 20 09/28/11 22:18 1634-04-4 ND ug/L 20.0 4.8 20 09/28/11 22:18 91-20-3 ND ug/L 20.0 5.2 20 09/28/11 22:18 100-42-5 ND ug/L 20.0 6.6 20 09/28/11 22:18 630-20-6 ND ug/L 20.0 8.0 20 09/28/11 22:18 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 17 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-12 Labll): 92103091007 Collected: 09/23/11 10:20 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 156 ug/L 20.0 9.2 20 09/28/11 22:18 127-18-4 Toluene ND ug/L 20.0 5.2 20 09/28/11 22:18 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.6 20 09/28/11 22:18 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 7.0 20 09/28/11 22:18 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 9.6 20 09/28/11 22:18 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 5.8 20 09/28/11 22:18 79-00-5 Trichloroethene 44.2 ug/L 20.0 9.4 20 09/28/11 22:18 79-01-6 Trichlorofluoromethane ND ug/L 20.0 4.0 20 09/28/11 22:18 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 8.2 20 09/28/11 22:18 96-18-4 Vinyl acetate ND ug/L 40.0 7.0 20 09/28/11 22:18 108-05-4 Vinyl chloride ND ug/L 20.0 12.4 20 09/28/11 22:18 75-01-4 m&p-Xylene ND ug/L 40.0 13.2 20 09/28/11 22:18 179601-23-1 o-Xylene ND ug/L 20.0 4.6 20 09/28/11 22:18 95-47-6 4-Bromofluorobenzene (S) 94 % 70-130 20 09/28/11 22:18 460-00-4 Dibromofluoromethane (S) 109 % 70-130 20 09/28/11 22:18 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 20 09/28/11 22:18 17060-07-0 Tbluene-d8 (S) 95 % 70-130 20 09/28/11 22:18 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 18 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 Labll): 92103091008 Collected: 09/22/11 15:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 125 10.8 5 09/28/11 22:41 67-64-1 ND ug/L 5.0 1.2 5 09/28/11 22:41 71-43-2 ND ug/L 5.0 1.5 5 09/28/11 22:41 108-86-1 ND ug/L 5.0 0.85 5 09/28/11 22:41 74-97-5 ND ug/L 5.0 0.90 5 09/28/11 22:41 75-27-4 ND ug/L 5.0 1.3 5 09/28/11 22:41 75-25-2 ND ug/L 10.0 1.4 5 09/28/11 22:41 74-83-9 ND ug/L 25.0 4.8 5 09/28/11 22:41 78-93-3 ND ug/L 5.0 1.2 5 09/28/11 22:41 56-23-5 ND ug/L 5.0 1.2 5 09/28/11 22:41 108-90-7 ND ug/L 5.0 2.7 5 09/28/11 22:41 75-00-3 ND ug/L 5.0 0.70 5 09/28/11 22:41 67-66-3 ND ug/L 5.0 0.55 5 09/28/11 22:41 74-87-3 ND ug/L 5.0 1.8 5 09/28/11 22:41 95-49-8 ND ug/L 5.0 1.6 5 09/28/11 22:41 106-43-4 ND ug/L 25.0 12.6 5 09/28/11 22:41 96-12-8 ND ug/L 5.0 1.0 5 09/28/11 22:41 124-48-1 ND ug/L 5.0 1.4 5 09/28/11 22:41 106-93-4 ND ug/L 5.0 1.0 5 09/28/11 22:41 74-95-3 ND ug/L 5.0 1.5 5 09/28/11 22:41 95-50-1 ND ug/L 5.0 1.2 5 09/28/11 22:41 541-73-1 ND ug/L 5.0 1.6 5 09/28/11 22:41 106-46-7 ND ug/L 5.0 1.0 5 09/28/11 22:41 75-71-8 ND ug/L 5.0 1.6 5 09/28/11 22:41 75-34-3 ND ug/L 5.0 0.60 5 09/28/11 22:41 107-06-2 ND ug/L 5.0 2.8 5 09/28/11 22:41 75-35-4 158 ug/L 5.0 0.95 5 09/28/11 22:41 156-59-2 ND ug/L 5.0 2.4 5 09/28/11 22:41 156-60-5 ND ug/L 5.0 1.4 5 09/28/11 22:41 78-87-5 ND ug/L 5.0 1.4 5 09/28/11 22:41 142-28-9 ND ug/L 5.0 0.65 5 09/28/11 22:41 594-20-7 ND ug/L 5.0 2.4 5 09/28/11 22:41 563-58-6 ND ug/L 5.0 0.65 5 09/28/11 22:41 10061-01-5 ND ug/L 5.0 1.3 5 09/28/11 22:41 10061-02-6 ND ug/L 5.0 0.60 5 09/28/11 22:41 108-20-3 ND ug/L 5.0 1.5 5 09/28/11 22:41 100-41-4 ND ug/L 5.0 3.6 5 09/28/11 22:41 87-68-3 ND ug/L 25.0 2.3 5 09/28/11 22:41 591-78-6 ND ug/L 5.0 1.6 5 09/28/11 22:41 99-87-6 ND ug/L 10.0 4.8 5 09/28/11 22:41 75-09-2 ND ug/L 25.0 1.6 5 09/28/11 22:41 108-10-1 ND ug/L 5.0 1.0 5 09/28/11 22:41 1634-04-4 ND ug/L 5.0 1.2 5 09/28/11 22:41 91-20-3 ND ug/L 5.0 1.3 5 09/28/11 22:41 100-42-5 ND ug/L 5.0 1.6 5 09/28/11 22:41 630-20-6 ND ug/L 5.0 2.0 5 09/28/11 22:41 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 19 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 Labll): 92103091008 Collected: 09/22/11 15:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 960 ug/L 10.0 4.6 10 09/29/11 17:32 127-18-4 Toluene ND ug/L 5.0 1.3 5 09/28/11 22:41 108-88-3 1,2,3-Trichlorobenzene ND ug/L 5.0 1.6 5 09/28/11 22:41 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 1.8 5 09/28/11 22:41 120-82-1 1,1,1-Trichloroethane ND ug/L 5.0 2.4 5 09/28/11 22:41 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 1.4 5 09/28/11 22:41 79-00-5 Trichloroethene 304 ug/L 5.0 2.4 5 09/28/11 22:41 79-01-6 Trichlorofluoromethane ND ug/L 5.0 1.0 5 09/28/11 22:41 75-69-4 1,2,3-Trichloropropane ND ug/L 5.0 2.0 5 09/28/11 22:41 96-18-4 Vinyl acetate ND ug/L 10.0 1.8 5 09/28/11 22:41 108-05-4 Vinyl chloride ND ug/L 5.0 3.1 5 09/28/11 22:41 75-01-4 m&p-Xylene ND ug/L 10.0 3.3 5 09/28/11 22:41 179601-23-1 o-Xylene ND ug/L 5.0 1.2 5 09/28/11 22:41 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 5 09/28/11 22:41 460-00-4 Dibromofluoromethane (S) 107 % 70-130 5 09/28/11 22:41 1868-53-7 1,2-Dichloroethane-d4 (S) 112 % 70-130 5 09/28/11 22:41 17060-07-0 Tbluene-d8 (S) 88 % 70-130 5 09/28/11 22:41 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 20 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 Labll): 92103091009 Collected: 09/22/11 14:15 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 125 10.8 5 09/28/11 23:04 67-64-1 ND ug/L 5.0 1.2 5 09/28/11 23:04 71-43-2 ND ug/L 5.0 1.5 5 09/28/11 23:04 108-86-1 ND ug/L 5.0 0.85 5 09/28/11 23:04 74-97-5 ND ug/L 5.0 0.90 5 09/28/11 23:04 75-27-4 ND ug/L 5.0 1.3 5 09/28/11 23:04 75-25-2 ND ug/L 10.0 1.4 5 09/28/11 23:04 74-83-9 ND ug/L 25.0 4.8 5 09/28/11 23:04 78-93-3 ND ug/L 5.0 1.2 5 09/28/11 23:04 56-23-5 ND ug/L 5.0 1.2 5 09/28/11 23:04 108-90-7 ND ug/L 5.0 2.7 5 09/28/11 23:04 75-00-3 ND ug/L 5.0 0.70 5 09/28/11 23:04 67-66-3 ND ug/L 5.0 0.55 5 09/28/11 23:04 74-87-3 ND ug/L 5.0 1.8 5 09/28/11 23:04 95-49-8 ND ug/L 5.0 1.6 5 09/28/11 23:04 106-43-4 ND ug/L 25.0 12.6 5 09/28/11 23:04 96-12-8 ND ug/L 5.0 1.0 5 09/28/11 23:04 124-48-1 ND ug/L 5.0 1.4 5 09/28/11 23:04 106-93-4 ND ug/L 5.0 1.0 5 09/28/11 23:04 74-95-3 ND ug/L 5.0 1.5 5 09/28/11 23:04 95-50-1 ND ug/L 5.0 1.2 5 09/28/11 23:04 541-73-1 ND ug/L 5.0 1.6 5 09/28/11 23:04 106-46-7 ND ug/L 5.0 1.0 5 09/28/11 23:04 75-71-8 ND ug/L 5.0 1.6 5 09/28/11 23:04 75-34-3 ND ug/L 5.0 0.60 5 09/28/11 23:04 107-06-2 ND ug/L 5.0 2.8 5 09/28/11 23:04 75-35-4 136 ug/L 5.0 0.95 5 09/28/11 23:04 156-59-2 ND ug/L 5.0 2.4 5 09/28/11 23:04 156-60-5 ND ug/L 5.0 1.4 5 09/28/11 23:04 78-87-5 ND ug/L 5.0 1.4 5 09/28/11 23:04 142-28-9 ND ug/L 5.0 0.65 5 09/28/11 23:04 594-20-7 ND ug/L 5.0 2.4 5 09/28/11 23:04 563-58-6 ND ug/L 5.0 0.65 5 09/28/11 23:04 10061-01-5 ND ug/L 5.0 1.3 5 09/28/11 23:04 10061-02-6 ND ug/L 5.0 0.60 5 09/28/11 23:04 108-20-3 ND ug/L 5.0 1.5 5 09/28/11 23:04 100-41-4 ND ug/L 5.0 3.6 5 09/28/11 23:04 87-68-3 ND ug/L 25.0 2.3 5 09/28/11 23:04 591-78-6 ND ug/L 5.0 1.6 5 09/28/11 23:04 99-87-6 ND ug/L 10.0 4.8 5 09/28/11 23:04 75-09-2 ND ug/L 25.0 1.6 5 09/28/11 23:04 108-10-1 ND ug/L 5.0 1.0 5 09/28/11 23:04 1634-04-4 ND ug/L 5.0 1.2 5 09/28/11 23:04 91-20-3 ND ug/L 5.0 1.3 5 09/28/11 23:04 100-42-5 ND ug/L 5.0 1.6 5 09/28/11 23:04 630-20-6 ND ug/L 5.0 2.0 5 09/28/11 23:04 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 21 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 Labll): 92103091009 Collected: 09/22/11 14:15 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 997 ug/L 5.0 2.3 5 09/28/11 23:04 127-18-4 Toluene ND ug/L 5.0 1.3 5 09/28/11 23:04 108-88-3 1,2,3-Trichlorobenzene ND ug/L 5.0 1.6 5 09/28/11 23:04 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 1.8 5 09/28/11 23:04 120-82-1 1,1,1-Trichloroethane ND ug/L 5.0 2.4 5 09/28/11 23:04 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 1.4 5 09/28/11 23:04 79-00-5 Trichloroethene 331 ug/L 5.0 2.4 5 09/28/11 23:04 79-01-6 Trichlorofluoromethane ND ug/L 5.0 1.0 5 09/28/11 23:04 75-69-4 1,2,3-Trichloropropane ND ug/L 5.0 2.0 5 09/28/11 23:04 96-18-4 Vinyl acetate ND ug/L 10.0 1.8 5 09/28/11 23:04 108-05-4 Vinyl chloride ND ug/L 5.0 3.1 5 09/28/11 23:04 75-01-4 m&p-Xylene ND ug/L 10.0 3.3 5 09/28/11 23:04 179601-23-1 o-Xylene ND ug/L 5.0 1.2 5 09/28/11 23:04 95-47-6 4-Bromofluorobenzene (S) 90 % 70-130 5 09/28/11 23:04 460-00-4 Dibromofluoromethane (S) 106 % 70-130 5 09/28/11 23:04 1868-53-7 1,2-Dichloroethane-d4 (S) 115 % 70-130 5 09/28/11 23:04 17060-07-0 Tbluene-d8 (S) 89 % 70-130 5 09/28/11 23:04 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 22 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-15 Labll): 92103091010 Collected: 09/22/11 10:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/01/11 16:07 67-64-1 ND ug/L 1.0 0.25 1 10/01/11 16:07 71-43-2 ND ug/L 1.0 0.30 1 10/01/11 16:07 108-86-1 ND ug/L 1.0 0.17 1 10/01/11 16:07 74-97-5 ND ug/L 1.0 0.18 1 10/01/11 16:07 75-27-4 ND ug/L 1.0 0.26 1 10/01/11 16:07 75-25-2 ND ug/L 2.0 0.29 1 10/01/11 16:07 74-83-9 ND ug/L 5.0 0.96 1 10/01/11 16:07 78-93-3 ND ug/L 1.0 0.25 1 10/01/11 16:07 56-23-5 ND ug/L 1.0 0.23 1 10/01/11 16:07 108-90-7 ND ug/L 1.0 0.54 1 10/01/11 16:07 75-00-3 0.98J ug/L 1.0 0.14 1 10/01/11 16:07 67-66-3 ND ug/L 1.0 0.11 1 10/01/11 16:07 74-87-3 ND ug/L 1.0 0.35 1 10/01/11 16:07 95-49-8 ND ug/L 1.0 0.31 1 10/01/11 16:07 106-43-4 ND ug/L 5.0 2.5 1 10/01/11 16:07 96-12-8 ND ug/L 1.0 0.21 1 10/01/11 16:07 124-48-1 ND ug/L 1.0 0.27 1 10/01/11 16:07 106-93-4 ND ug/L 1.0 0.21 1 10/01/11 16:07 74-95-3 ND ug/L 1.0 0.30 1 10/01/11 16:07 95-50-1 ND ug/L 1.0 0.24 1 10/01/11 16:07 541-73-1 ND ug/L 1.0 0.33 1 10/01/11 16:07 106-46-7 ND ug/L 1.0 0.21 1 10/01/11 16:07 75-71-8 ND ug/L 1.0 0.32 1 10/01/11 16:07 75-34-3 ND ug/L 1.0 0.12 1 10/01/11 16:07 107-06-2 ND ug/L 1.0 0.56 1 10/01/11 16:07 75-35-4 9.4 ug/L 1.0 0.19 1 10/01/11 16:07 156-59-2 ND ug/L 1.0 0.49 1 10/01/11 16:07 156-60-5 ND ug/L 1.0 0.27 1 10/01/11 16:07 78-87-5 ND ug/L 1.0 0.28 1 10/01/11 16:07 142-28-9 ND ug/L 1.0 0.13 1 10/01/11 16:07 594-20-7 ND ug/L 1.0 0.49 1 10/01/11 16:07 563-58-6 ND ug/L 1.0 0.13 1 10/01/11 16:07 10061-01-5 ND ug/L 1.0 0.26 1 10/01/11 16:07 10061-02-6 ND ug/L 1.0 0.12 1 10/01/11 16:07 108-20-3 ND ug/L 1.0 0.30 1 10/01/11 16:07 100-41-4 ND ug/L 1.0 0.71 1 10/01/11 16:07 87-68-3 ND ug/L 5.0 0.46 1 10/01/11 16:07 591-78-6 ND ug/L 1.0 0.31 1 10/01/11 16:07 99-87-6 ND ug/L 2.0 0.97 1 10/01/11 16:07 75-09-2 ND ug/L 5.0 0.33 1 10/01/11 16:07 108-10-1 ND ug/L 1.0 0.21 1 10/01/11 16:07 1634-04-4 ND ug/L 1.0 0.24 1 10/01/11 16:07 91-20-3 ND ug/L 1.0 0.26 1 10/01/11 16:07 100-42-5 ND ug/L 1.0 0.33 1 10/01/11 16:07 630-20-6 ND ug/L 1.0 0.40 1 10/01/11 16:07 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 23 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-15 Labll): 92103091010 Collected: 09/22/11 10:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 194 ug/L 1.0 0.46 1 10/01/11 16:07 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/01/11 16:07 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/01/11 16:07 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/01/11 16:07 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/01/11 16:07 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/01/11 16:07 79-00-5 Trichloroethene 3.9 ug/L 1.0 0.47 1 10/01/11 16:07 79-01-6 Trichlorofluoromethane 1.2 ug/L 1.0 0.20 1 10/01/11 16:07 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/01/11 16:07 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/01/11 16:07 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/01/11 16:07 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/01/11 16:07 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/01/11 16:07 95-47-6 4-Bromofluorobenzene (S) 94 % 70-130 1 10/01/11 16:07 460-00-4 Dibromofluoromethane (S) 102 % 70-130 1 10/01/11 16:07 1868-53-7 1,2-Dichloroethane-d4 (S) 112 % 70-130 1 10/01/11 16:07 17060-07-0 Tbluene-d8 (S) 103 % 70-130 1 10/01/11 16:07 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 24 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 Labll): 92103091011 Collected: 09/22/11 09:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 62.5 5.4 2.5 09/28/11 23:49 67-64-1 ND ug/L 2.5 0.62 2.5 09/28/11 23:49 71-43-2 ND ug/L 2.5 0.75 2.5 09/28/11 23:49 108-86-1 ND ug/L 2.5 0.42 2.5 09/28/11 23:49 74-97-5 ND ug/L 2.5 0.45 2.5 09/28/11 23:49 75-27-4 ND ug/L 2.5 0.65 2.5 09/28/11 23:49 75-25-2 ND ug/L 5.0 0.72 2.5 09/28/11 23:49 74-83-9 ND ug/L 12.5 2.4 2.5 09/28/11 23:49 78-93-3 ND ug/L 2.5 0.62 2.5 09/28/11 23:49 56-23-5 ND ug/L 2.5 0.58 2.5 09/28/11 23:49 108-90-7 ND ug/L 2.5 1.4 2.5 09/28/11 23:49 75-00-3 1.5J ug/L 2.5 0.35 2.5 09/28/11 23:49 67-66-3 ND ug/L 2.5 0.28 2.5 09/28/11 23:49 74-87-3 ND ug/L 2.5 0.88 2.5 09/28/11 23:49 95-49-8 ND ug/L 2.5 0.78 2.5 09/28/11 23:49 106-43-4 ND ug/L 12.5 6.3 2.5 09/28/11 23:49 96-12-8 ND ug/L 2.5 0.52 2.5 09/28/11 23:49 124-48-1 ND ug/L 2.5 0.68 2.5 09/28/11 23:49 106-93-4 ND ug/L 2.5 0.52 2.5 09/28/11 23:49 74-95-3 ND ug/L 2.5 0.75 2.5 09/28/11 23:49 95-50-1 ND ug/L 2.5 0.60 2.5 09/28/11 23:49 541-73-1 ND ug/L 2.5 0.82 2.5 09/28/11 23:49 106-46-7 ND ug/L 2.5 0.52 2.5 09/28/11 23:49 75-71-8 ND ug/L 2.5 0.80 2.5 09/28/11 23:49 75-34-3 ND ug/L 2.5 0.30 2.5 09/28/11 23:49 107-06-2 ND ug/L 2.5 1.4 2.5 09/28/11 23:49 75-35-4 10.6 ug/L 2.5 0.48 2.5 09/28/11 23:49 156-59-2 ND ug/L 2.5 1.2 2.5 09/28/11 23:49 156-60-5 ND ug/L 2.5 0.68 2.5 09/28/11 23:49 78-87-5 ND ug/L 2.5 0.70 2.5 09/28/11 23:49 142-28-9 ND ug/L 2.5 0.32 2.5 09/28/11 23:49 594-20-7 ND ug/L 2.5 1.2 2.5 09/28/11 23:49 563-58-6 ND ug/L 2.5 0.32 2.5 09/28/11 23:49 10061-01-5 ND ug/L 2.5 0.65 2.5 09/28/11 23:49 10061-02-6 ND ug/L 2.5 0.30 2.5 09/28/11 23:49 108-20-3 ND ug/L 2.5 0.75 2.5 09/28/11 23:49 100-41-4 ND ug/L 2.5 1.8 2.5 09/28/11 23:49 87-68-3 ND ug/L 12.5 1.2 2.5 09/28/11 23:49 591-78-6 ND ug/L 2.5 0.78 2.5 09/28/11 23:49 99-87-6 ND ug/L 5.0 2.4 2.5 09/28/11 23:49 75-09-2 ND ug/L 12.5 0.82 2.5 09/28/11 23:49 108-10-1 ND ug/L 2.5 0.52 2.5 09/28/11 23:49 1634-04-4 ND ug/L 2.5 0.60 2.5 09/28/11 23:49 91-20-3 ND ug/L 2.5 0.65 2.5 09/28/11 23:49 100-42-5 ND ug/L 2.5 0.82 2.5 09/28/11 23:49 630-20-6 ND ug/L 2.5 1.0 2.5 09/28/11 23:49 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 25 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 Labll): 92103091011 Collected: 09/22/11 09:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 249 ug/L 2.5 1.2 2.5 09/28/11 23:49 127-18-4 Toluene ND ug/L 2.5 0.65 2.5 09/28/11 23:49 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.5 0.82 2.5 09/28/11 23:49 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.5 0.88 2.5 09/28/11 23:49 120-82-1 1,1,1-Trichloroethane ND ug/L 2.5 1.2 2.5 09/28/11 23:49 71-55-6 1,1,2-Trichloroethane ND ug/L 2.5 0.72 2.5 09/28/11 23:49 79-00-5 Trichloroethene 4.9 ug/L 2.5 1.2 2.5 09/28/11 23:49 79-01-6 Trichlorofluoromethane 1.8J ug/L 2.5 0.50 2.5 09/28/11 23:49 75-69-4 1,2,3-Trichloropropane ND ug/L 2.5 1.0 2.5 09/28/11 23:49 96-18-4 Vinyl acetate ND ug/L 5.0 0.88 2.5 09/28/11 23:49 108-05-4 Vinyl chloride ND ug/L 2.5 1.6 2.5 09/28/11 23:49 75-01-4 m&p-Xylene ND ug/L 5.0 1.6 2.5 09/28/11 23:49 179601-23-1 o-Xylene ND ug/L 2.5 0.58 2.5 09/28/11 23:49 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 2.5 09/28/11 23:49 460-00-4 Dibromofluoromethane (S) 105 % 70-130 2.5 09/28/11 23:49 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 2.5 09/28/11 23:49 17060-07-0 Tbluene-d8 (S) 91 % 70-130 2.5 09/28/11 23:49 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 26 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-17 Labll): 92103091012 Collected: 09/22/11 09:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/28/11 19:38 67-64-1 ND ug/L 1.0 0.25 1 09/28/11 19:38 71-43-2 ND ug/L 1.0 0.30 1 09/28/11 19:38 108-86-1 ND ug/L 1.0 0.17 1 09/28/11 19:38 74-97-5 ND ug/L 1.0 0.18 1 09/28/11 19:38 75-27-4 ND ug/L 1.0 0.26 1 09/28/11 19:38 75-25-2 ND ug/L 2.0 0.29 1 09/28/11 19:38 74-83-9 ND ug/L 5.0 0.96 1 09/28/11 19:38 78-93-3 ND ug/L 1.0 0.25 1 09/28/11 19:38 56-23-5 ND ug/L 1.0 0.23 1 09/28/11 19:38 108-90-7 ND ug/L 1.0 0.54 1 09/28/11 19:38 75-00-3 ND ug/L 1.0 0.14 1 09/28/11 19:38 67-66-3 0.33J ug/L 1.0 0.11 1 09/28/11 19:38 74-87-3 ND ug/L 1.0 0.35 1 09/28/11 19:38 95-49-8 ND ug/L 1.0 0.31 1 09/28/11 19:38 106-43-4 ND ug/L 5.0 2.5 1 09/28/11 19:38 96-12-8 ND ug/L 1.0 0.21 1 09/28/11 19:38 124-48-1 ND ug/L 1.0 0.27 1 09/28/11 19:38 106-93-4 ND ug/L 1.0 0.21 1 09/28/11 19:38 74-95-3 ND ug/L 1.0 0.30 1 09/28/11 19:38 95-50-1 ND ug/L 1.0 0.24 1 09/28/11 19:38 541-73-1 ND ug/L 1.0 0.33 1 09/28/11 19:38 106-46-7 ND ug/L 1.0 0.21 1 09/28/11 19:38 75-71-8 ND ug/L 1.0 0.32 1 09/28/11 19:38 75-34-3 ND ug/L 1.0 0.12 1 09/28/11 19:38 107-06-2 ND ug/L 1.0 0.56 1 09/28/11 19:38 75-35-4 15.6 ug/L 1.0 0.19 1 09/28/11 19:38 156-59-2 ND ug/L 1.0 0.49 1 09/28/11 19:38 156-60-5 ND ug/L 1.0 0.27 1 09/28/11 19:38 78-87-5 ND ug/L 1.0 0.28 1 09/28/11 19:38 142-28-9 ND ug/L 1.0 0.13 1 09/28/11 19:38 594-20-7 ND ug/L 1.0 0.49 1 09/28/11 19:38 563-58-6 ND ug/L 1.0 0.13 1 09/28/11 19:38 10061-01-5 ND ug/L 1.0 0.26 1 09/28/11 19:38 10061-02-6 ND ug/L 1.0 0.12 1 09/28/11 19:38 108-20-3 ND ug/L 1.0 0.30 1 09/28/11 19:38 100-41-4 ND ug/L 1.0 0.71 1 09/28/11 19:38 87-68-3 ND ug/L 5.0 0.46 1 09/28/11 19:38 591-78-6 ND ug/L 1.0 0.31 1 09/28/11 19:38 99-87-6 ND ug/L 2.0 0.97 1 09/28/11 19:38 75-09-2 ND ug/L 5.0 0.33 1 09/28/11 19:38 108-10-1 ND ug/L 1.0 0.21 1 09/28/11 19:38 1634-04-4 ND ug/L 1.0 0.24 1 09/28/11 19:38 91-20-3 ND ug/L 1.0 0.26 1 09/28/11 19:38 100-42-5 ND ug/L 1.0 0.33 1 09/28/11 19:38 630-20-6 ND ug/L 1.0 0.40 1 09/28/11 19:38 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 27 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-17 Labll): 92103091012 Collected: 09/22/11 09:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 7.5 ug/L 1.0 0.46 1 09/28/11 19:38 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/28/11 19:38 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/28/11 19:38 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/28/11 19:38 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/28/11 19:38 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/28/11 19:38 79-00-5 Trichloroethene 3.4 ug/L 1.0 0.47 1 09/28/11 19:38 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/28/11 19:38 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/28/11 19:38 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/28/11 19:38 108-05-4 Vinyl chloride 7.6 ug/L 1.0 0.62 1 09/28/11 19:38 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/28/11 19:38 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/28/11 19:38 95-47-6 4-Bromofluorobenzene (S) 93 % 70-130 1 09/28/11 19:38 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/28/11 19:38 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 1 09/28/11 19:38 17060-07-0 Tbluene-d8 (S) 90 % 70-130 1 09/28/11 19:38 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 28 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-18 Labll): 92103091013 Collected: 09/22/11 11:30 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/04/11 04:51 67-64-1 ND ug/L 1.0 0.25 1 10/04/11 04:51 71-43-2 ND ug/L 1.0 0.30 1 10/04/11 04:51 108-86-1 ND ug/L 1.0 0.17 1 10/04/11 04:51 74-97-5 ND ug/L 1.0 0.18 1 10/04/11 04:51 75-27-4 ND ug/L 1.0 0.26 1 10/04/11 04:51 75-25-2 ND ug/L 2.0 0.29 1 10/04/11 04:51 74-83-9 ND ug/L 5.0 0.96 1 10/04/11 04:51 78-93-3 ND ug/L 1.0 0.25 1 10/04/11 04:51 56-23-5 ND ug/L 1.0 0.23 1 10/04/11 04:51 108-90-7 ND ug/L 1.0 0.54 1 10/04/11 04:51 75-00-3 1.4 ug/L 1.0 0.14 1 10/04/11 04:51 67-66-3 0.43J ug/L 1.0 0.11 1 10/04/11 04:51 74-87-3 ND ug/L 1.0 0.35 1 10/04/11 04:51 95-49-8 ND ug/L 1.0 0.31 1 10/04/11 04:51 106-43-4 ND ug/L 5.0 2.5 1 10/04/11 04:51 96-12-8 ND ug/L 1.0 0.21 1 10/04/11 04:51 124-48-1 ND ug/L 1.0 0.27 1 10/04/11 04:51 106-93-4 ND ug/L 1.0 0.21 1 10/04/11 04:51 74-95-3 ND ug/L 1.0 0.30 1 10/04/11 04:51 95-50-1 ND ug/L 1.0 0.24 1 10/04/11 04:51 541-73-1 ND ug/L 1.0 0.33 1 10/04/11 04:51 106-46-7 ND ug/L 1.0 0.21 1 10/04/11 04:51 75-71-8 ND ug/L 1.0 0.32 1 10/04/11 04:51 75-34-3 ND ug/L 1.0 0.12 1 10/04/11 04:51 107-06-2 ND ug/L 1.0 0.56 1 10/04/11 04:51 75-35-4 ND ug/L 1.0 0.19 1 10/04/11 04:51 156-59-2 ND ug/L 1.0 0.49 1 10/04/11 04:51 156-60-5 ND ug/L 1.0 0.27 1 10/04/11 04:51 78-87-5 ND ug/L 1.0 0.28 1 10/04/11 04:51 142-28-9 ND ug/L 1.0 0.13 1 10/04/11 04:51 594-20-7 ND ug/L 1.0 0.49 1 10/04/11 04:51 563-58-6 ND ug/L 1.0 0.13 1 10/04/11 04:51 10061-01-5 ND ug/L 1.0 0.26 1 10/04/11 04:51 10061-02-6 ND ug/L 1.0 0.12 1 10/04/11 04:51 108-20-3 ND ug/L 1.0 0.30 1 10/04/11 04:51 100-41-4 ND ug/L 1.0 0.71 1 10/04/11 04:51 87-68-3 ND ug/L 5.0 0.46 1 10/04/11 04:51 591-78-6 ND ug/L 1.0 0.31 1 10/04/11 04:51 99-87-6 ND ug/L 2.0 0.97 1 10/04/11 04:51 75-09-2 ND ug/L 5.0 0.33 1 10/04/11 04:51 108-10-1 ND ug/L 1.0 0.21 1 10/04/11 04:51 1634-04-4 ND ug/L 1.0 0.24 1 10/04/11 04:51 91-20-3 ND ug/L 1.0 0.26 1 10/04/11 04:51 100-42-5 ND ug/L 1.0 0.33 1 10/04/11 04:51 630-20-6 ND ug/L 1.0 0.40 1 10/04/11 04:51 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 29 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-18 Labll): 92103091013 Collected: 09/22/11 11:30 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 7.1 ug/L 1.0 0.46 1 10/04/11 04:51 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/04/11 04:51 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/04/11 04:51 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/04/11 04:51 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/04/11 04:51 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/04/11 04:51 79-00-5 Trichloroethene 0.72J ug/L 1.0 0.47 1 10/04/11 04:51 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/04/11 04:51 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/04/11 04:51 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/04/11 04:51 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/04/11 04:51 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/04/11 04:51 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/04/11 04:51 95-47-6 4-Bromofluorobenzene (S) 103 % 70-130 1 10/04/11 04:51 460-00-4 Dibromofluoromethane (S) 88 % 70-130 1 10/04/11 04:51 1868-53-7 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 10/04/11 04:51 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 10/04/11 04:51 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 30 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-20 Labll): 92103091014 Collected: 09/22/11 13:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/28/11 16:58 67-64-1 ND ug/L 1.0 0.25 1 09/28/11 16:58 71-43-2 ND ug/L 1.0 0.30 1 09/28/11 16:58 108-86-1 ND ug/L 1.0 0.17 1 09/28/11 16:58 74-97-5 ND ug/L 1.0 0.18 1 09/28/11 16:58 75-27-4 ND ug/L 1.0 0.26 1 09/28/11 16:58 75-25-2 ND ug/L 2.0 0.29 1 09/28/11 16:58 74-83-9 ND ug/L 5.0 0.96 1 09/28/11 16:58 78-93-3 ND ug/L 1.0 0.25 1 09/28/11 16:58 56-23-5 ND ug/L 1.0 0.23 1 09/28/11 16:58 108-90-7 ND ug/L 1.0 0.54 1 09/28/11 16:58 75-00-3 0.72J ug/L 1.0 0.14 1 09/28/11 16:58 67-66-3 ND ug/L 1.0 0.11 1 09/28/11 16:58 74-87-3 ND ug/L 1.0 0.35 1 09/28/11 16:58 95-49-8 ND ug/L 1.0 0.31 1 09/28/11 16:58 106-43-4 ND ug/L 5.0 2.5 1 09/28/11 16:58 96-12-8 ND ug/L 1.0 0.21 1 09/28/11 16:58 124-48-1 ND ug/L 1.0 0.27 1 09/28/11 16:58 106-93-4 ND ug/L 1.0 0.21 1 09/28/11 16:58 74-95-3 ND ug/L 1.0 0.30 1 09/28/11 16:58 95-50-1 ND ug/L 1.0 0.24 1 09/28/11 16:58 541-73-1 ND ug/L 1.0 0.33 1 09/28/11 16:58 106-46-7 ND ug/L 1.0 0.21 1 09/28/11 16:58 75-71-8 ND ug/L 1.0 0.32 1 09/28/11 16:58 75-34-3 ND ug/L 1.0 0.12 1 09/28/11 16:58 107-06-2 ND ug/L 1.0 0.56 1 09/28/11 16:58 75-35-4 ND ug/L 1.0 0.19 1 09/28/11 16:58 156-59-2 ND ug/L 1.0 0.49 1 09/28/11 16:58 156-60-5 ND ug/L 1.0 0.27 1 09/28/11 16:58 78-87-5 ND ug/L 1.0 0.28 1 09/28/11 16:58 142-28-9 ND ug/L 1.0 0.13 1 09/28/11 16:58 594-20-7 ND ug/L 1.0 0.49 1 09/28/11 16:58 563-58-6 ND ug/L 1.0 0.13 1 09/28/11 16:58 10061-01-5 ND ug/L 1.0 0.26 1 09/28/11 16:58 10061-02-6 ND ug/L 1.0 0.12 1 09/28/11 16:58 108-20-3 ND ug/L 1.0 0.30 1 09/28/11 16:58 100-41-4 ND ug/L 1.0 0.71 1 09/28/11 16:58 87-68-3 ND ug/L 5.0 0.46 1 09/28/11 16:58 591-78-6 ND ug/L 1.0 0.31 1 09/28/11 16:58 99-87-6 ND ug/L 2.0 0.97 1 09/28/11 16:58 75-09-2 ND ug/L 5.0 0.33 1 09/28/11 16:58 108-10-1 ND ug/L 1.0 0.21 1 09/28/11 16:58 1634-04-4 ND ug/L 1.0 0.24 1 09/28/11 16:58 91-20-3 ND ug/L 1.0 0.26 1 09/28/11 16:58 100-42-5 ND ug/L 1.0 0.33 1 09/28/11 16:58 630-20-6 ND ug/L 1.0 0.40 1 09/28/11 16:58 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 31 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-20 Labll): 92103091014 Collected: 09/22/11 13:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/28/11 16:58 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/28/11 16:58 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/28/11 16:58 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/28/11 16:58 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/28/11 16:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/28/11 16:58 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/28/11 16:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/28/11 16:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/28/11 16:58 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/28/11 16:58 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/28/11 16:58 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/28/11 16:58 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/28/11 16:58 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 1 09/28/11 16:58 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/28/11 16:58 1868-53-7 1,2-Dichloroethane-d4 (S) 118 % 70-130 1 09/28/11 16:58 17060-07-0 Tbluene-d8 (S) 94 % 70-130 1 09/28/11 16:58 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 32 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-21 Labll): 92103091015 Collected: 09/21/11 16:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/28/11 17:21 67-64-1 ND ug/L 1.0 0.25 1 09/28/11 17:21 71-43-2 ND ug/L 1.0 0.30 1 09/28/11 17:21 108-86-1 ND ug/L 1.0 0.17 1 09/28/11 17:21 74-97-5 ND ug/L 1.0 0.18 1 09/28/11 17:21 75-27-4 ND ug/L 1.0 0.26 1 09/28/11 17:21 75-25-2 ND ug/L 2.0 0.29 1 09/28/11 17:21 74-83-9 ND ug/L 5.0 0.96 1 09/28/11 17:21 78-93-3 ND ug/L 1.0 0.25 1 09/28/11 17:21 56-23-5 ND ug/L 1.0 0.23 1 09/28/11 17:21 108-90-7 ND ug/L 1.0 0.54 1 09/28/11 17:21 75-00-3 0.88J ug/L 1.0 0.14 1 09/28/11 17:21 67-66-3 ND ug/L 1.0 0.11 1 09/28/11 17:21 74-87-3 ND ug/L 1.0 0.35 1 09/28/11 17:21 95-49-8 ND ug/L 1.0 0.31 1 09/28/11 17:21 106-43-4 ND ug/L 5.0 2.5 1 09/28/11 17:21 96-12-8 ND ug/L 1.0 0.21 1 09/28/11 17:21 124-48-1 ND ug/L 1.0 0.27 1 09/28/11 17:21 106-93-4 ND ug/L 1.0 0.21 1 09/28/11 17:21 74-95-3 ND ug/L 1.0 0.30 1 09/28/11 17:21 95-50-1 ND ug/L 1.0 0.24 1 09/28/11 17:21 541-73-1 ND ug/L 1.0 0.33 1 09/28/11 17:21 106-46-7 ND ug/L 1.0 0.21 1 09/28/11 17:21 75-71-8 ND ug/L 1.0 0.32 1 09/28/11 17:21 75-34-3 ND ug/L 1.0 0.12 1 09/28/11 17:21 107-06-2 ND ug/L 1.0 0.56 1 09/28/11 17:21 75-35-4 ND ug/L 1.0 0.19 1 09/28/11 17:21 156-59-2 ND ug/L 1.0 0.49 1 09/28/11 17:21 156-60-5 ND ug/L 1.0 0.27 1 09/28/11 17:21 78-87-5 ND ug/L 1.0 0.28 1 09/28/11 17:21 142-28-9 ND ug/L 1.0 0.13 1 09/28/11 17:21 594-20-7 ND ug/L 1.0 0.49 1 09/28/11 17:21 563-58-6 ND ug/L 1.0 0.13 1 09/28/11 17:21 10061-01-5 ND ug/L 1.0 0.26 1 09/28/11 17:21 10061-02-6 ND ug/L 1.0 0.12 1 09/28/11 17:21 108-20-3 ND ug/L 1.0 0.30 1 09/28/11 17:21 100-41-4 ND ug/L 1.0 0.71 1 09/28/11 17:21 87-68-3 ND ug/L 5.0 0.46 1 09/28/11 17:21 591-78-6 ND ug/L 1.0 0.31 1 09/28/11 17:21 99-87-6 ND ug/L 2.0 0.97 1 09/28/11 17:21 75-09-2 ND ug/L 5.0 0.33 1 09/28/11 17:21 108-10-1 ND ug/L 1.0 0.21 1 09/28/11 17:21 1634-04-4 ND ug/L 1.0 0.24 1 09/28/11 17:21 91-20-3 ND ug/L 1.0 0.26 1 09/28/11 17:21 100-42-5 ND ug/L 1.0 0.33 1 09/28/11 17:21 630-20-6 ND ug/L 1.0 0.40 1 09/28/11 17:21 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 33 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-21 Labll): 92103091015 Collected: 09/21/11 16:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/28/11 17:21 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/28/11 17:21 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/28/11 17:21 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/28/11 17:21 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/28/11 17:21 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/28/11 17:21 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/28/11 17:21 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/28/11 17:21 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/28/11 17:21 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/28/11 17:21 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/28/11 17:21 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/28/11 17:21 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/28/11 17:21 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 1 09/28/11 17:21 460-00-4 Dibromofluoromethane (S) 108 % 70-130 1 09/28/11 17:21 1868-53-7 1,2-Dichloroethane-d4 (S) 116 % 70-130 1 09/28/11 17:21 17060-07-0 Tbluene-d8 (S) 92 % 70-130 1 09/28/11 17:21 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 34 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-22 Labll): 92103091016 Collected: 09/21/11 15:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/28/11 17:44 67-64-1 ND ug/L 1.0 0.25 1 09/28/11 17:44 71-43-2 ND ug/L 1.0 0.30 1 09/28/11 17:44 108-86-1 ND ug/L 1.0 0.17 1 09/28/11 17:44 74-97-5 ND ug/L 1.0 0.18 1 09/28/11 17:44 75-27-4 ND ug/L 1.0 0.26 1 09/28/11 17:44 75-25-2 ND ug/L 2.0 0.29 1 09/28/11 17:44 74-83-9 ND ug/L 5.0 0.96 1 09/28/11 17:44 78-93-3 ND ug/L 1.0 0.25 1 09/28/11 17:44 56-23-5 ND ug/L 1.0 0.23 1 09/28/11 17:44 108-90-7 ND ug/L 1.0 0.54 1 09/28/11 17:44 75-00-3 ND ug/L 1.0 0.14 1 09/28/11 17:44 67-66-3 ND ug/L 1.0 0.11 1 09/28/11 17:44 74-87-3 ND ug/L 1.0 0.35 1 09/28/11 17:44 95-49-8 ND ug/L 1.0 0.31 1 09/28/11 17:44 106-43-4 ND ug/L 5.0 2.5 1 09/28/11 17:44 96-12-8 ND ug/L 1.0 0.21 1 09/28/11 17:44 124-48-1 ND ug/L 1.0 0.27 1 09/28/11 17:44 106-93-4 ND ug/L 1.0 0.21 1 09/28/11 17:44 74-95-3 ND ug/L 1.0 0.30 1 09/28/11 17:44 95-50-1 ND ug/L 1.0 0.24 1 09/28/11 17:44 541-73-1 ND ug/L 1.0 0.33 1 09/28/11 17:44 106-46-7 ND ug/L 1.0 0.21 1 09/28/11 17:44 75-71-8 ND ug/L 1.0 0.32 1 09/28/11 17:44 75-34-3 ND ug/L 1.0 0.12 1 09/28/11 17:44 107-06-2 ND ug/L 1.0 0.56 1 09/28/11 17:44 75-35-4 ND ug/L 1.0 0.19 1 09/28/11 17:44 156-59-2 ND ug/L 1.0 0.49 1 09/28/11 17:44 156-60-5 ND ug/L 1.0 0.27 1 09/28/11 17:44 78-87-5 ND ug/L 1.0 0.28 1 09/28/11 17:44 142-28-9 ND ug/L 1.0 0.13 1 09/28/11 17:44 594-20-7 ND ug/L 1.0 0.49 1 09/28/11 17:44 563-58-6 ND ug/L 1.0 0.13 1 09/28/11 17:44 10061-01-5 ND ug/L 1.0 0.26 1 09/28/11 17:44 10061-02-6 0.14J ug/L 1.0 0.12 1 09/28/11 17:44 108-20-3 ND ug/L 1.0 0.30 1 09/28/11 17:44 100-41-4 ND ug/L 1.0 0.71 1 09/28/11 17:44 87-68-3 ND ug/L 5.0 0.46 1 09/28/11 17:44 591-78-6 ND ug/L 1.0 0.31 1 09/28/11 17:44 99-87-6 ND ug/L 2.0 0.97 1 09/28/11 17:44 75-09-2 ND ug/L 5.0 0.33 1 09/28/11 17:44 108-10-1 0.32J ug/L 1.0 0.21 1 09/28/11 17:44 1634-04-4 ND ug/L 1.0 0.24 1 09/28/11 17:44 91-20-3 ND ug/L 1.0 0.26 1 09/28/11 17:44 100-42-5 ND ug/L 1.0 0.33 1 09/28/11 17:44 630-20-6 ND ug/L 1.0 0.40 1 09/28/11 17:44 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 35 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-22 Labll): 92103091016 Collected: 09/21/11 15:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/28/11 17:44 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/28/11 17:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/28/11 17:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/28/11 17:44 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/28/11 17:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/28/11 17:44 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/28/11 17:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/28/11 17:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/28/11 17:44 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/28/11 17:44 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/28/11 17:44 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/28/11 17:44 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/28/11 17:44 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 1 09/28/11 17:44 460-00-4 Dibromofluoromethane (S) 108 % 70-130 1 09/28/11 17:44 1868-53-7 1,2-Dichloroethane-d4 (S) 116 % 70-130 1 09/28/11 17:44 17060-07-0 Tbluene-d8 (S) 90 % 70-130 1 09/28/11 17:44 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 36 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-23 Labll): 92103091017 Collected: 09/23/11 15:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/29/11 05:33 67-64-1 ND ug/L 1.0 0.25 1 09/29/11 05:33 71-43-2 ND ug/L 1.0 0.30 1 09/29/11 05:33 108-86-1 ND ug/L 1.0 0.17 1 09/29/11 05:33 74-97-5 ND ug/L 1.0 0.18 1 09/29/11 05:33 75-27-4 ND ug/L 1.0 0.26 1 09/29/11 05:33 75-25-2 ND ug/L 2.0 0.29 1 09/29/11 05:33 74-83-9 ND ug/L 5.0 0.96 1 09/29/11 05:33 78-93-3 ND ug/L 1.0 0.25 1 09/29/11 05:33 56-23-5 ND ug/L 1.0 0.23 1 09/29/11 05:33 108-90-7 ND ug/L 1.0 0.54 1 09/29/11 05:33 75-00-3 ND ug/L 1.0 0.14 1 09/29/11 05:33 67-66-3 ND ug/L 1.0 0.11 1 09/29/11 05:33 74-87-3 ND ug/L 1.0 0.35 1 09/29/11 05:33 95-49-8 ND ug/L 1.0 0.31 1 09/29/11 05:33 106-43-4 ND ug/L 5.0 2.5 1 09/29/11 05:33 96-12-8 ND ug/L 1.0 0.21 1 09/29/11 05:33 124-48-1 ND ug/L 1.0 0.27 1 09/29/11 05:33 106-93-4 ND ug/L 1.0 0.21 1 09/29/11 05:33 74-95-3 ND ug/L 1.0 0.30 1 09/29/11 05:33 95-50-1 ND ug/L 1.0 0.24 1 09/29/11 05:33 541-73-1 ND ug/L 1.0 0.33 1 09/29/11 05:33 106-46-7 ND ug/L 1.0 0.21 1 09/29/11 05:33 75-71-8 ND ug/L 1.0 0.32 1 09/29/11 05:33 75-34-3 ND ug/L 1.0 0.12 1 09/29/11 05:33 107-06-2 ND ug/L 1.0 0.56 1 09/29/11 05:33 75-35-4 12.4 ug/L 1.0 0.19 1 09/29/11 05:33 156-59-2 ND ug/L 1.0 0.49 1 09/29/11 05:33 156-60-5 ND ug/L 1.0 0.27 1 09/29/11 05:33 78-87-5 ND ug/L 1.0 0.28 1 09/29/11 05:33 142-28-9 ND ug/L 1.0 0.13 1 09/29/11 05:33 594-20-7 ND ug/L 1.0 0.49 1 09/29/11 05:33 563-58-6 ND ug/L 1.0 0.13 1 09/29/11 05:33 10061-01-5 ND ug/L 1.0 0.26 1 09/29/11 05:33 10061-02-6 ND ug/L 1.0 0.12 1 09/29/11 05:33 108-20-3 ND ug/L 1.0 0.30 1 09/29/11 05:33 100-41-4 ND ug/L 1.0 0.71 1 09/29/11 05:33 87-68-3 ND ug/L 5.0 0.46 1 09/29/11 05:33 591-78-6 ND ug/L 1.0 0.31 1 09/29/11 05:33 99-87-6 ND ug/L 2.0 0.97 1 09/29/11 05:33 75-09-2 ND ug/L 5.0 0.33 1 09/29/11 05:33 108-10-1 ND ug/L 1.0 0.21 1 09/29/11 05:33 1634-04-4 ND ug/L 1.0 0.24 1 09/29/11 05:33 91-20-3 ND ug/L 1.0 0.26 1 09/29/11 05:33 100-42-5 ND ug/L 1.0 0.33 1 09/29/11 05:33 630-20-6 ND ug/L 1.0 0.40 1 09/29/11 05:33 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 37 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-23 Labll): 92103091017 Collected: 09/23/11 15:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 143 ug/L 1.0 0.46 1 09/29/11 05:33 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/29/11 05:33 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/29/11 05:33 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/29/11 05:33 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/29/11 05:33 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/29/11 05:33 79-00-5 Trichloroethene 6.8 ug/L 1.0 0.47 1 09/29/11 05:33 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/29/11 05:33 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/29/11 05:33 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/29/11 05:33 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/29/11 05:33 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/29/11 05:33 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/29/11 05:33 95-47-6 4-Bromofluorobenzene (S) 88 % 70-130 1 09/29/11 05:33 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 09/29/11 05:33 1868-53-7 1,2-Dichloroethane-d4 (S) 116 % 70-130 1 09/29/11 05:33 17060-07-0 Tbluene-d8 (S) 91 % 70-130 1 09/29/11 05:33 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 38 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-24 Labll): 92103091018 Collected: 09/22/11 15:45 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 62.5 5.4 2.5 09/29/11 09:44 67-64-1 ND ug/L 2.5 0.62 2.5 09/29/11 09:44 71-43-2 ND ug/L 2.5 0.75 2.5 09/29/11 09:44 108-86-1 ND ug/L 2.5 0.42 2.5 09/29/11 09:44 74-97-5 ND ug/L 2.5 0.45 2.5 09/29/11 09:44 75-27-4 ND ug/L 2.5 0.65 2.5 09/29/11 09:44 75-25-2 ND ug/L 5.0 0.72 2.5 09/29/11 09:44 74-83-9 ND ug/L 12.5 2.4 2.5 09/29/11 09:44 78-93-3 ND ug/L 2.5 0.62 2.5 09/29/11 09:44 56-23-5 ND ug/L 2.5 0.58 2.5 09/29/11 09:44 108-90-7 ND ug/L 2.5 1.4 2.5 09/29/11 09:44 75-00-3 ND ug/L 2.5 0.35 2.5 09/29/11 09:44 67-66-3 ND ug/L 2.5 0.28 2.5 09/29/11 09:44 74-87-3 ND ug/L 2.5 0.88 2.5 09/29/11 09:44 95-49-8 ND ug/L 2.5 0.78 2.5 09/29/11 09:44 106-43-4 ND ug/L 12.5 6.3 2.5 09/29/11 09:44 96-12-8 ND ug/L 2.5 0.52 2.5 09/29/11 09:44 124-48-1 ND ug/L 2.5 0.68 2.5 09/29/11 09:44 106-93-4 ND ug/L 2.5 0.52 2.5 09/29/11 09:44 74-95-3 ND ug/L 2.5 0.75 2.5 09/29/11 09:44 95-50-1 ND ug/L 2.5 0.60 2.5 09/29/11 09:44 541-73-1 ND ug/L 2.5 0.82 2.5 09/29/11 09:44 106-46-7 ND ug/L 2.5 0.52 2.5 09/29/11 09:44 75-71-8 ND ug/L 2.5 0.80 2.5 09/29/11 09:44 75-34-3 ND ug/L 2.5 0.30 2.5 09/29/11 09:44 107-06-2 ND ug/L 2.5 1.4 2.5 09/29/11 09:44 75-35-4 1AJ ug/L 2.5 0.48 2.5 09/29/11 09:44 156-59-2 ND ug/L 2.5 1.2 2.5 09/29/11 09:44 156-60-5 ND ug/L 2.5 0.68 2.5 09/29/11 09:44 78-87-5 ND ug/L 2.5 0.70 2.5 09/29/11 09:44 142-28-9 ND ug/L 2.5 0.32 2.5 09/29/11 09:44 594-20-7 ND ug/L 2.5 1.2 2.5 09/29/11 09:44 563-58-6 ND ug/L 2.5 0.32 2.5 09/29/11 09:44 10061-01-5 ND ug/L 2.5 0.65 2.5 09/29/11 09:44 10061-02-6 ND ug/L 2.5 0.30 2.5 09/29/11 09:44 108-20-3 ND ug/L 2.5 0.75 2.5 09/29/11 09:44 100-41-4 ND ug/L 2.5 1.8 2.5 09/29/11 09:44 87-68-3 ND ug/L 12.5 1.2 2.5 09/29/11 09:44 591-78-6 ND ug/L 2.5 0.78 2.5 09/29/11 09:44 99-87-6 ND ug/L 5.0 2.4 2.5 09/29/11 09:44 75-09-2 ND ug/L 12.5 0.82 2.5 09/29/11 09:44 108-10-1 ND ug/L 2.5 0.52 2.5 09/29/11 09:44 1634-04-4 ND ug/L 2.5 0.60 2.5 09/29/11 09:44 91-20-3 ND ug/L 2.5 0.65 2.5 09/29/11 09:44 100-42-5 ND ug/L 2.5 0.82 2.5 09/29/11 09:44 630-20-6 ND ug/L 2.5 1.0 2.5 09/29/11 09:44 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 39 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-24 Labll): 92103091018 Collected: 09/22/11 15:45 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 243 ug/L 2.5 1.2 2.5 09/29/11 09:44 127-18-4 Toluene ND ug/L 2.5 0.65 2.5 09/29/11 09:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.5 0.82 2.5 09/29/11 09:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.5 0.88 2.5 09/29/11 09:44 120-82-1 1,1,1-Trichloroethane ND ug/L 2.5 1.2 2.5 09/29/11 09:44 71-55-6 1,1,2-Trichloroethane ND ug/L 2.5 0.72 2.5 09/29/11 09:44 79-00-5 Trichloroethene 6.2 ug/L 2.5 1.2 2.5 09/29/11 09:44 79-01-6 Trichlorofluoromethane ND ug/L 2.5 0.50 2.5 09/29/11 09:44 75-69-4 1,2,3-Trichloropropane ND ug/L 2.5 1.0 2.5 09/29/11 09:44 96-18-4 Vinyl acetate ND ug/L 5.0 0.88 2.5 09/29/11 09:44 108-05-4 Vinyl chloride ND ug/L 2.5 1.6 2.5 09/29/11 09:44 75-01-4 m&p-Xylene ND ug/L 5.0 1.6 2.5 09/29/11 09:44 179601-23-1 o-Xylene ND ug/L 2.5 0.58 2.5 09/29/11 09:44 95-47-6 4-Bromofluorobenzene (S) 90 % 70-130 2.5 09/29/11 09:44 460-00-4 Dibromofluoromethane (S) 106 % 70-130 2.5 09/29/11 09:44 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 2.5 09/29/11 09:44 17060-07-0 Tbluene-d8 (S) 92 % 70-130 2.5 09/29/11 09:44 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 40 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-26 Labll): 92103091019 Collected: 09/21/11 13:36 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/29/11 05:55 67-64-1 ND ug/L 1.0 0.25 1 09/29/11 05:55 71-43-2 ND ug/L 1.0 0.30 1 09/29/11 05:55 108-86-1 ND ug/L 1.0 0.17 1 09/29/11 05:55 74-97-5 ND ug/L 1.0 0.18 1 09/29/11 05:55 75-27-4 ND ug/L 1.0 0.26 1 09/29/11 05:55 75-25-2 ND ug/L 2.0 0.29 1 09/29/11 05:55 74-83-9 ND ug/L 5.0 0.96 1 09/29/11 05:55 78-93-3 ND ug/L 1.0 0.25 1 09/29/11 05:55 56-23-5 ND ug/L 1.0 0.23 1 09/29/11 05:55 108-90-7 ND ug/L 1.0 0.54 1 09/29/11 05:55 75-00-3 3.2 ug/L 1.0 0.14 1 09/29/11 05:55 67-66-3 0.23J ug/L 1.0 0.11 1 09/29/11 05:55 74-87-3 ND ug/L 1.0 0.35 1 09/29/11 05:55 95-49-8 ND ug/L 1.0 0.31 1 09/29/11 05:55 106-43-4 ND ug/L 5.0 2.5 1 09/29/11 05:55 96-12-8 ND ug/L 1.0 0.21 1 09/29/11 05:55 124-48-1 ND ug/L 1.0 0.27 1 09/29/11 05:55 106-93-4 ND ug/L 1.0 0.21 1 09/29/11 05:55 74-95-3 ND ug/L 1.0 0.30 1 09/29/11 05:55 95-50-1 ND ug/L 1.0 0.24 1 09/29/11 05:55 541-73-1 ND ug/L 1.0 0.33 1 09/29/11 05:55 106-46-7 ND ug/L 1.0 0.21 1 09/29/11 05:55 75-71-8 ND ug/L 1.0 0.32 1 09/29/11 05:55 75-34-3 ND ug/L 1.0 0.12 1 09/29/11 05:55 107-06-2 ND ug/L 1.0 0.56 1 09/29/11 05:55 75-35-4 ND ug/L 1.0 0.19 1 09/29/11 05:55 156-59-2 ND ug/L 1.0 0.49 1 09/29/11 05:55 156-60-5 ND ug/L 1.0 0.27 1 09/29/11 05:55 78-87-5 ND ug/L 1.0 0.28 1 09/29/11 05:55 142-28-9 ND ug/L 1.0 0.13 1 09/29/11 05:55 594-20-7 ND ug/L 1.0 0.49 1 09/29/11 05:55 563-58-6 ND ug/L 1.0 0.13 1 09/29/11 05:55 10061-01-5 ND ug/L 1.0 0.26 1 09/29/11 05:55 10061-02-6 ND ug/L 1.0 0.12 1 09/29/11 05:55 108-20-3 ND ug/L 1.0 0.30 1 09/29/11 05:55 100-41-4 ND ug/L 1.0 0.71 1 09/29/11 05:55 87-68-3 ND ug/L 5.0 0.46 1 09/29/11 05:55 591-78-6 ND ug/L 1.0 0.31 1 09/29/11 05:55 99-87-6 ND ug/L 2.0 0.97 1 09/29/11 05:55 75-09-2 ND ug/L 5.0 0.33 1 09/29/11 05:55 108-10-1 ND ug/L 1.0 0.21 1 09/29/11 05:55 1634-04-4 ND ug/L 1.0 0.24 1 09/29/11 05:55 91-20-3 ND ug/L 1.0 0.26 1 09/29/11 05:55 100-42-5 ND ug/L 1.0 0.33 1 09/29/11 05:55 630-20-6 ND ug/L 1.0 0.40 1 09/29/11 05:55 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 41 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-26 Labll): 92103091019 Collected: 09/21/11 13:36 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/29/11 05:55 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/29/11 05:55 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/29/11 05:55 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/29/11 05:55 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/29/11 05:55 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/29/11 05:55 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/29/11 05:55 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/29/11 05:55 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/29/11 05:55 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/29/11 05:55 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/29/11 05:55 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/29/11 05:55 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/29/11 05:55 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 1 09/29/11 05:55 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 09/29/11 05:55 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 1 09/29/11 05:55 17060-07-0 Tbluene-d8 (S) 92 % 70-130 1 09/29/11 05:55 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 42 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-1 Labll): 92103091020 Collected: 09/23/11 18:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 2500 217 100 10/01/11 16:55 67-64-1 ND ug/L 100 25.0 100 10/01/11 16:55 71-43-2 ND ug/L 100 30.0 100 10/01/11 16:55 108-86-1 ND ug/L 100 17.0 100 10/01/11 16:55 74-97-5 ND ug/L 100 18.0 100 10/01/11 16:55 75-27-4 ND ug/L 100 26.0 100 10/01/11 16:55 75-25-2 ND ug/L 200 29.0 100 10/01/11 16:55 74-83-9 ND ug/L 500 96.0 100 10/01/11 16:55 78-93-3 ND ug/L 100 25.0 100 10/01/11 16:55 56-23-5 ND ug/L 100 23.0 100 10/01/11 16:55 108-90-7 ND ug/L 100 54.0 100 10/01/11 16:55 75-00-3 ND ug/L 100 14.0 100 10/01/11 16:55 67-66-3 ND ug/L 100 11.0 100 10/01/11 16:55 74-87-3 ND ug/L 100 35.0 100 10/01/11 16:55 95-49-8 ND ug/L 100 31.0 100 10/01/11 16:55 106-43-4 ND ug/L 500 252 100 10/01/11 16:55 96-12-8 ND ug/L 100 21.0 100 10/01/11 16:55 124-48-1 ND ug/L 100 27.0 100 10/01/11 16:55 106-93-4 ND ug/L 100 21.0 100 10/01/11 16:55 74-95-3 ND ug/L 100 30.0 100 10/01/11 16:55 95-50-1 ND ug/L 100 24.0 100 10/01/11 16:55 541-73-1 ND ug/L 100 33.0 100 10/01/11 16:55 106-46-7 ND ug/L 100 21.0 100 10/01/11 16:55 75-71-8 ND ug/L 100 32.0 100 10/01/11 16:55 75-34-3 ND ug/L 100 12.0 100 10/01/11 16:55 107-06-2 ND ug/L 100 56.0 100 10/01/11 16:55 75-35-4 7610 ug/L 100 19.0 100 10/01/11 16:55 156-59-2 53.OJ ug/L 100 49.0 100 10/01/11 16:55 156-60-5 ND ug/L 100 27.0 100 10/01/11 16:55 78-87-5 ND ug/L 100 28.0 100 10/01/11 16:55 142-28-9 ND ug/L 100 13.0 100 10/01/11 16:55 594-20-7 ND ug/L 100 49.0 100 10/01/11 16:55 563-58-6 ND ug/L 100 13.0 100 10/01/11 16:55 10061-01-5 ND ug/L 100 26.0 100 10/01/11 16:55 10061-02-6 ND ug/L 100 12.0 100 10/01/11 16:55 108-20-3 ND ug/L 100 30.0 100 10/01/11 16:55 100-41-4 ND ug/L 100 71.0 100 10/01/11 16:55 87-68-3 ND ug/L 500 46.0 100 10/01/11 16:55 591-78-6 ND ug/L 100 31.0 100 10/01/11 16:55 99-87-6 ND ug/L 200 97.0 100 10/01/11 16:55 75-09-2 ND ug/L 500 33.0 100 10/01/11 16:55 108-10-1 ND ug/L 100 21.0 100 10/01/11 16:55 1634-04-4 ND ug/L 100 24.0 100 10/01/11 16:55 91-20-3 ND ug/L 100 26.0 100 10/01/11 16:55 100-42-5 ND ug/L 100 33.0 100 10/01/11 16:55 630-20-6 ND ug/L 100 40.0 100 10/01/11 16:55 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 43 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-1 Labll): 92103091020 Collected: 09/23/11 18:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2010 ug/L 100 46.0 100 10/01/11 16:55 127-18-4 Toluene ND ug/L 100 26.0 100 10/01/11 16:55 108-88-3 1,2,3-Trichlorobenzene ND ug/L 100 33.0 100 10/01/11 16:55 87-61-6 1,2,4-Trichlorobenzene ND ug/L 100 35.0 100 10/01/11 16:55 120-82-1 1,1,1-Trichloroethane ND ug/L 100 48.0 100 10/01/11 16:55 71-55-6 1,1,2-Trichloroethane ND ug/L 100 29.0 100 10/01/11 16:55 79-00-5 Trichloroethene 2610 ug/L 100 47.0 100 10/01/11 16:55 79-01-6 Trichlorofluoromethane ND ug/L 100 20.0 100 10/01/11 16:55 75-69-4 1,2,3-Trichloropropane ND ug/L 100 41.0 100 10/01/11 16:55 96-18-4 Vinyl acetate ND ug/L 200 35.0 100 10/01/11 16:55 108-05-4 Vinyl chloride ND ug/L 100 62.0 100 10/01/11 16:55 75-01-4 m&p-Xylene ND ug/L 200 66.0 100 10/01/11 16:55 179601-23-1 o-Xylene ND ug/L 100 23.0 100 10/01/11 16:55 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 100 10/01/11 16:55 460-00-4 Dibromofluoromethane (S) 105 % 70-130 100 10/01/11 16:55 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 100 10/01/11 16:55 17060-07-0 Tbluene-d8 (S) 104 % 70-130 100 10/01/11 16:55 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 44 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-3 Labll): 92103091021 Collected: 09/23/11 19:35 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 250 21.7 10 09/29/11 10:07 67-64-1 ND ug/L 10.0 2.5 10 09/29/11 10:07 71-43-2 ND ug/L 10.0 3.0 10 09/29/11 10:07 108-86-1 ND ug/L 10.0 1.7 10 09/29/11 10:07 74-97-5 ND ug/L 10.0 1.8 10 09/29/11 10:07 75-27-4 ND ug/L 10.0 2.6 10 09/29/11 10:07 75-25-2 ND ug/L 20.0 2.9 10 09/29/11 10:07 74-83-9 ND ug/L 50.0 9.6 10 09/29/11 10:07 78-93-3 ND ug/L 10.0 2.5 10 09/29/11 10:07 56-23-5 ND ug/L 10.0 2.3 10 09/29/11 10:07 108-90-7 ND ug/L 10.0 5.4 10 09/29/11 10:07 75-00-3 ND ug/L 10.0 1.4 10 09/29/11 10:07 67-66-3 ND ug/L 10.0 1.1 10 09/29/11 10:07 74-87-3 ND ug/L 10.0 3.5 10 09/29/11 10:07 95-49-8 ND ug/L 10.0 3.1 10 09/29/11 10:07 106-43-4 ND ug/L 50.0 25.2 10 09/29/11 10:07 96-12-8 ND ug/L 10.0 2.1 10 09/29/11 10:07 124-48-1 ND ug/L 10.0 2.7 10 09/29/11 10:07 106-93-4 ND ug/L 10.0 2.1 10 09/29/11 10:07 74-95-3 ND ug/L 10.0 3.0 10 09/29/11 10:07 95-50-1 ND ug/L 10.0 2.4 10 09/29/11 10:07 541-73-1 ND ug/L 10.0 3.3 10 09/29/11 10:07 106-46-7 ND ug/L 10.0 2.1 10 09/29/11 10:07 75-71-8 ND ug/L 10.0 3.2 10 09/29/11 10:07 75-34-3 ND ug/L 10.0 1.2 10 09/29/11 10:07 107-06-2 14.7 ug/L 10.0 5.6 10 09/29/11 10:07 75-35-4 9290 ug/L 100 19.0 100 09/29/11 17:55 156-59-2 ND ug/L 10.0 4.9 10 09/29/11 10:07 156-60-5 ND ug/L 10.0 2.7 10 09/29/11 10:07 78-87-5 ND ug/L 10.0 2.8 10 09/29/11 10:07 142-28-9 ND ug/L 10.0 1.3 10 09/29/11 10:07 594-20-7 ND ug/L 10.0 4.9 10 09/29/11 10:07 563-58-6 ND ug/L 10.0 1.3 10 09/29/11 10:07 10061-01-5 ND ug/L 10.0 2.6 10 09/29/11 10:07 10061-02-6 ND ug/L 10.0 1.2 10 09/29/11 10:07 108-20-3 ND ug/L 10.0 3.0 10 09/29/11 10:07 100-41-4 ND ug/L 10.0 7.1 10 09/29/11 10:07 87-68-3 ND ug/L 50.0 4.6 10 09/29/11 10:07 591-78-6 ND ug/L 10.0 3.1 10 09/29/11 10:07 99-87-6 ND ug/L 20.0 9.7 10 09/29/11 10:07 75-09-2 ND ug/L 50.0 3.3 10 09/29/11 10:07 108-10-1 ND ug/L 10.0 2.1 10 09/29/11 10:07 1634-04-4 ND ug/L 10.0 2.4 10 09/29/11 10:07 91-20-3 ND ug/L 10.0 2.6 10 09/29/11 10:07 100-42-5 ND ug/L 10.0 3.3 10 09/29/11 10:07 630-20-6 ND ug/L 10.0 4.0 10 09/29/11 10:07 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 45 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-3 Labll): 92103091021 Collected: 09/23/11 19:35 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 132 ug/L 10.0 4.6 10 09/29/11 10:07 127-18-4 Toluene ND ug/L 10.0 2.6 10 09/29/11 10:07 108-88-3 1,2,3-Trichlorobenzene ND ug/L 10.0 3.3 10 09/29/11 10:07 87-61-6 1,2,4-Trichlorobenzene ND ug/L 10.0 3.5 10 09/29/11 10:07 120-82-1 1,1,1-Trichloroethane ND ug/L 10.0 4.8 10 09/29/11 10:07 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 2.9 10 09/29/11 10:07 79-00-5 Trichloroethene 71.3 ug/L 10.0 4.7 10 09/29/11 10:07 79-01-6 Trichlorofluoromethane ND ug/L 10.0 2.0 10 09/29/11 10:07 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.1 10 09/29/11 10:07 96-18-4 Vinyl acetate ND ug/L 20.0 3.5 10 09/29/11 10:07 108-05-4 Vinyl chloride 40.0 ug/L 10.0 6.2 10 09/29/11 10:07 75-01-4 m&p-Xylene ND ug/L 20.0 6.6 10 09/29/11 10:07 179601-23-1 o-Xylene ND ug/L 10.0 2.3 10 09/29/11 10:07 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 10 09/29/11 10:07 460-00-4 Dibromofluoromethane (S) 106 % 70-130 10 09/29/11 10:07 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 10 09/29/11 10:07 17060-07-0 Tbluene-d8 (S) 99 % 70-130 10 09/29/11 10:07 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 46 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-5 Labll): 92103091022 Collected: 09/23/11 17:20 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 20.4J ug/L 50.0 4.3 2 09/29/11 10:30 67-64-1 ND ug/L 2.0 0.50 2 09/29/11 10:30 71-43-2 ND ug/L 2.0 0.60 2 09/29/11 10:30 108-86-1 ND ug/L 2.0 0.34 2 09/29/11 10:30 74-97-5 ND ug/L 2.0 0.36 2 09/29/11 10:30 75-27-4 ND ug/L 2.0 0.52 2 09/29/11 10:30 75-25-2 ND ug/L 4.0 0.58 2 09/29/11 10:30 74-83-9 20.7 ug/L 10.0 1.9 2 09/29/11 10:30 78-93-3 ND ug/L 2.0 0.50 2 09/29/11 10:30 56-23-5 ND ug/L 2.0 0.46 2 09/29/11 10:30 108-90-7 ND ug/L 2.0 1.1 2 09/29/11 10:30 75-00-3 ND ug/L 2.0 0.28 2 09/29/11 10:30 67-66-3 ND ug/L 2.0 0.22 2 09/29/11 10:30 74-87-3 ND ug/L 2.0 0.70 2 09/29/11 10:30 95-49-8 ND ug/L 2.0 0.62 2 09/29/11 10:30 106-43-4 ND ug/L 10.0 5.0 2 09/29/11 10:30 96-12-8 ND ug/L 2.0 0.42 2 09/29/11 10:30 124-48-1 ND ug/L 2.0 0.54 2 09/29/11 10:30 106-93-4 ND ug/L 2.0 0.42 2 09/29/11 10:30 74-95-3 ND ug/L 2.0 0.60 2 09/29/11 10:30 95-50-1 ND ug/L 2.0 0.48 2 09/29/11 10:30 541-73-1 ND ug/L 2.0 0.66 2 09/29/11 10:30 106-46-7 ND ug/L 2.0 0.42 2 09/29/11 10:30 75-71-8 ND ug/L 2.0 0.64 2 09/29/11 10:30 75-34-3 ND ug/L 2.0 0.24 2 09/29/11 10:30 107-06-2 1.5J ug/L 2.0 1.1 2 09/29/11 10:30 75-35-4 1760 ug/L 20.0 3.8 20 09/29/11 18:18 156-59-2 14.7 ug/L 2.0 0.98 2 09/29/11 10:30 156-60-5 ND ug/L 2.0 0.54 2 09/29/11 10:30 78-87-5 ND ug/L 2.0 0.56 2 09/29/11 10:30 142-28-9 ND ug/L 2.0 0.26 2 09/29/11 10:30 594-20-7 ND ug/L 2.0 0.98 2 09/29/11 10:30 563-58-6 ND ug/L 2.0 0.26 2 09/29/11 10:30 10061-01-5 ND ug/L 2.0 0.52 2 09/29/11 10:30 10061-02-6 ND ug/L 2.0 0.24 2 09/29/11 10:30 108-20-3 ND ug/L 2.0 0.60 2 09/29/11 10:30 100-41-4 ND ug/L 2.0 1.4 2 09/29/11 10:30 87-68-3 ND ug/L 10.0 0.92 2 09/29/11 10:30 591-78-6 ND ug/L 2.0 0.62 2 09/29/11 10:30 99-87-6 ND ug/L 4.0 1.9 2 09/29/11 10:30 75-09-2 ND ug/L 10.0 0.66 2 09/29/11 10:30 108-10-1 ND ug/L 2.0 0.42 2 09/29/11 10:30 1634-04-4 ND ug/L 2.0 0.48 2 09/29/11 10:30 91-20-3 ND ug/L 2.0 0.52 2 09/29/11 10:30 100-42-5 ND ug/L 2.0 0.66 2 09/29/11 10:30 630-20-6 ND ug/L 2.0 0.80 2 09/29/11 10:30 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 47 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-5 Labll): 92103091022 Collected: 09/23/11 17:20 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 73.9 ug/L 2.0 0.92 2 09/29/11 10:30 127-18-4 Toluene ND ug/L 2.0 0.52 2 09/29/11 10:30 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.66 2 09/29/11 10:30 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.70 2 09/29/11 10:30 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.96 2 09/29/11 10:30 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.58 2 09/29/11 10:30 79-00-5 Trichloroethene 69.7 ug/L 2.0 0.94 2 09/29/11 10:30 79-01-6 Trichlorofluoromethane ND ug/L 2.0 0.40 2 09/29/11 10:30 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.82 2 09/29/11 10:30 96-18-4 Vinyl acetate ND ug/L 4.0 0.70 2 09/29/11 10:30 108-05-4 Vinyl chloride 14.0 ug/L 2.0 1.2 2 09/29/11 10:30 75-01-4 m&p-Xylene ND ug/L 4.0 1.3 2 09/29/11 10:30 179601-23-1 o-Xylene ND ug/L 2.0 0.46 2 09/29/11 10:30 95-47-6 4-Bromofluorobenzene (S) 86 % 70-130 2 09/29/11 10:30 460-00-4 Dibromofluoromethane (S) 104 % 70-130 2 09/29/11 10:30 1868-53-7 1,2-Dichloroethane-d4 (S) 109 % 70-130 2 09/29/11 10:30 17060-07-0 Tbluene-d8 (S) ill % 70-130 2 09/29/11 10:30 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 48 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 Labll): 92103091023 Collected: 09/23/11 16:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 250 21.7 10 10/01/11 17:20 67-64-1 ND ug/L 10.0 2.5 10 10/01/11 17:20 71-43-2 ND ug/L 10.0 3.0 10 10/01/11 17:20 108-86-1 ND ug/L 10.0 1.7 10 10/01/11 17:20 74-97-5 ND ug/L 10.0 1.8 10 10/01/11 17:20 75-27-4 ND ug/L 10.0 2.6 10 10/01/11 17:20 75-25-2 ND ug/L 20.0 2.9 10 10/01/11 17:20 74-83-9 ND ug/L 50.0 9.6 10 10/01/11 17:20 78-93-3 ND ug/L 10.0 2.5 10 10/01/11 17:20 56-23-5 ND ug/L 10.0 2.3 10 10/01/11 17:20 108-90-7 ND ug/L 10.0 5.4 10 10/01/11 17:20 75-00-3 ND ug/L 10.0 1.4 10 10/01/11 17:20 67-66-3 ND ug/L 10.0 1.1 10 10/01/11 17:20 74-87-3 ND ug/L 10.0 3.5 10 10/01/11 17:20 95-49-8 ND ug/L 10.0 3.1 10 10/01/11 17:20 106-43-4 ND ug/L 50.0 25.2 10 10/01/11 17:20 96-12-8 ND ug/L 10.0 2.1 10 10/01/11 17:20 124-48-1 ND ug/L 10.0 2.7 10 10/01/11 17:20 106-93-4 ND ug/L 10.0 2.1 10 10/01/11 17:20 74-95-3 ND ug/L 10.0 3.0 10 10/01/11 17:20 95-50-1 ND ug/L 10.0 2.4 10 10/01/11 17:20 541-73-1 ND ug/L 10.0 3.3 10 10/01/11 17:20 106-46-7 ND ug/L 10.0 2.1 10 10/01/11 17:20 75-71-8 ND ug/L 10.0 3.2 10 10/01/11 17:20 75-34-3 ND ug/L 10.0 1.2 10 10/01/11 17:20 107-06-2 ND ug/L 10.0 5.6 10 10/01/11 17:20 75-35-4 750 ug/L 10.0 1.9 10 10/01/11 17:20 156-59-2 4.9J ug/L 10.0 4.9 10 10/01/11 17:20 156-60-5 ND ug/L 10.0 2.7 10 10/01/11 17:20 78-87-5 ND ug/L 10.0 2.8 10 10/01/11 17:20 142-28-9 ND ug/L 10.0 1.3 10 10/01/11 17:20 594-20-7 ND ug/L 10.0 4.9 10 10/01/11 17:20 563-58-6 ND ug/L 10.0 1.3 10 10/01/11 17:20 10061-01-5 ND ug/L 10.0 2.6 10 10/01/11 17:20 10061-02-6 ND ug/L 10.0 1.2 10 10/01/11 17:20 108-20-3 ND ug/L 10.0 3.0 10 10/01/11 17:20 100-41-4 ND ug/L 10.0 7.1 10 10/01/11 17:20 87-68-3 ND ug/L 50.0 4.6 10 10/01/11 17:20 591-78-6 ND ug/L 10.0 3.1 10 10/01/11 17:20 99-87-6 ND ug/L 20.0 9.7 10 10/01/11 17:20 75-09-2 ND ug/L 50.0 3.3 10 10/01/11 17:20 108-10-1 ND ug/L 10.0 2.1 10 10/01/11 17:20 1634-04-4 ND ug/L 10.0 2.4 10 10/01/11 17:20 91-20-3 ND ug/L 10.0 2.6 10 10/01/11 17:20 100-42-5 ND ug/L 10.0 3.3 10 10/01/11 17:20 630-20-6 ND ug/L 10.0 4.0 10 10/01/11 17:20 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 49 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 Labll): 92103091023 Collected: 09/23/11 16:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1120 ug/L 10.0 4.6 10 10/01/11 17:20 127-18-4 Toluene ND ug/L 10.0 2.6 10 10/01/11 17:20 108-88-3 1,2,3-Trichlorobenzene ND ug/L 10.0 3.3 10 10/01/11 17:20 87-61-6 1,2,4-Trichlorobenzene ND ug/L 10.0 3.5 10 10/01/11 17:20 120-82-1 1,1,1-Trichloroethane ND ug/L 10.0 4.8 10 10/01/11 17:20 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 2.9 10 10/01/11 17:20 79-00-5 Trichloroethene 262 ug/L 10.0 4.7 10 10/01/11 17:20 79-01-6 Trichlorofluoromethane ND ug/L 10.0 2.0 10 10/01/11 17:20 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.1 10 10/01/11 17:20 96-18-4 Vinyl acetate ND ug/L 20.0 3.5 10 10/01/11 17:20 108-05-4 Vinyl chloride ND ug/L 10.0 6.2 10 10/01/11 17:20 75-01-4 m&p-Xylene ND ug/L 20.0 6.6 10 10/01/11 17:20 179601-23-1 o-Xylene ND ug/L 10.0 2.3 10 10/01/11 17:20 95-47-6 4-Bromofluorobenzene (S) 97 % 70-130 10 10/01/11 17:20 460-00-4 Dibromofluoromethane (S) 108 % 70-130 10 10/01/11 17:20 1868-53-7 1,2-Dichloroethane-d4 (S) 112 % 70-130 10 10/01/11 17:20 17060-07-0 Tbluene-d8 (S) 102 % 70-130 10 10/01/11 17:20 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 50 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Labll): 92103091024 Collected: 09/23/11 15:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 500 43.4 20 09/29/11 11:16 67-64-1 ND ug/L 20.0 5.0 20 09/29/11 11:16 71-43-2 ND ug/L 20.0 6.0 20 09/29/11 11:16 108-86-1 ND ug/L 20.0 3.4 20 09/29/11 11:16 74-97-5 ND ug/L 20.0 3.6 20 09/29/11 11:16 75-27-4 ND ug/L 20.0 5.2 20 09/29/11 11:16 75-25-2 ND ug/L 40.0 5.8 20 09/29/11 11:16 74-83-9 ND ug/L 100 19.2 20 09/29/11 11:16 78-93-3 ND ug/L 20.0 5.0 20 09/29/11 11:16 56-23-5 ND ug/L 20.0 4.6 20 09/29/11 11:16 108-90-7 ND ug/L 20.0 10.8 20 09/29/11 11:16 75-00-3 11.1J ug/L 20.0 2.8 20 09/29/11 11:16 67-66-3 ND ug/L 20.0 2.2 20 09/29/11 11:16 74-87-3 ND ug/L 20.0 7.0 20 09/29/11 11:16 95-49-8 ND ug/L 20.0 6.2 20 09/29/11 11:16 106-43-4 ND ug/L 100 50.4 20 09/29/11 11:16 96-12-8 ND ug/L 20.0 4.2 20 09/29/11 11:16 124-48-1 ND ug/L 20.0 5.4 20 09/29/11 11:16 106-93-4 ND ug/L 20.0 4.2 20 09/29/11 11:16 74-95-3 ND ug/L 20.0 6.0 20 09/29/11 11:16 95-50-1 ND ug/L 20.0 4.8 20 09/29/11 11:16 541-73-1 ND ug/L 20.0 6.6 20 09/29/11 11:16 106-46-7 ND ug/L 20.0 4.2 20 09/29/11 11:16 75-71-8 ND ug/L 20.0 6.4 20 09/29/11 11:16 75-34-3 ND ug/L 20.0 2.4 20 09/29/11 11:16 107-06-2 ND ug/L 20.0 11.2 20 09/29/11 11:16 75-35-4 71.1 ug/L 20.0 3.8 20 09/29/11 11:16 156-59-2 ND ug/L 20.0 9.8 20 09/29/11 11:16 156-60-5 ND ug/L 20.0 5.4 20 09/29/11 11:16 78-87-5 ND ug/L 20.0 5.6 20 09/29/11 11:16 142-28-9 ND ug/L 20.0 2.6 20 09/29/11 11:16 594-20-7 ND ug/L 20.0 9.8 20 09/29/11 11:16 563-58-6 ND ug/L 20.0 2.6 20 09/29/11 11:16 10061-01-5 ND ug/L 20.0 5.2 20 09/29/11 11:16 10061-02-6 ND ug/L 20.0 2.4 20 09/29/11 11:16 108-20-3 ND ug/L 20.0 6.0 20 09/29/11 11:16 100-41-4 ND ug/L 20.0 14.2 20 09/29/11 11:16 87-68-3 ND ug/L 100 9.2 20 09/29/11 11:16 591-78-6 ND ug/L 20.0 6.2 20 09/29/11 11:16 99-87-6 ND ug/L 40.0 19.4 20 09/29/11 11:16 75-09-2 ND ug/L 100 6.6 20 09/29/11 11:16 108-10-1 ND ug/L 20.0 4.2 20 09/29/11 11:16 1634-04-4 ND ug/L 20.0 4.8 20 09/29/11 11:16 91-20-3 ND ug/L 20.0 5.2 20 09/29/11 11:16 100-42-5 ND ug/L 20.0 6.6 20 09/29/11 11:16 630-20-6 ND ug/L 20.0 8.0 20 09/29/11 11:16 79-34-5 D3 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 51 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Labll): 92103091024 Collected: 09/23/11 15:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 107 ug/L 20.0 9.2 20 09/29/11 11:16 127-18-4 Toluene ND ug/L 20.0 5.2 20 09/29/11 11:16 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 6.6 20 09/29/11 11:16 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 7.0 20 09/29/11 11:16 120-82-1 1,1,1-Trichloroethane ND ug/L 20.0 9.6 20 09/29/11 11:16 71-55-6 1,1,2-Trichloroethane ND ug/L 20.0 5.8 20 09/29/11 11:16 79-00-5 Trichloroethene 10.3J ug/L 20.0 9.4 20 09/29/11 11:16 79-01-6 Trichlorofluoromethane ND ug/L 20.0 4.0 20 09/29/11 11:16 75-69-4 1,2,3-Trichloropropane ND ug/L 20.0 8.2 20 09/29/11 11:16 96-18-4 Vinyl acetate ND ug/L 40.0 7.0 20 09/29/11 11:16 108-05-4 Vinyl chloride ND ug/L 20.0 12.4 20 09/29/11 11:16 75-01-4 m&p-Xylene ND ug/L 40.0 13.2 20 09/29/11 11:16 179601-23-1 o-Xylene ND ug/L 20.0 4.6 20 09/29/11 11:16 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 20 09/29/11 11:16 460-00-4 Dibromofluoromethane (S) 105 % 70-130 20 09/29/11 11:16 1868-53-7 1,2-Dichloroethane-d4 (S) 110 % 70-130 20 09/29/11 11:16 17060-07-0 Tbluene-d8 (S) 97 % 70-130 20 09/29/11 11:16 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 52 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RINSATEA Labll): 92103091025 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/29/11 06:18 67-64-1 ND ug/L 1.0 0.25 1 09/29/11 06:18 71-43-2 ND ug/L 1.0 0.30 1 09/29/11 06:18 108-86-1 ND ug/L 1.0 0.17 1 09/29/11 06:18 74-97-5 ND ug/L 1.0 0.18 1 09/29/11 06:18 75-27-4 ND ug/L 1.0 0.26 1 09/29/11 06:18 75-25-2 ND ug/L 2.0 0.29 1 09/29/11 06:18 74-83-9 ND ug/L 5.0 0.96 1 09/29/11 06:18 78-93-3 ND ug/L 1.0 0.25 1 09/29/11 06:18 56-23-5 ND ug/L 1.0 0.23 1 09/29/11 06:18 108-90-7 ND ug/L 1.0 0.54 1 09/29/11 06:18 75-00-3 0.54J ug/L 1.0 0.14 1 09/29/11 06:18 67-66-3 0.55J ug/L 1.0 0.11 1 09/29/11 06:18 74-87-3 ND ug/L 1.0 0.35 1 09/29/11 06:18 95-49-8 ND ug/L 1.0 0.31 1 09/29/11 06:18 106-43-4 ND ug/L 5.0 2.5 1 09/29/11 06:18 96-12-8 ND ug/L 1.0 0.21 1 09/29/11 06:18 124-48-1 ND ug/L 1.0 0.27 1 09/29/11 06:18 106-93-4 ND ug/L 1.0 0.21 1 09/29/11 06:18 74-95-3 ND ug/L 1.0 0.30 1 09/29/11 06:18 95-50-1 ND ug/L 1.0 0.24 1 09/29/11 06:18 541-73-1 ND ug/L 1.0 0.33 1 09/29/11 06:18 106-46-7 ND ug/L 1.0 0.21 1 09/29/11 06:18 75-71-8 ND ug/L 1.0 0.32 1 09/29/11 06:18 75-34-3 ND ug/L 1.0 0.12 1 09/29/11 06:18 107-06-2 ND ug/L 1.0 0.56 1 09/29/11 06:18 75-35-4 ND ug/L 1.0 0.19 1 09/29/11 06:18 156-59-2 ND ug/L 1.0 0.49 1 09/29/11 06:18 156-60-5 ND ug/L 1.0 0.27 1 09/29/11 06:18 78-87-5 ND ug/L 1.0 0.28 1 09/29/11 06:18 142-28-9 ND ug/L 1.0 0.13 1 09/29/11 06:18 594-20-7 ND ug/L 1.0 0.49 1 09/29/11 06:18 563-58-6 ND ug/L 1.0 0.13 1 09/29/11 06:18 10061-01-5 ND ug/L 1.0 0.26 1 09/29/11 06:18 10061-02-6 ND ug/L 1.0 0.12 1 09/29/11 06:18 108-20-3 ND ug/L 1.0 0.30 1 09/29/11 06:18 100-41-4 ND ug/L 1.0 0.71 1 09/29/11 06:18 87-68-3 ND ug/L 5.0 0.46 1 09/29/11 06:18 591-78-6 ND ug/L 1.0 0.31 1 09/29/11 06:18 99-87-6 ND ug/L 2.0 0.97 1 09/29/11 06:18 75-09-2 ND ug/L 5.0 0.33 1 09/29/11 06:18 108-10-1 ND ug/L 1.0 0.21 1 09/29/11 06:18 1634-04-4 ND ug/L 1.0 0.24 1 09/29/11 06:18 91-20-3 ND ug/L 1.0 0.26 1 09/29/11 06:18 100-42-5 ND ug/L 1.0 0.33 1 09/29/11 06:18 630-20-6 ND ug/L 1.0 0.40 1 09/29/11 06:18 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 53 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RINSATEA Labll): 92103091025 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/29/11 06:18 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/29/11 06:18 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/29/11 06:18 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/29/11 06:18 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/29/11 06:18 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/29/11 06:18 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/29/11 06:18 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/29/11 06:18 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/29/11 06:18 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/29/11 06:18 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/29/11 06:18 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/29/11 06:18 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/29/11 06:18 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 1 09/29/11 06:18 460-00-4 Dibromofluoromethane (S) 108 % 70-130 1 09/29/11 06:18 1868-53-7 1,2-Dichloroethane-d4 (S) 115 % 70-130 1 09/29/11 06:18 17060-07-0 Tbluene-d8 (S) 92 % 70-130 1 09/29/11 06:18 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 54 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RINSATE B Labll): 92103091026 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 43.2 ug/L 25.0 2.2 1 09/29/11 06:41 67-64-1 ND ug/L 1.0 0.25 1 09/29/11 06:41 71-43-2 ND ug/L 1.0 0.30 1 09/29/11 06:41 108-86-1 ND ug/L 1.0 0.17 1 09/29/11 06:41 74-97-5 ND ug/L 1.0 0.18 1 09/29/11 06:41 75-27-4 ND ug/L 1.0 0.26 1 09/29/11 06:41 75-25-2 ND ug/L 2.0 0.29 1 09/29/11 06:41 74-83-9 ND ug/L 5.0 0.96 1 09/29/11 06:41 78-93-3 ND ug/L 1.0 0.25 1 09/29/11 06:41 56-23-5 ND ug/L 1.0 0.23 1 09/29/11 06:41 108-90-7 ND ug/L 1.0 0.54 1 09/29/11 06:41 75-00-3 ND ug/L 1.0 0.14 1 09/29/11 06:41 67-66-3 ND ug/L 1.0 0.11 1 09/29/11 06:41 74-87-3 ND ug/L 1.0 0.35 1 09/29/11 06:41 95-49-8 ND ug/L 1.0 0.31 1 09/29/11 06:41 106-43-4 ND ug/L 5.0 2.5 1 09/29/11 06:41 96-12-8 ND ug/L 1.0 0.21 1 09/29/11 06:41 124-48-1 ND ug/L 1.0 0.27 1 09/29/11 06:41 106-93-4 ND ug/L 1.0 0.21 1 09/29/11 06:41 74-95-3 ND ug/L 1.0 0.30 1 09/29/11 06:41 95-50-1 ND ug/L 1.0 0.24 1 09/29/11 06:41 541-73-1 ND ug/L 1.0 0.33 1 09/29/11 06:41 106-46-7 ND ug/L 1.0 0.21 1 09/29/11 06:41 75-71-8 ND ug/L 1.0 0.32 1 09/29/11 06:41 75-34-3 ND ug/L 1.0 0.12 1 09/29/11 06:41 107-06-2 ND ug/L 1.0 0.56 1 09/29/11 06:41 75-35-4 ND ug/L 1.0 0.19 1 09/29/11 06:41 156-59-2 ND ug/L 1.0 0.49 1 09/29/11 06:41 156-60-5 ND ug/L 1.0 0.27 1 09/29/11 06:41 78-87-5 ND ug/L 1.0 0.28 1 09/29/11 06:41 142-28-9 ND ug/L 1.0 0.13 1 09/29/11 06:41 594-20-7 ND ug/L 1.0 0.49 1 09/29/11 06:41 563-58-6 ND ug/L 1.0 0.13 1 09/29/11 06:41 10061-01-5 ND ug/L 1.0 0.26 1 09/29/11 06:41 10061-02-6 ND ug/L 1.0 0.12 1 09/29/11 06:41 108-20-3 ND ug/L 1.0 0.30 1 09/29/11 06:41 100-41-4 ND ug/L 1.0 0.71 1 09/29/11 06:41 87-68-3 ND ug/L 5.0 0.46 1 09/29/11 06:41 591-78-6 ND ug/L 1.0 0.31 1 09/29/11 06:41 99-87-6 ND ug/L 2.0 0.97 1 09/29/11 06:41 75-09-2 ND ug/L 5.0 0.33 1 09/29/11 06:41 108-10-1 ND ug/L 1.0 0.21 1 09/29/11 06:41 1634-04-4 ND ug/L 1.0 0.24 1 09/29/11 06:41 91-20-3 ND ug/L 1.0 0.26 1 09/29/11 06:41 100-42-5 ND ug/L 1.0 0.33 1 09/29/11 06:41 630-20-6 ND ug/L 1.0 0.40 1 09/29/11 06:41 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 55 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RINSATE B Labll): 92103091026 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/29/11 06:41 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/29/11 06:41 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/29/11 06:41 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/29/11 06:41 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/29/11 06:41 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/29/11 06:41 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/29/11 06:41 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/29/11 06:41 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/29/11 06:41 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/29/11 06:41 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/29/11 06:41 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/29/11 06:41 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/29/11 06:41 95-47-6 4-Bromofluorobenzene (S) 93 % 70-130 1 09/29/11 06:41 460-00-4 Dibromofluoromethane (S) 106 % 70-130 1 09/29/11 06:41 1868-53-7 1,2-Dichloroethane-d4 (S) 115 % 70-130 1 09/29/11 06:41 17060-07-0 Tbluene-d8 (S) 92 % 70-130 1 09/29/11 06:41 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 56 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DUPLICATEA LabID: 92103091027 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 31.1J ug/L 250 21.7 10 09/29/11 11:39 67-64-1 ND ug/L 10.0 2.5 10 09/29/11 11:39 71-43-2 ND ug/L 10.0 3.0 10 09/29/11 11:39 108-86-1 ND ug/L 10.0 1.7 10 09/29/11 11:39 74-97-5 ND ug/L 10.0 1.8 10 09/29/11 11:39 75-27-4 ND ug/L 10.0 2.6 10 09/29/11 11:39 75-25-2 ND ug/L 20.0 2.9 10 09/29/11 11:39 74-83-9 44.9J ug/L 50.0 9.6 10 09/29/11 11:39 78-93-3 ND ug/L 10.0 2.5 10 09/29/11 11:39 56-23-5 ND ug/L 10.0 2.3 10 09/29/11 11:39 108-90-7 ND ug/L 10.0 5.4 10 09/29/11 11:39 75-00-3 ND ug/L 10.0 1.4 10 09/29/11 11:39 67-66-3 ND ug/L 10.0 1.1 10 09/29/11 11:39 74-87-3 ND ug/L 10.0 3.5 10 09/29/11 11:39 95-49-8 ND ug/L 10.0 3.1 10 09/29/11 11:39 106-43-4 ND ug/L 50.0 25.2 10 09/29/11 11:39 96-12-8 ND ug/L 10.0 2.1 10 09/29/11 11:39 124-48-1 ND ug/L 10.0 2.7 10 09/29/11 11:39 106-93-4 ND ug/L 10.0 2.1 10 09/29/11 11:39 74-95-3 ND ug/L 10.0 3.0 10 09/29/11 11:39 95-50-1 ND ug/L 10.0 2.4 10 09/29/11 11:39 541-73-1 ND ug/L 10.0 3.3 10 09/29/11 11:39 106-46-7 ND ug/L 10.0 2.1 10 09/29/11 11:39 75-71-8 ND ug/L 10.0 3.2 10 09/29/11 11:39 75-34-3 ND ug/L 10.0 1.2 10 09/29/11 11:39 107-06-2 ND ug/L 10.0 5.6 10 09/29/11 11:39 75-35-4 1540 ug/L 10.0 1.9 10 09/29/11 11:39 156-59-2 12.2 ug/L 10.0 4.9 10 09/29/11 11:39 156-60-5 ND ug/L 10.0 2.7 10 09/29/11 11:39 78-87-5 ND ug/L 10.0 2.8 10 09/29/11 11:39 142-28-9 ND ug/L 10.0 1.3 10 09/29/11 11:39 594-20-7 ND ug/L 10.0 4.9 10 09/29/11 11:39 563-58-6 ND ug/L 10.0 1.3 10 09/29/11 11:39 10061-01-5 ND ug/L 10.0 2.6 10 09/29/11 11:39 10061-02-6 ND ug/L 10.0 1.2 10 09/29/11 11:39 108-20-3 ND ug/L 10.0 3.0 10 09/29/11 11:39 100-41-4 ND ug/L 10.0 7.1 10 09/29/11 11:39 87-68-3 ND ug/L 50.0 4.6 10 09/29/11 11:39 591-78-6 ND ug/L 10.0 3.1 10 09/29/11 11:39 99-87-6 ND ug/L 20.0 9.7 10 09/29/11 11:39 75-09-2 ND ug/L 50.0 3.3 10 09/29/11 11:39 108-10-1 ND ug/L 10.0 2.1 10 09/29/11 11:39 1634-04-4 ND ug/L 10.0 2.4 10 09/29/11 11:39 91-20-3 ND ug/L 10.0 2.6 10 09/29/11 11:39 100-42-5 ND ug/L 10.0 3.3 10 09/29/11 11:39 630-20-6 ND ug/L 10.0 4.0 10 09/29/11 11:39 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 57 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DUPLICATEA LabID: 92103091027 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 195 ug/L 10.0 4.6 10 09/29/11 11:39 127-18-4 Toluene ND ug/L 10.0 2.6 10 09/29/11 11:39 108-88-3 1,2,3-Trichlorobenzene ND ug/L 10.0 3.3 10 09/29/11 11:39 87-61-6 1,2,4-Trichlorobenzene ND ug/L 10.0 3.5 10 09/29/11 11:39 120-82-1 1,1,1-Trichloroethane ND ug/L 10.0 4.8 10 09/29/11 11:39 71-55-6 1,1,2-Trichloroethane ND ug/L 10.0 2.9 10 09/29/11 11:39 79-00-5 Trichloroethene 74.9 ug/L 10.0 4.7 10 09/29/11 11:39 79-01-6 Trichlorofluoromethane ND ug/L 10.0 2.0 10 09/29/11 11:39 75-69-4 1,2,3-Trichloropropane ND ug/L 10.0 4.1 10 09/29/11 11:39 96-18-4 Vinyl acetate ND ug/L 20.0 3.5 10 09/29/11 11:39 108-05-4 Vinyl chloride ND ug/L 10.0 6.2 10 09/29/11 11:39 75-01-4 m&p-Xylene ND ug/L 20.0 6.6 10 09/29/11 11:39 179601-23-1 o-Xylene ND ug/L 10.0 2.3 10 09/29/11 11:39 95-47-6 4-Bromofluorobenzene (S) 93 % 70-130 10 09/29/11 11:39 460-00-4 Dibromofluoromethane (S) 107 % 70-130 10 09/29/11 11:39 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 70-130 10 09/29/11 11:39 17060-07-0 Tbluene-d8 (S) 101 % 70-130 10 09/29/11 11:39 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 58 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DUPLICATE B Labll): 92103091028 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 2500 217 100 10/01/11 17:44 67-64-1 ND ug/L 100 25.0 100 10/01/11 17:44 71-43-2 ND ug/L 100 30.0 100 10/01/11 17:44 108-86-1 ND ug/L 100 17.0 100 10/01/11 17:44 74-97-5 ND ug/L 100 18.0 100 10/01/11 17:44 75-27-4 ND ug/L 100 26.0 100 10/01/11 17:44 75-25-2 ND ug/L 200 29.0 100 10/01/11 17:44 74-83-9 ND ug/L 500 96.0 100 10/01/11 17:44 78-93-3 ND ug/L 100 25.0 100 10/01/11 17:44 56-23-5 ND ug/L 100 23.0 100 10/01/11 17:44 108-90-7 ND ug/L 100 54.0 100 10/01/11 17:44 75-00-3 ND ug/L 100 14.0 100 10/01/11 17:44 67-66-3 ND ug/L 100 11.0 100 10/01/11 17:44 74-87-3 ND ug/L 100 35.0 100 10/01/11 17:44 95-49-8 ND ug/L 100 31.0 100 10/01/11 17:44 106-43-4 ND ug/L 500 252 100 10/01/11 17:44 96-12-8 ND ug/L 100 21.0 100 10/01/11 17:44 124-48-1 ND ug/L 100 27.0 100 10/01/11 17:44 106-93-4 ND ug/L 100 21.0 100 10/01/11 17:44 74-95-3 ND ug/L 100 30.0 100 10/01/11 17:44 95-50-1 ND ug/L 100 24.0 100 10/01/11 17:44 541-73-1 ND ug/L 100 33.0 100 10/01/11 17:44 106-46-7 ND ug/L 100 21.0 100 10/01/11 17:44 75-71-8 ND ug/L 100 32.0 100 10/01/11 17:44 75-34-3 ND ug/L 100 12.0 100 10/01/11 17:44 107-06-2 ND ug/L 100 56.0 100 10/01/11 17:44 75-35-4 7330 ug/L 100 19.0 100 10/01/11 17:44 156-59-2 ND ug/L 100 49.0 100 10/01/11 17:44 156-60-5 ND ug/L 100 27.0 100 10/01/11 17:44 78-87-5 ND ug/L 100 28.0 100 10/01/11 17:44 142-28-9 ND ug/L 100 13.0 100 10/01/11 17:44 594-20-7 ND ug/L 100 49.0 100 10/01/11 17:44 563-58-6 ND ug/L 100 13.0 100 10/01/11 17:44 10061-01-5 ND ug/L 100 26.0 100 10/01/11 17:44 10061-02-6 ND ug/L 100 12.0 100 10/01/11 17:44 108-20-3 ND ug/L 100 30.0 100 10/01/11 17:44 100-41-4 ND ug/L 100 71.0 100 10/01/11 17:44 87-68-3 369J ug/L 500 46.0 100 10/01/11 17:44 591-78-6 ND ug/L 100 31.0 100 10/01/11 17:44 99-87-6 ND ug/L 200 97.0 100 10/01/11 17:44 75-09-2 ND ug/L 500 33.0 100 10/01/11 17:44 108-10-1 ND ug/L 100 21.0 100 10/01/11 17:44 1634-04-4 ND ug/L 100 24.0 100 10/01/11 17:44 91-20-3 ND ug/L 100 26.0 100 10/01/11 17:44 100-42-5 ND ug/L 100 33.0 100 10/01/11 17:44 630-20-6 ND ug/L 100 40.0 100 10/01/11 17:44 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 59 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DUPLICATE B Labll): 92103091028 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1480 ug/L 100 46.0 100 10/01/11 17:44 127-18-4 Toluene ND ug/L 100 26.0 100 10/01/11 17:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 100 33.0 100 10/01/11 17:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 100 35.0 100 10/01/11 17:44 120-82-1 1,1,1-Trichloroethane ND ug/L 100 48.0 100 10/01/11 17:44 71-55-6 1,1,2-Trichloroethane ND ug/L 100 29.0 100 10/01/11 17:44 79-00-5 Trichloroethene 2170 ug/L 100 47.0 100 10/01/11 17:44 79-01-6 Trichlorofluoromethane ND ug/L 100 20.0 100 10/01/11 17:44 75-69-4 1,2,3-Trichloropropane ND ug/L 100 41.0 100 10/01/11 17:44 96-18-4 Vinyl acetate ND ug/L 200 35.0 100 10/01/11 17:44 108-05-4 Vinyl chloride ND ug/L 100 62.0 100 10/01/11 17:44 75-01-4 m&p-Xylene ND ug/L 200 66.0 100 10/01/11 17:44 179601-23-1 o-Xylene ND ug/L 100 23.0 100 10/01/11 17:44 95-47-6 4-Bromofluorobenzene (S) 95 % 70-130 100 10/01/11 17:44 460-00-4 Dibromofluoromethane (S) 106 % 70-130 100 10/01/11 17:44 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 70-130 100 10/01/11 17:44 17060-07-0 Tbluene-d8 (S) 104 % 70-130 100 10/01/11 17:44 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 60 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DUPLICATE C Labll): 92103091029 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 54.5 ug/L 25.0 2.2 1 10/01/11 18:09 67-64-1 ND ug/L 1.0 0.25 1 10/01/11 18:09 71-43-2 ND ug/L 1.0 0.30 1 10/01/11 18:09 108-86-1 ND ug/L 1.0 0.17 1 10/01/11 18:09 74-97-5 ND ug/L 1.0 0.18 1 10/01/11 18:09 75-27-4 ND ug/L 1.0 0.26 1 10/01/11 18:09 75-25-2 ND ug/L 2.0 0.29 1 10/01/11 18:09 74-83-9 ND ug/L 5.0 0.96 1 10/01/11 18:09 78-93-3 ND ug/L 1.0 0.25 1 10/01/11 18:09 56-23-5 ND ug/L 1.0 0.23 1 10/01/11 18:09 108-90-7 ND ug/L 1.0 0.54 1 10/01/11 18:09 75-00-3 ND ug/L 1.0 0.14 1 10/01/11 18:09 67-66-3 ND ug/L 1.0 0.11 1 10/01/11 18:09 74-87-3 ND ug/L 1.0 0.35 1 10/01/11 18:09 95-49-8 ND ug/L 1.0 0.31 1 10/01/11 18:09 106-43-4 ND ug/L 5.0 2.5 1 10/01/11 18:09 96-12-8 ND ug/L 1.0 0.21 1 10/01/11 18:09 124-48-1 ND ug/L 1.0 0.27 1 10/01/11 18:09 106-93-4 ND ug/L 1.0 0.21 1 10/01/11 18:09 74-95-3 ND ug/L 1.0 0.30 1 10/01/11 18:09 95-50-1 ND ug/L 1.0 0.24 1 10/01/11 18:09 541-73-1 ND ug/L 1.0 0.33 1 10/01/11 18:09 106-46-7 ND ug/L 1.0 0.21 1 10/01/11 18:09 75-71-8 ND ug/L 1.0 0.32 1 10/01/11 18:09 75-34-3 ND ug/L 1.0 0.12 1 10/01/11 18:09 107-06-2 ND ug/L 1.0 0.56 1 10/01/11 18:09 75-35-4 ND ug/L 1.0 0.19 1 10/01/11 18:09 156-59-2 ND ug/L 1.0 0.49 1 10/01/11 18:09 156-60-5 ND ug/L 1.0 0.27 1 10/01/11 18:09 78-87-5 ND ug/L 1.0 0.28 1 10/01/11 18:09 142-28-9 ND ug/L 1.0 0.13 1 10/01/11 18:09 594-20-7 ND ug/L 1.0 0.49 1 10/01/11 18:09 563-58-6 ND ug/L 1.0 0.13 1 10/01/11 18:09 10061-01-5 ND ug/L 1.0 0.26 1 10/01/11 18:09 10061-02-6 ND ug/L 1.0 0.12 1 10/01/11 18:09 108-20-3 ND ug/L 1.0 0.30 1 10/01/11 18:09 100-41-4 ND ug/L 1.0 0.71 1 10/01/11 18:09 87-68-3 ND ug/L 5.0 0.46 1 10/01/11 18:09 591-78-6 ND ug/L 1.0 0.31 1 10/01/11 18:09 99-87-6 ND ug/L 2.0 0.97 1 10/01/11 18:09 75-09-2 ND ug/L 5.0 0.33 1 10/01/11 18:09 108-10-1 ND ug/L 1.0 0.21 1 10/01/11 18:09 1634-04-4 ND ug/L 1.0 0.24 1 10/01/11 18:09 91-20-3 ND ug/L 1.0 0.26 1 10/01/11 18:09 100-42-5 ND ug/L 1.0 0.33 1 10/01/11 18:09 630-20-6 ND ug/L 1.0 0.40 1 10/01/11 18:09 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 61 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DUPLICATE C Labll): 92103091029 Collected: 09/23/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 10/01/11 18:09 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/01/11 18:09 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/01/11 18:09 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/01/11 18:09 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/01/11 18:09 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/01/11 18:09 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/01/11 18:09 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/01/11 18:09 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/01/11 18:09 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/01/11 18:09 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/01/11 18:09 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/01/11 18:09 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/01/11 18:09 95-47-6 4-Bromofluorobenzene (S) 96 % 70-130 1 10/01/11 18:09 460-00-4 Dibromofluoromethane (S) 108 % 70-130 1 10/01/11 18:09 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 70-130 1 10/01/11 18:09 17060-07-0 Tbluene-d8 (S) 103 % 70-130 1 10/01/11 18:09 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 62 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK Labll): 92103091030 Collected: 09/22/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (M113K) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 09/29/11 04:47 67-64-1 ND ug/L 1.0 0.25 1 09/29/11 04:47 71-43-2 ND ug/L 1.0 0.30 1 09/29/11 04:47 108-86-1 ND ug/L 1.0 0.17 1 09/29/11 04:47 74-97-5 ND ug/L 1.0 0.18 1 09/29/11 04:47 75-27-4 ND ug/L 1.0 0.26 1 09/29/11 04:47 75-25-2 ND ug/L 2.0 0.29 1 09/29/11 04:47 74-83-9 ND ug/L 5.0 0.96 1 09/29/11 04:47 78-93-3 ND ug/L 1.0 0.25 1 09/29/11 04:47 56-23-5 ND ug/L 1.0 0.23 1 09/29/11 04:47 108-90-7 ND ug/L 1.0 0.54 1 09/29/11 04:47 75-00-3 ND ug/L 1.0 0.14 1 09/29/11 04:47 67-66-3 0.38J ug/L 1.0 0.11 1 09/29/11 04:47 74-87-3 ND ug/L 1.0 0.35 1 09/29/11 04:47 95-49-8 ND ug/L 1.0 0.31 1 09/29/11 04:47 106-43-4 ND ug/L 5.0 2.5 1 09/29/11 04:47 96-12-8 ND ug/L 1.0 0.21 1 09/29/11 04:47 124-48-1 ND ug/L 1.0 0.27 1 09/29/11 04:47 106-93-4 ND ug/L 1.0 0.21 1 09/29/11 04:47 74-95-3 ND ug/L 1.0 0.30 1 09/29/11 04:47 95-50-1 ND ug/L 1.0 0.24 1 09/29/11 04:47 541-73-1 ND ug/L 1.0 0.33 1 09/29/11 04:47 106-46-7 ND ug/L 1.0 0.21 1 09/29/11 04:47 75-71-8 ND ug/L 1.0 0.32 1 09/29/11 04:47 75-34-3 ND ug/L 1.0 0.12 1 09/29/11 04:47 107-06-2 ND ug/L 1.0 0.56 1 09/29/11 04:47 75-35-4 ND ug/L 1.0 0.19 1 09/29/11 04:47 156-59-2 ND ug/L 1.0 0.49 1 09/29/11 04:47 156-60-5 ND ug/L 1.0 0.27 1 09/29/11 04:47 78-87-5 ND ug/L 1.0 0.28 1 09/29/11 04:47 142-28-9 ND ug/L 1.0 0.13 1 09/29/11 04:47 594-20-7 ND ug/L 1.0 0.49 1 09/29/11 04:47 563-58-6 ND ug/L 1.0 0.13 1 09/29/11 04:47 10061-01-5 ND ug/L 1.0 0.26 1 09/29/11 04:47 10061-02-6 ND ug/L 1.0 0.12 1 09/29/11 04:47 108-20-3 ND ug/L 1.0 0.30 1 09/29/11 04:47 100-41-4 ND ug/L 1.0 0.71 1 09/29/11 04:47 87-68-3 ND ug/L 5.0 0.46 1 09/29/11 04:47 591-78-6 ND ug/L 1.0 0.31 1 09/29/11 04:47 99-87-6 ND ug/L 2.0 0.97 1 09/29/11 04:47 75-09-2 ND ug/L 5.0 0.33 1 09/29/11 04:47 108-10-1 ND ug/L 1.0 0.21 1 09/29/11 04:47 1634-04-4 ND ug/L 1.0 0.24 1 09/29/11 04:47 91-20-3 ND ug/L 1.0 0.26 1 09/29/11 04:47 100-42-5 ND ug/L 1.0 0.33 1 09/29/11 04:47 630-20-6 ND ug/L 1.0 0.40 1 09/29/11 04:47 79-34-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 63 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK Labll): 92103091030 Collected: 09/22/11 00:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 09/29/11 04:47 127-18-4 Toluene ND ug/L 1.0 0.26 1 09/29/11 04:47 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 09/29/11 04:47 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 09/29/11 04:47 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 09/29/11 04:47 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 09/29/11 04:47 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 09/29/11 04:47 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 09/29/11 04:47 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 09/29/11 04:47 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 09/29/11 04:47 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 09/29/11 04:47 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 09/29/11 04:47 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 09/29/11 04:47 95-47-6 4-Bromofluorobenzene (S) 92 % 70-130 1 09/29/11 04:47 460-00-4 Dibromofluoromethane (S) 106 % 70-130 1 09/29/11 04:47 1868-53-7 1,2-Dichloroethane-d4 (S) 114 % 70-130 1 09/29/11 04:47 17060-07-0 Tbluene-d8 (S) 91 % 70-130 1 09/29/11 04:47 2037-26-5 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 64 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 QC Batch: MSV/16819 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92103091001,92103091002,92103091003,92103091004,92103091005,92103091006,92103091007, 92103091008,92103091009,92103091011,92103091012,92103091014,92103091015,92103091016 METHOD BLANK: 665388 Matrix: Water Associated Lab Samples: 92103091001,92103091002,92103091003,92103091004,92103091005,92103091006,92103091007, 92103091008,92103091009,92103091011,92103091012,92103091014,92103091015,92103091016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/28/11 16:35 1,1,1-Trichloroethane ug/L ND 1.0 09/28/11 16:35 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/28/11 16:35 1,1,2-Trichloroethane ug/L ND 1.0 09/28/11 16:35 1,1-Dichloroethane ug/L ND 1.0 09/28/11 16:35 1,1-Dichloroethene ug/L ND 1.0 09/28/11 16:35 1,1-Dichloropropene ug/L ND 1.0 09/28/11 16:35 1,2,3-Trichlorobenzene ug/L ND 1.0 09/28/11 16:35 1,2,3-Trichloropropane ug/L ND 1.0 09/28/11 16:35 1,2,4-Trichlorobenzene ug/L ND 1.0 09/28/11 16:35 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/28/11 16:35 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/28/11 16:35 1,2-Dichlorobenzene ug/L ND 1.0 09/28/11 16:35 1,2-Dichloroethane ug/L ND 1.0 09/28/11 16:35 1,2-Dichloropropane ug/L ND 1.0 09/28/11 16:35 1,3-Dichlorobenzene ug/L ND 1.0 09/28/11 16:35 1,3-Dichloropropane ug/L ND 1.0 09/28/11 16:35 1,4-Dichlorobenzene ug/L ND 1.0 09/28/11 16:35 2,2-Dichloropropane ug/L ND 1.0 09/28/11 16:35 2-Butanone (MEK) ug/L ND 5.0 09/28/11 16:35 2-Chlorotoluene ug/L ND 1.0 09/28/11 16:35 2-Hexanone ug/L ND 5.0 09/28/11 16:35 4-Chlorotoluene ug/L ND 1.0 09/28/11 16:35 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/28/11 16:35 Acetone ug/L ND 25.0 09/28/11 16:35 Benzene ug/L ND 1.0 09/28/11 16:35 Bromobenzene ug/L ND 1.0 09/28/11 16:35 Bromochloromethane ug/L ND 1.0 09/28/11 16:35 Bromodichloromethane ug/L ND 1.0 09/28/11 16:35 Bromoform ug/L ND 1.0 09/28/11 16:35 Bromomethane ug/L ND 2.0 09/28/11 16:35 Carbon tetrachloride ug/L ND 1.0 09/28/11 16:35 Chlorobenzene ug/L ND 1.0 09/28/11 16:35 Chloroethane ug/L ND 1.0 09/28/11 16:35 Chloroform ug/L ND 1.0 09/28/11 16:35 Chloromethane ug/L ND 1.0 09/28/11 16:35 cis-1,2-Dichloroethene ug/L ND 1.0 09/28/11 16:35 cis-1,3-Dichloropropene ug/L ND 1.0 09/28/11 16:35 Dibromochloromethane ug/L ND 1.0 09/28/11 16:35 Dibromomethane ug/L ND 1.0 09/28/11 16:35 Dichlorodifluoromethane ug/L ND 1.0 09/28/11 16:35 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 65 of 81 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 METHOD BLANK: 665388 Matrix: Water Associated Lab Samples: 92103091001,92103091002,92103091003,92103091004,92103091005,92103091006,92103091007, 92103091008,92103091009,92103091011,92103091012,92103091014,92103091015,92103091016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diisopropyl ether ug/L ND 1.0 09/28/11 16:35 Ethylbenzene ug/L ND 1.0 09/28/11 16:35 Hexachloro-1,3-butadiene ug/L ND 1.0 09/28/11 16:35 m&p-Xylene ug/L ND 2.0 09/28/11 16:35 Methyl-tert-butyl ether ug/L ND 1.0 09/28/11 16:35 Methylene Chloride ug/L ND 2.0 09/28/11 16:35 Naphthalene ug/L ND 1.0 09/28/11 16:35 o-Xylene ug/L ND 1.0 09/28/11 16:35 p-Isopropyltoluene ug/L ND 1.0 09/28/11 16:35 Styrene ug/L ND 1.0 09/28/11 16:35 Tetrachloroethene ug/L ND 1.0 09/28/11 16:35 Toluene ug/L ND 1.0 09/28/11 16:35 trans- 1,2-Dichloroethene ug/L ND 1.0 09/28/11 16:35 trans- 1, 3-Dichloropropene ug/L ND 1.0 09/28/11 16:35 Trichloroethene ug/L ND 1.0 09/28/11 16:35 Trichlorofluoromethane ug/L ND 1.0 09/28/11 16:35 Vinyl acetate ug/L ND 2.0 09/28/11 16:35 Vinyl chloride ug/L ND 1.0 09/28/11 16:35 1,2-Dichloroethane-d4 (S) % 116 70-130 09/28/11 16:35 4-Bromofluorobenzene (S) % 91 70-130 09/28/11 16:35 Dibromofluoromethane (S) % 107 70-130 09/28/11 16:35 Toluene-d8 (S) % 93 70-130 09/28/11 16:35 LABORATORY CONTROL SAMPLE: 665389 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.7 103 70-130 1,1,1-Trichloroethane ug/L 50 50.9 102 70-130 1,1,2,2-Tetrachloroethane ug/L 50 50.7 101 70-130 1,1,2-Trichloroethane ug/L 50 52.2 104 70-130 M-Dichloroethane ug/L 50 50.7 101 70-130 M-Dichloroethene ug/L 50 54.6 109 70-132 1,1-Dichloropropene ug/L 50 53.8 108 70-130 1,2,3-Trichlorobenzene ug/L 50 49.9 100 70-135 1,2,3-Trichloropropane ug/L 50 49.5 99 70-130 1,2,4-Trichlorobenzene ug/L 50 46.1 92 70-134 1,2-Dibromo-3-chloropropane ug/L 50 57.0 114 70-130 1,2-Dibromoethane (EDB) ug/L 50 53.1 106 70-130 1,2-Dichlorobenzene ug/L 50 54.3 109 70-130 1,2-Dichloroethane ug/L 50 55.1 110 70-130 1,2-Dichloropropane ug/L 50 54.1 108 70-130 1,3-Dichlorobenzene ug/L 50 54.2 108 70-130 1,3-Dichloropropane ug/L 50 54.5 109 70-130 1,4-Dichlorobenzene ug/L 50 50.3 101 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 66 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 LABORATORY CONTROL SAMPLE: Parameter 665389 Units Spike Conc. LCS Result 2,2-Dichloropropane ug/L 50 54.1 2-Butanone (MEK) ug/L 100 112 2-Chlorotoluene ug/L 50 58.1 2-Hexanone ug/L 100 103 4-Chlorotoluene ug/L 50 59.0 4-Methyl-2-pentanone (MIBK) ug/L 100 100 Acetone ug/L 100 143 Benzene ug/L 50 52.5 Bromobenzene ug/L 50 52.0 Bromochloromethane ug/L 50 51.1 Bromodichloromethane ug/L 50 53.6 Bromoform ug/L 50 51.6 Bromomethane ug/L 50 64.1 Carbon tetrachloride ug/L 50 52.3 Chlorobenzene ug/L 50 49.3 Chloroethane ug/L 50 56.8 Chloroform ug/L 50 54.8 Chloromethane ug/L 50 56.3 cis-1,2-Dichloroethene ug/L 50 50.3 cis-1,3-Dichloropropene ug/L 50 49.7 Dibromochloromethane ug/L 50 51.5 Dibromomethane ug/L 50 50.1 Dichlorodifluoromethane ug/L 50 43.4 Diisopropyl ether ug/L 50 57.2 Ethylbenzene ug/L 50 53.4 Hexachloro-1,3-butadiene ug/L 50 52.5 m&p-Xylene ug/L 100 104 Methyl-tert-butyl ether ug/L 50 58.2 Methylene Chloride ug/L 50 57.5 Naphthalene ug/L 50 48.6 o-Xylene ug/L 50 49.2 p-Isopropyltoluene ug/L 50 49.9 Styrene ug/L 50 50.6 Tetrachloroethene ug/L 50 50.4 Toluene ug/L 50 52.2 trans- 1,2-Dichloroethene ug/L 50 51.5 trans- 1, 3-Dichloropropene ug/L 50 51.4 Trichloroethene ug/L 50 52.9 Trichlorofluoromethane ug/L 50 54.1 Vinyl acetate ug/L 100 ill Vinyl chloride ug/L 50 55.5 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Tbluene-d8 (S) % LCS % Rec % Rec Limits 108 58-145 112 70-145 116 70-130 103 70-144 118 70-130 100 70-140 143 50-175 105 70-130 104 70-130 102 70-130 107 70-130 103 70-130 128 54-130 105 70-132 99 70-130 114 64-134 110 70-130 113 64-130 101 70-131 99 70-130 103 70-130 100 70-131 87 56-130 114 70-130 107 70-130 105 70-130 104 70-130 116 70-130 115 63-130 97 70-138 98 70-130 100 70-130 101 70-130 101 70-130 104 70-130 103 70-130 103 70-132 106 70-130 108 62-133 ill 66-157 ill 69-130 105 70-130 97 70-130 101 70-130 103 70-130 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 67 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 665806 665807 IVIS MSD 92103091014 Spike Spike IVIS MSD IVIS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual M-Dichloroethene ug/L ND 50 50 62.8 60.0 126 120 70-166 4 30 Benzene ug/L ND 50 50 57.0 58.1 114 116 70-148 2 30 Chlorobenzene ug/L ND 50 50 57.4 56.4 115 113 70-146 2 30 Toluene ug/L ND 50 50 57.3 59.9 115 120 70-155 5 30 Trichloroethene ug/L ND 50 50 55.0 49.9 110 100 69-151 10 30 1,2-Dichloroethane-d4 (S) % 112 111 70-130 4-Bromofluorobenzene (S) % 92 90 70-130 Dibromofluoromethane (S) % 104 104 70-130 Tbluene-d8 (S) % 90 96 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 68 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 QC Batch: MSV/16822 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92103091017,92103091018,92103091019,92103091021,92103091022,92103091024,92103091025, 92103091026,92103091027,92103091030 METHOD BLANK: 665518 Matrix: Water Associated Lab Samples: 92103091017,92103091018,92103091019,92103091021,92103091022,92103091024,92103091025, 92103091026,92103091027,92103091030 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/29/11 04:24 1,1,1-Trichloroethane ug/L ND 1.0 09/29/11 04:24 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/29/11 04:24 1,1,2-Trichloroethane ug/L ND 1.0 09/29/11 04:24 1,1-Dichloroethane ug/L ND 1.0 09/29/11 04:24 1,1-Dichloroethene ug/L ND 1.0 09/29/11 04:24 1,1-Dichloropropene ug/L ND 1.0 09/29/11 04:24 1,2,3-Trichlorobenzene ug/L ND 1.0 09/29/11 04:24 1,2,3-Trichloropropane ug/L ND 1.0 09/29/11 04:24 1,2,4-Trichlorobenzene ug/L ND 1.0 09/29/11 04:24 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/29/11 04:24 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/29/11 04:24 1,2-Dichlorobenzene ug/L ND 1.0 09/29/11 04:24 1,2-Dichloroethane ug/L ND 1.0 09/29/11 04:24 1,2-Dichloropropane ug/L ND 1.0 09/29/11 04:24 1,3-Dichlorobenzene ug/L ND 1.0 09/29/11 04:24 1,3-Dichloropropane ug/L ND 1.0 09/29/11 04:24 1,4-Dichlorobenzene ug/L ND 1.0 09/29/11 04:24 2,2-Dichloropropane ug/L ND 1.0 09/29/11 04:24 2-Butanone (MEK) ug/L ND 5.0 09/29/11 04:24 2-Chlorotoluene ug/L ND 1.0 09/29/11 04:24 2-Hexanone ug/L ND 5.0 09/29/11 04:24 4-Chlorotoluene ug/L ND 1.0 09/29/11 04:24 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/29/11 04:24 Acetone ug/L ND 25.0 09/29/11 04:24 Benzene ug/L ND 1.0 09/29/11 04:24 Bromobenzene ug/L ND 1.0 09/29/11 04:24 Bromochloromethane ug/L ND 1.0 09/29/11 04:24 Bromodichloromethane ug/L ND 1.0 09/29/11 04:24 Bromoform ug/L ND 1.0 09/29/11 04:24 Bromomethane ug/L ND 2.0 09/29/11 04:24 Carbon tetrachloride ug/L ND 1.0 09/29/11 04:24 Chlorobenzene ug/L ND 1.0 09/29/11 04:24 Chloroethane ug/L ND 1.0 09/29/11 04:24 Chloroform ug/L ND 1.0 09/29/11 04:24 Chloromethane ug/L ND 1.0 09/29/11 04:24 cis-1,2-Dichloroethene ug/L ND 1.0 09/29/11 04:24 cis-1,3-Dichloropropene ug/L ND 1.0 09/29/11 04:24 Dibromochloromethane ug/L ND 1.0 09/29/11 04:24 Dibromomethane ug/L ND 1.0 09/29/11 04:24 Dichlorodifluoromethane ug/L ND 1.0 09/29/11 04:24 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 69 of 81 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 METHOD BLANK: 665518 Matrix: Water Associated Lab Samples: 92103091017,92103091018,92103091019,92103091021,92103091022,92103091024,92103091025, 92103091026,92103091027,92103091030 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Diisopropyl ether ug/L ND 1.0 09/29/11 04:24 Ethylbenzene ug/L ND 1.0 09/29/11 04:24 Hexachloro-1,3-butadiene ug/L ND 1.0 09/29/11 04:24 m&p-Xylene ug/L ND 2.0 09/29/11 04:24 Methyl-tert-butyl ether ug/L ND 1.0 09/29/11 04:24 Methylene Chloride ug/L ND 2.0 09/29/11 04:24 Naphthalene ug/L ND 1.0 09/29/11 04:24 o-Xylene ug/L ND 1.0 09/29/11 04:24 p-Isopropyltoluene ug/L ND 1.0 09/29/11 04:24 Styrene ug/L ND 1.0 09/29/11 04:24 Tetrachloroethene ug/L ND 1.0 09/29/11 04:24 Toluene ug/L ND 1.0 09/29/11 04:24 trans- 1,2-Dichloroethene ug/L ND 1.0 09/29/11 04:24 trans- 1, 3-Dichloropropene ug/L ND 1.0 09/29/11 04:24 Trichloroethene ug/L ND 1.0 09/29/11 04:24 Trichlorofluoromethane ug/L ND 1.0 09/29/11 04:24 Vinyl acetate ug/L ND 2.0 09/29/11 04:24 Vinyl chloride ug/L ND 1.0 09/29/11 04:24 1,2-Dichloroethane-d4 (S) % 116 70-130 09/29/11 04:24 4-Bromofluorobenzene (S) % 92 70-130 09/29/11 04:24 Dibromofluoromethane (S) % 107 70-130 09/29/11 04:24 Toluene-d8 (S) % 92 70-130 09/29/11 04:24 LABORATORY CONTROL SAMPLE: 665519 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.3 109 70-130 1,1,1-Trichloroethane ug/L 50 51.5 103 70-130 1,1,2,2-Tetrachloroethane ug/L 50 49.6 99 70-130 1,1,2-Trichloroethane ug/L 50 52.3 105 70-130 M-Dichloroethane ug/L 50 51.3 103 70-130 M-Dichloroethene ug/L 50 54.3 109 70-132 1,1-Dichloropropene ug/L 50 53.0 106 70-130 1,2,3-Trichlorobenzene ug/L 50 48.5 97 70-135 1,2,3-Trichloropropane ug/L 50 49.7 99 70-130 1,2,4-Trichlorobenzene ug/L 50 43.9 88 70-134 1,2-Dibromo-3-chloropropane ug/L 50 54.0 108 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.0 108 70-130 1,2-Dichlorobenzene ug/L 50 54.3 109 70-130 1,2-Dichloroethane ug/L 50 55.1 110 70-130 1,2-Dichloropropane ug/L 50 54.6 109 70-130 1,3-Dichlorobenzene ug/L 50 54.0 108 70-130 1,3-Dichloropropane ug/L 50 55.4 ill 70-130 1,4-Dichlorobenzene ug/L 50 50.6 101 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 70 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 LABORATORY CONTROL SAMPLE: Parameter 665519 Units Spike Conc. 2,2-Dichloropropane ug/L 50 2-Butanone (MEK) ug/L 100 2-Chlorotoluene ug/L 50 2-Hexanone ug/L 100 4-Chlorotoluene ug/L 50 4-Methyl-2-pentanone (MIBK) ug/L 100 Acetone ug/L 100 Benzene ug/L 50 Bromobenzene ug/L 50 Bromochloromethane ug/L 50 Bromodichloromethane ug/L 50 Bromoform ug/L 50 Bromomethane ug/L 50 Carbon tetrachloride ug/L 50 Chlorobenzene ug/L 50 Chloroethane ug/L 50 Chloroform ug/L 50 Chloromethane ug/L 50 cis-1,2-Dichloroethene ug/L 50 cis-1,3-Dichloropropene ug/L 50 Dibromochloromethane ug/L 50 Dibromomethane ug/L 50 Dichlorodifluoromethane ug/L 50 Diisopropyl ether ug/L 50 Ethylbenzene ug/L 50 Hexachloro-1,3-butadiene ug/L 50 m&p-Xylene ug/L 100 Methyl-tert-butyl ether ug/L 50 Methylene Chloride ug/L 50 Naphthalene ug/L 50 o-Xylene ug/L 50 p-Isopropyltoluene ug/L 50 Styrene ug/L 50 Tetrachloroethene ug/L 50 Toluene ug/L 50 trans- 1,2-Dichloroethene ug/L 50 trans- 1, 3-Dichloropropene ug/L 50 Trichloroethene ug/L 50 Trichlorofluoromethane ug/L 50 Vinyl acetate ug/L 100 Vinyl chloride ug/L 50 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Tbluene-d8 (S) % Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS Result LCS % Rec % Rec Limits Qualifiers 48.2 96 58-145 99.3 99 70-145 58.3 117 70-130 96.0 96 70-144 58.9 118 70-130 95.1 95 70-140 123 123 50-175 52.5 105 70-130 51.9 104 70-130 51.4 103 70-130 54.3 109 70-130 51.4 103 70-130 65.5 131 54-130 LO 54.2 108 70-132 51.1 102 70-130 56.5 113 64-134 55.1 110 70-130 57.9 116 64-130 50.1 100 70-131 47.8 96 70-130 53.0 106 70-130 51.5 103 70-131 41.4 83 56-130 55.7 ill 70-130 54.8 110 70-130 50.2 100 70-130 105 105 70-130 55.3 ill 70-130 58.3 117 63-130 46.0 92 70-138 49.2 98 70-130 49.5 99 70-130 51.8 104 70-130 50.9 102 70-130 52.5 105 70-130 51.8 104 70-130 50.0 100 70-132 54.3 109 70-130 54.6 109 62-133 104 104 66-157 56.0 112 69-130 102 70-130 97 70-130 101 70-130 100 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 71 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 665810 665811 IVIS MSD 92103091019 Spike Spike IVIS MSD IVIS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual M-Dichloroethene ug/L ND 50 50 63.0 61.9 126 124 70-166 2 30 Benzene ug/L ND 50 50 60.6 57.4 121 115 70-148 5 30 Chlorobenzene ug/L ND 50 50 56.5 58.4 113 117 70-146 3 30 Toluene ug/L ND 50 50 60.8 57.8 122 116 70-155 5 30 Trichloroethene ug/L ND 50 50 52.4 54.6 105 109 69-151 4 30 1,2-Dichloroethane-d4 (S) % 112 112 70-130 4-Bromofluorobenzene (S) % 91 89 70-130 Dibromofluoromethane (S) % 105 105 70-130 Tbluene-d8 (S) % 97 91 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 72 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 QC Batch: MSV/16831 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92103091010,92103091020,92103091023,92103091028,92103091029 METHOD BLANK: 666075 Matrix: Water Associated Lab Samples: 92103091010,92103091020,92103091023,92103091028,92103091029 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/01/11 11:14 1,1,1-Trichloroethane ug/L ND 1.0 10/01/11 11:14 1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/01/11 11:14 1,1,2-Trichloroethane ug/L ND 1.0 10/01/11 11:14 1,1-Dichloroethane ug/L ND 1.0 10/01/11 11:14 1,1-Dichloroethene ug/L ND 1.0 10/01/11 11:14 1,1-Dichloropropene ug/L ND 1.0 10/01/11 11:14 1,2,3-Trichlorobenzene ug/L ND 1.0 10/01/11 11:14 1,2,3-Trichloropropane ug/L ND 1.0 10/01/11 11:14 1,2,4-Trichlorobenzene ug/L ND 1.0 10/01/11 11:14 1,2-Dibromo-3-chloropropane ug/L ND 5.0 10/01/11 11:14 1,2-Dibromoethane (EDB) ug/L ND 1.0 10/01/11 11:14 1,2-Dichlorobenzene ug/L ND 1.0 10/01/11 11:14 1,2-Dichloroethane ug/L ND 1.0 10/01/11 11:14 1,2-Dichloropropane ug/L ND 1.0 10/01/11 11:14 1,3-Dichlorobenzene ug/L ND 1.0 10/01/11 11:14 1,3-Dichloropropane ug/L ND 1.0 10/01/11 11:14 1,4-Dichlorobenzene ug/L ND 1.0 10/01/11 11:14 2,2-Dichloropropane ug/L ND 1.0 10/01/11 11:14 2-Butanone (MEK) ug/L ND 5.0 10/01/11 11:14 2-Chlorotoluene ug/L ND 1.0 10/01/11 11:14 2-Hexanone ug/L ND 5.0 10/01/11 11:14 4-Chlorotoluene ug/L ND 1.0 10/01/11 11:14 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 10/01/11 11:14 Acetone ug/L ND 25.0 10/01/11 11:14 Benzene ug/L ND 1.0 10/01/11 11:14 Bromobenzene ug/L ND 1.0 10/01/11 11:14 Bromochloromethane ug/L ND 1.0 10/01/11 11:14 Bromodichloromethane ug/L ND 1.0 10/01/11 11:14 Bromoform ug/L ND 1.0 10/01/11 11:14 Bromomethane ug/L ND 2.0 10/01/11 11:14 Carbon tetrachloride ug/L ND 1.0 10/01/11 11:14 Chlorobenzene ug/L ND 1.0 10/01/11 11:14 Chloroethane ug/L ND 1.0 10/01/11 11:14 Chloroform ug/L ND 1.0 10/01/11 11:14 Chloromethane ug/L ND 1.0 10/01/11 11:14 cis-1,2-Dichloroethene ug/L ND 1.0 10/01/11 11:14 cis-1,3-Dichloropropene ug/L ND 1.0 10/01/11 11:14 Dibromochloromethane ug/L ND 1.0 10/01/11 11:14 Dibromomethane ug/L ND 1.0 10/01/11 11:14 Dichlorodifluoromethane ug/L ND 1.0 10/01/11 11:14 Diisopropyl ether ug/L ND 1.0 10/01/11 11:14 Ethylbenzene ug/L ND 1.0 10/01/11 11:14 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 73 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 METHOD BLANK: 666075 Matrix: Water Associated Lab Samples: 92103091010,92103091020,92103091023,92103091028,92103091029 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L 0.92J 1.0 10/01/11 11:14 m&p-Xylene ug/L ND 2.0 10/01/11 11:14 Methyl-tert-butyl ether ug/L ND 1.0 10/01/11 11:14 Methylene Chloride ug/L ND 2.0 10/01/11 11:14 Naphthalene ug/L ND 1.0 10/01/11 11:14 o-Xylene ug/L ND 1.0 10/01/11 11:14 p-Isopropyltoluene ug/L ND 1.0 10/01/11 11:14 Styrene ug/L ND 1.0 10/01/11 11:14 Tetrachloroethene ug/L ND 1.0 10/01/11 11:14 Toluene ug/L ND 1.0 10/01/11 11:14 trans- 1,2-Dichloroethene ug/L ND 1.0 10/01/11 11:14 trans- 1, 3-Dichloropropene ug/L ND 1.0 10/01/11 11:14 Trichloroethene ug/L ND 1.0 10/01/11 11:14 Trichlorofluoromethane ug/L ND 1.0 10/01/11 11:14 Vinyl acetate ug/L ND 2.0 10/01/11 11:14 Vinyl chloride ug/L ND 1.0 10/01/11 11:14 1,2-Dichloroethane-d4 (S) % 110 70-130 10/01/11 11:14 4-Bromofluorobenzene (S) % 97 70-130 10/01/11 11:14 Dibromofluoromethane (S) % 108 70-130 10/01/11 11:14 Tbluene-d8 (S) % 101 70-130 10/01/11 11:14 LABORATORY CONTROL SAMPLE: 666076 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 52.3 105 70-130 1,1,1-Trichloroethane ug/L 50 44.8 90 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.7 107 70-130 1,1,2-Trichloroethane ug/L 50 50.1 100 70-130 1,1-Dichloroethane ug/L 50 50.5 101 70-130 1,1-Dichloroethene ug/L 50 52.2 104 70-132 1,1-Dichloropropene ug/L 50 46.1 92 70-130 1,2,3-Trichlorobenzene ug/L 50 51.4 103 70-135 1,2,3-Trichloropropane ug/L 50 52.2 104 70-130 1,2,4-Trichlorobenzene ug/L 50 50.4 101 70-134 1,2-Dibromo-3-chloropropane ug/L 50 57.6 115 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.1 104 70-130 1,2-Dichlorobenzene ug/L 50 50.0 100 70-130 1,2-Dichloroethane ug/L 50 54.1 108 70-130 1,2-Dichloropropane ug/L 50 52.1 104 70-130 1,3-Dichlorobenzene ug/L 50 50.7 101 70-130 1,3-Dichloropropane ug/L 50 51.2 102 70-130 1,4-Dichlorobenzene ug/L 50 48.6 97 70-130 2,2-Dichloropropane ug/L 50 37.3 75 58-145 2-Butanone (MEK) ug/L 100 96.8 97 70-145 2-Chlorotoluene ug/L 50 50.6 101 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 74 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 LABORATORY CONTROL SAMPLE: Parameter 666076 Units Spike Conc. 2-Hexanone ug/L 100 4-Chlorotoluene ug/L 50 4-Methyl-2-pentanone (MIBK) ug/L 100 Acetone ug/L 100 Benzene ug/L 50 Bromobenzene ug/L 50 Bromochloromethane ug/L 50 Bromodichloromethane ug/L 50 Bromoform ug/L 50 Bromomethane ug/L 50 Carbon tetrachloride ug/L 50 Chlorobenzene ug/L 50 Chloroethane ug/L 50 Chloroform ug/L 50 Chloromethane ug/L 50 cis-1,2-Dichloroethene ug/L 50 cis-1,3-Dichloropropene ug/L 50 Dibromochloromethane ug/L 50 Dibromomethane ug/L 50 Dichlorodifluoromethane ug/L 50 Diisopropyl ether ug/L 50 Ethylbenzene ug/L 50 Hexachloro-1,3-butadiene ug/L 50 m&p-Xylene ug/L 100 Methyl-tert-butyl ether ug/L 50 Methylene Chloride ug/L 50 Naphthalene ug/L 50 o-Xylene ug/L 50 p-Isopropyltoluene ug/L 50 Styrene ug/L 50 Tetrachloroethene ug/L 50 Toluene ug/L 50 trans- 1,2-Dichloroethene ug/L 50 trans- 1, 3-Dichloropropene ug/L 50 Trichloroethene ug/L 50 Trichlorofluoromethane ug/L 50 Vinyl acetate ug/L 100 Vinyl chloride ug/L 50 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Tbluene-d8 (S) % Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS Result LCS % Rec % Rec Limits Qualifiers ill 70-144 51.9 104 70-130 109 109 70-140 128 128 50-175 49.8 100 70-130 50.0 100 70-130 49.8 100 70-130 50.4 101 70-130 53.8 108 70-130 69.6 139 54-130 LO 53.1 106 70-132 50.4 101 70-130 65.8 132 64-134 53.2 106 70-130 53.0 106 64-130 49.6 99 70-131 51.1 102 70-130 50.1 100 70-130 50.2 100 70-131 52.7 105 56-130 51.1 102 70-130 49.0 98 70-130 49.2 98 70-130 100 100 70-130 54.1 108 70-130 60.9 122 63-130 54.1 108 70-138 52.2 104 70-130 51.1 102 70-130 54.9 110 70-130 47.9 96 70-130 49.8 100 70-130 50.5 101 70-130 50.2 100 70-132 53.5 107 70-130 58.9 118 62-133 95.8 96 66-157 55.2 110 69-130 102 70-130 100 70-130 94 70-130 98 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 75 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 666077 666078 IVIS MSD 92103225001 Spike Spike IVIS MSD IVIS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual M-Dichloroethene ug/L ND 50 50 59.9 64.2 120 128 70-166 7 30 Benzene ug/L ND 50 50 53.6 55.7 107 111 70-148 4 30 Chlorobenzene ug/L ND 50 50 52.2 54.2 104 108 70-146 4 30 Toluene ug/L ND 50 50 53.3 55.9 107 112 70-155 5 30 Trichloroethene ug/L ND 50 50 50.5 53.5 101 107 69-151 6 30 1,2-Dichloroethane-d4 (S) % 103 108 70-130 4-Bromofluorobenzene (S) % 94 95 70-130 Dibromofluoromethane (S) % 100 101 70-130 Tbluene-d8 (S) % 98 100 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 76 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 QC Batch: MSV/16848 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92103091013 METHOD BLANK: 667439 Matrix: Water Associated Lab Samples: 92103091013 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/03/11 21:59 1,1,1-Trichloroethane ug/L ND 1.0 10/03/11 21:59 1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/03/11 21:59 1,1,2-Trichloroethane ug/L ND 1.0 10/03/11 21:59 1,1-Dichloroethane ug/L ND 1.0 10/03/11 21:59 1,1-Dichloroethene ug/L ND 1.0 10/03/11 21:59 1,1-Dichloropropene ug/L ND 1.0 10/03/11 21:59 1,2,3-Trichlorobenzene ug/L ND 1.0 10/03/11 21:59 1,2,3-Trichloropropane ug/L ND 1.0 10/03/11 21:59 1,2,4-Trichlorobenzene ug/L ND 1.0 10/03/11 21:59 1,2-Dibromo-3-chloropropane ug/L ND 5.0 10/03/11 21:59 1,2-Dibromoethane (EDB) ug/L ND 1.0 10/03/11 21:59 1,2-Dichlorobenzene ug/L ND 1.0 10/03/11 21:59 1,2-Dichloroethane ug/L ND 1.0 10/03/11 21:59 1,2-Dichloropropane ug/L ND 1.0 10/03/11 21:59 1,3-Dichlorobenzene ug/L ND 1.0 10/03/11 21:59 1,3-Dichloropropane ug/L ND 1.0 10/03/11 21:59 1,4-Dichlorobenzene ug/L ND 1.0 10/03/11 21:59 2,2-Dichloropropane ug/L ND 1.0 10/03/11 21:59 2-Butanone (MEK) ug/L ND 5.0 10/03/11 21:59 2-Chlorotoluene ug/L ND 1.0 10/03/11 21:59 2-Hexanone ug/L ND 5.0 10/03/11 21:59 4-Chlorotoluene ug/L ND 1.0 10/03/11 21:59 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 10/03/11 21:59 Acetone ug/L ND 25.0 10/03/11 21:59 Benzene ug/L ND 1.0 10/03/11 21:59 Bromobenzene ug/L ND 1.0 10/03/11 21:59 Bromochloromethane ug/L ND 1.0 10/03/11 21:59 Bromodichloromethane ug/L ND 1.0 10/03/11 21:59 Bromoform ug/L ND 1.0 10/03/11 21:59 Bromomethane ug/L ND 2.0 10/03/11 21:59 Carbon tetrachloride ug/L ND 1.0 10/03/11 21:59 Chlorobenzene ug/L ND 1.0 10/03/11 21:59 Chloroethane ug/L ND 1.0 10/03/11 21:59 Chloroform ug/L ND 1.0 10/03/11 21:59 Chloromethane ug/L ND 1.0 10/03/11 21:59 cis-1,2-Dichloroethene ug/L ND 1.0 10/03/11 21:59 cis-1,3-Dichloropropene ug/L ND 1.0 10/03/11 21:59 Dibromochloromethane ug/L ND 1.0 10/03/11 21:59 Dibromomethane ug/L ND 1.0 10/03/11 21:59 Dichlorodifluoromethane ug/L ND 1.0 10/03/11 21:59 Diisopropyl ether ug/L ND 1.0 10/03/11 21:59 Ethylbenzene ug/L ND 1.0 10/03/11 21:59 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 77 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 METHOD BLANK: 667439 Matrix: Water Associated Lab Samples: 92103091013 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L 0.85J 1.0 10/03/11 21:59 m&p-Xylene ug/L ND 2.0 10/03/11 21:59 Methyl-tert-butyl ether ug/L ND 1.0 10/03/11 21:59 Methylene Chloride ug/L ND 2.0 10/03/11 21:59 Naphthalene ug/L ND 1.0 10/03/11 21:59 o-Xylene ug/L ND 1.0 10/03/11 21:59 p-Isopropyltoluene ug/L ND 1.0 10/03/11 21:59 Styrene ug/L ND 1.0 10/03/11 21:59 Tetrachloroethene ug/L ND 1.0 10/03/11 21:59 Toluene ug/L ND 1.0 10/03/11 21:59 trans- 1,2-Dichloroethene ug/L ND 1.0 10/03/11 21:59 trans- 1, 3-Dichloropropene ug/L ND 1.0 10/03/11 21:59 Trichloroethene ug/L ND 1.0 10/03/11 21:59 Trichlorofluoromethane ug/L ND 1.0 10/03/11 21:59 Vinyl acetate ug/L ND 2.0 10/03/11 21:59 Vinyl chloride ug/L ND 1.0 10/03/11 21:59 1,2-Dichloroethane-d4 (S) % ill 70-130 10/03/11 21:59 4-Bromofluorobenzene (S) % 96 70-130 10/03/11 21:59 Dibromofluoromethane (S) % 107 70-130 10/03/11 21:59 Tbluene-d8 (S) % 102 70-130 10/03/11 21:59 LABORATORY CONTROL SAMPLE: 667440 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.5 109 70-130 1,1,1-Trichloroethane ug/L 50 48.8 98 70-130 1,1,2,2-Tetrachloroethane ug/L 50 51.7 103 70-130 1,1,2-Trichloroethane ug/L 50 50.5 101 70-130 1,1-Dichloroethane ug/L 50 52.5 105 70-130 1,1-Dichloroethene ug/L 50 49.8 100 70-132 1,1-Dichloropropene ug/L 50 51.0 102 70-130 1,2,3-Trichlorobenzene ug/L 50 47.7 95 70-135 1,2,3-Trichloropropane ug/L 50 48.3 97 70-130 1,2,4-Trichlorobenzene ug/L 50 48.6 97 70-134 1,2-Dibromo-3-chloropropane ug/L 50 46.9 94 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.3 105 70-130 1,2-Dichlorobenzene ug/L 50 51.8 104 70-130 1,2-Dichloroethane ug/L 50 56.8 114 70-130 1,2-Dichloropropane ug/L 50 52.7 105 70-130 1,3-Dichlorobenzene ug/L 50 52.2 104 70-130 1,3-Dichloropropane ug/L 50 52.4 105 70-130 1,4-Dichlorobenzene ug/L 50 50.0 100 70-130 2,2-Dichloropropane ug/L 50 45.2 90 58-145 2-Butanone (MEK) ug/L 100 81.6 82 70-145 2-Chlorotoluene ug/L 50 51.2 102 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 78 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 LABORATORY CONTROL SAMPLE: Parameter 667440 Units Spike Conc. LCS Result 2-Hexanone ug/L 100 86.6 4-Chlorotoluene ug/L 50 52.4 4-Methyl-2-pentanone (MIBK) ug/L 100 94.6 Acetone ug/L 100 89.2 Benzene ug/L 50 51.8 Bromobenzene ug/L 50 51.3 Bromochloromethane ug/L 50 55.5 Bromodichloromethane ug/L 50 51.0 Bromoform ug/L 50 51.5 Bromomethane ug/L 50 48.5 Carbon tetrachloride ug/L 50 51.5 Chlorobenzene ug/L 50 52.3 Chloroethane ug/L 50 46.1 Chloroform ug/L 50 55.3 Chloromethane ug/L 50 56.4 cis-1,2-Dichloroethene ug/L 50 50.5 cis-1,3-Dichloropropene ug/L 50 54.3 Dibromochloromethane ug/L 50 51.7 Dibromomethane ug/L 50 51.0 Dichlorodifluoromethane ug/L 50 54.8 Diisopropyl ether ug/L 50 52.9 Ethylbenzene ug/L 50 50.4 Hexachloro-1,3-butadiene ug/L 50 44.4 m&p-Xylene ug/L 100 104 Methyl-tert-butyl ether ug/L 50 52.6 Methylene Chloride ug/L 50 59.6 Naphthalene ug/L 50 46.8 o-Xylene ug/L 50 53.6 p-Isopropyltoluene ug/L 50 53.6 Styrene ug/L 50 56.0 Tetrachloroethene ug/L 50 50.4 Toluene ug/L 50 50.7 trans- 1,2-Dichloroethene ug/L 50 51.0 trans- 1, 3-Dichloropropene ug/L 50 51.2 Trichloroethene ug/L 50 53.5 Trichlorofluoromethane ug/L 50 45.4 Vinyl acetate ug/L 100 97.7 Vinyl chloride ug/L 50 57.9 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Tbluene-d8 (S) % LCS % Rec % Rec Limits 87 70-144 105 70-130 95 70-140 89 50-175 104 70-130 103 70-130 ill 70-130 102 70-130 103 70-130 97 54-130 103 70-132 105 70-130 92 64-134 ill 70-130 113 64-130 101 70-131 109 70-130 103 70-130 102 70-131 110 56-130 106 70-130 101 70-130 89 70-130 104 70-130 105 70-130 119 63-130 94 70-138 107 70-130 107 70-130 112 70-130 101 70-130 101 70-130 102 70-130 102 70-132 107 70-130 91 62-133 98 66-157 116 69-130 103 70-130 100 70-130 100 70-130 98 70-130 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 79 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 667441 667442 IVIS MSD 92103433006 Spike Spike IVIS MSD IVIS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual M-Dichloroethene ug/L 1.4 50 50 52.8 60.6 103 118 70-166 14 30 Benzene ug/L ND 50 50 55.4 55.1 ill 110 70-148 1 30 Chlorobenzene ug/L ND 50 50 57.9 54.5 116 109 70-146 6 30 Toluene ug/L ND 50 50 58.1 57.3 116 115 70-155 1 30 Trichloroethene ug/L 140 50 50 198 199 116 117 69-151 0 30 1,2-Dichloroethane-d4 (S) % 101 105 70-130 4-Bromofluorobenzene (S) % 101 92 70-130 Dibromofluoromethane (S) % 84 93 70-130 Tbluene-d8 (S) % 96 99 70-130 Date: 10/05/2011 04:04 PM REPORT OF LABORATORY ANALYSIS Page 80 of 81 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103091 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference k MEMO ini 11111FIR1111151110 SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. 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"'5 ;� ;iz a. v) 0 P o rg 'W* cc w z 0 0 V) LL LU .0 W co 4 z CL E j CD C/) E 5 JOR -*4- 0 'o Vam A 0 (D co r 13 E 5 3 c co kv; F- pa-C I .2 w ow 0 L- = w cu CL E (1) -0 E c Me cr U) lz o 0 < I w a4o- # W311 1 "Ic4i "I q*j W) ol MXL i (N/A) joelul seldweS cq (N/,k) J91003 poleas L6 Apolsno T- rl: 0 > 2 (N/A) 801 o (N UO POA1939 0 00 ui dwo.L LL V im UJ 14 C6 cu 'a CD 0 0 c W) 0 0 & W- -= uj\ a LU .010 -i -i E CL IL co CO) %- %- 0 0 0 LU 0 E W z cu Z Z o Document Name: Sample Condition Upon Document Revised: July 20, 2011 Receipt (SCUR) Page 1 of 2 ..,R?acie Analytical' Document No.: Issuing Authorities: F-ASV-CS-003-rev.06 Pace Asheville Quality Office Client Name: L F Project Where Received: F'j Huntersville ZOA-0sheville 17 Eden 0. r%1X31V.1"-,, Courier: f! Fed Ex F-1 ups,7 us Gommercial7 Pace Other PX ClientO ��;l HNZ: a te'0_0 Custody Seal on Cooler/Box Present: yes ;a`�no Seals intact: yes 4- _�-n o R1 11-.11. NEER; IM 'N V@� Packing Material: 0--b-u�bb e Wrap 7,1,-R�ble Bags 0 None EJ Other Thermometer Used: n#2 -803440)31, Type of 1ce<9 Blue None 44---S�amp�l'es on ice, cooling process has begun Temp Correction Factorr: Add u trid'_ 0 .. -7 - C Corrected Cooler Temp.: C Biological Tissue is Frozen: Yes No N/A Date and Initials of erso xam7ing =e !Z6. contents: ..-,,oO -./ I Temp should be above freezing to 60C Comments: Chain of Custody Present: ;?Yre_s0No ON/A 1. Chain of Custody Filled Out: ;;-Ywe-s ONo ON/A 2. Chain of Custody Relinquished: �>Ts 0 No ON/A 3 Sampler Name & Signature on COC: 1e0o Os- E I No EIN/A 4. Samples Arrived within Hold Time: ,20'res 0 No ON/A 5. Short Hold Time Analysis (<72hr): DYes RTN0"o EIN/A 6. [Rush Turn Around Time Requested: DYesX0 ON/A 7. Sufficient Volume: oEnYes E3No ON/A 8. Correct Containers Used: es DNo ON/A 9. -Pace Containers Used: Yes DNo EIN/A Containers Intact: Yes FNo EIN/A 10. Filtered volume received for Dissolved tests DYes ElNo ZON�/A 11. Sample Labels match COC: /5Yes DNo ON/A 12. -includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. E]No D N/A 13. All containers needing preservation are found to be in ,,.�Yes compliance with EPA recommendation. . ;?1es El No El N/A 4 00"' exceptions X-0A)oI ifo rm, TOC, O&G, WI-DRO (water) DNo Initial when completed Samples checked for dechlorination: V��s E]Yes F�No �X/A 14. Headspace in VOA Vials (>6mm): F No _E1 N/A 15. Trip Blank Present: ___ZYes ,,,P<es ONo 1,_�<A 16. Trip Blank Custody Seals Present ?'Ies 0 No A race Trip Blank Lot # (if purchased): Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: Field Data Required? Y / N SCURF Review: D a t e: I qhco A/ I SRF Review: 94A) IDate: I I i Note: Whenever th s a discreepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DLEHNR Cetfic-lation Office 11 i.e out oil hold, incorrectpreseR/ative, out, of temp, incoirrect containers' 2w Document Name: Sample Condition Upon Revised: july 20, 2-101 1 Docum an L I eAnalW-ical Receipt (SCUR) Page 1 of 2 Document No.: Issuing Authorities: F-ASV-CS-003-rev.06 Pace Asheville Quality Of fice. J:Z Client Name: Project # IAJ epoe 49P%^C;"eA: ig I I TZ I V U L rl L O.Ai Courier: Fed Ex uPSL C1 p onall..-. USPX. ClientD Cornmercial.-LJ Pace Other e:- ate:` r9j::;`D D Custody Seal on Cooler/Box Present: yes no Seals intact: !7 y e s no P m e: Packing Material: c3tubble Wrap 0.,216-ble Bags None Other �4 Thermometer Used: J42(��n�#21.-803 403-1�. Type of Ice Blue None D-�55—m-61es on ice, cooling process has begun f U t a c Temp Correction Fa�c:tor-:- Add ubtra-c C 4t' Corrected Cooler Temp.: J C Biological Tissue is Frozen: Yes No N/A Date and Initial f ersory-exam /�ning contents:— X-7 Temp should be above freezing to 60C Comments: Chain of Custody Present: es n No R N/A 1 Chain of Custody Filled Out: P-Ye-s 0 No 0 N/A 2.- Chain of Custody Relinquished: DNo ON/A 3. Sampler Name & Signature on COC: -2�s 2!!�e� ONo ON/A 4. Samples Arrived within Hold Time: __,,�es ONo ON/A 5. Short Hold Time Analysis (<72hr): DYes i�o ON/A 6. Rush Turn Around Time Requested: 0YesX0 ON/A 7. Sufficient Volume: /4nYes DNo ON/A 8 Correct Containers Used: Xe s DNo ON/A 9. -Pace Containers Used: znly'es El No EIN/A Containers Intact: /ErY-es El No ON/A 10. Filtered volume received for Dissolved tests E]Yes . []No .0 'N/A 11. Sample Labels match COC: /E5Y"'es 0 No ON/A 12. -includes date;/time/ID/Analysis Matrix: J--00, All containers needing preservation have been checked. DNo 13 N/A 13. All containers needing preservation are found to be in compliance with EPA recommendation. )a<es" E]No ON/A exceptions/,<0A)oliform, TOC, O&G, WI-DRO (water) 1:1 DNo Initial when completed Samples checked for dechlorination: MYes.-[]No �WIA 14. Headspace in VOA Vials ( >6mm): 0-Y-'es E]No 10 N/A 15. Trip Blank Present: L�Kes C- El No KIA 16. Trip Blank Custody Seals Present 0 'S ONo Pace Trip Blank Lot # (if Client Notification/ Resolution: Field Data Required? Y N Person Contacted: D a e /T i me..: uommennts/ Resolutiolm. SCURF Reviewdl D- at e: SRF Review Dato: EHN' affer-ting Norlh -i�� '-Orrlp, ies, cor—o"thi ili be see-m 1�,D the, 1\10111h. Caroiina D- r N e.: there is a dis',-;:rep;ancN,, tiance qar*rp c is wil Ir -Ortain--rc' D, U. *, , -, i i i C, a I � I C C "t -L 0 U, 0; e .......... Document Name: Sample Condition Upon Document Revised.; July 213, 2011 3n c ceAna&tcal Receipt (SCUR) P age 1 of 2 Document No.: Issuing Authorities: F-ASV-CS-003-rev.06 Pace Asheville Quality Office Client Name: Pro;ect # Rekoci V Vu. L un' - rsv:! z-he- -:lie rl I LIC� ]Ile V I i Courier: L Fed Ex 1jPS USP C1 �'O Client,' r,,ommerci-ILJ Pace Other p lona, Proj..-DUe*:: Custody Seal on Cooler/Box Present: F-1 yes no Seals intact: i7 yes _,�o P r: N Packing Material: L�f'§ubble Wrap E],eilftle Bags None Other Thermometer Used: n#2 '-8 0 3 4 4 0 :�3, 4�0 Blue None [�� �am�les on ice, cooling process has begun Type of lcej u tr Temp Correction Factorr.: Add :ubtr C Corrected Cooler Temp.: C Biological Tissue is Frozen: Yes No N/A Date and Initial f ersoi)�,exam ing s eo, 7"v contents: W, Temp should be above freezing to 60C Comments: -4 Chain of Custody Present: 21'es EJNo EIN/A 1 Chain of Custody Filled Out: (,_��s 0 No 0 N/A 2. Chain of Custody Relinquished: py-G-S ONo 0 N/A 3 Sampler Name & Signature on COC: ;Xe_� DNo 0 N/A 4. Samples Arrived within Hold Time: es DNo 11 N/A 5. Short Hold Time Analysis (<72hr): DYes 0�0 0 N/A 6. Rush Turn Around Time Requested: 0YesX0 0 N/A 7, Sufficient Volume: ..,--flYes ONo ON/A Correct Containers Used: es E]No EIN/A 9. -Pace Containers Used: Yes 1_7lNo EIN/A Containers Intact: A!TYes ONo ON/A 10. Filtered volume received for Dissolved tests E]Yes FlNo Z `N/A 11. Sample Labels match COC: /?5Y'es 0 No El N/A 12. -Includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. 0 No El N/A 13. All containers needing preservation are found to be in compliance with EPA recommendation. )2<'s E]No EIN/A exrceptionsZ<A)oIiforrn, TOC, O&G, WI-DRO (water) IIXS DNo Initial when completed Samples Checked for dechlorination: E]Yes -[]No PK/A 14. Headspace in VOA Vials ( >6mm): XY" 'es F No .1E1 N/A 15. Trip Blank Present: Yes N o ss KIA 16. Trip Blank Custody Seals Present e 11:1 No Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Field Data Required? y N Person Contacted: D a te-. /T i rn e: Uomrneint's/ Resolutiom. SCURF Review:, �1 ED a L SRF Review: Datin: law I YAZ li be sew, 1- th,= N-r1h iina D-HNR isl.rewpmcy afieram -ia corritpiarticee, sarr 1. P i eS, ca c o Q t h TO' �'M VVi 1-0 N o 1 e: there:, Is a di g N c th Caro 'I i r L� V L i 'S I ;Ci;j- Cej- n. a -or-f-*nor-', e �'C: J I i C Q !.I e- nk e ".r tcl I i I - I Z' Cer'Lifi-lafir.)r Offi:'k-, Pr 1A ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27288 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (336)623-8921 October 10, 2011 Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 RE: Project: FORMERANDREX INDUSTRIES Pace Project No.: 92103092 (828)254-7176 Dear Mr. Alexander: Enclosed are the analytical results for sample(s) received by the laboratory on September 26, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures PIC, R�b REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (704)875-9092 Page 1 of 21 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 CERTIFICATIONS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Asheville Certification III)s 2225 Riverside Dr., Asheville, NC 28804 South Carolina Certification #: 99030001 Florida/NELAP Certification E87648 Virginia Certification #: 00072 Massachusetts Certification M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Virgina/VELAP Certification #: 460147 North Carolina Wastewater Certification #: 40 REPORT OF LABORATORY ANALYSIS Page 2 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ceAnalytical —pacelabsxom Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Project: Pace Project No.: Lab ID FORMER ANDREX INDUSTRIES 92103092 Sample ID Matrix Date Collected Date Received 92103092001 MW-5 Water 09/23/11 09:50 09/26/11 11:30 92103092002 MW-6 Water 09/23/11 18:40 09/26/11 11:30 92103092003 MW-7 Water 09/23/11 09:25 09/26/11 11:30 92103092004 MW-9 Water 09/23/11 14:35 09/26/11 11:30 92103092005 MW-10 Water 09/23/11 13:50 09/26/11 11:30 92103092006 MW-11 1 Water 09/23/11 13:05 09/26/11 11:30 92103092007 MW-12 Water 09/23/11 10:20 09/26/11 11:30 92103092008 MW-13 Water 09/22/11 15:00 09/26/11 11:30 92103092009 MW-14 Water 09/22/11 14:15 09/26/11 11:30 92103092010 RW-1 Water 09/23/11 18:05 09/26/11 11:30 92103092011 RW-3 Water 09/23/11 19:35 09/26/11 11:30 92103092012 RW-5 Water 09/23/11 17:20 09/26/11 11:30 92103092013 RW-6 Water 09/23/11 16:40 09/26/11 11:30 92103092014 RW-7 Water 09/23/11 15:50 09/26/11 11:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 21 ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Lab ID FORMER ANDREX INDUSTRIES 92103092 Sample ID Method Analysts Analytes Reported Laboratory 92103092001 MW-5 SM 5310B SAJ 1 PASI-A 92103092002 MW-6 SM 5310B SAJ 1 PASI-A 92103092003 MW-7 SM 5310B SAJ 1 PASI-A 92103092004 MW-9 SM 5310B SAJ 1 PASI-A 92103092005 MW-10 SM 5310B SAJ 1 PASI-A 92103092006 MW-11 SM 5310B SAJ 1 PASI-A 92103092007 MW-12 SM 5310B SAJ 1 PASI-A 92103092008 MW-13 SM 5310B SAJ 1 PASI-A 92103092009 MW-14 SM 5310B SAJ 1 PASI-A 92103092010 RW-1 SM 5310B SAJ 1 PASI-A 92103092011 RW-3 SM 5310B SAJ 1 PASI-A 92103092012 RW-5 SM 5310B SAJ 1 PASI-A 92103092013 RW-6 SM 5310B SAJ 1 PASI-A 92103092014 RW-7 SM 5310B SAJ 1 PASI-A REPORT OF LABORATORY ANALYSIS Page 4 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5 Labll): 92103092001 Collected: 09/23/11 09:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.9 mg/L 1.0 1.0 1 10/03/11 19:20 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 5 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 Labll): 92103092002 Collected: 09/23/11 18:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 17.8 mg/L 1.0 1.0 1 10/03/11 19:30 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 6 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 Labll): 92103092003 Collected: 09/23/11 09:25 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon ND mg/L 1.0 1.0 1 10/03/11 19:40 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 7 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Labll): 92103092004 Collected: 09/23/11 14:35 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 4.0 mg/L 1.0 1.0 1 10/03/11 19:50 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 8 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Sample: MW-10 Labll): 92103092005 Collected: 09/23/11 13:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 311 mg/L 10.0 10.0 10 10/06/11 15:35 7440-44-0 M6 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 9 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11 Labll): 92103092006 Collected: 09/23/11 13:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.6 mg/L 1.0 1.0 1 10/05/11 15:04 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 10 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-12 Labll): 92103092007 Collected: 09/23/11 10:20 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 329 mg/L 10.0 10.0 10 10/06/11 15:51 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 11 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-13 Labll): 92103092008 Collected: 09/22/11 15:00 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.1 mg/L 1.0 1.0 1 10/05/11 15:32 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 12 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 Labll): 92103092009 Collected: 09/22/11 14:15 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/05/11 15:42 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 13 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-1 Labll): 92103092010 Collected: 09/23/11 18:05 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 4590 mg/L 500 500 500 10/06/11 16:03 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 14 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-3 Labll): 92103092011 Collected: 09/23/11 19:35 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 138 mg/L 10.0 10.0 10 10/06/11 16:15 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 15 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-5 Labll): 92103092012 Collected: 09/23/11 17:20 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 462 mg/L 100 100 100 10/06/11 16:25 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 16 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 Labll): 92103092013 Collected: 09/23/11 16:40 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 4.5 mg/L 1.0 1.0 1 10/05/11 16:23 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 17 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Labll): 92103092014 Collected: 09/23/11 15:50 Received: 09/26/11 11:30 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3010 mg/L 100 100 100 10/06/11 16:42 7440-44-0 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 18 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 QC Batch: WETA/10645 Analysis Method: SM 531 OB QC Batch Method: SM 5310B Analysis Description: 531 OB TOC Associated Lab Samples: 92103092001,92103092002,92103092003,92103092004 METHOD BLANK: 666747 Matrix: Water Associated Lab Samples: 92103092001,92103092002,92103092003,92103092004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 10/03/11 14:48 LABORATORY CONTROL SAMPLE: 666748 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.9 99 90-110 MATRIX SPIKE SAMPLE: 666749 92103215001 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 2.9 25 26.7 95 75-125 MATRIX SPIKE SAMPLE: 666751 92103438001 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 3.2 25 26.5 93 75-125 SAMPLE DUPLICATE: 666750 92103215002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 35.8 36.1 1 20 SAMPLE DUPLICATE: 666752 92103438002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 13.4 13.2 2 20 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 19 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 QC Batch: WETA/10666 Analysis Method: SM 531 OB QC Batch Method: SM 5310B Analysis Description: 531 OB TOC Associated Lab Samples: 92103092005,92103092006,92103092007,92103092008,92103092009,92103092010,92103092011, 92103092012,92103092013,92103092014 METHOD BLANK: 667555 Matrix: Water Associated Lab Samples: 92103092005,92103092006,92103092007,92103092008,92103092009,92103092010,92103092011, 92103092012,92103092013,92103092014 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 10/05/11 14:17 LABORATORY CONTROL SAMPLE: 667556 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.1 96 90-110 MATRIX SPIKE SAMPLE: 667557 92103092005 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 311 25 312 4 75-125 M6 MATRIX SPIKE SAMPLE: 667559 92103330001 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 4.5 25 29.2 99 75-125 SAMPLE DUPLICATE: 667558 92103092006 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 3.6 3.5 3 20 SAMPLE DUPLICATE: 667560 92103330004 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 5.4 5.4 1 20 Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 20 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103092 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference k MEMO ini 11111FIR1111151110 SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES PASI-A Pace Analytical Services - Asheville ANALYTE QUALIFIERS M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. Date: 10/10/2011 03:21 PM REPORT OF LABORATORY ANALYSIS Page 21 of 21 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. E 0 E 0 cr E 0 C>U NEW z uj 0 LLJ D cc (A U I LL 0 .�5 w OD z �ze LU cl L L uj Im V z D 0 W L L Uj Z D L L IV— c VT 0 cu E L- cu 0 JOR z t5 a) c 8 -:07 0 (D ;p 2 -W cu CL 0 T 0 :, r_ 0 0 L: 0) 2 a. (L .2 0 0 c (D E -a cc s C > 0 C) < a. w w m CL 2 (L (D -C F- cc E 1.0- C; z L: 0 m a. 0 E E 0 m :3 C 0 0 cn z z 0 . I- m t t 5 0 >% r- a) a) tr CL CL 2 0 o :3 o- a. a. "d c x CE cu C4 U- V1 cc - —1 '�: 8 0 q:::r... JOR 0 (D V 0 e c cc cc a 0- 0=1 cr E ca cr 0 o E U) a, 10 uj C,� to 0 C� z T qo a. 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E Document Name: Sample Condition Upon Document Revised: uly 20, 2011 `0 Receipt (SCUR) Page 1 of 2 ;ai ceAnalyfical Document No.: Issuing Authorities: F-ASV-CS-003-rev.06 Pace Asheville Qualitv Office Client Name: OL-F Project# q2,10-3MZ" Where Received: F'j Huntersville_.... Asheville 17 Eden 'o Courier: F71 Fed Ex F� upsf—1 us lient[I CC; ercialF Pace Other P, VI 1911m C Rp a n �o Custody Seal on Cooler/Box Present: yes no Seals intact: yes o -me sy N*� a Packing Material: P--�ubble Wrap,',.',�1�6ubble Bags 0 NoneE] Other Type of lc%� Thermometer Used: >? Blue None -F�� �Samples on ice, cooling process has begun Temp Correction Factor: Add bg �tra 0,7 C Corrected Cooler Temp.: 2, !�j C Biological Tissue is Frozen: Yes No N/A Date and Initials of rson ami ing I P ;Z 7, ]::e contents: Temp should be above freezing to 6*C Comments: Chain of Custody Present: ,0res ONo EIN/A Chain of Custody Filled Out: �Kes 0 No ON/A 2. Chain of Custody Relinquished: Xes 0 No ON/A 3. Sampler Name & Signature on COC: E]Xs""'E]No EIN/A 4. Samples Arrived within Hold Time: g>ee"s� 0 N o El N/A 5 Short Hold Time Analysis (<72hr): DYes ;Ko' El N/A 6. Rush Turn Around Time Requested: DYes P<O 1:1 N/A 7 Sufficient Volume: s 0 No ON/A 8. Correct Containers Used: /ElY"'es DNo ON/A 9. -Pace Containers Used: DNo EIN/A Containers Intact: F<es ONo 1771 N/A 10. Filtered volume received for Dissolved tests DYes E]No .o�NIA 11. Sample Labels match COC: e"-�OYes DNo EIN/A 12. -includes date/time/ID/Analysis Matrix: k.- All containers needing preservation have been checked. ;,Yps E]No ON/A 13. All containers needing preservation are found to be in compliance EPA ��es E]No EIN/A with recommendation. 000*�&G, WI-DRO (water) exceptions: VOA, colifory,-4TOC, DYes Initial when completed Samples checked for dechlorination: ElYes E]No PK/A 14. Headspace in VOA Vials (>6mm): Xes 0 No ON/A 15. Trip Blank Present: DYes E]No -'�N/A. 16. Trip ElNo 41 �N/A Blank Custody Seals Present DYes Pace Trip Blank Lot # (if purchased): Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: Field Data Required? Y / N IA-1 CAO SCURF Review: I Date: SRF Review: I L�?gff I 113ate: [�Iocpht I Note: Whenever thbis a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Off ice i.e out of hold, inf--.o!,,rel-.+L;Dr.�nserva't"ive, out oftemp, incorrect containers ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27288 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (336)623-8921 October 10, 2011 Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 RE: Project: FORMERANDREX INDUSTRIES Pace Project No.: 92103334 (828)254-7176 Dear Mr. Alexander: Enclosed are the analytical results for sample(s) received by the laboratory on September 29, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures PIC, R�b REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (704)875-9092 Page 1 of 39 Pace Analytical Services, Inc. Pace Analytical Services, Inc. acmnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.p,?celabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: FORMERANDREX INDUSTRIES Pace Project No.: 92103334 Charlotte Certification III)s 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. M 99006003 Virginia Drinking Water Certification #: 00213 Connecticut Certification#: PH-01 04 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DHH Drinking Water # LA 100031 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460144 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 39 ceAnalytical —pacelabsxom Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Project: Pace Project No.: Lab ID FORMER ANDREX INDUSTRIES 92103334 Sample ID Matrix Date Collected Date Received 92103334001 SM-1 Water 09/28/11 10:30 09/29/11 08:22 92103334002 SM-2 Water 09/28/11 10:25 09/29/11 08:22 92103334003 SM-3 Water 09/28/11 10:20 09/29/11 08:22 92103334004 SM-4 Water 09/28/11 10:10 09/29/11 08:22 92103334005 SM-5 Water 09/28/11 10:05 09/29/11 08:22 92103334006 SM-6 Water 09/28/11 09:55 09/29/11 08:22 92103334007 JW-1 Water 09/28/11 10:45 09/29/11 08:22 92103334008 CS-11 Water 09/28/11 12:35 09/29/11 08:22 92103334009 CS-2 Water 09/28/11 12:25 09/29/11 08:22 92103334010 BC-1 Water 09/28/11 13:30 09/29/11 08:22 92103334011 BC-2 Water 09/28/11 13:20 09/29/11 08:22 92103334012 BC-3 Water 09/28/11 13:10 09/29/11 08:22 92103334013 BC-4 Water 09/28/11 13:00 09/29/11 08:22 92103334014 BC-5 Water 09/28/11 12:50 09/29/11 08:22 92103334015 TRIP BLANK Water 09/28/11 00:00 09/29/11 08:22 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 39 ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Lab ID FORMER ANDREX INDUSTRIES 92103334 Sample ID Method Analysts Analytes Reported Laboratory 92103334001 SM-1 EPA 8260 MCK 63 PASI-C 92103334002 SM-2 EPA 8260 MCK 63 PASI-C 92103334003 SM-3 EPA 8260 MCK 63 PASI-C 92103334004 SM-4 EPA 8260 MCK 63 PASI-C 92103334005 SM-5 EPA 8260 MCK 63 PASI-C 92103334006 SM-6 EPA 8260 MCK 63 PASI-C 92103334007 JW-11 EPA 8260 MCK 63 PASI-C 92103334008 CS-11 EPA 8260 MCK 63 PASI-C 92103334009 CS-2 EPA 8260 MCK 63 PASI-C 92103334010 BC-1 EPA 8260 MCK 63 PASI-C 92103334011 BC-2 EPA 8260 MCK 63 PASI-C 92103334012 BC-3 EPA 8260 MCK 63 PASI-C 92103334013 BC-4 EPA 8260 MCK 63 PASI-C 92103334014 BC-5 EPA 8260 MCK 63 PASI-C 92103334015 TRIP BLANK EPA 8260 MCK 63 PASI-C REPORT OF LABORATORY ANALYSIS Page 4 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-1 Labll): 92103334001 Collected: 09/28/11 10:30 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 00:55 67-64-1 3.9 ug/L 1.0 0.25 1 10/06/11 00:55 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 00:55 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 00:55 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 00:55 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 00:55 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 00:55 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 00:55 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 00:55 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 00:55 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 00:55 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 00:55 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 00:55 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 00:55 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 00:55 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 00:55 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 00:55 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 00:55 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 00:55 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 00:55 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 00:55 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 00:55 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 00:55 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 00:55 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 00:55 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 00:55 75-35-4 ND ug/L 1.0 0.19 1 10/06/11 00:55 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 00:55 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 00:55 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 00:55 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 00:55 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 00:55 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 00:55 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 00:55 10061-02-6 0.41J ug/L 1.0 0.12 1 10/06/11 00:55 108-20-3 0.42J ug/L 1.0 0.30 1 10/06/11 00:55 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 00:55 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 00:55 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 00:55 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 00:55 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 00:55 108-10-1 27.7 ug/L 1.0 0.21 1 10/06/11 00:55 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 00:55 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 00:55 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 00:55 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 00:55 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 5 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-1 Labll): 92103334001 Collected: 09/28/11 10:30 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 10/06/11 00:55 127-18-4 Toluene 1.9 ug/L 1.0 0.26 1 10/06/11 00:55 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 00:55 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 00:55 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 00:55 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 00:55 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 00:55 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 00:55 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 00:55 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 00:55 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 00:55 75-01-4 m&p-Xylene 0.88J ug/L 2.0 0.66 1 10/06/11 00:55 179601-23-1 o-Xylene 0.51J ug/L 1.0 0.23 1 10/06/11 00:55 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 1 10/06/11 00:55 460-00-4 Dibromofluoromethane (S) 88 % 70-130 1 10/06/11 00:55 1868-53-7 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 10/06/11 00:55 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 10/06/11 00:55 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 6 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-2 Labll): 92103334002 Collected: 09/28/11 10:25 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 01:19 67-64-1 1.3 ug/L 1.0 0.25 1 10/06/11 01:19 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 01:19 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 01:19 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 01:19 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 01:19 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 01:19 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 01:19 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 01:19 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 01:19 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 01:19 75-00-3 0.31J ug/L 1.0 0.14 1 10/06/11 01:19 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 01:19 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 01:19 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 01:19 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 01:19 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 01:19 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 01:19 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 01:19 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 01:19 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 01:19 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 01:19 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 01:19 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 01:19 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 01:19 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 01:19 75-35-4 ND ug/L 1.0 0.19 1 10/06/11 01:19 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 01:19 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 01:19 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 01:19 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 01:19 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 01:19 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 01:19 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 01:19 10061-02-6 0.35J ug/L 1.0 0.12 1 10/06/11 01:19 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 01:19 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 01:19 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 01:19 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 01:19 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 01:19 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 01:19 108-10-1 25.2 ug/L 1.0 0.21 1 10/06/11 01:19 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 01:19 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 01:19 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 01:19 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 01:19 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 7 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-2 Labll): 92103334002 Collected: 09/28/11 10:25 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.68J ug/L 1.0 0.46 1 10/06/11 01:19 127-18-4 Toluene 0.60J ug/L 1.0 0.26 1 10/06/11 01:19 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 01:19 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 01:19 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 01:19 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 01:19 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 01:19 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 01:19 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 01:19 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 01:19 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 01:19 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 01:19 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 01:19 95-47-6 4-Bromofluorobenzene (S) 100 % 70-130 1 10/06/11 01:19 460-00-4 Dibromofluoromethane (S) 98 % 70-130 1 10/06/11 01:19 1868-53-7 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 10/06/11 01:19 17060-07-0 Tbluene-d8 (S) 110 % 70-130 1 10/06/11 01:19 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 8 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-3 Labll): 92103334003 Collected: 09/28/11 10:20 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 01:44 67-64-1 0.85J ug/L 1.0 0.25 1 10/06/11 01:44 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 01:44 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 01:44 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 01:44 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 01:44 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 01:44 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 01:44 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 01:44 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 01:44 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 01:44 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 01:44 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 01:44 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 01:44 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 01:44 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 01:44 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 01:44 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 01:44 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 01:44 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 01:44 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 01:44 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 01:44 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 01:44 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 01:44 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 01:44 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 01:44 75-35-4 ND ug/L 1.0 0.19 1 10/06/11 01:44 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 01:44 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 01:44 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 01:44 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 01:44 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 01:44 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 01:44 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 01:44 10061-02-6 0.33J ug/L 1.0 0.12 1 10/06/11 01:44 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 01:44 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 01:44 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 01:44 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 01:44 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 01:44 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 01:44 108-10-1 21.6 ug/L 1.0 0.21 1 10/06/11 01:44 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 01:44 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 01:44 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 01:44 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 01:44 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 9 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-3 Labll): 92103334003 Collected: 09/28/11 10:20 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.61J ug/L 1.0 0.46 1 10/06/11 01:44 127-18-4 Toluene 0.39J ug/L 1.0 0.26 1 10/06/11 01:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 01:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 01:44 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 01:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 01:44 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 01:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 01:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 01:44 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 01:44 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 01:44 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 01:44 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 01:44 95-47-6 4-Bromofluorobenzene (S) 97 % 70-130 1 10/06/11 01:44 460-00-4 Dibromofluoromethane (S) 89 % 70-130 1 10/06/11 01:44 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 10/06/11 01:44 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 10/06/11 01:44 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 10 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-4 Labll): 92103334004 Collected: 09/28/11 10:10 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 02:08 67-64-1 0.35J ug/L 1.0 0.25 1 10/06/11 02:08 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 02:08 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 02:08 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 02:08 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 02:08 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 02:08 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 02:08 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 02:08 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 02:08 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 02:08 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 02:08 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 02:08 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 02:08 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 02:08 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 02:08 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 02:08 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 02:08 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 02:08 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 02:08 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 02:08 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 02:08 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 02:08 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 02:08 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 02:08 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 02:08 75-35-4 0.58J ug/L 1.0 0.19 1 10/06/11 02:08 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 02:08 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 02:08 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 02:08 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 02:08 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 02:08 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 02:08 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 02:08 10061-02-6 0.22J ug/L 1.0 0.12 1 10/06/11 02:08 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 02:08 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 02:08 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 02:08 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 02:08 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 02:08 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 02:08 108-10-1 15.5 ug/L 1.0 0.21 1 10/06/11 02:08 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 02:08 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 02:08 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 02:08 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 02:08 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 11 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-4 Labll): 92103334004 Collected: 09/28/11 10:10 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 2.1 ug/L 1.0 0.46 1 10/06/11 02:08 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 02:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 02:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 02:08 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 02:08 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 02:08 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 02:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 02:08 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 02:08 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 02:08 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 02:08 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 02:08 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 02:08 95-47-6 4-Bromofluorobenzene (S) 97 % 70-130 1 10/06/11 02:08 460-00-4 Dibromofluoromethane (S) 81 % 70-130 1 10/06/11 02:08 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 10/06/11 02:08 17060-07-0 Tbluene-d8 (S) 104 % 70-130 1 10/06/11 02:08 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 12 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-5 Labll): 92103334005 Collected: 09/28/11 10:05 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 02:32 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 02:32 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 02:32 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 02:32 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 02:32 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 02:32 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 02:32 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 02:32 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 02:32 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 02:32 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 02:32 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 02:32 67-66-3 0.31J ug/L 1.0 0.11 1 10/06/11 02:32 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 02:32 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 02:32 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 02:32 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 02:32 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 02:32 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 02:32 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 02:32 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 02:32 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 02:32 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 02:32 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 02:32 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 02:32 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 02:32 75-35-4 0.39J ug/L 1.0 0.19 1 10/06/11 02:32 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 02:32 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 02:32 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 02:32 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 02:32 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 02:32 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 02:32 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 02:32 10061-02-6 0.19J ug/L 1.0 0.12 1 10/06/11 02:32 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 02:32 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 02:32 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 02:32 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 02:32 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 02:32 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 02:32 108-10-1 12.3 ug/L 1.0 0.21 1 10/06/11 02:32 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 02:32 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 02:32 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 02:32 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 02:32 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 13 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-5 Labll): 92103334005 Collected: 09/28/11 10:05 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.7 ug/L 1.0 0.46 1 10/06/11 02:32 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 02:32 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 02:32 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 02:32 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 02:32 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 02:32 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 02:32 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 02:32 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 02:32 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 02:32 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 02:32 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 02:32 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 02:32 95-47-6 4-Bromofluorobenzene (S) 95 % 70-130 1 10/06/11 02:32 460-00-4 Dibromofluoromethane (S) 91 % 70-130 1 10/06/11 02:32 1868-53-7 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 10/06/11 02:32 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 10/06/11 02:32 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 14 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-6 Labll): 92103334006 Collected: 09/28/11 09:55 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 02:56 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 02:56 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 02:56 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 02:56 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 02:56 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 02:56 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 02:56 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 02:56 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 02:56 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 02:56 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 02:56 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 02:56 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 02:56 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 02:56 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 02:56 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 02:56 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 02:56 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 02:56 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 02:56 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 02:56 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 02:56 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 02:56 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 02:56 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 02:56 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 02:56 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 02:56 75-35-4 0.24J ug/L 1.0 0.19 1 10/06/11 02:56 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 02:56 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 02:56 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 02:56 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 02:56 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 02:56 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 02:56 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 02:56 10061-02-6 0.16J ug/L 1.0 0.12 1 10/06/11 02:56 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 02:56 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 02:56 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 02:56 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 02:56 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 02:56 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 02:56 108-10-1 9.9 ug/L 1.0 0.21 1 10/06/11 02:56 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 02:56 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 02:56 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 02:56 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 02:56 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 15 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-6 Labll): 92103334006 Collected: 09/28/11 09:55 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 1.3 ug/L 1.0 0.46 1 10/06/11 02:56 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 02:56 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 02:56 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 02:56 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 02:56 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 02:56 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 02:56 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 02:56 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 02:56 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 02:56 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 02:56 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 02:56 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 02:56 95-47-6 4-Bromofluorobenzene (S) 96 % 70-130 1 10/06/11 02:56 460-00-4 Dibromofluoromethane (S) 82 % 70-130 1 10/06/11 02:56 1868-53-7 1,2-Dichloroethane-d4 (S) 103 % 70-130 1 10/06/11 02:56 17060-07-0 Tbluene-d8 (S) 108 % 70-130 1 10/06/11 02:56 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 16 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: JW-11 Labll): 92103334007 Collected: 09/28/11 10:45 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 03:21 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 03:21 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 03:21 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 03:21 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 03:21 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 03:21 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 03:21 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 03:21 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 03:21 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 03:21 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 03:21 75-00-3 0.41J ug/L 1.0 0.14 1 10/06/11 03:21 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 03:21 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 03:21 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 03:21 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 03:21 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 03:21 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 03:21 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 03:21 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 03:21 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 03:21 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 03:21 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 03:21 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 03:21 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 03:21 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 03:21 75-35-4 3.7 ug/L 1.0 0.19 1 10/06/11 03:21 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 03:21 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 03:21 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 03:21 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 03:21 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 03:21 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 03:21 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 03:21 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 03:21 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 03:21 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 03:21 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 03:21 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 03:21 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 03:21 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 03:21 108-10-1 ND ug/L 1.0 0.21 1 10/06/11 03:21 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 03:21 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 03:21 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 03:21 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 03:21 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 17 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: JW-11 Labll): 92103334007 Collected: 09/28/11 10:45 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 17.2 ug/L 1.0 0.46 1 10/06/11 03:21 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 03:21 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 03:21 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 03:21 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 03:21 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 03:21 79-00-5 Trichloroethene 2.1 ug/L 1.0 0.47 1 10/06/11 03:21 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 03:21 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 03:21 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 03:21 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 03:21 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 03:21 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 03:21 95-47-6 4-Bromofluorobenzene (S) 100 % 70-130 1 10/06/11 03:21 460-00-4 Dibromofluoromethane (S) 94 % 70-130 1 10/06/11 03:21 1868-53-7 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 10/06/11 03:21 17060-07-0 Tbluene-d8 (S) 97 % 70-130 1 10/06/11 03:21 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 18 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 Labll): 92103334008 Collected: 09/28/11 12:35 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 03:45 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 03:45 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 03:45 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 03:45 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 03:45 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 03:45 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 03:45 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 03:45 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 03:45 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 03:45 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 03:45 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 03:45 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 03:45 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 03:45 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 03:45 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 03:45 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 03:45 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 03:45 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 03:45 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 03:45 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 03:45 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 03:45 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 03:45 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 03:45 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 03:45 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 03:45 75-35-4 3.3 ug/L 1.0 0.19 1 10/06/11 03:45 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 03:45 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 03:45 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 03:45 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 03:45 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 03:45 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 03:45 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 03:45 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 03:45 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 03:45 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 03:45 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 03:45 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 03:45 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 03:45 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 03:45 108-10-1 ND ug/L 1.0 0.21 1 10/06/11 03:45 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 03:45 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 03:45 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 03:45 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 03:45 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 19 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 Labll): 92103334008 Collected: 09/28/11 12:35 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 17.5 ug/L 1.0 0.46 1 10/06/11 03:45 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 03:45 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 03:45 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 03:45 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 03:45 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 03:45 79-00-5 Trichloroethene 1.6 ug/L 1.0 0.47 1 10/06/11 03:45 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 03:45 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 03:45 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 03:45 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 03:45 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 03:45 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 03:45 95-47-6 4-Bromofluorobenzene (S) 94 % 70-130 1 10/06/11 03:45 460-00-4 Dibromofluoromethane (S) 105 % 70-130 1 10/06/11 03:45 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 1 10/06/11 03:45 17060-07-0 Tbluene-d8 (S) 101 % 70-130 1 10/06/11 03:45 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 20 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 Labll): 92103334009 Collected: 09/28/11 12:25 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 04:09 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 04:09 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 04:09 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 04:09 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 04:09 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 04:09 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 04:09 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 04:09 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 04:09 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 04:09 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 04:09 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 04:09 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 04:09 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 04:09 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 04:09 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 04:09 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 04:09 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 04:09 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 04:09 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 04:09 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 04:09 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 04:09 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 04:09 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 04:09 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 04:09 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 04:09 75-35-4 0.81J ug/L 1.0 0.19 1 10/06/11 04:09 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 04:09 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 04:09 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 04:09 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 04:09 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 04:09 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 04:09 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 04:09 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 04:09 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 04:09 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 04:09 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 04:09 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 04:09 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 04:09 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 04:09 108-10-1 ND ug/L 1.0 0.21 1 10/06/11 04:09 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 04:09 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 04:09 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 04:09 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 04:09 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 21 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 Labll): 92103334009 Collected: 09/28/11 12:25 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 7.3 ug/L 1.0 0.46 1 10/06/11 04:09 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 04:09 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 04:09 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 04:09 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 04:09 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 04:09 79-00-5 Trichloroethene 0.84J ug/L 1.0 0.47 1 10/06/11 04:09 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 04:09 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 04:09 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 04:09 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 04:09 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 04:09 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 04:09 95-47-6 4-Bromofluorobenzene (S) 97 % 70-130 1 10/06/11 04:09 460-00-4 Dibromofluoromethane (S) 103 % 70-130 1 10/06/11 04:09 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 70-130 1 10/06/11 04:09 17060-07-0 Tbluene-d8 (S) 104 % 70-130 1 10/06/11 04:09 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 22 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-1 Labll): 92103334010 Collected: 09/28/11 13:30 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 04:33 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 04:33 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 04:33 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 04:33 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 04:33 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 04:33 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 04:33 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 04:33 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 04:33 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 04:33 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 04:33 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 04:33 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 04:33 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 04:33 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 04:33 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 04:33 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 04:33 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 04:33 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 04:33 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 04:33 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 04:33 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 04:33 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 04:33 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 04:33 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 04:33 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 04:33 75-35-4 2.0 ug/L 1.0 0.19 1 10/06/11 04:33 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 04:33 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 04:33 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 04:33 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 04:33 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 04:33 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 04:33 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 04:33 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 04:33 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 04:33 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 04:33 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 04:33 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 04:33 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 04:33 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 04:33 108-10-1 0.81J ug/L 1.0 0.21 1 10/06/11 04:33 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 04:33 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 04:33 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 04:33 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 04:33 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 23 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-1 Labll): 92103334010 Collected: 09/28/11 13:30 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 3.4 ug/L 1.0 0.46 1 10/06/11 04:33 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 04:33 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 04:33 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 04:33 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 04:33 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 04:33 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 04:33 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 04:33 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 04:33 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 04:33 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 04:33 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 04:33 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 04:33 95-47-6 4-Bromofluorobenzene (S) 99 % 70-130 1 10/06/11 04:33 460-00-4 Dibromofluoromethane (S) 102 % 70-130 1 10/06/11 04:33 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 70-130 1 10/06/11 04:33 17060-07-0 Tbluene-d8 (S) 109 % 70-130 1 10/06/11 04:33 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 24 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-2 Labll): 92103334011 Collected: 09/28/11 13:20 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 04:58 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 04:58 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 04:58 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 04:58 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 04:58 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 04:58 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 04:58 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 04:58 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 04:58 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 04:58 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 04:58 75-00-3 0.95J ug/L 1.0 0.14 1 10/06/11 04:58 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 04:58 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 04:58 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 04:58 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 04:58 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 04:58 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 04:58 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 04:58 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 04:58 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 04:58 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 04:58 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 04:58 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 04:58 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 04:58 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 04:58 75-35-4 6.4 ug/L 1.0 0.19 1 10/06/11 04:58 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 04:58 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 04:58 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 04:58 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 04:58 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 04:58 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 04:58 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 04:58 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 04:58 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 04:58 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 04:58 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 04:58 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 04:58 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 04:58 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 04:58 108-10-1 ND ug/L 1.0 0.21 1 10/06/11 04:58 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 04:58 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 04:58 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 04:58 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 04:58 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 25 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-2 Labll): 92103334011 Collected: 09/28/11 13:20 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 14.3 ug/L 1.0 0.46 1 10/06/11 04:58 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 04:58 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 04:58 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 04:58 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 04:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 04:58 79-00-5 Trichloroethene 2.1 ug/L 1.0 0.47 1 10/06/11 04:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 04:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 04:58 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 04:58 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 04:58 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 04:58 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 04:58 95-47-6 4-Bromofluorobenzene (S) 99 % 70-130 1 10/06/11 04:58 460-00-4 Dibromofluoromethane (S) 109 % 70-130 1 10/06/11 04:58 1868-53-7 1,2-Dichloroethane-d4 (S) 113 % 70-130 1 10/06/11 04:58 17060-07-0 Tbluene-d8 (S) 110 % 70-130 1 10/06/11 04:58 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 26 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-3 Labll): 92103334012 Collected: 09/28/11 13:10 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 05:22 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 05:22 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 05:22 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 05:22 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 05:22 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 05:22 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 05:22 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 05:22 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 05:22 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 05:22 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 05:22 75-00-3 1.6 ug/L 1.0 0.14 1 10/06/11 05:22 67-66-3 0.43J ug/L 1.0 0.11 1 10/06/11 05:22 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 05:22 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 05:22 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 05:22 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 05:22 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 05:22 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 05:22 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 05:22 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 05:22 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 05:22 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 05:22 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 05:22 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 05:22 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 05:22 75-35-4 5.2 ug/L 1.0 0.19 1 10/06/11 05:22 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 05:22 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 05:22 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 05:22 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 05:22 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 05:22 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 05:22 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 05:22 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 05:22 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 05:22 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 05:22 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 05:22 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 05:22 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 05:22 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 05:22 108-10-1 ND ug/L 1.0 0.21 1 10/06/11 05:22 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 05:22 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 05:22 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 05:22 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 05:22 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 27 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-3 Labll): 92103334012 Collected: 09/28/11 13:10 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 6.8 ug/L 1.0 0.46 1 10/06/11 05:22 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 05:22 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 05:22 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 05:22 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 05:22 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 05:22 79-00-5 Trichloroethene 1.5 ug/L 1.0 0.47 1 10/06/11 05:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 05:22 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 05:22 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 05:22 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 05:22 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 05:22 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 05:22 95-47-6 4-Bromofluorobenzene (S) 94 % 70-130 1 10/06/11 05:22 460-00-4 Dibromofluoromethane (S) 106 % 70-130 1 10/06/11 05:22 1868-53-7 1,2-Dichloroethane-d4 (S) 110 % 70-130 1 10/06/11 05:22 17060-07-0 Tbluene-d8 (S) 106 % 70-130 1 10/06/11 05:22 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 28 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-4 Labll): 92103334013 Collected: 09/28/11 13:00 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 05:46 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 05:46 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 05:46 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 05:46 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 05:46 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 05:46 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 05:46 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 05:46 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 05:46 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 05:46 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 05:46 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 05:46 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 05:46 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 05:46 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 05:46 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 05:46 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 05:46 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 05:46 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 05:46 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 05:46 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 05:46 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 05:46 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 05:46 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 05:46 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 05:46 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 05:46 75-35-4 ND ug/L 1.0 0.19 1 10/06/11 05:46 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 05:46 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 05:46 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 05:46 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 05:46 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 05:46 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 05:46 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 05:46 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 05:46 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 05:46 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 05:46 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 05:46 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 05:46 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 05:46 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 05:46 108-10-1 ND ug/L 1.0 0.21 1 10/06/11 05:46 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 05:46 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 05:46 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 05:46 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 05:46 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 29 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-4 Labll): 92103334013 Collected: 09/28/11 13:00 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 10/06/11 05:46 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 05:46 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 05:46 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 05:46 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 05:46 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 05:46 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 05:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 05:46 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 05:46 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 05:46 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 05:46 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 05:46 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 05:46 95-47-6 4-Bromofluorobenzene (S) 94 % 70-130 1 10/06/11 05:46 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1 10/06/11 05:46 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 70-130 1 10/06/11 05:46 17060-07-0 Tbluene-d8 (S) 104 % 70-130 1 10/06/11 05:46 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 30 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-5 Labll): 92103334014 Collected: 09/28/11 12:50 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/06/11 06:10 67-64-1 ND ug/L 1.0 0.25 1 10/06/11 06:10 71-43-2 ND ug/L 1.0 0.30 1 10/06/11 06:10 108-86-1 ND ug/L 1.0 0.17 1 10/06/11 06:10 74-97-5 ND ug/L 1.0 0.18 1 10/06/11 06:10 75-27-4 ND ug/L 1.0 0.26 1 10/06/11 06:10 75-25-2 ND ug/L 2.0 0.29 1 10/06/11 06:10 74-83-9 ND ug/L 5.0 0.96 1 10/06/11 06:10 78-93-3 ND ug/L 1.0 0.25 1 10/06/11 06:10 56-23-5 ND ug/L 1.0 0.23 1 10/06/11 06:10 108-90-7 ND ug/L 1.0 0.54 1 10/06/11 06:10 75-00-3 ND ug/L 1.0 0.14 1 10/06/11 06:10 67-66-3 ND ug/L 1.0 0.11 1 10/06/11 06:10 74-87-3 ND ug/L 1.0 0.35 1 10/06/11 06:10 95-49-8 ND ug/L 1.0 0.31 1 10/06/11 06:10 106-43-4 ND ug/L 5.0 2.5 1 10/06/11 06:10 96-12-8 ND ug/L 1.0 0.21 1 10/06/11 06:10 124-48-1 ND ug/L 1.0 0.27 1 10/06/11 06:10 106-93-4 ND ug/L 1.0 0.21 1 10/06/11 06:10 74-95-3 ND ug/L 1.0 0.30 1 10/06/11 06:10 95-50-1 ND ug/L 1.0 0.24 1 10/06/11 06:10 541-73-1 ND ug/L 1.0 0.33 1 10/06/11 06:10 106-46-7 ND ug/L 1.0 0.21 1 10/06/11 06:10 75-71-8 ND ug/L 1.0 0.32 1 10/06/11 06:10 75-34-3 ND ug/L 1.0 0.12 1 10/06/11 06:10 107-06-2 ND ug/L 1.0 0.56 1 10/06/11 06:10 75-35-4 ND ug/L 1.0 0.19 1 10/06/11 06:10 156-59-2 ND ug/L 1.0 0.49 1 10/06/11 06:10 156-60-5 ND ug/L 1.0 0.27 1 10/06/11 06:10 78-87-5 ND ug/L 1.0 0.28 1 10/06/11 06:10 142-28-9 ND ug/L 1.0 0.13 1 10/06/11 06:10 594-20-7 ND ug/L 1.0 0.49 1 10/06/11 06:10 563-58-6 ND ug/L 1.0 0.13 1 10/06/11 06:10 10061-01-5 ND ug/L 1.0 0.26 1 10/06/11 06:10 10061-02-6 ND ug/L 1.0 0.12 1 10/06/11 06:10 108-20-3 ND ug/L 1.0 0.30 1 10/06/11 06:10 100-41-4 ND ug/L 1.0 0.71 1 10/06/11 06:10 87-68-3 ND ug/L 5.0 0.46 1 10/06/11 06:10 591-78-6 ND ug/L 1.0 0.31 1 10/06/11 06:10 99-87-6 ND ug/L 2.0 0.97 1 10/06/11 06:10 75-09-2 ND ug/L 5.0 0.33 1 10/06/11 06:10 108-10-1 ND ug/L 1.0 0.21 1 10/06/11 06:10 1634-04-4 ND ug/L 1.0 0.24 1 10/06/11 06:10 91-20-3 ND ug/L 1.0 0.26 1 10/06/11 06:10 100-42-5 ND ug/L 1.0 0.33 1 10/06/11 06:10 630-20-6 ND ug/L 1.0 0.40 1 10/06/11 06:10 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 31 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-5 Labll): 92103334014 Collected: 09/28/11 12:50 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene 0.58J ug/L 1.0 0.46 1 10/06/11 06:10 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/06/11 06:10 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/06/11 06:10 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/06/11 06:10 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/06/11 06:10 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/06/11 06:10 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/06/11 06:10 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/06/11 06:10 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/06/11 06:10 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/06/11 06:10 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/06/11 06:10 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/06/11 06:10 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/06/11 06:10 95-47-6 4-Bromofluorobenzene (S) 95 % 70-130 1 10/06/11 06:10 460-00-4 Dibromofluoromethane (S) 108 % 70-130 1 10/06/11 06:10 1868-53-7 1,2-Dichloroethane-d4 (S) 114 % 70-130 1 10/06/11 06:10 17060-07-0 Tbluene-d8 (S) 103 % 70-130 1 10/06/11 06:10 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 32 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK Labll): 92103334015 Collected: 09/28/11 00:00 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans- 1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (M113K) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Analytical Method: EPA 8260 ND ug/L 25.0 2.2 1 10/05/11 22:54 67-64-1 ND ug/L 1.0 0.25 1 10/05/11 22:54 71-43-2 ND ug/L 1.0 0.30 1 10/05/11 22:54 108-86-1 ND ug/L 1.0 0.17 1 10/05/11 22:54 74-97-5 ND ug/L 1.0 0.18 1 10/05/11 22:54 75-27-4 ND ug/L 1.0 0.26 1 10/05/11 22:54 75-25-2 ND ug/L 2.0 0.29 1 10/05/11 22:54 74-83-9 ND ug/L 5.0 0.96 1 10/05/11 22:54 78-93-3 ND ug/L 1.0 0.25 1 10/05/11 22:54 56-23-5 ND ug/L 1.0 0.23 1 10/05/11 22:54 108-90-7 ND ug/L 1.0 0.54 1 10/05/11 22:54 75-00-3 ND ug/L 1.0 0.14 1 10/05/11 22:54 67-66-3 ND ug/L 1.0 0.11 1 10/05/11 22:54 74-87-3 ND ug/L 1.0 0.35 1 10/05/11 22:54 95-49-8 ND ug/L 1.0 0.31 1 10/05/11 22:54 106-43-4 ND ug/L 5.0 2.5 1 10/05/11 22:54 96-12-8 ND ug/L 1.0 0.21 1 10/05/11 22:54 124-48-1 ND ug/L 1.0 0.27 1 10/05/11 22:54 106-93-4 ND ug/L 1.0 0.21 1 10/05/11 22:54 74-95-3 ND ug/L 1.0 0.30 1 10/05/11 22:54 95-50-1 ND ug/L 1.0 0.24 1 10/05/11 22:54 541-73-1 ND ug/L 1.0 0.33 1 10/05/11 22:54 106-46-7 ND ug/L 1.0 0.21 1 10/05/11 22:54 75-71-8 ND ug/L 1.0 0.32 1 10/05/11 22:54 75-34-3 ND ug/L 1.0 0.12 1 10/05/11 22:54 107-06-2 ND ug/L 1.0 0.56 1 10/05/11 22:54 75-35-4 ND ug/L 1.0 0.19 1 10/05/11 22:54 156-59-2 ND ug/L 1.0 0.49 1 10/05/11 22:54 156-60-5 ND ug/L 1.0 0.27 1 10/05/11 22:54 78-87-5 ND ug/L 1.0 0.28 1 10/05/11 22:54 142-28-9 ND ug/L 1.0 0.13 1 10/05/11 22:54 594-20-7 ND ug/L 1.0 0.49 1 10/05/11 22:54 563-58-6 ND ug/L 1.0 0.13 1 10/05/11 22:54 10061-01-5 ND ug/L 1.0 0.26 1 10/05/11 22:54 10061-02-6 ND ug/L 1.0 0.12 1 10/05/11 22:54 108-20-3 ND ug/L 1.0 0.30 1 10/05/11 22:54 100-41-4 ND ug/L 1.0 0.71 1 10/05/11 22:54 87-68-3 ND ug/L 5.0 0.46 1 10/05/11 22:54 591-78-6 ND ug/L 1.0 0.31 1 10/05/11 22:54 99-87-6 ND ug/L 2.0 0.97 1 10/05/11 22:54 75-09-2 ND ug/L 5.0 0.33 1 10/05/11 22:54 108-10-1 ND ug/L 1.0 0.21 1 10/05/11 22:54 1634-04-4 ND ug/L 1.0 0.24 1 10/05/11 22:54 91-20-3 ND ug/L 1.0 0.26 1 10/05/11 22:54 100-42-5 ND ug/L 1.0 0.33 1 10/05/11 22:54 630-20-6 ND ug/L 1.0 0.40 1 10/05/11 22:54 79-34-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 33 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TRIP BLANK Labll): 92103334015 Collected: 09/28/11 00:00 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1.0 0.46 1 10/05/11 22:54 127-18-4 Toluene ND ug/L 1.0 0.26 1 10/05/11 22:54 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 0.33 1 10/05/11 22:54 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 0.35 1 10/05/11 22:54 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 0.48 1 10/05/11 22:54 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 0.29 1 10/05/11 22:54 79-00-5 Trichloroethene ND ug/L 1.0 0.47 1 10/05/11 22:54 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.20 1 10/05/11 22:54 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 0.41 1 10/05/11 22:54 96-18-4 Vinyl acetate ND ug/L 2.0 0.35 1 10/05/11 22:54 108-05-4 Vinyl chloride ND ug/L 1.0 0.62 1 10/05/11 22:54 75-01-4 m&p-Xylene ND ug/L 2.0 0.66 1 10/05/11 22:54 179601-23-1 o-Xylene ND ug/L 1.0 0.23 1 10/05/11 22:54 95-47-6 4-Bromofluorobenzene (S) 97 % 70-130 1 10/05/11 22:54 460-00-4 Dibromofluoromethane (S) 92 % 70-130 1 10/05/11 22:54 1868-53-7 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 10/05/11 22:54 17060-07-0 Tbluene-d8 (S) 93 % 70-130 1 10/05/11 22:54 2037-26-5 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 34 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 QC Batch: MSV/16889 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 92103334001,92103334002,92103334003,92103334004,92103334005,92103334006,92103334007, 92103334008,92103334009,92103334010,92103334011,92103334012,92103334013,92103334014, 92103334015 METHOD BLANK: 668600 Matrix: Water Associated Lab Samples: 92103334001,92103334002,92103334003,92103334004,92103334005,92103334006,92103334007, 92103334008,92103334009,92103334010,92103334011,92103334012,92103334013,92103334014, 92103334015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1, 1, 1,2-Tetrachloroethane ug/L ND 1.0 10/05/11 22:30 1, 1, 1 -Trichloroethane ug/L ND 1.0 10/05/11 22:30 1, 1,2,2-Tetrachloroethane ug/L ND 1.0 10/05/11 22:30 1, 1,2-Trichloroethane ug/L ND 1.0 10/05/11 22:30 1,1-Dichloroethane ug/L ND 1.0 10/05/11 22:30 1,1-Dichloroethene ug/L ND 1.0 10/05/11 22:30 1,1-Dichloropropene ug/L ND 1.0 10/05/11 22:30 1,2,3-Trichlorobenzene ug/L ND 1.0 10/05/11 22:30 1,2,3-Trichloropropane ug/L ND 1.0 10/05/11 22:30 1,2,4-Trichlorobenzene ug/L ND 1.0 10/05/11 22:30 1,2-Dibromo-3-chloropropane ug/L ND 5.0 10/05/11 22:30 1,2-Dibromoethane (EDB) ug/L ND 1.0 10/05/11 22:30 1,2-Dichlorobenzene ug/L ND 1.0 10/05/11 22:30 1,2-Dichloroethane ug/L ND 1.0 10/05/11 22:30 1,2-Dichloropropane ug/L ND 1.0 10/05/11 22:30 1,3-Dichlorobenzene ug/L ND 1.0 10/05/11 22:30 1,3-Dichloropropane ug/L ND 1.0 10/05/11 22:30 1,4-Dichlorobenzene ug/L ND 1.0 10/05/11 22:30 2,2-Dichloropropane ug/L ND 1.0 10/05/11 22:30 2-Butanone (MEK) ug/L ND 5.0 10/05/11 22:30 2-Chlorotoluene ug/L ND 1.0 10/05/11 22:30 2-Hexanone ug/L ND 5.0 10/05/11 22:30 4-Chlorotoluene ug/L ND 1.0 10/05/11 22:30 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 10/05/11 22:30 Acetone ug/L ND 25.0 10/05/11 22:30 Benzene ug/L ND 1.0 10/05/11 22:30 Bromobenzene ug/L ND 1.0 10/05/11 22:30 Bromochloromethane ug/L ND 1.0 10/05/11 22:30 Bromodichloromethane ug/L ND 1.0 10/05/11 22:30 Bromoform ug/L ND 1.0 10/05/11 22:30 Bromomethane ug/L ND 2.0 10/05/11 22:30 Carbon tetrachloride ug/L ND 1.0 10/05/11 22:30 Chlorobenzene ug/L ND 1.0 10/05/11 22:30 Chloroethane ug/L ND 1.0 10/05/11 22:30 Chloroform ug/L ND 1.0 10/05/11 22:30 Chloromethane ug/L ND 1.0 10/05/11 22:30 cis-1,2-Dichloroethene ug/L ND 1.0 10/05/11 22:30 cis-1,3-Dichloropropene ug/L ND 1.0 10/05/11 22:30 Dibromochloromethane ug/L ND 1.0 10/05/11 22:30 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 35 of 39 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 METHOD BLANK: 668600 Matrix: Water Associated Lab Samples: 92103334001,92103334002,92103334003,92103334004,92103334005,92103334006,92103334007, 92103334008,92103334009,92103334010,92103334011,92103334012,92103334013,92103334014, 92103334015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dibromomethane ug/L ND 1.0 10/05/11 22:30 Dichlorodifluoromethane ug/L ND 1.0 10/05/11 22:30 Diisopropyl ether ug/L ND 1.0 10/05/11 22:30 Ethylbenzene ug/L ND 1.0 10/05/11 22:30 Hexachloro-1,3-butadiene ug/L 0.991 1.0 10/05/11 22:30 m&p-Xylene ug/L ND 2.0 10/05/11 22:30 Methyl-tert-butyl ether ug/L ND 1.0 10/05/11 22:30 Methylene Chloride ug/L ND 2.0 10/05/11 22:30 Naphthalene ug/L 0.28J 1.0 10/05/11 22:30 o-Xylene ug/L ND 1.0 10/05/11 22:30 p-Isopropyltoluene ug/L ND 1.0 10/05/11 22:30 Styrene ug/L ND 1.0 10/05/11 22:30 Tetrachloroethene ug/L ND 1.0 10/05/11 22:30 Toluene ug/L ND 1.0 10/05/11 22:30 trans- 1,2-Dichloroethene ug/L ND 1.0 10/05/11 22:30 trans- 1, 3-Dichloropropene ug/L ND 1.0 10/05/11 22:30 Trichloroethene ug/L ND 1.0 10/05/11 22:30 Trichlorofluoromethane ug/L ND 1.0 10/05/11 22:30 Vinyl acetate ug/L ND 2.0 10/05/11 22:30 Vinyl chloride ug/L ND 1.0 10/05/11 22:30 1,2-Dichloroethane-d4 (S) % 107 70-130 10/05/11 22:30 4-Bromofluorobenzene (S) % 94 70-130 10/05/11 22:30 Dibromofluoromethane (S) % 92 70-130 10/05/11 22:30 Tbluene-d8 (S) % 100 70-130 10/05/11 22:30 LABORATORY CONTROL SAMPLE: 668601 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 55.2 110 70-130 1,1,1-Trichloroethane ug/L 50 48.2 96 70-130 1,1,2,2-Tetrachloroethane ug/L 50 55.9 112 70-130 1,1,2-Trichloroethane ug/L 50 51.5 103 70-130 1,1-Dichloroethane ug/L 50 49.8 100 70-130 1,1-Dichloroethene ug/L 50 51.0 102 70-132 1,1-Dichloropropene ug/L 50 51.4 103 70-130 1,2,3-Trichlorobenzene ug/L 50 49.1 98 70-135 1,2,3-Trichloropropane ug/L 50 52.7 105 70-130 1,2,4-Trichlorobenzene ug/L 50 49.4 99 70-134 1,2-Dibromo-3-chloropropane ug/L 50 55.1 110 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.8 110 70-130 1,2-Dichlorobenzene ug/L 50 50.7 101 70-130 1,2-Dichloroethane ug/L 50 54.8 110 70-130 1,2-Dichloropropane ug/L 50 52.7 105 70-130 1,3-Dichlorobenzene ug/L 50 50.8 102 70-130 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 36 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 LABORATORY CONTROL SAMPLE: Parameter 668601 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,3-Dichloropropane ug/L 50 52.9 106 70-130 1,4-Dichlorobenzene ug/L 50 49.1 98 70-130 2,2-Dichloropropane ug/L 50 42.3 85 58-145 2-Butanone (MEK) ug/L 100 103 103 70-145 2-Chlorotoluene ug/L 50 50.7 101 70-130 2-Hexanone ug/L 100 ill ill 70-144 4-Chlorotoluene ug/L 50 52.3 105 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 ill ill 70-140 Acetone ug/L 100 117 117 50-175 Benzene ug/L 50 53.1 106 70-130 Bromobenzene ug/L 50 50.5 101 70-130 Bromochloromethane ug/L 50 51.7 103 70-130 Bromodichloromethane ug/L 50 51.4 103 70-130 Bromoform ug/L 50 55.5 ill 70-130 Bromomethane ug/L 50 63.9 128 54-130 Carbon tetrachloride ug/L 50 49.9 100 70-132 Chlorobenzene ug/L 50 53.2 106 70-130 Chloroethane ug/L 50 62.0 124 64-134 Chloroform ug/L 50 53.1 106 70-130 Chloromethane ug/L 50 54.9 110 64-130 cis-1,2-Dichloroethene ug/L 50 49.2 98 70-131 cis-1,3-Dichloropropene ug/L 50 54.1 108 70-130 Dibromochloromethane ug/L 50 51.5 103 70-130 Dibromomethane ug/L 50 54.0 108 70-131 Dichlorodifluoromethane ug/L 50 52.8 106 56-130 Diisopropyl ether ug/L 50 50.9 102 70-130 Ethylbenzene ug/L 50 51.7 103 70-130 Hexachloro-1,3-butadiene ug/L 50 49.6 99 70-130 m&p-Xylene ug/L 100 107 107 70-130 Methyl-tert-butyl ether ug/L 50 53.0 106 70-130 Methylene Chloride ug/L 50 60.6 121 63-130 Naphthalene ug/L 50 51.5 103 70-138 o-Xylene ug/L 50 54.5 109 70-130 p-Isopropyltoluene ug/L 50 52.5 105 70-130 Styrene ug/L 50 57.4 115 70-130 Tetrachloroethene ug/L 50 49.9 100 70-130 Toluene ug/L 50 51.2 102 70-130 trans- 1,2-Dichloroethene ug/L 50 50.5 101 70-130 trans- 1, 3-Dichloropropene ug/L 50 53.2 106 70-132 Trichloroethene ug/L 50 55.4 ill 70-130 Trichlorofluoromethane ug/L 50 55.8 112 62-133 Vinyl acetate ug/L 100 87.4 87 66-157 Vinyl chloride ug/L 50 53.6 107 69-130 1,2-Dichloroethane-d4 (S) % 95 70-130 4-Bromofluorobenzene (S) % 102 70-130 Dibromofluoromethane (S) % 93 70-130 Tbluene-d8 (S) % 99 70-130 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 37 of 39 Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 668602 668603 IVIS MSD 92103334001 Spike Spike IVIS MSD IVIS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual M-Dichloroethene ug/L ND 50 50 66.1 60.9 132 122 70-166 8 30 Benzene ug/L 3.9 50 50 62.3 63.7 117 119 70-148 2 30 Chlorobenzene ug/L ND 50 50 55.5 57.8 ill 116 70-146 4 30 Toluene ug/L 1.9 50 50 59.1 61.2 114 119 70-155 3 30 Trichloroethene ug/L ND 50 50 53.4 56.0 107 112 69-151 5 30 1,2-Dichloroethane-d4 (S) % 108 105 70-130 4-Bromofluorobenzene (S) % 99 97 70-130 Dibromofluoromethane (S) % 102 98 70-130 Tbluene-d8 (S) % 97 99 70-130 Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 38 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103334 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference k MEMO ini 11111FIR1111151110 SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES PASI-C Pace Analytical Services - Charlotte Date: 10/10/2011 03:29 PM REPORT OF LABORATORY ANALYSIS Page 39 of 39 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. T w w ci I -.:I < 14 tz) 0 z r-A Z 0 LO 2 x w *0 rA 0 4) (A (,/\ Z 0 LO a 0 m 0 CL %0 ui _j A ui (N/,k) ouijolqo jenppa�j z < :z W CLi LL 4) J: a- U) 0 z -I -j E W, cc Al 4) V O� co OF r N hk Jqqjo loueqle" 0 M> VSzeN 2 1 T < HOUN 10H X X F� z ':ONH 0 4- 6 cc o E 0 L- c 1.02 E m z C: 0 f '(6 i� �'OSZH Ul pa/u;asejdun < 0 uj 4) > C (U E 0 0 r (D 2? p cu 0 o 0 cc 0 r- 2 0- w o S�l 3 N I VIN 00 :10 # *r, US -S o a. m af 2C, af PNCO11031100 IV dN:313ldNVS cc um 0 uj 43 go LUL 0 I uj F- t4i z (? c 2 0 EL Z LLJ .-& ::X z;: tu 0 o uj < *A4 0 uj io4- rz:- IV z .0 0 LU LL LU U) LL 0 Of < C) U) uj 0 cc < cl E -.0- .s ia (dV400=0 9"0=0) 3dU 3ldViVS 2- z (D 'a 1- L: (D -0 (40101 S9POO P!IBA 99s) 3000 XRUM o 0 0 cc C Q E cc z E :3 z 3: F- CL —i -j CL w U) w a �: 0 0 F- 0 cr 4) 4) a. a) 0- 0 f f a 0 U) a: W- 0 Q. a- 0- 00 (D 25 L< w F-0 < C: :2 (D U) 4) c -w 78 CL L .C: cc -C U) +� r F- 0 o z 4, w LU C4Z r= 4:s� C) z 0 x U- Lij ci 0 .0 W 2- j CD z CL cc E 0 < c .5D o E C 0 F- 0 0 0 cn q) r-) Q 0 4) 0 m a E 0 Cl) CD cc E co cc # W31 FT M) ol Go I U) cc < ui Document Name: Sample Condition Upon !;acReceipt (SCUR) cieAnalyfical Document No.: F-ASV-CS-003-rev.06 Client Name: '4� Document Revised: July 20, 2011 Page 1 of 2 Issuing Authorities: Pace Asheville Quality Office Project # q Z16333 Y Where Received: Huntersville E]--As�he—ville 17 Eden Courier: F! Fed ExE] UPS17 USP�SELf�C[iientI7 CommercialF Pace Other pfi. h I I, . .1� W. . .... R -Z Custody Seal on Cooler/Box Present: yes EJ., �o Seals intact: El yes e 7 n Packing Material: E] Bubble I Bubble Bags None Other P e ` Bubbl Thermometer Used: IR Gun Type of Ice: et lue None amples on ice, cooling process has begun Temp Correction Factor: Add btract 4!5� C Corrected Cooler Temp.: C Temp should be above freezing to 6'OC Biological Tissue is Frozen: Yes No N/A Comments: Date and Ini. 1 0 a content Chain of Custody Present: O*eg—O No 0 N/A 1 1 . Chain of Custody Filled Out: JZLYes7--0No ON/A 2. Chain of Custody Relinquighed: ELYe-,-T�No ON/A 3. Sampler Name & Signature on COC: O>e--E]No ON/A 4. Samples Arrived within Hold Time: PY'6'5�EiNo ON/A 5 Short Hold Time Analysis�'(<72hr): DYes Eblo�/A 6. Rush Turn Around Time Requested: DYes E]No EWA--7- Sufficient Volume: F I -e s- o El N/A 8. Correct Containers Used: -Pace Containers Used: K31-e-s- DNo L�-Y�s 'D No R N/A ON/A 9. Containers Intact: El N/A 10. Filtered volume received for Dissolved tests DYes []No EWA, 44. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: Ze�No El N/A 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptionQ)o liform, TOC, O&G, WI-DRO (water) g.� N o N-YV�AfN. El Yes E51q 0 El N/A 1:1 N/A 13. 3 i nitial when completed Samples checked for dechlorination: E]Yes E]No E4117A0O" 14. Headspace in VOA Vials (>6mm): DYes K;M�O�N/A 15. Trip Blank Present: Trip Blank Custody Seals Present ,Pace Trip Blank Lot # (if purchased): FlYes E]No E]Yes E]No /A rN/A 16. Client Notification/ Resolution: Field Data Requilred? Y N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: I Date: C7111 1 SRF Review: I I D a t e: I 711Z r7 /// I Note: Whenever t iss a. discrepranCy affecting North Carolina complianc-e sample,,---,, a copy oVis form will be sent- 'to the North *-,'--'.a'rolina"DEHNR T L Ce rl ific,.ation Off Pce ( Le ou-t- of hold, incoleirecat Preservative, out of temp, incorrect containers) rT w ir 1� F- < z 0 m Z LO 2 ui pA *0 IV) LO w F- "F LO a 0 CL C\i 4) LO (L w < (N/A) Guliolqo jenppe�j IL z Z) o < w Ji Z w 7Z z 0 w U, E j D (L z :0 9) Q cu w E 0 cr w urizif ipllve&m J9410 —C loueqlen C>u 4) (D ':OZSZeN HOeN 10H z LU ':ONH 0 b; Vi E 0 L- E m CL "OSZH 0 10- 0 0 z =03 a) f 1 peAjesejdun < = L.) > w Co C c 0 < E 0 Q a c 0 2 0 4? 0 CL X CL 0) 4) 'M 0 c m M CL 0- (D 0 cc a- S�13NIViNOO JO # IA M r4 D U N011031100 IV dIN31 3ldVYVS LLJ P, LL 0 0 ZV1, �W- Lu 0 CL LLJ z 0 w < 0 LU w 0 LLI cl) 0 w (L < � I-- 0(l) w 0 4- cc v < 0 0 (dV400=0 9"0=0) 3dki 3-ldVYVS z I- L: (49101 SOPOO P!18A 99S) 3000 Milm (D f -2 0 0) .0 0- 0 E m E :3 3: F- 3: -1 -1 CL w U) CL w 0 �: �: W 0 3: F- 0 M o 11 v - 0 0 >% (1) m r- z z z 4- 0 cr 4) a) cL (1) 0- 0 0 U) Ir X C) CL 10- a. 1 00 cc (D x x t3) W F- c 0 cu m 16- 1- 0 0- co 0;� ;rc P o w D z c U- m C� 0 cc c .2 m E U j 0) I C) E vo �m lz .2 0. 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U. w X z w N z 0 z 0 acie Analytical Document Name: Sample Condition Upon Document Revised: July 20, 2011 -Receipt (SCUR) Page 1 of 2 Document No.: Issuing Authorities: F-ASV-CS-003-rev.06 Pace Asheville Quality Office Client Name: Pro ect # Y Where Received: Hun'tersville [�]�eville 17 Eden Courier: E] Fed Ex F� ups,7 uspsL4o-o �crle�nto CommercialE] Pace Other Custody Seal on Cooler/Box Present: [] yes �no Seals intact: R yes [tno Packing Material: 0 Bubble Bubble Bags None Other Thermometer Used: IR Gu=- 053, Type of Ice: W5e Blue None L_j SWples on ice, cooling process has begun A A -1 1 7t%AL-&-- -a oog) d07 .4% 0e, Corrected Cooler Temp.: C Temp should be above freezing to 60C Biological Tissue is Frozen: Yes No N/A Comments: A 1 -0017 Date and Ini of rso 11 V* contents*. -71 z9 Chain of Custody Present: 9-Yg�sNo EIN/A 1. Chain of Custody Filled Out: 49-re-s�'L]No ON/A 2. Chain of Custody Relinquished: Z*n"—O No 0 N/A 3. Sampler Name & Signature on COC: No 0 N/A 4. Samples Arrived within Hold Time: 1676�s —Ej No ON/A 5. Short Hold Time Analysis (<72hr): E]Yes QNa--4�4N/A 6. Rush Turn Around Time Requested: DYes []No JaWA-j. Sufficient Volume: EtT-e�sNo ON/A 8. Correct Containers Used: -Pace Containers Used: 4;*aT--0No 4�1 �es E7 No ON/A ON/A 9. Containers Intact: e1Y."as-0 No ON/A 10. Filtered volume received for Dissolved tests []Yes E]No -t 1 . Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: 9YVs--0 No El N/A 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions(Q, coliform, TOC, O&G, Wl-DR0 (water) ?;*es—ENo EIN/A R:*,�sNo EIN/A RYes 9405—" 13. InitinI imhan r, initial when completed Samples checked for dechlorination: DYes E]No Headspace in VOA Vials (>6mm): E]Yes PfTo"'ITN/A 15. Trip Blank Present: Trip Blank Custody Seals Present [Pace Trip Blank Lot # (if purchased): E]Yes []No E]Yes ONo N/A N/A 16. Client Notificationl Resolution: Person Contacted: Comments/ Resolution: Date./Time: Field Datca Requilred? Y / N SCURF Reviewd D . te S R F R ev i ew: Data: e I Note: Whenever th is a discrepancy affecting Nor'th Carolina comiplianr,e samples, a c4VKthis form will be sent to the North Carolina D�:HNR %-f Ct T C er-1, ification Off lCe i.e. out- of hold, incorrect preese,�A/ative, out of temp, inCorrec� containers) I I � I �.JL � L t-_; I I I I L ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden. NC 27288 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (336)623-8921 October 10, 2011 Mr. Andy Alexander Bunnell-Lammons Engineering 6004 Ponders Court Greenville, SC 29615 RE: Project: FORMERANDREX INDUSTRIES Pace Project No.: 92103336 (828)254-7176 Dear Mr. Alexander: Enclosed are the analytical results for sample(s) received by the laboratory on September 29, 2011. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards, where applicable, unless otherwise narrated in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures PIC, R�b REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (704)875-9092 Page 1 of 20 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 CERTIFICATIONS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Asheville Certification III)s 2225 Riverside Dr., Asheville, NC 28804 South Carolina Certification #: 99030001 Florida/NELAP Certification E87648 Virginia Certification #: 00072 Massachusetts Certification M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Virgina/VELAP Certification #: 460147 North Carolina Wastewater Certification #: 40 REPORT OF LABORATORY ANALYSIS Page 2 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ceAnalytical —pacelabsxom Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE SUMMARY Project: Pace Project No.: Lab ID FORMER ANDREX INDUSTRIES 92103336 Sample ID Matrix Date Collected Date Received 92103336001 SM-1 Water 09/28/11 10:30 09/29/11 08:22 92103336002 SM-2 Water 09/28/11 10:25 09/29/11 08:22 92103336003 SM-3 Water 09/28/11 10:20 09/29/11 08:22 92103336004 SM-4 Water 09/28/11 10:10 09/29/11 08:22 92103336005 SM-5 Water 09/28/11 10:05 09/29/11 08:22 92103336006 SM-6 Water 09/28/11 09:55 09/29/11 08:22 92103336007 JW-1 Water 09/28/11 10:45 09/29/11 08:22 92103336008 CS-11 Water 09/28/11 12:35 09/29/11 08:22 92103336009 CS-2 Water 09/28/11 12:25 09/29/11 08:22 92103336010 BC-1 Water 09/28/11 13:30 09/29/11 08:22 92103336011 EIC-2 Water 09/28/11 13:20 09/29/11 08:22 92103336012 EIC-3 Water 09/28/11 13:10 09/29/11 08:22 92103336013 EIC-4 Water 09/28/11 13:00 09/29/11 08:22 92103336014 EIC-5 Water 09/28/11 12:50 09/29/11 08:22 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 20 ceAnalytical —pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Lab ID FORMER ANDREX INDUSTRIES 92103336 Sample ID Method Analysts Analytes Reported Laboratory 92103336001 SM-1 SM 5310B SAJ 1 PASI-A 92103336002 SM-2 SM 5310B SAJ 1 PASI-A 92103336003 SM-3 SM 5310B SAJ 1 PASI-A 92103336004 SM-4 SM 5310B SAJ 1 PASI-A 92103336005 SM-5 SM 5310B SAJ 1 PASI-A 92103336006 SM-6 SM 5310B SAJ 1 PASI-A 92103336007 JW-11 SM 5310B SAJ 1 PASI-A 92103336008 CS-11 SM 5310B SAJ 1 PASI-A 92103336009 CS-2 SM 5310B SAJ 1 PASI-A 92103336010 BC-1 SM 5310B SAJ 1 PASI-A 92103336011 BC-2 SM 5310B SAJ 1 PASI-A 92103336012 BC-3 SM 5310B SAJ 1 PASI-A 92103336013 BC-4 SM 5310B SAJ 1 PASI-A 92103336014 BC-5 SM 5310B SAJ 1 PASI-A REPORT OF LABORATORY ANALYSIS Page 4 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-1 Labll): 92103336001 Collected: 09/28/11 10:30 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 2.2 mg/L 1.0 1.0 1 10/07/11 16:52 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 5 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-2 Labll): 92103336002 Collected: 09/28/11 10:25 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.7 mg/L 1.0 1.0 1 10/07/11 17:04 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 6 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-3 Labll): 92103336003 Collected: 09/28/11 10:20 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.7 mg/L 1.0 1.0 1 10/07/11 17:14 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 7 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-4 Labll): 92103336004 Collected: 09/28/11 10:10 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.4 mg/L 1.0 1.0 1 10/07/11 17:24 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 8 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-5 Labll): 92103336005 Collected: 09/28/11 10:05 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/07/11 17:54 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 9 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SM-6 Labll): 92103336006 Collected: 09/28/11 09:55 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/07/11 18:14 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 10 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: JW-11 Labll): 92103336007 Collected: 09/28/11 10:45 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 8.7 mg/L 1.0 1.0 1 10/07/11 18:30 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 11 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-1 Labll): 92103336008 Collected: 09/28/11 12:35 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 3.2 mg/L 1.0 1.0 1 10/07/11 18:44 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 12 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: CS-2 Labll): 92103336009 Collected: 09/28/11 12:25 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/07/11 18:54 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 13 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-1 Labll): 92103336010 Collected: 09/28/11 13:30 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.2 mg/L 1.0 1.0 1 10/07/11 19:04 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 14 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-2 Labll): 92103336011 Collected: 09/28/11 13:20 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.5 mg/L 1.0 1.0 1 10/07/11 19:18 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 15 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-3 Labll): 92103336012 Collected: 09/28/11 13:10 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/07/11 19:28 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 16 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-4 Labll): 92103336013 Collected: 09/28/11 13:00 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.6 mg/L 1.0 1.0 1 10/07/11 19:38 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 17 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BC-5 Labll): 92103336014 Collected: 09/28/11 12:50 Received: 09/29/11 08:22 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 5310B Total Organic Carbon 1.8 mg/L 1.0 1.0 1 10/07/11 19:48 7440-44-0 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 18 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 QC Batch: WETA/10684 Analysis Method: SM 531 OB QC Batch Method: SM 5310B Analysis Description: 531 OB TOC Associated Lab Samples: 92103336001,92103336002,92103336003,92103336004,92103336005,92103336006,92103336007, 92103336008,92103336009,92103336010,92103336011,92103336012,92103336013,92103336014 METHOD BLANK: 668627 Matrix: Water Associated Lab Samples: 92103336001,92103336002,92103336003,92103336004,92103336005,92103336006,92103336007, 92103336008,92103336009,92103336010,92103336011,92103336012,92103336013,92103336014 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 10/07/11 15:01 LABORATORY CONTROL SAMPLE: 668628 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 22.4 90 90-110 MATRIX SPIKE SAMPLE: 668629 92103587001 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 7.3 25 29.7 90 75-125 MATRIX SPIKE SAMPLE: 668631 92103336005 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 1.6 25 25.8 97 75-125 SAMPLE DUPLICATE: 668630 92103587002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 9.0 9.1 1 20 SAMPLE DUPLICATE: 668632 92103336006 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Organic Carbon mg/L 1.6 1.6 3 20 Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 19 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. ceAnalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 980OKinceyAve. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALIFIERS Project: FORMER ANDREX INDUSTRIES Pace Project No.: 92103336 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference k MEMO ini 11111FIR1111151110 SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. LABORATORIES PASI-A Pace Analytical Services - Asheville Date: 10/10/2011 04:13 PM REPORT OF LABORATORY ANALYSIS Page 20 of 20 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 161 L L CD 0 CL CO) (N/A),guliolqo jenpse�j of L L cc Su z L L �J5 AW 4) Am w < CD 0") �e w 0 (V\ z 00 z FX a M F- o SOF fiA tA U') (N/A) OUPONO lenplse�j CL Z z 0 L) —Z Z, L L AMR 4) cn w (L F CO JAZ z w AW 0 4) cr 4) 4. cc — J9410 lu C'U > loueqlevy CO) COZSZeN < HOBN IOH V z w co 0 cu T OONH 9 0 0 10 E cu z "OSZH peAjesgidun S 0 0 0 < 0 :0 E 2 cu CL co a. L: 7= 2 o- 1111— (D 0 co ULJ 4) > E 0 10 'a < 4) T- m 0 iL w cm (D CC CU a. 2 0 Cc o- S�13NIViNOO =10 # tA cu U NOL031100 IV dIN31 3ldVYVS Lij F- a LL 2 0 0 1 LU 0 w OL 2 z w 0 LLJ rAs w w -j -j 0 w F- U) 0 LLI a. F<- m 0 CO 0 < = cu E 0 w (dVYOO=O WdO=O) 3dU 3-ldVYVS — z (49101 SOPCO P!IeAeas) 3000 XPLLM (D L- -2 L: 4) m I I c 0 9,6 1, r 0 0 6 F- 0 (D 0 cu E m z Q 1--, 4) E z 46 a) 3: �- -i j a. of u) (L w 0) 5-;;t < 0 4) , (D 0 a. Id- a. 1 -00 0(.) 0 , SO, x X cc 4) U) z 0 z 0 LU -j co *0 LL 0 (D 4- U) a- 0 CL o CIO Cc& r4 a ��Vp LLJ D a z D z 0 cz U- 0 Lu LIJ j 0 C� ca J CL 6 CO z 0 c JOR < c � AD r 13 C cc 0 0 o E 47 & cr 0 E o < (U E uj a. ix cr 0 # W311 .4, w '01 a) 4- 0 z 0 am E Analytical Pacv&4bs. Corr) Name: barnple Cond Receipt (SCUR) Document No.: F-ASV-CS-003-rev.06 Client Name: M Document Revised: July 20, 2011 Page 1 of 2 Issuing Authorities: Pace Asheville Quality Office Project# 11 Where Received: 7 Huntersville [9-'A_s&viIle 17 Eden Courier: [I Fed Ex F� ups,7 USPSff!"'&rient[J CommercialD Pace Other Custody Seal on Cooler/Box Present: yes �no_ Seals intact: yes fi--n—b* Packing Material: [] Bub ubble Bags None Thermometer Used: IR Gun _03 Type of Ice: I emp Correction Factor: Add tract —C Corrected Cooler Temp.: C Biological Tissue i Temp should be abovp- frPPAnn tr) r,0(1 Chain of Custody Present: DY-9-s—EINo ON/A Chain of Custody Filled Out: W*eT-_0 No 0 N/A Chain of Custody Relinquished: Z;*ez—D No 11 N/A Sampler Name.& Signature on COC: ZY-et- El No 0 N/A Samples Arrived within Hold Time: Z;*0'9--D No 1:1 N/A Short Hold Time -Analysis (<72hr): 0 Yes OLL9�- N/A Rush Turn Around Time Requested: E]Yes E]No Sufficient Volume: ZLYe�s-�No ON/A Correct Containers Used: -Pace Containers Used: D No Q*ee--DNo ON/A ON/A Containers Intact: Z IYe - ser 0 N o 1:1 N/A Filtered volume received for Dissolved tests E]Yes E]No E1WLA_ Sample Labels match COC: -includes dateAime/ID/Analysis Matrix:_, /'/J Zb�oe�No �. El N/A TiTcontainers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coliformNT��&G, WI-DRO (water) jtt* �sNo El N/A Z re- 5 �[: I No El N/A Samples checked for dechlorination: --.[:]Yes FlYes []No jl�:�� Headspace in VOA Vials ( >6mm): DYes 6<o ON/A Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): DYes nNo DYes nNo N/A N/A Other Blue None G_S_XM_Pes on ice, cooling process has begun Client Notification/ Resolution: Field Data Required? Y N Person Contacted- Date/Time: Comments/ Resolution: SCURF Rev1ewL,:V.1& Da'L-e- 2. SRF Reviewl s f=1 lDate: 1713C)711 or. Note: Whenever t,&7s a. discreDancy affecting North Carolina clompliance samQles, a copy S form be sen-' to. the North �_.'arolina Dr:HNR L Certificaation Off Ica, ( i.e oul- of hold, incolrrec't preservative, out of ternpi, incorrec-t c'ontainem CIL. APPENDIX C IUSTORICAL LABORATORY ANALYSES RESULTS SUMMARY TABLES AND TIME VS. CONCENTRATION PLOTS Monitoring Well MW-1 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 ath 2nd 3rd 4th lst 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant I Tetrachloroethene 7,400 8,600 3,400 900 NS 860 3,600 3,500 880 NS 1,400 183 74 170 190 320 40 26 10 8.0 18 110 AB AB AB Trichloroethene 124 ND 21 2.6 NS ND 40 ND 3.7 NS ND ND 2.7 29 47 ND 1.0 1.2 ND ND ND 6.9 AB AB AB Chloroform 1.2 ND 1.7 9 NS 7 ND ND 17 NS ND ND 15 7 ND ND 1.1 1 ND 1.1 ND ND ND AB AB AB Vinyl Chloride ND ND ND ND NS ND ND ND ND INS I ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1, 1 -Trichloroethane ND 340 ND ND NS ND ND ND ND I NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,1,2-Trichloroethane ND I ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1 -Dichloroethene ND ND ND ND NS ND ND ND ND_ NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloroethane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND -ND, ND ND ND ND AB AB AB Trans 1,2-Dichloroethene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Cis 1,2-Dichloroethene NA NA NA NA NS NA NA NA NA NS NA NA NA 17 30 ND 0.82 ND ND ND ND 18.6 AB AB AB Trichlorofluoromethane ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloropropane ND I ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Chlorobenzene ND ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,4-Dichlorobenzene ND ND ND ND NS ND ND ND ND NS ND EF ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,1,1,2-Tetrachloroethane NA NA I NA INA I NS NA NA NA NA NS NA NA NA NA NA NA NA NA NA I NA I NA I ND AB AB AB TOTAL CHLORINATEDS DETECTED 17,52518,94013,4231912 1 NS 1 867 13,64013,5001 901 1 NS 11,4001 183 1 92 1 223 1 267 1 320 1 43 1 27 1 11 1 8.0 1 18 1 116 AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NS = Not Sampled; recovery system being monitored for aquifer modeling. The laboratory results from MW-1 were inadvertently labeled as MW-2 during the 2nd quarter 1994. The correction has been made on this spreadsheet. Mw-1 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-2 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3 d 0& 4t 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant Tetrachloroethene NP 640 81 76 NS 110 130 100 78 NS 66 69 28 76 41 31 19 17 12 13 19 6.9 AB AB AB Trichloroethene NP ND 1.7 7.3 NS 13 21 12 12 NS 13 ND ND 16 11 6.4 2.9 2.4 2.7 2.6 1.7 0.71 AB AB AB Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND 0.69 ND ND ND ND ND ND AB AB AB Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1, 1 -Trichloroethane NP 91 ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND. AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 2.8 17 4.1 4.1 ND 1.8 0.83 1.2 ND AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ��N D N D ND ND AB AB AB 1,4-Dichlorobenzene NPtND ND ND NS ND ND ND ND NS ND I NT) NTD ND ND AB AB AB 1, 1, 1,2-Tetrachloroethane !NA NAINAINAINSINA1 NA I NA -- NA ND AB AB AB TOTAL CHLORINATEDS DETECTED I NP 17311 83 1 83 1 NS 11231 1511 1121 90 1 NS 1 79 1 69 1 28 1 95 69 1 42 1 26 1 19 1 17 16 1 22 7.6 AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. The laboratory results from MW-2 were inadvertently labeled as MW-1 during the 2nd quarter 1994. The correction has been made on this spreadsheet. MW-2 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-3 Concentrations in Parts per Billion (gg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 — 3rdT4th 2nd 3rd 4th 1st 2nd 3rd 4th Ist 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant I Tetrachloroethene NP 18,000 350 140 NS 11 80 12 34 NS 9.2 623 600 38 160 91 89 29 39 55 45 820 AB AB AB Trichloroethene NP 700 26 21 NS 2.8 12 3.1 5 NS 1.7 149 430 13 95 20 3.7 3.2 3.9 5.0 3.6 26.6 AB AB AB Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND 1.1 ND ND ND ND ND ND ND AB AB B AB Vinyl Chloride NP ND 34 49 NS 7.2 17 10 7.8 NS ND ND 59 3.5 11 ND ND ND 0.84 ND ND 2.6 AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB JB 1, 1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND 1.1 ND ND ND ND ND ND ND AB AB B AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND 1.30 ND ND ND ND ND ND ND ND ND 0.55 AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Trans 1,2-Dichloroethene NP ND 0.74 ND NS ND ND ND ND NS ND 1.57 ND ND ND ND ND ND ND ND ND ND AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 20 130 18 ND ND 2.3 0.53 1.2 40.9 AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND N ND ND ND ND AB AB AB 1,1,1,2-Tetrachloroeffiane NA NA NA NA NS NAI NA I NA I NA I NS I NA I NA NA I NA I NA I NA NA NA NA ND AB AB AB TOTAL CHLORINATEDS DETECTED I NP 118,7001 411 12101 NS 1 21 1 1091 25 1 47 INS 1 10.91 775 1 1,0891 75 1 398 1 129 1 93 1 32 1 46 1 61 1 50 1 891 AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-3 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 1.xls Checked by: TJB Monitoring Well MW-4 Concentrations in Parts per Billion (gg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 E3r d 4th 2nd 3rd 4th lst 2nd 3rd 4th Ist 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant Tetrachloroethene— NP 1,100 630 510 NS 680 620 560 360 N S 250 363 410 840 630 180 560 170 200 200 150 230 AB AB AB Trichloroethene NP 620 230 220 NS 230 300 280 200 NS 180 248 240 430 410 160 500 140 170 170 180 275 AB AB — AB Chloroform NP ND ND ND NS ND ND 22 ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NS 2.5 ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND 3.4 ND AB AB_ AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 190 180 69 210 74 98 88 120 148 AB AB AB Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloropropane NP 4.5 3.3 ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND 0.75 0.78 AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1, 1,2-Tetrachloroediane NA NA NA NA NS NA NA NA NA NS NA NA NA NA NA NA ];A I A ]�A NA NA ND AB AB AB TOTAL CHLORINATEDS DETECTED — NPI 1,725 1863 1730 1 NS 1913 1920 1 862 1560 1 NS 1 430 1 611 1 650 1 1,4601 1,2201 409 1 1,2701 384 1 468 1 458 1 454 1 654 AB AB AB — Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-4 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 1.xls Checked by: TJB Monitoring Well MW-5 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd 4th 2.d 3rd 4th lst 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant Tetrachloroethene NP 49,000 23,000 7,200 NS 9,200 7,800 7,600 9,000 NS 25,000 3,200 1,500 5,500 980 NS 25_ dry 120 150 610 106 2,160 3,750 2,340 Trichloroethene NP 300 470 ND NS ND 15 ND 23 NS ND ND ND - ND— ND NS 23 dry 1.0 8.9 7.2 7.0- 5.0 14.0 74.9 Chloroform NP ND 13 ND NS ND 20 ND 38 NS ND ND 14 ND ND NS ND dry ND ND ND 0.61 1.2 1 4.2 1 ND Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry I ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP 530 8.9 ND_ NS ND 2.8 ND ND NS ND ND ND ND I ND NS ND dry ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP ND 6.8 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND 1,2-Dichloroethane NP ND 1.2 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND 2.1 ND NS ND ND ND ND NS ND ND ND ND ND NS ND dry ND ND ND ND ND I ND I Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 86 710 1 NS 1 13 dry 1 2.6 1 22 8 1 21 19 9.1 3,420 Trichlorofluoromethane NP ND NO ND NS ND 1.3 ND ND NS ND NO ND ND ND NS ND dry ND ND ND I ND ND ND ND_ 1,2-Dichloropropane NP N2__ ND ND NS ND ND ND ND NS ND ND ND D ND NS ND ND ND ND ND ND Chlorobenzene NP ND 130 ND NS ND ND ND ND NS ND ND ND ND ND NS ND ND ND ND ND ND 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND I ND ND P ND ND ND ND ND 1,1,1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA T— — — NA ND ND ND ND TOTAL CHLORINATEDS I DETECTED I NP 49,830 1 23,632 1 7,200 1 NSI 9,200 1 7,8391 7,600 1 9,061 1 NS 1 25,000 1 3,200 1 1,514 1 5,586 1 1,690 1 NS 1 40 1 dry 1 124 1 181 625 135 21,11,11,185 311,777 '; RV; Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled, well dry or in use as pilot test recovery point. Mw-5 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-6 Concentrations in Parts per Billion (�Lg/l) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998. 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 - 3rd T 4th 2.d 3rd 4th 1st 2ml 3rd 4th lst I 2ml 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant Tetrachloroethene NP 40,000 37,000 7,600 NS 27,000 7,700 7,300 7,000 NS 3,500 3,270 3,300 12,000 4,700 5,100 7,800 5,900 3,200 1,000 5,000 3,050 3,580 270 2,160 Trichloroethene NP 1,600 6,500 290 NS 1,600 330 260 310 NS ND 162 160 2,700 1,500 1,200 1,800 860 390 110 150 251 267 58 110 Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND I ND ND ND ND ND ND ND ND ND Vinyl Chloride NP ND 280 47 NS ND 99 1 ND 84 NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND- ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP I ND 1.7 ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP I ND 17 ND NS ND ND ND ND NS -ND ND 5.49 ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND 1.32 ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND 45 ND NS ND ND ND ND NS ND 20.2 ND ND ND ND ND ND 4.5 ND 1.8 1.4 ND ND ND Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 8,900 3,800 4,500 2,800 210 390 270 110 207 284 85 328 Trichlorofluoromethane NP ND 28 ND NS ND ND ND ND NS- ND 2.82 ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP ND I ND ND NS ND ND ND ND INS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene I NP I ND 9.5 ND NS ND ND ND ND NS ND 2.17 ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene I NP NP 1.8 ND NS ND ND ND ND NS ND ND ND �_�ND ND ND ND ND ND ND 4.6 3.5 ND ND ND 1,1,1,2-Tetrachloroethane I NA NA NA NA NS NA NA NA NA NS NA NA NA I NA NA NA NA NA NA NA NA ND ND ND N TOTAL CHLORINATEDS DETECTED I NP 141,600143,8831 7,9371 NS 128,60018,12917,56017,3941 NS 13,5001 3,464 1 3,460 123,600110,000110,800112,4001 6,970 1 3,9851 1,380 1 5,266 1 3,5131 4,131 413 2,598 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-6 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xls Checked by: TJB Monitoring Well MW-7 Concentrations in Parts per Billion (�tg/l) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 m3rd4th 1993 1994 1 5 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant I Tetrachloroethene NP 6.0 8.3 12 NS 76 46 27 13 NS 41 165 11 10 3.6 72 ND 1.9 1.4 1.4 1.3 ND 36 92 165 Trichloroethene NP ND ND NS ND ND ND ND NS ND ND ND ND ND 24 ND ND ND ND ND ND ND ND ND Chloroform NP -ND ND ND. ND. NS 1.2 ND 1.1 ND NS 2.2 6.24 1.2 2 ND 0.62 ND NDI 0.67 ND ND ND ND 0.6 0.51 Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP ND ND ND NS ND. ND. ND ND NS. ND. ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA ND ND 20 ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NDINDINDINS ND ND ND ND NS ND ND ND ND_ ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NAIN INAINAINSTNA =NANA NAINSINAI NA I NA NA NA I NA NA I NA NA -F NA NA ND ND ND ND TOTAL CHLORINATEDS DETECTED NP 1 6.01 8.31 12 1 NS 1771 46 1 28 1 13 INS 1 43 1 171 1 12 1 12 1 3.6 1 117 1 ND 1 1.9 1 2.1 1 1.4 1 1.3 1 ND 36 93 166 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-7 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 1.xis Checked by: TJB Monitoring Well MW-8 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number J1 1-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd Elh U 2nd 3rd 4th 1st 2nd 3rd 4th lst I 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant I Tetrachloroethene NP 78 24 620 NIS 20 950 900 1,500 NIS 39 675 570 420 80 8.7 19 24 15 23 40 13 AB AB AB Trichloroethene NP 4.5 ND 68 NIS ND 29 66 68 NIS 1.1 53.4 58 14 8.4 1.8 ND ND ND ND 2.9 ND AB AB AB Chloroform NP ND ND ND NIS ND ND 8.5 ND NIS ND ND ND ND ND ND ND ND ND I ND ND ND AB AB AB Vinyl Chloride NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1, 1 -Trichloroethane NP ND ND ND NIS ND ND I ND ND INS I ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1,2-Trichloroethane NP I ND ND ND NIS ND ND ND ND NIS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,1-Dichloroethene NP ND ND ND NS_ ND ND ND ND NIS ND. ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NIS ND ND ND ND NIS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 26 46 1.1 ND ND ND ND 3.9 ND AB AB AB Trichlorofluoromethane NP ND ND ND NIS ND ND I ND ND NIS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloropropane NP NP_ ND ND INS ND I ND I ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Chlorobenzene NP ND ND ND NIS ND ND ND ND NIS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND INA ND ND AB AB AB 1, 1, 1,2-Tetrachloroethane NA NA NA NA NIS NA NA NA NA NIS NA I NA NA NA NA NA NA NA NA NA ND AB AB AB TOTAL CfH-OFJNATEDS DETECTED NP 1 83 1 24 1 6881 NIS 1201 979 1 975 1 1,568 INSI 40 1 728 1 628 1 460 1 134 1 12 1 19 1 24 1 15 1 23 1 47 1 13 AB AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. Mw-8 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 l.xls Checked by: TJB Monitoring Well MW-8A Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 1 3rd 4th 2.d 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant Tetrachloroethene NP 1,800 640 3,900 NS 970 3,400 3,700 6,300 NS 1,200 3,470 3,400 1,600 1,900 1,100 400 400 420 110 190 247 AB AB AB Trichloroethene NP 96 25 250 NS 39 190 240 270 NS ND 250 220 ND 410 95 79 47 42 10 20 16 AB AB AB Chloroform NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Vinyl Chloride NP ND ND ND NS ND 2.8 ND ND NS ND 4.29 ND ND ND ND ND ND ND ND ND ND AB AB AB 1,1,1-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,1,2-Trichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1 -Dichloroethene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloroethane NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Trans 1,2-Dichloroethene NP ND ND ND NS ND 1.9 ND ND NS ND 3.11 ND ND ND ND ND ND ND ND ND ND AB AB AB Cis 1,2-Dichloroethene NP NA NA NA NS NA NA NA NA NS NA NA NA 120 430 160 150 83 80 17 40 28.4 AB AB AB Trichlorofluoromethane NP ND ND ND NS ND 0.92 ND ND NS, ND 1.78 ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloropropanc NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Chlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,4-Dichlorobenzene NP ND ND ND NS ND ND ND ND NS ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,1,1,2-Tetrachloroethane NA NA NA NA NS NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA ND AB AB AB TOTAL CHLORINATEDS DETECTED I NP 11,8961 66514,1501 NS 11,00913,59613,94016,5701 NS 11,2001 3,729 1 3,620 1 1,7201 2,740 1 1,355 1 629 1 530 1 542 1 137 1 250 292 AB AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; recovery system being monitored for aquifer modeling. MW-8A Prepared by: AWA 1022-32 Andres: Historical Well Tables 201 I.xls Checked by: TJB Monitoring Well MW-9 Concentrations in Parts per Billion (�tg/l) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3 d urih 4 2nd 3rd 4th Ist 2nd 3rd 4th lst 2.d 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 1,900 4,550 3,800 3,600 3,600 1,100 270 2,200 1,700 1,000 680 4,730 4,840 5,080 4,180 Trichloroethene NP NP NP NP NP NP NP NP NP NP ND 608 620 570 970 270 66 250 140 92 98 341 234 145 107 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 4.4 ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND 9.42 ND ND ND ND 100 28 24 ND 10 2.5 ND ND ND 1,1,1-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP I NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND 0.74 ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 1.89 ND ND ND ND 0.5 ND ND ND 3.6 1.1 ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP--NP NP NP NP NP NP NP NP NP ND 8.81 ND ND ND ND 5.6 ND 2.6 ND 2.2 7 ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA 920 1,100 260 300 500 400 240 1 80 180 466 376 259 191 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 2.31 ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP. NP NP ND 6.29 ND ND ND ND 28 6.8 1.5 ND L2. 2 1.6 ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 5.6 ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NA NP NP NP -- NP NP NP NP NP NA NA NA NA NA NA NA NA NA NA NA 0.70 ND ND ND TOTAL CHLORINATEDS DETECTED NPI NPI NP I NPI NP I NP I NP I NPI NP I NP 1 1,9001 5,1871 4,420 1 5,090 1 5,670 1 1,6301 780 1 2,985 1 2,268 1 1,332 976 5,551 5.450 5,484 4,478 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. Mw-9 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xls Checked by: TR3 Monitoring Well MW-10 Concentrations in Parts per Billion (Rg/1) Andrex Industries Asheville, North Carolina BLE Job Number JII-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 1 3rd 4th 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd _ 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 4,700 4,920 5,400 9,900 4,200 4,500 3,500 900 800 590 1,200 3,360 1,910 3,160 182 Trichloroethene NP NP NP NP NP NP NP NP NP NP 400 484 480 920 400 450 440 120 74 54 120 180 76 127 75 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND 3.07 ND ND ND ND ND ND ND ND 2.7 ND ND ND ND 1,1,1-Trichloroethatie NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Ij-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 2.00 ND ND ND ND ND ND ND ND 3.5 ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.9 Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 7.69 ND ND ND ND ND ND 1.2 ND 2.6 5 ND ND 15.2 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA 2,300 1,300 870 620 320 220 160 270 426 169 253 1,460 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 4.94 ND ND ND ND ND ND ND ND 2.9 ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP �L NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND 2.51 ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP P NMNP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NA NA NA NA MA N 1.2 ND ND TOTAL C14LORINATEDS DETECTED I NPI NPI NP I NPI NPI NP I NP I NP I NP I NP 15,1001 5,424 1 5,880 113,1201 5,900 1 5,820 1 4,560 1 1,340 1 1,095 1 804 1,602 3,973 2,156 3,540 1,735 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. I�M-lo Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-11 Concentrations in Parts per Billion (gg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd Mh 4t 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 1,400 3,050 1,800 3,600 2,100 1,800 2,200 2,200 1,000 1,100 NS 975 791 2,400 2,130 Trichloroethene NP NP NP NP NP NP NP NP NP NP 190 370 240 410 280 300 110 330 230 180 NS 89 56 196 93 Chloroform NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 12 ND ND ND NS ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP ND ND 36 110 ND ND 22 ND 9.7 ND NS ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP ND 1.74 ND ND ND ND 1.7 ND ND ND NS ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP. NP NP ND 5.95 ND ND ND ND 5.8 ND 2.2 ND NS 2.2 ND 5.2 ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA 1,000 770 530 980 480 490 380 NS 153 156 337 163 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND 3.02 ND ND ND ND I ND ND ND NS ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND NS ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND 9.77 ND ND N ND 5.1 ND 2.2 ND NS ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND 2.08 ND ND ND ND 1.3 ND ND ND NS ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP I NP I NPFNIP INPI NP I NP I NP NP I NA NA NA NA NA NA NA I NA NA NA NS ND ND ND ND TOTAL CHLORINATEDS DETECTED NP NP I NP I NP I NP I NPI NPI NP I NP INPI 1,5901 3,443 1 2,076 1 5,1201 3,1501 2,630 1 3,339 1 3,0101 1,7341 1,6601 NS 1 1,2191 1,0031 2,9381 2,386, Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-11 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xis Checked by: TJB Monitoring Well MW-12 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1 95 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd [&�h 4t 2nd 3rd 4th lst 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP 5,300 3,810 1,500 3,500 2,800 3,200 220 130 220 65 930 135 1,010 3,590 156 Trichloroethene NP NP NP NP NP NP NP NP NP NP ND 6.07 ND ND ND 550 3 ND ND ND 5 1.4 10 11 44 Chloroform NP NP NP NP NP NP NP NP NP NP ND 20.8 ND ND ND ND 1.3 ND ND ND ND 1.3 2.8 ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11.3 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 14.2 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NA NA NA ND ND 750 2.8 ND ND ND 1.4 5 15 16,810 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND -6.1 ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NPINPINPINPINPINP NP NP NP ND ND ND ND ND ND ND I ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NPINPINPINPINPINPINPINP NP NA I NA I N,1 N,1 NA NA NA I NA NA ND 1.1 ND ND I TOTAL CHLOMNATEDS DETECTED I NP NP I NP I NP I NP I NP I NP I NP I NP I NP 1 5,3001 3,837 1 1,5001 3,500 1 2,8001 4,500 1 227 1 130 1 220 1 65 1 941 1 139 -F1,0291 3,616 7 011; Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-12 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-13 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1 95 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd [zh 4t 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2.d 2.d 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 788 2,100 2,900 4,100 2,600 5,100 760 420 1,100 530 356 683 1,420 960 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 174 450 480 440 440 690 99 170 110 69 42 81 97 304 Chloroform NP NP NP, NP, NP NP. NP NP NP NP. NP. ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 1.48 ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP, NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND . ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 3.5 ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP, NP, NP NP NP. NP NP ND ND ND ND ND ND ND ND_ ND I ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 1.1 0.62 ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 990 1,300 1,000 1,500 230 130 300 200 121 256 241 158 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND 2.7 ND ND 1.5 ND 1,2-Dichloropropane NP, NP NP NP, NP NP NP, NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NL_ NP NP NP. NP. NP I NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND_ 1,4-Dichlorobenzene NP NP NP NP NP I NP I NP NP, NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NPINPINPINPINPINPINPINP NA NA I NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLORINATEDS DETECTED NP I NP NP I NP I NP I NPI NP I NP I NP I NPI NPI 963 12,5501 4,370 1 5,8401 4,040 1 7,290 1 1,0891 720 1 1,5101 807 1 519 1,020 1,7591 1,422 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-13 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xls Checked by: TJB Monitoring Well MW-14 Concentrations in Parts per Billion (gg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 m3rdi 4th 2nd 3rd 4th Ist 2nd 3rd 4th Ist 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 231 280 1,100 650 570 510 250 440 320 340 375 377 867 997 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 74.9 110 220 160 190 180 120 220 130 170 196 174 396 331 Chloroform NP NP NP, NP. NP NP. NP . NP NP NP. NP ND ND ND— ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 1.76 ND ND ND ND ND ND ND ND 2.8 ND ND ND ND 1, 1, 1 -Trichloroethane NP, NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND I,I-Dichloroethene NP NP NP NP NP, NP NP NP, NP NP NP ND ND ND ND ND ND ND ND ND 3.8 0.79 ND 1.7 ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP. NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP I NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 140 110 100 90 64 95 77 120 123 91 206 136 Trichlorofluoromethane, NP NP NP NP NP NP, NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP, NP NP NP, NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP. NP. NP NP NP NP NP NP NP. NP ND ND ND 11TD ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NPINPINPINP NP NP NP NP NP I NP NA NA NA NA NA NA NA NA NA ND ND ND TOTAL CHLORINATEDS DETECTED NP I NP I NP I NP I NP NP I NP I NP I NP INPI NP 1 308 1 390 1 1,4601 920 1 860 1 780 1 434 1 755 1 527 1 637 1 695 642 1,471 1 44 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-14 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 l.x1s Checked by: TJB Monitoring Well MW-15 Concentrations in Parts per Billion (jig/]) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 19 7 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 M 2nd 3rd 4th lst 2nd 3rd 4th 1st 2nd 2.nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 71 45 92 70 71 110 110 90 100 130 171 197 704 194 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 2.59 2.4 4.6 2 2.4 2.7 ND ND ND 2.4 3.4 3.7 4.2 3.9 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.71 0.98 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Ij-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 2.0 ND ND 5.7 ND 6 ND 4.5 6.3 6.6 8.0 9.4 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 1.25 ND 2.9 2 1.8 2.5 ND ND ND 3.1 1.3 1.1 1.6 1.2 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND 1.7 ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP N� NP NP NP �NA NA NA NA NA NA ND ND ND ND TOTAL CHLORMATEDS DETECTED I NPI NPI NP I NP I NP INPI NP I NP I NP I NP I NP 1 75 1 47 1 102 1 74 1 77 1 121 1 110 1 96 1 100 1 140 1 182 208 719 209 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-15 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJ13 Monitoring Well MW-16 Concentrations in Parts per Billion (Vg/1) Andrex Industries Asheville, North Carolina BLE Job Number JII-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 EE� 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th lst 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 65.7 77 180 150 76 190 120 150 200 190 434 245 401 249 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 2.66 3.7 5.4 5 5.3 6.8 ND 2.6 ND 4.5 6.6 5.3 8.4 4.9 Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND 0.8 ND 1.5 1.5 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND I ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 2.7 3.4 4.7 12 ND 8.4 5.1 8 13 9.3 16 11 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 1.24 1.6 5.2 4.4 7.1 6.2 ND ND ND 4.1 3.6 ND 3.4 1.8 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA I NA NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NP I NP INPI NP 1 70 1 82 1 193 1 162 1 93 1 215 1 120 1 161 1 205 1 207 1 458 260 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-16 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-17 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 E3 r�d �4 th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 320 410 430 82 78 29 52 82 54 100 17 24 18 7.5 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 36 86 54 35 27 13 14 20 11 13 8.2 7.2 4.3 3.4 Chloroform NP NP NP, NP, NP NP. NP NP NP. NP. NP 0.36 ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP 5.68 12 12 17 14 10 8.6 5 1.6 3.2 2.7 5.9 7.9 7.6 1, 1, 1 -Trichloroethane NP, NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP I NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP. NP. NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP. NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP. NA NA 150 64 41 47 43 37 23 33 33 39 18 16 Trichlorofluoromethane NP. NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND, ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP, NP. NP. NP. NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroediane NP NP NP NP NP NP NP NP NP , NP, N NA NA I NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLORINATEDS DETECTED I I NP NP NP NP NP NP NP NP NP I NP I NP 1 362 15081 646 1 198 1 160 99 118 144 90 149 62 76 48 34 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-17 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xls Checked by: TJB Monitoring Well MW-18 Concentrations in Parts per Billion (jig/]) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 M 2nd 3rd 4th lst 2nd 3rd 4th 1st 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.7 1.1 0.7 ND ND 277 7.1 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND 0.53 ND ND 0.9 ND 1.3 1.5 1.6 1.4 1.1 4.3 0.7 Chloroform NP NP NP NP NP NP NP NP NP NP NP 121.5 20 1 20 1 14 10 1 11 4.0 3.9 2.7 2 1.1 1.2 1.5 1.4 Vinyl Chloride NP I NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Ij-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND I ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND 0.98 NID Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP �NA NA I NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLORMATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NP I NP I NP I NP 1 22 1 20 1 21 1 14 1 10 1 12 1 4.0 1 5.9 1 5.3 1 4.3 1 2.5 2.3 78,1 1 9.2 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-18 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJ13 Monitoring Well MW-19 Concentrations in Parts per Billion (Vg/1) Andrex Industries Asheville, North Carolina BLE Job Number JII-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 EE� 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 8 5 13 16 7.7 16.0 19.0 NP NP NP NP NP NP NP Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND 1.1 2 0.58 1.10 1.60 NP NP NP NP NP NP NP Chloroform NP NP NP NP NP NP NP NP NP NP NP 1.51 1.1 3.3 4.1 3.3 6.8 5.9 NP NP NP NP NP NP NP Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND I ND ND ND ND ND NP NP NP NP NP NP NP 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 6 6.1 1.7 4.7 5.6 NP NP NP NP NP NP NP Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND D ND NP NP NP NP NP NP NP 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP- 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA I NA NA NA NA NA NA NP mP IIJP NP NP NP NP TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NP I NP I NP I NP 1 10 1 6 1 23 1 28 1 13 1 29 1 32 1 NP I NP I NP I NP NP NP NP Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-19 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-20 Concentrations in Parts per Billion (Vg/1) Andrex Industries Asheville, North Carolina BLE Job Number JII-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd 4th 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 0.59 0.72 Vinyl Chloride NP I NP NP I NP I NP NP NP NP NP NP NP ND ND I ND ND ND I ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND IND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenz ne NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP _NLPL[2ND NP NA NA NA NA NA :!NA:l NA NA NA ND ND ND ND_ TOTAL CHLORINATEDS DETECTED I NP NP NP NP NP NP NP NP NP NP I NP ND I ND ND ND ND ND ND I ND ND ND ND I ND 1 0.59 0.72 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-20 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-21 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number JII-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 EE� 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND 1.5 0.64 ND 0.81 1.5 1.4 ND 1.1 0.81 ND 1.0 0.88 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND I ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP 17 NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP_ NP NP NP NA NA NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLORINATEDS DETECTED I NP NP NP NP NP NP NP NP NP NP NP ND ND 1.5 1 0.6 ND 0.8 1.5 1.4 ND 1.1 0.8 ND 1.0 0.88 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-21 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-22 Concentrations in Parts per Billion (Vg/1) Andrex Industries Asheville, North Carolina BLE Job Number JII-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 EE� 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NPJ NP NP NP NA I NA NA I NA NA NA NA NA NA NA ND ND TOTAL CHLORINATEDS DETECTED I NP NP NP NP NP NP NP NP I NP NP I NP I ND IND I ND I ND I ND I ND I ND I ND I ND I ND I ND ND Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-22 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-23 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1 95 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd [zh 4t 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2.d 2.d 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 490 1,300 1,500 910 690 520 290 150 83 79 174 36 124 143 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 16.1 42 72 56 56 29 15 12 6.6 6.3 18.8 2.9 7.6 6.8 Chloroform NP NP NP, NP, NP NP. NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP I NP 0.25 ND ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1-Trichloroethane NP, NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND_ ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND 10 ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP. NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP, NP NP, NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP, NP NP NP NP NP NP NP NA NA 190 160 96 120 60 30 16 15 42 5.8 15 12 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND— ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene P NP PP NP NP NPINPINPINP NP NP NP ND ND ND I ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane MNP N NP NP NPINPINPINPINPINPINPI NA NA NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLORINATEDS DETECTED NP NP NP I NP I NP I NPI NP I NP I NP I NPI NP 1 506 1 1,3521 1,7621 1,1261 842 1 669 1 365 1 192 1 106 1 100 1 234 45 147 162 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-23 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xls Checked by: TJB Monitoring Well MW-24 Concentrations in Parts per Billion (jig/]) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 19 7 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 M 2nd 3rd 4th lst 2nd 3rd 4th 1st 2nd 2.nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 930 550 360 230 120 120 54 17 NS NS 33 72 430 243 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 3.67 ND ND ND ND ND ND ND NS NS 0.82 1.1 2.7 6.2 Chloroform NP NP NP NP NP NP NP NP NP NP NP 16.07 ND ND I ND ND I ND ND I ND NS I NS ND I ND ND I ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND Ij-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA ND 7.1 ND ND ND ND NS NS 0.72 ND 2.0 1.4 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP 3.84 ND ND ND ND ND ND ND NS NS ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND NS NS ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP ND ND 14 ND ND ND ND ND NS NS ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP �NN PF N NP NP NA NA —� NA NA NA NA NA NA NS NS ND ND ND ND TOTAL CHLORMATEDS DETECTED I NPI NPI NP I NP I NP INPI NP I NP I NP I NP I NP 1 944 1 550 1 360 1 237 1 120 1 120 1 54 1 17 1 NS I NS 1 35 73 435 251 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. NS = Not Sampled; well was compromised, to be repaired in 2005. MW-24 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJ13 Monitoring Well MW-25 Concentrations in Parts per Billion (Vg/1) Andrex Industries Asheville, North Carolina BLE Job Number JII-1022-32 Yearly Quarter 1991 1993 1994 1995 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 EE� 2nd 3rd 4th lst 2nd 3rd 4th lst 2nd 2nd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant I Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP 400 450 750 670 650 1,000 1,100 NP NP NP NP NP NP NP Trichloroethene NP NP NP NP NP NP NP NP NP NP NP 80.6 88 130 170 140 190 270 NP NP NP NP NP NP NP Chloroform NP NP NP NP NP NP NP NP NP NP NP 0.43 ND ND ND ND ND ND NP NP NP NP NP NP NP Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND 11 ND ND NP NP NP NP NP NP NP 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NA NA 38 ND 38 100 71 NP NP NP NP NP NP NP Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND NP NP NP NP NP NP NP 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP 2.14 5.8 ND ND ND NP NP NP NP NP NP NP Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND NP NP NP NP NP NP NP 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND NP NP NP NP NP NP NP 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP NP NP NP NP NP NP NA NA NA NA NA NP mP IIJP NP NP NP NP TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NP I NP I NP I NP 1 483 15441 918 1 840 1 839 1 1,2901 1,441 1 NP I NP I NP I NP NP NP NP Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-25 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well MW-26 Concentrations in Parts per Billion (�Lg/l) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 M 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.62 1.60 0.70 ND Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP 12 9.9 7.6 7.7 4.8 4.3 2.7 ND 3.7 3.3 2.9 3.2 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Tricbloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroethane NP NP NP NP NP LT�P NP NP NP NP NP NP NA NA NA NA NA NA NA NA NA ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 12 10 7.6 7.7 4.8 4.3 2.7 ND 4.3 AS) 3.2 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit. NA = Data not available. NP = Well not present at time of sampling. MW-26 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xls Checked by: TR3 Recovery Well RW-1 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1 91 1993 1994 1 95 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 3rd 4th 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant Tetrachloroethene NP NP 26,000 25,000 38,000 26,000 22,000 27,000 34,000 24,000 16,000 13,900 5,400 39,000 14,000 7,800 10,000 10,000 10,000 4,900 3,510 16,000 8,330 19,800 2,010 Trichloroethene NP NP 1,400 960 ND 700 920 870 1,200 1,400 1,200 924 1,400 7,100 1,100 640 530 ND 330 240 203 365 233 179 2,610 Chloroform NP NP ND ND ND 16 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.1 ND ND ND Vinyl Chloride NP NP ND 95 ND ND 38 49 ND ND ND ND ND 100 ND ND ND ND ND ND 3 ND ND ND ND 1, 1, 1 -Trichloroethane NP NP ND ND ND 12 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1, 1,2-Trichloroethane NP NP ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND ND ND ND ND 2 ND ND ND ND Ll-Dichloroethene NP NP ND ND ND ND ND 4.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroediane NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP ND ND ND 6 13 9 ND ND ND ND ND ND ND ND ND ND ND ND 3 3.3 ND ND 53 Cis 1,2-Dichloroethene NP NP NA NA NA NA NA NA NA NA NA NA NA 9,700 4,100 1,400 1,400 810 1,300 590 594 417 293 168 7,6101 Trichlorofluoromethane NP NP ND ND ND ND ND 12 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3 4.9 ND ND ND 1,4-Dichlorobenzene NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.0 ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8.4 ND ND ND_ TOTAL CHLORINATEDS DETECTED I NPI NP 127,400 126,055 138,000 1 26,734 1 22,971 1 27,947 135,200 1 25,400 1 17,200 1 14,824 1 6,800 155,900 1 19,200 1 9,840 1 11,930 1 10,810 1 11,630 1 5,730 1 4,318 116,8021 8,856 20,147 12,283 Quarterly groundwater sampling was initiated during the second quarter, 1993. ND = Not Detected at the method detection limit NA = Data not available. NP = Well not present at time of sampling RW-1 Proparod by: AWA 1022-32 And- Historical Well Tablcs 201 1.x1s Ch.kcd by: TJB Recovery Well RW-2 Concentrations in Parts per Billion (jig/1) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 0� 2nd 3rd 4th lst 2nd 3rd 4th Ist 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th 1st 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP 1,400 2,800 740 1,800 900 1,990 2,500 930 2,000 1,700 1,700 1,200 260 99 110 76.7 AB AB AB Trichloroethene NP NP NP NP NP NP 91 290 330 95 ND 165 260 54 370 280 280 190 20 4.7 12 3.6 AB AB AB Chloroform NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Vinyl Chloride NP NP NP NP NP NP ND 9.2 ND ND ND ND ND 99 ND ND ND ND ND ND 3.1 ND AB AB AB 1, 1, 1 -Trichloroethanc NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1,2-Trichloroethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1 -Dichloroethene NP NP NP NP NP NP ND 0.73 ND ND ND ND ND ND ND ND ND ND ND ND 3.6 ND AB AB AB 1,2-Dichloroethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Trans 1,2-Dichloroethene NP NP NP NP NP NP ND 3.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Cis 1,2-Dichloroethene NP NP NP NP NP NP NA NA NA NA NA NA NA 420 480 210 230 140 42 44 210 5.9 AB AB AB Trichlorofluoromethane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,2-Dichloropropane NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB Chlorobenzene NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1,4-Dichlorobenzene NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND AB AB AB 1, 1, 1,2-Tetrachloroethane NP P NP NP NP NP NA NA NA NA —4 NA NA NA NA NA NA NA I NA NA NA ND AB TOTAL CHLORINATEDS DETECTED I NP I NPI NPI NP I NP I NP 11,49113,10311,07011,8951 900 12,155 12,760 1 1,50312,8501 2,19012,2101 1,5301 322 1 148 1 339 86 AB Quarterly groundwater sampling was initiated during the second quarter, 1993. AB = Well abandoned. ND = Not Detected at the method detection limit NA = Data not available. NP = Well not present at time of sampling RW-2 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 Lxls Checked by: TJB Monitoring Well RW-3 Concentrations in Parts per Billion (�Lg/l) Andrex Industries Asheville, North Carolina BLE Job Number Jll-1022-32 Yearly Quarter 1991 1993 1994 1995 1996 1997 1998 1999 2000 2001 2002 2003 2004 2005 2008 2009 2010 2011 M 2nd 3rd 4th 1st 2nd 3rd 4th 1st 2nd 3rd 3rd 4th 4th 4th 4th 4th 4th 4th 4th Ist 4th 4th 3rd Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP 8,000 1,700 1,500 4,400 4,200 2,400 6,400 2,500 4,060 12,100 10,700 132 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND 15 ND 8.2 ND ND 35 89 369 43.8 ND 71.3 Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP ND 3.7 ND 1.5 ND ND ND 1.3 1.3 ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP I NP NP NP ND ND ND ND ND ND ND ND ND ND ND 40 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Tricbloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.79 ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 1.7 ND ND 14.7 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND 0.97 ND ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP I NP NP NP ND 18 ND 16 ND ND 51 120 992 59.8 ND 9,290 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,4-Dichlorobenzene_ NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1, 1,2-Tetrachloroethane NP NP NP NP NP L�LP_ NP NP NP NP NP NP NP NA NAj NA NA NA NA NA NA 1.2 ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 8,0001 1,7371 1,500 1 4,426 1 4,200 1 2,400 1 6,486 1 2,710 5,427 12,204 10,700 9.548 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-3 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 I.xls Checked by: TR3 Monitoring Well RW-4 Concentrations in Parts per Billion (lAg/1) Andrex Industries Asheville, North Carolina BLE Job Number J1 1-1022-32 Yearly Quarter 19 1 1993 1994 1 5 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2010 2011 2009 2010 3rd 4th 2nd 3rd 4th Ist 2nd 3rd 4th lst 2nd 3rd 3rd 4th 4th lst 4th 4th 4th 4th 4th 4th lst lst 3rd 4th 4th Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 4,000 1,000 1,200 3,000 1,900 640 610 3,050 3,050 3,050 AB AB Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 320 250 79 240 170 56 50 167 167 167 AB AB Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND AB AB Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND 22 ND ND ND AB AB 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND I ND ND AB AB 1, 1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND AB AB 1,1-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 0.53 ND ND ND ND ND ND ND ND AB AB 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND AB AB Trans 1,2-Dichloroethene NP NP NP NP NP NP. NP NP NP NP NP NP NP NP NP ND 11 ND ND ND ND 1.8 4.4 4.4 4.4 AB AB Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 600 470 310 810 470 170 240 307 307 307 AB AB Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 1.1 ND ND ND ND ND ND ND ND AB AB 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND AB AB Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP N NP NP ND ND ND ND ND ND ND 0.79 0.79 0.79 AB AB 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP�NP NP NP ND ND ND ND ND ND ND ND ND ND AB AB 11,1,1,2-Tetrachloro d NP NP NP NP NP NP, NP NP NP NP NP NP I NP NP NP NA NA NA I NA NA NA NA 1.0 1.0 1.0 AB AB TOTAL CHLORINATEDS i DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 4,920 1 1,733 1 1,5891 4,050 1 2,540 1 866 1 924 3,530 1 3,530 3,530 AB AB ND = Not Detected at the method detection limit. AB = Well abandoned. NP = Well not present at time of sampling. RW-4 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 1.xls Checked by: TJB Monitoring Well RW-5 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J1 1-1022-32 Yearly Quarter 19 1 1993 1994 1 95 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2010 2011 2009 2010 3rd 4th 2.d 3rd 4th Ist 21nd 3rd 4th lst 2nd 3rd 3rd 4th 4th lst 4th 4th 4th 4th 4th 4th lst lst 3rd 4th 4th Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 5,000 1,300 4,200 1,200 2,100 2,100 1,300 4,500 4,500 4,500 1,030 74 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 560 410 430 82 170 160 130 240 240 240 58 70_ Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.54 0.54 0.54 1 ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 1.1 1.1 1.1 ND 14 1, 1, 1 -Trichloroethane NP NP NP NP I NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 1.1 ND ND ND ND ND 0.5 0.5 0.5 ND 1.5 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 12 ND ND ND ND 2.6 7 7 7 ND 14.711 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 770 850 1400 300 540 470 340 541 541 541 349 1,760 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 3.3 ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 1.2 1.2 1.2 ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroetha-- NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP NA NA NA I NA NA NA NA 1.7 1.7 1.7 ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 6,330 1 2,576 1 6,030 1 1,582 1 2,810 1 2,730 1 1,773 1 5,293 5,293 5,293 1,437 1,934 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-5 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 1.xls Checked by: TJB Monitoring Well RW-6 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J1 1-1022-32 Yearly Quarter 19 1 1993 1994 1 95 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2010 2011 2009 2010 3rd 4th 2.d 3rd 4th Ist 21nd 3rd 4th lst 2nd 3rd 3rd 4th 4th Ist 4th 4th 4th 4th 4th 4th lst lst 3rd 4th 4th Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 2,500 1,900 3,000 2,300 1,500 4,300 740 1,880 1,880 1,880 2,250 1,120 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 260 320 290 200 150 190 73 169 169 169 98 262 Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND Vinyl Chloride NP NP NP NP NP NP NP NP NP NP I NP NP NP NP NP ND 1.8 ND ND ND ND ND ND —ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP_ NP NP NP NP NP ND 3.5 ND ND ND ND ND 4 4 4 ND 4.9 Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 570 640 1,000 610 460 140 440 346 346 346 279 750 Trichlorofluoromethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Chlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND 0.55 0.55 0.55 ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,1,2-Tetrachloroetbs - NP NP NP NP NP, NP NP NP NP NP NP NP NP NP NP NA NA NA , NA NA NA . NA 0.64 0.64 0.64 ND . ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP INPI NP I NP I NP I NP I NP I NP I NP I NP I NP 1 3,330 1 2,865 1 4,290 1 3,110 1 2,110 1 4,630 1 1,253 1 2400 2,400 1 2,400 2,627 1 11 ,137 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-6 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 1.xls Checked by: TJB Monitoring Well RW-7 Concentrations in Parts per Billion (pg/1) Andrex Industries Asheville, North Carolina BLE Job Number J1 1-1022-32 Yearly Quarter 19 1 1993 1994 1 95 1996 1997 1998 1999 2000 2000 2001 2002 2003 2004 2005 2008 2010 2011 2009 2010 3rd 4th 2.d 3rd 4th Ist 21nd 3rd 4th lst 2nd 3rd 3rd 4th 4th lst 4th 4th 4th 4th 4th 4th lst lst 3rd 4th 4th Contaminant Tetrachloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 2,300 1,300 2,200 2,300 2,100 1,700 700 855 855 855 2,090 107 Trichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 250 220 400 300 280 200 99 95 95 95 104 10 Chloroform NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND 11.1 Vinyl Chloride NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 13 1 ND ND ND ND ND ND —ND ND ND ND ND 1, 1, 1 -Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,1,2-Trichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1, 1 -Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloroethane NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND Trans 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP ND 6.6 ND ND ND ND ND 2.3 2.3 2.3 ND ND Cis 1,2-Dichloroethene NP NP NP NP NP NP NP NP NP NP NP NP NP NP NP 450 410 1,100 810 640 460 260 188 188 188 219 71.1 Trichlorofluoromethane NP. NP. NP NP NP NP Np NP NP NP NP NP NP NP NP ND ND ND ND ND ND ND ND ND ND ND ND 1,2-Dichloropropane NP NP NP P L NP NP NP NP NP NP NP NP NP ND ND ND ND ND I ND ND ND ND Chlorobenzene NP NP NP _�L p Np P NP NP p Np NP NP W NP NP NP NP NP ND 4.2 ND ND ND ND ND 1,4-Dichlorobenzene NP NP NP NP NP NP NP NP Np Np NP NP NP NP ND I— I'D ND ND ND ND 1,1,1,2-Tetrachloroetha-- NP NP NP NP NP NP NP NP NP NP NP ND ND ND ND TOTAL CHLORINATEDS DETECTED I NPI NPI NP I NPI NP I NP I NP I NP I NP I NP I NP I NP I NP I NP I NP 1 3,000 1 1,954 1 3,700 1 3,410 1 3,020 1 2,360 1 1,058 1 1,141 11141 11141 211,111,413 200 ND = Not Detected at the method detection limit. NP = Well not present at time of sampling. RW-7 Prepared by: AWA 1022-32 Andrex Historical Well Tables 201 1.xls Checked by: TJB Total Chlorinated VOC Concentrations in MW-1 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 10,000 9,000 8,000 7,000 6,000 5,000 4,000 3,000 2,000 1,000 0 rn It kr) 00 01� C) — m kr) �O 00 1:? 91 91 91 91 91 1:? 91 91 Month -Year Lai Total Chlorinated VOC Concentrations in MW-2 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 EM 700 ME 500 400 300 200 100 0 ! i i i i i i i i i i i i -i -i -I i i i i i a) Month -Year Total Chlorinated VOC Concentrations in MW-3 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. J10-1022-30 /-U,UUU - 18,000 16,000 14,000 12,000 10,000 8,000 6,000 - 4,000 - 2,000 - o m W) 110 r__ "0 (7� tn 110 rl- 00 1711 I'll Month -Year Total Chlorinated VOC Concentrations in MW-4 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 z'VVV 1,800 1,600 1,400 1,200 1,000 800 600 400 200 0 CA rn I:t kr) 00 rn kn 1:? 91 91 91 91 91 cj III IN I III EMSEP900HEN Month -Year Total Chlorinated VOC Concentrations in MW-5 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 60,000 50,000 40,000 30,000 C-) 20,000 10,000 0 (7\ C) m It tn r- 00 m kr) 00 1�1 91 91 91 91 91 91 91 91 91 Month -Year Total Chlorinated VOC Concentrations in MW-6 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 DU'UUU 45,000 40,000 35,000 30,000 25,000 cd 20,000 15,000 10,000 5,000 0 N fn It tn �10 r__ 00 fn 00 Month -Year Total Chlorinated VOC Concentrations in MW-7 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 Em 160 140 120 100 80 60 E DS 20 0 i i i i i 1-11 i i �i _01 I'll - I i 144 i i i i C) - N m 't Month -Year Total Chlorinated VOC Concentrations in MW-8 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 mm 1,600 1,400 1,200 1,000 800 600 ROTOR K11111 0 ! i i -I- ! V it ! - i i i i i - i I I I I i i i i 01� C) N m It W) �10 1 00 (7� a) N m 't W) �C rl- 00 Month -Year Total Chlorinated VOC Concentrations in MW-8A 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 7,000 6,000 5,000 4,000 ZE 3,000 Lail 2,000 1,000 0 ! i i i i i i i i i i i i i i m� i i i i i i i cl� C) m lzt kf) 00 C� C) — m 1�t kr) 110 r--- 00 C� C) 1�1 91 1:? 91 91 1:? 1:? 1:? 1:? 1:? 91 Month -Year Lei, 7,000 6,000 5,000 4,000 3,000 2,000 1,000 Total Chlorinated VOC Concentrations in MW-9 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 01� C) N It W) 110 1 00 (7� a) N Month -Year Lail Total Chlorinated VOC Concentrations in MW-10 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 14,000 12,000 10,000 8,000 6,000 4,000 2,000 m kn 110 r— 00 cl� C) — m kr) 1�0 00 CN 1� 91 91 91 1:? 1:? 1:? 1:? 91 91 91 U U U U U U U U U U U 0 V 0 0 V 0 V a) a) a) a) a) a) a) a) a) V V 0 Month -Year 6,000 5,000 4,000 3,000 2,000 1,000 Total Chlorinated VOC Concentrations in MW-11 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 01� C) N It W) 110 1 00 (7� a) N Month -Year Lei, Total Chlorinated VOC Concentrations in MW-12 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 8,000 7,000 6,000 5,000 4,000 .3 UUU 2,000 1,000 0 ! i i i i i i i i i i i ;,.� 1 Z—d� i i 1� i i i i (71, C) rq m 't W) �10 1 00 (7� a) N It kn �10 Month -Year Total Chlorinated VOC Concentrations in MW-13 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 8,000 7,000 6,000 5,000 4,000 3,000 2,000 1,000 0 ! i i i i i i i i i i i i i i i i i i i i i i cl� C) — m lzt kr) 00 C� C) — m 1�t kr) 110 r--- 00 C� C) 0? 1�1 1�1 1�1 91 1:? 91 91 1:? 1:? 1:? 1:? 1:? 91 Month -Year Total Chlorinated VOC Concentrations in MW-14 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 M 1,600 1,400 1,200 1,000 800 600 Hirt, KBE 0 ! i i i i i i i i i i i i i i i i i i i i i i 01� C) N It W) 110 1 00 (7� a) N M 't W) 00 C� N Month -Year Lail Total Chlorinated VOC Concentrations in MW-15 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 EM F11111 R11111 500 400 300 200 0 ! i i i i i i i i i i i i i i i i i i i i i (f) r- 00 C) — N M It kn 110 r__ 00 91 91 1:? 1:? 1� 1� 1:? 1� 1� Month -Year Total Chlorinated VOC Concentrations in MW-16 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 500 450 400 350 300 250 200 (_� 150 �111j' 50 0 rq fn It W) �10 rl- 00 C� C) N m 't tn 110 Month -Year 700 600 500 400 ZE 300 Lail �Xflf [OR 0 cl� C) — C� 1�1 C�' Total Chlorinated VOC Concentrations in MW-17 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 m W) 1�0 r11_ 00 C� C) — m lzt kn �O 00 C� C) CA 1:? 91 91 1:? 1:? 1:? 1:? Month -Year Total Chlorinated VOC Concentrations in MW-18 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 300 250 200 150 100 50 0 ! i i i i i i i i i i i i _m� :; -1 29 i C� C) m It kn 00 cl� C) m It W') 00 1� 91 1:? 91 91 91 91 91 Month -Year w 35 30 25 20 15 to 5 Total Chlorinated VOC Concentrations in MW-19 3rd Quarter 1991 - 4th Quarter 2010 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 Month -Year It W) 01� C) Total Chlorinated VOC Concentrations in MW-20 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 0.80 0.70 0.60 0.50 0.40 0.30 0.20 0.10 0.00 41 i i$ i 0 N rn It kr) r__ 00 kr) 11C r 00 cl� 1:? 91 1:? 1:? 91 V V a) a) V 0 a) 0 V V V V 0 Q V V a) Month -Year Total Chlorinated VOC Concentrations in MW-21 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 1.60 11 U11111 1.20 1.00 0.80 0.60 =DA 0.20 0.00 ! i i i i i i i * 6 ! i i \.4i i i i w- i i i 4- I 'almelmalmlF Month-Year Total Chlorinated VOC Concentrations in MW-22 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 1.00 0.90 0.80 0.70 0.60 0.50 0.40 0.30 0.20 0.10 0.00 (71, C) Cq rn 't W) 110 1 00 W) 91 91 110 r__ 00 Month -Year Total Chlorinated VOC Concentrations in MW-23 3rd Quarter 1991 - 4th Quarter 2010 Andrex Industries, Asheville, NC BLE Job No. J10-1022-30 2,000 1,800 1,600 1,400 1,200 1,000 800 600 400 200 0 't W) 110 rl- 00 01� C) �10 Month -Year Total Chlorinated VOC Concentrations in MW-24 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 1,000 900 800 700 600 500 400 300 200 100 0 CIA fn 't tn 110 rl- Oc (01� m 110 Month -Year Lail Total Chlorinated VOC Concentrations in MW-25 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 1,600 1,400 1,200 1,000 800 600 400 200 0 ! i i i i i i i i i i i i i i i i i i i i i i 01� a) Cq m 't W) �10 r__ 00 W) �10 r__ 00 all C) 91 1�1 1�1 91 91 Month -Year 14 12 to 8 6 4 2 (71, C) Total Chlorinated VOC Concentrations in MW-26 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 rq fn It W) �10 1 00 (71, C) rq fn 't kn 110 1 00 C) C) C) C) C) C) C� C� C� C� C� C� C� C) Month -Year Total Chlorinated VOC Concentrations in RW-1 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 60,000 50,000 40,000 30,000 20,000 10,000 0 ! i i i i i i i i i i i i i i i i i i i i i i 01� C) N 't W) 110 1 00 C) It tn 1 00 1:? Month -Year Lail Total Chlorinated VOC Concentrations in RW-2 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 3,500 3,000 2,500 2,000 1,500 1,000 500 0 Cq m It W) 110 r__ 00 W) 110 rl- 00 all C) Month -Year Fill A Total Chlorinated VOC Concentrations in RW-3 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 14,000 12,000 10,000 8,000 6,000 4,000 MILO 0 ! i i i i i i i i i i i i i i i i i i i i i i C" C) m It kr) coo M kr) 00 C� 1:? 91 Month -Year Total Chlorinated VOC Concentrations in RW-4 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 6,000 5,000 4,000 3,000 C-) 2,000 1,000 0 ! i i i i i i i i i i i i i i i i i i i i i i C� C) - N m It kr) 00 C" C) - m It tf) 11C r- 00 C� C) CA 0? 1�1 C�' C�' 91 1:? 91 91 1:? 1:? 1:? 1:? 1:? 91 Month -Year C Total Chlorinated VOC Concentrations in RW-5 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 7,000 6,000 5,000 4,000 3,000 2,000 1,000 0 ! i i i i i i i i i i i i i i i i i i i i i i m It kn 110 rl- 00 't W) 00 01� C) N Month -Year 5,000 4,500 4,000 3,500 3,000 2,500 2,000 1,500 1,000 500 0 Total Chlorinated VOC Concentrations in RW-6 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 C) - N 't I � I I � [101 Month -Year Le Total Chlorinated VOC Concentrations in RW-7 3rd Quarter 1991 - 3rd Quarter 2011 Andrex Industries, Asheville, NC BLE Job No. Jll-1022-32 4,000 3,500 3,000 2,500 2,000 1,500 1,000 500 0 m It kf) 00 cl� C) m kn 00 V V V V V V a) V a) V a) 0 a) 0 a) 0 a) 0 Month -Year