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HomeMy WebLinkAboutWI0100089_Pilot Test Update_20101102ENGINEERING & HYDROGEO L 0 G 231 HAYWOOD STREET. ASHEVILLE, NC 28801 TEL.828.26 1.3350 FAC.828.281.3351 WWW.ALTAMOMTKNVIRONMKNTAL.COM November 2, 2010 Mr. Thomas Slusser Aquifer Protection Section—UIC Program Department of Environment and Natural Resources ;:7j.< 401 Oberlin Road, Suite 150 Raleigh, North Carolina 27605 Subject: Pilot Test Update Tyco Electronics Corporation Ul 1396 Charlotte Highway Fairview, North Carolina Underground Injection Control Permit W10100089 Dear Mr. Slusser, On behalf of Tyco Electronics Corporation (TEC), Altamont Environmental, Inc. (Altamont) has completed the pilot test for in situ chemical oxidation (ISCO) treatment to address contaminated groundwater at the TEC facility, located at 1396 Charlotte Highway in Fairview, North Carolina, as described in the December 23, 2009 Pilot Te5t Work Plan (Work Plan). The pilot test injection process performed satisfactorily and this update is not being made as a permit requirement. Rather, we want to make you aware that we intend to complete additional groundwater monitoring to gatige the dissipation of the permanganate into the soil and groundwater matrix surrounding our injection well. The objective of the ongoing pilot test is to evaluate the efficacy of the sodium permanganate ISCO treatment to reduce source area contaminant mass. The sodium permanganate injection was completed on September 14 and 15, 2010 at the TEC facility, as detailed in the Work Plan and Soofium Permanganate Injection Event Summary submitted to you on October 15, 2010. Four groundwater sampling events were conducted after the injection as follows: • August 11, 2010—pre-injection • September 22, 2010—post-injection (one week after) • October 6, 2010—post-injection (three weeks after) • October 19, 2010—post-injection (five weeks after) The groundwater samples were analyzed for volatile organic compounds (VOCs), select total metals, nitrate, sulfate, chloride, and alkalinity. WN-1-10M The laboratory analytical results will be summarized in a forthcoming report. We are writing this letter today to inform you that five weeks following the injection event, residual sodium P:\TEC\Fairview\Correspondeiice"\Pilot Test-2010\Ltr-DEN R-Pi lot Test Update-10-29-2010-Final. Doc Mr. Slu-sser November 2, 2010 Rag e 2 of 2. permanganate: is still evident in RW_6 pilot test) and RW-7- _(obs&rVation.WelI for the purposes of this (the.injection Well for the purposes of this pilot test.). The excess �s.od_iurn permanganate is.ind.icated by the color ofthe water in. RW'_6 (pink) and RW_7 -(purple). - It appears as tHough.the sodium,- r 'the Well.: permanganate:is moving.slowly out from RW-7, but:a large q'uantity still emains in NEXT STEPS Altamont� proposes to document whether there is a change in color in.RW-'6 and RW-7 every two weeks between now and December 31, 2010, or uri til the color dissipates, whichever occurs first; Gro.undwater will be. placed i . n, clear gl . ass container . s and the . color will be c ompared to containers from each: preceding event. � Water levels and c'olor:samples will also b,e obtained from the,.: .�surrounding monitoring wells used as observation wells during this test (MW-3,..MW-7, M.W-725, MW_ 2:6,-MW-39, MW-40, and MW-41).* the event, a sum.marywill. be An addition to summarizing.the laboratory analytical results from.. submitted after the further colorimetric monitoring has been-com pleted. The summary will.indicate 1: whether the sod itArn perma hganate has dissipated from the injection well. Thank you for -your time and consideration on this -project. Please feel free to call o.rrespond With any questions or comments.' Sincerely, ALTAMONT ENVIRONMENTAL, INC. S_ - Christopher F. ilbert; P.E.. cc: Mr. Glen Foster, Tyco'Elec-tronics Corporation Mr. Bobby Lutfy, Nor-th Carolina Department of Environment and Natural. Resources (DENR), Inactive Hazardous Sites Branch P�\TEC�Fairview\correspo.nden:ce\Pilot Test 2010.\Ltr-DENR-Pilot Test Update-10-29-201.0-Final. Doc. ENGINEERING & HYDROGEOLOG 231 HAYWOOD STREET, ASHEVILLE, NC 2880'i TEL.820.261.3350 FAC.828.281.3351 AR 03 WWW. ALTA NOMTKINIVINON N UNTAL.CON TRANSMITTAL LETTER To: Mr. Thomas Slusser - DENR UIC Program From: Mr. Evan Yurkovich (-t� Date: February 28, 2011 cc: Mr. Landon Davidson - DENR DWQ; Mr. Bobby Lutfy - DENR; Mr. Glen Foster - TEC Subject: TEC-Fairview Sodium Permanganate Injection Pilot Test P:\TEC\Fa i rview\Correspondence\Pi lot Test-2010\Pilot Test Report\tra ns-DEN R-Pi lot Test Report.doc N G I N E E R I N G & H Y D R 0 G E 0 L 0 G Y IRE:CEIVED I UENt"t� 1 O�Va AQUI�;R-Ppo-r�r"Tlm "'MIOK ,MAR 0 3 N11 Sodium Permanganate Injection Pilot Test Report Tyco Electronics Corporation Fairview, North Carolina February 28, 2011 Prepared for Tyco Electronics Corporation P. 0. Box 3608 MS 161-S3 Harrisburg, PA 17105-3608 (717) 986-7916 Prepared by Altamont Environmental, Inc. 231 Haywood Street Asheville, NC 28801 (828) 281-3350 Sodium. Permanganate Injection Pilot Test Report February 28. 12011. --TEC7Fairview Page.1ii Table of. Contents 1.0 Executive Summary.: ........ ................... ...................................... ............................. 2.0:: Background, ......................... ................. ........................................................ ............. 2 :2.1 Site'History ......................................................................................................................... 2 2.2. Pre -injection Hydrogeologic Assumptions ........................ .................... ....................... 3 2.3 Pre -injection Rationale ................... ............................................................................... 4 8..0 New M.Onito r-ing. Wells ..... ............... ........ I ............................................................................ 5. 3.1 Well Construction ................................................................................ ..................... 5 3.2 Lithology .......... E..�; ............... . ............................................... ........ .............. ...... 5 3.3 Drill, Cuttings Management ............................................................................................... 5 3.4 Top of Casing Survey.-.... .......... .......................... ................................................... �6 3.5'. Well Development ............................................................................................................... 6 3.6 Baseline Groundwater Monitoring..� ...................... ...... ............................ ..................... 6 n oor Air Evaluation.... 3.1 1 d ................................................ ............................ ............................... 6 4.0 S6dium:Permanganate Injection .... ...... .............. .............................. : ............................. 7 5.0 Post Injection Groundwater Monitoring.:. .... .............. ............................................ ...... d 4 8 .5.1 Groundwater Sampling .. ............. I ........................................................................................... 8 5.2- Addition.al.,Groundwater Gauging ..................................................................................... 8 5.3. Further Sodium Permanganate Monitoring .......................................... ....................... 8 6.0 Findings ............................. ............ ............. ....................... ................................. 10 6.1 -Groundwater Results .............................................. ................................. ..................... 10 6.1.1 Groundwater Gauging ............................... ........ .................................... 10 .6.1.2. Volatile Organic Compounds ........................ .......................... .......................... 10 6.1.3 Metals ........... w .................................................. .............................................. 1.0 6.1.4 Other Parameters ....... ................. ................ ...................... .......... 6.1.5 Color ................................................................................................................ 11 .6.2 Injection* Results ..... ............................................... ...... ........ ...... ........ ................... 11 7.0-.- Recommendations ................................................................. ...................................... 13 .8.0 References ........... ............................................. ........ .................................................. 1.4 P,\TEC\Fairvie�w\C6rrespondenbe\Pilot Test 2010\Pilot Test Report\Pilot Test Report finalLoc a February 28 2011. Sodium. Permangan. te Injection PilotTe§t Report TEC7Fairview Page iv Figures 1. Site Location 24: Pilot Test Site Plan 3a. Pro Piiot:Test Potentiometric and -Concentration Map' 3b.'Post Pilot Test Potentiometric and Concentration Map .3c. Post:Pilot Test Potentiometric and Concentration Map 4. Time Versus Concentration Graphs' a. MW-39 Trichloroethene b. MW-39 Tetrachloroethene c. MW-40 Trichloroethene d.- RW-06 Trichloroethene e. RW-06 Tetrachloroethene 6: Pilot Te'st-Hydrographs for Pilot Test Monitoring Wells a. September 14,:2010 b. September 15, 2010 Tables 1. Pilot Test Groundwater Elevations Pilot Te s*t Volatile Organic Compound Groundwater Analytical Results 3 Pilot Test Metals Groundwater Analytical Results In 6ters., 4. Pilot Test Water Quality Para 5. Sodium Permanganate Injection Event Summary Append,ices A.' DENR Issuance of Injection Permit dated June 21, 2010 B.: Well Construction Records C.1' Lithology Logs D. Waste Manifests and Analytical Results for Drill Cuttings E. Groundwater Development and.Sampli ng Logs F.: Laboratory Analytical Reports G.:. Photographs P:\TEC\Fairview drrespondende\Pilot Test 2010\Pilot Test Report\P11ot Test Report Fina].Doc \C. Sodium Permanganate Injection Pilot,Td:st Report.. F.ebruary.28, .201-1 TEC7Fairview . Page 1 1-0.�: Executive Summary Altam6nt Environmental, Inc. (Altamont) conducted a sodium permanganate injection pilot test at. the Tyco E.lectronics.Corporation.(TEC) facility locatedat 1396 Charlotte Highway in, Fairview,. North Carolina. The. objective of the:pilot test was to'evaluate-the efficacy of the sodium permanganate in:situ chemical oxidation t to reduce source area contaminant mass so that concentrations in the groundwater at the OSCO) treatmen site are, at'acceptable' levels (that demonstrate- source control). A Pilot Test'Work Plan was submitted by Altamont to the North Carolina, Department of Environment and Natural R-e.sbutc.es.([ . ?ENR), Division.of Waste: Management, SuperfundSection, Inactive Hazardous Site' - Branch (IHSB) on.De cember 23, 2009. The work plan contained the rationale for.ISCO treatment to address the contaminated groundwater at the TEC facility Within. a 30-foot radius of recovery.well RW-07. An underground injection control (UIC) permit application was submitte.d'to.the DENR, in accordance -With 15A N . CA . C:02C.0211, on March 24, 2010. The sodium permanganate injection was approved by the North. Carolina DENR Division of Water Quality (DWQ) UIC Program and the Injection Permit, W10100089, was issued on June 21, 2010. The permit is effective from June 21, 2010 until, May 31, 2012. The. permit is. included.as A ppendix.A. As partofthe pilottest, three additiohal.monitoeing wells. were installed and. baseline groundwater samples were collected. -The sodium perm . angana . te pilot test injection was conducted in September 2010. The - groundwater was monitored during threq.post-injectioa sampling: events. Sodium permanganate continued to exist in recovery well RW-07, so additional groundwater monitoring Was conducted from November 2010 until January 20:L1. Based on theresults of this pilot test, sodium permanganate.still: exists in. the injection well RW-07. Before sodium permanganate injection pilot test study, the any additional conclusions can be drawn. fronthis . exces5sodium permanga.n.ate - remaining in th.ewater column of the recovery well RW-.07 must be addressed. P:\TEC\Fairview\C(irrespondence\Pilot Test 2010\13i lot Test Report\Pilot Test Report: Final:Doc Sodiurn Permanganate Injection Pilot.Test Report. February 28, 2011 TEC-Fairview . Page. 2 2.0�: Background p 2.1..; �Site History. .The Tyco Electronics, Corporation JEC) site (formerly known as Communications:Instruments, Inc.) islocated at 1396 Charlotte Highway (US Route 74), in Fairview, North Carolina (Figure 1). TEC formerly Manufactured relays (electronic and electromechanical switches).:. Currently, the facility is.used for assembly of electronic components. .-Environmental assessment -activities have been performed at the facility since the early 1990s. Based upon. the previous assessments, chlorinated solvents and associated breakdown: products. are present in the groundwater under much of the site at concentrations. above associated: North Carolina groundwater -standards,::as prpmu-Igated in 15A North:Carolina Administrative Code (NCAC) 2L,*.0202.(2L Standards). Descriptions and the locations of the major sources of groundwater contamination are as follows: 1) Aforme'rsolvent disposal area, located in the northwest corner of the TEC.facility 2) Former burn and acid pits located in the northern parking lot 3) . Aformer septic system leach.field adjacent to Cane Creek, in the eastern part of the site, near the current groundwater remediation: building As part of the previous assessments-, 48rhonitoring Wei Is/pi ezo meters -have been installed to measure and I I p predict groundwater flow and. to dete.rmine groundwater quality. Altarnont col.le.cts groundwater samples from selected monitoring wells at the site as part Of semiannual groundwater and surface water monitoring. The most re cent sampling eventwas in Noverhber 2010 (as documented in- Altarnont's Semiannual Progress Report, dated December 23, 2010).i In addition to the -semiannual -monitoring, there is also active groundwater. purn'o-and-tteat remediation p occurring at the site. Six recover 'ells a e I ated on -site. Two clustered extraction wells,� RW-'06 and RW- ..y w oc OT'are located in the northwest corner.of the manufacturing building in the,area:of a former solvent, disposal area. These wells contain the _Mghest concentrations of chlorinated v Ibtile organic compounds (VOCS a n of' n Recovery wells RW-01, RM-02, and R*04.are locited downgradie. t RW-06a dRW-07a'nd...� provide mass.recovery and aid in.reducing� movement of contami.natiorf..off7site. Historically RW-03 has contained the, lowest: concentrations of chlorinated' solvents and is mostly used -for groundwater hydraulic: control.: The impacted groundwater is treated on -site using air stri ping and carbon adsorption techniques. p The-treatedgroundwater is discharged to, theshearby surface water body Cane Creek tinder the 6uthority Of a National Pollution Discharge Elimination System (NPDES) permit. Based upon the information gathered, d 'ring previous groundwater assessment 'and recovery work, Altamont u has -divided groundwater.occurrence into:three categories: (1) the: unconsolidated regolith, (2) the partially weathered bedrock, and (3) the bedrock Zones. The zones are hydraulically connected. At most parts ofthe site, the hydraulic gradient between these zones is upward. Groundwater flow in' all three Zones is approximately southeast. Concentrations:of chlorinated solvents have.been detected ingroundweitersamples collected from all three zone& Concentrations were especially h.igh in:the. area near RW-0.6 and RW,-07.,: During the May-2010. sampling event, two. of the six,of the maxim u m concentrations exceeding the. 2L Standards were detected'in the sample:collected from RW-07. On'the basis of these conditions", TLC evaluated remediation.:technologies that.would complement the -operating pump-a.nd-treat system and. more aggressively address thegroundwater contamination. Altamorit, on behalf of TEC, performed a pilot test 6 d applied an in -situ chemical. oxidation: (ISCO) technology near RW_' 06 and RW-07 to reduce the source area contamination. ISCO uses non-specific -oxidizers that: react rapidly P:\TEC\Fairview orrespondence\Pilot Test 2010\ \C Pilot Test Repo�t\Pilot Test Report Final*Doc Sodium. Permanganate Injection Pildt.Test Report February 28, 2011. TEC-Fairview... Page.3 With u ..(nbt rally.occurring) organic substrates and contaminants in the aquifer environment. The oxidation reactions involve breaking chemical bonds. and removing. electrons. For this pilot test, sodium permanganate Was used, as the ISCO agent.:'Sodiun! permangbriate has been demonstrated to be'effective in oxidizing chlorinated ethenes, such: as the primary contaminants detected in the'groundwate.r at the site. Its effectiveness: in oxidizing non-ethene compounds that have been identified in the groundwater, such as dichlorodifluoroMethane and 1,1,2-tri-chip.rotrifluorpethan.e, Pre less well - documented. I n. prepa ration f6 r th is. pi I ot testi. a work pla n Was su b m itted to M r.. Bo b by Lutfy of the -N o rth Ca ro I i na Department-of.Environment and Natural Resources (DENR), Division of Waste Management, Superfund Section, Inactive Hazardous Sites Branch (IHSB) on December 23, 2009. The work plan provided information on the proposed injection location, the pre-existing groundwater monitoring locations; detected- - grouridwater-quality data from recent sampling, and other site features'l.n the area. ofthe proposed pilot test. Additionallyl �an' Underground Injection Control (U IC) application was submitted.to M r.- Thomas Sluss,er of the DENR, Division of Water Quality, Aquifer. Protection Section, Groundwater Protection Unit on March 22, 2010.- The:UIC.Application provided information onthe injection fluid composition, the injection ratibnalei th'e in -rotection Unit ,,jection, procedure and equipment, and the monitoring plan., The Groundwater P issued UIC permit::WI0100089 on June 21,2010. This report summarizes the following pilottest activities: The instal.lation of new monitoring wells The collection of baseline groundwater samples The collection of indoor air sarnp�es The injection of sodium. permanganate The collection of post -injection groundwater samples .-The evaluation of results and'pr6vision of recommendations Additi-onally,.this report provides recommendations regarding the use of sodium permanganate in oxidizing these compounds and reducing groundwater contamination in the.source area near RW-06 and RW-.07. 2.2 Pre -injection Hydrogeologic Assumptions Regionally: the site is located in the Blue Ridge Physiographib Province. Topogralphically, the site lies just west of Cane Creek near the southern base.of-the Swannan.oa Mountains. The ground surface at the site�.' slopes gently torthe southeast toward the -creek. According to the Bedrock Geologic Map of the:Oteen 7.5- Minute Quadrangle,, North Carolina (Cattanach and Merschat, 2008), the bed rock, u nderlyi ng the site is haracterized as a schistose greywackei part of the Ashe M.etamorphic Suite., The Brevard fault zone, a major:structure:which includes mylonitic and. cataclastic rocks, is.located just east of the site. As introduced in the previous section, groundwater underlying the site is'dividedinitothreP categorJes- (1), unconsolidated regolith, (2) partially weathered. bedrock,, and (3) bedrock zones.: The zones are hydraulically connected.. The:depth to bedrock atthe site ranges from approximately 6 to 85 feet below -ground surface (bgs),: At the Iodation of the pilot test, the depth to bedrock is approximbteIV 60 f6et-bgS. The unconsolidated soils:are commonly silty. clayey fine- sands to.sandy silts with: clay'. Oenerally,the permeability and grain size increases:in the regolith, present as saprolite in the. pilot test area, and partially: weathered rockvith depth. The bedrock:is variablyfra6t ured. The frequendy of the fractures tends to decrease with -depth below the top of bedrock. P:\TEC.\Fairview\Cbrrespondence\Pilot Test 2010\Pilot Test Report\Pilot Test Report Final.Doc Sodium Permanganate Injection PilotTest Report February 28, 2011 TEC-Fairview Page 4 On the basis of aquifer tests (pumping and step drawdown tests) pbrformed in 1994, hydraulic conductivities are estimated to range from 2,to 4 feet per day (feet/day)-for the saprolite, 6 to 10 feet/day for the partially weathered rock (transition zone), and 0.001 to 10 feet/day in the bedrock (Aquifer Pumping Test Report, General Instrument Corporation Hatboro, Pennsylvania and Communication Instruments, Inc. - Fairview, North.Carolina, RETEC, January:1995). The Water table at the site was measured in November 2010 to range from just a few feet below grade to 33 feet-bgs. in general,. groundwater flows -southeasterly toward Cane Creek, however on a more localized scale groundwater appears to flow radially from a southwest to southeast direction mimicking topography. 2.3 Pre -injection Rationale As described in - Principles and Practices of In Situ Chemical Oxidation Using Permanganate (Siegrist and others, 2001),permanganate oxidizes chlorinated solvents through a hydroxylati,oh process. Site contaminants, such'as chlorinated s . olv . e . nts, b I rea k: down ultimately to carbon dioxide, chlorine, hydroxides, water, -and metals. Permanganate reactions can reduce pH, increase reduction potential (Eh), reduce natural oxygen demand, and increase ion concentrations. The objective of the pilottest Was to:evaluate the efficacy of the sodium permanganate ISCO treatmentto-. reduce source area contaminant mass. - A pilot test site plan is included as Figure 2. The target.depth zone of the pilot.test was 30 to. 50 feet-bgs, which encompasses the lower uncorisolidated.regolith. The area of influence of the pilot test was anticipated to extend about 20 feet radially from the injection well RW-07.. The proposed injectant volume and concentration: Was based on the hydraulic properties of the aquifer and the permanganate natural oxidant demand (PNOD) of the soils in -the areasfrom the target depth interval. The, hydraulic.propert . ies of the aquifer were estimated from field tests and.the PNOD was obtained from a laboratory test performed by Carus Corp bration (see the UIC permit application). The PNOD test indicated that the amount of excess sodium permanganate.(NaMn04) needed to satisfy the naturally occurring demand was relatively low. Part of the::ration.ale behind the pilot test:was that if the results demonstrated that the ISCO treatment would be effective, thedata from the pilot test:would. be:used to design a full-scale source area treatment system. P:\TEC\Fairview\Cbrrespondenbe\Pilot Test 2010\1311ot Test Report\Pilot Test Reporl:—Final.Doc Sodium Pbrmanganate Injection Pilot.Test Report.: TEC-Fairview . 3.0:. New Monitoring Wells February 28, 2011. Page 5 On July 27, 2010, Altamont contracted Geologic Exploration, Inc. (Geo.logic) of Statesville, -North Carolina, a wells near RW-06 and RW-07, in orderto evaluate the. licensed Well driller,lo install three moni effectiveness of the sodium permanganate to degrade the contaminants within the source area . . The wells were designated. as MW-3.9, MW-40, and: MW-41 and located west, northwest, and northeast of the injection well RW-07, respectively. Well locations. are shown on Figure 2. 3A Well Construction The monitoring wells were installed using a 4.25-inch inside diameter:and e.ight-inch outside diameter hollow: stem augers. The wells were constructed of two�inch diameter O..02-inch sIot polyvinyl chloride (PVC) screen installed to bracket the water table. The.screen was connected to a tW6_inch diameter PVC riser and: . installed in the borehole to about six.inbhes below the ground surface. Sand was placed in the borehole annu.lus to Pne.foot above the screen, followed by one foot of hydrated ' ben ' tonite, with neat cement grout to the ground surface. The surface completiona were enclosed within a flush mount six-inch manhole. The water table monitoring wells were completed as follows: MW-39:: total depth of 50 feet below 'round surface (feet-bgs), twenty -foot screen located between 9 30to 50 feet-bgs MW-40: total depth of 5 1 feet-bgs, twenty -foot screen located between. 31 to 51 feet-bgs MW-41- total: depth of 49 ft-bgs, twefity-fo6t sc.reen located between 29 to 49 ft-bgs. Well construction details are described on the:Well Construction Records included as Appendix B. 362.:: Lithology Soils encountered during well.construction consisted'mostly of moist orange red:sandy silt to silty clay materials. Bedrock was not encountered: during the water table well installations. Based on well records of RW-06, bedrock is located at approximately 60 feet-bgs. The soils that were enco.untered are consistent: with the pro -test assumptions that are discussed in Section 2.2. Lithology is described- in more detail in the Litholdgic Logs included as Appendix. C.: 3.3� Drill Cuttings Management: Throughout drilling, drill cuttingsand IDW were transferred into 55-gallon,drums.. The solid drill cuttings, were allowed to settle.. The supernatant (groundwater and drilling fluid) from the cuttings were decanted: and disposed -through the groundwater -treatment system. Representative soil'samples were collected from the drums for each of the new:monit.oring wells on:August 31, 2010 and analyzed for chlorinated VOCs method 8260/5035A, in accordance with the North Carolina -in"guidance document: (North Carolina,Ha2ardous Waste Section 2005). -.contained Based on the analytical results from.the: drum.sampling, seven drums:were designated as. non -hazardous, and the contents were disposed of -properly at the Herita- go Subtitle D landfill in Charlotte, North Carolina.. Since the results from the,other four drums contained VOC concentrations over the North Carolina Hazaedous Waste Section's "contained -in" Policy for Soil Contaminated with. Listed.Hazardous Waste levels fo r d1sposa 1, th e. co rite nts.h ad to be, prope rly. d isposed of at th e H eritage S u btitl e- C [a ndfi I I i n East Live rpoo 1, Ohio. The drill butting- analytical results and Waste manifestsare included as Appenclix D. P:\TEC\Fairview\Cdrrespondenbe\Pilot Test 2010\Pilot Test Report\Pilot Test Report final.Doc Sodium- Permanganate Injection Pilot Test Report.. February 28-, 2011 TEC-Fairview Page:6 374 Top of: Casing Survey On Ja nuary 25, 201�, the elevation and loca tion. of the top of ground -surface and top of well casings were� surveyed. by a licensed North. Carolina land surveyor, Wes Cole Land Surveying, PA of Asheville, North Carolina. The surveywas:used to determine the groundwater elevations associated With the monitoring Well sample collection and analysis. -The groundwater elevations associated with the sampling events are summarized on Table 1. W0.11 Development The monitoring wells were developed on July 30, 2010 by pumping,at,least five. well volumes usinga battery .operated Proactive purge pump. The wells were pumped until turbidity readings decreased to approximately 50 nephelometric tubidity units (NTUs). More information is described in the well development logs included in Appendix E. The development water was containerized and transported to the on -site groundwater remediation system:fortrebtment and disposal. 3.6. Baseline. Groundwater Monitoring:-: On August 11,.2010, Altamont collected baseline groundwater elevations and samples from MW-39, MW-: 40, MW-41,..RW-06, and RW-07. Samples from the monitoring wells were purged using low -flow techniques (US Environmental Protection Agency [EPA] 1996).: During purging, the pH, specific conductivity, dissolved oxygen, oxiclation�reduction potential (ORP), turbidity, and temperature Were- measured and recorded every: three: -Minutes.-- Well purging continued until these parameters stabilized (three successive readings in which pH 0.1 unit-, specific conductivity 8:percent; temperature, idissolved.oxygen:and turbidity 10: . . percent; and ORP 10 millivolts). 'Sam ples collected from the recovery wells Were obtained using the dedicated' electric submersible pumps and the sample port on the effluent line.: Well sampling logs are included in:Appendix:E. After purging, groundwater samples were collected, transferred to sample contaihers,:placed in a cooler on ice, and delivered to Pace Analytical Services in: Asheville, North Carolina (Pace):for analysis. Samples were analyzed for the following parameters - Volatile organic compounds (VOCs) using EPA Method 8260 Select total metals (lead, chromium arsenic, zinc, cadmium, copper and:merpury) using EPAMethod 6010/7000 ... ... Nitrate.sulfate, and chloride using EPA,Method 300 (ion chromatograph Y) Alkalinity using EPA Method.310.1, SM 232'013 The groundwater elevations, analytical results, and"field parameters are summarized on Tables 1, 2, 3 and. tidbl:repprt and chain -of -custody form are included i 4, respectively.: the: laboratory analy'' n Appendix F. 3.1 IndoorAirEvaluation 0 u -2011, Altamont screened the indoor air quality within the northwest part of the manufacturing n A gust 11, building with an organic vapor analyzer (QVA).. Abackground-air reading was collected near the entrance:to the TEC facility prior to collecting the indoor air readings. Reaclings� were obtained from within the room Where RW-06.and RW-07.are located -and at the recovery wellheads. 'No detections: of VOCS were detected with the OVA in any of the locationsscreened. P:\TEC.\Fairv!eW\Cdrrespondence\Pilot Test 2010\13i lot Test Report\Pi lot Test Report: Final. Doc r Sodium Permanganbte Injection Pilot.Test Report. February 28, 2011 TEC-Fairview Page 7 4.0: Sodium Permanganate Injection Altamont contracted AE Drilling Services, LLC (AE Drilling) of Greenville, South Carolina,.a licensed well driller., to conduct the sodium permanganate irijection.on September J-4 and 15, 2010. The injection event issurnmarized in more detail on Table 5. Based on the results from the PNOD tests, described in Section 2.3, Altamont ordered and injected 2,2W . pounds (4 drums) of Re.mOx@ L ISCO reagent_,(CAS# 10101-50-5), 40% sod.iUM:permanganate. The shipped concentration of approximately 40% was diluted to:a 10% solution using a.500-gbllon in -line high density,: polyethylene (HDPE).mixer/tank. The solution. wasAiluted by- using water from.the TEC facility from the municipal.waters em. A manifold and: pressurerelease valve were installed downstrearn of the mixing Vst tank in order to -allow for* release of the solution if the pressure were tobeconne'too great. in order to perform the injection, Altamont and AE Drilling installed a single packer around 30 ft-bgs, just above1hescreehed interval in:the injection well RW-07. A one -and -a -half -inch galvanized steel pipe extended'from the top of the packer to 6 pressure gauge ands'ampling.port at the wellhead. Thediluted.: solution was pumped under pressure into RW-07 into the educator pipe and forced through the screened interval into the formation material. The sodium permanganate injection began on.-Septemb.er:14, 2010 with five'separate injections being performe& The injection concluded on September-16, 2010-with another four separate injections. The i-niections consisted of diluted batch.es.of the 10% solution over approximately 1 to 2: hour periods. The tota I Volume.of.the 10% solution pumped into the subsurface through RW-07 was gallo'ns. P:\TEC.\Fa i rview\Corres po n den ce\Pi lot Test-2010\Pilot Test Report\Pilot Test Report —Final, Doc Sodium Pe'rmanpriate Injection Pildt,Test Report., TEC-Fairview February 28, 2011, Page.8. 5..0 Post 10jection Groundwater Monitoring 5.1 Groundwater Sampling. Altamont conducted three post -injection gro.u. ndwat.er. Monitoring events,on, September 22, 201Q, October 6, 2010,:and:'October 19, 2010 (Which are*bne week, three weeks, and five weeksafter thesodiurn permanganate injection was performed, respectively). Groundwater elevations and samples were collected from MW-39, MW40, MW-41., RW-06, and RW-07.. Samples from the monitoring wells were purged using low -flow techniques (EPA.1996). During purging, the OH, specific conductivity, dissolved oxygen, oxidation-reduction potential (ORP),.turbidity, and temperature were measured::and recorded every:lhree -minutes.: WeIJ purging dontinued.until these parameters stabilized (three successive readings in which pH 0.1 unit;.specific conductivity +/- 3 percent; temperature, dissolved oxygen, and turbidity 10 percent --.and ORP-+/- 10 millivolts). Well sampling logs are included. in Appendix E. amples were not collected from RW-07 on October 6,2010 due to the presence.of.excess.sodium permanganate in the groundwater in ' dicated bya very dark purplecolor. The discoloration was observed during all of the'sa,m-pling events in RW-07. The preseh ce of excess sodium permangqnate likely indicates: the absence of VOCs in the groundwater within the well: A pink color was also observed in the groundwater collected from RW-06-during the October. 6 and 22, 201-0 sampling events.' How.ever, samples from RW-06 Were still submitted for.laboratory analysis. After.purging, groundwater samples were:collectedi transferred -to: sample oontainersi: placed in a cooler on ice, and deliver,ed to Pace Analytical Services.:in Asheville, North Carolina (Pace) fbra..halysis. Samples were. a nalyzed for the:follo'wing parameters: Volatile organic comp6unds:(VOCs) using EPA Method 8260 Select -total metals (lead, chromium, arsenic, zi nc, cadmium, copper, and-Mercury).using EPA Method 6010/7000.: NitraW,-�sulfate, and chloride using EPA Method 300 (ion chromatography) Alkalinity using EPA Method 310.1, SM 2320B The groundwater elevations and analytical results:are summarized on -Table: 1, 2, ancl-3, respectively. Th e laboratory analytical reports and chain -of -custody forms are included in Appendix. F. 5.2 :'Additional: Groundwater Gauging As:described in the preceding sections, the groundwater elevation was gauged in the. recovery wells and Monitoring wells (RW-06, RW-07, MW-03, MW-17,- MW-25, MW-26, and the three newly installed monitoring wells MW-39 through MW-4:1):,as part' of the pre- and po.st-injection groundwater sampling events. The groundwater elevations are summarized on Table 1. 5.3 fukther.Sodium Permangonate*-.Monitoring Since:excess sodium permanganate was'detected in RW-07 duringthe final post -injection groundwater mon itori ng: event, Altbmont provided,Mr.:Thomas Slusser of the North Carolina DENR Aquifer Protection Section, ' Groundwater Protection Unit, UIC Program, a Pilot Test Update letter ' dated November 2, 2010. The letter.hotified tK 0 DENR that Altamo nt would further, investigate th e excess sodium permanganate by documenting changes'in'color in samples collected from RW-06 and RW-07. P:\TEC\Fa i rvi eW\Cd rrespo nd en be\P! lot Test-2010\Pilot Test Report\Pilot Test Report :Final,Doc Sodium Permanganate Injection Pilot Test Report February 28, 2011 TEC-Fairview Page.9 On Nove Mber 1-0, 2010, November.2 3, 2010, December 9, 2010, and January 5, 2011, Altamont collected groun dwater samples from RW-06 and RW-07. The samples were collected fromAhe top portion of the water column using a disposable polyethylene bailer and:'placed into a one -quart Mason jar. Groundwater. elevations were . also: obtained from the two red.overy wells and MW-03, MW-17,.MW-25, and MW-26., which are shown on Table 1. The groundWat er samples that were collected were compared to each other from Week to week.. The:water obtained from RW-07 during each monitoring eve n-t continued to have -a very dark purple color and did not - show any change in color. The water obtained from RW-06 was relatively clear and contained no obvious. signs of sodium permanganate. P:\jEC\Fairview\Cdrrespondence\Pilot Test 2010\Pi lot Test Report\Pilot Test Report :Fi naL Doc Sodium P6rmanganate Injection Pilot Test Report February 28, 2011 TEC-Fairview Page 10 6.0 Findings 6 Groundwater Results Four ground . wat I er sampling events7were conducted as part of the sodium permanganate injection pilot test on the monitoring wells within the vicinity of the source area. Monitoring wells -MW-39,_ MW-40, MW-41, RW- 06, an - d RW-07 were"sampled on August 11, 2010 (one week prior to the injection), September 22, 2010. (one W eek afterlhe injection), October 6, 2010 (three weeks after the injection), and bc'tober 19, 2010 (fi . ve weeks after the injection). Analytical results are summarized on Tables 2 and 3.:, q 6.1.1 -'Groundwater Gauging As described in the preceding sections, the groundwater elevation was.gauged in the recovery wells (RW-0.6 and RW-07) and� monitoring wells (MW-03, MW-.17:, MW-2.5, MW-26, and the three newly installed. monitoring wells MW-39 through. M.W-41) as part of the.pre- and post -injection groundwater sampling events. The groundwater elevations are summarized on Table 1., fhere.was'very little change in �groundwater elevations between the puging:events. The water table appears to slightly d ecrease from the September 22, 2010 event to the October 6, 2010 event,. and then. slightly increase in the October 19, 2010 event in the Wells. 6.1.2 YolatileDr&nic Compounds The pre -injection groundwater samples were collected on August 11, 2010.1 The analytical results indicated volatile organic compourids (VOCs), tetrachlbroethene, toluene, -1,1,1-trichloroethane, and trichloroet.hene, exceeding their respective 2L Standard. in mbn.ito.ring wells MW-39 and MW-4.0, and recovery wells RW-06- and RW-07. Monitoring well MW-41 did not contain any detections of VOCs::over the 2L Standard during this event: The -new monitoring well MW39 installed West of RW-07, contairied -a relatively high.detection of. trichloroethene at 156,000 micrograms per liter-(pg/L) during this initial event.... The. post -injection samples collected in September andOctober 2010:contained lower concentrations of..� VOCS'thanin the initial sampling event.in August 2010.� Concentrations of VOCs in RWO - 7 Were not detected above laboratory reporting limits during the lJost-injection sampling. This was predictable given the excess sodium� permanganate in the groundwater sample as indicated by the:deep purple. color.. The concentrations detected in: samples collected from:MW-39 of'tetrachlotoethene, toluene, l-,1,1-trichldroethane trichl.oroethene'exceeded the 2.L Standard: and remained relatively constant throughout the sampling events. The changes in concentrations are shown on the p re and post Pilot Test potentiometric.and concentration-... mapsaincluded cis Figures:3a, 3b, and 3d and on the "Time Versus Cohcentrbtion" graphs included as Figures 4a through 46. The sodium' ct ears to have affected the recovery wells,by permangbriate inje ion app decreasing the VOC.concentrations,whereas the new monitoring well concentrations remained relatively constant, throughout the event indicating that the -$odium permanganate has not reached -those wells. 6.1.3 Metals Recovery well RW-06 contained detections of.arsenic and lead over their respective 2L Standard in the pre - in . ection groundwater analytical results. The ost-lojebtlon results indicated a decre ase in concentrations of P arsenic, lead, and zinc, below the 2L Standard. Chromium was detected over the 2L'Standard in the, October 6 and 19, 2010:sam pl ingresu Its. Pre -injection metal concentrations Were not detected in: recovery well RW-07. The September 22, 2010 results contained arsenic, chromium, mercury and lead detected. over their. respective 2L Standard, but. - showed concentrations decrease throughout the rest of the post -injection monitoring events. P,\TEC\Fa 1 rview\Correspon den ce\Pi lot Test 2010\Pilot Test Report\Pilot Test Report Final.Doc Sodium Permanganate Injection Pilot Test Report February 28, 2011 TEC-Fairview Page 11 Monitoring wells MW-39, MW-40, and MW-41:contained analytical results that stayed relatively constant throughout -the, pre- and post -injection sampling events. MW-39 contained cadmium, chromium, and lead concentrations over their respective 2L Standards,:and both MW-40 and MW-41:had only detections of chromium over the 2L Standard during the sampling events. Even thoug . h t . he mon I ito . ring wells contained metal con . c . entrations over their respective 2L Standard, the cbricbritrations: do not pos,e a risk to. human. health.. Explanation of the. metal concentrations is'discussed in Section 6.2. 6.1.4 Other Parameters Detection - s of alkalinity and nitrate were detected in all of the pilot test injection monitoring wells but below their 2L Standard.'Concentrations were'relativel consistent in MW-39, MW-40, MW741, and RW-06,. y whereas alkalin . ity concentrations detected in�.RW-07 increased. Chloride was detected in RW-06 but was below the 2L Standard. The rest of the monitoring�' ells did not contain other detections. 6.1.5 Color throughout the groundwater monitoring -events, the groundwater in the monitoring wells MW-39, MW-40, and MW-41 remained constant with'high tu rbidity- read i ngs and orange -brown colorations.- The groundwater in R*06 was clear in the pre-inje I ction event,and then . contained a pink coloration during the post -injection sampling events. The color of the groundwater in RW-07.was clear in the pre -injection. events and then contained a dark purple color throughout the post -injection monitoring events. A photograph is included in Appendix G. demonstrating the coloration in RW-07.: 6.2 Injebtion Results Based on thepost-injectio I n groundwater monitoring sampling eve nts and fufther-inve,6,tigation. conducted from November 201b to January 2011, sodium permanganate still exists within RW�07. Some of the sodium permanganate that was injected, remains Within 'the water column of the� recovery Well and has not dissipated into the aquifer. Groundwater observed in RW-06 contained a pink coloration during thp.0o,,4-injection sampling events but was clear during thefurther sodiumpermanganate . monitoring. This difference in coloration could be due to the fact that the.groundwater sample:was collected at 50 feet bgs and the further monitoring samples were. collected frbrh'the top of the water colurrin. The pink coloration during the sampling does indicate that the sodium permanganatd has reached the well. there was very little: change in groundwater elevations between the pre- andpost injection gauging events.. Hydrog-raphs presenting the elevations for the Pilot:Test monitoring wells MW-3, MW-39, MW-40, and MW-41 are included as Figure 5a and 5b. Based on the analytical results during the post -injection sampling events for RW._06 and RW-07, the VOC groundwater concentrations have been d.ecrebs6d.by.the sodium perrhangphate., The groundwater concentrations in the monitoring wells MW-39, MW- . 40, and MW-41 did n ot. chang e during the post -injection sampling events indicating that the sodium permanganate has not reached those wells yet. Meta Lconcentrations in the mo.n itoring -wells. remained relatively constantfrorn'the baseline sampling event and throughout:the post injection events.- The metals that were detected in:the groundwater samples are known to.occur naturally within the soils in this region of North Carolina. Based upon Altamont's i : nterpretation of the color -coded surface- map'published in the United States Geological Survey Professional I Paper. 1648, Geochemical Landscapes of the: Conterminous United States.- New Map Presentations for 22 Elements (USGS Professional Paper:1648), naturally occurring -metals such as arsenic, chromium, copper, mercury,- lead, and zinc occur withinvestern North.' Carolina.. P:\TEC\Fairview\Correspondende\Pilot Test 2010\Pilot Test Report\Pilot Test Report—Final.Doc Sodium- Permanganate Injection PilotTest Report February 28, 2011. TEG-Fairview . Page 12 Metals concentrations in samples collected frorn RW-06 and RW-07 increased abovegroundwater quality. -07 and standards fo.Ilowing injection (Table:3). Perm a nga nate.was introduced directly into RW permanganate Was observed in RW-06. The observed concentrations of metals detected. in samples collected from RW-06 and RW-'07 may have been, caused. by metal impurities present in the perman ganate solution or by:changes in the mobility of metals. Regarding the mobility of metals, as can be seen on Table 4, the: pH did not decrease following injection of permariganate (a decrease in pH -can mobilize metals). Although- the injection of. permanganate temporarily increased the oxid.ation:reduction:potential (ORP) of the groundwater (an increase in ORP can -mobilize metals), the oxidation. reduction potential will decrease as the. permanganate is consumed during the conversion of VOCs to.innocuous products. Eventually, the ORP Will reach its lowest, stable, natura.lstate (pre-injectionstate). Regardless of the cause, we propose to monitor tfie metals- concentrations in these wells:to confirm the expected decrease overtime. P:\TEC\Fairview\C6rrespondence\Pi lot Test 2010\Pilot Test Report\Pilot Test Report final.Doc Sodium Permanganate Injection Pilot.Test Report February 28, 2011 TEC717airview Page 13 7.0 Recommendations Before any add . itional conclusions can be drawn from this.sodium permanganatb injecti.ori.:pilot test study,- p the -excess sod! u m- permanganate,remaining in the water column of the recovery. well RW-07 must be addressed. 'Factors that may be affectingthe sodium permanganate dissipation include: Low permanganate natural oxidant demand (PNOD) and lack of depletion of the oxidant dose Permeability loss due to ISCO-induced particle -generation (e.g. manganese dioxide [Mn021), pore filling of the surrounding formation and well filter pack, and stagnation of theioxidant within the Water colum n* of RW-07 The sodium perma riganate that remains within the water column of RW-07.needs to be investigated further to.,determine if:its presence is indicative of. conditions both within the well and withinAhe surrounding aquifer or if the permanganate exists only within.:the watercolumn of RW-07 due to occlusion:of the well filter pack. Altamont recommends agitation of the water within the well and removal of at least three well volumes from RW-*07. If agitation and groundwater remoVals-prove. difficult then filter pack. may be heavily occluded and. well redevelopment may be necessary. If the agitation �and removal of the groundwater can be completed U' Ity and the purple color does -not persist; then the remaining�sodium permanganate was witho t much difficu -likely due to temporary filter pack occlusion. If the agitation- and removal ofthe groundwater can be completed Without much difficulty and the purple color persists following removal ofat least three, well volumes, that would.likely indicate thatthe sodium: -permanganate is -present within the surrounding aqu'ifer and that the excess permanganatb is. most probably due to a lower7than-measured PNOD. If the PNOD was underestit'nated, then the remaining sodium permangariatb should be moved into the surrounding aquifer by additional measures. To move the remain.ing sodium permanganat6 into the surrounding aquifer, Altamont recommends pumping groun.dwaterfrom RW.-07 into MW-39. MW-39 will be -converted from an observation Well into an injection well., . Groundwater from RW-07 will be transferred into:MW-39 using the recovery, well pump in RW-07. The pump,in.RW-07 is equipped with a variable frequency drive and totalizing metet to control -and measure flow. The pump:.is constructed of stainless steel. Other -materials (e.g. discharge pipe) will be reviewed to dete . rmine compatibility with sadium permanganate. incompatible materials will be� replaced with cbmpatible-materials..-7he well�constructibn record for:MW-39 is included'in Appendix B. MW-39 and.RW-07 have approximately the same total depth. Altamont estimate's that the hydraulic conductivity associated with.the soil around these wells is similar. This is based upon a comparison betw.een.the recharge rates recorded on ' the low-flbw sampling!bgs for the wells'(seO Appendix Q. Although the hydraulic conductivities around these wells are similar,: RW-07 is.a 6-inch diameter- well and MW-391s a-2-inch diameter. well.. r i. Altamo.nt -estimates that the rate at which MW-3 9.will acceptfluid without groundwater moundin ' g will be lower -than the rate at which RW-07 accepts fluid. Given the approximately 2 gallon- per minute (gpm) inject. ion rate associated with RW-07 during the pilot test, Altamont estimates an -approximately 0.5 gpm injection rate for.MW-39 (this will be confirmed in the fiel,d). If the purple color -persists in the groundwater in RW-07 following agitation and groundwater removal, Altamont anticipates pumping groundwater at a rate.of about 0.5 gpm from RW-07 into MW-39 Using the existing pump. Untilthe pi . I ot test i s . completed recovery: . wells'RW- . 06 and RW-07 will'remain off-I.ine from the groundwater. remediation system. P:\TEC\Fairview\Cbrrespondence\PilotTest-2010\Pilot Test Report\Pilot Test Report final.Doc Sodium. Permanganbte Injection Pilot Test Report February 28, 2011. TEC-Fairview Page 14 8.01 Refere'nces Altamont Environmental, Inc. August 10, 2000.- Semiannual Progress Report, Tyco Electronics Corporation:, Fairview, North Carolina. Altamont Environmental, Inc. December: 23Y200 . 9. Pilot-T . est Work Plan, Tyco Electronics Corporatio n, Fairview- North Carolina. Alta mont. Envi ronmenta 1, Inc. March 22,2010. Underground Injection -Control (UIC) application, Tyco Electronics Corporation, FairvieW, North. Carolina.. North: C'aroli.na:Department of Environment and Natural, Resources, Division of Water Quality, Groundwater Protection Urilt.'June 21, 2010..::UIC permit W10100089. Cattahach,:B.L." . and Merchat, C.E. 200&. Bedrock Geologic Map of theOteen 7.57Minute Quadrangle, North Carolina, Cattanach. RETEC. January 1995. Aquifer Pumping Test.Report, General Instrument Corporation Hatboro, Pennsylvania., and -Co rmun:ication Instruments, Inc.: Fairview, North Carolina.. Siegrist, R1., Urynowicz, M.A.,West, O.R., Crimi, M.-L., and Lowe, K.S., 2001.� Pri,nciples,and Practices of In Situ Chemical Oxidation Using Permanganate. Battelle Press, Columbus,- Ohio.: North Carolina Hazardous Waste Sectiom May. 20i 2005. "C . on I tained-in" Policy.f or Soil Conta minated with -1isted Hazardous Waste. United States Environmental Protection Agency (EPA)., April 1996. Low -Flow (Minimal Drawdown) Ground - Water Sampling Procedures. United States Geological Survey (USGS) Professional Paper 1648, Geochemical Landscapes of the Conterminous'Uhited States - New Map.PrOseht.ations for 22 Elements.. P:\TEC\Fairview\Correspondence\Pi lot Test 2010\Pilot Test Report\Pilot Test Report-H nal. Doc S38noij Q';VV qV. v� i7a. Site Location C8 eek 'Vr- 17 % 14 A KW P99 r , 21 j 8 e r4' 0. Y, USGS Topo Map: Oteen Quadrangle 1962 Revised:1990 0 Created AI,TAMONT FNVIRONMFNTAI.. I\C. SITE LOCATION MAP FIGURE 50 COLLEGE SMEEr, ASHEVILLE, NC 28801 Tel. 929.281.3350 F=. 828 281.3351 TEC-FAIRVIEW 1396 CHARLOTTE HIGHWAY DRAWN BY: EVAN YLIRKOVICH SCALE BUNCOMBE COUNTY, NORTH CAROLINA PROJECT MANAGER: CHRIS GILBERT 0 1,000 2,000 CLIENT: TEC MMMMMMMMME====== Feet DATE: 1/7/08 P:\TEC\Fairview1F1gures\G1S\Sfte Location MW-17 I SITE MAP SOURCES: TIGHE & BOND - SITE BUILDINGS, PROPERTY LINES, AND PARKING ARE4S FROM SITE PLAN DATED JUNE 22, 2006 PETIT PROFESSIONAL SERVICES - MONITORING WELL AND RECOVERY WELL LOCATIONS FROM SURVEY DATA RECEIVED FEBRUARY 19, 2008 WES COLE SURVEY - A40NITORING WELLS FROM SURVEY DATA RECEIVED JANUARY 31, 2011 BUNCOMBE COUNTY GIS - OFFSITE PROPERTY BOUNDARIES, ACCESSED JANUARY 2008 mw-26% MW-25 MW-40j MW4 DATE ,MW-3 DESCRIPTION I a *�W-41 S13-011) m LEGEND MW--3 WATER TABLE MONITORING WELL MW-17 DEEP REGOLITH MONITORING WELL MW-26 BEDROCK MONITORING WELL RW-I GROUNDWATER RECOVERY WELL RW-7 GROUNDWATER RECOVERY WELL USED AS AN INJECTION WELL F- ENGINEERING & HYDROGEOLOG-Y---] 231 HAYWOOD STREET, ASHEYILLE, NC 28801 TEL. 828. 281. 33 50 FAC . 828 .28 1.335 1 W W W . A L T A M 0 N I E N V I R 0 N M E N T A L . C Q H DRAWN BY: EVAN YURKOVICH PROJECT MANAGER: CHRIS GILBERT SCALE(FEET) CLIENT: TEC-FAIRVIEW 20 0 20 DATE: 02/09/2011 Is PILOT TEST SITE PLAN I FIGURE � TEC - FAIRVIEW 1396 CHARLOTTE HIGHWAY 2 BUNCOMBE COUNTY, 40 NORTH CAROLINA a P � \TE C \F AIRV I EW\ F IGURES\CAD\P I LOTTEST\P I LOTTESTS I TEPLAN lim 99 m me lem MW-17 MW-26() @MW-25 1. SITE AW SOURCES. WHE & BOND - SITE BUILDINGS, PROPEIM LNM AND PARKING AREAS FROM SfX PLAN D4MD JUNE 22, 2006 PEW PROFMAONAL SDMCES - MONITORING AND RECOV� WEU LOCATIONS FROM SURWY DATA RECEMD FE9RUARY 19, 2" On COLE SUR16EY - MONITORING KELL LOa4ZOAS FROM SURWY D41A RECEIVED "AAARY 311, 20?0 BUNCOMBE COUNTY GIS - OFTSITE PROPERTY BOUNDARIES ACCESSED JANU4RY 2008 2. ABBRE144710AIS, PCE - 7EMCHLOROETHEAE, WE - 7RICHLOROEDEME, A19A - MICROGRAMS PER LITER J. GROUNDWATER D"ATIONS KRE OBTAINED ON SEPTEMBER 14, 2010 AND ANALYTCAL RESULTS FROM THE PRE MEC77ON 84SEVNE SAMPL11W CONDUCTED ON AUGUST 11, 2010. IPCE: 1,720 kG/L TCE: 156,000 IJG/Li DATE PCE: < 2.0 PG/ TCE: 11.1 WG/L PCE: < 1.0 PG/L t,MW-40 TICE 2.0 MG/L� (2263.14) (22 53Y�F_%�_ 4 \ 5, 1 If. ��t A' V`\ (2258.'9"1) I MW-41 (2263.45) DESCRIPTION 6V49) m, JPCE: 44.7 PG/L N----tTCE-. 466 PG/L RW-6 PCE: 139 pG/L TCE: 6,470 OG/L 23 1 H A YWOOD S TREET, ASHEVILLE , N C 28 80 1 TEL. 828. 281 .3350 FAC - 828.281- 3351 W W W . A L T A H 0 N T E N � I R 0 N M E N T A L . C 0 M DRAWN BY: EVAN YURKOVICH PROJECT MANAGER: CHRIS GILBERT SCALE(FEET) CLIENT: TEC-FAIRVIEW 10 0 10 DATE: 02/24/2011 LEGEND MW­3 WATER TABLE MONITORING WELL lfW— 17 DEEP REGOLITH MONITORING WELL MW-26 13EDROCK MONITORING WELL RW-6 GROUNDWATER RECOVERY WELL RW-7 GROUNDWATER RECOVERY WELL USED AS AN INJECTION WELL (2258.91) GROUNDWATER ELEVATION GROUNDWATER CONTOUR INFERRED GROUNDWATER CONTOUR PILOT TEST FIGURE PRE -INJECTION RESULTS SEPTEMBER 14, 2010 TEC - FAIRVIEW 3a - 1396 CHARLOTTE HIGHWAY BUNCOMBE COUNTY, NORTH CAROLINA 20 ' I P:\TEC\FAIRVIEw\FIGURES\CAD\PILOTTEST\PRE PILOTTESTGWLEVELS m T m RX lem [an MW-17 MW-26() OMW-25 1. S17E U4P SOURCES., 7)GHE & BOND - SITE BUXDWGS, PROPERTY LNES, AND PARPONG AREAS FROM SITE PLAN WED JUNE 22, 2006 PE77T PROFESSIOAVIL SDWES - MONAORM AND RECOVERY WELL LOCAWAS FRO04 SURVEY D,47A RECOVED FEBRUARY 19, 2008 Wn COLE SURWY - AJONPORING KU LOCATIONS FROM SURVEY WA RECENED JAWARY 37, 2010 BUNCOMBE COUNTY GS - OFFSITE PROPERTY BOUNDARIES ACCESSED JANL44RY 2008 2. ABBREM77ONS' PCE - 71MMOROETHEW 7CE - 77WHLOROEVENE, AVA - MACROMAOS PER LITER 3. GROUNDWA7ER El"ATIONS 067AINED ON SEPMMER 15, 201D AND SEPTEWBER 16, 2010 FOR RW-07. AX4LYl)C_4L RESULTS FROM THE POST WECTON S4MPLkW COMX4C7ED ON SEPMARER 22, 2010 ],,)ZU PG/L. TCE: 151,000 PG/L. PCE: < 1.0 WG/L IVIW�-40 TCE: < 1.0 �G/L. (2264.07) MW-41 4 22640 F__ (2264.25) mw—�q R 7 (222 8 �sb"b 26 . 0)/ bs!� RW-6- MW-3 (2258.90) F_N G IN E E R ING & H.Y D R 0 G E 0 L 0 _Gy__] 231 HAYWOOD STREET, AsHEVILLE, NC 2880 1 TEL.828.281.3350 FAC.828. 281. 3351 - . A L T AMON TEN V IRONM E N T A L . COM DRAWN BY: EVAN YURKOVICH SCALE(FEET) PROJECT MANAGER: CHRIS GILBERT CLIENT: TEC-FAIRVIEW 10 0 10 DATE DESCRIPTION BY CHK APV] DATE: 02/2512011 LEGEND (4 MW-3 WATER TABLE MONITORING WELL @ MW-17 DEEP REGOLITH MONITORING WELL 0 MW-26 BEDROCK MONITORING WELL RW-5 GROUNDWATER RECOVERY WELL RW— 7 GROUNDWATER RECOVERY WELL USED AS AN INJECTION WELL (2258.90) GROUNDWATER ELEVATIONS GROUNDWATER CONTOURS INFERRED GROUNDWATER CONTOURS PILOT TEST FIGURE POST -INJECTION RESULTS SEPTEMBER 15, 2010 TEC - FAIRVIEW — 1396 CHARLOTTE HIGHWAY 3b BUNCOMBE COUNTY, 20 NORTH CAROLINA 0 P:\TEC\FAIRVIEW\FIGURES\CAD\PILOTTEST\POST PILOTTESTGWLEVELS m I a-j Eim Ecm [am MW-17 MW-26() (DMW-25 1. SHE "Ap SOURCES., WHE & BONO - SgE BUILDINGS. PROPERTY ONES, AIND PARNINC AREAS FROM SITE PLAN DAMD JUNE 22, 2006 PE7V PROFFSSIOM4L SERVICES - MoNflOROX AND RECOVERY WELL LOCADOAS FROM SURVEY 1147A RECEIVED FEBRUARY 19, 20138 *0 COLE SURVEY - MOWORING WELL LOC4770AIS FROM SURVEY LVITA RECEMD JANLARY 31, 2010 BUAICOMBE COUNTY CS - OFrS/7r PROPERTY BOUNLURIES ACCESSED aWWRY 2008 2. ABBREV1477ONS. PCE - M7RACHLOROMENE. 7CE - 7RCHLOROEMDVE, poll - MICROGRAMS PER LnER 3 GROUNDWATER EUVAWAIS AND AAl4LY7r_4L RESUL7S FROM THE POST ZWEC7)ON SAMPLING COADUC7ED ON OCTOBER 79, 201a IPCE: 1,540 PG/L TCE: 156,000 WGILI PCE: < 1.0 PG/ TCE: 2.9 w PCE: < 1.0 PG/L MW-40 TCE: < 1.0 pG/L 4 (22�6'2.74) MW-41 (2263.39) , 10) mw- rl% v 2 22 . 18 PCE: < 10.0 PG/L TCE: < 10.0 OG/L RW-6 __PCE: < 5,000 PG/L CE: < 5,000 PG/L *MW-3 (2258.54) ENGINEERING & H YDRO)610LO� 23 1 H AYWOOD STREET, ASHEVILLE, INC 28801 TEL. 828.281.3350 FAC. 828.281.3351 W W W . A L T A M 0 N T E N Y I R 0 N M E N T A L . C 0 M DRAWN BY: EVAN YURKOVICH PROJECT MANAGER: CHRIS GILBERT SCALE (FEET) CLIENT: TEC-FAIRVIEW 10 0 10 DATE DESCRIPTION BY I MCHKAPI DATE� 02/25/2011 LEGEND "W-J WATER TABLE MONITORING WELL MW- 17 DEEP REGOLITH MONITORING WELL MW-26 BEDROCK MONITORING WELL RW-6 GROUNDWATER RECOVERY WELL RW-7 GROUNDWATER RECOVERY WELL USED AS AN INJECTION WELL (2258.54) GROUNDWATER ELEVATIONS GROUNDWATER CONTOURS INFERRED GROUNDWATER CONTOURS PILOT TEST FIGURE POST —INJECTION RESULTS OCTOBER 19, 2010 TEC — FAIRVIEW — 1396 CHARLOTTE HIGHWAY 3c BUNCOMBE COUNTY, 20 NORTH CAROLINA ' I P:\TEC\FAIRVIEw\FIGURES\CAD�PILOTTEST\POST PILOTTESTGWLEVELS 180,000 160,000 140,000 120,000 C: . 4-j ro 1- 100,000 0 80,000 U 60,000 0 40,000 0 -r- U 20,000 Figure 4a Hydrograph and Trichloroethene Concentration vs. Time Monitoring Well MW-39 TEC-Fairview Trichloroethene Concentration 8/11/2010 9/22/2010 10/6/2010 10/19/2010 Sampling Date P:\TEC\Fairview\Analytical and Data\Water\Pilot Test\Pilot Test -Time vs Conc_graphs.xls 2262.6 2262.4 4-J ra 2262.2 Q") 2262.0 tt7 2261.8 2261.6 UJ .2 fa 2261.4 2261.2 o 6 2261.0 2,000 1,800 81,600 :L C .2L,400 SL,200 (5,000 800 0 0 bUU :E 400 X Figure 4b Hydrograph and Tetrachloroethene Concentration vs. Monitoring Well MW-39 TEC-Fairview Time 8/11/2010 9/22/2010 10/6/2010 10/19/2010 Sampling Date P:\TEC\Fairview\Analytical and Data\Water\Pilot Test\Pilot Test —Time vs Conc_graphs.xIs 2262.6 2262.4 2262.2 4Q-J) a) 4-- 2262.0 C: 0 2261.8 Ui 2261.6 fo 2261.4 C: =3 0 2261.2 0 2261.0 2260.8 U ;C5 (1) 0 0 -F 12.0 WIXII 8.0 6.0 4.0 2.0 Me Figure 4c Hydrograph and Trichloroethene Concentration vs. Time Monitoring Well MW-40 TEC-Fairview 8/11/2010 9/22/2010 10/6/2010 10/19/2010 Sampling Date P:\TEC\Fairview\Analytical and Data\Water\Pilot Test\Pilot Test —Time vs Conc_graphs.xls 2263.4 2263.2 2263.0 4'j Qj 2262.8 0) 4-- C 0 22152.6 4- 2262.4 2262.2 0 2262.0 0 2261.8 500 450 400 ZZ 350 U 300 0 4-J 250 C 0 200 A 150 -C 4-J 0) 2 100 Y 50 0 Figure 4d Hydrograph and Trichloroethene Concentration vs. Time Recovery Well RW-06 TEC-Fairview 8/11/2010 9/22/2010 10/6/2010 10/19/2010 Sampling Date P:\TEC\Fairview\Analytical and Data\Water\Pilot Test\Pilot Test —Time vs Conc_graphs.xls 2268.0 W-0110w, 4--J 2264.0 C 2262.0 .0 Ui 2260.0 LQ) -&-j fo _0 2258.0 0 L- (D 2256.0 50.0 45.0 40.0 :z-- 35.0 30.0 0 4-0 0 25.0 C 0 20.0 L A a) C 15.0 0 10.0 0 .r- U 5.0 ro 1-- 0.0 Figure 4e Hydrograph and Tetrachloroethen Concentration vs. Time Recovery Well RW-06 TEC-Fairview Tetrachloroethene Concentration s Groundwater Elevation 29.0 < 5.0 < 10.0 C) 0 H H 0 0 0 H CD 0 r-I 0 rq N N N LO 0 0) H 00 0) r-I Sampling Date 0 �I P:\TEC\Fairview\Analytical and Data\Water\Pilot Test\Pilot Test —Time vs Conc_graphs.xls 2268.0 2266.0 2264.0 12 4-- 2262.0 M LU L- 2260.0 M 2258.0 "0 (D 2256.0 2266.00 2265.00 2264.00 2263.00 0 2262.00 2261.00 0 2260.00 2259.00 2258.00 Figure 5a Pilot Test Hydrograph September 14, 2010 Pilot Test Monitoring Wells TEC-Fairview 19. _70. _7 10 -7s. 6' 4�9 17& i90 .:,�? .�96' . i90 Time P:\TEC\Fairview\AnaIyticaI and Data\Water\Pilot Test\Pilot Test Hydrographs.xlsx 2266.00 2265.00 2264.00 2263.00 C 0 M (v 2262.00 M 2261.00 C 0 2260.00 2259.00 2258.00 Figure 5b Pilot Test Hydrograph September 15,, 2010 Pilot Test Monitoring Wells TEC-Fairview > ?(? <�- 1?7. �> 1% -?L?6' �p i90 . �> .�)7 Time P:\TEC\Fairview\AnaIyticaI and Data\Water\Pilot Test\Pilot Test Hydrographs.xlsx TABLES Table I Pilot Test Groundwater Elevations TEC-:Fairview Buncombe County, North Carolina Well ID Date Time Depth to Water Level (feet below TOC) TOC Elevation (ft-MSL) Elevation of Groundwater Surface (ft-MSQ Total Depth of Well (feet below TOC) Length of Water Column (feet) 0 /10 8:15 6.25 2265.16 2258.91 15.28 9.03 9/14/10 09/14/10 10:30 6.25 2265.16 2258.91 15.28 9.03 7/14 09/14/10 9/14/10 11:40 6.22 2265.16 2258.94 15.28 9.06 09/14/10 9/14/101 12:15 6.23 2265.16 2258.93 15.28 9.05 09/14/10 13:30 6.21 2265.16 2258.95 15.28 9.07 09/14/10 15:00 6.21 2265.16 2258.95 15.28 9.07 09/14/10 15:35 6.19 2265.16 2258.97 15.28 9.09 09/14/10 ' 16:35 6.20 2265.16 2258.96 15.28 9.08 09/15/10 7:30 6.29 2265.16 2258.87 15.28 8.99 09/15/10 8:50 6.29 2265.16 2258.87 15.28 8.99 MW-3 09/15/10 10:20 6.28 2265.16 2258.88 15.28 9.00 09/15/10 11:10 6.25 2265.16 2258.91 15.28 9.03 09/15/10 13:20 6.26 2265.16 2258.90 15.28 9.02 09/20/10 13:43 13.41 2265.16 2251.75 15.28 1.87 09/22/10 14:25 6.68 2265.16 2258.48 15.28 8.60 10/06/10 13:47 6.20 2265.16 2258.96 15.28 9.08 10/19110' .13:50 6.62 2265.16 2258.54 15.28 8.66 11/10/10 14:00 6.21 2265.16 2258.95 15.28 9.07 11/23/10 11:20 6.23 2265.16 2258.93 15.2� 9.05 12/09/10 12:00 5.44 2265.16 2259.72 15.28 9.84 01/05/11 13:10 5.27 2265.16 2259.89 15.28 10.01 -09/1-4/10-- ---8:15--- 1AO-- ----2223.-06 2221-.66- -----6.-2 - -.4.80 - 09/14/10 10:30 1.32 2223.06 2221.74 6.2 4.88 09/14/10 11:40 1.32 2223.06 .2221.74 6.2 4.88 09/14/10 12:15 1.28 2223.06 2221.78 6.2 4.921 09/14/10 13:30 1.32 2223.06 2221.74 6.2 4.88 09/14/10 15:00 1.31 2223.06 2221.75 6.2 4.89 09/14/10 1 15:35 1.30 2223.06 2221.76 6.2 4.90 09/14/10 16:35 1.34 2223.06 2221.72 6.2 4.86 09/15/10 7:30 1.42 2223.06 2221.64 6.2 4.78 09/15/10 8:50 1.38 2223.06 2221.68 &2 4.82 MW-17 09/15/10 10:20 1.32 2223.0*6 2221.74 6.2 4.88 09/15/10 11:10 1.32 2223.06 2221.74 6.2 4.88 09/20/10 13:44 1.78 2223.06 2221.28 6.2 4.42 09/22110 14:26 1.82 2223.06 2221.24 .6.2 4.38 10/06/10 13:47 1.16 2223.06 2221.90 6.2 5.04 10/19/10 1-3:50 1.54 2223.06 2221.52 6.2 4.66 11/10/10 14:00 1.24 2223.06 2221.82 6.2 4.96 11/23/10 11:20 1.27 2223.06 2221.79 6.2 4.93 12/09/10 12:00 .0.05 2223.06 2223.01 6.2 6.15 01/05/11 13:10 0.03 2223.06 2223.03 6.2 6.17 I I I I PATECVairvieMAnalytical and Data\Water\Pilot Test\TEC-Pilot Test -New Wells-GW-Results.XLS Page 1 of 4 . Table I Pilot Test. Groundwater Elevations TEC-Fairview Buncombe County, North Carolina Well ID Date Time Depth to Water Level (feet below TOC) TOC Elevation (ft-MSL) Elevation of Groundwater Surface (ft-MSL) Total Depth of Well (feet below TOC) Length of Water Column (feet) 09/14/10 8:15 14.03 2280.19 2266.16 59.5 45.47 09/14/10 11:40 13.60 2280.19 2266.59 59.5 45.90 09/14/10 13:30 13.85 2280.19 2266.34 59.5 45.65 09/14/10 16:35 13.65 2280.19 2266.54 59.5 45.85 09/15/10 7:30 13.95 2280.19 2266.24 59.5 45.55 MW725 09/15/10 10:20 13.87 2280.19 2266.32 59.5 45.63 09/20/10 13:46 14.13 2280.19 2266.06 59.5 45.37 09/22/10 14:29 14.27 2280.19 2265.92 59.5 45.23 10/06/10 13:52 13.88 2280.19 2266.31 59.5 45.62 10/19/10 13:50 14.20 2280.19 2265.99 59.5 45.30 01/05/11 13:10 13.25 2280.19 2266.94 59.5 46.25 09/14/10 8:15 14.02 2280.22 2266.20 85.0 70.98 09/14/10 11:40 13.90 2280.22 2266.32 85.0 71.10 09/14/10 13:30 13.90 2280.22 2266.32 85.0 71.10 09/14/10 16:35 13.87 2280.22 2266.35 85.0 71.13 09/15/10 7:30 13.99 2280.22 2266.23 85.0 71.01 MW-26 09/15/10 10:20 13.90 2280.22 2266.32 85.0 71.10 09/20/10 13:47 14.24 2280.22 2265.98 85.0 70.76 09/22/10 '14:30 14.29 2280.22 2265.93 85.0 70.71 10/06/10 13:52 13.92 2280.22 2266.30 85.0 71.08 10/19/10 13:50 14.22 2280.22 2266.00 85.0 70.78 01/05/11 13:10 13.26 2280.22 2266.96 85.0 1_134 08/11/10 11:44 5.15 2266.58 2261.43 50.0 44.85 09/14/10 8:15 4.05 2266.58 2262.53 50.0 45.95 09/14/10 10:30 3.16 2266.58 2263.42 50.0 46.84 7 09/14/10 11:40 3.30 2266.58 2263.28 50.0 46.70 09/14/10 12:15 3.10 2266.58 2263.48 50.0 46.90 09/14/10 13:30 3.30 2266.58 2263.28 50.0 46.70 09/14/10 15:00 3.25 2266.58 2263.33 50.0 46.75 09/14/10 15:35 2.71 2266.58 2263.87 50.0 47.29 09/14/10 16:35 2.95 2266.58 2263.63 50.0 47.05 09/15/10 7:30 3.50 2266.58 2263.08 50.0 46.50 09/15/10 8:50 3.10 2266.58 2263.48 50.0 46.90 09/15/10 10:20 3.01 2266.58 2263.57 50.0 46.99 MW-39 09/15/10 11:10 2.52 2266.58 2264.06 50.0 47.48 09/15/10 13:20 2.40 2266.58 2264.18 50.0 47.60 09/16/10 1 16:20 4.10 2266.58 2262.48 50.0 45.90 09/20/10 13:48 4.34 2266.58 2262.24 50.0 45.66 09/22/10 11:05 4.46 2266.58 2262.12 50.0 45.54 10/06/10 10:43 4.03 2266.58 2262.55 50.0 45.97 10/19/10 10:44 4.40 2266.58 2262.18 50.0 45.60 11/10/10 14:00 4.17 2266.58 2262.41 50.0 45.83 11/23/10 11:20 4.20 2266.58 2262.38 50.0 45.80 12/09/10 12:00 3.53 2266.58 2263.05 50.0 46.47 01/05/11 13:10 3.31 2266.58 2263.27 50.0 46.69 P:\TEC\Fairview\Analytical and Data\Water\Pilot Test\TEC-Pilot Test -New Wells-GW-Results.XLS Pade 2 of 4 Table 1 Pilot Test Groundwater Elevations TEC-Fairview Buncombe County, North Carolina Well ID Date .. Time I Depth to Water Level (feet below TOC) TOC Elevation (ft-MSL) Elevation of Groundwater Surface (ft-MSL) Total Depth of Well (feet below TOC) Length of Water Column (feet) 08/11/10 - 10:55 3.83 2266.22 2262.39 51.0 - 47.17 09/14/10 8:15 3.08 2266.22 2263.14 51.0 47.92 09/14/10 10:30 2.60 2266.22 2263.62 51.0 48.40 09/14/10 11:40 .2.63 2266.22 2263.59 51.0 48.37 09/14/10 12:15 2.50 2266.22 2263.72 51.0 48.50 09/14/10 13:3 0 2.61 2266.22 2263.61 51.0 48.39 09/14/10 15:00 2.61 2266.22 2263.61 51.0 48.39 09/14/10 15,35 2.30 2266.22 2263.92 51.0 48.70 09/14/10 16:35 2.42 2266.22 2263.80 51.0 48.58 09/15/10 7:30 2.91 2266.22 2263.31 51.0 48.09 09/15/10 8:50 2.58 2266.22 2263..64 51.0 48.42 MW-40 09/15/10 10:20 2.47 2266.22 2263.75 51.0 48.53 09/15/10 11:10 2.20 2266.22 2264.02 51.0 48.80 09/15/10 13:20 2.15 2266.22 2264.07 51.0 48.85 09/16/10 16:20 3.00 2266.22 2263.22 51.0 48.00 09/20/10 13:49 3.29 2266.22 2262.93 51.0 47.71 09/22/10 10:07 3.38 2266.22 2262.84 51.0 47.62 10/06/10 9:38 3.02 2266.22 2263.20 51.0 -47.98 10/19/10 9:47 3.48 2266.22 2262.74 51.0 47.52 11/10/10 14:00 3.11 2266.22 2263.11 51.0 47.89 11/23/10 11:20 3.15 2266.22 2263.07 51.0 47.85 .12/09/10 12-:0-0- _DNM_ .2266.22 - --5-1.0- - 01/05/11 13:10 2.46 2266.22 2263.76 51.0 48.54 08/11/10 9:52 3.22 2266.81 2263.59 49.0 45.78 09/14/10 8:15 3.36 2266.81 2263.45 49.0 45164 09/14/10 10:30 2.91 2266.81 2263.90. 49.0 46.09 09/14/10 11:40 2.99 2266.81 2263.82 49.0 46.01 09/14/10 12:15 2.90 2266.81 2263.91 49.0 46.10 09/14/10 13:30 2.98 .2266.81 2263.83 49.0 46.02 09/14/10 15:00 2.96 2266.81 2263.85 -49.0 46.04 09/14/10 15:35 2.75 2266.81 2264.06 49.0 46.25 09/14/10 16:35 2.85 2266.81 2263.96 49.0 46.15 09/15/10 7:30 2.95- 2266.81 2263.86 49.0 46.05 09/15/10 8:50 2.82 2266.81 2263.99 49.0 46.18 MW-41 09/15/10. 10:20 2.79 2266.81 2264.02 49.0 46.21 09/15/10 11:10 2.62 2266.81 2264.19 49.0 46.38 09/15/10 13:20 2.56 2266.81 2264.25 49.0 46.44 09/16/10 16:20 3.20 2266.81 2263.61 49.0 45.80 09/20/10 13:50 3.34 2266.81 2263.47 49.0 45.66 09/22/10 9:00 3.43 2266.81 2263.38 49.0 45.57 10/06/10 8:35 3.12 2266.81 2263.69 49.0 45.88. 10/19/10 8:48 3.42 2266.81 2263.39 49.0 45.58 11/10/10 14:00 3.215 2266.81 2263.56 49.0 45.75 11123/10 11:20 3.29 2266.81 2263.52 49.0 45.71 12/09/10 12:00 2.73 2266.81 2264.08 49.0 46.27 01/05/11 13:10 2.59 2266.81 2264.22 49.0 46.41 PATECVairview\Analytical and Data\Water\Pflot Test\TEC-Pilot Test -New Wells-GW-Results.XLS - Page 3 of 4 Table 1 Pilot Test Groundwater Elevations TEC-Fairview Buncombe County, North Carolina Well ID Date Time Depth to Water Level (fe et below TOC) TOC Elevation _IMSQ Elevation of Groundwater Surface (ft-MSQ Total Depth of Well (feet below TOC) Length of Water Column (feet) 08/11/10 12:52 DNM 2267.48 ------- 120.0 ------- 09/14/10 8:15 8.99 2267.48 2258.49 120.0 111.01 09/14/10 10:30 6.53 2267.48 2260.95 120.0 113.47 09/14/10 11:40 6.50 2267.48 2260.98 120.0 113.50 09/14/10 12:15 6.46 2267.48 2261.02 120.0 113.54 09114/10 13:30 6.45 2267.48 2261.03 120.0 113.55 09/14/10 15:00 6.44 2267.48 2261.04 120.0 113.56 09/14/10 15:35 6.43 2267.48 2261.05 120.0 113.57 09/14/10 16:35 6.45 2267.48 2261.03 120.0 113.55 09/15/10 7:30 6.60 2267.48 2260.88 120.0 113.40 09/15/10 8:50 6.52 2267.48 2260.96 120.0 113.48 RW-06 09/15/10 10:20 6.50 2267.48 2260.98 120.0 113.50 09/15/10 11:10 6.50 2267.48 2260.98 120.0 113.50 09/15/10 13:20 6.49 2267.48 2260.99 120.0 1 113.51 09/16/10 16:20 6.50 2267.48 2260.98 120.0 113.50 09/20/10 13:54 6.54 2267.48 2260.94 120.0 113.46 09/22/10 12:07 6.61 2267.48 2260.87 120.0 113.39 10/06/10 11:40 6.44 2267.48 2261.04 120.0 113.56 10/19/10 11:43 6.82 2267.48 2260.66 120.0 113.18 11/10/10 14:00 6.87 2267.48 2260.61 120.0 113.13 11/23/10 11:20 6.97 2267.48 2260.51 120.0 113.03 ----12/Q9/-10- 12:00 6.46 2267.48 2261.02 120.0 113.54. 01/05/11 13:10 6.34 2267.48 2261.14 120.0 113.66 1 08/11/10 12:45 DNM 2267.30 ------- 50.0 ------- 09114/10 8:15 3.11 2267.30 2264.19 50.0 46.89 09/14/10 10:30 3.12 2267.30 2264.18 50.0 46.88 09/14/10 11:40 3.10 2267.30 2264.20 50.0 46.90 09/14/10 12:15 3.10 2267.30 2264.20 50.0 46.90 09/14/10 13:30 3 .03 2267.30 2264.27 50.0 46.97 09/14/10 15:00 - 3.10 2267.30 2264.20 50.0 46.90 09/14/10 15:35 3.10 2267.30 2264.20 50.0 46.90 09/16/10 16:20 5.10 2267.30 2262.20 50.0 44.90 RW-07 09/20110 13:56 5.30 2267.30 2262.00 50.0 44.70 09/22/10 13:02 5.33 2267.30 2261.97 50.0 44.67 10/06/10 12:40 4.32 2267.30 2262.98 50.0 45.68 10/19/10 12:40 4.45 2267.30 2262.85 50.0 45.55 11/10/10 14:00 4.20 2267.30 2263.10 50.0 45.80 11/23/10 11:20 4.20 2267.30 2263.10 50.0 45.80 12/09/10 12:00 3.62 2267.30 2263.68 50.0 46.38 01/05/11 1310 3.43 2267.30 2263.87 50.0 1 4 .57 Notes: 1. TOC means Top of Casing 2. ft-MSL means feet below Mean Sea Level. PATEC\Fairview\AnaIyticaJ and Data\Water\Pilot Test\TEC-Pilot Test -New Wells-GW-Results.XLS Page 4 of 4 -NI Ti3'LJIC 2 Pilot Test VOC Groundwater Analytical Results TEC-Fairview Buncombe County, North Carolina Volatile Organic Compounds (VOCs) (U (U Qj (D r- M Qj (U (U Sample LU E 1 Q. 2 r a) a) 0 Well ID Collection a) fo 01 0) 0 0 2 0 0. 0 N U 0 0 (U (U (U Date rz 0 0 0 .2 -6 2 2 U Y 0 0 0 0 9 ra E 19 -2 0" H �4 H N (U CU It It: rIj (0 r 4 0 H U U 8111/2010 < 5.0 < 1.0 < 1.0 22.8 2.6 2.2 10.9 < 1.0 < 1.0 < 2.0 '414.7 < 1.0 5.3 -466- 3.0 < 1.0 9/22/2010 < 25.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.01 5.2 < 5.0 < 5.0 < 10;0 29,.Q < 5.0 6.2 339 < 10.0 < 5.0 RW-06 10/6/2010 < 25.0 < 5.0 < 5.0 < 5.0 < 5.0 < 5.Oi < 5.0 < 5.0 < 5.0 < 10.0 < 5.0 < 5.0 < 5.0 < 5.0 < 10.0 < 5.0 10/19/2010 < 50.0 < 10.0 < 10.0 < 10.0 < 10.0 < 10.0 < 10.0 < 10.0 < 10.0 < 20.0 < 10.0 < 10.0 < 10.0 < 10.0 < 20.0 < 10.0 8/11/2010 < 5.0 3.3 < 1.0 '34.4 < 1.01 < 1.0 '�IM' 18.7 < 2.0 �3'39,.' 145 ��.':'5.9'01�.' -47,0 .,6,1 63.2 25.3 9/22/2010 < 100,000 < 20,000 < 20,000 < 20;000 < 20,000 < 20,OdO, < 20,000 < 20,000 < 20,000 < 40,000 < 20,000 < 20,000 < 20,000 < 20,000 < 40,000 < 20,000 RW-07 10/6/2010 NA . NA NA NA NA NA I NA NA NA NA NA NA NA NA- NA NA 10/19/2010 < 25,000 < 5,000 < 5,000 < 5,000 < 5,000 < 5,000 < 5,000 < 5,000 < 5,000 <. 10,000 < 5,000 < 5,000 < 5,000 < 5,000 < 10,000 < 5,000 8/11/2010 < 5,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 2,000 ;!�,2;686.'� -11,2010 1 < 2,000 < 1,000 9/2212010 < 5,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 6'050-,� 1320:, �-151,000,� < 2,000 < 1,000 MW-39 10/6/2010 < 5,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 < 1,000 <1,000 7 O-A "-XTqo, < 2,000 < 1,000 10119/2010 5,610:, < 1,000 1 < 1,000 < 1,000 < 1,000 < 1.000 < 1,000 < 1,000 < 1,000 < 2,000 Ij54'0�.':'.'.�141;4150,. 1'0,,�AO, -156jO' do < 2,000 < 1,000 8/1112010 < 10.0 < 2.0 5.9- < 2.0 < 2.0 < 2A < 2.0 < 2.0 < 2.0 < 4.0 < 2.0 < 2.0 < 2.0 11.1. < 4.0 < 2.0 9/22/2010 < 5.0 < 1.0 2.8 < 1.0 <-1.0 < 1.0� < LO < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 -,,4.5. < 2.0 < 1.0 MW-40 10/6/2010 < 590 < 1.0 2.9 < 1.0 < 1.0 < 1.01 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.10 < 1.0 :.3�T < 2.0 < 1.0 10/19/2010 < 5.0 < 1.0 3.4 < 1.0 < 1.0 .5c 1.0 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 2.9 < 2.0 < 1.0 8/11/2010 < 5.0 < 1.0 4.2 < 1.0 < 1.0 < :L.Oi < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 2.0 < 2.0 < 1.0 9/22/2010 < 5.0 1 < 1.0 3.4 < 1.0 < LO -� 1.0� < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 MW-41 1016/2010 < 5 < 1.0 3.5 < 1.0 -cc 1.0 < 1!01 < 1.0 < 1.0 < 1.0 < 2.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 10/19/2010 < 1.0 5.0 < 1.0 < 1.0 < 1.0, < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0 2L Standards 0.3 70 1,000 7 6 1 _ 70 600 1 5 0.7 600 200 3 500 500 Notes: 1. This table only includes compounds that were recently and historically detected above method detection limits. 2. The complete suite of compounds can be found in the individual analytical reports. 3. Concentrations are in micrograms per liter (pg/L). 4. "<" means the result is less than the method reporting limit. 5. 2L Standards from North Carolina Administrative Code (NCAQ Ttle 15A, Subchapter 2L, effective jahuary 1, 2010. 6. Bold indicates a detection over the laboratory reporting limit and shaded indicates exceedance of the 2L Standard. 7. NL indicates a 2L standard is not listed. P:%TEMFalrvlew\Analytical and Data\Water\Pilot Test\TEC-Pilot Test -New Wells-GW_Results.XLS Page 1 of I Table 3 Pilot Test. Groundwater Analy�ical Results TEC-Fairview Buncombe County, North Carolina Metals E Sample E E tM Im E Well ID Collection 2 U a) bate E CL CD M 0 -j N iz 0 U 0 in z 8/11/2010 4.7�-,,- < 1.0 < 5.0 < 5.0 < 0.20 6-1-.-4"-,-' 3 . 7.8 45.2 < 0.10 < 5.0 17.8 RW-06 9122/2010 < 5.0 < 1.0 < 5.0 < 5.0 < 0.20 < 5.0 30.8 35.0 2.8 5.2 < 5.0 10/612010 < 5.0 < 1.0 < 5.0 0.38 < 5.0 < 16.0 41.8 2.8 < 50.0 < 5.0 10/19/2010 < 5.0 < 1.0 -,�1,17,- < 5.0 < 0.20 < 5.0 17.4 42.0 3.2 5.0 - < 5-.0 8/11/2010 <5.0 < 1.0 < 5.0 < 5.0 < 0.20 < 5.0 < 10.0 14.7 2.7 < 5.0 < 5.0 RW-07 9/22/2010 j,'4,to < 100 J, 86,01. < 500 31, 526 < 1,000 259 < 1,000 < 10,000 < 25,000 10/6/2010 < 500 < 100 -ii-*QO - < 500 < 20.0 < 500 < 1,000 418 < 20.0 < 25,000 < 5.0 10/19/2010 < 500 < 100 758,'-., < 500 < 2.0 < 500 < 1,000 < 25,000 < 10.0 < 5,000 < 5,000 8/11/201 0 < 5.0 5�2 42 , 1-� 228 < 0.20 3k'' 498 17.9 0.46 < 5.0 < 5.0 MW-39 9/22/2010 < 5.0 -3'§1" 210 < 0.20 '�B115- 467 14.4 0.48 < 5.0 < 5.0 10/6/2010 < 5.0 1.0 -j43-�:.', 184 0.20 359; 416 17.8 0.14 < 5.0 < 5.0 10/19/2010 < 5.0 '--6;0; 218 0.26 4 A 6 493 15.4 0.34 < 5.0 < 5.0 8111/2010 < 5.0 < 1.0 .69.4 25.5 < 0.20 < 5.0 41.0 15.8 2.8 < 5.0 < 5.0 MW-40 9/22/2010 < 5.0 < 1.0 10.0 < 0.20 < 5.0 18.9 12.4 2.9 < 5.0 < 5.0 lo-/6-/2010- -< -5- .0 < 1.0 --89"3, 32.5 < 0.20 5.1 41.6 14.6 2.6 < 5.0 < 5 0 10/19/2010 < 5.0 < 1.0 -921,- .3 31.7 < 0.20 < 5.0 58.9 10.2 2.7 < 5.0 < 5.0 8111/2010 < 5.0 < 1.0 i2T�--, 94.1 < 0.20 12.9 124 10.5 3.2 < 5.0' < 5.0 MW-41 9/22/2010. < 5.0 < 1.0 ;12�, 82.8 < 0.20 11.1 95.9 10.3 3.3 < 5.0 < 5.0 10/6/2010 < 5.0 < 1.0 'B'3; '2-, 70.5 < 0.20 9.1 69.6 12.6_ 3.2 < 5.0 < 5.0 10/19/2010 < 5.0 < 1.0 7.1 < 5.0 < 0.20 < 5.0 < 10.0 10.2 3.3 < 5.0 < 5.0 2L Standards -10 10 1,000 . 1 15 1,000 NIL 10 250 1 250 Notes: 1. This table only includes compounds that were recently and historically detected above method detection limits. 2. The complete suite of compounds can be found in the individual analytical reports. 3. Concentrations are In micrograms per liter (pg/L). 4. 11<11 means the result is less than the method reporting limit. 5. 2L Standards from North Carolina Administrative Code (NCAC) Title 15A, Subchapter 2L, effective January 1, 2010. 6. Bold Indicates a detection over the laboratory reporting limit and shaded indicates exceeclance of the 2L Standard. 7. NIL indicates a 2L standard is not listed. P:\TEC\Fairview\Analytical and nata\Water\Pilot Test\TEC_Pilot Test -New Wei Is-GW-Results.X L-q Page I of I Table 4 Pilot Test Water Quality,Parameters TEC-Fairview Buncombe County, North Carolina Well ID Date Dissolved Oxygen (mg/L) Oxygen Reduction Potential (MV) pH Specific Conductance (PS) Temperature (00 Turbidity (NTU) 08/11/10 6.85 30.1 5.82 80 16.50 21.92 RW-06 09/22/10 0.00 516 5.97 134 16.92 2.97 10/06/10 7.96 572 6.06 172 16.98 3.02 10/19/10 4.98 624.4 6.03 103 16.59 3.01 08/11/10 17.42 161.6 5.57 39 17.78 2.20 RW-07 09/22/10 0.00 718 6.67 37.9 17.90 117.0 10/06/10 7.65 652 6.85 960 17.62 53.64 10/19/10 5.57 713.3 6.54 3413 17.03 40.97 08/11/10 3.24 221.9 5.15 35 18.82 190.4 MW-39 09/�2/10 - 0.00 289 5.40 51 17.44 740.4 10/06/10 0.20 230 5.46 - 57 17.21 745.7 10/19/10 3.73 178.3 5.53 38 16.74 377.7 08/11/10 16.83 212.5 5.13 38 18.58 23.46 MW-40 09/22/10 4.09 268 5.28 61 17.18 104.5 10/06/10 2.50 258 5.44 60 17.42 296.9 10/19/10 3.21 207.4 5.67 45 16.61 368.0 08/11/10 10.83 208.3 5.34 42 17.00 900.0 MW-41 09/-22/10 - -3-.54 - -320- 5.25- 68- - 16.-96- - - -654:0-- 10/06/10 5.46 262 5.25 75 '16.79 530.6 10/19/10 5.27- 230.6 5.14 50 15.78 496.7 Notes: 1. pH measured in standard units 2. 'C denotes degrees Celsius 3. pS denotes microsiemens 4. MV denotes millivolts 5. mg/L denotes milligrams per liter 6. NTU denotes nephelometric turbidity units 7. Parameters are those measured following stabilization. P:\TEC\Fairview\Analytical and Data\Water\Pilot Test\TEC-Pilot Test -New Wells-GW-Results.XLS Page I of I Sodium Permanganat! ,1on Event Summary Tyc , 0 Electronics corporation F airview, North Carolina I Time Approximate NaIVInO4 Concentration Approximate Injection Flow Rate (gprn`) Calculated Injection Flow Rate (gpO) Pressure Reading at Wellhead (Psid Approximate Incremental Volume Injected Approximate' Cumulahve ., to Vol, injected :1 Depth to Water (feet below TOC) - RW 07 RW-00 I MW- ITIMI-ITM W-41 1AW-03 MW-17 MW-26 MW-25 Notes/Observations 9/14/2010 8:15 AM 3.11. 8.99 4.05 3.08 3.36 6.25 1.40 14.02' 14.03 Mix Batch #1 consisting of approximately 100 gallons water and 25 gallons 40% NaMnC, 9:35 AM 10:30 AM IWA 0.9 to L2 3-8 4 Begin Injection HL 3.12 6.53 116 2m6O 2.91 6.25 L.2 10:45 AM 125 125 top 111 .1 Mix Batch 112 consisting of pp..,.a,.Iy 100 gallons water and 25 gallons 40% N.MnO4. 11:00 AM 11:40 AM 10% 0.95 to 1.4 1.3 2 I Begin Injection #2. 1 3.10 1 6.50 1 3.30 6.22 132 13.90 13.60 12:15 PM 12.30 PM 3.10 1 6.46 1 3.10 6.23 L28 NMr NMT 120 245 Stop Injeell-In #2. Mix Batch #3 consisting of approximately 100 gallons water and 25 gallon 40% NaMnO,. 1:00 PM 1:30 PM ID -A 0.99 to L6 1.2 2 I gin Injection #3. 3.30 6.21 1.32 13.90 13.85 2:40 PM 120 365 Stop Injection #3. Mix Batch 44 consisting of approximately 100 gallons water and 25 gallons 40% NaMnO4. 2:55 PM 10 1.95 2.3 4 gin Infection 04. 3:00 PM 3.10 1 6.44 1 3.25 2.61 2.96 6.21 L31 NMT NNTr 3:35 PM 2*07 1 3.10 6.43 2.71 2.30 2.75 6.19 L30 NMT NIAT 3:50 PM 125 490 Stop Injection 04. Mix Batch #5 consisting of approximately 120 gallons water and 25 gallons 40-A NaMnC,. 4:20 PM 4131 AM �10% L76 to 2.05 Ll 4 Begin Infection #5. 1 NlAr 1 6.45 11 2.95 2.42 2 5 6.20 L34 1 13.87 13.65 1 5:30 PM .2. - Stop Injection #S. Stand down forthe evening. 9/15/10 7:005AM Mix Eltach III mrsIstin, of approximately 10D gallons water and 25 gallons 40-1 NaMnO4. -2,15 7,30 Am 8:20AM 10% 21o2.3 23 2 NMT 1 6.60 6,11 1,42 11,19 13.95 -Begin Infection HIS. 115 7�5 stop Injecti n tffi. Mix Batch U7 consisting of approximately 100 gallons waterand 2.5 gallons 40A NaMnO, 8:45 AM 8:50 AM IM/6 L9 to 2.3 2.1 2 Beef Injection #7. NMT 6.52 3.10 2.58 L38 NMI 9:40 AM 115 850 p Injection H7. Mix Batch #8 consisting of piproximately140 Ilons water and 35 gallons a 40ga % NaMnO,. 10:15AM 10:20AM 1frA L76 to 2.01 L9 2 B in Infection One. N M�r 6.50 3.01 279 11:10AM 11:45 AM NMr 50 2m62 - 170 :::102: t 7 Stop Injection 08. Mix Batch 09 consisting of pproximately 140 gallons mtgr and 35 gallons 40% NaMnC,. 12:30 PM :20 IM IV/ 1 1.8 to 2.7 1 1.9 1 2 1 Begin Inlection #9. NIVIT 6.49 2.40 2.15 2.56 6.26 NMr NMI NKr I �_2 PM 175 i 1195 I Stop Infection #9. Notes: 1 =flow rate measured at the gauge at the well head. 2 - pump In well was pulled at about 7:50 AM 9/13/10 NMT = No measurement taken. 3 Volume measured based on graduated 225 gallon square poly tanL 4 Calculated flow rate based on volume Injected over time. P.\TEC\Falmiew\Co�spandence\Pilot Test_2010VIeld Work\Injectlon Event Record.,do, APPENDICES APPENDIX A DENR Issuance of Injection Permit dated June 21, 2010 AVAI HCDEHR North Carolina Department of Environment and Natural Resources Division of Water Quality Beverly Eaves Perdue Coleeri H, Sullins Dee Freeman Governor Director Secretary June 21, 20 i 0 Richard Surninski Tyco Elecfronics Corporation P.O. Box 3608, M/S 140-42 Harrisburg, PA 17105 Reff: issuance of Injection Pernift-W10100089 Tyep Electronics Corp. Facility Fairview,Buncombe, i:',ounty, North. Carolina. Dear Mr. Suminski: In accordance with the application received on March 24, 2010, and the supporting data.teceived May 25. 2010, and Julie 9, , 2010 we are forwarding permit number W10100089. This pqftxlit :is to inject sodium permanganate to rem6diate n vents at the, facility referenced above. This permit shall be effective from gro�;i�ater contami ated with chlorinated sol ; � and shall be subject to the conditions and limitations stated therem, including the the date of issViance iffitil May 3 1, 2012, requirement to submit a final project evaluation as stated in PART. VII — MONITORING AND REPORTING REQUIREMENTS. ?lease read the entire pern-4t to ensure that you are aw are of all compliance requirements of the permit. You will need to notify this office by telephone 48 hours prior to initiation of operation -of the facility. In order to continue unintprrqpted legal use of the'Injection. facility for fhe..-statedpuipose, you must submit an application to renew if you the permit 120 days prior to its expiration date, Please contact me at 9.19-715-6164 or Thonlas.Slusser(omcdelingov have any questibils-abon.t your permit, Best Regards, Thomas Slusser, L.G. Program Manager Underground Inj ection. Control Program cc: Landon Davidson, Asheville Regional Office Alec MacBeffi, Altamont Environmental,. 231 Hayv,,00d St... Asheville, NC 28801 Robert Luftly, DWM Superfund Section WI0100089 Permit File AQUIFER PROTEGTI'ON SECTION 1636 Mail ServioeCenter, Raleigh. North Carolina 27699-1636 Location: 2728 Cal�ltal Boulevard, Raleigh. North Carolina 27604 One Phone: 919-733-3221 \ FAX 1: 919-715-0588; PAY 2- 619�7115-6048 � Customer SeNice: 1 -877-62376748 NorthQtrolffia Internal: wimt.hwatemuality.org Aaturaffiz An Equal Opportunity I Atii(mative kli,, Employer V NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH, NORTH CAROLINA - PERMIT FOR THE CONSTRUCTION AND OPERATION OF A WELL FOR INJECTION In accordance with the provisions ofArticle 7, Chapter 87; Article 21, Chapter 143, and. other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Tyco Electronics Corporation FOR THE OPERATION OF I TYPE 51 INJECTION WELL, defined in Title 15A North Carolina Administrative Code 2C.0209(e)(3)(C), to inject sodium permanganate, for the chemical oiidation of chlorinated solvents. These injection wells/points will be located at the Tyco Electronics Corporation facility located at 1396 Charlotte Highway in Fairview, Buncombe County, North Carolina, and will be operated in accordance with the Application submitted March 24, 2010, and in conformity with the specifications and supporting data submitted May 25, 20 10, and June 9, 2010, all ofwhich are filed with the Departmentbf Environment and Natural Resources and are considered a part of this permit. This pmViit is for Operation only and does not waive any prqvisions of the Water Use Act or any other applicable Laws,'Rules, -or -Regulatiqns. 'Operation and use of an injection well shall be in .compliance with Title 15A North Carolina Administrative Code 2C.01 00 and.0200, and any other Laws, Rules, and Regulations pertaining to well construction and use. This permit shall be effective, unless I revoked, from the date of its issuance until May 3 r, 2012, and shall be subject to the specified conditions and limitations set forth in Parts I through X hereof. Permit issued this the 21 st day of June, 2010. ,,V\,Cole�n H. Sullins, Director Division of Water Quality By Authority of the Environmental Management Commission. PermitNo. WI0100089 PAGE I OF 6 ver. Jan.2010 AP[U!C-6 M PART I - WELL CONSTRUCTION GENERAL CONDITIONS 1. The Permittee must comply with all conditions ofthis permit and with the standards and criteria specified in Criteria and Standards Applicable to Injection Wells (15ANCAC 2C.0200). Any noncompliance with conditions of this permit constitutes a violation of the North Carolina Well Construction Act and is grounds for enforcement action as provided for in N.C.G.S. 87-94. 2. This permit shall become voidable unless the -facility is constructed in accordance with the conditions of this permit, the approved plans and specifications, and other supporting data. 3. This permit is valid only for construction of the number of injection wells described in the application and other supporting data. Construction of additional injection wells must be approved in advance by the Aquifer Protection Section. 4. Each injection well shall not hydraulically connect separate aquifers. 5. Each injection well shall be constructed in such a manner that water from land surface cannot migrate into the gravel pack or well screen. 6. Each injection well shall be secured to reasonably insure against unauthorized access and use. Each well shall be permanently labeled with a warning that it is for injection purposes and the entrance to each well must be secured with a locking cap. 7. Each injection well shall be afforded reasonable protection against damage during construction and' 'Use. 8. Each injection well shall have permanently affixed an identification plate. 9. Within 30 ays of completion of well construction, a completed Well Construction Record (Form GW-1) must be -submitted for each injection well to - Aquifer Protection Section-UIC Program DENR-Division.of Water Quality 1636 Mail Service Center Raleigh, NC 27699-1636 PART 11 - WELL CONSTRUCTION SPECIAL CONDITIONS At least forty-eight (48) hours priorto cdnstr-acting each injectionwell, thePermittee shall notifythe Aquifer Protection Section -Underground Injection Control (UIC) Central Office staff, telephone number (919) 715-6164 and the Asheville Regio nal Office Aquifer Protection Section Staff, telephone number (828) 296-4500. Permit No. WI0100089 PAGE 2 OF 6 ver. Jan.201 0 APAJIC-6 PART M - OPERATION AND USE GENERAL CONDITIONS 1. This permit is effective only wit respect to the nature, volume ofmaterials, rate,ofinjection, and number of injection wells as described in the application and other supporting data. '2. This permit is not transferable without prior notice to, and. approval by, the Director of the Division of Water Quality (Director). in the event there is a desire for the facility to change ownership, or there is a name change of the Permittee, a formal permit amendment request must be submitted to the Director, including any supporting materials as maybe appropriate, at least 3 0 days prior to the date of the change. 3. The issuance of this permit shall not relieve the Permittee*ofthe responsibility of complying with any and all statutes, rules, regulations, or ordinances which maybe imposed by other local, state, and federal agencies which have jurisdiction. Furthermore, the issuance of this permit does not imply that all regulatory requirements have been met. PART IV - PERFORMANCE STANDARDS The injection facility shall be effectively maintained and operated at all times so -that there is no contamination of groundwater which will render it unsatisfactory for normal use. In the event that the facility fhils to- perform satisfactorily, including the creation of nuisance conditions or failure of the injection zone to adequately assimilate the injected fluid, the Permittee shall take immediate corrective actions including those actions that may be required by the Division- of W�ter Quality such as the repair, modification, or abandonment of the injection facility. 2. The Peirnittee shall be required to comply with the terms and conditi�ons of this permit even if compliance re4uires a reduction or elimination of the perinitted activity. 3. The issuance of this permit shall not relieve- the Permittee of the responsibility for damages to surface or groundwater resulting from the operation of this facility. PART V - OPERATION AND MAINTENANCE REQUIREMENTS 1. The injection facility shall be properly maintained and op . erated at all times. 2. The Permittee must notify the Division and receive pnor written approval from the Director of any planned physical alterations or additions in the permitted facility or activity not specifically authorized by the permit. 3. At least forty-eight (48) hours prior to the initiation of the operation of the facility for injection, the Permittee must.not-ifyby telephone the Aquifer Protection Section-UIC, Central 0Aice staff, telephone number (919) 715-6164. Notification is required so that Division staff can inspect or otherwise review the injection facility and determine if it.is in compliance with permit conditions. Pennit No. W101 00089 PAGE 3 OF 6 ver. Jan-.2010 AP/UIC-6 PART VI - INSPECTIONS Any duly authorized officer, employee, or representative of the Division of Water Quality may, upon presentation of credentials, enter and inspect any property, premises, or place on or related to the injection facility at any reasonable time ' for the purpose of determining compliance with this permit, may inspect or copy any records that must be maintained under the terms and conditions of this permit, and may obtain samples of groundwater, surface water, or injection fluids. 2. Department representatives shall have reasonable access for purposes of inspection, observation, and sampling associated with injection and any related facilities as provided for in N.C.G.S. 87- 90. 3.. Provisions shall be made for collecting any necessary and appropriate samples associated with the injection facility activities. PART VII - MONITORING AND REPORTING REQUIREMENTS 1 The proposed monitoring plan included in the application shall be followed. All sample results shall be submitted to the Aquifer Protection Section's Asheville Regional Office and the Raleigh Central Office. Any monitoring (including groundwater, surface water, or soil sampling) deemed necessary by the Division of Water Quality to ensure surface and ground water protection, will be established and an acceptable sampling reportir�g schedule shall be followed. 2. The Permittee shall submit an Injection Event Record within 30 days of completing each injection. 3. The Permittee shall produce a final project evaluation within 9 months after completing all injection -related activity associated with this permit or produce a project interim evaluation before submitting a renewal application for this permit. This document shall assess the injection projects findings in a written summary. The final project evaluation shall also contain monitoring well sampling data, contaminant plume maps and potentiometric surface maps. 4. The monitoring. results and the final . project evaluation shall be submitted to: and to: Aquifer Protection Section-UIC Program DENR-Division of Water Quality 1636*Mail Service Center Raleigh, NC 27699-1636 Aquifer Protection Section DENR-DWQ Asheville Regional Office 2090 U.S. Highway 70 Swannanoa, NC 28778 Permit No. W10 100089 JAGE40F6 ver. Jan.2010 A-P/UIC-6 5. The Permittee gliall report by telephone, within 48 hours ofthe occurrence or first knowledge of the occurrence, to the Asheville Regional Office, telephone number 828-296-4500, any of the following: (A)Any occurrence at the injection facility which results in any.unusual operating . circumstances; (B) Any failure due to known or unknown reasons, that renders the facility incapable of proper injection operations, such as mechanical or electrical failures. 6. Where the P ermitte6 becomes aware of an omission of any relevant facts in a permit application, or of any incorrect information submitted in said application or in any report to the Director, the relevant and correct facts or information shall be promptly submitted to the Director by the Permittee. 7. 'hi the event that the permitted facility fails to perform satisfactorily, the Permittee shall take such � immediate action as maybe required by the Director. I PART VIII - PERMIT RENEWAL In order to continue uninterrupt ed legal use of the injection facility for the stated purpose, the Pennittee must submit an application to renew the permit 120 days prior to its expiration date. PART IX - CHANGE OF WELL STATUS I The Permittee shall provide written notification within 15 days of any change of status of an injection - well. - Such a change would include the discontinued use -of a Well for injection. Na well is taken completely out of service, temporarily, the Permittee must install a sanitary seal. If a well is not to be used fo r any purpose that well must be permanently abandoned according to 15A NCAC 2C .0 113, Well Construction Standards.. 2. When operations have ceased at the facility and a well will no longer be used for any purpose, the Permittee shall a�andon that injectiPil well in accordance witl�the procedures. specified;in 15A NCAC 2b .01 f3­(b), including but not limited to the following: (A) All casing and screen mateHals ' may be removed prior to initiation of abandom-nent procedures if such removal will not cause or contribute. to contamination of the groundwaters. (B) The entire depth of each welf shall be sounded before it is scaled to insure freedom from obstructions that 'May interfere with scaling operations.' (C) The well shall be thoroughly disinfected, prior to sealing, if the Director determines that failure to do so could lead to the contamination of an underground source of drinking water. (D) Drilled wells shall be completely filled with cement grout or bentonite grout, which shall PAGE50F6 Pennit No. W10 100089 ANUIC-6 ver. Jan.2010 be introduced into the well through a pipe which extends to the bottom ofthe well and is raised as the well is filled. (E) In the case of gravel -packed wells in which the casing and screens have not been removed, neat -cement, orbentonite grout shall be injected into thewell completely filling it from the bottom of the casing to the top. (F) In those cases when, as a result of the injection operations, a subsurface cavity has been created, each well shall be abandoned in such a manner that will prevent the movement of fluids into or between underground sources of drinking water and in accordance with the term's and. conditions of the permit. (G) The Permittee shall submit a Well Abandonment Record (Form GW-30) as specified in 15A NCAC 2C.0213(h)(1) within 30 days of completion of abandonment. 3. The written documentation required in Part IX (1) and (22) (G) shall be submitted to: Aquifer Protection Section-UIC Program DENR-Division of Water Quality 1636 Mail Service Center Raleigh, NC 27699-1636 PART X — WORKER PRECAUTIONS DURING APPLICATION 1 Some effects reported to be associated with the product proposed to be used are as follows: eye, skin, nose, throat, and lung irritation'. If the product is released into the environment in a way that could result'in a suspension of fine solid or liquid particles (e.g., grinding, blending, vigorous shaking or mixing), then proper personal protective equipment should be used. The application process should be reviewed by an industrial hygienist. to ensure that the most appropriate personal protective equipment is used. 2. Persons working with these products should wear goggles or a face shield, gloves, and protective clothing. Face and body protection should be used for* anticipated splashes or sprays. 3. Eating, drinking, smoking, handling contact lenses, and applying cosmetics should not be per mitted in the application area during or immediately following application. 4. Safety controls should be in place to ensure that the check valve and the pressure delivery systems are working properly. 5. The Material Safety Data Sheets shoulabe followed to prevent incompatible or adverse reactions and injuries. Permit No. WIO 100089 PAGE 6 OF 6 ver. Jan.2010 APIMC-6 APPENDIX B Well Construction Records NoNRESIDENTIAL WELL CONSTRUCTION RECORD North Carolina Department of Environment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 2581 1. WELL CONTRACTOR: BRIAN THOMAS Well Contractor (individual) Name GEOLOGIC EXPLORATION, INC. Well Contractor Company Name STREET ADDRESS 176 COMMERCE BLVD STATESVILLE NC 28625 City or Town State Zip Code 704 . - 872-7686 Area code- Phone number 2. WELL INFORMATION: SITE WELL ID #(if applicable) MW-39 STATE WELL PERMIT#(if applicable) DWQ or OTHER PERMIT #Cif applicable) WELL USE (Check Applicable Box) Monitoring ZI MunicipaltPubliG r-1 Industdal/Commercial LI Agricultural Ei Recovery El Injection 0 IrrigationEl Other 0 (list use) DATEDRILLED 07/27/10-07/28/10 TIME COMPLETED AM El PM [I 3. WELL LOCATION: CITY: FAIRVIEW COUNTY UNION 1396 CHARLOTTE HIGHWAY 28730 (Street Name, Numbers, Community, SubdhAslon, Lot No., Parcel, Zip Code) TOPOGRAPHIC / LAND SETTING: E]Slope []Valley []Flat []Ridge E] Other (check-appropiriate bax) LATITUDE May be in degrees, minutes, seconds or LONGITUDE in a decimal format Latitude/longitude source: EiGPS Ei Topographic map (location of well must be shown on a USGS topo map and attached to this form if not using GPS) 4. FACILITY- is the name of the business where the well is located. FACILITY ID #(if applicable) NAME OF FACILITY TYCO ELECTRONICS STREETADDRESS 1396 CHARLOTTE HIGHWAY FAIRVIEW NC 28730 City or Town State Zip Code CONTACT PERSON TYCO ELECTRONICS, INC MAILING ADDRESS 1396 CHARLOTTE HIGHWAY FAIRVIEW NC 28730 City or Town State Zip Code Area code - Phone number 5. WELL DE TAILS: a. TOTAL DEPTH: 60-0 FEET b. DOES WELL REPLACE EXISTING WELL? YESo NOE] c. WATER LEVEL Below Top of Casing: 39.0 FT. (Use "+" if Above Top of Casing) d. TOP OF CASING IS 0.0 FT. Above Land Surface* *Top of casing terminated atlor b�low land surface may reqUire a variance in accordance with 15A NCAC 2C.01 I B. e. YIELD (gipmy NIA METHOD OF TEST N/A f. DISINFECTION: Type NIA -Amount N/A g. WATER ZONES (depth): From To From To From�__To From To From To From To 6. CASING: Thickness/ Depth Diam er WOht Material From 0.0 To 30.0. Ft. 2 INCA SC 40 PVC From To - Ft._ From To Ft._ 7. GROUT: Depth Material Method From 0.0 To 26.0 Ft. Portland bentonite I SLURRY From To -Ft__ From To Ft 8. SCREEN: Depth Diameter Slot Size Material From 30.0 To 50-0 Ft. 2.0 in. -010 - in. PVC From To Ft. in. - in. From To Ft. in. _ in. 9. SANDIGRAVEL PACK: Depth Size Material From 28.0 To 50.0 Ft. 20-40 FINE SILICA SAND From -To- Ft._ From To Ft. 10. DRILLING LOG From To Formation Description 0.0 1.0 ASPHALT/GRAVEL 1.0 5.D BROWN SILTY CLAY 5.0 23.0 RED SILTY CLAY 23.0 41.0 TAN SILTY CLAY 41.0 50.0 TAN SILT CLAY/PARTIAL WEATHER ROCK 11. REMARKS: BENTON ITE SEAL FROM 26.0 TO 28.0 FT E I ER F HAT H EL A CONSTRUCTED IN ACCORDANCE WrrH S CONS- U0 ""' "LLUY"�� "" ffll'�W TA �OPYOF' H� y T T T SW 0 By C L C C T is K-, A E R 'ON AN �RD AND �THAO W L 00" T ST s P C. B� � I D OWNER As E Rov DE To 08/11 11 0 .4 I ATURE OF CERTIFIED WELL CONTRACT R DATE BRIAN THOMAS PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Form GW-1b 1617 Mail Seirvice Center- Raleigh, NC 27699-1617 Phone No. (919) 733-7015 ext 668.- Rev. 7105 5.. NONRESIDENTIAL WELL CONSTRUCTION RECORD North Carolina Department of Environment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 2581 1. WELL CONTRACTOR: BRIAN THOMAS Well Contractor (Indi%,idual) Name GEOLOGIC EXPLORATION, INC. Well Contractor Company Name STREET ADDRESS 176 COMMERCE BLVD STATESVILLE NC 28625 City or Town State Zip Code (704 - 872-7686 Area code- Phone number 2. WELL INFORMATION: SITE WELL ID#(if applicable) MW-40 STATE WELL PERMIT#(if applicable) DWQ or OTHER PERMIT #(if applicable) WELL USE (Check Applicable Box) Monitoring gi Municipal/Public El Ind ustdal/Commerci al Ei Agriculturalo Recovery E] Injection IrrigationD Other E] (list use) DATEDRILLED 07/27/10-07128110 TIMECOMPLETED AM Ei PM D 3. WELL LOCATION: CITY.. FAIRVIEW COUNTY UNION 1396 CHARLOTTE HIGHWAY 28730 (Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code) TOPOGRAPHIC / LAND SETTING: E]Slope oValley L]FIat E]Ridge C] Other -- ­ - - -(check appropriate -box) LATITUDE M be in degrees, minutes, seconds or LONGITUDE in a decimal fornnat. Latitude/longitude source: EiGPS [:iTopographicrnap (location of well -must be shown on a USGS topo map and attached to this form ff not using GPS) 4. FACILITY- is the name of the business where the well is lorated. FACILITY ID #(if applicable) NAME OF FACILITY TYCO ELECTRONICS STREET ADDRESS 1396 CHARLOTTE HIGHWAY FAIRVIEW NC 28730 City or Town State Zip Code CONTACT PERSON TYCO ELECTRONICS, INC MAILING ADDRESS 1396 CHARLOTTE HIGHWAY FAIRVIEW NC 28730 City or Town State Zip Code Area code - Phone number 6. WELL DETAILS: - a. TOTAL DEPTH: 51.0 FEET b. DOES WELL REPLACE EXISTING WELL? YES 0 NO [D c. WATER LEVEL Below -fop of Casing: 39.0 FT. (Use "+" if Above Top of Casing). d. TOP OF CASING IS 0.0 FT. Above Land Surface *Top of casing terrninated atlor below land surface may require a variance in accordance vAth 15A NCAC 2C .0118. e. YIELD (gpm): NIA METHOD OF TEST N/A f. DISINFECTIOM: Type N/A Amount NIA g. WATER ZONES (depth): From -To- From- To From To From To From -To- From- To 6. CASING: Thickness/ Depth Diam er WePht Material From 0-0 To 31 .0 Ft. 2 INCA SC 40. PVC From To- Ft._ From To Ft._ 7. GROUT: Depth Material Method From 0.0 To 26.0 Ft. Portland bentonite SLURRY From To Ft. Frorn-_ To Ft. 8. SCREEN: Depth Diameter Slot Size Material From 31 .0 To. 51,0 Ft. 2-0 in. .010 - in. PVC From To Ft. -in. - in. From- To- Ft. in. - in. 9. SANDIGRAVEL PACK: Depth Size Material From 28.0 To 51.0 Ft. 20-40 FINE SILICA SAND From To Ft._ From To- Ft. 10. DRILLING LOG From To Formation Description 0.0 1.0 ASPHALT/GRAVEL 1.0 6:0 BROWN SILTY CLAY 6.0 24.0 RED SIL TIY CLAY 24.0 40.0 TAN §ILTY CLAY 40.0 51.0 TAN SILT CLAYIPARTIAL WEATHER ROCK 11. REMARKS: BENTONITE SEAL FROM 26.0 TO 28.0 FT I DO HEREBY CERTIFY THATTHIS WELLWAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS S BEEN PROVIDEDTOTHE W -LOWNER. 08/11/10' FIEDNVf-L1!6M�%1 DATE BRIAN THOIAAS PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit the original to the Division of Water Quality within 30 days. Attn: information Mgt., Form GWA b 16417 Nflail Service Center- Raleigh, NG 27699-161 71 P�ioi-[eNo.(919)733-7104..5ext568. Rev. 7/05 NONRESIDENTL�a WELL CONST* RUCTION RECORD 6 :M North Carolina Department of Environment and Natural Resources- Division of Water Quality WELL CONTRACTOR CERTIFICATION # 2581 1. WELL CONTRACTOR: BRIAN THOMAS Well Contractor (Individual) Name GEOLOGIC EXPLORATION, INC. Well Contractor Company Name STREET ADDRESS 176 COMMERCE BLVD STATESVILLE NC 28625 City or Town State Zip Code (704 - 872-7686 Area code- Phone number 2. WELL INFORMATION: SITE WELL ID*(if applicable) MW-41 STATE WELL PERMIT#(if applicable) DWQ or OTHER PERMIT #(if applicable) WELL USE (Check Applicable Box) Monitoring 91 Municipal/Public[] lndustdal/CommercialEl AgriculturaIE] Recovery El Injection Irtrigation[:3 Other E] (list use) DATE DRILLED 07127/10 - 07/28/io TIME COMPLETED AM E) PM o 3. WELL LOCATION: CITY: FAIRVIEW COUNTY UNION 1396 CHARLOTTE HIGHWAY 28730 (Street Name, Numbers, Community, Subdivision, Lot No., Parcel, Zip Code) TOPOGRAPHIC /LAND SETTING: DSIope ElValley EiFlat E]Ridge E] Other -_ - - - -(check appropriate -box) - LATITUDE May be in degre minutes, seconds dr LONGITUDE in a decimal format Latitude/longitude source: EIGPS Ei Topographic map (location of we# must be shown on a USGS topo map and attached to this form if not using GPS) 4. FACILITY- is t he name of the business where the well is located. FACILITY ID #(if applicable) ' NAMEOFFACILITY TYCO ELECTRONICS STREET ADDRESS 1396 CHARLOTTE HIGHWAY - FAIRVIEW NC 28730 City or Town State Zip Code CONTACT PERSON TYCO ELECTRONICS, INC MAILING ADDRESS 1396 CHARLOTTE HIGHWAY FAIRVIEW NC 28730 City or Town State Zip Code Area code - Phone number 6. WELL DETAILS: a. TOTAL DEPTH: 49-0 FEET b. DOES WELL REPLACE EXISTING WELL? YES 0 NO 91 c. WATER LEVEL Below Top of Casing: 39.0 T. (Use 'Wif Above Top of Casing) d. TOP OF CASING IS 0.0 FT. Above Land Surface* *Top of casing terminated atlor below land surface may require a variance in accordance with 15A NCAC 2C.01 18. e.'YIELD(gpm): N/A METHOD OF TEST N/A f. DISINFECTION: Tipe NIA Amount N/A 9. WATER ZONES (depth): From- To- From- To From- Tc- From- To From- To- From - To 6. CASING: Thickness/ .. Depth Diam er WeAt Material From 0-0 To 29.0 Ft. 2 INCO SC 40 . PVC From- To- Ft.- From- To- Ft-_ 7. GROUT: Depth Material Method From 0.0 To 25.0 Ft. Portland bentonite SLURRY From To- Ft. From To Ft. 8. SCREEN: Pepth Diameter Slot Size Material From 29-0 To 4 9.0 Ft. 2.0 in. .010 in. PVC From- To - Ft.- in. - in. From- To Ft. in. _ in. S. SANDIGRAVEL PACK: Depth Size Material From 27.0 To 49.0 Ft. 20-40 FINE SILICA SAND From To Ft. From -To- Ft. 10. DRILLING LOG From To Formation Description 0.0 1.0 ASPHALT/GRAVEL 1.0 6.0 .13ROA SILTY CLAY 6.0 24.0 RED SILTY CLAY 24.0 49.0 TAN SILTY CLAY 11. REMARKS: BENTON ITE SEAL FROM 25.0 TO 27.0 FT' I DO HEREBY CERTIFY THATTHIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS �RRE S BEEN PROVIDED TO THE WELLDWNER. Ir 08/11/10 AIQED VWA A" 'L-- DATE 13RIAN THOMAS PRINTED NAME OF PERSON CONSTRUCTING THE WELL Submit the original to the Division of Water Quality within 30 days. Attn: Information Mgt., Jnl� Form GW-1 b Mail Seirvice Cen'ter - Raleigh, NO 27699-i 6117 Phone No. (919) 733-7015 ext 568. Rev. 7/05 APPENDIX C Lithology Logs WELL NUMk3t:K MVV-,IUVV I En I ENZYME" I Raw rem PAGE I OF 2 L ENGINEERING YDROGEO LOGY ------- - - - ------- CLIENT TEC-Fairview PROJECT NAME Pilot Test Plan PROJECT NUMBER 2281.53 PROJECT LOCATION Fairview, NC DATESTARTED 7/27/10 COMPLETED 7/27/10 GROUND ELEVATION — HOLESIZE 8 DRILLING CONTRACTOR Geologic Exploration — GROUND WATER LEVELS: DRILLINGMETHOD DIEDRICKD120HSA -VAT TIME OF DRILLING 7.Oft LOGGED BY Amy Bondurant CHECKED BY Alec Macbeth AT END OF DRILLING --- NOTES Sunnv and hot, 90's AFTER DRILLING --- Lu (L Lu M WELL DIAGRAM MATERIAL DESCRIPTION Uj M 0-0 Lu Asphalt and gravels 10.6 3'L ------------------------------ SAND-soft, orange red, damp to moist, silty sand SM, trace granules SM 7.0 �Z — — — — — — — — — — — — — — — — — — — — — — — — — --- — — 8 7 -soft to meduim dense, orange, moist to wet, sandy silt to silty sand SP SM. SAND mostly fine grain sand, some silt 6.2 SP_ SM 7.6 ysa — — — — — — — — — — — — — 5.9 — — — — — T silt to si t � SP- ooth drilling .H0 _��,�N_D-soft, wet, sandy d �rn 6.6 25 25 5.4 SP_ 01 SM 0 co 0 LU 3.4 Grout Seal WELL NUMBERM-39WT PAGE OF 2 E: H�y F �Aq I 1� R 14'd' CLIENT TEC-F6!rview PROJECT NAME Pilot Test.Plan. PROJECT NUMBER 2281.53 PROJECT LOCATION Fairview, NO LLI E: F_ W W M . 0 0_0 MATERIAL DESCRIPTION CL -a WELL DIAGRAM W 0- D C6. 0 2i z < co 35 SAND -soft, wet, sandy: silt to(silty sand SP-SM, smooth drilling (continued) Sp- SM Sand#2 40.; .40.0 - — — — — - — — — — — — — — — 2" PVC Sch;' SAND -soft, wzt I silty sand SC -SM, mostly sand, some silt, trace clay 40 0.010" slot 4 . 4 Sc- :SM 45: .48.0 — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — SAND -soft, moist to Wet, silty sand with gravels SPG, increase in gravels at 49.0 2.6 SP ft bgs 50 50.0 1.8 Bottom of hole at 510.0 feet. .0 co LU co WELL NUMBER MW-40WT I PAGE 1 OF 2 E N G IN E E R ING 14 Y DR 0 G E 0 LID Gy CLIENT TEC-Fairview PROJECT NUMBER 2281.53 PROJECTNAME PilotTestPlan PROJECT LOCATION Fairview, NC DATE STARTED 7/27/10 COMPLETED 7/27/10 GROUND ELEVATION HOLE SIZE 8 DRILLING CONTRACTOR Geologic Exploration GROUND WATER LEVELS: DRILLINGMETHOD DIEDRICKD120HSA �Z AT TIME OF DRILLING 6.Oft LOGGED BY Amy Bondurant CHECKED BY Alec Macbeth AT END OF DRILLING NOTES Partly Cloudy, 90's AFTER DRILLING --- Lu a- C� U) z: a_ � uj Lu M 0 Z _j (L 6 MATERIAL DESCRIPTION CL WELL DIAGRAM W _j 2 M D _j :) § co 0 (6 1 :E z z zi IL 0 25 2: 0 3C LU (L M LLj z W .1 3, Asphalt and gravels 1 0 -------------------- -so CC_A� fi, orange re moist to wet, sandy silty clay CL, mostly clay, some silty, trace sand and granules, micaceous. � =90002'mv — — — — — — — — — — — — — — — — — — — — — — — — — — — — — SILT -soft, light orange yellow, wet, clayey sandy silt ML, mostly silt, 0 some fine grain sand, trace clay Milli 5-5-5-5 SS -135.0 (continued Next Page) 0 10 Cement Grout Seal PAGE 2 OF 2 W �551 AN P�7g =Rg I CLIENT TEC-FairvieW 7' PROJECTNAME PilotTestPlan PROJECT NUMBER .2281.53 PROJECT LOCATION Falr�iew, NC W Lu Cl) LU: ?�V D E w M OZ-1 Z) 0 MATERIAL DESCRIPTION WELL DIAGRAM w -12 (L _j > ED 0 2z Oz (D co 35 SAND -dense, orange red,'molst, clayey sandy silt to silty sand SP -SC mostly medium to fine grain sand, some silt,trace clay and gravels, trace relic structures present, micace.ous Sp- S 10-8-12-1 4 0 _d :(20) San #2 40 40.0 - — --- — — — — — — — — — — — — — — — — — — — — - SAND -dense, light. orange'yellow, moist, silty sand.SP -SM,. mostly sand, some silt, saprolite, hard drilling 2" PV.G Sch. :40 0.010" slot 45- SP_- SM p 50 51.0 - - BottoMof-holeat-51.0 feet. _p b q kY 0 (L q LLJ WELL NUMBER MVV-41VV I WA PAGE 1 OF 2 _if_N'_ _G_ I, N -L E* R I _N G' A _Y_ D--R---O--,G- E--O-,--L 0­ G-*--Y- j CLIENT TEC-Fairview PROJECT NAME Pilot Test Plan PROJECT NUMBER 2281.53 PROJECT LOCATION Fairview, NC DATE STARTED 7/27110 COMPLETED 7/27/10 GROUND ELEVATION HOLE SIZE 8 DRILLING CONTRACTOR Geologic Exploration - GROUND WATER LEVELS: DRILLINGMETHOD DIEDRICKD120HSA VAT TIME OF DRILLING 6.Oft LOGGED BY Amy Bondurant CHECKED BY -Alec Macbeth AT END OF DRILLING --- NOTES PartIV Cloudy, 90's AFTER DRILLING --- LU M W (D MAT WELL DIAGRAM zi, Lu M (L 0 ERIAL DESCRIPTION _j :2 z (D U) n Asphalt and gravels, some sand 0.4 3'L ----------------------------------- CLAY-soft, orange yellow, moist to wet, silty clay, mostly clay, some silt, some gravels, micaceous, trace fine grain sand, manganese rich relic structures 0 present CL- 17 ML 9.0 — — — — — — — — — — — — — — — — — — — — — — — — — — SILT -soft to medium stiff, orange red, wet, sandy silt ML, mostly silt, some fine 10 0 grain sand, smooth drilling 20 M L �1.1`11 0 — 0 SILT -medium stiff, light orange red, moist to wet, sandy silt ML, mostly silt, some sand, trace clay, trace gravels to granules, saprolite — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — 1 .4.. .4 2 25 5 ML 30 LU Grout Bentonite Seal W 35 (Continued Next Page) WELL NUMBER MW-41WT V.3 0 IT% ME a 914, 111 PAGE 2 OF 2 G IN E�L!_�I.G ------- - -- YD ROG EO LOG Y :�:LIENT TEC- airview PROJECT NAME Pilot Test Plan PROJECT NUMBER 2281.53 PROJECT LOCATION Fairview, NG Uj T_ CL W c6 0 '1� W W co C) M CL 0 MATERIAL DESCRIPTION WELL DIAGRAM w _j :�E C6 EL Z) 2 z 40 45 0 z Uj SILT -medium stiff, light orange red, moist to wet, sandy silt ML, mostly silt, some J. sand, trace clay, trace gravels to granules, saprolite (continued) Sand #2 2" PVC Sch. 40 0.010" slot ML 0 45.0 0 — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — SILT -hard, light orange red, moist to wet, sandy silt ML, gravels of weathered rock, PWR ML 49.0 0.1 Bottom of hole at 49.0 feet APPENDIX D Waste Manifests and Analytical Results for Drill Cuttings Nov.11. 2010 6:49AM No. 0822 P. 2 Piliase print or type. (FoA desianed for use an elite (12-618l'tirbewdler.1 KnrM AnnrnvArl MR NA grignArl UNIFORM WARDOILIS I. Generator ID Number 2.Pagelof 3, Ernergenty Response Phone 4�-ManifastTmcklngNumbqr,,,: WASTE'MANIFEST �7UZ­fleraloes I Name-anO Mailing Addrm J, rAners(o(,s �b Address (ir different 1han-mailing oddress) "T JOHN -F A Z I Y." TV(,'(" E-V!- ID 1706 )Q1,411 FRA2. F Generatio(a Phone; 6. Transpoder 1 Company Name U.S, EPA ID Number i L Z� 7. T . fanspoder 2 Company Name U.19, EPAID Number B. Designated Facility Name ana Site Address; U.S. EPA ID Number J5 .1 T W. 7 Fadlily'a Phone: 98, Ob. U.S. DOTDescflpdotk jIncluding ProperShippIng Narne, HazardClass, IDNumber, 10. Containers Ii. Total 12. Unit Jim and PacIdnq Group (if any)) WIlVol. 13. Waste Codes NO. Type 1 �1 A %Q'771 HAZ A 1, -TWx-4,,,,j j r C If(l 0 F. 1'7( 2 LU 3. 4. --iFG--Pedal Handling linsir uctions enclAddliforial Informadon j, 15. GENERATOR'SIOFFEROWS CERTIPICATION., I hereby declare that the contents of this con4lgrimeril ate killy and accuraielydosClibed above by the proper shipping name, and are classified, packaged, marked,ond labaled/placarded,and ate in all respects in propet condIllon for t(ansport according to applicable Internationaland national governmenlail reguladons. If BXportEhipmentand I Brn �6 Primary Exporter. I ce* that [he conlenis ofthls consIgnment conlorm to the terms ofthe attached EPAAcknowledgmeni of Consonl. I cetW that [he waste mmimizalfon statement Identified In 40 CFR 262.27(s) (If I am a large quaritilygeneralor) or (b) (Ill am a small quantity generator) fa*hue.. Generalovat0fiefor's PrintedfTyped Name 6ignalure Month Day year j Ilk —InIernadonal T6. ShIP(nenle E] import 10 U.S. apm from U'S.. Pori of entlyPyl- 1 Transporter sIgnsture (for exports on1h. DBle leaving U.S.: 17, TransportarAcknowledlifneril of Rewipi of Materials Transporlar I Pdnie&Tyoed Name Signature ---9(-3nT--Ta-y- Year 'i ;v 11 j k.) -.1. A 1,0. S, Tfa�s�porWr 2 Pd�rftdffyped N�sffle signature Month Day Year f5 il). Discrepancy i8a. Discrepancy Indication Spare El Quantity El Type El Residue El Partial Rojection El Full Rejection Manlfesl. Reference Number 1 Ob. Allemaie Fadily (or Generator) U.8, EPA ID Number LIC Fadli�Ls Phone: Lu 16c. Signature ofAliernale Ricillty, (or Ganersior) Month Day Year Hazardous Waste Report Mariagerrient Method Cod63 (i.e., codes for ha2atdous waste (reatmani, d1sposal, and recycling systems) 4. 20. DeEiansted ftdlilir Owner or Operator CerillIcElon of receipt of hazardous maledaN covered by the manlfesi except as rided in Flem 16a Tgn-M—ffyped N=E­ Signature Month Day Year A T 1 1 =0 A I A= A - � 4 A N6NI A OQQQ ct-11 Q l, Q 1 V " U i..[ !lL,,Jb Vl ill. 1— GIENEWOR'S INITIAL COPY No-v. 11. -2010 6: 49AM No. 0822. P. 3 LAND DISPOSAL RESTRICTIONS (LDR) I of I H ER iTAG E NOTIC5 AND CERTIFICATION ENVIRONMENTAL SER=Es 3eneratoir Name: TYCO ELECTRONICS SVC ID 1706 Manifest Tracking No.: 000362963WAS EPA I.D. No.: NCDO992167.96 (1) Waste Does Not Meet Applicable Treatment Standards: This is a restricted waste that does not meet the applicable treatment siandards set forth In Subpart D of 40 GFR Part 268. I certify that the information provided on this and any additional p ages of this LDR notification is true, accurate and complete. Print Na Authorized Signature: M000 Company[Title: t (2) (3) (4) (5) (6) Manifest Hazardous Waste Codes Wastewater Or Subcategory Underlying Applioable Page/Une Non Wastewater (fl applicable) Goristituanis Certification NVVW 48 YES Subcategory Dosorlp�on 48 TC, WASTE MANAQED IN N ON- SYSTSM Thleformis required for Fool -FOO5 spent solvents, characteristic wastes requiring identificatlonof underlying haiardousconstItuents, orforF039 leachaleonly. For each F001 -FOOS spent solvent, characteristic waste requiring Identification of Underlying hazardous c6nstiluents, or F039 Regulated Consilluent(s) (Che6k all that apply) 1.1 2 1,1.1-TRICHLC 11.1 202 Recei*ved Time Nov.11. 2010 6:56AM No,2393 Nov. I 1. 2010 6: 49AM —L 1. Z21 E� -4 -S :21 0 — ^-D r--) 1:> No, 0822 P. 4 HAZMAT BILL OF - I 1.offisror's ID Number - 2, Page i of 3. Emergenq Response ITWF-- F4T(acklng Number LAMMWIFEST- I I I I ( Suo) 32C.- 11.221 1 1294620-?()'%'1:3 'SOIC ID 1706 �10U FR.A-?,TLrR, T, I A TRjMqL!�nm1qM!dlr% 1706 / JUR 'FlIAZI CHARLOTTE HIGHWAY L;:1l9ci CHARLOTTE HIGHWAY FRI&RQUff, 11(�, 2f,730 CIA I RV I' R erar's Phone: ( 828 100 4 r7EM,, 1,-?*4b — rmnsportee 1 Company Name U.S. EPA ID Number HL"RITACTLE TRAX5PORT, 1'i\V)05-8*,M 114 lil"': R I Q.� U.S. EPA ID Number 4 1 1— 2, Y"M1�0M.111,1TAL SERVICES ILLC -1-1 porIPM0 FOAD CHARLOTTE, HC 2:?2153 acil Phone: (704)391-4500 sa. 9b, U.S. 00TO-EcriPtIonftcludIng Pfoper ShIpping Name, Hazard Class, ID Number, 10. Conialner3 11. Total 12. uAll HM and Pscldng G(odp (il any)) No, Quanlily wlivol. 2. 4. 6. 7 a] HandlipAloqmcflons and Additional Information ER 1 Z KERY TAGE, ( 144 1�4c'71 14. OFFEROR's CERTIFICATION: I hereby declare that the contents or this cansignmenl are fully and accuiataly descdbed above by the pfoper shipping name, and are classlfied, packag&d, marked and labeled1placard9d, and are In all respects In proper condition for [ransporlaccordIng to applIcable International and nallon0l governmerital fagulEll�'18--.1 Offaroes PrIntediTyped Name Signature--) Month Day Year 7�) 13� 15. Transporter AcknoWledgmenl of Recelpj of Ma�-dalS TMASPOW I PrintedlTyped Name Month Day Year 0 /7 Transportar2 PrinleMypedmama A,' �Slqnaiure Month Day Year -7D Discrepanq < - 'sclepan'y; U- ,-�17. Designated Facility Owner a rOperslor Carlificallon of recelpt of hazardous 011) of Lading/Mahirest covered by the manifest except as noted In hem 16 Z P6 I T WN 0 'n' (D ftledffyped Name SIgnature e c e iv d TimenNov, 11,w2010m 15:56,AMmNo. 2393 Month Day "I ^- SRAMPOM OVION�INI^l 1:01101AII011 Tracking Number: Material Name: For Assistance Contact Customer Service: 1-800-881-1098 Material Characterization Profile Section 1: Generator Information Brator Name: Tyco Electronics Corvoration Billing Contact: Sue Brewer Brator EPA ID: NCD099216798 Billing Name: Altamont Environmental, Inc. Pickup Address: 1396 Charlotte Highway Billing Address: 231 Haywood Street Asheville, NC 28801 Technical Contact: Alec Macbeth Billing Phone: 828-281-3350 Phone: 828-281-3350 Billing Fax: 828-281-3351 Fax: 828-281-3351 Mailing Address: 231 Haywood Street Asheville _NC28801 section 2. Material Description & Characteristics Name of Material: Personal protective equipment (e.g., tyveks, nitrile gloves) and decon pit Pl9stic and residue (Drums labeled Vs 1, 4. and 1D Process Generating Material: Drilling borings for monitoring wells Shipping Information: Quantity I Units [I Gallons El Cubic Yards El Tons E] Totes E Drums Per: 0 Once El Day El Month 0 Year Is the material off -specification or discarded commercial product? El Yes ED No If yes, is an MSDS available? El Yes El No El MSDS attached. Is the material a hazardous waste as defined in RCRA (40 CFR 261)? 0 Yes E No If yes, list waste codes: Is the mate rial/wastewate r subject to a CWA Categorical Pretreatment Standa d (40 CFR 400-471)? El Yes E No List: Composition (key compounds, soil, water, PPE, debris, etc.): Used Oil Manag ment Parameters: PPEI to ai)i)rox. 95 % Halogens: BTU Value: Sulfur: Moisture: Plastic sheeting to approx. 4 % 0 �1000 ppm 0 � 2 (13TIL111 000 [b) Mf2% approx. I Sediment residue from decon pit 0:�4000ppm El 2-5 (BTU/1 000 11b) 1:1 to approx. 1 % 0— D 5-9 (BTIJ/1 000 [b) Rebuttable? [19-12 (BTU/1 000 lb) Ash Viscosity (Sus): to % D Yes D No 0 > 12 (BTU/1 000 lb) 0:5 1% N/A 0 N/A I I Description: Color: brown Odor: none —fsical State @ 701F: pH: Specific Gravity: Flash Point: TSS: TDS: ck all that apply) Df2 0 <12.5 0 < 0.8 0 < 1301F El � 200 ppm 0 < 0.5 ppm ree Liquid 0 % to <5 [I a 12.5 00.8-1.2 El < 140*F 0 < 1000 ppm 0 < 1.0 ppm 0 Sludge — % 0<9 11 D � 1.2 El 140 - 200'F El � 5000 ppm D > 1.0 ppm E Solid 100 % D � 2001F D > 5000 Ppm 0 N/A 0 Pumpable — % NIA Pourable % —E] Oil & Grease: El BOD5 E] COD: Ammonia: _ ppm Cyanides: Contains Chelating PCBs? 0 > 100 ppm 0 , 200 ppm Sulfides: _ ppm 0 � 0.02 ppm Agents?: 0 Yes 0 No El > 5% El < 2000 ppm Phenols: ppm 0 < 0.1 ppm 0 Yes 0 No Conc.: NIA D < 7500 ppm _ 0 � 5 pp'm If yes, list: Radioactive? 0 > 7500 PPM 11 � 5 ppm [3 Yes 0 No 0 —ppm Does the material contai n phthalates?: El Yes 0 No If yes, Identity: Section 3: Chemical Constituents: Metals: Metal results below are: M Total E] TCLP BRL: Initial here If all results below are represented as Below Regulatory Levels • Antimony: — PPM 0 Cobalt: — PPM 0 Molybdenum: — ppm 0 Tin: — PPM • Arsenic: — PPM 0 Copper: — ppm D Nickel: — PPM D Titanium: — PPM • Barium: ppm 0 Lead: — PPM 0 Selenium: — ppm D Vanadium: — PPM • Cadmium: PPM 0 Mercury: — PPM D Silver: — PPM El Zinc: — PPM D Chromium: ppm Organics: Organic results below are: E] Total [:1 TCLP BRIL: Initial here If all results below are represented as Below Regulatory Levels 0 Bis(2-ethylhexyl)phthalate: — ppm 0 o-Cresol: — PPM uoranthene: — PPM [I Carbazole: — PPM El p-cresol: — PPM 4,6-Trichlorophenol: — PPM D n-Decane: — rMm D 2,3-DichIoroar0ine. m -tadecane� 100m Section 4: Certification: I certify under penalty of law that this document, all attachments and supporting materials were prepared and presented by me under my direct supervision and that the information provided is a true, accurate and complete representation of the waste materials to be presented for evaluation and management by Shamrock Environmental. Furthermore, I agree that any waste materials managed under any approval issued by Shamrock Environmental pursuant to this request will be transported, delivered and tendered to be in conformance with the material characterization profile. Where Shamrock Environmental determines a material to be non -conforming, the generator shall be responsible for all costs associated with timely return of the material to generator or for other alternate and lawful managemen of he no onforming material conducted on behalf of the generator. Z ............. Alec Macbeth nerator Signature Printed Name Altamont Geologis 9/21/10 Company Name Title Date [I Additional pages attached SEC Profile Rev 03/2010 N, ^_ SHAMPOCK AVICINMINIM COIIOIAIIO� Tracking Number: Material Name: For Assistance Contact Customer Service: 1-800-881-1098 Material Characterization Profile -section 1: Uenerator Intormation ierator Name: Tyco Electronics Corporation Billing Contact: Sue Brewe ierator EPA ID: NCD099216798 Billing Name: Altamont Environmental, Inc. Pickup Address: 1396 Charlotte Highway Billing Address: 231 Haywood Street Asheville, NC 28801 Technical Contact: Alec Macbeth Billing Phone: 828-281-3350 Phone: 828-281-3350 Billing Fax: 828-281-3351 Fax: 828-281-3351 Mailing Address: 231 Haywood Street Asheville, NC 28801 -��-n-2:----------Mat—eri-albes-cription Characteri - stics; NameofMaterial: Soil (soil cuttings) generated from advancing monitoring w9ll borings (Drums labeled #'s 2,3,8 and 10) Process Generating Material: Drilling borings for monitoring -wells Shipping Information: Quantity 4 Units E] Gallons El Cubic Yards El Tons El Totes 0 Drums Per: 2 Once El Day El Month El Year Is the material off -specification or discarded commercial product? El Yes E No If yes, is an MSDS available? El Yes El No El MSDS attached. Is the material a hazardous waste as defined in RCRA (40 CFR 261)? E] Yes 0 No If yes, list waste codes: . - Is the materiallwastewater subject to a CWA Categorical Pretreatment Stand (40 CFR 400-471)? E] Yes Z No List: Composition (key compounds, soil, water, PPE, debris, etc.): Used Oil Manag ment Parameters: soil to approx. 95 % Halogens: BTU Value: Sulfur: Moisture: water to approx. 4 % 0 :S1 000 ppm 0 < 2 (BTU/1000 11b) O�2% approx. 5% VOCs (see lab report for DS-40 and DS-41) [I :S 4000 ppm [12-5 (BTU/1 000 1b) [:15-9 (BTU/1000 11b) 0— to approx. I % to % Rebuttable? D 9-12 (BTU11 000 lb) Ash Viscosity (Sus): D Yes 0 No D > 12 (BTL1/1 000 lb) 0 1 % NIA 0 N/A sc'ipti' on: Color: brown Odor: none Physical State @ 70OF: pH: Specific Gravity: Flash Point: TSS: TDS: ,ck all that apply) D :s 2 [1 <12.5 0 <0.8 0 < 130'F 0 - 200 ppm El < 0.5 ppm 7ree Liquid approx. 4 % 0�5 D a 12.5 00.8-1.2 0 < 140*F 0 < 1000 ppm D < 1.0 ppm [:1 Sludge — % IR Solid aporox. 96 % < 9 13 > 1.2 D 140 - 200'F [I :S 5000 ppm El > 1.0 ppm D Pumpable % 0 > 200*F D > 5000 ppm 0 NIA 10 NIA 0 Pourable % Oil & Grease: El BOD5 Ej COD: Ammonia: _ ppm Cyanides: Contains Chelating PCBs? [I > 100 ppm El < 200 ppm Sulfides: — ppm 121 � 0.02 ppm Agents?: ElYes 0 No 0 > 5% 0 < 2000 pprn Phenols: ppm D � 0.1 ppm D Yes ki No Conc.: N/A 0 :s 7500 pprn _ 0 � 5 pp,m If yes, list: Radioactive? D > 7500 ppm 11 a 5 ppm 0 Yes 0 No 0 — ppm Does the material contain Yes M No If yes, Identify: Section 3: Chemical Constituents: eta s: Metal results below are: E Total E] TCLP BRIL: Initial here if all results below are represented as Below Regulatory Levels D Antimony: — Ppm El Cobalt: Ppm 0 Molybdenum: — PPM 0 Tin: — ppm ED Arsenic: NQ ppm 0 Copper: 47.3- 133 ppm D Nickel: — PPM 0 Titanium: — ppm D Barium: —ppm 0 Lead: 5.2 -17.6 pprn D Selenium: ppm D Vanadium: — Ppm D Cadmium: — ppm 0 Mercury: No - 0.011 ppm 0 Silver: — Ppm 0 Zinc: 68 - 84.9 ppm 0 Chromium: 92-176 ppm Organics: Organic results below are: El Total El TCLP BRIL: Initial here If all results below are represented as Below Regulatory Levels 13 Bis(2-ethylhexyl)phthalate: — IDIOM 11 o-cresol: — ppm 0 Fluorant ene: — PPM 11 Carbazole: — Pprn El p-Cresol: — PPM 11 2,4.6-Trichlorophenol: — ppm D n-Decane I — Dr)m Section 4: Certification: 2,3-Dichloroaniline: M Ictadecane: V-111— I certify under penalty of law that this document, all attachments and supporting materials were prepared and presented by me under my direct supervision and that the information provided is a true, accurate and complete representation of the waste materials to be presented for evaluation and management by Shamrock Environmental. Furthermore, I agree that any waste materials managed under any approval issued by Shamrock Environmental pursuant to this request will be transported, delivered and tendered to be in conformance with the material characterization profile. Where Shamrock Environmental determines a material to be non -conforming, the generator shall be responsible for all costs associated with timely return of the material to generator or for other alternate and lawful ma�ement of the nononforrnmg material conducted on behalf of the generator. . 1%,4 Alec Macbeth ierator Signature Printed Name Altamont Geologist 9/21110 ComDanv Name Title Date 0 Additional pages attached SEC Profile Rev 03LI010 ac Analj&al _www.pacerabs.com September 08, 2010 Mr. Chris Gilbert Altamont Environmental 231 Haywood Street Asheville, NC 28801 RE: Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville', 14C 28078 (704)875-9092 Dear Mr. Gilbert: Enclosed are the analytical results for sample(s) received by the laboratory on August 31, 2010. The results relate only to the samples included in this report. Resul ' ts reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing -was- performed -at -our- Race Huntersville- laboratory -unless -otherwise footnotad. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lord Patton lorri.pafton@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. leco, Page I of 27 G a eAnaljftal :www.pac;elabs.com Project: TEC-PI LOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Ashevilie, NC 28804 (828)254-7176 CERTIFICATIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification 113s 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/LELAP Certification #: 04034 South Carolina Drinking Water Cert. *: 99006003 New Jersey Certification#: NC01 2 Virginia Certification #: 00213 North Carolina Drinking Water Certification *: 37706 Connecticut Certification *: PH-01 04 North Carolina Field Services Certification #: 5342 Flonda/NELAP Certification #: E87627 North Carolina Wastewater Certification #: 12 Kentucky LIST Certification * 84 Pennsylvania Certification #: 68-00784 Louisiana DHH Drinking Water# LA 100031 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 27 'aceAnaiXical" ww.pacelabs.corn Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Sample: DS-40 Lab ID: 9276626001 Collected: 08/31/10 12:46 Received: 08/31/10 14:02 Matrix: Solid Results reported on a "dry -weight" basis Parameters I Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826016035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 81.5 1 09101/10 19:37 67-64-1 Benzene ND ug1kg .4.1 1 09/01/10 19:37 71-43-2 Bromobenzene ND ug/kg 4.1 1 09/01/10 19:37 108-86-1 Bromochloromethane ND ug/kg 4.1 1 09101110 19:37 74-97-5 Bromodichloromethane ND ug/kg 4.1 1 09/01/10 19:37 75-27-4 Bromoform ND ug1kg 4.1 1. 09/01/10 19:37 76-25-2 Bromomethane ND ug/kg 8.1 1 09/01110 19:37 74-83-9 2-Butanone (MEK) ND ug/kg 81.5 1 09/01/10 19:37 78-93-3 n-Butylbenzene ND ug1kg 4.1 1 09/01/10 19:37 104-51-8 sec-Butylbenzene ND ug/kg 4.1 1 09/01/10 19:37 135-98-8 tert-Butylbenzene ND ug/kg 4.1 1 09/01/10 19:37 98-06-6 Carbon tetrachloride ND ug1kg 4.1 1 09/01/10 19:37 56-23-5 Chlorobenzene ND ug1kg 4.1 1 09/01/10 19:37 108-90-7 Chloroethane ND ug1kg 8.1 1 09/01/10 19:37 75-00-3 Chloroform ND ug/kg 4.1 1 09/01/10 19:37 67-66-3 Chloromethane ND ug/kg 8.1 1 09/01110 19:37 74-87-3 "2-Chlorotoluene ND ug/kg 4.1 1 09/01/10 19:37 95-49-8 --)4-Chlorotoluene ND ug/kg 4.1 1 09/01/10 19:37 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 4.1 1 09/01/10 19:37 96-12-8 Dibromochloromethane ND uglkg 4.1 1 09101110 19:37 124-48-1 1,2-Dibromoethane. (EDB) ND-ug/kg -4.1 -1- 09/01/10 19:37 106-93-4 Dibromomethane ND ug/kg 4.1 1 09101/10 19:37 74-95-3 1,2-Dichlorobenzene ND ug/kg 4.1 1 09/01110 19:37 95-50-1 1,3-Dichlorobenzene ND ug/kg 4.1 1 09/01/10 19:37 541-73-1 1,4-Dichlorobenzene ND ug/kg 4.1 1 09/01/10 19:37 106-46-7 Dichlorodifluoromethane ND ug/kg 8.1 1 09101110 19:37 75-71-8 1,1-Dichloroethane ND ug/kg 4.1 1 09/01/10 - 19:37 75734-3 1,2-Dichloroethane ND uglkg 4.1 1 09/01/10 19:37 107-06-2 1,1-Dichloroethene ND ugtkg 4.1 1 09/01/10 19:37 75-35-4 cis-1,2-Dichloroethene ND ug1kg 4.1 1 09/01/10 19:37 156-59-2 trans-1,2-Dichloroethene ND ug/kg 4.1 1 09101110 19:37 156-60-5 1,2-Dichloropropane ND ug/kg 4.1 1 09/01/10 19:37 78-87-5 1,3-Dichloropropane ND ug/kg 4.1 1 09/01110 19:87 142-28-9 2,2-Dichloropropane- ND ug/kg 4.1 1 09/01/10 19:37 594-20-7 I,I-Dichloropropene ND ug/kg 4.1 1 09/01110 19:37 563-58-6 cis-1,3-Dichloropropene ND ug/kg 4.1 1 09/01/10 19:37 10061-01-5 trans-1,3-Dichloropropene ND ug/kg 4.1 1 09101/10 19:37 10061-02-6 Diisopropyl ether ND ug/kg 4.1 1 09/01/10 19:37 108-20-3 Ethylbenzene ND ug/kg 4.1 1 09/01/10 19:37 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 4.1 1 09/01/10 19:37 87-68-3 2-Hexanone ND ug/kg 40.7 1 09/01/10 19:37 591-78-6 lsopropylbenzene (Cumene) ND ug/kg 4.1 1 09/01/10 19:37 98-82-8 p-Isopropyltoluene ND ug/kg 4.1 1 09/01/10 19:37 99-87-6 Methylene Chloride ND ug/kg 16.3 1 09/01/10 19:37 75-09-2 4-Methyl-2-pentanone (MlBK) ND ugtkg 40.7 1 09/01/10 19:37 108-10-1 Methyl-tert-butyl ether ND ug/kg 4tl 1 09/01/10 19:37 1634-04-4 0ate: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS Page 3 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. a OeAnayical www.pacelabs.com Project: TEC-PI LOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC �8804 (828)264-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilie, NG 28078 (704)875-9092 Sample: DS-40 Lab ID: 9276626001 Collected: 08/31/10 12:46 Received: 08/31/10 14:62 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826015036A Volatile Organics Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Tr'imethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-XyIene_ r6mofluoromethane (S) Tbluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Date: 09/0812010 03:44 PM Analytical Method: EPA 8260 ND ug/kg 4.1 1 09/01/10 19:37 91-20-3 ND ug/kg 4.1 1 09/01/10 19:37 103-65-1 ND ug/kg 4.1 1 09/01/10 19:37 100-42-5 ND ug/kg 4.1 1 09/01/10 19:37 630-20-6 ND ug/kg 4.1 1 09/01/10 19:37 79-34-5 ND uglkg 4.1 1 09/01/10 19:37 127-18-4 ND ug/kg 4.1 1 09/01/10 19:37 108-88-3 ND ug/kg 4.1 1 09/01/10 19:37 87-61-6 ND ug/kg 4.1 1 09/01/10 19:37 120-82-1 ND ug1kg 4.1 1 09/01110 19:37 71-55-6 ND ug1kg 4.1 1 09/01/10 19:37 79-06-5 6.9 ug/kg 4.1 1 09/01/1019:37 79-01-6 ND ug/kg 4.1 1 09101/10 19:37 75-69-4 ND ug/kg 4.1 1 09/01/10 19:37 96-18-4 ND ug/kg 4.1 1 09/01/10 19:37 95-63-6 ND ug1kg 4.1 1 09/01/10 19:37 108-67-8 ND ug/kg 40.7 1 09101/10 19:37 108-05-4 ND ug/kg 8.1 1 09/01/10 19:37 75-01-4 ND ug/kg 8.1 1 09/01/10 19:37 1330-20-7 ND ug/kg 8.1 1 09/01/10 19:37 179601-23-1 ND qg/kg --4.1 --1- 09/01/10 19-037- -95-47-6 97 % 70-130 1 09/01/10 19:37 1868-53-7 99 % 70-130 1 09101/10 19:37 2037-26-5 94 % 70-130 1 091Y1/10 19:37 460-00-4 97 % 70-132 1 09/01/10 19:37 17060-07-0 Analytical Method: ASTM D2974-87 47.9 % 0.10 1 09/03/10 11:24 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. IC Cc" Page 4 of 27 a eAnaljdical 0 Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DS-40 Lab ID: 9276626002 Collected: 08/31110 12:46 Received: 08/31/10 14:02 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV TCLP Analytical Method: EPA 8260 Benzene ND ug/L 165 33 09/02110 21:36 71-43-2 2-Butanone (MEK) ND ug/L 330 33 09/02110 21:36 78-93-3 Carbon tetrachloride ND ug/L 165 33 09/02/10 21:36 56-23-5 Chlorobenzene NQ ug/L 165 33 09102/10 21:�6 108-90-7 Chloroform ND ug/L 165 33 09/02/10 21:36 67-66-3 1,4-Dichlorobenzene ND ug/L 165 33 09/02/10 21:36 106-46-7 1,2-Dichloroethane ND ug/L 165 33 09/02/10 21:36 107-06-2 M-Dichloroethene ND ug/L 165 33 09/02/10 21:36 75-35-4 Tetrachloroethene ND ug/L 165 33 09/02/10 21:36 127-18-4 Trichloroethene ND ug/L 165 33 09/02/10 21:36 79-01-6 Vinyl chloride ND ug/L 165 33 09102/10 21:36 75-01-4 1,2-Dichloroethane-d4 (S) 96 % 70-130 33 09/02/10 21:36 17060-07-0 Tbluene-d8 (S) 99 % 67-135 33 09/02/10 21:36 2037-26-5 4-Bromofluorobenzene (S) 98 % 70-130 33 09102/10 21:36 460-00-4 Dibromofluoromethane (S) 98 % 70-130 33 09/02110 21:36 1868-53-7 )Date: 09108/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, . without the written consent of Pace Analytical Services, Inc.. -1 Page 5 of 27 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (828)254-7176 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. WoAnalXical Asheville, NC 28804 ANALYTICAL RESULTS Project: TEC-PI LOT TEST 08/31 Pace Project No.: 9276626 Sample: DS-41 Lab ID: 9276626003 Collected: 08/31/10 12:50 Received: 08/31/10 14:02 Matrix: Solid Results reported on a "alty-weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug1kg 147 1 09/01/10 19:55 67-64-1 Benzene ND ug1kg 7.3 1 09/01/10 19:65 71-43-2 Bromobenzene ND ug1kg 7.3 1 09/01/10 19:55 108-86-1 Bromochloromethane ND ug1kg 7.3 1 09/01/10 19:65 74-97-5 Bromodichloromethane ND ug/kg 7.3 1 09/01110 19:55 75-27-4 Bromoform ND ug1kg 7.3 1 09/01/10 19:55 75-25-2 Bromomethane ND ug1kg 14.7 1 09/01/10 19:55 74-83-9 2-Butanone (MEK) ND ug/kg 147 1 09/01/10 19:55 78-93-3 n-Butylbenzene ND ug/kg 7.3 1 09/01/10 19:55 104-51-8 sec-Butylbenzene ND ug/kg 7.3 1 09/01/10 19:55 135-98-8 tert-Butylbenzene ND ug/kb 7.3 1 09/01/10 19:55 98-06-6 Carbon tetrachloride ND ug/kg 7.3 1 09/01/10 19:55 56-23-5 Chlorobenzene Nb ug/kg 7.3 1 09/01/10 19:55 108-90-7 Chloroethane ND ug/kg 14.7 1 09/01/10 19:55 75-00-3 Chloroform' ND ug/kg 7.3 1 09/01/10 19:55 67-66-3 Chloromethane ND ug1kg 14.7 1 09101/10 19:55 .74-87-3 2-Chlorotoluene ND ug/kg 7.3 1 09101/10 19:55 95-49-8 4-Chlorotoluene ND ug/kg 7.3 1 09/01/10 19:55 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 7.3 1 09/01/10 19:55 96-12-8 Dibromochloromethane ND ug/kg 7.3 1 09/01/10 19:55 124-48-1 1,2-Dibromoethane (EDB) -ND tlg/kg_ 7.3 -11- 09/01/1019:55 -1-06rg.3-4- 51bro-m-om-eth-an-e- Na ug/kg 7.3 1 09/01/10 19:55 74-95-3 1,2-Dichlorobenzene ND ug/kg 7.3 1 09/01/10 19:55 95-5G-1 1,3-Dichlorobenzene ND uglkg 7.3 1 09/01/10 19:55 541-73-1 1,4-Dichlorobenzene ND ug/kg 7.3 1 09/01/10 19:55 106-46-7 Dichlorodifluoromethane ND ug/kg 14.7 1 09101/10 19:55 75�71-8 1,1-Dichloroethane ND ug/kg 7.3 1 09/01/10 19:55 75-34-3 1,2-Dichloroethane ND ug/kg 7.3 1 09/01/10 19:55 1 W-06-2 1,1-Dichloroethene ND ug/kg 7.3 1 09/01/10 19:55 75-35-4 cis-1,2-Dichloroethene ND ug/kg 7.3 1 09/01/10 19:55 156-59-2 trans-1,2-Dichloroethene ND ug/kg 7.3 1 09101110 19:55 156-60-5 1,2-Dichloropropane ND ug/kg 7.3 1 09/01/10 19:55 78-87-5 113-Dichloropropane ND ug/kg 7.3 1 09/01/10 19:55 142-28-9 2,2-Dichloropropane ND ug/kg 7.3 1 09/01/10 19:55 594-20-7 1,1-Dichloropropene ND ug/kg 7.3 1 09101/10 19:55 563-58-6 cis-1,3-Dichloropropene ND ug/kg 7.3 1 09/01/10 19:55 10061-01-5 trans-1,3-Dichloropropene ND ug/kg 7.3 1 bg/ol/lo 19:55 10061-02-6 Diisopropyl ether ND ug/kg 7.3 1 09/01/10 19:55 108-20-3 Ethylbenzene ND. ug1kg 7.3 1 09/01 �11 0 -19:55 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 7.3 1 09/01110 19:55 87-6 8-3 2-Hexanone ND ug/kg 73.3 1 09/01/10 19:55 591-78-6 Isopropylbenzene (Cumene) ND ug/kg 7.3 1 og/ovio 19:55 98-82-8 p-Isopropyltoluene ND ug/kg 7.3 1 09/01/10 19:55 99-87-6 Methylene Chloride ND ug/kg 29.3 1 09101110 19:55 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/kg 73.3 1 09/01110 19:55 108-IQ-1 Methyl-tert-butyl ether ND ug/kg 7.3 1 09/01/10 19:55 1634-04-4 Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of PaceAnalytical Services, Inc.. Page 6 of 27 a CeAn4lyfical Wwwwacehibs.com Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DS-41 LabID: 9276626003 Collected: 08/31/10 12:50 Received: 08/31/10 14:02 Matrix: Solid Resuffs reporfed on a "dty4eight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260/503SA Volatile Organics Analytical Method: EPA 8260 Naphthalene ND ug/kg 7.3 1 n-Propylbenzene ND uglkg 7.3 1 Styrene - ND ug/kg 7.3 1 1,1,1,2-Tetrachloroethane. ND uglkg 7.3 1 1,1,2,2-Tetrachloroethane NID ug/kg 7.3 1 Tetrachloroethene 8.0 ug/kg 7.3 1 Toluene ND ug/kg 7.3 1 1,2,3-Trichlorobenzene ND ug/kg 7.3 1 12,4-Trichlorobenzene ND ug/kg 7.3 1 1,1,1-Trichloroethane 22.7 ug/kg 7.3 1 1,1,2-Tr'ichloroethane ND ug/kg 7.3 1 Tdchloroethene 245 ugtkg 7.3 1 Trichlorofluoromethane ND ug/kg 7.3 1 1,2,3-TrichlorQpropane ND ug/kg 7.3 1 1,2,4-Trimethylbenzene ND ug/kg 7.3 1 1,3,5-T(imethylbenzene ND ug/kg 7.3 1 ,,Jinyl acetate ND ug/kg 73.3 1 chloride ND ug/kg 14.7 1 _,�Lfinyl Xylene (Total) ND ug/kg 14.7 1 m&p-Xylene ND ug1kg 14.7 1 - O-Xylene _ND ug1kg - - 7.3 1 Dibromofluoromethane (S) 98 % 70-130 1 Tbluene-d8 (S) 98 % 70-1 30 1 4-Bromofluorobenzene (S) 95 % 70-130 1 1,2-Dichloroethane-d4 (S) 97 % 70-132 1 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 49.7 % 0.10 1 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACCG,* 09/01/10 19:55 91-20-3 09/01/10 19:55 103-65-1 09/01/10 19:55 100-42-5 09101/10 19:55 630-20-6 09101/10 19:55 79-34-5 09/01/10 19:55 127-18-4 09/01/10 19:55 108-88-3 09/01/10 19:55 87-61-6 09/01/10 19:55 120-82-1 09101/10 19:55 71-55-6 09/01/10 19:55 79-00-5 09/01/10 19:55 79-01-6 09/01/10 19:55 75-69-4 09101/10 19:55 96-18-4 09/01/10 19:55 95-63-6 09101/10 19:55 108-67-8 09/01/10 19:55 108-05-4 09/01/10 19:55 75-01-4 09101/10 19:55 1330-20-7 09/01/10 19:55 179601-23-1 09/01110 19:55 95-47-6 09101/10 19:55 1868-53-7 09/01/10 19:55 2037-26-5 09/01/10 19:55 460-00-4 09/01/10 19:55 17060-07-0 09/03/10 11:24 Page 7 of 27 acMnayical WWW'PaGelabsoom Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800KInceyAve. Suite 100 Huntersvlll�, NC 28078 (704)875-9092 Sample: DS-41 LabID: 9276626004 Collected: 08/31/10 12:60 Received: 08/31/10 14:02 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV TCLP Analytical Method: EPA 8260 Benzene ND ugIL 165 33 09/02/10 21:55 71-43-2 2-Butanone (MEK) ND ug/L 330 33 09/02/10 21:55 78-93-3 Carbon tetrachloride ND ug/L 166 33 09102/10 21:55 56-23-5 Chlorobenzene ND ug/L 165 33 09/02110 21:55 108-90-7 Chloroform ND ug/L 165 33 09/02/10 21:55 67-66-3 1,4-Dichlorobenzene ND ug/L 165 33 09/02/10 21:65. 106-46-7 1,2-Dichloroethane ND ug/L 165 33 09/02/10 21:55 107-06-2 1,1-Dichloroethene ND ug/L 165 33 09/02/10 21:55 75-35-4 Tetrachloroethene ND ug/L 165 33 09/02110 21:55 127-18-4 Trichloroethene ND ug/L 165 33 09/02/10 21:55 79-01-6 Vinyl i chloride ND ug/L 165 33 09/02110 21:55 75-01-4 1,2-Dichloroeth.ane-d4 (S) 96 70-130 33 09102/10 21:55 17060-07-0 Tbluene-d8 (S) 99 % 67-135 33 09/02110 21:55 2037-26-5 4-Bromofluorobenzene (S) 98 % 70-130 33 09/02/10 21:55 460-00-4 Dibromofluoromethane (S) 98 % 70-130 33 09102/10 21:55 1868-53-7 Date: 09/08/2010 �03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. 1� ACC,#. Page 8 of 27 Pace Analytical Services, Inc. Pace Analytical Services, Inc. /5a'XAnalyt 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 . jda1v Asheville, NC 28804 Huntersville, NC 28078 mm.pao-labs.com (828)254-71 i(i (704)875-9092 ANALYTICAL RESULTS Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Sample: DS-39 LabID: 9276626005 Collected: 08/31/10 13:00 Received: 08/31110 14:02 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8 26015036A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 12600 100 09/01/10 23:00 67-64-1 Benzene ND ug/kg 631 100 09/01/10 23:00 71-43-2 Bromobenzene ND ug/kg 631 100 09/01/10 23:00 108-86-1 Bromochloromethane ND ug/kg 631 100 09/01/10 23:00 74-97-5 Bromodichloromethane ND ug/kg 631 100 09101/10 23:00 75-27-4 Bromoform ND ug/kg 631 100 09/01/10 23:00 75-25-2 Bromomethane ND ug/kg 1260 100 09/01/10 23:Ob 74-83-9 2-Butanone (MEK) ND ugtkg 12600 100 09/01/10 23:00 78-93-3 n-Butylbenzene ND ug/kg 631 100 09/01/10 23:00 104-51-8 sec-Butylbenzene ND ug/kg 631 100 09/01/10 23:00 135-98-8 tert-Butylbenzene ND ug/kg 631 100 09/01/10 23:00 98-06-6 Carbon tetrachloride ND ug/kg 631 100 09/01/10 23:00 56-23-5 Chlorobenzene ND ug1kg 631 100 09/01/10 23:00 108-90-7 Chloroethane ND ug/kg 1260 100 09/01/10 23:00 75-00-3 Chloroform ND ug1kg 631 100 09/01110 23:00 67-66-3 Chloromethane ND ug/kg 1260 100 09/01/10 23:00 74-87-3 ',2-Chlorotoluene ND ug/kg 631 100 09/01/10 23:00 95-49-8 )I-Chlorotoluene ND ug/kg 631 100 09/01/10 23:00 106-43-4 1,2-Dibromo-3-chloropropane ND ugtkg 631 100 09101/10 23:00 96-12-8 Dibromochloromethane ND ug/kg 631 100 09/01/10 23:00 124-48-1 4i-2-bibromoethane-(EDB) -ND-ug/kg- 631 —100 09/01110 23:00 106-93-4 Dibromomethane ND ug/kg 631 100 09/01/10 23:00 74-95-3 1,2-Dichlorobenzene ND ug/kg 631 100 09/01/10 23:00 95-50-1 1,3-Dichlorobenzene ND ug/kg 631 100 09/01/10 23:00 541-73-1 1,4-Dichlorobenzene ND uAg 631 100 09/01/10 23:00 106-46-7 Dichlorodifluoromethane ND ug/kg 1260 100 09/01/10 23:00 76-71-8 1,1-Dichloroethane ND ug/kg 631 100 09/01110 23:00 75-34-3 1,2-Dichloroethane ND uglkg 631 100 09/01110 23:00 107-06-2 1,1-Dichloroethene 1270 ug/kg 631 100 09/01/10 23:00 75-35-4 cis-1,2-Dichloroethene 1090 ugtkg 631 100 09101/10 23:00 156-59-2 trans-1,2-Dichloroethene ND ug/kg 631 100 09/01/10 23:00 156-60-5 1,2-Dichloropropane ND ug/kg 631 100 09/01/10 23:00 78-87-5' 1,3-Dichloropropane ND ug/kg 631 100 09/01/10 23:00 142-28-9 2,2-Dichloropropane ND ug/kg 631 100 09/01/10 23:00 594-20-7 I,I-Dichloropropene ND ug/kg 631 100 09/01/10 23:00 563-58-6 cls-1,3-Dichloropropene ND ug/kg 631 100 09/01/10 23:00 10061-01-5 trans-1,3-Dichloropropene ND ug/kg 631 100 09/01/10 23:00 10061-02-6 Diisopropyl ether ND ug/kg 631 100 09/01/10 23:00 108-20-3 Ethylbenzene 2760 ug1kg 631 100 09/01/10 23:00 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 631 100 09/01/10 23:00 87-68-3 2-Hexanone ND ug/kg 6310 100 09/01/10 23:00 591-78-6 Isopropylbenzene (Cumene) ND.ug/kg 631 100 09/01/10 23:00 98-82-8 p-Isopropyltoluene 860 ug/kg 631 100 09/01/10 23:00 99'-87-6 Methylene Chloride ND ug/kg 2520 100 09/01/10 23:00 75-09-2 4-Methyl-2-pentanone (MIBK) ND uglkg 6310 100 09/01/10 23:00 108-10-1 Methyl-tert-butyl ether ND ug/kg 631 100 09101/10 23:00 1634-04-4 ---;Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS Page 9 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. a eAnaoical Wim.pacelabs.rom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NG 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite too Hunt6rsville, NC 28078 (704)876-9092 Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Sample: DS-39 LabID: 9276626005 Collected: 08/31/1013:00 Received: 08/31/1014:02 Matrix: Solid Results reported on a "dry -weight" basis Paramete.rs Results Units Report Limit DF Prepared Analyzed CAS No. Qual 826016035A Volatile Organics Analytical Method: EPA 8260 Naphthalene ND ug/kg 6131 100 09/01/10 23:00 91-20-3 n-Propylbenzene ND ug1kg 631 100 09101/10 23:00 103-65-1 Styrene ND ug1kg 631 100 09/01/10 23:00 100-42-5 1,1,1,2-Tetrachloroethane ND ug/kg 631 100 09/01110 23:00 630-20-6 1,1,2,2-Tetrachloroethane ND ug/kg 631 100 09/01/10 23:00 79-34-5 Tetrachloroethene 21800 ug1kg 631 100 09101110 23:00 127-18-4 Toluene 2860 ug/kg 631 100 09/01/10 23:00 108-88-3 1,2,3-Trichlorobenzene ND ug1kg 631 100 09/01/10 23:00 87-61-6 1,2,4-Trichlorobenzene ND ug/kg 631 100 09/01/10 23:00 120-82-1 1,1,1-Trichloroethane 9520 ug/kg 031 100 09/01/10 23:00 71-55-6 1,1,2-Trichloroethane ND ugfkg 631 100 09/01/10 23:00 79-00-5 Trichloroethene 78100 ug/kg 31600 5000 09/02/10 12:36 79-01-6 Trichlorofluoromethane ND ug1kg 631 100 09/01/10 23:00 75-69-4 1,2,3-Trichloropropane ND ug[kg 631 100 09/01/10 23:00 96-18-4 1,2,4-Trimethylbenzene 3280 ug/kg 631 100 09/01/10 23:00 95-63-6 1,3,5-T(imethylbenzene 1690 ug/kg 631 100 09/01/10 23:00 108-67-8 Vinyl acetate ND ug1kg 6310 100 09/01/10 23:00 108-05-4 Vinyl chloride ND ug/kg 1260 100 09/01/10 23:00 75-01-4 Xylene (Total) 15300 ug/kg 1260 100 09/01/10 23:00 1330-20-7 m&p-Xylene 12300 ug/kg 1260' 100 09/01/10 23:00 179601-23-1 o-Xylene 3010 uglkg 631 100 09101/10-23-00 95-47-6 - - - 151bromofi-w- oromethane (S) 93 % 70-130 100 09/01/10 23:00 1868-53-7 Toluene -dB (S) 96 % 70-130 100 09/01/10 23:00 2037-26-5 4-Bromofluorobenzene (S) 95 % 70-130 100 09101/10 23:00 460-00-4 1,2-Dichforoethane-d4 (S) 85 % 70-132 100 09/01/10 23:00 17060-07-0 Percent Moisture Analytical Meth od: ASTM D2974-87 Percent Moisture 44.8 % 0.10 1 09/03/10 11:24 Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 10 of 27 aceftpical, www.paceAsbs.com Project: TEC-Pl LOT TEST 08131 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DS-39 LablD: 9276626006 Collected: 08/31/10 13:00 Received: 08/31/10 14:02 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) ,—,,,Date: 09/0812010 03:44 PM Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L NID. ug/L 669 ug/L 14400 ug/L ND ug/L 97 % 99 % 101 % 99 % 500 100 09/08/10 13:40 71-43-2 1000 100 09/08/10 13:40 78-93-3 500 100 09/08/10 13:40 56-23-5 500 100 09/08/10 13:40 108-90-7 500 100 09108110 13:40 67-66-3 500 100 09/08/10 13:40 106-46-7 500 100 09/08/110 13:40 107-06-2 500 100 09/08/10 13:40 75-35-4 500 100 09/08 /10 13:40 127-18-4 500 100 09108/10 13:40 79-01-6 500 100 09/08110 13:40 75-01-4 70-130 100 09/08/10 13:40 17060-07-0 67-135 100 09108/10 1 �1:40 2037-26-5 70-130 100 09/08/10 13:40 460-00-4 70-130 100 09108110 13:40 1868-53-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACC,' Page 11 of 27 Mnalj&al iyww. aWab&roM ac" Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Astieville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078. (704)875-9092 Sample: TRIP BLANK. LablD: 9276626007 Collected: 08/31/1000:00 Received: 08/31/1014:02 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 09/02/10 01:32 67-64-1 Benzene ND ug/L 1.0 1 09/02/10 01:32 71-43-2 Bromobenzene ND ug/L 1.0 1 09/02/10 01:32 108-86-1 Bromochloromethane ND ug/L 1.0 1 09/02/10 01:32 74-97-5 Bromodichloromethane ND ug/L 1.0 1 09/02/10 01:32 75-27-4 Bromoform ND ug/L 1.0 1 09/02/10 01:32 75-25-2 Bromomethane ND ug/L 2.0 1 09/02/10 01:32 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 09/02/10 01:32 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 09/02/10 01:32 56-23-5 Chlorobenzene. ND ug/L 1.0 1 09/02/10 01:32 108-90-7 Chloroethane ND ug/L 1.0 1 09/02/10 01:32 75-00-3 Chloroform ND ug/L 1.0 1 09/02/10 01:32 67-66-3 Chloromethane ND ug/L 1.0 1 09/02/10 01:32 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 09/02/10 01:32 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 09/02110 01:32 106-43-4 1,2-Dibromo-3-ch1oropropane ND ug/L 5.0 1 09/02110 01:32 96-12-8 Dibromochloromethane ND ug/L 1.0, 1 09/02/10 01:32 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 09/02/10 01:32 106-93-4 Dibromomethane ND ug[L 1.0 1 09/02/10 01:32 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 09/02/10 01:32 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 09/02110 01:32 541-73-1 1,4�Dichlorobenzene ND ug/L- - 1-.0 1- - -- - - -- -09/02/10 01:32- 1064W.- Dichlorodifluoromethane ND ug/L 1.0 1 09/02/10 01:32 75-71-8 M-Dichloroethane ND ug/L 1.0 1 09/02/10 01:32 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 09/02/10 01:32 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 09/02/10 01:32 75-35-4 cis-1,2.:Dichloroethene ND ug/L 1.0 1 09?02/10 01:32 156-59-2 trans-1,2-Dichloroethene ND ug/L' 1.0 1 09/02/10 01:32 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 09/02/10 01:32 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 09/02/10 01:2�2 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 09/02/10 01:32 594-20-7 IJ-Dichloropropene ND ug/L 1.0 1 09/02/10 01:32 663-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 09/02/10 01-32 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 09/02/10 01:32 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 09/02/10 01:32 108-20-3. Ethylbenzene ND ug/L 1.0 1 09/02/10 01:32 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 09/02/10 01:32 87-68-3 2-Hexanone ND ug/L 5.0 1 09/02/10 01:32 591-78-6 p-isopropyltoluene ND ug/L 1.0 1 09/02/10 01:32 99-87-6 Methylene Chloride ND ug/L 2.0 1 09/02110 01:32 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 09/02/10 01:32 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 09/02/10 01:32 1634-04-4 Naphthalene ND ug/L 1.0 1 09/02110 01:32 91-20-3 Styrene ND ug/L 1.0 1 09/02/10 01:32 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 09/02/10 01:32 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 09/02/10 01:32 79-34-5 Tetrachloroethene ND ug/L 1.0 1 09/02110 01:32 127-18-4 Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pa6e Analytical Services, Inc.. Page 12 of 27 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2226 Riverside Dr. 980OKinceyAve. Sufte'100 aceAnalj&al Asheville, NC 28804 Huntersville, NC 28078 wwwpicelabacom (828)254-7176 (704)875-'9092 ANALYTICAL RESULTS Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Sample: TRIP BLANK LabID: 9276626007 Collected: 08/31/10 00:00 Received: 08/31/10 14:02 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed . CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 09102/10 01:32 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 09/02/10 01:32 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 09/02/10 01:32 120-82-1. 1,1,1-Trichloroethane ND ug/L 1.0 1 09/02110 01:32 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 09102/10 01:32 79-00-5 Trichloroethene ND ug/L 1.0 1 00/02/10 01:32 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 09/02/10 01:32 75-694 1,2,3-Trichloropropane ND ug/L 1.0 1 09/02/10 01:32 96-18-4 Vinyl acetate ND ug/L 2.0 1 09/02/10 01:32 108-05-4 Vinyl chloride ND ug/L 1.0 1 09/02110 01:32 75-01-4 m&p-Xylene. ND ug/L 2.0 1 '09/02/10 01:32 179601-23-1 o-Xylene ND ug/L 1.0 1 09102/110 01:32 95-47-6 4-Bromofluorobenzene (S) 94 % 70-130 1 09/02/10.01:32 460-00-4 Dibromofluoromethane (S) 98 % 70-130 1 09/02/10 01:32 1868-53-7 1,2-Dichloroethane-d4 (S) W % 70-130 1 09/02/10 01:32 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/02/10 01:32 2037-26-5 Date: 09/08/2010 03:44 PM REPORT OF LABORA71 ORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. AGCo, Page 13 of 27 WxAnalXical" Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 l(inceyAve. Suite loo wwwpacelab&pom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-Pl LOT TEST 08/31 Pace Project No.: 9276626 QC Batch: MSV/12107 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV TCLP Associated Lab Samples: 9276626002,9276626004 METHOD BLANK: 492263, Matrix: Water Associated Lab Samples: 9276626002,9276626004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1-Dichloroethene ug/L ND 5.0 09/02/10 11:59 1,2-Dichloroethane ug/L ND 5.0 09/02/10 11:59 1,4-Dichlorobenzene ug/L ND 5.0 09/02/10 11:59 2-Butanone (MEK) ug/L ND 10.0 09/02/10 11:59 Benzene ug/L ND 5.0 09/02/10 11:59 Carbon tetrachloride ug/L ND 5.0 09/02/10 11:59 Chlorobenzene ug/L ND 5.0 09/02/10 11:59 Chloroform ug/L ND 5.0 09/02/10 11:59 Tetrachloroethene ug/L ND 5.0 09/02/10 11:59 Trichloroethene ug/L ND 5.0 09/02/10 11:59 Vinyl chloride ug/L ND 5.0 09/02/10 11:59 1,2-Dichloroethane-d4 (S) % 105 70-130 09/02/10 11:59 4-Bromofluorobenzene (S) % 97 70-130 09/02/10 11:59 Dibromofluoromethane (S) % 103 70-130 09/02/10 11:59 Toluene-d8 (S) % 98 67-135 09/02/10 11:59 LABORATORY CONTROL SAMPLE: - 492264 - Spike LCS LCS % Rec Parameter Units. Conc. Result % Rec Limits Qualifiers 1,1-Dichloroethene ug/L 50 61.6 123 70-141 1,2-Dichloroethane ug/L 50 58 .1 116 70-139 1,4-Dichlorobenzene ug/L 50 62.9 106 70-141 2-Butanone (MEK) ug/L 100 126 126 63-150 Benzene ug/L so 55.6 'I'll 70-132 Carbon tetrachloride ug/L 50 66.5 133 70-150 Chlorobenzene ug/L 50 56.7 113 70-134 Chloroform ug/L 50 58.0 116 70-130 Tetrachloroethene ug/L 50 59.6 119 70-137 Trichloroethene ug/L 50 .56.9 114 70-131 Vinyl chloride ug/L 50 56.7 113 56-144 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 99 70-130 Dibromofluoromethane (S) % 101 70-130 Toluene-d8 (S) % 99 67-135 Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACCo, Page 14 of 27 ace-1 Analytical wmpacelabscom Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: - MSV/12159 Analysis Method: ' EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV TCLP Associated Lab Samples: 9276626006 METHOD BLANK: 494327 Matrix: Water Associated Lab Samples: 9276626006 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersv Ille, NG 28078 (704)875-9092 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1-Dichloroethene ug/L ND 5.0 09/08/10 13:03 1,2-Dichloroethane ug/L ND 5.0 09/08110 13:03 1,4-Dichlorobenzene ug/L ND 5.0 09/08110 13:03 2-Butanone (MEK) ug/L ND 10.0 09/08/10 13:03 Benzene ug/L ND 5.0 09/08/10 13:03 Carbon tetrachloride ug/L ND 5.0 09/08/10 13:03 Chlorobenzene ug/L ND 5.0 09/08/10 13:03 Chloroform ug/L ND 5.0 09/08/10 13:03 Tetrachloroethene ug/L ND 5.0 09/08/10 13:03 Trichloroethene ug/L ND 5.0 09/08/10 13:03 Vinyl chloride ug/L ND 5.0 09/08/10 13:03 1,2-Dichloroethane-d4 (S) % 96 70-130 09/08/10 13:03 4-Bromofluorobenzene (S) % 100 70-130 09/08/10 13:03 Dibromofluoromethane'(S) % 98 70-130 09/08/10 13:03 Toluene-d8 (S) % 98 67-135 09/08/10 13:03 LABORATORY 00NTROLSAMPLE:- -494328 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1-Dichloroethene ug/L 50 53.4 107 70-141 1,2-Dichloroethane ug/L 50 50.8 102 70-139 1,4-Dichlorobenzene ug/L 50 52.9 106 70-141 2-Butanone (MEK) ug/L 100 104 104 63-150 Benzene ug/L 50 52.0 104 70-132 Carbon tetrachloride ug/L 50 54.1 108 70-150 Chlorobenzene ug/L 50 52.9 106 70-134 Chloroform ug/L 50 52.2 104 70-130 Tetrachloroethene ug/L 50 55.4 ill 70-137 Tdchloroethene ug/L 50 56.1 112 70-131 Vinyl chloride ug/L 50 51.4 103 56-144 1,2-Dichloroethane-d4 (S) % 91 70-130 4-Bromofluorobenzene (S) % 102 70-130 Dibromofluoromethane (S) % 96 70-130 Tbluene-d8 (S) % 99 67-135 --,)Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. ACC, Page 15 of 27 ceAnalXical" wmpadelabs.00m ac, Project: TEC-PI LOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. . 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MSW12092 QC Batch Method: EPA 8260 Associated Lab Samples: 9276626007 Analysis Method: Analysis Description: EPA 8260 8260 MSV Low Level METHOD BLANK: 491521 Matrix: Water Associated Lab Samples: 9276626007 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/01110 22:34 1,1,1-Trichloroethane ug/L ND 1.0 09/01/10 22:34 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/01/10 22:34 1,1,2-Trichloroethane ug/L ND 1.0 09/01/10 22:34 1,1-Dichloroethane ug/L ND 1.0 09101/10 22:34 1,1-Dichloroethene ug/L ND 1.0 09/01/10 22:34 1,1-Dichloropropene ug/L ND 1.0 09/01/10 22:34 1,2,3-Tdchlorobenzene ug/L ND 1.0 09/01/10 22:34 1,2,3-Tdchloropropane ug/L ND 1.0 09/01/10 22:34 1,2,4-Trichlorobenzene ug/L ND 1.0 09/01/10 22:34 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/01/10 22:34 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/01/10 22:34 1,2-Dichlorobenzene ug/L ND 1.0 09/01/10 22:34 1,2-Dichloroethane ug/L ND 1.'0 09/01/10 22:34 1,2-Dichloropropane ug/L ND 1.0' 09101/10 22:34 1,3-Dichlorobenzene ug1L ND 1.0 09/01110 22:34 1,3-Dichloropropane ug/L ND 1.0 09/01/10 22:34 1,4-Dichlorobenzene - --ug/L- ND 1.0- 09101/10 22.34 2,2-Dichloropropane ug/L ND 1.0 09/01/10 22:34 2-Butanone (MEK) ug/L ND 5.0 09/01/10 22:34 2-Chlorotoluene ug/L ND 1.0 09/01/10 22:34 2-Hexanone ug/L ND 5.0 09/01/1.0 22:34 4-Chlorotoluene ug/L ND 1.0 09/01/10 22:34 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/01110 22:34 Acetone ug/L ND 25.0 09/01/10 22:34 Benzene ug/L ND 1.0 09/01/10 22:34 Bro'mobenzene ug/L ND 1.0 09/01/10 22:34 Bromochloromethane ug/L ND 1.0 09/01/10 22:34 Bromodichloromethane ug/L ND 1.0 09101110 22:34 Bromoform ug/L ND 1.0 09/01/10 22:34 Bromomethane ug/L ND 2.0 09/01110 22:34 Carbon tetrachloride ug/L ND 1.0 09/01/10 22:34 Chlorobenzene ug/L ND 1.0 09/01/10 22:34 Chloroethane ug/L ND 1.0 09101/10 22:34 Chloroform ug/L ND 1.0 09/01/10 22:34 Chloromethane ug/L ND 1.0 09/01/10 22:34 cis-1,2-Dichloroethene ug/L ND 1.0 09/01/10 22:34 cis-1,3-Dichloropropene ug/L ND 1.0 09101110 22:34 Dibromochloromethane ug/L ND 1.0 09/01/10 22:34 Dibromomethane ug/L ND 1.0 09/01/10 22:34 Dichlorodifluoromethane ug/L ND 1.0 09/01/10 22:34 Diisopropyl ether ug/L ND 1.0 09/01/10 22:34 Ethylbenzene ug/L ND 1.0 09/01/10 22:34 Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. .0 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 27 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 9800 Kincey Ave. Suite 100 aceAna0cal Riverside Dr. www.pacetabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 METHOD BLANK: 491521 Associated Lab Samples: Parameter 9276626007 Units Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers HexachloroA,3-butadiene ug/L ND 1.0 09/01110 22:34 m&p-Xylene ug/L ND 2.0 09/01110 22:34 Methyl-tert-butyl ether ug/L ND 1.0 09/01/10 22:34 Methylene Chloride ug/L ND 2.0 09/01/10 22:34 Naphthalene ug/L ND 1.0 09/01/10 22:34 o-Xylene ug/L ND 1.0 09/01110 22:34 p-Isopropyltoluene ug/L ND 1.0 09/01/10 22:34 Styrene ug/L ND 1.0 09/01110 22:34 Tetrachloroethene ug/L ND 1.0 09/01/10 22:34 Toluene ug/L ND 1.0 09/01/10 22:34 trans-1,2-Dichloroethene ug/L ND 1.0 09/01/10 22:34 trans-1,3-Dichloropropene ug/L ND 1.0 09/01/10 22:34 Trichloroethene ug/L ND 1.0 09/01/10 22:34 Trichlorofluoromethane ug/L ND 1.0 09/01/10 22:34 Vinyl acetate ug/L ND 2.0 09/01/10 22:34 Vinyl chloride ug/L ND 1.0 09/01/10 22:34 1,2-Dichloroethane-d4 (S) % 100 70-130 09/01/10 22:34 4-Bromofluorobenzene (S) % 94 70-130 09/01/10 22:34 Dibromofluoromethane (S) % 95 70-130 09/01/10 22:34 Toluene-d8 (S) % 99 70-130 09/01/10 22:34 LABORATORY CONTROL SAMPLE: Parameter 491522 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 54.3 109 70-130 1,1,1-Trichloroethane ug/L 50 59.2 118 70-130 1,1,2,2-Tetrachloroethane ug/L 50 52.8 106 70-130. 1,1,2-Trichloroethane ug/L 50 59.5 119 70-130 1,1-Dichloroethane ug/L 50 61.7 123 70-130 M-Dichloroethene ug/L 50 62.6 125 .70-132 1,1-Dichloropropene ug/L 50 58.0 116 70-130 1,2,3-Trichlorobenzene ug/L 50 53.3 107 70-135 1,2,3-Trichloropropane ug/L 60 45.7 91 70-130 1,2,4-Trichlorobenzene ug/L 50 52.3 105 70-134 1,2-Dibromo-3-chloropropane ug/L 50 53.3 107 70-130 1,2-Dibromoethane (EDB) ug/L 50 51.6 103 70-130 1,2-Dichlorobenzene ug/L 50 51.3 103 70-130 1,2-Dichloroethane ug/L 50 59.5 119 70-130 1,2-Dichloropropane ug/L 50 54.3 109 70-130 1,3-Dichlorobenzene ug/L 50 51.4 103 70-130 1,3-Dichloropropane ug/L 50 52.4 105 70-130 1,4-Dichlorobenzene ug/L 50 51.3 103 70-130 2,2-Dichloropropane ug/L 50 52.8 106 68-145 2-Butanone (MEK) ug/L 100. 108 108 70-145 2-Chlorotoluene ug/L 50 53.0 106 70-130 �'Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS Page 17 of 27 This report shall not be reproduced, except in full, Without the written consent of Pace Analytical Services, Inc.. ceAnayical www.p4celabs.com Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 LABORATORY CONTROL SAMPLE: 491522 Parameter Units 2-Hexanone ug/L 4-Chlorotoluene ug/L 4-Methyl-2-pentanone (MIBK) ug/L Acetone ug/L Benzene ug/L Bromobenzene ug/L Bromochloromethane ug/L Bromod ichlorom ethane ug/L Brornoform ug/L bromomethane ug/L Carbon tetrachloride ug/L Chlorobenzene ug/L Chloroethane ug/L Chloroform ug/L Chloromethane ug/L cis-1,2-DiGhloroethene ug/L cis-1,3-Dichloeopropene ug/L Dibromochloromethane ug/L Dibromomethane ug/L Dichlorodifluoromethane ug/L Diisopropyl ether ug/L Ethylbenzene ug/L Hexachloro-1,3-butadiene !jg/L m&p�-_Xyl-ene ug/L Methyl-tert-butyl ether ug/L Methylene Chloride ug/L Naphthalene ug/L o-xylene ug/L p-lsopropyltoluene ug/L Styrene ug/L Tetrachloroethene ug/L Toluene ug/L trans-1,2-Dichloroethene ug/L trans-1,3-Dichloropropene ug/L Trichloroethene ug/L Trichlorofluoromethane ug1L Vinyl acetate ug/L Vinyl chloride ug/L 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Toluene-d8 (S) % Date: 09/08/2010 03:44 PM Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROLDATA Pace Analytical Services, Inc. .9800 KinceyAve. Suite 100 Huntersville, NC 28078 (7_04)M-9092 Spike Conc. LCS Result LCS % Rec % Rec Limits . Qualifiers 100 108 108 70-144 50 52.3 105 70-130 100 108 108 70-140 100 ill ill 50-175 50 60.8 122 70-130 50 51.5 103 70-130 50 60.7 121 70-130 50 54.6 109 70-130' 50 52.4 105 70-130 50 55.7 ill 54-130 50 58.9 118 70-132 50 56.4 113 70-130 50 59.3 119 64-134 50 56.4 113 70-130 50 48.8 98 64-130 50 58.7 117 70-131 50 5 2.3 105 70-130 50 53.0 106 70-130 50 57.6 115 70-131 50 57.1 114 56-130 50 54.4 109 70-130 50 55.2 110 70-130 50 50.5 101 -70-130 100 ill ill 70-130 50 54.3 109 70-130 50 54.6 109 63-130 50 52.1 104 70-138 50 51.3 103 70-130 50 53.0 106 70-130 50 48.4 97 70-130 60 53.7 107 70-130 50 58.7 117 70-130 50 58.7 117 70-130 50 53.4 107 70-132 50 56.5 113 70-130 50 59.7 119 62-133 100 107 107 66-157 50 59.7 119 69-130 92 70-130 99 70-130 103 70-130 101 70-130 -REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 27 /5I AnaV�CdD 1ace Wwwpacelabacom Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 491523 491524 IVIS MSD 9276673008 Spike Spike IVIS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Resuft Result % Rec % Rec Limits RPD Qual 1,1-Dichloroethene ug/L ND 50 50 64.2 63.7 128 127 70-166 1 Benzene ug/L ND 50 50 64.1 64.9 128 130 70-148 1 Chlorobenzene ug/L ND 50 60 60.0 58.9 120 118 70-146 2 Toluene ug/L ND 50 50 61.7 61.2 123 122 70-155 1 Trichloroethene ug/L ND 50 50 58.4 57.5 117 115 69-151 2 1,2-Dichloroet,hane-d4 (S) % 101 100 70-130 4-Bromofloorobenzene (S) % 94 92 70-130 Dibromofluoromethane (S) % 98 97 70-130 Tbluene-d8 (S) - % 95 98 70-130 -..,)ate: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, Inc.. Page 19 of 27 Pace Analytical Services, Inc. Pace Analytical Services, Inc. eAnaljftalo 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 QC Batch: MSW12093 Analysis Method: QC Batch Method: EPA 8260 Analysis Description: Associated Lab Samples: 9276626001,9276626003,9276626005 EPA 8260 8260 MSV 6035A Volatile Organics METHOD BLANK: 491594 Matrix: Solid Associated Lab Samples: 9276626001,9276626003,9276626005 Blank Reporting Parameter Units Result Lirriit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug1kg ND 5.0 09101/10 14:22 1,1,1-Trichloroethane ug1kg ND 5.0 09/01/10 14:22 1,1,2,2-Tetrachloroethane ug/ko ND 5.0 09/01/10 14:22 1,1,2-Trichloroethane ugtkg ND 5.0 09/01/10 14:22 1,1-Dichloroethane ug/kg ND 5.0 09/01/10 14:22 1,1-Dichloroethene ug/kg ND 5.0 09/01/10 14:22 1,1-Dichloropropene ug1kg ND 5.0 09101/10 14:22 1,2,3-Trichlorobenzene ug/kg ND 5.0 09101/10 14:22 1,2,3-Trichloropropane ug/kg ND 5.0 09/01/10 14:22 1,2,4-Trichlorobenzene ug/kg ND 5.0 09/01/10 14:22 1,2,4-Trimethylbenzene ug/kg ND 5.0 09/01/10 14:22 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/01/10 14:22 1,2-Dibromoethane (EDB) ug1kg ND 5.0 09101/10 14:22 1,2-Dichlorobenzene ug/kg ND 5.0 09/01/10 14:22 1,2-Dichloroethane ugtkg ND 5.0 09/01/10 14:22 1,2-Dichloropropane ug1kg ND 5.0 09/01/10 14:22 1,3,5-Trimethylbenzene ugfkg ND 5.0 09/01i10 14:22 1,34)i6filor-obenzenhe ug/kg ­N 1� - - -- - -5.6 W10 1 A 6 4: n 1,3-Dichloropropane. ug1kg ND 5.0 09101/10 14:22 1,4-Dichlorobenzene ug/kg ND 5.0 09/01/10 14:22 2,2-Dichloropropane ug/kg ND 5.0 09/01/10 14:22 2-Butanone (MEK) ug/kg ND 100 09101/10 14:22 2-Chlorotoluene ug/kg ND 5.0 09/01/10 14:22 2-Hexanone ug/kg ND 50.0 09101/10 14:22 4-Chlorotoluene ug/kg ND 6.0 09/01/10 14:22 4-Methyl-2-pentanone (MlBK) ugikg ND 50.0 09/01/10 14:22 Acetone ug/kg ND 100 09/01/10 14:22 Benzene ugtkg ND 5.0 09/01/10 14:22 Bromobenzene ug/kg ND 5.0 09/01/10 14:22 Bromochloromethane ug/kg ND 5.0 09/01/10 14:22 Bromodichloromethane ug/kg ND 5.0 09/01/10 14:22 Bromoform ug/kg ND 5.0 09/01/10 14:22 Bromomethane ug1kg ND 10.0 09101/10 14:22 Carbon tetrachloride ug1kg ND 5.0 09/01/10 14:22 Chlorobenzene ug1kg ND 5.0 09101/10 14:22 Chloroethane ug/kg ND 10.0 09/01110 14:22 Chloroform ug[kg ND 5.0 09/01/10 14:22 Chloromethane ug/kg ND 10.0 09/01/10 14:22 cis-1,2.-Dichloroethene ug/kg ND 5.0 09/01/10 14:22 cis-1,3-Dichloropropene ug/kg ND 5.0 09/01/10 14:22 Dibromochloromethane ug1kg ND 5.0 09/01/10 14:22 Dibromomethane ug/kg ND 6.0 09/01/10 14:22 Dichlorodifluoromethane ug1kg ND 10.0 09/01/10 14:22 Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS Page 20 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. a Analjtical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 ce www.pa&elabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 METHOD BLANK: 491594 Associated Lab Samples: Parameter Matrix: Solid 9276626001,9276626003,9276626005 Blank Reporting Units Result Limit Analyzed Qualifiers Dlisopropyl ether ug/kg ND 5.0 09/01/10 14:22 Ethylbenzene ug/kg ND 6.0 09/01/10 14:22 Hexachloro-1,3-butadiene ug1kg ND 6.0 09/01/10 14:22 Isopropylbenzene (Cumene) ug/kg ND 5.0 09/01/10 14:22 m&p-Xylene ug/kg ND 10.0 09/01/10 14:22 Methyl-tert-butyl ether ug1kg ND 5.0 09/01/10 14:22 Methylene Chloride ug/kg ND 20.0 09101 /10 14:22 n-Butylbenzene uglkg ND 5.0 09/01/10 14:22 n-Propylbenzene ug/kg ND 6.0 09/01/10 14:22 Naphthalene ug/kg ND 5.0 09/01110 14:22 o-Xylene ug/kg ND 5.0 09/01/10 14:22 p-Isopropyltoluene ug/kg ND 5.0 09/01/10 14.22 sec-Butylbenzene ug1kg ND 5.0 09/01/10 14:22 Styrene ug/kg ND 5.0 09/01/10 14:22 tert-Butylbenzene uglkg ND 5.0 09/01/10 14:22 Tetrachloroethene ug1kg ND 5.0 09101/10 14:22 Toluene ug/kg ND 5.0 09/01/10 14:22 ,trans-1,2-Dichloroethene ug1kg ND, 5.0 09/01/10 i4:22 trans-1,3-Dichloropropene ug/kg ND 5.0 09/01/10 14:22 Trichloroethene ug1kg ND 5.0 09/01/10 14:22 Trichlorofluoromethane ug1kg ND 5.0 09/01/10 14:22 Vinyrface-t-ate- -ug-/kg-- -ND- 50.0 --09/01/10 14:22 Vinyl chloride ug/kg ND 10.0 09/01/10 14:22 Xylene (Total) ug1kg ND 10.0 09/01/10 14:22 1,2-Dichloroethane-d4 (S) % 103 70-132 09/01/10 14:22 4-Bromofluorobenzene IS) % 96 70-130- 09/01110 14:22 Dibromofluoromethane (S) % 100 70-130 09/01/10 14:22 Tbluene-d8 (S) % 99 70-130 09/01/10 14:22 LABORATORY CONTROL SAMPLE: Parameter 491595 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/kg 50 59.5 119 70-131 1,1,1-Trichloroethane * ug[kg 50 55.6 ill 70-141 1,1,2,2-Tetrachloroethane ug/kg 50 61.3 123 70-130 1,1,2-Trichloroethane ug/kg 50 59.6 119 70-132 M-Dichloroethane ug1kg 50 57.3 115 70-143 1, 1 -Dichloroethene ug[kg 60 55.1 110 70-137 1,1-Dichloropropene ug/kg 50 50.1 100 70-135 1,2,3-Trichlorobenzene ug[kg 50 54.2 108 69-153 1,2,3-Tric - hloropropane ug1kg 50 56.8 114 70-130 1,2,4-Trichlorobenzene ug/kg 50 56.0 .112 55-171 1,2,4-Trimethylbenzene ug/kg 50 55.2 110 70-149 1,2-Dibromo-3-chloropropane ug1kg 50 62.1 124 68-141 1,2-Dibromoethane (EDB) ug/kg 50 59.5 119 .70-130 \---�Date: 0910812010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, withoutt he written consent of Pace Analytical Services, Inc.. Qualifiers Page 21 of 27 aneAnayical www.pacelabs.com Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 LABORATORY CONTROL SAMPLE: 491595 Parameter 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene -Ch.loroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) m&p-Xylene Methyl-tert-butyl ether Methylene Chloride n-Butylbenzene n-Propylbenzene Naphthalene o-Xylene p4sopropyltoluene sec-Butylbenzene Styrene tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene Date: 09/0812010 03:44 PM ug/kg ugtkg ug/kg ug1kg ug/kg ug/kg ugtkg ug/kg ug/kg ug/kg ug/kg ug/kg ug1kg ug/kg ug/kg ug1kg ug/kg ug/kg ug1kg ug/kg ug/kg ug/kg -ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg' ug1kg ug/kg ug/kg ug/kg Units Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville', �C 28804 (828)254-7176 QUALITY CONTROL DATA Spike LCS Conc. Result 50 56.3 50 56.9 5b 55.2 50 55.6 50 56.8 50 56.5 50 53.7 50 55.2 100 108 50 54.2 100 120 50 56.8 100 ill 100 101 50 55.5 50 57.5 50 54.7 50 56.9 50 56.2 50 63.5 50 64.9 50 57.1 -50- 61.8 50 57.1 50 46.4 50 55.7 50 54.5 50 56.0 50 59.5 50 52.7 50 52.5 50 58.7 50 55.2 50 59.5 100 119 60 52.8 50 52.3 50 55.7 50 59.2 50 54.3 50 59.6 50 57.5 50 56.6 50 58.9 50 58.4 50 58.5 50 66.0 50 53.9 LCS % Rec % Rec Limits 113 70-140 114 70-137 110 70-133 ill 70-143 114 70-144 113 '70-132 107 70-142 110 68-152 108 70-149 108 70-141 120 70-149 114 70-149 ill 70-153 101 70-157 ill 70-130 115 70-141 109 70-149 114 70-130 112 70-131 64-136 130 70-154 114 70-135 124- -68-151- 114 70-130 93 70-132 ill 70-140 i oq� 70-137 112 70-130 119 70-136 105 36-148 105 70-139 117 70-137 110 70-145 119 70-141 119 70-140 106 45-150 105 70-133 ill 65-155 118 76-148 109 70-148 119 70-141 115 70-148. 113 70-145 118 70-138 117 70-143 117 70-140 112 70-130 108 70-136 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the wriften consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite loo Huntersville, NC 28078 (704)875-9092 Qualifiers Page 22 of 27 Pace Analytical Services, Inc. a AnaIXical 2225 Riverside Dr. ce vm*pecefabacom Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 LABORATORY COJNTROL SAMPLE: 491595 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers trans-1,3-Dichloropropene ug1kg 50 53.8 108 70-138 Trichloroethene ug1kg 50 55.8 .112 70-132 Trichlorofluoromethane ug/kg 50 58.2 116 69-134 Vinyl acetate ug/kg 100 63.8 64 24-161 Vinyl chloride ug1kg 50 58.9 118 55-140 Xylene (Total) ug/kg 150 178 119 70-141 1,2-Dichloroethane-d4 (S) % 105 70-132.. 4-Bromofluorobenzene (S) % 101 70-130 Dibromofluoromethane (S) % 100 70-130 Tbluene-d8 (S) % 99 70-130 MATRIX SPIKE SAMPLE: 492092 9276654012 Spike MS MS % Rec Parameter Units Result Conc. Result % Red Limits 1,1-Dichloroethbne ug/kg ND .40 45.4 114 49-180 Benzene ug/kg ND. 40 41.8 105 50-166 Chlorobenzene ug/kg ND 40 39.4 98 43-169 Toluene ug1kg ND 40 42.2 101 52-163 Trichloroethene ugtkd ND 40 .41.2 103- .49-167 1,2-Dichloroethane-d4 (S) % 102 70-132 4-Bromofluorobenzene (S) % 97 70-130 Dibromofluoromethane (S) % 100 70-130 Toluene-d8 (S) % 98 .70-130 SAMPLE DUPLICATE: 492093 Parameter 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-DiGhloroethane M-Dichloroethene IJ-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorob6nzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-chloropropane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3, 5-Trimethyl benzene 1,3-Dichlorobenzene I----- �)ate: 09/08/2010 03:44 PM ug/kg ug/kg ug1kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug1kg ug/kg ug/kg ug/kg ug1kg ug/kg ug/kg ug/kg ug/kg Units 9276656001 Result ND ND 'ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Dup. Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 23 of 27 aaeAnayical WWW.Pacelabs.00'm Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Me. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 SAMPLE DUPLICATE: 492093 9276656001 Dup Parameter Units Result Result RPD Qualifiers 1,3-Dichloropropane ug/kg ND ND 1,4-Dichlorobenzene ug1kg ND ND 2,2-Dichloropropane ug/kg ND NP 2-Butanone (MEK) ug/kg ND ND 2-Chlorotoluene ug/kg ND ND 2-Hexanone ugtkg ND ND 4-Chlorotoluene uglkg ND ND 4-Methyl-2-pentanone (MIBK) ug/kg ND ND Acetone ug/kg ND ND Benzene ug/kg ND ND Bromobenzene ug/kg ND ND Bromochloromethane ug/kg. ND ND Bromodichloromethane ug/kg ND ND Bromoform ug/kg ND ND Bromomethane ug/kg ND ND Carbon tetrachloride ug/kg ND ND Chlorobenzene ug/kg ND ND Chloroethane ug1kg ND ND Chloroform ug/kg ND ND Chloromethane ug/kg ND ND cis-1,2-Dichloroethene ug/kg ND ND cis-1,3-Dichloropropene ug1kg ND ND Dibrornochloromethane- ug1kg ND- ND- Dibromomethane ug1kg ND ND Dichlorodifluoromethane ug/kg ND ND Diisopropyl ether ug/kg ND ND Ethylbenzene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Isopropylbenzene (Cumene) ug1kg ND ND m&p-Xylene ug/kg ND ND Methyl-tert-butyl ether ug/kg ND ND Methylene Chloride ug/kg ND ND n-Butylbenzene ug1kg ND ND n-Propylbenzene ug/kg ND ND Naphthalene ug/kg ND ND o-Xylene ug/kg ND ND p-Isopropyltoluene ug/kg ND ND sec-Butylbenzene ugtkg ND ND Styrene ug1kg ND ND tert-Butylbenzene ug/kg ND ND Tetrachloroethene ug/kg ND ND Toluene ug/kg ND ND trans-1,2-Dichloroethene ug/kg N.D ND trans-1,3-Dichloropropene ug/kg ND ND Trichloroethene ug/kg ND ND Trichlorofluoromethane ug/kg ND ND Vinyl acetate ug/kg ND ND Vinyl chloride ug/kg ND ND Date: 09/0812010 03:44 PM REPORT OF LABORATORY ANALYSIS Page 24 of 27 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnayicale www.pacelabs.com Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 . Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA SAMPLE DUPLICATE: 492093 9276656001 Dup Parameter Units Result Result RPD Qualifiers Xylene (Total) ug/kg ND ND 1,2-Dichloroethane-d4 (S) % 102 108 5 4-Bromofluorobenzene (S), % 96 97 1 Dibromofluoromethane IS) % 99 102 3 Tbluene-d8 IS) % 100 100 0 --jDate: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 (704)875-9092 Page 26 of 27 aicieAnalidical. wwwpacelabs cam Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: . PMST/3393 Analysis Method: ASTIVI D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 9276626001,9276626003,9276626005 SAMPLE DUPLICATE: 492733 9276626001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 47.9 47.6 1 SAMPLE DUPLICATE: 492734 9276858005 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 8-.6 11.4 28 R1 Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Servi - ces, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 27 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2MAnayicall" 2225 Riverside Dr. b800 Kincey Ave. Suite 100 wwpacelab&OOM Asheville, NC 28804 Huntersville, NC 28078 (828)264-7176 (704)875-9092 QUALIFIERS Project: TEC-PILOT TEST 08/31 Pace Project No.: 9276626 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to th.e reported data due to changes in.sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unround ' ed data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. ANALYTE QUALIFIERS R1 RPD value was outside control limits. /Date: 09/08/2010 03:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, Inc.. ACC��' Page 27 of 27 /07 eAnalydcal' ";ac, www.pacelabs.com CHAIN -OF -CUSTODY if Analytical I Request Document The Chain -of -Custody is a LEGAL DOCUMENT. Ail relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Report To: N__ __ Attention: Company�� 1409452 'EAJjri4 VA" e-C, �J Ip r- Address Copy To: van VJ company OEM REGPLAToRy. AGENCY-.. 4,1(cm 1,1L PC, I'm I Ad -IIIIIIIIIIM NPDES F GROUND WATER DRINKING WATER r LIST r RCRA r OTHER En& To: . @�SjkW&W F urchase Order No.: Pace Quote w_" 1d Reference: Phri,Fak !IF Project Name; - t-a + Pace Project -Site Location -3-3,50 c Manager. Requested Due DaterrAT,. Project Number Pace Profile P. :$TATE.' equepted.Ahilysis Filtered (Y/N) Section 0 Matrix C E, Required Client Information MATRIX COLLECTED Preservatives Drinking Water DW 0 L) Water 6 0 Waste Water VWT VW COMPOSITE COMPOSITE Produc, t P END/GRAB Soll/Solld SL 0 0 Cn SAMPLE ID oil OL L) a) Wipe WP (A-Z 0.9 Air AR w 0. uJ z 0 Sample IDS MUST BE UNIQUE Tissue TS 0 0 LU 2 Other OT 0 z 0 a) C, 6 `� z IL (L (.) LL -, �L cn ' , C 0 ce C 0 C a) = 1,'?, -7 C C-2 C 0 r- z W Car , DATE TIME DATE TIME U) 4k =),a: z z boa �R I I I I I I 1w Pace Project No./ Lab IA. bc- 4o L G I tol-b 17-qi- 5 do 2 3 JAJ--16 13W 4- -rAp 7 4 e :24 10el 7 6 7 8 9 I I I it 12. ADDITIONAL COMMENTS RELl Q I§NED BY I AFFILIATION DATE. EP. P,PY./AFFIL(ATJON 44C Te. DATE TIME SAMPLE CONDITIONS k 1,(4AA id?(Lu I q_-- 6 Z_ 1 e-%,- >- V 'iA N E ORIGINAL PRINT Name of SAMPLER: Amin& L) .28 E E SIGNATURE of SAMPLER: J___�_RATE Signal I t (MM1DD1YY): JJ 1, Note: By signing this farm you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.51/6 per mont F-ALL-Q-020rev.07, �,�2007 $ampke Condition Upon Receipt keAnafj4ical' Client Name:__/m'___,_ Project # I-,L-7 c 4 2 Where Received: El Huntersvilell Asheville Eden Courier: Fed Ex E] UPS E]USPSeE��Client ElCommercialE] Pace Other P I Custody Seal on Cooler/Box Present: Elyes 2r-no Seals intact: El yes erno :N4R*,,Dber.Wti._' Packing Material: E] Bubble Wrap 2<ub--ble Bags El None []Other W :e Thermometer Uselle!�n#) 14-648-44 Type of Ic I Blue None les on ice, cooling process has begun f < <Enamp Temp Correction Factor: Add C Corrected Cooler Temp.:--- C Biological Tissue is Frozen: Yes No Date and Initials of ersqpXxamining Temp should be above freezing to 6*C Comments: contents: — Chain of Custody Present: �es bNo ON/A 1. Chain of Custody Filled Out: _Q-YL-9_0No ONIA 2. Chain of Custodv Relinquished: r-LW.-. r_1M. FU11A 1.1 Sampler Name & Signature on COC: )21--s -PNO DWA 4. Sampl �s Arrived within Hold Time: 21ee'.0N. ONIA 5. Short Hold Time Analysis (<72hr): DYes 21 r. ON/A 6. Rush Turn Around Time Requested: zf_ �Y-- DNo ONIA 7. Sufficient Volume: _Plres ONo ONIA 8. Correct Containers Used: 21'Yes 0No EIN/A -Pace Containers Used: Vfe-.' ElNo CIN/A 9. Containers Intact: 94rcl No' 0 N/A 10. Filtered volume received for Dissolved tests DYes DNo PWX' "11. Saimple - Labels - m - at . ch COC: - ��es bNo 0 NIA -includes date/timeffi/Analysis Matrix: < 12. All containers needing preservation have been checked. EIY.. CIN. CIN/A' All containers needing preservation are found to be in compliance with EPA recommendation. 45 Yes (_)No ON/A 13. exception.s: VOA, coliform, TOC, O&G, WI-DRO (water). Oyes IFIK. Initial when completed tion: OYes DNo ITNIA 14. Headspace in VIDA Vials (>6Mm): DYes 11]No.,�w 15. Trip Blank Present: DYes DNo P1N1 16. Trip Blank Custody Seals Present DYes DNo Z/A Face Trip Blank Lot # (if purcha ed): Client Notification/ Resolution: Field Data Required? Y N Person Contacted: Dateffime: Comments/ Resolution: Project Manager Review: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wiff'bEi sent to the North Carolin'a DEHNR Certification Off ice ( i.e out of. hold, incorrect preservative, out of temp, incorrect containers) F-ASV-CS-03-Rev.() , alceAnalyfical ".pacelahqom October 08, 2010 Mr. Chris Gilbert Altamont Environmental 231 Haywood Street Asheville, NC 28801 RE: Project: TEC PILOT TEST 09/28 Pace Project No.: 9278539 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KiriceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Gilbert: Enclosed are the analytical results for sample(s) received by the laboratory on September 28, 2010. The results relate only to the samples included in this report. Results reported ' herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the. report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratary- uriless -otherwise-footnoted- All - Microbiological analyses were performed at the . laboratory where the samples were received. If you have any questions concerning this report,. please feel free to contact me. Sincerely, _75r:6�� Lord Patton lorri.patton@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Mithout the written consent of Pace Analytical Services, Inc.. ACCG� Page 1 of 7 a ceAnaiXicalo wmpawa4com Project: TEC PILOT TEST 09/28 Pace Project No.: 9278539 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Connecticut Certification #: PH-0106 Florida/NELAP Certification #: E87648 Massachusetts Certification *: M-NCO30 New Jersey Certification #: NC01 I North Carolina Bioassay Certification #: 9 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800KInceyAve. Sufte100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 CERTIFICATIONS North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pennsylvania Certification #: 68-03578 South Carolina Bioassay Certification #: 99030002 South Carolina Certification #: 99030001 Virginia Certification *: 00072 REPORT OF LABORATORY ANALYSIS 'Page 2 of 7 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ,0 Jceftljtical Wwpacelabscom Project: TEC PILOT TEST 09/28 Pace Project No.: 9278539 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville , NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: TCLPM-01 Lab ID: 9278639001 Collected: 09/28/10 11:05 Received: 09128110 12:00 Matrix: Solid Results repotted on a "dry�weight" basis Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6010 MET 1CP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 10105110 17:40 Arsenic ND mg/L 0.025 1 10/06/10 13:35 10/07/10 13:33 7440-38-2 Barium 1.6 mg/L 0.025 1 10/06/10 13:35 10107/10 13:33 7440-39-3 Cadmium ND mg/L 0.0090 1 10/06/10 13:35 .10107/10 13:33 7440-43-9 Chromium ND mg/L 0.025 1 10/06/10 13:35 10/07110 13:33 7440-47-3 Lead ND mg/L 0.025 1 10106/10 13:35 10/07/10 13:33 7439-92-1 Selenium ND mg/L 0.050 1 10/06/10 13:35 10/07110 13:33 7782-49-2 Silver ND mg/L 0.025 1 10/06/10 13:35 10/07/10 13:33 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 10/05/10 17:40 Mercury NO ug/L 0.20 1 10106/10 15:15 10/08/10 12:01 7439-97-6 Date: 10/08/2010 04:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without1he written consent of Pace Analytical Services, Inc.. Page 3 of 7 acleAnaljtical wwwpacelab&com Project: TEC PILOT TEST 09/28 Pace Project No.: 9278539 QC Batch: MPRP17186 QC Batch Method: EPA 3010 Associated Lab Samples: 9278539001 METHOD.BLANK: 507882 Associated Lab Samples: 9278539001 Parameter Arsenic Barium Cadmium Chromium Lead Selenium Silver mg/L mg/L mg/L mg/L mg/L mg/L mg/L Units Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: Analysis Description: Matrix: Water EPA6010 6010 MET TCLP Blank Result Reporting Limit - Analyzed Qualifiers ND 0.025 10/07/10 12:06 ND 0.025 10/07/10 12:06 ND 0.0050 10/07/10 12:06 ND 0.025 10/07/10 12:06 ND 0.025 10/07/10 12:06 ND 0.050 10/07/10 12:06 ND 0.025 10/07/10 12:06 Pace Analytical Services, Inc. 980OKinceyAve. Suite100 H untersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 607883 Spike LCS LCS .%Rec Parameter Units Conc. Result % Rec Limits Qualifiers Arsenic mg/L 2.5 2.7 109 80-120 Barium mg/L 2.5 2.4 96 80-120 Cadmium mg/L 2.5 2.5 102 80-120 Chromium mg/L 2.5 2.5 102 80-120 -Lead - mg/L 2.5- - -2.4- -- 96- -80120 - Selenium mg/L 2.5 2.9 114 80-120 Silver mg/L 1.2 1.2 96 80-120 MATRIX SPIKE SAMPLE: Parameter 507884 Units 9277836010 Result Spike Conc. IVIS Result IVIS % Rec % Rec Limits Qualifiers Arsenic mg/L ND 2.5 2.3 91 75-125 Barium mg1L 1.9 2.5 -3.4 63 75-125 MO Cadmium mg/L ND 2.5 2.1 86 75-125 Chromium mg/L ND 2.5 2.1 85 75-125 Lead mg/L ND 2.5 2.0 81 75-125 Selenium mg/L ND 2.5 2.3 92 75-125 Silver mg/L ND 1.2 1.0 80 75-125 SAMPLE DUPLICATE: 507885 9277836012 Dup Parameter Units Result Result RPD Qualifiers Arsenic mg/L ND ND Barium mg/L ND .0062J Cadmium mg/L ND ND Chromium mg/L I ND .0027J Lead mg/L ND ND Date: 10/08/2010 04:16 PM REPORT OF LABORATORY ANALYSIS Page 4 of 7 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Acl"� CeAnapical WWWpacekb&OOM Project: TEC PILOT TEST 09/28 Pace Project No.: 9278539 SAMPLEDUPLICATE: 507885 Parameter Selenium Silver .--,,Date: 1010812010 04:16 PM Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA 9277836012 Dup Units Result Result mg/L ND ND mg/L ND ND RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 7 acmnaljftal www.pacelabs.com Project: TEC PILOT TEST 09/28 Pace Project No.: 9278539 QC Batch: MERP/3052 QC Batch Method: EPA 7470 Associated Lab Samples: 9278539001 METHOD BLANK: 507919 Associated Lab Samples: 9278539001 Parameter Units Mercury ug/L LABORATORY CONTROL SAMPLE: 507920 Parameter Units Mercury ug/L MATRIX SPIKE SAMPLE: 507921 Parameter Units Mercury ug/L MATRIX SPIKE SAMPLE: 507923 Parameter Units Mercury ug/L SAMPLE DUPLICATE: 507922 Parameter Units Mercury ug/L Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, N6 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: EPA 7470 Analysis Description: 7470 Mercury TCLP Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.20 10/08/10 11:11 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)87.5-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers . 2.5 2.3 91 80-120 9277836010 Spike IVIS MS % Rec Result Conc. Result % Rec Limits Qualifiers ND 2.6 1.9 75 75-125 9278852001 Spike IVIS MS % Rec Result Conc. Result % Rec Limits Qualifiers ND 2.5 1.7 70 75-125 MO 9277836012 Dup Result Result RPD Qualifiers ND ND SAMPLE DUPLICATE: 507924 9278854001 Dup Parameter Units Result Result RPD Mercury ug/L ND ND Date: 10/08/2010 04:16 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 6 of 7 Pace Analytical Services, Inc. Pace Analytical Services, Ind. ceAnalj4ical 2225 Riverside Dr. 98001<inceyA�e. Suite 100 www.pacelabs.com Asheville, NC 28804 Hu'ntersville, NC 28078 (828)254-7176 (704)875-9092 QUALIFIERS Project: TEC PILOT TEST 09/28 Pace Project No.: 9278539 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenyihydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. - ANALYTE QUALIFIERS Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. Date: 10/08/2010 04:16 PM REPORT OF LABORATORY ANALYSIS Page 7 of 7 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. , , ACCo�. Ju ,l)!2neAnal i� ... �A q1, CHAIN-OF-CUSTODYI/ Analytical Request Document The Chain -of -Custody is a LEGAL DOCOMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: Of Required Client Informatilon, Required Project Information: Invoice Information: Company: Report To: Attention: 1 139 -6561 14 rt, 5 (,-1 L 6LN-L 1 5 vi� is tL e L--,,, t:-,u Address: 2-3, Copy To: 'A tL Company Name: --11U11131 Alw two LLt" L Address: NPDES GROUND WATER DRINKJNGWATFR - LIST RCRA OTHER -t," 5 13 all To: fh Purchasyrder No., Pace Quote 44 Reference: Faic Project P Lf I Name* L Mp.,or!", U �.s fto Lo c a tion P #ATE.�. pRLq' d Due DaterrAT: /5rylect Number. Pace Profile #., [( Sol rf . e:`1�*.;:'-:R qu6S.tedAnal�siifiltai Section D Matrix Codas iR — Required Client Information M lX / CODE 0. N COLLECTED 1-pservarives Drinking Water DW 2 0 11 z LD Water WT Waste W ter WW 0 composviE START COMPOSITE ENDIGRA13 Product P Soll/Solid SL 0 L) 4) SAMPLE ID oil OL Wipe WP Lu z; c: .1 (A-Z, 0-9 Air AR Lu Im Lu z 0 Sample IDS MUST BE UNIQUE Tissue IS 0 C.) Lu z Other OT L< Lu LU 0 a) JX -J 0. 2 0 , 260 CL 0 co Ca lzr5 5 < to DATE TIME DATE TIME < to 0 U r- :D Z 3: CU z cV z 2 6 (2 Pace Project No./ Lab LD TC-L fift-11 5 L e- 3 2- 3. 6 7 9 101 121 ADDITIONAL COMMENTS. RPLINQUIS BY I AFFILIATION T -A CqE PIE BY4 �fk , i F I PIL AT;ON.; TIME SAMPLE CONDITIONS d-e-<I—Acr Q 0 V ---L2 —7- ORIGINAL 0. S— PRINT Name of SAMPLER: E w z DATE Signed SIGNATURE of SAMPLER: E co (MMIDDIYY): Y-2 invoices not paid within 30 days. F-ALL- . Q-020rev.u� a UU7 �it Note: By signing this form you am accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per mc, FiceAna46cal' Client Name: Project #—"L'� Where Received: El Huntersville ;14 rsheville 0 Eden Courier: E] Fed Ex E] UPS E] uspSV�rClient El Commercial El Pace Other 00tional Custody Seal on Cooler/Box Present: Elyes L2"n-o Seals intact: F1 yes 'no Proj. Due D ' ate: Prdj. Name` Packing Material: *.E] Bubble Wrap L�BIZSle Bag's' El None ElOther Thermometer UseT��—VT4.-648-44 Type of lcq(s) Blue None eB-�-amples on ice, cooling process has begun Temp Correction Factor: Add /4u—btra Corrected Cooler Temp.: Lr C Temp should be above freezing to 60C Biological Tissue is Frozen: Yes No Comments: Dateand Initia"f Re. In expnining contents - Chain of Custody Present: 6Yes EIN. ONIA I Chain of Custody Filled Out: _PY—es DNo ON/A 2.- Chain of Custody Relinquished: PYe—s E]No ON/A 3. Sampler Name & Signature on COC: EIY-e, [IN. DNIA 4. Samples Arrived within Hold Time: E!r5e. EIN, ONIA 5. Short Hold Time Analysis (<72hr): []Yes Pilo' DN/A 6. Rush Turn Around Time Requested: O?e—s []No EIN/A 7. 7 0.- '4 to A 0 Sufficient Volume: gWs DNo ON/A 8. Z Correct Containers Used: -Pace Containers Used: -s DNo 12"Fes ONo ON/A ONZA 9. Containers Intact: ples ONo ON/A 10. Filtered volume received for Dissolved tests DYes DNo PVA- 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: s DNo ON/A 12. 13, Initial when completed All containers needing preservation have been checked. ��es DNo ON/A All containers needing preservation are found to be in compliance with EPA recommendation. ZY-e-. ONo EIN/A exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) 11YeV6N. Samples checked for clechlorination: DYes ONo EVIA 14. Headspace in VOA Vials ( >6mm): DYes DNo 9N/A 15. Trip Blank Present: Trip Blank Custody Seals Present [Pace Trip Blank Lot # (if purchased): I DYes DNo DYes ONo - ZWA PKA I 16. - Client Notification/ Resolution: Person . Contacted:-:,V Datefrime: Field Data Required? Y N Comments/ Resolution:, f 'd 10�' "G'c- Nax— 15 CL SCURF Review: SRF Review: Date., LT22 Note: Whenever there is a discrepancy affecting North Caro * lina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification'Office ( Le out of hold, incorrect preservative, out of temp, incorrect containers) F-ASV-CS-03-Rev.02 APPENDIX E Groundwater Development and Sampling Logs 231 HAYWOOD STREET. ASHEVILL.. NC 28801 TEL.82a.281.3350 FAC.820.281.3351 .W-...T T-1 Well Development Log FACII,ITYNAI�E: . TPIC. 1* LOCATION: P-V1 ew FIELD PERSONNEL: DATE: �L -3,1� - (c) ARRIVE TIME: 19,14-8 WEATHER: a4mca-7 -WELL NUMBER. MIN — 51— W WELL DIAMETER: I of . I TYPE OF CASING: 1�%�INT: k LUSH MO STICK-UP C zu� WELL DEPTH IN FEET (WD): 50�0 START TIME: WATER LEVEL IN FEET (wq: 3. Le 0 LENGTH OF WATER COLUMN: FEET (WD) - (WL) � (LWC) ONE CASING VOLUME GALLONS (LWC) x (WCV) THREE CASING VOLUMES:— GALLONS VVJ. =3q-:5 ACTUAL VOLUME DEVELOPED: GALLONS WELL CASING VOLUMES (WCV) 2"=0.17Gal/Ft 3"=0.38Gal/Ft 4"=0.66Gal/Ft 6"=1.5Gal/Ft 8"=2.6Gal/Ft . 12"=5.8Gal/Ft TIME DEVELOPMENT METHOD ESTIMATED FLOW RATE (gpm) GALLONS PURGED pH UNITS SPECIFIC COND. (gs) TEND (C-) DISSOLVED OXYGEN (mg/L) OXIDATION REDUCTION POTENTIAL (Inw-� TURBIDITY (NTU) DEPTH TO WATER (feet TOC) �5b 1 Z cowt 7' LP .015 L4:2- � 6 —,% & Los) - 0 1 J--.SL) 0 92, S;, te- q S, I th.- S-6 2.&0 /2qA-7- (fi OS .1 1 .00 it qz Sad .91 1D. 1Q1 q L( R '3?- w.46 qvf?, I elk .1 -jo.- a U.Lfa i-� NU-3 14.* 10 %:T2-- 4S,l A.20 PROTECTIVE CASING-._R&A PAD: OCK: VEGETATION: PtUW— ACCESS: r"rme F Eldl Signature: Date: Comments: Notes: jiS=micro-Siemen C' = degrees Celsius mg/L = milligrams per liter mv = millivolt NTU = nephelometric turbidity units P:\Templates\GW & Drilling Forms\Well Development Log.xls Page I of I NO 0 1,11 WIN 0 MIAMI I d_ 8; 231 HAYWOOD SVREET. ASHEVILLE. NC 2BB01 V EL.828.281.3350 FAC.828.281.3351 WWW.AL?­ONYC1HVI.aNMK"Y^L.CON Well Develonment Lop & FAciLrrYNANffi-. - 1EG scuem I wT P1 LDT DATE: '11 150 1 IQ LOCATION: ARRIVE TIME: FIELD PERSONNEL: Yk TV-bM C WEATHER: S tin WELLNUNMER: Mw-40-11irr WELL DEPTH IN FEET (WD): START TE�E: WELL DLA0,1ETER; Z"I. WATER LEVEL IN FEET (WL): TYPE OF CASING: PIL LENGTH OF WATER COLUDAN: FEET S OINT: (WD) - (WL) � (LWC) PFLUSHMO /STICK-UP ONE CASING VOLUNE: GALLONS S_ co S: (LWC) x (WCV) THREE CASING VOLUMES: A. -to GALLONS 64� =4 ACTUAL VOLUME DEVELOPED GALLONS WELL C ' ASING VOLUMES (WCV) 2"=0.l7GaL1Ft 3"=0.38Gal/Ft 4"=0.66Gal/Ft 6".=1.5Gal/Ft 8"=2.6Gal/Ft l2"=5.8GaVFt THv1E DEVELOPMENT ESTIMATED GAI-LONS PH SPECIFIC TENT DISSOLVED OXIDATION TURBIDrFY -DEPTH TO NET,40D FLOW RATE (gpm) PURGED UNTrS COND. (C-) OXYGEN REDUCTION (NTU) WATER (gs) (mg/L) POTENTIAL (feet TOC) L2- 10 PUMP ft M I L) Uq* 2 t 1870 IS 4-to ZR,_� I 1-,V% V,, 5 —1 I<co M I:;-- - I �-wl ae. IV -6- _V41 . 1 )40 Goo U, ZZ cz D6.0-79 jbq.2 %ot 221, go A; -3D I U 71— S -7-4 1%-D 680-0 34,1 t, 21 tp. W (F '4 4c 247.1) 4t). 10 -4-4 U- 43 5'7,b 56.0 40"20 PROTECTIVE Ck:-VEGETATI ON: ACCESS: Field Personnel Signature: Date: U V ej VU� +%I ,LV Notes: pLS = micro-Siemen A C'= degrees Celsius n1g/L = milligrams per liter A MV = millivolt NTU = nephelometric turbidity units q &A wcAA v,<At 3.e P.\Templates\GW & Drilling Forms\Well Development Log.xls Page I of 1 CC*(( IOA4%- H 231 HAYWOOD STREET. A.HEVMLE. NC 26801 TEL.828.281.335 0 FA..828,281.3351 WP.11'nPvP1nim..1.+ T -- FACILITY NAME: —rF c- DATE: ;;f V? So It LOCATION: Mw — LH— wr-- - ARRIVE TIME: Into FIELD PERSONNEL: VtrmA.# m:a -M4w-Mw",3t MEATHER: !NV) r) I ( WELLNUMBER: MAP— � WELL DEPTH IN FEET (WD): START TUE: 16Se WELL DIAMETER- TYPE OF CASING: WATER LEVEL IN FEET c- LENGTH OF WATER COLUMN FEET MEASURING POINT: (WD) - (WL) = (LWC) ICUSH =MO STICK-UP ONE CASING VOLUME: GALLONS COMMENTS: (LWC) x (WCV) THREE CASINO VOLUMES:. GALLONS 5%clul"A Vz ACTUAL voLumE DEvELoPED.-4.S GALL . oNs WELL CASING VOLLTNES (wCV) 2"=0.17Gal/Ft 3"=0.38Gal/Ft 4"=0.66Gal/Ft 6"=1.5GalfFt 8"=2.6Ga1/Ft 12"=5.8Gal/Ft TIME DEVELOPMENT METHOD ESTIKATFD FLOW RATE (gpm) GALLONS PURGED pH UNITS SPECIFIC COND. TENT (CO) DISSOLVED OXYGEN OXIDATION TURBIDITY DEPTH TO REDUCTION NTU) WATER (PS) �mg/L) _POTENTIAL (feet TOC) 105V DIU" a DAw AA 11-011 j &( .,U I L 2A. 2— 5&4 -C IS.--b LQ f3tV Ij -L 110.015 9. 13b - q- 3W.11 26 HUI 0c I Le-7. A ZC) U-01 kl kq-1 ZAS IS4. -50 10.61 SQ ((P. L�, a Lf 1 43 :0: to-, f) I 'EV5. A5.). 7,5.7.(,* _— 1 c---s PROTECTIVE CASING: PAD: L 0 CK._,/VE GETATI ON: Vu ACCBSS: lField Personnel Signature: Date: C.---6- UAO A4 —1� Notes: AS—micro-Siemen wo� OL V— C' � degrees Celsius mg/L = milligrams per liter �14 %V1-41'- MV = millivolt NTU � nephelometric turbidity units M. P:\Templates\GW & Drilling Forms\Well Development Log.xis Page I of 1 231 HAYWOOD STREET. ASH.1111E. C 28E)01 TEL.82B.281.3350 FAC.828.281.3351 WWW.ALTAM0P1TMNVJR0NMENTAL.C.M Equipment Documentation & Instrument Calibration Data Sheet Equipment Documentation EaUiDment or meters used tn t;ikp mpnciir�mn�f- 1. q -.f— Equipment Type Serial Number Brand Date of Use 150-ft Water Level 26154 Solinist 150-ft Water Level 22754 Solinist 0- Water L vel 150 Testwell 15.0-ft Drawdown MP30-1527 QED Other Micro TPW Turbidity Meter ers, survey equipment, etc.): Calibration Standards Exp Date Instrument Serial # Instrument Reading 0.02 NTU 10.0 NTU 1000 NTU och �10(1 QQQ6et&n. 07-1 051 &V Initial: o. o3 Initial: Initial: 003 Cal: 6 .07' Cal: I q5— - Cal: 1. 5 TIMEk, YSI 556 Mult!Darameter Meter Instrument Serial Number 07D100979 Instrument Readings Calibration Expiration Date Dissolved Oxygen Initial: 9'at Cal: mr0g: T me, fma. � NA QC* AM Time: Meas: - Mid Day Timd: Check: PM Time: Check:. NA pH 7 S.U. report to 0.1 5.U. Initial: It . Cal. -7 M Time: pH 4 S.U. report to Initial: L[LUf Cal: Time: 0.1 5.U. pH 10 S.U. report to 0.1 5.U. 'JA Initial: Cal: QC* pH 7 S.U. report M Time:844TIMeas: Ig)l 1MId Day Time: Check: PM Time:. Check: to 0.15. U... Spec.Cond Initial- Ca: Time: 447184123 rn�** "'Le QC* 84 mS AM Time Meas: Mid Day Time: Check: PM Time: �C h �ec k: L--ORP 200 /�'V Cal: nature: Note 1. Electronic 1p e/h'tc/arbkrate/d according to tftt4nanufacturer's operation manual. NIP 2. Specific Cond�uci,�ity should be calibrated according to values representative of historic range. 3. Order of Calibration is as follows : Specific Conductivity, pH 7, pH 4, pH 3.0, OkP, QC checks. 4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If readings are out of these ranges, meter needs to be r6calibrated. 5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours. 6. ** Indicates to choose a Specific Conductivity buffer of 447, U04, or 23 mS which is closest to historical readings from the project locatic P:VI`ernpIates\GW-DrIII Ing Forms\Calibration Data Sheet YSI 556-Rev I Page I of 1 231 HAYWOOD STREET, AsHEVILLE. NC 28801 TEL.82B.281.3350 FAC.828.281.3351 WWW.�L.'r�t4QNTFNVKROr4MEr4TAL..=�M Low -Flow Sampling Data Sheet Project Name: Well M. -M'VV - 3 1 VU'T- Project Number:' Screen Interval: bgs Personnel: Depth to Water: -toe Stickup: Date: 61),110 Depth of Pump Intake:' L�L) toe Drawdown Set: toe Arrive at Well: J . 11 A Start Time: -11 E53 Sample Time: Finish Sample Time: Leave Well: Time DTW (feet) Temp (0c) Conductivity (PS) DO (mg/L). pH (S.U.) ORP (MV) Turbidity NTU Le I 12'A 53 I a - 0 k 5,11 1 LQ- 5 041.4 t1sl S 1 4 Is ALP lo.9-0 5.5 3 V1q, 3 4 41 . 2� 12`2- E-95 msl q qq 2-, t 3to. -1 0 B Z, C) I L-) 18, 2)5 2-Mle O�IL+ slio V-7, `3, 2, 3 ta kT [ 0-3 _35 - 35 3,2-k S't'o zaeq­ 22-u -3,% .5 �oi 0 1 B. &E- 2.q 1Z V 90. ST"ILTZAT[ON 3 successive readings, 3 minutes apart: within +/- 10% DO and Wbidity; +1-3%Conductivity; +1-0.1pHunit, +A10;nVfoF0RP from EPA - Low -Flow Winimal Drawdown) Groundwater Sampling Procedures, April 1996 Time between discharge cycles during sample collection: 40 SCC- Comments: "Mple Sampling Technician Name: Sianature: 29 P:\Templates\GW & Drilling Forms\Low Flq)#'�Opling Form—Rev-l.xls Project Name: -W(, Project Number: Personnel: Date: 231 HAYWOOD STREET, AsHEVILLE. NC 2B801 TEL.828.281.3350 FAC.B28.2BI.3351 WWW.AL.YAblaNYF-MVllRCr4MENYA�.=QM Low -Flow SampUng Data Sheet WellID: WIJ4- 011;-rl— Screen Interval: 5t-:31 bgs Depth to Water: toe Stickup:. Depth of Pump Intake: toe YlvavuAnwirn Qdh*e trv- Arrive at Well: i 0-5R5 Start Time: Sample Time: Finish Sample Time: Leave Well: Time DTW (fe et Temp KY., Conductivity (AS) DO (mg/L) I PH (S.U.) ORP (mv) Turbidity NTU �2(9' OT JS2, k4l -7'5� 07- 3 5 (D 5, (0 4 5 4, 13 91 5-S �51 -3 194.0 43, 81 _4 I 1 19-00 5 '2- TO. 0 3,3, co L 3 F) 1(g 82 .210.5 C23 1 qv�? STABILIZATION 3 successive readings, 3 minutes apart: within +/- 10% DO and turbidity; +1-3%Co.—.ducdv.-ty; +1-0JpHUnit;- +A10M.Vf0.rO-JLP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 time between discharge cycles during sample collection: Comments: ple name: JAN 0 If V1, Sampling Technician Name: Ainv fmdMA(7Ui14 Signature: P:\Templates\GW & Drilling Forms\Low Flow Sampling Forrn—Rev-1.xls Project Name: "Tcc' Project Number: Personnel: Date: ALTAmONT ENVIRONMENTAL, INC. A 231 HAYWOOD STREET, AsHEVILLE. NC 2BB01 TEL.B28.281.3350 FAC.B28.2B1.3351 WWW.AL.IrAMOMTEr4vlkor4mwmyAL..=�m Low -Flow Sampling Data Sheet I I Well ID: IAYq -4 Screen Interval: iAll - 2_cJ . bgs Arrive at Well: Start Time: 0 Dep�h to Water: Sample Time: L?3Le Stickup: Finish Sample Timet Depth of Pump Intake: 31-0 toc Leave Well: 1063 1prawdo n Set: -LOC Time DTW (feet) Temp (oC) Conductivity .(9S) DO (1ng/L) pR (S.U.) ORP (m:V) N� Turbidity NTU 160'9 io 19 33S 8,(9 1 10M 1000 0 Z3 1.1 - s (e 1CRO.s L)= _0 3�35 13-15 q 3 WA -7, �).Zq 3,3-5 13?71 4�% 600, C> 11. 3,35 Q. 0y__ 2_09 � 3 5:50, 0 10,33 3, 35 2_0 13 9 V101 STABMMA'HON 3 successive readings, 3 minutes apart: within +/- 10% DO and tuFbidity, +1-3%Conductivity, +I-O.IpHunit; +A10MVforOR_P from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 Time between discharge cycles during sample collection: I CP, 3 UP t!!� Comments: ",&Inple Sampling Technician Name: Signature: PATemplates\GW & Drilling FormsTb�Flow Sampling Form—Rev-l.xls 231 HAYWOOD STREET, ASHEVILLE. NC 26801 TEL.B2B.281.3350 FAC.B2B.261.3351 WWW.AL.'rAMQHTF-NVlnOMr4�r4VAg--C--M Low -Flow Sampling Data Sheet Project Name: J 5C, eJLqr-z?—r,7<T— Well 11D: E'N-10 Project Number: 2201 B I Screen I nterval: bgs Personnel: i--, VWe 0 U4 Depth to Water: toc A-M �La ifA6-7— Stickup: Date: '109 Depth of Pump Intake: toc Drawddwn Set: toc Arrive at Well: -15 1, Start Time: Sample Time: Finish Sample Time: Leave Well: Time DTW (feet) Temp (oC) Conductivity (AS) DO (mg/L) PH (S.U.) ORP (MV) Turbidity NTU �'s 0 60 -3611 2 1. STABILIZA110N 3 successive readings, 3 minutes apart: within +/- 10% DO and turbidity, +1-3%Conductivay, +I-0.1pHun1t; +1-10i-VforOR-P from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 Time between discharge cycles during sample collection: Comments: wYa \Iyulw .��mple Sampling Technician Name: Signature: P:\Ternplates\GW & Drilling Forms\Lo-,v Flow'-Srmpling Form—Rev-l.x19 Project Name: Project Number: 1161 Personnel: Date: W MET 'Now VA Eel L 231 HAYWOOD STREET, ASHEVILLE, NC 26801 TEL.828.281.3350 FAC.82B.281.3351 WWW.A9-rAr4Or4TMKV1 RON NMNTA&.COb1 Low -Flow Sampling Data Sheet Well ID: Rw —0 - Screen Interval: bgs Depth to Water: toe Stickup: epth of Pump Intake: toe Drawdown Set: toe Arrive at Well: Start Time: Sample Time: i2�50 Finish Sample Time: Leave Well: Time DTW Temp Conductivity DO pH ORP Turbidity (fept) (00 —=--Lmg/L) (S.U.) (mv) NTU st — STABILIZA110N 3 successive readings, 3 minutes apart: 'Within +/- 10% DO and turbidity, +43%Conduclivity; +A0.1pHanit; +I-10MVforORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996.- Time between discharge cycles during sample collection: Comments: —1ple name: Sampling Technician Name: P:\ Templates\GW & Drilling Forms\Low Flow Sampling Form —Rev- I.xls RAN I IT-1211 M111 a 231 HAYWOOD STREET, ASHEVILLE, NC 28801 TEL.e28.281.3350 FAC.B2B.28t.3351 WWW.ALTAMONTENVIROMMIENTAIL.COM Equip . ment Documentation & Instrument Calibration Data Sheet Calibration Documentation Name: Person Conducting Calibration: Number: Date of Calibration: Location: Td%V%A-CW Date of Field Measurpmk-nf-z- Equipment Documentation FnijinmPnt nr 111Equipment Type Serial Number Brand VV-11 I VC1 IIIrL Ivc, 111v 150-ft Water Level 26154 Solinist 150-ft Water Level 22754 Solinist 150-ft Water Level 150 Testwell 150-ft Drawdown M P30-1527 QED .10ther Micro Calibration I instrument Standards Exp Date I Serial # 200601045 YSI 914i Miltinnrnmai-ar Unfmr ars, survey equipment, etc.): Instrument Reading 10.0 NTU 1 1000 NTU ��itial., linitial:--t- L.dl: Ott,, I ua,: ? q:7 JCal: I ime: ITime: C&,:;i _,_ �Time: Instrument Serial Number 07DIO0979 Instrument Readings Calibration Expiration Date Dissolved oxygen Initial: Cal: mmHg: im Time:,gP,, NA QC* AM Time: Meas: Mid Day Time: LCheck: T- -PM Time— Check: NA —report p H 7 SU to 0.1 S.U. —Ir�ltial- Cal: Time: z 3, 7a PH 4 S.U. report to 0. 1 S. U. Initial: Cal: — Time: ago 7 PH 10 S.U. report to 0. initial: Cal: Time: 0%4 1 S. U. QC* PH 7 S.U. report 0.1 S.U. Meas: Time: Check: PM Time: Check: Spec.Cond. 447184/23 mS** Initial: Cal: Time: QC* 84 mS �V— Meas: Mid Day Time: -'dh—eck-.RM -rime— Check ORP 200 mV Initial: Ca ITime: I. Electronic equipment calibrated according to the manufacturer's operation manual. 2. Specific Conductivity should be calibrated according to values representative of historic range, 3. Order of Calibration is as follows : Specific Conductivity, PH 7, PH 4, PH 10, ORP, QC checks. 4. QC Acceptable Ranges: PH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If readings are out of these ranges, meter needs to be recalibrated. 5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours. 6. ** Indicates to choose a Specific Conductivity buffer of 447, 84, or 23 mS which is closest to historical readincis from the project locatic P:\Templates\GW-Dril ling Forms\Calibration Data Sheet YSI 556-Rev 1.xIs Page I of I n., k 1 01 M a 0 oil, Ill �E 4. E �G 231 HAYWOOD STREET, ASHEVILLrz, NC 28801 TEL.BP-8.281.3350 FAC.828.281.3351 WWW.AL.TAI-IONTENVIRONf4ENTAL.COM Low -Flow Samplinq Loci PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: citgn h3a to SAMPLING PERSONNEL: E.Yurkovich WEATHER- 'a--6e, zw' Well ID: . q (j, — - Screen Interval: bgs Depth b Stickup: C3,0 Depth of Pump Intake: qo —toc Drawdown Set: 5'a, toc COMMENTS: Wee !a" V-12W 4"i'l Q2?Ag%k' Arrive at Well: - Start Time: Sample Time: Finish Sample Time:_ Leave Well: 100- till jjq3 Time DTW (feet) Temp (oQ Specific Cond. (VS) DO (mg/L) pH (S.U.) f eoof t to 0. 1 S. U. ORP (mv) Turbidity (NTU) F. io cf— I Aqq W-1 ITO —123-4 577: n..Io x, --K3 4-o V 12 1 .. .%D. 6C 0 ')q� 6, � �an E010 H7 I i C1 -63� 6, q D83 '7 6,5 3- 614Q P95- 0600 6, 10 7S7 401 C'n S�qn .9�n Time between recharge during sample collection: P- C I ISampling Personnel Signature: Date: NOTES: STABILIZATION 3 successive readings, 3 minutes apart: within +/- 105vo DO and turbidity, -PI-3floConductivIty, +1-0.1joHun1t. -i-1-10ml/forORP from EPA - Low -Flow flVinimal Drawdown) Groundwater Sampling Procedures, April 199 6 bgs below ground surface toc top of casing 'C = degrees Celsius S.U. = standard units [LS = micro-Slemen per cubic centimeter ORP = oxidation reduction potential DO dissolved oxygen mv, = millivolt mg/L = milligrams per liter NTU = nephelometric turbidity units Samples are arnaly7-ed immediately upon collection. P:\Templates\GW & Drilling Forms\Low Flow Sampling Fdrm—Rev-2.xls . Page 3. of I E 7 N'"I# I W� E K. _R 1: N G Y, 231 HAYWOOD STREET. AsHEVILLE, NC 28801 TEL.828.2SI.3350 FAC.828.281.335-1 WWW.ALTAr4CNTENVlRDr4MEr4TAL.COM 1. . . Low -Flow Sampling Log PROJECT NAME- TEC-Fairview -PROJECT NUMBER: 2281.54 LOCATION: F81rview, NC SAMPLING PERSONNEL: E.Yurkovich WEATHER: almAj�, Well ID: 401 1 q10 Lj _t Screen Interval: — 571 bgs Depth to Water: toc Stickup: Depth of Pump Intake: L41"D _t0c brawdown Set: toc COMMENTS: Well gN4&W Arrive at Well: Start Time: fq3 Sample Time: loq� Finish Sample Time: 'iogj& Leave Well: 12 Time DTW (feet) Temp K) �pecific Cond. (PS) DO (mg/L) pH (S.U.) report to 0.1 S.U. ORP (MV) Turbidity (NTU) 6"5z. 3,92 11,64 e;oq aeo 6. 3Z .0.41 W-1.9-DL GCI2 r;.52 CA q,g 6.3 1. 94i? i-4-73 "YOM) 9 1+Q �5 17m; Ga- It '55,30 '264T Time between recharge during sample collection: IN &—as 4!a) U?q Sampling Personnel Signature: Date: NOTES: STABILIZATION successive Teadings, 3 minutes apart: +/ 0. 1 pH unit- -1-/- 10 m V for ORP within +/- 10 Yo DO and turbidity, - 3% Conductivity, +/ from EPA - Low -Flow (MinlmalDrawdown) Groundwater Sampling Procedures, April 1996 bgs below ground surface toc topof casing 'C = degrees Celsius S.U. = standard units 1.6 = micro-Slemen per cubic centimeter ORP = oxidation reduction potential DO = dissolved oxygen mv = millivolt mg/L = milligrams per liter NTU = nephelometric turbidity units Samples are analyzed immediately upon collecLion. P:\Templates\GW & Drilling Forms\Low Flow Sampling Form_Rev-2.xls Page I of I WRI E'k.R.IN,G _,H 231 HAYWOOD STREET, ASHEVILLE. NC 28801 TEL.828.281.3350 FAC.828.281.3351 WWW.AL-.Ar4ONTV,NVlROP4MENTAL.COM Low -Flow Sampling Log PROJECT NAME: TEC-Fairview PROJECT NUMBER ' 2281-54 LOCATION: Fairview, NC DATE, q1-1-2 to SAMPLING PERSONNEL- E.Yurkovich WEATHER:. tee, e "V') Well ID: HwAi uT Arrive at Well: Screen Interval: bgs Start Time: Depth to Water: toc Sample Time: Stickup: 060 Finish Sample Time: !qZ1 is - Depth of Pump Intake: toc Leave Well: 4,0W Drawdown Set: toc COMMENTS: dc;8n %) Time DTW (feet) Temp (IC) Specific Cond. (PS) DO (mg/L) pH (S.U.) repolt to 0.1 S.U.'— ORP (mv) Turbidity (NTU) R. 219 19/6 pq. a I 'q S � q, 11 OL -6,51 17 1 19 A. -35 11-'a5 -5�, aZ 3ko '9W4. 0 1 4-11 11-Ac? sol - - 4.a - 0 8�aq.- L4 C4 %90 cosq-c� i e between recharge during sample colle tion: C=� ze-c's, a Sampling Personnel Signature: Date: NOTES: STABILIZATION 3 successive readings' ' 3 minutes apart: within +/- 10% Do and turbidity; +1-3% Conductivity; +I-0.1pHunit; V-20ml/forORP from EPA - Low -Flow (idlinimalDrawdown) Groundwatersampling Procedures, April 1996 bgs below ground surface toc top of casing *C = degrees Celsius S.U. = standard units I.tS = micro-Siemen per cubic centimeter ORP = oxidation reduction potential DO = diss'olved oxygen mv = millivolt mg/L = milligrams per liter NTU = nephelometric turbidity units Samples are analyzed Ininiediately upon collection. P:\Templates\GW & Drilling Forms\Low Flow Sampling Form—Rev-2.xis Page I of 1 N E N � i:k E�1� Fi i,N q: _y' d'y'.. 1­11,1� 6h�'O,G'.E� 231 HAYWOOD STREET. AsHEVILLF. NC 28801 TEL.828.281.3350 FAC.828.281.3351 WWW.AL—.Af4CR7EF4VlROr4r4Ff4TAL.COM Low -Flow Sampling Log PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DAT E: SAMPLING PERSONNEL: E.Yurkovich WEATHER: CAftw, 5LAnw aaa Well ID: Rw- ca Screen Interval: to bgs Depth to Water: C_q --toc Stickup: Oro Depth of Pump Intake: g�p —toc Drawdown Set: toc COMMENTS: Wed MX&atneg& Arrive at Well: Start Time: Sample Time: Finish Sample Time: Leave Well: ej�"R sm�A-N" VaCT 11F4 I 143T Time DTW (feet) Temp (10 Specific Cond. (PS) DO (MCl/L) pH (S.U.) report to 0.15. U. ORP (mv) Turbidity (NTU) 4'&Qi oleo ib_ G-S 1 711cff co droo L s-19a _goo 5_07 at 92 Time between recharge during sample collection: — fla 49 ISampling Personnel Signature: V!77 Daie: NOTES: STABILIZATION 3 successive readings, 3 minutes apart: within -i-l- 10% DO and turb/dIt -3FIoConductivity; +1-0.1pHun1t,' +I-20mVtbrORP . y; +/ from EPA - Low -Flow (MinimalDrawdown) Groundwater Sampling Procedures, April 1996 bgs below ground surface toc top of casing *C =degrees Celsius S.U. =standard units ItS micro-Slemen per cubic centimeter ORP = oxidation reduction potential DO dissolved oxygen mv.,-- millivolt mg/L = milligrams per liter NTU = nephelometric turbidity units Samples are analyzed immediately upon collection. P:\Templates\GW & Drilling Forms\Low Flow Sampling Form_Rev-2.xls Page 1 of I -f:y N E E� R I N �G;, j 231 HAYWOOD STREET. ASHEVILLE. NC 2BB01 TFL.828.281.3350 FAC.BP-8.281.3351 WWW.AL.TAMCt4TENVARCUMEf4TAL.Cor4 Low -Flow Sam6lina Loa -PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 -LOCATION: Fairview, NC DATE: CTW 6OR-1- -SAMPLING PERSONNEL: E.YurkoVich WEATI Well ID:_ TQ%Vj_ 7 Arrive at Well: Screen Interval: SO 4,,a --bgs Start Time: Depth to Water: toc Sample Time: Stickup: Finish Sample Time: Depth of Pump Intake: _t0c Leave Well: Drawdown Set: —toc COMMENTS: Time DTW (feet) 7 emp K) Specific Cond. (11S) DO (mg/L) pH (S.U.) report to 0.1 S.U. ORP (mv) Turbidity (NTU) _[71 ta L L &.qa (03. .90 -I :76, 1%6. a Q ::ar --p A.eol mg 1A10 Time between recharge during sample collection: Sampling Personnel Signature: Date: NOTES: STABILIZATION 3 successive readings, 3 minutes apart: within +/- 10% DO and turbidity, -i-l- 3% Conductivit y- 0 1 pH un t; 10 m V fo� ORp from EPA - Low -Flow OyilnlmalDrawdown) Groundwatersampling Procedures, April :L996 bgs below ground surface toc top. of casing *C = degrees Celsius S.U. = standard units i.tS = micro-Slemen per cubic centimeter ORP = oxidation reduction potential -DO = dissolved oxygen mv ='millivolt mg/L = milligrams per liter NTU = nephelometric turbidity units Samples are analyzed immediately upon collection. P:\Templates\GW & Drilling Forms\Low Flow Sampling Form—Rev-2.xls Page 1 of I H 'Y ' G,9,& &�&Y 231 14AYWOOD STREET. ASHEVILLE, NC 28801 TEL.828.2el-3350 FAC.828.281.3351 WVdW.ALTA MONTENV I RON ME NTAL.GOM Low -Flow Sampling Log PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: JO &Igblo SAMPLING PERSONNEL: E.Yurkovich WEATHER: Well ID: HjAf_ Sq "7r. Screen Interval: bgs Depth to Water: 0 toc Stickup: CIO Depth of Pump Intake: L40 toc Drawdown Set: —toc COMMENTS: VICA WdAJ-V_ Arrive at Well: Start Time: Sample Time: Finish Sample Time: Leave Well: V�eA Time DTW (feet) Temp Specific Cond. (PS) DO ,,(mg/L) IOU pH (S.U.) report to 0. 1.5. U. ORP (mV) Turbidity (NTU) Ion 121(914 757 �51 1;iro I -Pm 7 5_1 16- 19137 9901 _q 6r4,. jgt, yo Gro __ _ _ e),11 alqq 5.7 - 0 �'93 & " q, 63 0,30 61qco 9 ac.) 5 711:57 Time between recharge during sample collection: Per sonnel Signature: Date: NOTES: STABILIZATION 3 successive readings, 3 minutes apart: within -1-/- 10% DO and turbldity,, +/- 3% Conductivity; -1-/- 0.1 pH un1t. +/- 10 mVfor ORP from EPA - Low -Flow (Minimal Drawdowr)) Groundwater Sampling Procedures, April 1996 bgs below ground surface toc top of casing *C = degrees Celsius S.U. standard units JLS = micro-Slemen per cubic centimeter ORP oxidation reduction potential .DO = dissolved oxygen mv millivolt mg/L = milligrams Per liter NTU nephelometric turbidity units Samples are analyzed immediately upon collection. ---- CI-1-1 C­ D,,,-') -1� . P;;np 1 nf I �E'JEI'R_ 1, N:-Gl 231 HAYWOOD STREET. ASHEVILLE. NC 2BB01 TEL.828.281.335() FAC.828.281.3351 WWW.ALTADIONTENVIROMMIENTAL.COM Low -Flow Sampling Log PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: 10 _(q G—hnio SAMPLING PERSONNEL: E.Yurkovich WEATHER: 61e-nAr. aO' Well ID: MW-140 Arrive at Well: qS9 Screen -interval: 31 -f4 5-1 bgs Start Time: �qq Depth to Water: 310�) . — toc Sample Time: /013 0 - Finish Sample Time: Stickup: a 1011: Depth of Pump Intake: toc Leave Well: Drawdown Set: toc COMMENTS: -(,rc kc.±Lrp %,&,ral 4urbq, w44, a ip�-A c&r V Time DTW (feet) Temp (1Q Specific Cond. (PS) DO (mg/L) pH (S.U.1 rep oft to 0. 1 S. U. ORP (mv) Turbidity (NTU) 7 13 � 3 9 1,2101 21 1709 61 e:71. — __ 7"Gia' _�&A cicu e914 4111 5, 10C4 -15, 6.914 1 C309 gqq Gla-560 17, 5@::� q. 16 Time between recharge during sample collection: Sampling Personnel Signature: Date: NOTES- S I TABILIZATION 3 successive readings, 3 minutes apart: within +/- 10% DO and turbidity; +1-3Y.Conduct(v1ty,, +1-0.1joHun1t,' +I-10ml/forORP from. EPA - Low -Flow (Minimal Drawdown) GroundwaterSampling Procedures, April 1996 bgs =.below ground surface toc top of casing *C degrees Celsius S.U. = standard units J.LS micro-Siemen per cubic centimeter ORP = oxidation reduction potential DO dissolved oxygen mv = millivolt mg/L = milligrams per liter NTU = nephelometric turbidity units Samples are analyzed immediately upon collection. P-1T=mnI=f-nc%r-,1A1 JZ, r1rillinn ;:nrmc%1 MAI Finifti rnmnlinrt F:nrm Rpv-?.Ylq Paoe I of.1 y" 231 HAYWOOD ISTREET, ASHEVILLE, NC 28801 TEL.828.261.3350 FAC.1328.281.3351 WWW.ALTAMONTElMVlRCf4MMNTAL.CCY4 Low -Flow Sampling Log PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: to /0' /'901.0 SAMPLING PERSONNEL: E.Yurkovich WEATHER: ofoc"11 cfeo'r 400 Well ID: Arrive at Well: Screen Interval: bgs Start Time: Depth to Water: 19� toc Sample Time: Stickup: Finish Sample Time: Depth of Pump Intake: —toc Leave Well: Drawdown Set: toc COMMENTS- iA ZV611 lnf'A�r �6& 4-or. ck naont Time DTW (feet) Temp VQ Specific Cond. (P§) DO (mb /Q pH (S.U.) report t6 0. 151 U. ORP (mv) Turbidity (NTU) 7, 47G '3,92 17'3+ 3� s.:jq zs' I b '?Q %51 ozz J9 _13AT- _T_ 711� 51 Iq v4p.5 9065 lu I r'_74 , ig; _X, U '3(09-3 10L - I so �17U 50& o Ar.; '�P(o - 13� 1 OL Raq -Zb4 --g-W04 a (P 630, (P Time between recharge during sample collection: 6? Sampling Personnel Signature - Date: rq/(3/k­' NOTES: STABILIZATION 3 successive readings, 3 minutes apart: within -,L/- 10% DO and turb/dIty; *1-3% Conductivity; +1-0.1pHun1t,' +I-10ml/forORP from EPA - Low -Flow (MInimal Drawdown) Groundwater Sampling Procedures, April 199 6 bgs below ground surface toc top of casing 'C = degrees Celsius S.U. = standard units I.LS = micro-Slemen per cubic centimeter ORP = oxidation reduction potential DO = dissolved oxygen mv = millivolt mg/L = milligrams per liter NTU = nephelometric turbidity 6nIts Samples are analyzed immediately upon collection. - ­.— . _. . .1 ­1 1 _... '___ ­­ n ,I- . V.n. I �f I 231 HAYWOOD STREET. ASHEVILLE. NC 28801 TEL.82EI.2BI.3330 FAC.828.281.3351, WWW-ALTAMONTENVIROMMENTAL.COM I Low -Flow Sampling Log PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: id/4/9010 SAMPLING PERSONNEL: E.Yurkovich WEATHER: aealf Well ID:_ Arrive at Well: Screen Interval: bgs StartT!me:— Depth to Water: Ze'W —toc Sample Time: Stickup: 0,4D Finish Sample Time: Depth of Pump Intake: toc Leave Well: Drawdown Set: toc COMMENTS: Time DTW (feet) Temp (1Q Specific Cond. (PS) DO (mg/L) pH (S.U.) report to 0.1 S.U. ORO (mv) Turbidity (NTU) COM 16,Sq -::T.(0'& Ing eVQ _152. X 610-q- qqj Ist cel- 11-2;6 eq &104 7,;r) (a co r,5q5- 'o."'?:�- 9,1r) 6' up 57,03 qi 70 IWO /0,& 11, __:P111 W89 Time between recharge during sample collection: q 6- C-.) Gan — Sampling Personnel Signature: Date: NOTES: STABILIZATION 3 successive readings, 3 minutes apart: wlthia+1-1016DO�ndturbldity; +1-3016 Conductivity- +I-0.1pHun1t; -k1-10mVtbr0RP from EPA - Low -Flow (MInimal Drawdown) Groundwater Sampling Procedures, April 1996 bgs below ground surface toc top of casing 'C = degrees Celsius S.U. = standard units I.LS = mIcr07Slemen per cubic centimeter ORP = oxidation reduction potential DO = dissolved oxygen mv = millivolt i-ng!L = milligrams per liter NTU = nephelametric turbidity units Samples are analyzed immediately upon collection. . -1 - . I' - - � ­ , ."- pnn. I nf I 231 HAYWOOD STREET. ASHEVILLE. NC 28801 TFL.8213.2el.SiSO 'FAC.828.281.3351 WWW.ALTAMONTIENVIRONMENTAL.COM Low -Flow Sampling Log PROJECT NAME: TEC-Fairview PROJECT NUM,PER: 2281.54 LOCATION: Fairview, NC DATE: iehblaxalo SAMPLING PERSONNEL: E.Yurkovich WEATHER: 0,taW GC)o Well ID: Arrive at Well: Screen Interval: tO jl�—G bgs Start Time. Depth to Water: 14-3Q toc Sample Time: Stickdp: 0,0 Finish Sample Time: Depth of Pump Intake: 40 toc Leave Well: Drawdown Set: (02 toc COMMENTS: I &XQ VS14 Time DTW (feet) Temp (IC) Specific Cond. (PS) DO (Mg/Q p H (S. U.) repolt to 0.1 S. U. ORP (mv) Turbidity (NTU) Psi. A'Srx 1!5 61 1 4?39 f;3; jp qq a0l, actT IOL54 4ena -7.& 460 31 1,50po 4, ua .1, sf I at) 14'?, (P'3 130�; —qLQQL 1-11577 0 61-'O'e ((OT T me between recharge during sample collectiom -I- NI z 11 Ca SwN; Sampling Personnel Signature: Date: /0/4/6 NOTES: STABILIZATION 3 successive readings, 3 minutes apart: w1th1n+1-10F*D0andturb1d1ty, -1�1-3% Conductivity; +1-0.1pHun1t' +1-10ml/forORP from EPA - Low -Flow (Minimal Drawdown) Groundwater5ampling Procedures, April 1996 bgs below ground surface toc top- of casing 'C = degrees Celsius S.U. = standard units I.tS = micro-Siemen per cubic centimeter ORP = oxidation reduction potential DO = dissolved oxygen mv = millivolt mg./L = milligrams per liter NTU = nephelometric turbidity units Samples are analyzed immediately upon collection. I—- ­—, , -... U­ D­ -) -1, Pace I of I WER a 1111.121IM31111111111111 N,31T1 I 231 HAYWOOD STREET. ASHEVILLt. NC 28801 TEL.828.281.3350 FAC.828.281.3351 WWW.ALTAK0KTZXV1R0NMCNTAL.00f4 Equipment Documentation &'Instrument Calibration Data Sheet Callbration Documentation Person Conductina Calibrati of Field Measurements: Equiument Documentation Equipment or meters used to take measurements (e q water level meters, survey equipment, etc.): Equipment Type Serial Number Brand Date of Use 150-ft Water Level 26154 Solinist 150-ft Water Level 22754 Solinist - Water L vel 150 Testwell 150-ft Drawdown MP30-1527 QED Other I Mirm TPW.Tiirhirfii-v Mpt-pr Calibration Standards Exp Date Instrument Serial # Instrument Reading 0.02 NTU 10.0* NTU 1060 NTU 200601045 Initial: Initial: 1,3.11 Initial: q34q Cal: Cal: 10,0 Cal: /0-ho Time: qq� Time: -74R Time: -;6-0 I _XS4=_qeRMiiIfln;;ramt-tPr Mptpr U04im, Instrument Serial Number 10TS0.5 Instrument Readings Calibration Expiration Date Dissolved Oxygen Initial: Cal: mmHg: Time: NA QC* AM Time: Me.as: Mid Day Time: Check: PM Time: Chock: NA PH 7 S.U. report to a.7 s. u. Initial: pHmV: Cal: —70 pHmV: Time:4.q4 p H 4 S. U. report to 0.1 S.U. Initial: pHmV: Cal: q to pHmV: Time: -, . � q-T PH 10 S.U. report to 0.1 5.U. Initial: pHmV: Cal: 10-0 pHmV: Time: QC* PH 7 S.U. repottlAM to Ol 5.U. Time: Meas: Mid Day Time: __V(-qz Check: PM Time: Check: Spec.Cond. 447/84/23 mS** Initial: Cal: I Time: I QC* 84 mS AM Time: Meas: Mid DayTime: Check: PM Time: Check: ORP 200 mV Initial: Cal: Time: njores: 1. Electronic equipment calibrated according to the manufacturer's operation manual. 2. Specific Conductivity should be calibrated according to values representative of historic range. 3. Order of Calibration is as follows : Specific Conductivity, PH 7, PH 4, PH 10, ORP, QC checks. 4. QC Acceptable Ranges: PH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If readings are out of these ranges, meter needs to be recalibrated. 5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours. 6. ** Indicates to choose a Specific Conductivity buffer of 447, 84, or 23 mS which is closest to historical readings from -the project locatic P:XTernp1ates\GW-Dri1I1ng Forms\Calibration Data Sheet YSI 556-Rev 2.xIs Page 1 of 1 231 HAYWOOD STREET. ASHEVILLE, NC 28801 TEL.828.281.3350 FAC.828.281.3351 WWW.ALTAM0NTEMVIR0MMMNTAL.00M . Low -Flow Sampling Log PROIECT NAME: TEC-Fairview PROIECT NUMBEk: 2281.54 LOCATION. Fairview, NC DATE, 1(11m Iaew SAMPLING PERSONNEL: E.Yurkovich ' Af WEATHER: '-SLAIVX-1 Cie Well ID: Nw- sci k rt Screen Interval: sD � 40 "5Z bgs Depth to Water: toc Stickup: Depth of Pump Intake: 40 toc Drawdown Set: toc COMMENTS: Arrive at Well: Start'Time: Sample Time: Finish Sample Time: Leave Well: ja,4q NA M4 Time DTW (feet) Temp (IC) Specific Cond. (PS) DO! (mg/L) pH (S.U.) report to 011 S.U. ORP (mV) Turbidity (NTU) q,qc, q-Ts 40 0':. 1- Ga� i 5 q,-7 D5:5 N. a 105,10 161.2 rf a 3 31 q, 3, 6,65' 1_+F� aool?' U05 kwAb 1-7.0co i3l _v�,jqq 5,51 jyj�iy- oqp.,--+ 54S 5153 1,57 f3 Time between recharge d6ring sample collection: s ampling Personnel Sig nature: U Date: NOTES: STABILIZATION 3 successive readings, 3 minutes apart: within +/- 10% DO and turbidity,, +/- 3% Conductivity,- +/- 0.1 joH unit, +/- 10. MI/for ORP from EPA - Low -Flow (MinimalDrawdown) GroundwaterSampling Procedures, April 1996 bgs below ground surface toc top of casing. 'C = degrees Celsius S.U. = standard units J.15 = micro-Slemen per cubic centimeter ORP = oxidation reduction potential DO m dissolved ox�gen mv = millivolt mg/L = mlillgrarns per liter NTU = nephelometric turbidity units Samples -are analyzed immediately upon collection. pnn� 1 n I MEN 0 KIM MEN 0 No ITA I melogy I OL91 Vi' I mm :E.'E:R I 231 HAYw6ot) STREET, ASHEVILLE. NC 28801 TEL.828.281.3350 FAC.B28.281.3351 WWW.ALTAMONTENVAROHMENTAL.COM Low -Flow Sampling Log PROJECT NAME: TEC-Falrview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: #0 1 191";t0lo SAMPLING PERSONNEL: E.Yurkovich WEATHER: Well ID: . UAW— 40 Screen Interval: 3L bgs Depth to Water: toc . Stickup: Depth of Pump Intake: toc Drawdown Set: toc COMMENTS: ljeU Arrive at Well: Start Time: SampleTime: Finish Sample Time: Leave Well: Q q:�E /Ogo JoAt Time DTW (feet) Temp (IC) Specific Cond. (ps) DO (mg/L) pH (S.U.) rep oft to 0.1 S.U. ORP (mv) Turbidity (NTU0 Icso 1 3, qf jq 07 ql 5.(.01 .90-45 4122 h=q �Sdi a. 1VT R-4 4-15, i -4-- 7 11J. sk&' '3' W OV CW-17 M G Time between recharge during sample collection: swAc'y ISampling Personnel Signature: Date: &/uq/un NOTES- STABILIZATION 3 successive readings, 3 minutes apart: w1th1n-+1- 10% Do and turbidity,, +1-3% Conductivity, V-0.1pHun1t; +1-10ml/forORP from EPA - Low -Flow (MlnimalDrawdown) GroundwaterSampling Proceduresi April 1996 bgs below ground surface toc top of casing 'C = degrees'Celsius S.U. = standard units ILLS = micro-Slemen per cubic centimeter ORP = oxidation reduction potential DO = dissolved oxygen mv millivolt mg/L = milligrams per liter NTU nephelometric turbidity.units Samples are analyzed immediately upon collection. . I—- - —.1 1 _... ­-1:­; r___ 0_"') -1, Paap I of I 'H 1. N 113:� �.D R P';G:E, 231 HAYWOOD STREET, ASHEVILLE, NC 28801 TEL.e2a.261.33SO FAC.E128.2131.3351- WWW.ALTAMONTF-MV [RON M ENTAL.COM Low -Flow Samriiiina Loa PROJECT NA�E: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: SAMPLING PERSONNEL: E.Yurkovich WEATHER: Well ID: Mw- qj W T Screen Interval: Ll Depth to Water: --siqa Stickup: Depth of Pump Intake: Drawdown Set: -toc COMMENTS: Arrive at Wefl: bgs StartTime: toc Sample Time: Finish Sample Time: toc Leave Well: Time DTW (feet) Temp VQ Specific Cond. (gs) DO (mg/L) pH (S.U.) report to 011 S.U. ORP (mv) Turbidity (NTU) i62 R5. ".7 G? 51 -6 1 57 5�71 5� R9 -1 . 4717,�5_ a, 156 4. 7:7 1!1' As- p3o me between recharge during sample collection: = Sampling Personnel Signature: 9 Date: �0011qia NOTES: STABILIZATION B successive readings, 3 minutes apart: within -/-/- 10165 DO and turbidity,- +/- 3yo Conductivity;. +/- 0,1 joH unit; +/- 10 ml/for ORP from EPA - Low -Flow MnlmalDrawdown) Groundwater SamplIng Procedures, April 1996 bgs below ground surFace toc top of casing 'C = degrees Celsius S.U. = standard units ItS = micro-Siemen per cubic centimeter ORP = oxidation reduction potential DO = dissolved oxygen mv millivolt rng/L = milligrams per liter NTU nephelometric turbidity units Samples are analyzed immediately upon collection. r:­,%I �... r:I_j r_11,_ r:_ 231 HAYWOor) S ' TREET. ASHEVILLE. NC 28BOl T EL.828.261.3350 FAC.828.281.3351 WWW.ALTAr4ONTENVj RON M ENTAL.CO M Low -Flow Samplinq Loq PROJECT NAME: TEC-Fairview' PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: SAMPLING PERSONNEL: E.Yurkovich WEATHER: ' (:�Jea-rStm Uj, Well ID:— Screen Interval: RG bgs Depth to Water: --toc Stickup: Depth of Pump Intake: czr% toc Drawdown Set: toc COMMENTS: Arrive at Well: Start Time: Sample Time: Finish Sample Time: Leave Well: —j 3 _ Ic j P I Time DTW (feet) Temp (IC) Specific Cond. Ws) DO (mg/L) pH (S.U.) report to 0.1 S'U. ORP (mv) Turbidity (NTU) 1153713 119 -1:S 5 C91 (�2 erj 61 6,63 . , - - cat. 2 gig. - Time between recharge during sample collection:—. WA Sampling Personnel Signature: Date: NOTES: STABILIZATION 3 successive readings, 3 minutes apart: w1thIn 4-1- 105vo DO and turbldlty,- +/- 3961 Conductivity, +/- 0.1 PH unit; +/- 10 ml/for ORP from EPA - Low -Flow (Min1malDrawdown) Groundwater Sampling Procedures, April 1996 bgs below ground surface toc top of casing 'C = degrees Celsius S.U. = standard units ILS = micro-Slemen per cub ic cen . timeter ORP = oxidatiofi reduction potential DO = dissolved oxygen mv millivolt mg/L.= milligrams per liter NTU nephelometric turbidity units Samples are analyzed Immediately upon collection. P:\Templates\GVI & Drilling Forms\Low Flow S . ampling Form Rev-2.xis Paoe I of 1 7��'_,-E:N Gil"N tf'k, i'-; N 231 HAYWOOD STREET. ASH - EVILLE. NC 26801 TEL.82 8 .2al.3350 FAC-828.281.3351 W%VW-ALTAMONTENWI RON M ENTAL.COM LOW -Flow Samnlinn I nq PROJECT NAME: TEC-Fairview PROJECT NUMBER: 2281.54 LOCATION: Fairview, NC DATE: j0jll?fa§yo�� . SAMPLING PERSONNEL: E.Yurkovich WEATHER:' &Zb Well ID: 21" Arrive at Well: .Screen Interval: bgs Start Time: Depth to Water: toc Sample Time: Stickup: Finish Sample Time: De . pth of Pump Intake:_ toc Leave Well: Drawdown Set: to C CO'114MENTS- kL4�- Time q lei 51 DTW (feet) 55 Terfip 11c) C01+9 Spechic Cond. (PS) DO (mg/L) '71(d5 pH (S.U.) report to 0. 1.5. U, 4 15LI ORP (mv) Turbid ity (NTU) L4.7. Cr 3q[3- G sq Time between recharge during. sample colle( Sampling Personnel Signature: Date: Nu I t:�): STABILIZATION 3 successive readings, 3 minutes apart: within -h/- 10% DO and turblolly,- -I-/- 3yo Conductivity,, -h/- 0.1 joH unit;. */- 10 mVfor ORP from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 bgs below ground surface toc top of casing 'C = degrees Celsius S.U. = standard units j.E5 = micro-Siemen per cubic centimeter ORP = oxidation reduction potential DO = dissolve ' d oxygen mv millivolt mg/L = milligrams per liter NTU nephelometric turbidity units Samples are analyzed immediately upon collection. P:\Templates%GW & Drilling Forms\Low Flow Sampling Form—Rev-2.xis Page 1 of I APPENDIX IF Laboratory Analytical Reports Pace Analytical Services, Inc. Pace Analytical Services, Inc. a Analj(tical" 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 lcewmpaicefabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 August 18, 2010 Mr. Chris Gilbert Altamont Environmental 231. Haywood Street Asheville, NC 28801 RE: Project: TEC PILOT TEST 08/11 . Pace Project No.: 9275343 Dear Mr. Gilbert: Enclosed are the analytical results for sample(s) received by the laboratory on August 11, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and -Organic- testing was -performed -at-our-Pace-Huntersville labor.atory.-unless-o-therw-is-e-foQtnoted-.- All - Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri. Patton lorri.patton@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS Page I of 26 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. I a ceAnal . jdical ww.paceelmcom Cl Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification *: 9900'6001 Louisiana/LELAP Certification *: 04034 South Carolina Drinking Water Cert. *: 99006003 New Jersey Certification#: NC01 2 Virginia Certification *: 00213 North Carolina Drinking Water Certification 37706 Connecticut Certification #: PH-01 04 North Carolina Field Services Certification 5342 FloridaINELAP Certification E87627 North Carolina Wastewater Certification #: 12 Kentucky UST Certification 84 Pennsylvania Certification M 68-00784 Louisiana DHH Drinking Water# LA 100031 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Connecticut Certification#: PH-01 06 Florida/NELAP Certification E87648 Massachusetts Certification M-NC030 New Jersey Certification *: NC01 I North Carolina Bioassay Certification * 9 North Carolina Drinking Water Certification *: 37712 North Carolina Wastewater Certification #: 40 Pennsylvania Ceffification M 68-03578 South Carolina Bioassay Certification *: 99030002 South Carolina Certification * 99030001 Virginia Certification *: 00072 REPORT OF LABORATORY ANALYSIS Page 2 of 26 This report shall not be reproduced, except in full, without the written. consent of Pace Analytical Services, Inc.. Paxj�ql Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 LabID: 9275343001 Collected: 08/11/10 12:55 Received: 08/11/10 14:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 6010 MET ICP Analytical Method: EPA 6010 Pre paration Method: EPA 3010 Arsenic 24.7 ug/L 5.0 1 08/13/10 11:50 08/16/10 17:17 7440-38-2 Cadmium ND ug/L 1.0 1 08/13/10 11:50 08116/10 17:17 7440-43-9 Chromium ND ug/L 5.0 1 08/13/10 11:50 08/16110 17:17 7440-47-3 Copper ND ug/L 5.0 1 08/13110 11:50 08/16/10 17:17 7440-50-8 Lead 61.4 ug/L 5.0. 1 08/i3/10 11:50 08/16/10 17:17 7439-92-1 Zinc 37.8 ug/L 10.0 1 08/13/10 11:50 08116/10 17:17 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 08/12/10 18:bo 08/14/10 12:17 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L Benzene ND ug/L Bromobenzene ND ug/L Bromochloromethane ND ug/L Bromodichloromethane ND ug/L '3romoform ND ug/L 3romomethane ND ug/L 2-Butanone (MEK) ND ug/L Carbon tetrachloride ND ug/L Chlorobenzene ND ug/L -Chlorroethane- -ND -GO/L Chloroform ND ug/L Chloromethane NID ug/L 2-Chlorotoluene ND ug/L 4-Chlorotoluene NID ug/L 1,2-Dibromo-3-chloropropane. ND ug/L Dibromochloromethane ND ug/L 1,2-Dibromoethane (EDB) ND ug/L Dibromomethane ND ug/L 1,2-Dichlorobenzene ND ug/L 1,3-Dichlorobenzene ND ug/L 1,4-Dichlorobenzene ND ug/L Dichlorodifluoromethane 22.5 ug/L 1,1-Dichloroethane 2.2 ug/L 1,2-Dichloroethane ND ug/L 1,1-Dichloroethene 2.6 ug/L cis-1,2-Dichloroethene 10.9 ug[L trans-1,2-Dichloroethene ND ug/L 1,2-Dichloropropane ND ug/L 1,3-Dichloropropane ND ug/L 2,2-Dichloropropane ND ug/L 1,1-Dichloropropene NID ug/L Cis-1,3-Dichloropropene ND ug/L trans-1,3-Dichloropropene ND ug/L Diisopropyl ether ND ug/L .0ate: 08/18/2010 12:42 PM 25.0 1 08/14/10 06:01 67-64-1 1.0 1 08/14/10 06:01 71-43-2 1.0 1 08114/10 06:01 108-86-1 1.0 1 08114/10 06:01 74-97-5 1.0 1 08114/10 06:01 75-27-4 1.0 1 08114/10 06:01 75-25-2 2.0 1 08/14/10 06:01 74-83-9 5.0 1 08/14/10 06:01 78-93-3 1.0 1 08/14/10 06:01 56-23-5 1.0 1 08/14/10 06:01 108-90-7 -1-.0-- 1 08/14/10-06-01 75-00-3- 1.0 1 08/14/10 06:01 67-66-3 1.0 1 06/14/10 06:01 74-87-3 1.0 1 08114/10 06:01 95-49-8 1.0 1 08/14/10 06:01 106-43-4 5.0 1 08/14/10 06:01 96-12-8 1.0 1 08/14/10 06:01 124-48-1 1.0 1 08/14/10 06:01 106-93-4 1.0 1 08/14/10 06:01 74-95-3 1.0 1 08/14/10 06:01 95-50-1 1.0 1 08/14/10 06:01 541-73-1 1.0 1 08/14/10 06:01 106-46-7 1.0 1 08/14/10 06:01 75-71-8 1.0 1 08/14/10 06:01 75-34-3 1.0 1 08/14110 06:01 107-06-2 1.0 1 08/14110 06:01 75-35-4 1.0 1 �08/14/10 06:01 156-59-2 1.0 1 08/14/10 06:01 156-60-5 1.0 1 08/14/10 06:01 78-87-5 1.0 1 08/14/10 06:01 142-28-9 1.0 1 08/14/10 06:01 594-20-7 .1.0 1 .08/14/10 06:01 563-58-6 1.0 1 08/14/10 06:01 10061-01-5 1.0 1 08/14/10 06:01 10061-02-6 1.0 1 08/14/10 06:01 108-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Page 3of26 I a ceAnalytical wwwpac�lab&wn Project: TEC PILOT TEST 08111 Pace.Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pade Analytical Services, Inc. 9800KinceyAve. Sufte100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 LablD: 9275343001 Collected: 08111/1012:55 Received: 08/11/1014:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 'Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene NO ug[L Hexachloro-1,3-butadiene ND ug/L 2-Hexanone ND ug/L p-Isopropyltoluene ND ug/L Methylene Chloride ND ug/L 4-Methyl-2-pentanone, (MIBK) ND ug/L Methyl-tert-butyl ether ND ug/L Naphthalene ND ug/L Styrene ND ug/L 1,1,1,2-Tetrachloroethane ND ug/L 1,1,2,2-Tetrachloroethane ND ug/L Tetrachloroethene 44.7 ug/L Toluene ND ug/L 1,2,3-frichlorobenzene ND ug/L 1,2,4-T(ichlorobenzene ND ug/L 1,1,17Trichloroethane 6.3 ug/L 1,1,2-Trichloroethan.e ND ug/L Trichloroethene �466 ug/L Trichlorofluoromethane ND ug/L 1,2,a-Trichloropropane ND ug/L Vinyl acetate ND ug/L -Vinyl chloride -- --- -- ND-ug/L- - - - m&p-Xylene 3.0 ug/L p-Xylene ND ug/L 4-Bromofluorobenzene (S) 97 % Dibromofluoromet hane(S) ill % 1,2-Dichloroethane-d4 (S) 107 % Tbluene-d8 (S) 97 % 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 45.2 mg/L 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA353.2 Nitrogen, Nitrate ND mg/L 4600 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L ASTM D616-90 Sulfate Water Analytical Method: ASTM D516-90 Sulfate 17.8 mg/L , Date: 08/1812010 12:42 PM 1.0 1 08/14/10 06:01 100-41-4 1.0 1 08/14/10 06:01 87-68-3 5.0 1 08/14/10 06:01 591-78-6 1.0 1 08114/10 06:01 99-87-6 2.0 1 .08114110 06:01 75-09-2 5.0 1 08114110 06:01 108-10-1 1.0 1 08/14/10 06:01 1634-04-4 1.0 1 08/14/10 06:01 91-204 1.0 1 08/14/10 06:01 10042-5 1.0 1 08/14/10 06:01 630-20-6 1.0 1 08/14110 06:01 79-34-5 1.0 1 08/14/10 06:01 127-18-4 1.0 1 08/14110 06:01 108-88-3 1.0 1 08/14/10 06:01 87-61-6 1.0 1 08/14110 00:01 120-82-1 1.0 1 08/14/10 06:01 71-55-6 1.0 1 08/14/10 06:01 79-00-5 20.0 20 08/16/10 16:51 79-01-6 1.0 1 08/14/10 06:01 75-69-4 1.0 1 08/14/10 06:01 96-18-4 2.0 1 08/14/10 06:01 108-05-4 -1.0 -1- 08/14/10 06:01 -75=014-- - 2.0 1 08/14/10 06:01 179601m-23-1 1.0 1 08/14/10 06:01 95-47-6 70-130 1 08/14/10 06:01 460-�00-4 70-130 1 08/14/10 06:01 1868-53-7 70-130 1 08114/10 06:01 17060-07-0 70-130 1 08/14/10 06:01 2037-26-5 5.0 1 08/16/10 15:02 0.10 1 08111/10 23:32 5.0 1 08116/10 09:55 16887-00-6 5.0 1 08/17/10 15:46 14808-79-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 26 1�5a'ceAnalXicalo ww-pawabs.- Project: TEC PILOT TEST 08/11 Pace Project No.: , 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Lab ID: 9275343002 Collected: 08111/10 12:50 Received: 08/11/10 14:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Arsenic Cadmium Chromium Copper Lead Zinc 7470 Mercury Mercury 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene ChCuraetharie Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chlorooropane, Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane M-Dichloroethane 1,2-Dichloroethane M-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether �-- -,, Date: 08/18/2010 12:42 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010 N ' D ug/L 5.0 1 08/13/10 11:50 08/16110 17:20 7440-38-2 ND ug/L 1.0 1 08/13/10 11:50 08/16/10 17:20 7440-43-9 ND ug[L 5.0 1 08/13/10 11:50 08/16/10 17:20 7440-47-3 ND ug/L 6.0 1 08/13/10 11:50 08116/10 17:20 7440-50-8 ND ug/L 5.0 1 08/13110 11:50 08/16/10 17:20 7439-92-1 ND ug/L 10.0 1 08113/10 11:50 08/16/10 17:20 7440-66-6 Analytical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 1 08112/10 18:00 08/14/10 12:17 7439-97-6 Analytical Method: EPA 8260 ND ug/L 25.0 1 08114/10 06:26 67-64-1 ND ug/L 1.0 1 08/14/10 06:26 71-43-2 ND ug/L 1.0 1 08/14/10 06:26 108-86-1 ND ug/L 1.0 1 08/14110 06:26 74-97-5 ND ug/L 1.0 1 08114/10 06:26 75-27-4 ND ug/L 1.0 1 08/14/10 06:26 75-25-2 ND ug/L 2.0 1 08/14/10 06:26 74-83-9 ND ug/L 5.0 1 08114/10 06:26 78-93-3 6.1 ug/L 1.0 1 08/14/10 06:26 56-23-5 ND-ug/L 1.0 1 08/14/10 06:26 108-90-7 N D ug/L 1.0 1 -ag/14/1-0 06-26 -75-00-3 3.3 ug/L 1.0 1 08/14/10 06:26 67-66-3 ND ug/L 1.0 1 08114/10 06:26 74-87-3 ND ug/L 1.0 1 08/14/10 66:26 95-49-8 ND ug/L 1.0 1 08/14110 06:26 106-43-4 ND ug/L 5.0 1 08/14/10 06:26 96-12-8 ND ug/L 1.0 1 08/14/10 06:26 124-48-1 ND ug/L 1.0 1 08/14/10 06:26 106-93-4 ND ug/L 1.0 1 08/14/10 06:26 �4-95-3 ND ug/L 1.0 1 08/14/10 06:26 95-50-1 ND ug/L 1.0 1 08/14/10 06:26 541-73-1 ND ug/L 1.0 1 08/14/10 06:26 106-46-7 ND ug/L 1.0 1 08/14/10 06:26 75-71-8 ND ug/L 1.0 1 08/14/10 06:26 75-34-3 ND ug/L 1.0 1 08114/10 06:26 107-06-2 34.4 ug/L 1.0 1 08114/10 06:26 75-35-4 ND ug/L 1.0 1 08/14/10 06:26 156-59-2 ND ug/L 1.0 1 08/14/10 06:26 156-60-5 10.9 ug/L 1.0 1 08114/10 06:26 78-87-5 ND ug/L 1.0 1 08/14/10 06:26 142-28-9 ND ug/L 1.0 1 08/14/10 06:26 594-20-7 ND ug/L 1.0 1 08/14 ' 110 06:26 563-58-6 ND ug/L 1.0 1 08/14/10 06:26 10061-01-5 ND ug/L 1.0 1. 08/14/10 06:26 10061-02-6 ND ug/L 1.0 1 08/14/10 06:26 108-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACIO, Page 5 of 26 Pace Analytical Services, Inc. 2225 Riverside Dr. ceAnalytical :wwwpac . elabs.com Asheville, NC 28804 ac, (828)254-7176 ANALYTICAL RESULTS Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-7 Parameters LablID: 9275343002 Collected: 08/11/1012:50 Results Units Report Limit DF Received: 08/11/1014:40 Matrix:Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene 18.7 ug/L 1.0 1 08/14/10 06:26 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/14/10 06:26 87-68-3 2-Hexanone ND ug/L 5.0 1 08/14/10 06:26 691-78-6 p-Isopropyltoluene ND ug/L- 1.0 1 08/14/10 06:26 99-87-6 Methylene Chloride ND ug/L 2.0 1 08/14110 06:26 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L .5.0 1 08/14/10 06:26 108-10-1 Methyl-tert-butyl ether ND ug[L 1.0 1 08/14110 06:26 1634-04-4 Naphthalene ND ug/L 1.0 1 08/14110 06:26 91-20-3 Styrene ND ug/L 1.0 1 08/14/10 06:26 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/14/10 06:26 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08/14/10 06:26 79-34-5 Tetrachloroethene 139 ug/L 1.0 1 08114/10 06:26 127-18-4 Toluene 145 ug/L 1.0 1 08/14110 06:26 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/14/10 06:26 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/14/10 06:26 120-82-1 1, 1,1 -Tdchloroethane 690 ug/L 200 200 08/16/10 15:29 71-55-6 1,1,2-Tr'ichloroethane ND ug/L 1.0 1 08/14/10 06:26 79-00-5 Trichloroethene 6470 ug[L 200 200 08/16/10 15:29 79-01-6 Tnchlorofluoromethane ND ug/L 1.0 1 08/14/10 06:26 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 08/14/10 06:26 96-18-4 Vinyl acetate ND ug/L 2.0 1 08/14110 06:26 108-05-4 Vinyl chloride ND-ug/L - --1.0- .1 08114/-10-06:26- 75-01-4 - m&p�Xylene 63.2 ug/L 2.0 1. 08/14/10 06:26 179601-23-1 o-Xylene 25.3 ug/L 1.0 1 08/14/10 06:26 95-47-6 4-Bromofluorobenzene (S) 99 % 70-130 1 08/14/10 06:26 460-00-4 Dibromofluoromethane (S) 94 % 70-130 1 08/14/10 06:26 1868-53-7 U-Dichloroethane-& (S) 98 % 70-130 1 08/14110 06:26 17060-07-0 Tbluene-d8 (S) 100 % 70-130 1 08/14/10 06:26 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 14.7 mg/L 5.0 1 08/16/10 15:02 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA353.2 Nitrogen, Nitrate 2.7 mg/L 0.10 1 08/11/10 23:31 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 1 08/16/10 09:55 16887-00-6 ASTM D516-90 Sulfate Water Analytical Method ASTM D516-90 Sulfate ND mg/L 5.0 1 08/17/10 15:46 14808-79-8 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 26 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 KinceyAve. Suite 100 6ceAnalyficals Asheville, NC 28804 Huntersville, NC 28 . 078 www.pacdab&com (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Sample: MW-39VVT Parameters Lab ID: 9276343003 Results Units Collected: 08/11/1012:20 Report Limit DF Received: 08/1111014:40 Matrix:Water Prepared Analyzed CAS No. Qual. 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3010 Arsenic ND ug/L 5.0 1 08/13/10 11:50 08/16/10 17:24 7440-38-2 Cadmium 6.2 ug/L 1.0 1. 08/13/10 11:50 08/16/10 17:24 7440-43-9 Chromium 421 ug/L 5.0 1 08/13110 11:50 08/16/10 17:24 7440-47-3 Copper 228 ug/L 5.0 1 08/13/10 11:50 08/16/10 17:24 7440-50-8 Lead 382 ug/L 5.0 1 08/13/10 11:50 08/16/10 17:24 7439-92-1 Zinc 498 ug/L 10.0 1 08113110 11:50 08/16/10 17:24 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 08112/10 18:00 08/14110 12:17 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25000 1000 08116/10 15:65 67-64-1 Benzene ND ug/L 1000 1000 08/16/10 15:55 71-43-2 Bromobenzene ND ug/L 1000 1000 08/16/10 15:55 108-86-1 Bromochloromethane ND ug/L 1000 1000 08/16/10 15:65 74-97-5 Bromodichloromethane ND ug/L 1000 1000 08/16/10 15:55 75-27-4 Bromoform ND ug/L 1000 1000 08/16/10 15:55 75-25-2 Bromomethane ND ug/L 2000 1000 08/16110 15:55 74-83-9 2-Butanone (MEK) ND ug/L 5000 1000 08116/10 15:55 78-93-3 Carbon tetrachloride ND ugtL 1000 1000 08/16110 15:55 56-23-5 Chlorobenzene ND ug/L 1000 1000 08/16/10 15:55 108-90-7 Cfilo�oethia7ne ND -1000- -1000- -08/16/10 15:55 -75-�00-3 Chloroform ND ugtL 1000 1000 08/16/10 15:55 67-66-3 Chloromethane ND ug/L 1000 1000 08116110 15:55 74-87-3 2-Chlorotoluene ND ug/L 1000 100b 08/16/10 15:55 95-49-8 4-Chlorotoluene ND ug/L 1000 1000 08/16/10 15:55 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5000 1000 08/16/10 15:55 96-12-8 Dibromochloromethane ND ug/L 1000 1000 08/16/10 15:55 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1000 1000 08/16/10 15:55 106-93-4 Dibromomethane ND ug/L 1000 1000 08/16/10 15:55 74-95-3 1,2-Dichlorobenzene ND ug/L 1000 1000 08116110 15:55 95-50-1 1,3-Dichlorobenzene ND ug/L 1000 1000 08/16/10 15:55 541-73-1 1,4-Dichlorobenzene ND ug/L 1000 1000 08/16/10 15:55 106-46-7 Dichlorodifluoromethane ND ug/L 1000 1000 08116/10 15:55 75-71-8 I,I-Dichloroethane ND ug/L 1000 1000 08/16/10 15:55 .76-34--3 1,2-Dichloroethane ND ug/L 1000 1000 08/16/10 15:55 107-06-2 M-Dichloroethene ND ug/L 1000 1000 08/16110 15:55 75-35-4 cis-1,2-Dichloroethene ND ug/L 1000 1000 08/16/10 15:65 156-59-2 trans-1,2-Dichloroethene ND ug/L 1000 1000 08/16/10 15:55 156-60-5 1,2-Dichloropropane ND ug/L 1000 1000 08/16/10 15:55 78-87-5 1,3-Dichloropropane ND ug/L 1000 1000 08/16/10 15:55 142-28-9 2,2-Dichloropropane ND ug/L 1000 1000 08/16/10 15:55 594-20-7 1,1-Dichloropropene ND ug/L 1000 1000 08116/10 15:55 563-58-6 cis-1,3- ' Dichloropropene ND ug/L 1000 1000 08/16/10 15:55 10061-01-5 trans-1,3-Dichloropropene ND ug/L 100.0 1000 08/16/10 15:55 10061-02-6 Dlisopropyl ether ND ug/L 1000 1000 08/16/10 15:55 108-20-3 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS Page 7 of 26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ceAnaljftal www.pacwabs.com Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-39WT Lab ID: 9275343003 Collected: 08111/10 12:20 Received: 08/11/10 14:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichlorobthane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Tr'ichloropropane Vinyl -acetate Wnyl chl-pride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethan6 (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 353.2 Nitrogen, N021NO3 unpres Nitrogen, Nitrate 4500 Chloride Chloride ASTM D616-90 Sulfate Water Sulfate Analytical Method: EPA 8260 NO ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L NO ug/L 1720 ug/L 2680 ug/L ND ug/L ND ug/L 11200 ug/L ND ug/L 156000 ug/L ND ug/L ND ug/L ND ug/L -ND -ug/L ND ug/L ND ug/L 93 % 110 % 105 % 95 % Analytical, Method: SM 2320B 17.9 mg/L Analytical Method: EPA 353.2 0.46 mglL Analytical Method: SM 4500-CI-E N D mg/L Analytical Method: ASTM D516-90 ND mg/L 1000 1000 1000 1000 5000 1000 1000 1000 2000 1000 5000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000' 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 2000 1000 1000 -1000- 2000 1000 1.000 1000 70-130 1000 70-130 1000 70-130 1000 70-130 1000 5.0 1 0.10 1 5.0 1 5.0 1 08/16110 15:56 100-41-4 08/16110 15:55 87-68-3 08/16/10 15:56 .591-78-6 08/16/10 16:56 99-87-6 08/16/10 15:56 75-09-2 08/16/10 16:55 108-10-1 08/16/10 15:55 1634-04-4 08/16/10 15:55 91-20-3 08/16/10 16:55 100-42-5 08/16110 15:55 630-20-6 08/16110 15:55 79-34-6 08/16/1015:55 127-18-4 08116/10 15:55 108-88-3 08/16/10 15:55 87-61-6 08/16/10 15:55 120-82-1 08/16/10 15:55 71-55-6 08/16/10 15:55 79-00-5 08/16/10,15:55 79701-6 08/16/10 15:55 75-69-4 08/16/10 15:55 96-18-4 08/16/10 15:55 108-05-4 OW16/10-15:55 75-01-4 08/16/10 15:65 179601-23-1 08/16110 15:55 95-47-6 08/16/10 15;55 460-00-4 08/16/10 15:55 1868-53-7 08/16/10 15:55 17060-07-0 08/16110 15:55 2037-26-5 08/16/10 15:03 08111/10 23:30 08/16/10 09:55 16887-00-6 08117/10 15:46 14808-79-8 Date: 08/1812010 12:42 PM REPORT OF LABORATORY ANALYSIS Page 8 of 26 This report shall not be reproduced, except in full, without the written consentof PaceAnalyflcal Services, Inc.. PaceAnalj4kal" wwwpacelabscom Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-40WT LabID: 9275343004 Collected: 08/11/10 11:24 Received: 08/11/10 14:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP - Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic NID ug/L 5.0 1 08/13/10 11:50 08/16/10 17:28 7440-38-2 Cadmium NID ug/L 1.0 1 08/13/10 11:50 08/16/10 17:28 7440-43-9 Chromium 69.4 ug/L 5.0 1 08113/10 11:50 08/16/110 17:28 1440-47-3 Copper 25.5 ug/L 5.0 1 08/13/10 11:50 08/16/10 17:28 7440-50-8 Lead ND ug/L 5.0 1 .08/13110 11:50 08/16/10 17:28 7439-92-1 Zinc 41.0 ug/L 10.0 1 08/13/10 11:50 08/16/10 17:28 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA7470 Mercury ND ug/L 0.20 1 08/12/10 18:00 08/14/10 12:17 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NID ug/L 50.0 2 68/16/10 16:23 67-64-1 Benzene ND ug/L 2.0 2 08/16/10 16:23 71-43-2 Bromobenzene ND ug/L 2.0 2 08/16/10 16:23 108-86-1 Bromochloromethane ND ug/L 2.0 2 08/16/10 16:23 74-97-5 Bromodichloromethane NID ug/L 2.0 2 08/16110 16:23 76-27-4 Bromoform NID ug/L 2.0 2 08/16/10 16:23 75-25-2 �Bromomethane ND ug/L 4.0 2 08/16/10 16:23 74-83-9 2-Butanone (MEK) ND ug/L 10.0 2 08/16/10 16:23 78-93-3 Carbon tetrachloride NID ug/L 2.0 2 08/16/10 16:23 56-23-5 Chlorobenzene ND ug/L 2.0 2 08116/10 16:23 108-90-7 Chloroe hane ND ug/L 2.0 2 08/1-6/1016-23 16-00-3 Chloroform .5.9 ug/L 2.0 2 08/16110 16:23 67-66-3 Chloromethane ND ug/L 2.0 2 08/16/10 16:23 74-87-3 2-Chlorotoluene NID ug/L 2.0 2 08/16110 16:23 95-49-8 4-Chlorotoluene ND ug/L 2.0 2 08/16/10 16:23 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 10.0 2 08/16/10 16:23 96-12-8 Dibromochloromethane NID ug/L 2.0 2 08/16/10 16:23 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 2.0 2 08/16/10 16:23 106-93-4 Dibromomethane ND ug/L 2.0 2 08/16/10 16:23 74-95-3 1,2-Dichlorobenzene ND ug/L 2.0 2 08/16/10 16:23 95-50-1 1,3-Dichlorobenzene NID ug/L 2.0 2 08/16110 16:23 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 2 08116/10 16:23 106-46-7 Dichlorodifluoromethane ND ug/L 2.0 2 08116MO 16:23 75-71-8 1,1-Dichloroethane ND ug/L 2.0 2 08/16/10 16:23 75-34-3 1,2-Dichloroethane NID ug/L 2.0 2 08/16/10 16:23 107-06-2 1,1-Dichibroethene ND ug/L 2.0 2 08/16/10 16:23 75-35-4 cis-1,2-Dichloroethene ND ug/L 2.0 2 08116/10 16:23 156-59-2 trans-1,2-Dichloroethene ND ug/L 2.0 2 08/16110 16:23 156-60-5 1,2-Dichloropropane ND ug/L 2.0 2 08/16/1016:23 78-87-5 1,3-Dichloropropane ND ug/L 2.0 2 08/16/10 16:23 142-28-9 2,2-Dichloropropane NID ug/L 2.0 2 08116/10 16:23 594-20-7 11,1-Dichloropropene ND ug/L 2.0 2 68/16/10 16:23 56�-58-6 cis-1,3-Dichloropropene NID ug/L 2.0 2 08/16/10 16:23 10061-01-5 trans-1,3-Dichloropropene ND ug/L 2.0 2 08/16/10 16:23 10061-02-6 Diisopropyl ether NID ug/L- 2.0 2 08/16/10 16:23 108-20-3 ___,!Date: 08118/2010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Ace." Page 9 of 26 eAnalytical wwwpacelabs com ac, Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-40WT LablD: 9275343004 Collected: 08/11/1011:24 Received: 08/11/1014:40 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Me ' thylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-TetrachloroethEine 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Tr'ichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-T(tchloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane7d4 (S) Tbluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 363.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 4500 Chloride Chloride ASTM D51 6-90 Sulfate Water Sulfate Analytical Method: EPA 8260 ND. ug/L 2.0 2 08/16/10 16:23 100-41-4 ND ug/L 2.0 2 08/16110 16:23 87-68-3 ND ug/L 10.0 2 08/16/10 16:23 591-78-6 ND ug/L 2.0 2 08/16/10 16:23 99-87-6 ND ug/L 4.0 2 08/1 * 6110 16:23 75-09-2 ND ug/L 10.0 2 08/16/10 16:23 108-10-1 ND ug/L 2.0 2 08/16/10 16:23 1634-04-4 ND ug/L 2.0 2 08/16/10 16:23 91-20-3 ND ug/L 2.0 2 08/16/10 16:23 100-42-5 ND ug/L 2.0 2 08/16/10 16:23 630-20-6 ND ug/L 2.0 2 08/16/10 16:23 79-34-5 ND ug/L 2.0 2 08/16/10 16:23 127-18-4 ND ug/L 2.0 2 08/16/10 16:23 108-88-3 ND ug/L 2.0 2 08/16/10 16:23 87-61-6 ND ug[L 2.0 2 08/16/10 16:23 120-82-1 ND ug/L 2.0 2 08/16/10 16:23 71-55-6 ND ug/L 2.0 2 08/16/10 16:23 79-00-5 .11.1 ug/L 2.0 2 08/16/10 16:23 79-01-6 ND ug/L 2.0 2 08/16/10 16:23 76-69-4 ND ug/L 2.0 2 08/16110 16:23 96-18-4 ND ug/L .4.0- 2 08116/10 16:23 108-05-4 ND -ug/L 2.0 - 2 08/16/10 -16:23 -75r01A, - ND ug/L 4.0 2 08/16/10 16:23 179601-23-1 ND ug/L 2.0 2 08/16/10 16:23 95-47-6 95 % 70-130 2 08/16/10 16:23 .460-00-4 112 % 70-130 2 08/16/10 16:23 1868-53-7 105 % 70-130 2 08/16/10 16:23 17060-07-0 99 % 70-130 2 08/16/10 16:23 2037-26-5 Analytical Method: SM 2320B 16.8 mg/L 5.0 1 08/16/10 15:03 Analytical Method: EPA 353.2 2.8 mg/L 0.10 1 08/11/10 23:25 Analytical Method: SM 4500-CI-E ND mg/L 5.0 1 08/16/10 09:55 16887-00-6 Analytical Method: ASTM D516-90 ND mg/L 5.0 1 08/17110 15:49 14808-79-8 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS Page 10 of 26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. /�;alceAnalyticals 2225 Riverside Dr. 9800 Kiricey Ave. Suite 100 www.pacWabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Sample: MW-41WT LabID: 9275343005 Collected: 08111/10 10:36 Received: 08/11/10 14:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 08113/10 11:50 08/16/10 17:31 7440-38-2 Cadmium ND ug/L 1.0 1 08/13110 11:50 08/16/10 17:31 7440-43-9 Chromium 127 ug/L 5.0 1 08h3/10 11:50 08/16/10 17:31 7440-47-3 Copper 94.1 ug/L 5.0 1 08113/10 11:50 08/16/10 17:31 7440-50-8 Lead 12.9 ug/L 5.0 1 08/13/10 11:50 08116/10 17:31 7439-92-1 Zinc 124 ug/L 10.0 1 08/13110 11:50 08/16/10 17:31 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 08/12110 18:00 08114/10 12:17 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 08116/10 15:04 67-64-1 Benzene ND ug/L 1.0 1 08/16/10 16:04 71-43-2 Bromobenzene ND ug/L 1.0 1 08/16/10 15:04 108-86-1 Bromochloromethane ND ug/L 1.0 1 08/16/10 15:04 74-97-5 Bromodichloromethane ND ug/L 1.0 1 08/16/10 15:04 75-27-4 Bromoform ND ug/L 1.0 1 08/16/10 15:04 75-25-2 (Bromomethane i ND ug/L 2.0 1 08/16/10 15:04 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 08/16/10 15:04 78-93-3 Carbon tetrachloride ND ug/L 1,0 1 08/16/10 15:04 56-23-5 Chlorobenzene ug/L 1.0 1 08116/10 15:04 108-90-7 citionoe-thame _ND ND ug1L 1.6 bul 6h b i �-_04 ��_-06-_3_ Chloroform 4.2 ug/L 1.0 1 08/16/10 15:04 67-66-3 Chloromethane ND ug/L 1.0 1 08116/10 15:04 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 08/16/10 15:04 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 08/16110 15:04 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 08/16110 15:04 96-12-8 Dibromochloromethane ND ug/L 1.0 1 08/16110 15:04 124-48-1* 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/16/10 15:04 106-93-4 Dibromomethane ND ug/L 1.0 1 08/16/10 15:04 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 08/16/10 15:04 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 08/16/10 15:04 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 08/16/10 15:04 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 08/16/10 15:04 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 08/16/10 15:04 75-34-3 1,2 - Dichloroethane ND ug/L 1.0 1 08/16/10 15:04 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 08/16/10 15:04 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 08/16/10 15:04 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 08/16/10 15:04 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 08/16/10 15:04 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 08/16/10 15:04 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 08/16110 15:04 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 08/16110 15:04 563-58-6 c7is-1,3-Dichloropropene ND ug/L 1.0 1 08/16/10 15:04 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 08/16110 15:04 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 08/16110 15:04 108-20-3 "---,,!Date: 08/18/2010 12:42 PM REPORT OF LABORA71 ORY ANALYSIS This report sheH not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Acca, Page 11 of 26 Pace Analytical Services, Inc. Pace Analytical Services, Inc. . a ceAnaljNcal 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wwwpacekbs com Asheville, NC 28804 Huntersville, NG 28078 (828)254-7176 (704)875-9092 C, ANALYTICAL RESULTS Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Sample: MW-41W'r Lab ID: 9275343006 Collected: 08/11/10 10:36 Received: 08/11/10 14:40 Matrix- Water Parameters Results Units- Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug[L .1.0 1 08/16/10 15:04 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/16/10 15:04 87-68-3 2-Hexanone ND ug/L 5.0 1 08/16/10 15:04 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 08/1'6/10 15:04 99-87-6 Methylene Chloride ND ug/L 2.0 1 08/16110 15:04 76-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 08/16/10 15:04 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 08116/10 16:04 1634-04-4 Naphthalene ND ug/L 1.0 1 08/16110 15:04 91-20-3 Styrene ND ug/L 1.0 1 08116/10 15:04 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/16/10 15:04 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 08116/10 15:04 79-34-5 Tetrachloroethene ND ug/L 1.0 1 08116/10 15:04 127-18-4 Toluene ND ug/L 1.0 1 08/16/10 15:04 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/16/10 15:04 87-61-6 1,2,4-Tr'ichlorobenzene ND ug/L 1.0 1 08/16/10 15:04 120-82-1 1,1,1-T(ichloroethane ND ug/L 1.0 1 08/16/10 15:04 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 08/16110 15:04 79-00-5 Trichloroethene 2.0 ug/L 1.0 1 08/16/10 15:04 79-01-6 Trichlorofluoro methane ND ug/L 1.0 1 08/16/10 15:04 75-69-4 1,2,3-Trichloropropane ND ug/L 11.0 1 08/16/10 15:04 96-184 Viny, acetate ND ug/L .2.0 1 08/16/10 15:04 108-05-4 Vinyl -chloride -ND ug/L -- 1.0 -1- 081-16/10 15:04 75-01-4 m&p-Xylene ND ug/L 2.0 1 08/16/10 15:04 .179601-23-1 o-Xylene NO ug/L 1.0 1 08/16/10 15:04 95-47-6 4-Bromofluorobenzene (S) 99 % 70-130 1 08/16110 15:04 460-00-4 Dibromofluoromethane (S) 113 % 70-130 1 08/16/10 15:04 1868-53-7 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 08/16/10 15:04 17060- ' 07-0 Tbluene-d8 (S) 101 % 70-130 1 08/16/10 15:04 2037-26-5 232 OB Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 10.5 mg/L 5.0 1 08/16/10 15:04 353.2 Nitrogen, NO2/NO3 unpres; Analytical Method: E.PA 353.2 Nitrogen, Nitrate 3.2 mg/L 0.10 1 08111/10 23:24 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 1 08/16/10 09:55. 16887-00-6 ASTM D51 6-90 Sulfate Water Analytical Method: ASTM D516-90 Sulfate NO mg/L 5.0 1 08/17/10 15:49 14808-79-8 Page 12 of 26 Date: 08118/2010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shali not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 1�0aceAnalyfical"' Asheville, NC 28804 Huntersville, NC 28078 WWW.paW2b&=n (828)254-7176 (704)876-9092 ANALYTICAL RESULTS Project' TEC PILOT TEST 08/11 Pace Project No.: 9275343 Sample: TRIP BLANK Lab ID: 9275343006 Collected: 08/1111000:00 Received: 08111/1014:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 IVISV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 08/14/10 04:44 67-64-1 Benzene ND ug/L 1.0 1 08114110 04:44 *71-43-2 Bromobenzene ND ug/L 1.0 1 08/14110 04:44 108-86-1 Bromochloromethane ND ug/L 1.0 1 08/14/10 04:44 74-97-5 Bromodichloromethane ND ug/L 1.0 1 108/14/10 04:44 76-27-4 Bromoform ND ug/L 1.0 1 08/14110 04:44 75-26-2 Bromoniethane ND ug/L 2.0 1 08/14/10 04:44 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 08/14/10 04:44 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 08/14/10 04:44 56-23-5 Chlorobenzene ND ug/L 1.0 1 08114110 04:44 108-90-7 Chloroethane ND ug/L 1.0 1 08114/10 04:44 75-00-3 Chloroform ND ug/L 1.0 1 08/14110 04:44 67-66-3 Chloromethane ND ug/L 1.0 1 08114110 04:44 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 08/14110 04:44 96-49-8 4-Chlorotoluene ND ug/L 1.0 1 08114/10 04:44 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 08114/10 04:44 96-12-8 Dibromochloromethane ND ug/L 1.0 1 08114/10 04:44 124-48-1 1,2-Dibromoethane (PDB) ND ug/L 1.0 1 08/14110 04:44 106-93-4 Dibromomethane ND ug/L 1.0 1 08/14/10 04:44 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 08/14/10 04:44 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 08/14/10 04:44 541-73-1 1,4�Dichlorobenzene ND ug/L 1.0 1 08114/10 04:44 106-46-7- Dichlorodifluoromethane ND ug/L 1.0 1 08/14/10 04:44 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 08/14/10 04:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 08114/10 04:44 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 08/14/10 04:44 75-35-4 ci�-1,2-Diclhloroethene ND ug/L 1.0 1 08114/10 04:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 08/14/10 04:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 08/14/10 04:44. 78-87-5 1,3-Dichloropropane ND'ug/L 1.0 1 08/14110 04:44 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 08/14/10 04:44 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 08/14/10 04:44 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 08/14/10 04:44 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 08114/10.04:44 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 08/14110 04:44 108-20-3 Ethylbenzene ND ug/L 1.0 1 08114110 04:44 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 08/14110 04:44 87-68-3 2-Hexanone ND ug/L 5.0 1 08/14/10 04:44 691-78-6 p-Isopropyltoluene ND ug/L 1.0 1 08/14/10 04:44 99-87-6 Methylene Chloride ND ug/L 2.0 1 08/14/10 04:44 75-09-2 4-Methyl-2-pentanone (MlBK) ND ug/L 5.0 1 08/14/10 04:44 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 08/14/10 04:44 1634-04-4 Naphthalene ND ug/L 1-.0 1 .08/14/10 04:44 91-20-3 Styrene ND ug/L 1.0 1 08/14/10 04:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 08/14110 04:44 630-20-6 1,1,2,2-Tetrachlaroethane ND ug/L 1.0 1 08/14/10 04:44 79-34-6 Tetrachloroethene ND ug/L 1.0 1 08/14/10 04:44 127-18-4 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS Page 13 of 26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. - a eAnalytical C, ww.pa6d.ftc= Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave: Suite 100 Huntersville, NC 28078 (704)876-9092 Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Sample: TRIP BLANK Lab ID: 9275343006 Collected: 08/11/10 00:00 Received: 08/11/10 14:40 Matrix: Water Parameters Results Units Report Limit DIF Prepared Analyzed CAS No. Qua[ 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 08/14110 04:44 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 08/14110 04:44 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 08/14/10 04:44 120-82-1 1,1,1-Trichloro6thane ND ug/L 1.0 1 08/14/10 04:44 71-55-6 1,1,2-Trichloroethane ND ug/L .1.0 1 08/14/10 04:44 79-00-5 Trichloroethene ND ug/L 1.0 1 08114110 04:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 08/14110 04:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 08/14/10 04:44 96-18-4 Vinyl acetate ND ug/L 2.0 1 08/14/10 04:44 108-05-4 Vinyl chloride ND ug/L 1.0 1 08/14/10 04:44. 75-01-4 m&p-Xylene ND ug/L 2.0 1 08/14/10 04:44 179601-23-1 o-Xylene ND ug/L 1.0 1 08/14/10 04:44 95-47-6 4-Bromofluorobenzene (S) 97 % 70-130 1 08/14/10 04:44 460-00-4 Dibromofluoromethane (S) 109 % 70-130 1 08114/10 04:44 1868-53-7 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 08/14/10 04:44 17060-07-0 Tbluene-d8 (S) 98 % 70-130 1 08/14/10 04:44 2037-26-5 Date: 08/1812010 12:42 PM REPORT OF LABORATORY ANALYSIS Page 14 of 26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. C Analytical www.pacelabs.com Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 98001(inceyAve. Suiteloo Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA QC Batch: MPRP16850 Analysis Method:. EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9275343005 METHOD BLANK: 482512 Matrix: Water Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9275343005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 'Arsenic ug/L ND 5.0 08/16110 15:55 Cadmium ug/L ND 1.0 08/16/10 15:55 Chromium ug/L ND 6.0 08/16/10 15:55 Copper ug/L ND 5.0 08/16/10 15:55 Lead ug/L ND 5.0 08/16110 15:55 Zinc ug/L ND 10.0 08/16/10 15:55 LABORATORY CONTROL SAMPLE: .482513 Spike LCS- LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Arsenic ug/L 500 487 97 80-120 Cadmium ug/L 500 491 98 Chromium ug/L 500 493 99 80-120 Copper ug/L 500 486 97 80-120 Lead ug/L 500 489 98 80-120 -Zinc- ug/L 500 490 98 80-120 MATRIX SPIKE SAMPLE: 482514 9274639015 Spike IVIS IVIS % Rec Parametef Units Result Conc Result % Rec Limits Qualifiers Arsenic ug/L ND 500 502 100 75-125 Cadmium ug/L ND 500 495 99 75-125 Chromium ug/L ND 500 498 99 75-125 Copper ug/L ND 500 502 100 .75-125 Lead ug/L ND 560 485 97 75-125 Zinc ug/L 17.5 500 516 100 75-125 SAMPLE DUPLICATE: 482515 Parameter Arsenic Cadmium Chromium Copper Lead Zinc �'--'.,)ate: 08/18/2010 12:42 PIVI Units 9275159001 Result Dup Result RPD Qualifiers ug/L 61.8 57.3 8 ug/L ND ND ug/L 22.8 21.4 .6 ug/L 21.5 20.6 4 ug[L 6.3 5.9 6 ug/L 2290 2210 3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Acca# ' Page 15 of 26 Pace Analytical Services, Inc. ceApalXical 2225 Riverside Dr. . wmpa*ahcom Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 QC Batch: MERP/2946 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 9275343001, 9276343002, 9275343003, 9275343004, 9275343005 METHOD BLANK: 481821 Matrix: Water Associated Lab Samples: 9275343001, 9275343002, 927043003, 9275343004, 9275343005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 08/14/10 12:17 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)876-9092 LABORATORY CONTROL SAMPLE: 481822 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec. Limits Qualifiers Mercury ug/L 2.5 3.0 119 80-120 MATRIX SPIKE SAMPLE: 481823 9274639011 Spike IVIS MS. % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury ug/L 4.6 2.5 7.4 110 75-1 . 25 SAMPLE DUPLICATE: 481824 9274639012 Dup Parameter Units Result Result RPD Qualifiers Mercury ug/L 3.6 3.6 0 Date: 08118/2010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. AC,o,. Page 16 of 26 aceAnalyfical" www.pacelabs.com Project: TEC PILOT TEST 08/11 Pace Project No.: 9276343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA . QC Batch: MSW11876 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9275343005,9275343006 METHOD BLANK:' 482802 Matrix: Water Associated Lab Samples: 92753430 . 01,9275343002,9275343003,9276343004,9275343005,9275343006 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/14/10 04:19 1,1,1-Tr'ichloroethane ug�l- ND 1.0 08/14/10 04:19 1,12,2-Tetrachloroethane ug/L ND 1.0 08114/10 04:19 1,1,2-Trichloroethane ug/L ND 1.0 08/14/10 04:19 M-Dichloroethane ug/L ND 1.0 08/14/10 04:19 1,1-Dichloroethene ug/L ND 1.0 08/14/10 04:19 1,11-Dichloropropene ug/L ND 1.0 08/14/10 04:19 1,2,3-Trichlorobenzene ug/L ND 1.0 08114/10 04:19 1,2,3-Trichloropropane ug/L ND 1.0 08/14/10 04:19 1,2,4-Trichlorobenzene ug/L ND 1.0 08/14/10 04:19 1,2-Dibromo-3-chloropropane ug/L ND 6.0 08/14110 04:19 1,2-Dibromoethane (EDB) ug/L ND 1.0 08/14/10 04:19 1,2-Dichlorobenzene ug/L ND 1.0 08/14/10 04:19 1,2-Dichloroethane ug/L ND 1.0 08/14/10 04:19 1,2-Dichloropropane ug/L ND 1.0 08/14/10 04:19 1,3-Dichlorobenzene ug/L ND 1.0 08/14/1G04:19 1,3-Dichloropropane ug/L ND 1.0 08/14/10 04:19 1,4-Dichlorobenzene ug/L ND 1.0 08/14/10-04:19 2,2-Dichloropropane ug/L ND 1.0 08/14110 04:19 2-Butanone (MEK) ug/L ND 5.0 08/14/10 04:19 2-Chlorotoluene ug/L ND 1.0 08/14/10 04:19 2-Hexanone ug/L ND 5.0 08/14/10 04:19 4-Chlorotoluene ug[L ND 1.0 08/14/10 04:19 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 08/14/10 04:19 Acetone ug/L ND 25.0 08/14/10 04:19 Benzene ug/L ND 1.0 08114/10 04:19 Bromobenzene ug/L ND 1.0 08/14/10 04:19 Bromochloromethane ug/L ND 1.0 08/14/1.0 04:19 Bromodichloromethane ug/L ND 1.0 08/14/10 04:19 Bromoform -ug/L ND 1.0 08/14/10 04:19 Bromomethane ug/L ND 2.0 08114110 04:19 Carbon tetrachloride ug/L ND 1.0 08/14/10 04:19 Chlorobenzene ug/L ND 1.0 08/14/10 04:19 Chloroethane ug/L ND 1.0 08/14/10 04:19 Chloroform ug/L- ND 1.0 08/14/10 04:19 Chloromethane ug/L ND 1.0 08/14/10 04:19 cis-1,2-Dichloroethene ug/L ND 1.0 08114110 04:19 cis-1,3-Dichloropropene ug/L ND 1.0 08/14110 04:19 Dibromochloromethane ug/L ND 1.0 08114/10 04:19 Dibromomethane ug/L ND 1.0 08/14/10.04:19 Dichlorodifluoromethane ug/L ND 1.0 08/14/10 04:19 Diisopropyl ether ug/L ND 1.0 08/14/10 04:19 Ethylbenzene ug/L ND 1.0 08/14110 04:19 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Acco'. Qualifiers Pace Analytical Services,.Inc. 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 (704j875-9092 Page 17 of 26 acpeAnalyfical pacdabs.- Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 METHOD BLANK: 482802 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)2.54-7176 QUALITY CONTROL DATA Matrix: Water Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9275343005,9275343006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0. 08/14/10 04:19 m&p-Xylene ug/L ND 2.0 08/14/10 04:19 Methyl-tert-butyl ether ug/L ND 1.0 08/14110 04:19 Methylene Chloride ug/L ND 2.0 08/14/10 04:19 Naphthalene ug/L ND 1.'0 08/14/10 04:19 o-Xylene ug/L ND 1.0 08/14/10 04:19 p-Isopropyltoluene ug/L. ND 1.0 08/14110 04:19 Styrene ug/L ND 1.0 08/14/10 04:19 Tetrachloroethene ug/L ND 1.0 08/14/10 04:19 Toluene ug/L ND 1.0 08/14/10 04:19 trans-1,2-Dichloroethene ug/L ND 1.0 08/14/10 04:19 trans-1,3-Dichloropropene ug/L ND 1.0 08/14/10 04:19 Trichloroethene ug/L ND 1.0 08/14/10 04:19 Trichlorofluoromethane ug/L ND 1.0 08/14110 04:19 Vinyl acetate ug/L ND 2.0 08/14/10 04:19 Vinyl chloride ug/L ND 1.0 08/14/10 04:19 1,2-Dichloroethane-d4 (S) % 106 70-130 08/14/10 04:19 4-Bromofluorobenzene (S) % 92 70-130 08/1410 04:19 Dibromofluoromethane (S) % 109 70-130 08114/10 04:19 Toluene-d8 (S). % 102 70-130 08/14/10 04:19 METHOD BLANK: 484117 Matrix: Water Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9275343005,9275343006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachlo'roethane ug/L ND 1.0 08/16/10 11:39 1,1,1-Trichloroethane ug/L ND 1.0 08/16/10 11:39 1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/16/10 11:39 1,1,2-Trichloroethane ug/L ND 1.0 08/16/10 11:39 1,1-Dichloroethane ug/L ND 1.0 08/16/10 11:39 1,1-Dichloroethene uglL ND 1.0 08/16/10 11:39 1,1-Dichloropropene ug[L ND 1.0 08/16/10 11:39 1,2,3-Trichlorobenzene ug/L ND 1.0 08/16110 11:39 1,2,3-T(ichloropropane ug/L ND 1.0 08/16/10 11:39 1,2,4-T(ichlorobenzene ug/L ND 1.0 08/16/10 11:39 1,2-Dibromo-3-chloropropane ug/L ND 5.0 08116/10 11:39 1,2-Dibromoethane (EDB) ug/L ND 1.0 08/16/10 11:39 1,2-Dichlorobenzene ug/L ND 1.0 08/16/10 11:39 1,2-Dichloroethane ug/L ND 1.0 08/16/10 11:39 1,2-Dichloropropane ug/L ND 1.0 08/16/10 11:39 11,3-Dichloro�enzene ug/L ND 1.0 08/16/10 11:39 1,3-Dichloropropane ug/L ND 1.0 08/16/10 11:39 1,4-Dichlorobenzene ug/L ND 1.0 08/16/10 11:39 2,2-Dichloropropane ug/L ND 1.0 08/16/10 11:39 2-Butanone (MEK) ug/L I`4D 6.0 08/16/10 11:39 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 26 1�;a'ceAffllyticalo www.pacek-&.com Project: TEC PILOT TEST 08111 Pace Project No.: .9275343 METHOD BLANK: 484117 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 . (828)254-7176 QUALITY CONTROL DATA Matrix: Water Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9275343005,9275343006 Blank Reporting . Parameter Units Result Limit Analyzed Qualifiers 2-Chlorotoluene ug/L ND 1.0 08/16/10 11:39 2-Hexanone ug/L ND 5.0 08/16/1011:39 4-Chlorotoluene ug/L ND 1.0 08/1611011:39 4-Meihyl-2-pentanone (MIBK) ug/L ND 5.0 08/16/10 11:39 Acetone ug/L ND 25.0. 08/16110 11:39 Benzene ug/L ND 1.0 08116110 11:39 Bromobenzene ug/L ND 1.0 08116/1011:39 Bromochloromethane ug/L ND 1.0 08116/10 11:39 Bromodichloromethane ug/L ND 1,0 08/16110 11:39 Bromoform ug/L ND 1.0 08/16/10 11:39 Bromomethane ug/L ND 2.0 08/16110 11:39 Carbon tetrachloride ug/L ND 1.0 08/16/10 11:39 Chlorobenzene ug/L ND 1.0 .08/16/10 11:39 Chloroethane ug/L ND 1.0 08116/10 11:39 Chloroform ug/L ND 1.0 08/16110 11:39 Chloromethane ug/L ND 1.0 08/16110 11:39, cis-1,2-Dichloroethene ug/L ND 1.0 08/16/10 11:39 c.is-1,3-Dichloropropene ug/L �ND 1.0 08/16110 11:39 Dibromochloromethane ug/L ND 1.0 08/16/10 11:39 Dibromomethane ug/L ND 1.0 08/16/10 11:39 Dichlorodifluoromethane ug/L ND 1.0 08116/10 11:39 Dilsopropyl ether- -ug/L - ND- 1.0- 08/16/10-11039- Ethylbenzene ug/L ND 1.0 08/16/10 11:39 Hexachloro-1,3-butadiene ug/L ND 1.0 08/16/10 11:39 m&p-Xylene ug/L ND 2.0 08/16110 11:39 Methyl-tert-butyl ether ug/L ND 1.0 08/16/10 11:39 Methylene Chloride ug/L ND 2.0 08/16/10 11:39 Naphthalene ug/L ND 1.0 08116110 11:39 o-Xylene ug/L ND 1.0 08/16/10 11:39 p-Isopropyltoluene ug/L ND 1.0 08/16/10 11:39 Styrene ug/L ND 1.0 08/16/1011 :39 Tetrachloroethene ug/L ND 1.0 08/16/110 11:39 Toluene ug/L ND 1.0 08116/10 11:39 trans-1,2-Dichloroethene ug/L ND 1.0 08/16/10 11:39 trans-1,3-.Dichloropropene ug/L ND 1.0 08/16/10 11:39 Trichloroethene ug/L ND 1.0 08/16/10 11:39 Trichlorofluoromethane ug/L ND 1.0 08/16110 11:39 Vinyl acetate ug/L ND 2.0 08116/10 11:39 Vinyl chloride ug/L ND 1.0 08/16/10 11:39 1,2-Dichloroethane-d4 (S) % 104 70-130 08/16110 11:39 4-Bromofluorobenzene (S) % 98 70-130 08/16/10 11:39 Dibromofluoromethane (S) % 109 70-130 08/16/10 11:39 Tbluene-d8 (S) % 100 70-130 08/16110 11:39 Pace Analytical Services, Inc. 9800KInceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS Page 19 of 26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACCg,. 7aci . . 0 Analiftal www.pecolabs.com Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NG 28804 (828)254-7176 QUALITY CONTROL DATA' Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)876-9092 LABORATORY CONTROL SAMPLE: 482803 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 55.2 110 70-130 1,1,1-Trichloroethane ug/L 50 56.8 114 70-130 1,1,2,2-Tetrachloroethane ug/L 50 56.7 113 70-130 1,1,2-Trichloroethane ug/L 50 54.9 110 70-130 1,1-Dichloroethane ug/L 50 52.7 105 70-130 M-Dichloroethene ug/L 50 54.1 108 70-132 IJ-Dichloropropene ug/L 60 49.2 98 70-130 1,2,3-Tdchlorobenzene ug/L 50 54.5 109 70-135 1,2,3-Trichloropropane. ug/L 50 52.8 106 70-130 1,2,4-Tdchlorobenzene ug/L 50 52.9 106 70-134 1,2-Dibromo-3-chloropropane ug/L 50 53.5 107 70-130 1,2-Dibromoethane (EDB) ug/L 50 53.0 106 70-130 1,2-Dichlorobenzene ug/L 50 53.5 107 70-130 .1,2-Dichloroethane ug/L 50 56.3 113 70-130 1,2-Dichloropropane ug/L 50 49.1 98 70-130 1,3-DiGhlorobenzene ug/L 50 51.2 102 70-130 1,3-bichloropropane ug/L 50 61.5 103 70-130 1,4-Dichlorobenzene ug/L 50 50.4 101 70-130 2,2-Dichloropropane ugIL 50 42.3 85' 58-145 2-butanone (MEK) ug/L 100 109 109 70-145 2-Chlorotoluene ug/L 50 52.2 104 70-130 2-Hexanone ug/L I , 00 109 109 70-144 4-Chlorotoluene ug/L 50 52.6 105 70-130 4-M6tliyI-2--p-entan-one-(MI B-K) ug/L - 100 11 - 0 110 7 - 0-140 Acetone ug/L 100 120 120 50-175 Benzene ug/L 50 50.7 101 70-130 Bromobenzene ug/L 50 52.2 104 70-130 Bromochloromethane ug/L 50 59.3 119 70-130 Bromodichloromethane ug/L 50 54.7 109 70-130 Bromoform ug/L 50 55.2 110 70-130 Bromomethane ug/L .50 48.1 96 54-130 Carbon tetrachloride ug/L 50 54.3 109 70-132 Chlorobenzene ug/L 50 52.7 105 70-130 Chloroethane ug/L 50 46.3 .93 64-134 Chloroform ug/L 50 54.3 109 70-130 Chloromethane ug/L 50 47.8 96 64-130 cis-1,2-Dichloroethene ug/L 50 50.9 102 70-131 cis-1,3-Dichloropropene ug/L 50 50.6 101 70-130 Dibromochloromethane ug/L 50 55.0 110 70-130 Dibromomethane ug1L 50 58.2 116 70-131 Dichlorodifluoromethane ug/L 50 37.9 76 56-130 Dilsopropyl ether ug/L 50 51.6 103, 70-130 Ethylbenzene ug/L 50 50.9 102 70-130 Hexachloro-1,3-butadiene ug/L 60 49.9 100 70-130 m&p-Xylene ug/L 100 104 104 70-130 Methyl-tert-butyl ether ug/L 50 53.7 107 70-130 Methylene Chloride ug/L 50 50.9 102 63-130 Naphthalene ug/L 50 56.4 113 70-138 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS Page20of26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalyfical-' www.pacelab&com Pioject: TEC PILOT TEST 08/11 Pace Project No.: 9275343 LABORATORY CONTROL SAMPLE: 482803 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Parameter Units Spike Conc. o-Xylene ug/L 50 p-Isopropyltoluene ug/L 50 Styrene ug/L 50 Tetrachloroethene ug/L 50 Toluene ug/L 50 trans-1,2-Dichloroethene ug/L 50 trans-1,3-Dichloropropene ug/L 50 Trichloroet6ne ug/L 50 Tdchlorofluoromethane ug[L 50 Vinyl acetate ug/L 100 Vinyl chloride ug/L 50 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Tbluene-d8 (S) % MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 482804 9275214011 Parameter IJ-Dichloroethene- Benzene- Chlorobenzene Toluene Trichloroethene 1,2-Dichloroetha.ne-d4 (S) 4-BromofluorobenzL-ne (S) Dibromofluoromethane (S) Tbluene-d8 (S) Date: 08/18/2010 12:42 PM. Units Result ug/L ND - -ug/L- -ND ug/L ND ug/L ND ug/L ND MS Spike Conc. 50 50 50 50 50 LCS Result 53.8 52.8 53.9 51.2 55.0 62.9 52.3 54.2 47.7 101 45.5 482805 .MSD Spike MS Conc. Result 60 43.1 50 - 48A 50 51.2 50 54.3 50 54.9 LCS % Rec 108 106 108 102 110 106 105 108 95 101 91 109 102 105 102 % Rec Limits 70-130 70-130 70-130 70-130 70-130 70-130 70-132 70-130 62-133 66-157 69-130 70-130 70-130 70-130 70-130 MSD MS Result % Rec 46.5 86 51.1 97 53.9 102 58.3 109 58.7 110 102 96 106 101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers MSD % Rec % Rec Limits RPD Qual 93 70-166 7 102 -70-148 5 108 70-146 6 117 70-155 7 117 69-161 7 103 70-130 98 70-130 109 70-130 102 70-130 Page 21 of 26 F ceA *wpair bs.com Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 . (828)254-7176 QUALITY CONTROL DATA QC Batch: WET/134.47 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320B Alkalinity Associated Lab Samples: 9275343001, 9275343002, 9275343003, 9275343004, 9275343005 METHOD BLANK: 483446 Matrix: Water Associated Lab Samples: 9275343001, 9275343002, 9275343003, 9275343004, 9276343005 Blank Reporting Parameter Units Result Limit Analyzed Alkalinity, Total as CaCO3 mg/L ND . 5.0 08/16/10 14:55 LABORATORY CONTROL SAMPLE: 483447 Qualifiers Pace Analytical Services, Inc. 9800KInceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092. Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 50.4 101 90-110 SAMPLE DUPLICATE: 483448 9274796001 Dup Parameter Units Result Result RPD - Qualifiers Alkalinity, Total as CaCO3 mg/L 15.8 15.8 0 SAMPLE DUPLICATE: 483449 Parameter Alkalinity, Total as CaCO3 Date: 08118/2010 12:42 PM - . - 9275036010 Units Result mg/L 14.7 Dup Result RPD Qualifiers 14.7 0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. I" Acco, Page 22 of 26 AIVIXkal /5alce www.pacelabs.com Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA QC Batch: WETA17919 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9275343005 METHOD BLANK: 481701 Matrix: Water Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9276343005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.10 08111/10 23:00 LABORATORY CONTROL SAMPLE: 481702 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 5.0 99 90-110 MATRIX SPIKE SAMPLE: Parameter 481703 Units 'Nitrogen, Nitrate mg/L MATRIX SPIKE SAMPLE: Parameter 481705 Units Nitrogen, Nitrate mgiL SAMPLE DUPLICATE: 481704 Parameter Units Nitrogen, Nitrate mg/L SAMPLE DUPLICATE: 481706 Parameter Nitrogen, Nitrate _,)ate: 08/1812010 12:42 PM 9275214001 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers 0.85 5 6.3 109 90-110 9275244005 Spike- -MS IVIS % Rec Result Conc. Result % Rec Limits Qualifiers 4.2 5 8.8 92 90-110 9275214001 Dup Result Result RPD Qualifiers 0.85 0.83 2 9275244005 Units Result mg/L 4.2 Dup Result RPD Qualifiers 4.3 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 23 of 26 eAnalyficalo wwwpacOabacom ac, Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETAf7942 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 9275343001, 9275343002, 9275343003, 9275343004, 9275343005 METHOD BLANK: 483396 Matrix: Water Associated Lab Samples: 9275343001, 9275343002, 9275343003, 9275343004, 9275343005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 5.0 08/16/10 09:64 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 483397 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 21.1 106 90-110 MATRIX SPIKE SAMPLE: 483398 9275036010 Spike MS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chloride* mg/L ND 20 25.4 106 75-125 SAMPLE DUPLICATE: 483399 9275036011 Dup Parameter Units Result Result. RPD Qualifiers Chloride mg/L ND ND D7 Date: 08/18/2010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 26 1�;alceAnalyfical' ww.pacelabsxom Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETAR948 Analysis Method: ASTM D516-90 QC Batch Method: ASTM D516-90 Analysis Description: ASTM D516-90 Sulfate Water Associated Lab Samples: 9275343001,92753430�02,9275343003,9275343004,9275343005 METHOD BLANK: 483783 Matrix: Water Associated Lab Samples: 9275343001,9275343002,9275343003,9275343004,9276343005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/L ND 5.0 08/17/10 16:10 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 483784 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate mg/L 20 19.1 96 90-110 MATRIX SPIKE SAMPLE: 483785 9275036008 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers )Sulfate mg/L 158 20 135- -112 75-125 M1 MATRIX SPIKE SAMPLE: 483787 9275343005 -Spike _MS - MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mg/L ND 20 20.1 100 75-125 SAMPLE DUPLICATE: 483786 9275036009 Dup Parameter Units Result Result RPD Qualifiers Sulfate mg/L ND ND D7 SAMPLE DUPLICATE: 483788 9275421 * 001 Dup Parameter Units Result Result RPD Qualifiers Sulfate mg/L 90.9 102 '12 Date: 0811812010 12:42 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACCQ� Page 25 of 26 ' 0 Pace Analytical Services, Inc. Pace Analytical Services, Inc. ical 2225 Riverside Dr. 980OKinceyAve. Suite 100 oAnalyt wwwpaoslabs com Asheville, NC 28804 Huntersville, �C 28078 (828)254-7176 (704)875-9092 QUALIFIERS Project: TEC PILOT TEST 08/11 Pace Project No.: 9275343 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. ANALYTE QUALIFIERS D7 The sample and/or duplicate results for this parameter are less than the reporting limit, calculations are based on estimated values and may be statistically unreliable. Mi Matrix spike recovery exceeded QQ limits. Batch accepted based on laboratory control sample (L.CS) recovery. Date: 08118/2010 12:42 PM REPORT OF LABORATORY ANALYSIS Page 26 of 26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. CHAIN-OF-CMEN, )Y / Analytical Request Document y Is a L 2� ampleted accurately. 1),!;Ze,��alytical The Chain-of-Custod hjAL LJOCUMENT. All relevant fields must be c J wMilacelaos.com Page: Of Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: CXT� Report To: Attention: A - ?,PVI NJ: BAM 4 123OLMIJ4 L.- Vi 136 5841 V I Copy Add]N 4" 4AW P Zr To: Compan a a: REGUL.ATOR APENCY', f 1 .;5 rfd� Add"'�21' f- NPDES 77GROUND WATER r— DRINKING WATER LIST RCRA r OTHER E,nl Order No.: Pace 0, CbAp a6gL %�?se IR _ nce; -3-5,501 Fax: Project Name: Tec- Pi Pace Project iManager siteLocition 7A" Project RequCsted Due DatefrAP. -7 DAV.-:; Number: Pace Profile #: Requ6sted Analysis Filtered (YIN) S ction D Matrix Codes a Required Client Information MATRIX f CODE COLLECTED Preservatives ��M Drinking Water DW 0 z 0 Water WT Waste Water WW 0 GO COMPOSITE START compos[TE ENDIGRAD w Product P Soll/Sclid SL D, o. R SAMPLE ID oil OL WP of LU a r- Wipe (A-Z, 0-9 Air AR LLI 0 Lu Q. z �< V 0 Sample IDS MUST BE UNIQUE TIssue TS 0 (-) CL z 0 i! — Other OT X LU w 0' , 0. 0 C: � a- 0 0 N C!, as 101 3 tz DATE TIME DATE TIME < =S 1,51 z Z: z ca 1 z 1 210 I < * V I Pace Project No./ Lab I.D. I- NV 1 14275 - 54300 1 I rz, 7.5 3 -? -3 .0 4.2 7S 3 4 9,0d vA w - 4tw-r tIel-M 2� 5 If.500 5 1 1 YVVY1Y I I 1 11. JL-7 5 3 4 -lin 6 1 —Mir �6 le- 4 2--7 n e% e- 7 10 111 4T -T 121 I ADDITIONAL COMMENTS RiLINQUISHE6.BY ���TIO DATE TIME CEPTED.BY I AFFILIATION DAJE� TIME SAMPLE CONDITIONS 00, ORIGINAL SAMPLERN4ME-A 6 G A E' ,§i N T-911 7 R 0 PRINT Name of SAMPLER: CL E E w SIGNATURE SAMPLER: DATE Signed I of (MMIDDN)n: (D *Important Note: By signing this form you am accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any Invoices not pAd b,00 days. I F-Al_L-Q-UZUreV.U1, it�-rway-zuut I $ample Condition Upon Receipt I Pke Analygcal' Client Name:— A 1 t� _r Project # I :Z'25 -34 Ihere Received: El Huntersville',,Ferkheville El Eden Courier: E] Fed Ex UP8 E] USPS;216rient. D Commercial El Pace Other Custody Seal on Cooler/Box Present: El Yes Seals intact: El yes P-110, Packing Material: El Bubble Wrap. .2gu"b-ble Bags E] None ElOther- 406tko'na it�'-.. Pri& D 667 D Thermometer Used: I n#2 14-648-44 Type of Ice Blue None 'T_�amples on ice, cooling process has begun Tamn rnrrd-r-tir%n Ponfnr- fitiri I it �trn C Corrected Cooler Temp.: C Biological Tissue is Frozen: Yes No Date and. Initials of person exyfiining contents:, '-p c;—/// Temp should be above freezing to 6*C Comments.: Chain of Custody Present: ETYes UNo ON/A 1. Chain of Custody Filled Out: No 2!! ONIA 2. Chain of Custody Relinquished: _S2 2<00S ONO ONIA 3. Sampler Name & Signature on COC: ;,)A_�-ONO 0 N/A 4. Samples Arrived within Hold Time: C1y �Sll NO 0 WA 5. Short Hold Time Analysis (<72hr): -2 <e [IN. QN/A 6. .4 - Rush Turn Around Time Requested:* DYes VIl'o ON/A 7. Sufficient Volume: 0<_ 0 No ONIA 8. Correct Containers Used: Xe. ONO EIN/A '9. -Pace Containers Used: ��YesNo ON/A !Containers Intact: Xe. 0 No ON/A 10. Filtered volume received for Dissolved tests ONO ON/A 11. Sample Labels match COC: fY—e s ONO DNIA 12. -Includes date/time/[D/Analysis Matrix: All containers needing preservation . have been checked. 2<e. CIN. El WA 13. All containers needing preservation are found to be in /Yes ONO 11 N/A' 000-1e anc. w recommendation. compll;�e :� - �wA excep 5;��.,,ftrm,TOC, O&G,WI-DRO (water) OA, c Xy. ONO Initial when completed Samr �le—se'hecked for dechlorination: OYes ONO CW/-A00 14. Headspace in VOA Vials (>6mm): ,-El'Ye� ON. 0 NIA 15. Trip Blank Present: 4?!Yes. ONO El N/-A 16. Trip Blank Custody Seals Present '11�y­ ONO EIN/A Pace Trio Blank Lot # (if purchased): — Client Notification/ Resolution: Field Data Required? y Person Contacted: Date/7ime: Comments/ Resolution: Proi e: ,ect hlianager Review: Dat V Note: Whenever there is a discrepancy aff dcting North Cardina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e out.of hold, incorrect preserva.,,ivs, out oftemp, incorrect containers) F-ASV-CS-03-Rev.0-, ceAnalj4kal wmpacelabsxom' October 04, 2010 Mr. Chris Gilbert Altamont Environmental 231 Haywood Street Asheville, NC 28801 RE: Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)815-9092 Dear Mr. Gilbert: Enclosed are the. analytical results for sample(s) received by the laboratory on September 22, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the -body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed -at our Pace Huntersville laboratory -unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lord Patton lorri.pafton@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS Page I of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 0 a ceAnayical wmpacelaftaom Project: TEC-Fairvlew Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 - Charlotte Certification lDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/LELAP Certification #: 04034 South Carolina Drinking Water Cert. * 99006003 New Jersey Certification#: NCO12 Virginia Certification #: 00213 North Carolina Drinking Water Certification #: 37706 Connecticut Certification #: PH-01 04 North Carolina Field Services Certification *: 5342 Florida/NELAP Certification #: E87627 North Carolina Wastewater Certification *: 12 Kentucky LIST Certification *: 84 Pennsylvania Certification *: 68-00784 Louisiana DHH Drinking Water# LA 100031 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Drinking Water Certification *: 37712 Connecticut Certification#: PH-01 06 North Carolina Wastewater Certification *: 40 Florida/NELAP Certification E87648 Pennsylvania Certification #: 68-03578 Massachusetts Certification M-NC030 South Carolina Bioassay Certification *: 99030002 New Jersey Certification #: NC011 South Carolina Certification #: 99030001 North Carolina Bioassay Certification #: 9 Virginia Certification #: 00072 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnWj#a1'& 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wiviv.pacelabs.pom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Sample: MW-39WT Lab ID: 9278187001 Collected: 09/22/10 11:33 Received: 09/22/10 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 09/23/10 11:00 09129/10 23:15 7440-38-2 Cadmium 3.3 ug/L 1.0 1 09/23110-11:00 09/29/10 23:15 7440-43-9 Chromium 391 ug/L 5.0 1 09/23/10 11:00 09/29/10 23:15 7440-47-3 Copper 210 ug/L 5.0 1 09/23/10 11:00 09/29/10 23:15 7440-50-8 Lead 386 ug/L 5.0 1 09/23/10 11:00 09/29/10 23:15 7439-92-1 Zinc 467 ug/L 10.0 1 09123110 11:00 09129/10 23:15 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 09/28/10 09:26 09/28/10 11:03 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25000 1000 09124/10 15:38 67-64-1 Benzene ND ug/L 1000 1000 09/24110 15:38 71-43-2 Bromobenzene ND ug/L 1000 1000 09/24/10 15:38 108-86-1 Bromochloromethane, ND ug/L 1000 1000 09/24110 15:38 74-97-5 Bromodichloromethane ND ug/L 1000 1000 09/24/10 15:38 75-27-4 9romoform ND ug/L 1000 1000 09/24/10 15:38 75-25-2 "Iromomethane ND ug/L 2000 1000 09/24/10 15:38 74-83-9 2-Butanone (MEK) ND ug/L 5000 1000 09/24/10 15:38 78-93-3 Carbon tetrachloride ND ug/L 1000 1000 09/24/10 15:38 56-23-5 Chlorobenzene ND ug/L 1000 1000 09/24/10 15:38 108-90-7 Chloroethane- -ND ug/L 1000 1000 09/24110 15:38 75-00-3 Chloroform ND ug/L 1000 1000 09124/10 15:38 67-66-3 Chloromethane ND ug/L 1000 1000 09/24/10 15:38 74-87-3 2-Chlorotoluene ND ug/L 1000 1000 09/24/10 15:38 95-49-8 4-Chlorotoluene ND ug/L 1000 1000 09/24/10 15:38 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5000 1000 09/24/10 15:38 96-12-8 Dibromochloromethane ND ug/L 1000 1000 09/24/10 15:38 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1000 1000 09/24110 15:38 106-93-4 Dibromomethane ND ug/L 1000 1000 09/24/10 15:38 74-95-3 1,2-Dichlorobenzene ND ug/L 1000 1000 09/24110 15:38 95-50-1 1,3-Dichlorobenzene ND ug/L 1000 1000 09/24/10 15:38 541-73-1 1,4-Dichlorobenzene ND ug/L 1000 1000 09/24/10 15:38 106-46-7 Dichlorodifluoromethane ND ug/L 1000 1000 09/24/10 15:38 75-71-8 1,1-Dichloroethane ND ug/L 1000 1000 09/24/10 15:38 75-34-3 1,2-Dichloroethane ND ug/L 1000 1000 09/24/10 15:38 107-06-2 I,I-Dichloroethene ND ug/L 1000 1000 09124/10 15:38 75-35-4 cis-1,2-Dichloroethene ND ug/L 1000 1000 09/24/10 15:38 156-59-2 trans-1,2-Dichloroethene ND ug/L 1000 1000 09/24/10 15:38 156-60-5 1,2-Dichloropropane ND ug/L 1000 1000 09/24/10 15:38 78-87-5 1,3-Dichloropropane ND ug/L 1000 1000 09/24/10 15:38 142-28-9 2,2-Dichloropropane ND ug/L 1000 1000 09/24/10 15:38 594-20-7 1,1-Dichloropropene ND ug/L 1000 1000 09124/10 15:38 563-58-6 c7is-1,3-Dichloropropene ND ug/L 1000 1000 09/24/10 15:38 10061-01-5 trans-1,3-Dichlorop�opene ND ug/L 1000 1000 09/24/10 15:38 10061-02-6 Dfisopropyl ether ND ug/L 1000 1000 09/24/10 15:38 108-20-3 --,-,-,)ate: 10104/2010 09:51 AM REPORT OF LABORATORY ANALYSIS Page 3 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aneAnaljftal wwwpacelab&com Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 . (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-39Wr Lab ID: 9278187001 Collected: 09/22/10 11:33 Received: 09/22/10 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane' 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (S) Tbluene-d8 (S) 2320BAlkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 4600 Chloride Chloride Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L 6050 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND 6g/L 1320 ug/L 4740 ug/L ND ug/L ND ug/L 12300 ug/L ND ug/L 151000 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 104 % 118 % 123 % 93 % Analytical Method: SM 2320B 14.4 mg/L Analytical Method: EPA 300.0 ND.mg/L Analytical Method: EPA 353.2 0.48 mg/L Analytical Method: SM 4500-CI-E .ND mg/L 1000 1000 1000 1000 5000 1000 1000 1000 2000 1000 5000 1000 1000 .1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 1000 2000 1000 1000 1000 2000 1000 1000 1000 70-130 1000 70-130 1000 70-130 1000 70-130 1000 5.0 1 5.0 1 0.10 1 5.0 1 09/24/10 15:38 100-41-4 09/24110 15:38 87-68-3 09/24/10 15:38 591-78-6 09/24/10 15:38 99-87-6 09/24/10 15:38 75-09-2 09/24/10 15:38 108-10-1 09/24/10 15:38 1634-04-4 09/24/10 15:38 91-20-3 09/24/10 15:38 100-42-5 09/24/10 15:38 630-20-6 09/24110 15:38 79-34-5 09/24/10 15:38 127-18-4 09124/10 15:38 108-88-3 09/24/10 15:38 87-61-6 09/24/10 15:38 120-82-1 09/24/10 15:38 71-55-6 09124/10 15:38 79-00-5 09/24/10 15:�8 79-01-6 09/24/10 15:38 75-69-4 09/24/10 15:38 96-18-4 09/24/10 15:38 108-05-4 09/24/10 15:38 75-01-4 09124/10 15:38 179601-23-1 09124/10 15:38 95-47-6 09/24/10 1 5f38 460-00-4 09/24/10 15:38 1868-53-7 09/24/10 15:38 17060-07-0 09/24/10 15:38 2037-26-5 09/24/10 16:20 09/29/10 07:13 14808-79-8 09/23/10 23:01 09/29/10 11:09 16887-00-6 Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS Page4of25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. �0 .1�55'ceAndljtical' vmw.pacelabs.com Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-40WT LabID: 9278187002 Collected: 09122/10 10:41 Received: 09/22/10 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 09123/10 11:00 09/29/10 23:19 7440-38-2 Cadmium ND ug/L 1.0 1 09/23/10 11:00 09/29/10 23:19 7440-43-9 Chromium 27.3 ug/L 5.0 1 09/23/10 11:00 09/29/10 23:19 7440-47-3 Copper 10.0 ug/L 5.0 1 09123/10 11:00 09/29110 23:19 7440-50-8 Lead NID ug/L 5.0 1 09/23/10 11:00 09129110 23:19 7439-92-1 Zinc 18.9 ug/L 10.0 1 09/2M 0 11:00 09129/10 23:19 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 09/28/10 09:26 09/28/10 11:06 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 09/24/10,16:04 67-64-1 Benzene ND ug/L 1.0 1 09/24/10 16:04 71-43-2 Bromobenzene ND ug/L 1.0 1 09/24/10 16:04 108-86-1 Bromochloromethane ND ug/L 1.0 1 09/24/10 16:04 74-97-5 Bromodichloromethane NID ug/L 1.0 1 09/24/10 16:04 76-27-4 ND ug/L 1.0 1 09/24/10 16:04 75-25-2 Aromomethane ND ug/L 2.0 1 09/24/10 16:04 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 09/24/10 16:04 78-93-3 Carbon tetrachloride NID ug/L 1.0 1 09/24110 16:04 56-23-5 Chlorobenzene ND ug[L 1.0 1 09/24/10 16:04 108-90-7 Chlonbethane ND-tuo/L 1-0- -1 09/24/10 16:04 76-00-3- Chloroform 2.8 ug/L 1.0 1 09/24/10 16:04 67-66-3 Chloromethane ND ug/L 1.0 1 09/24/10 16:04 74-87-3 2-Chlorotoluene Nb ug/L 1.0 1 09/24/10 16:04 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 09/24/10 16:04 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 09/24/10 16:04 96-12-8. Dibromochloromethane ND ug/L 1.0 1 09/24/10 16:04 124-48-1 1,2-Dibromoethane (EDB) NID ug/L 1.0 1 09/24/10 16:04 106-93-4 Dibromomethane ND ug/L 1.0 1 09/24110 16:04 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 09/24110 16:04 95-50-1 1,3-Dichlorob'enzene ND ug/L 1.0 1 09/24110 16:04 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 09/24/10 16:04 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 09/24/10 16:04 75-71-8 1,1-Dichloroethane NID ug/L 1.0 1 09/24/10 16:04 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 09/24/10 16:04 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 09/24/10 16:04 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 09/24/10 16:04 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 09/24/10 16:04 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 09/24/10 16:04 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 09/24/10 16:04 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 09124/10 16:04 594-20-7 IJ-Dichloropropene ND ug/L 1.0 1 09/24/10 16:04 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 09/24110 16:04 10061-01-5 trans-1,3-Dlchlor�opropene ND ug/L 1.0 1 09/24/10 16:04 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 09124/10 16:04 108-20-3 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. �0 L.. Page 5 of 25 acieAnalXical www.pacelabs.com Project: TEC-Fairview Pilot Test Pace Project.No.: 9278187 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 . (704)875-9092 Sample: MW-40WT LablD: 9278187002 Collected: 09/22/10 10:41 Received: 09/22/10 16:22 Matrix: Water Parameters Results Units ReportLimit . DF Prepared Analyzed CAS No. ' Qual 8260 MSV Low Level Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-T(ichloroethane Trichloroethene Trichlorofluoromethane 1,,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (S) Tbluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, Nitrate 4600 Chloride Chloride Date:.10/04/2010 09:51 AM Analytical Method: EPA 8260 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 6.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ub/L 1.0 4.6 Lig/L 1.0 ND ug/L 1.0 .ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 100 % 70-130 118 % 70-130 124 % 70-130 99 % 70-130 Analytical Method: SM 2320B 12.4 mg/L 5.0 Analytical Method: EPA300.0 ND mg/L 5.0 Analytical Method: EPA.353.2 2.9 mg/L 0.10 Analytical Method: SM 4500-CI-E ND mg/L . 5.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 09/24/10 16:04 .100-41-4 09/24/10 16:04 87-68-3 09124/10 16:04 591-78-6 09/24/10 16:04 99-87-6 09/24/10 16:04 75-09-2 09/24/10 16:04 108-10-1 09/24/10 16:04 1634-04-4 09/24/10 16:04 91-20-3 09/24/10 16:04 100-42-5 09/24110 16:04 630-20-6 09/24/10 16:04 79-34-5 09/24/10 16:04 127-18-4 09/24/10 16:04 108-88-3 09/24/10 16:04 87-61-6 09/24110 16:04 120-82-1 09/24/10 16:04 71-55-6 09/24/10 16:04 79-00-5 09/24/10 16:04 79-01-6 09/24/10 16:04 75-69-4 09/24110 16:04 96-18-4 09/24/10 16:04 108-05-4 09/24/10 16:04 75-01-4 09/24/10 16:04 179601-23-1 09/24110 16:04 95-47-6 09/24/10 16:04 460-00-4 09124/10 16:04 1868-53-7 09/24/10 16:04 17060-07-0 09/24/10 16:04 2037-26-5 09/24/10 16:20 09/29/10 07:37 14808-79-8 09/23/10 22:56 09/29/10 11:09 16887-00-6 Page 6 of 25 a Analjtical' 1c ev&W'pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)264-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 2807.8 (704)875-9092 Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Sample: MW-41WT Lab ID: 9278187003 Collected: 09/22/1009:40 Received: 09/22/1016:22 Matdx:Water Parameters Results Units Report Limit DIF Prepared Analyzed CAS No. Qual 6010 MET 1CP Analytical Method: EPA6010 Preparation Method: EPA3010 Arsenic ND ug/L 5.0 1 09/23/10 11:00 09/29/10 23:23 7440-38-2 Cadmium NID ug/L 1.0 1 09/23110 11:00 09/29/10 23:23 7440-43-9 Chromium 126 ug/L 5.0 1 09/23/10 11:00 09/29110 23:23 7440-47-3 Copper 8.2.8 ug/L 5.0 1 09/23t10 11:00 09/29/10 23:23 7440-50-8- Lead 11.1 ug/L 5.0 1' 09/23/10 11:00 09/29/10 23:23 7439-92-1 Zinc 95.9 ug/L 10.0 1 09/23/10 11:00 09/29/10 23:23 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 09128110 09:26 09/28110 11:08 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 09/24/10 16:30 67-64-1 Benzene ND ug/L 1.0 1 09/24/10 16:30 71-43-2 Bromobenzene ND ug/L 1.0 1 09/24110 16:30 108-86-1 Bromochloromethane ND ug/L 1.0 1 09/24/10 16:30 74-97-5 Bromodichloromethane ND ug/L 1.0 1 09/24/10 16:30 75-27-4 3romoform NID ug/L 1.0 1 09/24/10 16:30 75-25-2 ND ug/L 2.0 1 09/24/10 16:30 74-83-9 2-Butanone (MEK) NID ug/L 5.0 1 09/24/10 16:30 78-93-3 Carbon tetrachloride NID ug/L 1.0 1 09/24/10 16:30 56-23-5 Chlorobenzene ND ug/L 1.0 1 09/24/10 16:30 108-90-7 Chloroetha-ne ND-ug-/L 1.0 1 09/24/10 16:30 - 75-00-3 Chloroform 3.4 ug/L 1.0 1 09/24/10 16:30 67-66-3 Chloromethane ND ug/L 1.0 1 09/24/10 16:30 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 09124/10 16:30 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 09/�4110 16:30 106-43-4 1,2-Dibromo-3-chloropropane NID ug/L 5.0 1 09/24/10 16:30 96-12-8 Dibromochloromethane ND ug/L 1.0 1 09/24/10 16:30 124-48-1 1,2-Dibromoethane (EDB) - NID ug/L 1.0 1 09124/10 16:30 106-93-4 Dibromomethane ND ug/L 1.0 1 09/24/10 16:30 74-95-3 1,2-Dichlorobenzene NID ug/L 1.0 1 09124/10 16:30 95-50-1 1,3-Dichlorobenzene ND ug/L -1.0 1 09/24/10 16:30 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 09/24/10 16:30 106-46-7 Dichlorodifluoromethane NID ug/L 1.0 1 09/24/10 16:30 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 09/24/10 16:30 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 09/24/10 16:30 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 09/24/10 16:30 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 09/24/10 16:30 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 09/241/10 16:30 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 09/24/10 16:30 78-87-5 1,3-Dichlor opropane ND ug/L 1.0 1 09/24/10 16:30 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 09/24/10 16:30 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 09/24/10 16:30 563-58-6 cis-1,3-Dichloropropene NID ug/L 1.0 1 09124/10 16:30 10061-01,-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 09/24/10 16:30 10061-02-6 Dilsopropyl ether ND ug/L 1.0 1 09/24/10 16:30 108-20-3 )Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS Page 7 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. WaeAnaljftal ww.pdce1abs.wm Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, KC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Sample: MW-41W'r Lab ID: 9278187003 Collected: 09/22/1009:40 Received: 0912211016:22 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 1.0 1 09/24/10 16:30 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 09/24/10 16:30 87-68-3 2-Hexanone ND ug/L 5.0 1 09/24/10 16:30 591-78-6 p-lsopropyltoluene ND ug/L 1.0 1 09/24/10 16:30 99-87-6 Methyiene Chloride ND ug/L 2.0 1 09/24/10 16:30 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 09/24/10 16:30 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 09/24/10 16:30 1634-04-4 Naphthalene ND ug/L 1.0 1 09/24/10 16:30 91-20-3 Styrene ND ug/L 1.0 1 09/24/10 16:30 100-42- - 5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 09/24/10 16:30 630-20-6 1,1,�,2-Tetrachloroethane ND ug/L 1.0 1 09/24110 16:30 79-34-5 Tetrachloroethene ND ug/L 1.0 1 09/24110 16:30 127-18-4 Toluene ND ug/L 1.0 1 09/24/10 16:30 108-88-3 1,2,3-Tr'ichlorobenzene ND ug/L 1.0 1 09/24/10 16:30 87-61-6 1,2,4-Tr'ichlorobenzene ND ug/L 1.0 1 09/24/10 16:30 120-82-1 1,1,1-T(ichloroethane ND ug/L 1.0 1 09/24/10 16:30 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 09/24110 16:30 79-00-5 Trichloroethene ND ug/L 1.0 1 09/24110 16:30 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 09124/10 16:30 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 09124/10 16:30 96-18-4 Vinyl acetate ND ug/L 2.0 1 09/24/10 16:30 108-05-4 Vinyl chloride ND ug/L 1.0 1 09124/10 16:30 75-01-4 m&p-Xylene ND ug/L 2.0 1 09/24/10 16:3b 179601-23-1 o-Xylene ND ug/L 1.6 1 09/24110 16:30 95-47-6 4-Bromofluorobenzene (S) 100 % 707130 1 09/24/10 16:30 460-00-4 Dibromofluoromethane (S) 118 % 70-130 1 09/24/10 16:30 1868-53-7 1,2-Dichloroethane-d4 (S) 122 % 70-130 1 09124/10 16:30 17060-07-0 Tbluene-d8 (S) 99 % 70-130 1 09/24/10 16:30 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCC3 10.3 mg/L 5.0 1 09/24110 16:20 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5.0 1 09/29110 08:48 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 3.3 mg/L 010 1 09/23/10 22:55 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 1 09/29/10 11:09 16887-00-6 Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9SOOKinceyAve. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Sample: RW-6 Parameters Lab ID: 9278187004 Collected: 09/22/10 12:37 Results Units Report Limit DF Received: 09122/10 16:22 Matrix: Water Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 09123/10 11:00 09/29/10 23:27 7440-38-2 Cadmium ND ug/L 1.0 1 09/23/10 11:00 09/29/10 23:27. 7440-43-9 Chromium ND ug/L 5.0 1 09/23110 11:00 09/29/10 23:27 7440-47-3 Copper ND ug/L 5.0 1 09/23/10 11:00 09129/10 23:27 7440-50-8 Lead ND ug/L 5.0 1 09123/10 11:00 09/29/10 23:27 7439-92-1 Zinc 30.8 ug/L 10.0 1 09/23/10 11:00 09/29/10 23:27 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 09/28/10 09:26 09/28/10 11:11 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 125 5 09/24/10 19:56 67-64-1 Benzene ND ug/L 5.0 6 09/24/10 19:56 71-43-2 Bromobenzene ND ug/L 5.0 6 06/24/10 19:56 108-86-1 Bromochloromethane ND ug/L 5.0 5 09/24/10 19:56 74-97-5 Bromodichlorom ethane ND ug/L 5.0 5 09/24110 19:56 75-27-4 ND ug/L 5.0 5 09/24/10 19:56 75-25-2 ,Iromomethane ND ug/L 10.0 5 09/24/10 19:66 74-83-9 -'-'-Butanone (MEK) ND ug/L 25.0 5 09/24/10 19:56 78-93-3 Carbon tetrachloride ND ug/L 5.0 5 09/24/10 19:56 56-23-5 Chlorobenzene ND ug/L 5.0 5 09/24110 19:56 108-90-7 Chloroethane ND ug/L 5.0 5 09/24/10 19:56- 75-00-3 Chloroform ND ug/L 5.0' 5 09/24/10 19:56 67-66-3 Chloromethane ND ug/L 5.0 5 09/24/10 19:56 74-87-3 2-Chlorotoluene ND ug/L 5.0 5 09/24/10 19:56 95-49-8 4-Chlorotoluene ND. ug/L 5.0 5 09/24/10 19:56 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 25.0 5 09/24110 19:56 96-12-8 Dibromochloromethane ND ug/L 5.0 5 09/24/10 19:56 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 5 09/24/10 19:56 106-93-4 Dibromomethane ND ug/L 5.0 5 09/24/10 19:56 74-95-3 1,2-Dichlorobenzene- ND ug/L 5.0 5 09/24/10 19:56 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 5 09124110 19:56 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 5 09/24/10 19:56 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 5 09/24/10 19:56 75-71-8 1,1-Dichloroethane ND ug/L 5.0 5 09124/10 19:56 75-34-3 1,2-Dichloroethane ND ug/L 5.0 5 09/24/10 19:56 107-06-2 1,1-Dichloroethene ND ug/L 5.0 5 09/24110 19:56 75-35-4 cis-1,2-Dichloroethene 5.2 ug/L 5.0 5 09/24/10 19:56 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 5 09/24/10 19:56 156-60-5 1,2-Dichloropropane ND ugIL 5.0 5 09/24/10 19:56 78-87-5 1,3-Dichloropropane ND ug/L 5.0 5 09/24110 19:56 142-28-9 2,2-Dichloropropane ND ug/L 5.0 5 09124/10 19:56 594-20-7 I,I-Dichloropropene NID ug/L 5.0 5 09/24110 19:56 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 5 09/24110 19:56 10061-01-5 trans-1,3-Dichloropropene ND ug/L 5.0 5 09/24/10 19:56 10061-02-6 Diisopropyl ether ND ug/L 5.0 5 09/24/10 19:56 108-20-3 -1)ate: 10/04/2010 09:51 AM REPORT OF -LABORATORY ANALYSIS - Page 9 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc Pace Analytical Services, Inc. Pace Analytical Services, Inc. eAnal 2225 Riverside Dr. 9800 KinceyAve. Suite 100 wwwmpa Gom Asheville, NC 28804 Huntersville, Nt 28078 ��acl . (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Sample: RW-6 Parameters Lab ID: 9278187004 Collected: 09/22/10 12:37 Results Units Report Limit DF Received: 09/22110 16:22 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 5.0 5 09/24/10 19:56 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 5 09/24/10 19:56 87-68-3 2-Hexanone ND ug/L 25.0 5 09/24/10 19:56 591-78-6 p-Isopropyltoluene ND ug/L 5.0 5 09/24/10 19:56 99-87-6 Methylene Chloride ND ug/L 10.0 5 09/24/10 19:56 75-09-2 4-Methyl-2-pentanone (MIBK) ND ugiL 25.0 5 09/24/10 19:56 108-10-1 Methyl-tert-butyl ether ND ug/L 5.0 5 09/24110 19:56 1634-04-4 Naphthalene ND ug/L 5.0 5 09/24/10 19:56 91-20-3 Styrene ND ug/L 5.0 5 09/24/10 19:66 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 5 09/24/10 19:66 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 09/24/10 19:56 79-34-5 Tetrachloroethene 29.0 ug/L 5.0 5 09/24/10 19:56 127-18-4 Toluene ND ug/L 5.0 5 09/24/10 19:56 108-88-3 1,2,3-Trichlorobenzene ND ug[L 5.0 5 09/24/10 19:56 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 5 09/24/1.0 19:56 120-82-1 1,1,1-Trichloroethane 6.2 ug/L 5.0 5 09/24/10 19:56 71-55-6 1,1,2-Trichloroethane ND ug/L 6.0 5 09/24/10 19:56 79-00-5 Trichloroethene 339 ug/L 5.0 5 09/24/10 19:56 79-01-6 Trichlorofluoromethahe ND ug/L 5.0 5 09/24110 19:56 75-69-4 1,2,3-Trichloropropeine ND ug/L 5.0 5 09/24/10 19:56 96-18-4 Vinyl acetate ND ug/L 10.0 5 09/24/10 19:56 108-05-4 Vinyl chloride ND ug/L 5.0 5- 09/24110 19:56 75-01-4 m&p-Xylene ND ug/L 10.0 5 09/24/10 19:56 179601-23-1 o-Xylene ND ug/L 5.0 5 09/24/10 19:56 95-47-6 4-Bromofluorobenzene (S) 101 % 70-130 5 09/24/10 19:56 460-00-4 Dibromofluoromethane (S) 115 % 70-136 5 09/24/10 19:56 1868-53-7 1,2-Dichloroethane-d4 (S) 122 % 70-130 5 09124/10 19:56. 17060-07-0 Tbluene-d8 (S) 93 % 70-130 5 09/24/10 19:56 2037-26-5 2320B Alkalinity Analytical Method: SM 21320B Alkalinity, Total as CaCO3 35.0 mg/L 5.0 1 09124/10 16:21 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5.0 1 09/29/10 09:11 14808-79-8 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 2.8 mg/L 0.10 1 09/23/10 28:02 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 6.2 mg/L 5.0 1 09/29/10 11:09 16887-00-6 Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. %o ACC,' Page10of25 a Aiiaijdical" 'Ce"apacelak.com Project: Pace Project No. Sample: RW-7 TEC-Fairview Pilot Test 9278187 Parameters Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID: 9278187005 Collected: 09/2211013:31 Received: 09/2211016:22 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 1440 ug/L 500 1 09123110 11:00 09/29/10 23:30 7440-38-2 Cadmium ND ug/L 100 1 09/23/10 11:00 09129/10 23:30 7440-43-9 D3 Chromium .2860 ug/L 500 1 09/23/10 11:00 09/29110 23:30 7440-47-3 Copper ND ug/L 500 1 09/23/10 11:00 09/29/10 23:30 7440-50-8 D3 Lead 626 ug/L 506 1 09/23110 11:00 09/29/10 23:30 7439-92-1 Zinc ND ug/L 1000 1 09/23110 11:00 09129/10 23:30 7440-66-6 D3 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 'Mercury 3.2 ug/L 0.20 1 09/28110 09:26 09/28/10 11:13 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 500000 20000 09/24110 16:55 67-64-1 D3 Benzene ND ug/L 20000 20000 09/24/10 16:55 71-43-2 Bromobenzene ND ug/L 20000 20000 09/24/10 16:55 108-86-1 Bromochloromethane ND ug/L 20000 20000 09/24/10 16:65 74-97-5 Bromodichloromethane ND ug/L 20000 20000 09124/10 16:55 75-27-4 '3romoform ND ug/L 20000 20000 09/24/10 16:55 16-25-2 3romomethane ND ug/L 40000 200110 09/24/10 16:55 74-83-9 2-Butanone (MEK) ND ug/L 100000 20000 09/24/10 16:55 78-93-3 Carbon tetrachloride ND ug/L 20000 20000 09/24/10 16:55 56-23-5 Chlorobenzene ND ug/L 20000 20000 09/24/10 16:55 108-90-7 Chloroethane ND ug/L 20000 20000 09/24/10 16:55 -75-00-3 Chloroform ND ug/L 20000 20000 09/24/10 16:55 67-66-3 Chlor6methane ND ug/L 20000 20000 09/24/10 16:55 74-87-3 2-Chlorotoluene ND ug/L 20000 20000 09/24110 16:55 95-49-8 4-C,hlorotoluene ND ug/L 20000 20000 09/24110 16:55 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 100000 20000 09/24/10 16:55 96-12-8 Dibromochloromethane ND ug/L 20000 20000 09/24/10 16:55 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 20000 20000 09124/10 16:55 106-93-4 Dibromomethane ND ug/L 20000 20000 09/24/10 16:55 74-95-3 1,2-Dichlorobenzene ND ug/L 20000 20000 09/24110 16:55 95-50-1 1,3-Dichlorobenzene ND ug/L 20000 20000 09/24/10 16:55 541-73-1 1,4-Dichlorobenzene ND ug/L 20000 20000 09/24/10 16:55 106-46-7 Dichlorodifluoromethane ND ug/L 20000 20000 09/24/10 16:55 75-71-8 1,1-Dichloroethane ND ug/L 20000 20000 09/24/10 16:55 75-34-3- 1,2-Dichloroethane ND ug/L 20000 20000 .09/24/10 16:55 107-06-2 1,1-Dichloroethene ND ug/L 20000 20000 09/24/10 16:55 75-35-4 cis-1,2-Dichloroethene ND ug/L 20000 20000 09/24/10 16:55 156-69-2 trans-1,2-Dichloroethene ND ug/L 20000 20000 09124/10 16:55 156-60-5 1,2-Dichloropropane ND ug/L 20000 20000 09/24110 16:55 78-87-5 1,3-Dichloropropane ND ug/L 20000 20000 09/24110 16:55 142-28-9 2,2-Dichloropropane ND ug/L 20000 20000 09/24/10 16:55 594-20-7 1,1-Dichloropropene ND ug/L 20000 20000 09/24/10 16:55 563-58-6 cis-1,3-Dichloropropene ND ug/L 20000 20000 09/24/1'0 16:55 10061-01-5 trans-1,3-Dichloropropene -ND ug/L 20000 20000 09/24110 16:55 10061-02-6 Dilsopropyl ether ND ug/L 20000 20000 09/24110 16:5.5 108-20-3 J)ate: 10/0412010 09:51 AM REPORT OF LABORATORY ANALYSIS Page 11 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Icca, Race Analytical Services, Inc. Pace Analytical Services, Inc. eAnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)?54-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Sample: RW-7 Lab ID: 9278187005 Collected: 09/22/10 13:31 Received: 09/22/10 16:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed . CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 20000 20000 09/24/10 16:55 100-41-4 Hexachloro-1,3-butadiene ND ug[L 20000 20000 09/24/10 16:65 87-68-3 2-Hexanone ND ug[L 100000 20000 09/24/10 16:55 591-78-6 p-Isopropyltoluene ND ug/L 20000 20000 09/24/10 16:55 99-87-6 Methylene Chloride ND ug[L 40000 20000 09/24/10 16:55 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 100000 20000 09/24/10 16:55 108-10-1 Methyl-tert-butyl ether ND ug/L 20000 20000 09/24110 16:55 1634-04-4 Naphthalene ND ug/L 20000 20000 09/24/10 16:55 91-20-3 Styrene ND ug/L 20000 20000 09/24/10 16:55 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 20000 20000 09124/10 16:55 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 20000 20000 09/24/10 16:55 79-34-5 Tetrachloroethene ND ug/L 20000 20000 09/24/10 16:55 127-18-4 Toluene ND ug/L 20000 20000 09/24/10 16:55 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20000 20000 09/24/10 16:55 87-61-6 1,2,4-T(ichlorobenzene ND ug/L 20000 20000 09/24/10 16:55 120-82-1 1,1,1-Tr'ichloroethane ND ug/L 20000 20000 09/24110 16:55 71-55-6 1,1,2-Trichloroethane ND ug/L 20000 20000 09/24110 16:55 79-00-5 Trichloroethene ND ug/L 20000 20000 09/24/10 16:55 79-01-6 Trichlorofluoromethane ND ug/L 20000 20000 09124/10 16:55 75-69-4 1,2,3-Trichloropropane ND ug/L 20000 20000 09/24110 16:55 96-18-4 Vinyl acetate ND ug/L 40000 20000 09/24/10 16:55 108-05-4 chloride ND ug/L 20000 20000 09/24/10 16:55 75-01-4 -Vinyl M&P-xylene ND ug/L 40000 20000 09/24/10 16:55 179601-23-1 o-Xylene ND ug/L 20000 20000 09/24/10 16:55 95-47-6 4-Bromofluorobenzene (S) 96 % 70-130 20000 09124/10 16:55 460-00-4 Dibromofluoromethane (S) 117 % 70-130 20000 09/24110 16:55 1868-53�7 1,2-Dichloroethane-d4 (S) 124 % 70-130 20000 09/24110 16:55 17060-07-0 Tbluene-d8 (S) 99 % 70-130 20000 09/24110 16:55 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 259 mg/L 5.0 1 09/24110 16:29 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 25000 5000 09/29/10 13:46 14808-79-8 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/L 1000 10000 09/23/10 23:07 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 10000 2000 09/29/10 11:11 16887-00-6 Date: 10/0412010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. D3 Page 12 of 25 QD Pace Analytical Services, Inc. Pace Analytical Services, Inc. 1�2ceAnalyfical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 wwwpacelabsxom Asheville, N.C.28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Sample: Trip Blank Lab LabID: 9278187006 Collected: 09/22/1000:00 Received: 09/22/1016:22 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone NID ug/L 25.0 1 09124/10 12:14 67-64-1 Benzene ND ug/L 1.0 1 09/24/10 12:14 71-43-2 Bromobenzene NID ug/L 1.0 1 09/24/10 12:14 108-86-1 Bromochloromethane NID ug/L, 1.0 1 09/24/10 12:14 74-97-5 Bromodichloromethane ND ug/L 1.0 1 09/24110 12:14 75-27-4 Bromoform NID ug/L 1.0 1 09/24110 12:14 75-25-2 Bromomethane ND ug/L 2.0 1 09/24/10 12:14 74-83-9 2-Butanone (MEK) NID ug/L 5.0 1 09/24/10 12:14 78-93-3 Carbon tetrachloride NID ug/L 1.0 1 09/24/10 12:14 56-23-5 Chlorobenzene ND ug/L 1.0 1 09124/10 12:14 108-90-7 Chloroethane NID ug/L 1.0 1 09/24/10 12:14 75-00-3 Chloroform ND ug/L 1.0 1 09124/10 12:14 67-66-3 Chloromethane NID ug/L 1.0 1 09/24/10 12:14 74-87-3 2-Chlorotoluene NID ug/L 1.0 1 09124/10 12:14 95-49-8 4-Chlorotoluene NID ug/L 1.0 1 09/24/10 12:14 106-43-4 1,2-Dibromo-3-chloropropane NID ug/L 5.0 1 09/24/10 12:14 96-12-8 Dibromochloromethane ND ug/L 1.0 1 09/24110 12:14 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 09124/10 12:14 106-93-4 Dibromomethane NID ug/L 1.0 1 09/24/10 12:14 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 09/24/10 12:14 95-50-1 1,3-Dichlorobenzene NID ug/L 1.0 1 09/24/10 12:14 641-73-1 1,4-Dichlorobenzene ND ug/L 1.0- 1 09/24/10 12:14 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 09/24/10 12:14 75-71-8 1,1-Dichloroethane ND ig/L 1.0 1 06124/10 12:14 75-34-3 .1,2-Dichloroethane ND ug/L 1.0 1 09/24/10 12:14 107-06-2 1,1-Dichloroethene NID ug/L 1.0 1 .09/24110 12:14 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 09/24110 12:14 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 09/24110 12:14 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 09/24/10 12:14 78-87-5 1,3-Dichloropropane NID ug/L 1.0 1 09/24/10 12:14 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 09/24ilO 12:14 594-20-7 1,1-Dichloropropene ND ug/L 1.D 1 09124/10 12:14 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 09124110 12:14 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 09/24/10 12:14 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 09/24/10 12:14 108-20-3 Ethylbenzene ND ug/L 1.0 1 09/24/10 12:14 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 09/24/10 12:14 87-68-3 2-Hexanone ND ug/L 5.0 1 09124/10 12:14 591-78-6 p-Isopropyltoluene NID ug/L 1.0 1 09124/10 12:14 99-87-6 Methylene Chloride NID ug/L 2.0 1 09124110 12:14 75-09-2 4-Methyl-2-pentanone (MIBK). NID ug/L 5.0 1 09124/10 12:14 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 . 1 09/24/10 12:14 1634-04-4 Naphthalene NID ug/L 1.0 1 09/24/10 12:14 91-20-3 Styrene NID ug1L 1.0 1 09/24/10 12:14 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 09124110 12:14 630-20-6 1,1,2,2-Tetrachloroethane NID ug/L 1.0 - 1 09/24/10 12:14 79-34-5 Tetrachloroethene NID ug/L 1.0 1 09124/10 12:14 127-18-4 ,---,,Date: 10104/2010 09:51 AM REPORT OF LABORATORY ANALYSIS Page 13 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ceAnalWical ww.pacelabsxom ac, Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Sample: Trip Blank Lab - LablD: 9278187006 Collected: 09/2M0 00:00 Received: 09/22/10 16:22 Matrix: Water Parameters Results I Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level AnalyfiGal Method: EPA 8260 Toluene ND ug/L 1.0 1 09/24110 12:14 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 09124/10 12:14 87-61-6 1,2,4-Tdchlorobenzene ND ug/L 1.0 1 09/24/10 12:14 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 09/24/10 12:14 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 09/24/10 12:114 79-00-5 Trichloroethene ND ug/L 1.6 1 09124/10 12:14 79-01-6 Tdchlorofluoromethane ND ug/L 1.0 1 09/24/10 12:14 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 09/24/10 12:14 96-18-4 Vinyl acetate ND ug/L 2.0 1 09/24/10 12:14 108-05-4 Vinyl chloride ND ug/L 1.0 1 09124/10 12:14 75-01-4 m&p-Xylene ND ug/L 2.0 1 09124/10*12:14 179601-23-1 o-Xylene ND ug/L 1.0 1 09/24110 12:14 95-47-6 4-Bromofluorobenzene (S) 106 % 70-130 1 09/24110 12:14 460-00-4 Dibrornofluorornethane (S) 118 % 70-130 1 09/24/10 12:14 1868-53-7 1,2-DiGhloroethane-d4 (S) 120 % 70-130 1 09/24/10 12:14 17060-07-0 Tbluene-d8 (S) 102 % 70-130 1 09/24/10 12:14 2037-26-5 Date: 10104/2010 09:51 AM REPORT OF LABORATORY ANALYSIS Page 14 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Acca, aceAnalytical QD www.pacelabs.com Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MPRP/7114 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: .9278187001, 9278187002, 9278187003, 9278187004, 9278187005 METHOD BLANK: 501469 Matrix: Water Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 Blank Reporting Parameter Units Result Limit Analyzed Arsenic ug/L ND 5.0 09/29/10 21:57 Cadmium ug/L ND 1.0 09/29/10 21:57 Chromium ug/L ND 5.0 09/29/10 21:57 Copper ug/L ND 5.0 09/29/10 21:57 Lead ug/L ND 5.0 09129/10 21:57 Zinc ug/L ND 10.0' 09/29110 21:57 LABORATORY CONTROL SAMPLE: 501470 Parameter Units Arsenic ug/L ' �"admium ug/L chromium ug/L Copper ug/L Lead ug/L Zinc ug/L MATRIX SPIKE SAMPLE: 501471 Parameter Units Arsenic ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Zinc ug/L SAMPLE DUPLICATE: 501472 Parameter Arsenic Cadmium Chromium Copper Lead Zinc 0ate: 10/04/2010 09:51 AM Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 471 94 80-120 500 473 96 80-120 500 482 96 80-120 500 478 96 80-120 500 476 95 80-120 500 .486 97 80-12 0 9278160011 Spike ]VIS IVIS % Rec Result Conc. Result % Rec Limits ND 500 478 96 75-125 ND 500 477 95 75-125 0.83J 500 482 96 75-125 ND 500 485 97 75-125 ND 500 479 96 75-125 7.5J 500 495 97 75-125 9278160012 Dup Units Result Result ug/L ND ND ug/L ND ND ug/L 0.54J 2AJ ug/L ND ND ug/L ND ND ug/L 6.8J 6.3J RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 15 of 25 QD Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 1.��IaoeAnaljdical Asheville, NC 2880'4 Huntersville, NC 28078 www.pace)abs.corn QUALITY CONTROL DATA Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 (828)254-7176 (704)875-9092 QC Batch: MERP/3033 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 METHOD BLANK: 503510 Matrix: Water Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20. 09128/10 10:26 LABORATORY CONTROL SAMPLE: 503511 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.4 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 603512 503513 IVIS MSD 9277984001 Spike Spike IVIS MSD IVIS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 1.5 1.4 60 57 75-125 4 M1 MATRIX SPIKE-& MATRIX SPIKE DUPLICATE: 503514 503515 IVIS MSD 9278038004 Spike Spike IVIS MSD IVIS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPID Qua[ Mercury ug/L ND 2.5 2.5 1.6 .08J 62 3 75-125 Mi Date: 10104/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. a AnaIXical" 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Ice wwwpacelab&coin Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 QC Batch: MSW12366 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005,9278187006 METHOD BLANK: 602507 Matrix: Water Associated Lab Samples; 9278187001,9278187002,9278187003,9278187004,9278187005,9278187006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/24/10 11:48 1,1,1-Trichloroethane ug/L ND 1.0 09/24/10 11:48 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09124/10 11:48 1,1,2-Trichloroethane ug/L ND 1.0 09/24/10 11:48 M-Dichloroethane ug/L ND 1.0 09/24/10 11:48 M-Dichloroethene ug/L ND 1.0 09/24/10 11:48 1,1-Dichloropropene ug/L ND 1.0 09/24/10 11:48 1,2,3-Trichlorobenzene ug/L ND 1.0 09/24/10 11:48 1,2,3-T(ichloropropane ug/L ND 1.0 09124/10 11:48 1,2,4-Trichlorobenzene ug/L ND 1.0 09/24/10 11:48 1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/24/10 11:48 1,2-Dibromoethane (EDB) ug/L ND 1.0 09/24/10 11:48 1,2-Dichlorobenzene ug/L ND 1.0 09/24/10 11:48 �1,2-Dichloroethane ug/L ND 1.0 09124/10 11:48 -'1,2-Dichloropropane ug/L ND 1.0 09/24/10 11:48 1,3-Dichlorobenzene ug/L ND 1.0 09/24110 11:48 1,3-Dichloropropane ug/L ND 1.0 09/24/10 11:48 1,4--Dichlorobenzene ug/L NO 1.0 09/24110 11:48 2,2-Dichloropropane ug/L ND 1.0 09/24/10 11:48 2-Butanone (MEK) ug/L NO 5.0 09/24/10 11:48 2-Chlorotoluene ug/L ND 1.0" 09/24110 11:48 2-Hexanone ug/L NO 5.0 09/24/10 11:48 4-Chlorotoluene ug/L ND 1.0 09/24/10 11:48 4-Methyl-2-pentanone (MIBK) ug/L NO 5.0 09/24110 11:48 Acetone ug/L ND 25.0 09/24/10 11:48 Benzene ug/L NO 1.0 09/24/10 11:48 Bromobenzene ug/L ND 1.0 09/24/10 11:48 Bromochloromethane ug/L ND 1.0 09124/10 11:48 Bromodichloromethane ug/L ND 1.0 09/24/10 11:48 Bromoform' ug/L ND 1.0 09/24/10 11:48 Bromomethane ug/L ND 2.0 09/24/10 11:48 Carbon tetrachloride ug/L ND 1.0 09/24/10 11:48 Chlorobenzene ud/L NO 1.0 09/24/10 11:48 Chloroethane ug/L ND 1.0 09/24/10 11:48 Chloroform ug/L ND 1.0 09/24/10 11:48 Chloromethane ugtL NO 1.0 09/24/10 11:48 cis-1,2-Dichloroethene ug/L ND 1.0 09/24/10 11:48 cis-1,3-Dichloropropene dg/L ND 1.0 09/24/10 11 *48 Dibromochloromethane ug/L ND 1.0 09/24110 11:48 Dibromomethane ug/L ND 1.0 09/24/10 11:48 Dichlorodifluoromethane ug/L ND 1.0 09/24110 11:48 Diisopropyl ether ug/L ND 1.0 09/24/10 11:48 Ethylbenzene ug/L ND 1.0 09/24/10 11:48 ,,___)Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.: Page 17 of 25 acieAnalyfical wmpacefabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NG 28804 (828)254-7176 QUALITY CONTROL DATA Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 METHOD BLANK: 502507 Matrix: Water Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005,9278187006 Blank Reporting Parameter Units Result Limit Analyzed Qualiflers Hexachloro-1,3-butadiene ug/L ND 1.0 09/24/10 11:48 m&p-Xylene ug/L ND 2.0 09/24/10 11:48 Methyl-tert-butyl ether ug/L ND 1.0 09/24/10 11:48 Methylene Chloride ug/L ND 2.0 09/24110 11:48 Naphthalene ug/L ND 1.0 09/24/10 11:48 o-Xylene ug/L ND 1.0 09/24/10 11:48 p-Isopropyltoluene ug/L ND 1.0 09/24/10 11:48 Styrene ug/L ND 1.0 09/24/10 11:48 Tetrachloroethene ug/L ND 1.0 09/24110 11:48 Toluene ug/L ND 1.0 09124110 11:48 trans-1,2-Dichloroethene ug/L ND 1.0 09/24/10 11:48 trans-1,3-Dichloropropene ug/L ND 1.0 09/24110 11:48 Trichloroethene ug/L ND 1.0 09/24/10 11:48 Trichlorofluoromethane ug/L NO 1.0 09/24/10 11:48 Vinyl acetate ug/L ND 2.0 09/24/10 11:48 Vinyl chloride ug/L NO 1.0 09/24/10 11:48 1,2-Dichloroethane-d4 (S) % 120 70-130 09/24/10 11:48 4-Bromofluorobenzene (S) % 103 70-130 09124/10 11:48 Dibromofluoromethane (S) % 118 70-130 09/24/10 11:48 Tbluene-d8 (S) % 101 70-130 09/24/10 11:48 LABORATORY CONTROL SAMPLE: Parameter 502508 Units Spike. Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 48.1 96 70-130 1,1,1-Trichloroethane ug/L 50 47.7 95 70-130 1,1,2,2-Tetrachloroethane ug/L 50 45.5 91 70-130 1,1,2-Trichloroethane ug/L 50 49.7 99 70-130 1,1-Dichloroethane ug/L 50 50.2 100 ' 70�1 30 1,1-Dichloroethene ug/L 50 46.7 93 70-132 1,1-Dichloropropene ug/L 50 42.8 86 70-130 1,2,3-Trichlorobenzene ug/L 50 44.3 89 70-135 1,2,3-T(ichloropropane ug/L 50 43.8 88 70-130 1,2,4-Trichlorobenzene ug/L 50 48. 5 97 70�134 1,2-Dibromo-3-chloropropane ug/L 50 47.8 96 70-130 1,2-Dibromoethane (EDB) ug/L 50 46.2 92 70-130 1,2-Dichlorobenzene ug/L 50 47.8 96 70-130 1,2-Dichloroethane ug/L 50 54.0 106 70-130 1,2-Dichloropropane ug/L 50 44.4 89 70-130 1,3-Dichlorobenzene ug/L 50 47.2 94 70-130 1,3-Dichloropropane ug/L 50 43.5 87 70-130 1,4-Dichlorobenzene ug/L 50 46.4 93 70-130 2,2-Dichloropropane ug/L 50 51.6 103 58-145 2-Butanone (MEK) ug/L 100 102 102 70-145 2-Chlorotoluene ug/L 50 47.7 95 70-130 Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, Inc.. Acco, Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Page 18 of 25 oeAnaljftal wwpacelabs.com Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 LABORATORY CONTROL SAMPLE: 502508 Parameter Units Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2-Hexanone ug/L 100 102 102 70-144 4-Chlorotoluene ug/L 50 48.2 96 70-130 4-Methyl-2-pentanone (MlBK) ug/L 100 102 102 70-140 Acetone ug/L 100 104 104 50-175 Benzene ug/L 50 45.6 91 70-130 Bromobenzene ug/L 50 48.2 96 70-130 Bromochloromethane, ug/L 50 46.7 93 70-130 Bromodichloromethane ug/L 50 46.4 93 70-130 Bromoform ug/L 50 49.6 99 70-130 Bromomethane ug/L 60 43.1 86 54-130 Carbon tetrachloride ug/L 50 56.3 113 70-132 Chlorobenzene ug/L 50 45.1 90 70-130 Chloroethane ug/L 50 51.4 103 64-134 Chloroform ug/L 50 53.1 106 70-130 Chloromethane ug/L 50 42.6 85 64-130 cis-1,2-Dichloroethene ug[L 50 48.2 96 70-131 cis-1,3-Dichloropropene ug/L 50 46.9 94 70-130 Dibromochloromethane ug/L 50 46.1 92 70-130 Dibromomethane ug/L 50 48.2 96 70-131 bichlorodifluoromethane ug/L 50 39.4 79 56-130 Diisopropyl ether ug/L 50 46.0 92 70-130 Ethylbenzene ug/L 50 46.6 93 70-130 Hexachloro-1,3-butadiene ug/L 50 43.7 87 70-130 m&p-Xyiene ug/L 100 97.1 97 70-130 Methyl-tert-butyl ether ug/L 50 47.0 94 70-130 Methylene Chloride ug/L 50 51.3 103 63-130 Naphthalene ug/L 50 45.8 92 70-138 o-Xylene ug/L 50 51.0 102 70-130 p-Isopropyltoluene ug/L 50 48.6 97 70-130 Styrene ug/L 50 49.1 98 70-130 Tetrachloroethene ug/L 50 45.4 91 70-130 Toluene ug/L 50 47.4 95 70-130 trans-1,2-Dichloroethene ug/L 50 47.9 96 70-130 trans-1,3-Dichloropropene ug/L 50 49.2 98 70-132 Trichloroethene ug/L 50 48.0 96 70-130 Trichlorofluoromethane ug/L 50 47.5 95 62-133 Vinyl acetate ug/L 100 55.3 55 66-157 LO Vinyl chloride ug/L 50 45.2 90 69-130 1,2-Dichloroethane-d4 (S) % 106 70-130 4-Bromofluorobenzene (S) % 99 70-130 Dibromofluoromethane (S) % 104 70-130 Toluene-d8 (S) % 102 70-130 (704)875-9092 I I I Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS Page 19 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 'o lacleAnaljdical WWW.Pacelablcom Project: TEC-FaIrview Pilot Test Pace Project No.: 9278187 Pac a Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 502509 502510 IVIS MSD 9278216002 Spike Spike IVIS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD I,I-Dichloroethene ug/L ND 50 50 60.4 60.8 121 122 70-166 1 Benzene ug/L ND 50 50 52.8 54.1 106 108 70-148 2 Chlorobenzene ug/L ND 50 50 53.1 55.6 106 Ill 70-146 5 Toluene ug/L ND 50 50 55.0 54.7 110 109 70-155 0 Trichloroethene ug/L ND 50 50 53.1 52.9 106 106 69-151 0 1,2-Dichloroethane-*d4 (S) % 118 119 70-130 4-Bromofluorobenzene (S) % 97 103 70-130 Dibromofluoromethane (S) % Ill 113 70-130 Toluene-d8 (S) % 96 96 70-130 Date: 10/0412010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Page 20 of 25 aceAnalytical www.pacelabs.com Project: , TEC-Fairview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WET/13874 Analysis Method: SM 2320B QC Batch Method: S.M 2320B Analysis Description: 2320BAlkalinity Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 METHOD BLANK: 502354 Matrix: Water Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 Blank Reporting Parameter Units Result Limit Analyzed Alkalinity, Total as CaCO3 mg/L ND 5.0 09/24/10 16:07 LABORATORY CONTROL SAMPLE: 502355 Spike Parameter Units Conc. Alkalinity, Total as CaCO3 mg/L 50 SAMPLE DUPLICATE: 502356 9277829006 Parameter Units Result Alkalinity, Total as CaCO3 mg/L 396 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS LCS % Rec Result %Rec Limits Qualifiers 48.4 97 90-110 Dup Result RPD Qualifiers 397 0 SAMPLE DUPLICATE: 502357 -9277850002 Dup Parameter Units Result Result RPD Qualifiers Alkalinity, Total as CaCO3 mg/L 40.1 41.2 3 ,)ate: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 21 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 ��aaeM*ica( Asheville, NC 28804 Huntersville, NC 28078 www.pacelabs.com (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 QC Batch: WETA18224 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 9278187001, 9278187002, 9278187003, 9278187004, 9278187005 METHOD BLANK: 602863 Matrix: Water Associated Lab Samples: 9278187001, 9278�187002, 9278187003, 9278187004, 9278187005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mgIL ND 5.0 09128/10 14:36 LABORATORY CONTROL SAMPLE: 502864 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate mg/L 30 28.4 95 MATRIX SPIKE SAMPLE: 502865 9277802006 Spike MS IVIS % ReG Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mg/L ND 30 27.7 82 MATRIX SPIKE SAMPLE: 502867 9277864002 Spike - - MS MS Rec - Parameter Units Result 'Conc. Result % Rec Limits Qualifiers Sulfate mg/L 65.9 30 97.1. 104 SAMPLE DUPLICATE: 502866 9277864001 Dup -Parameter Units Result Result RPD Qualifiers Sulfate mg/L 76.2. 72.9 5 SAMPLE DUPLICATE: 502868 Parameter Sulfate Date: 10/0412010 09:51 AM 9277864003 Dup Units Result Result mg/L 66.5 65.6 RPD Qualifiers 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. lPn" Page 22 of 25 -a ceAna6dical" www.pacelabs.com Project: TEC-Fairview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)815-9092 QUALITY CONTROL DATA QC Batch: WETA/8223 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 METHOD BLANK: 502286 Matrix: Water Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.10 09123/10 22:51 LABORATORY CONTROL SAMPLE: 502287 Parameter Units Nitrogen, Nitrate mg/L MATRIX SPIKE SAMPLE: 502288 Parameter Units �Nitrogen, Nitrate mg/L SAMPLE DUPLICATE: 502289 Parameter Units Nitrogen, Nitrate - mg/L Date: 10/04/2010 09:51 AM Sp lke LCS Conc. Result 5 5.1 LCS % Rec % Rec Limits Qualifiers 102 90-110 9278187002 Spike. MS MS Result Conc. Result % Rec 2.9 5 7.9 101 9278187002 Dup Result Result RPD Qualifiers 2.9 2.9 0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. % Rec Limits Qualifiers 90-110 Page 23 of 25 Pace Analytical Services, Inc. 2225 Riverside Dr. aoeMaOcal Asheville, NC 28804 www.pacelabs.com (828)254-7176 QUALITY CONTROL DATA Project: TEC-Fai rview Pilot Test Pace Project No.: 9278187 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: WETA/8256 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4600 Chloride Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187005 METHOD BLANK: 504309 Matrix: Water Associated Lab Samples: 9278187001,9278187002,9278187003,9278187004,9278187006 Blank Repoffing Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 5.0 09/29/10 11:09 LABORATORY CONTROL SAMPLE: 504310 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 21.8 109 90-110 MATRIX SPIKE SAMPLE: 504318 9278187001 Spike IVIS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chloride mg/L ND 20 25.9 109 75-125 MATRIX SPIKE SAMPLE: 504320 9278187003 Spike IVIS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chloride mg/L ND 20 26.0 75-125 SAMPLE DUPLICATE: 504319 9278187002 Dup Parameter Units Result Result RPD Qualifiers Chloride mg/L ND ND SAMPLE DUPLICATE: 504321 9278187004 Dup Parameter Units Result Result RPD Qualifiers Chloride mg/L 5.2 ND Date: 10/04/2010 09:51 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 26 /55'ceAnayical- wwwpacelabs.00m QUALIFIERS Project: TEC-Falrview Pilot Test Pace Project No.: 9278187 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplic * ate) DUP -Sample Duplicate, RPD - Relative Percent Difference NC - Not Calculable. U - Indicates the compound was analyzed for, but not detected. N-Nitro'sodiphenylamine decomposes . and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non4arget analytes or other matrix interference. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Date: 10/0412010 09:51 AM REPORT OF LABORATORY ANALYSIS Page 25 of 25 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. ACCG� ' ace?!MY-Y�ql* CHAIN-OF-CUSTODY-1A,ndlytical. Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. ------------- Page: Of Section A Section B Section C 1365588 Required Client Information: Required Project Information: Invoice Information: Company: Report To: Attention: Sla Address: Copy To: Company Name: At) OWYA04 ` ' - " . R�qIJLATOR-�-'AdgkY-- a26,11V, &Y., asyo Address: %V� - F NPDES . rr,-`GROUND WATER F- DRINKING WATER r LIST I RCRA r OTHER Email o:: Purchase Order No.: Pace Quote %1-. ta �X. Alf- "22M M- Reference: -92W �.- P foj.ct Name: MC Vl%+T& Tpace Prol act IManager. Site Locattloril TA TE-, Project Requested Due Date/TAT-.,� Number: Pace Profile #: Rku4teid. Analpis�F ilte d (YIN) Section D Matrix Code co Required Client information M Ix E COLLECTED Preservatives 2;.. 5;:. Ddnking Water DW Water WT 0 8 z 0 1, a COMPOSITE START COMPOSITE ENDIGRAB �3 Lu z Product P _71 8 S olli'Solid SL 0 SAMPLE ID Oil OL Wip WP W w (A-Z, 0-9 Air AR w 0 w z 0 r- Sample IDS MUST BE UNIQUE Tlssue TS Other OT 0 L3 (L Vw w 0 01), 41: a. W IL 0 L) ID to 0! 0 C: :R ft7 9/ 0 IS z Z3 w a) E a) DATE LIME DATE I TIME u) U :) = =� Z: z z 0 af Project No./ Lab I.D. 1 W-,14r UJr yg ho 1133 V-74 (0 kxi I X VXx 2 WW- L40 - VST WT ca 3 "w- At Or VT JJ6 -9 14 4. t?T- 1'233 1 N . . . . . . . . 6 7 9 10 .L2 ADDITIONAL COMMENTS RELINQUISHED JBY 1AFFIL . IATION :.T!ME �ACCRP�T D YIAFFILIATION 'A DATE TIM E SAMPLE CONDITIONS MP AME- ORIGINAL PRINT Name of SAMPLER: &kh-ra SIGNATURE of SAMPLER: cc E Note: By signing this form you are accepting Pac4Ys NET 30 day payment terms and agreeing to late charges of 1.5% per mon .15K.ld Wthin 30 day.. F-ALL-Q-020rev.07, 007 AkeAnalyficaf' ,,Nhere Received: Client Name: A"m t' - Project # 727?Z 97 - 1:1 Huntersville Zr Asheville D Eden Courier: D Fed Ex D UPSE] USPS Valent 11 commercial El Pace Other Custody Seal on Cooler/Box Present: Dyes e-no Seals intact: El yes )Z no Packing Material: D Bubble Wrap dBubble Bags 0 None FlOther Thermometer Used: tZ�2 14-648-44 Type of Ice: t Blue None Temp Correction Factor: Add Sodiwa 1015 C Opfional Proj. Due Date: Proi. Name: 2-"mples on ice, cooling -process has begun Corrected Cooler Temp.: C Temp should be above freezing to 60C Mological Tissue is Frozen: Yes No Comments: Date and Initials of person "amiping contents 72, X —t�, Chain of Custody Present: -EfYZs DNo DWA 1 Chain of Custody Filled Out: eKes []No bNIA 2. Chain of Custody Relinquished: O'Yes DNo ON/A 3. Sampler Name & Signature on COC: 'Ye� EIN. EIN/A 4. Samples Arrived within Hold Ti me: 21'Y"es DNo 0 N/A 5. Short Hold Time Analysis (42hr): Z'Ye, EIN. 0 N/A 6. 11u; Rush Turn Around Time Requested: OYes PC ON/A 7. Sufficient Volume: J2� []No EIN/A 8. Correct Containers Used: -Pace Containers Used: eYes DNo Yes DNo ON/A ON/A 9. - ��,'ontalners Intact: VfYes []No ON/A 10. P91tered volume received for Dissolved tests. OYes DN'. Y//A 11. Sample Labels match COC: P<es []No ON/A -includes date/time/ID/Analysis Matrix: 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance With EP . A recommendation. exceptions: VOA, co1iform,T0C,0&G,W1-DR0 (water) P4'es []No 9'(es E]No DYes DNo EIN/A EIN/A 13. Initial when completed Samples checked for dechlorination: DYes DNo /A 14. Headspace in VOA Vials (>6mm): DYes 0. EIN/A 15. Trip Blank Present: Trip Blank Custody Seals Present 1 Pace Trip Blank Lot# (if purchased): 2 rYes ONo Xes ONo ON/A EIN/A 16. Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Date/Time: Comments/ Resolution: ---3CURF Review:1 JDate: SRF Review: I ffeZ 113ate: --'�'4ote: Whenever there is a disicrepancy affecting North Caroliin compliance samples, a copy ofthis form will be sent to the North Certification Office ( Le out of hold3 incorrect preservative, out of temp, incorrect containers) �0 F-ASV-CS-03-Rev.02 Pace Analytical Services, Inc. Pace Analytical Services, Inc. PaAnalytical" 2225 Riverside br. 9800 KinceyAve. Suite 100 lce www.pacdabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 October 15, 2010 Mr. Chris Gilbert Altamont Environmental 231 Haywood Street Asheville, NC 28801 RE: Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace P roject No.: 9279170 Dear Mr. Gilbert: Enclosed are the analytical results for sample(s) received by the laboratory on October 06, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were pe ' rformed -at our Pace Asheville laboratory and Organic testing was performed at -our Pace Huntersville laboratory. unless -otherwise-fo-o-tnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, e C2 11� Lorri Patton lorri.pafton@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. A �age I of 28 a oeAnalytical C' wmpacelaftcom Project: TEC - FAIRVIEW PILOT TEST 1016 Pace Project No.: 9279170 Charlotte Certification lDs 9800 KinceyAve. Ste.100, Huntersville, NC 28078 Louisiana/LELAP Certification * 04034 New Jersey Certification#: NC01 2 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pennsylvania Certification #: 68-00784 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS South Carolina Certification *: 99006001 South Carolina Drinking Water Cert. *: 99006003 Virginia Certification *: 00213 Connecticut Certification *: PH-01 04 Florida/NELAP Certification E87627 Kentucky UST Certification 84 Louisiana DHH Drinking Water# LA 100031 Pace Analytical Services, Inc. 980OKinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Drinking Water Certification *: 37712 Connecticut Certification #: PH-01 06 North Carolina Wastewater Certification *: 40 Florida/NELAP Certification #: E87648 Pennsylvania Certification #: 68-03578 Massachusetts Certification #: M-NC030 South Carolina Bioassay Certification *: 99030002 New Jersey CertifiGation #: NC01 I South Carolina Certification #: 99030001 North Carolina Bioassay Certification * 9 Virginia Certification *: 00072 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, - without the written consent of Pace Analytical Services, Inc.. Page 2 of 28 - a eAnalytical ww.pacelabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite too Huntersville, NC 28078 (704)875-9092 Sample: MW-39 WT LablD: 9279170001 Collected: 10/06/10 11:14 Received: 10/06/10 14:48 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6.010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 1 ' 0/07/10 12:30 10/10/10 02:51 7440-38-2 Cadmium 1.0 ug/L 1.0 1 10/07110 12:30 10/10/10 02:51 7440-43-9 Chromium 343 ug/L 6.0 1 10/07/10 12:30 10/10/10 02:51 7440-47-3 Copper 184 ug/L .5.0 1 10/07/10 12:30 10/1 011 0 0'2:51 7440-50-8 Lead 359 ug/L 5.0 1 1.0/07/10 12:210 10/10110 02:51 7439-92-1 Zinc 416 ug/L 10.0 1 10/07/10 12:30 10/10/10 02:51 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury 0.20 ug/L 0.20 1 10107/10 20:20 10/13/10 15:32 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25000 1000 10/13/10 01:09 67-64-1 Benzene ND ug/L 1000 1000 '10/13/10 01:09 71-43-2 Bromobenzene ND ug/L 1000 1000 10/13/10 01:09 108-86-1 Bromochloromethane NID ug/L 1000 1000 10/13/10 01:09 74-97-5 Bromodichloromethane ND ug/L 1000 1000 10/13/10 01:09 75-27-4 Bromoform ND ug/L 1000 1000 10/13/10 01:09 75-25-2 �Bromomethane ND ug/L 2000 1000 10/13110 01:09 74-83-9 2-Butanone (MEK) ND ug/L 5000 1000 10/13/10 01:09 78-93-3 Carbon tetrachloride ND ug/L 1000 1000 l Oil 3/10 01:09 56-23-5 Chlorobenzene ND ug/L 1000 1000 10113/10 01:09 108-90-7 Chloroethane ND ug/L- 1000 1000 10113/10 01 -bg 76-00--3 Chloroform ND ug/L 1000 1000 10/13/10 01:09 67-66-3 Chloromethane ND ug/L 1000 1000 10/13/10 01:09 74-87-3 2-Chlorotoluene ND ug/L 1000 1000 10113/10 01:09 95-49-8 4-Chlorotoluene ND ug/L 1000 1000 10113110 01:09 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 6000 1000 10/13/10 01:09 96-12-8 Dibromochloromethane ND ug/L 1000 1000 10/13/10 01:09 124-48-1 1,2-Dibromoethane (EDB) ND ug/L .1000 1000 10/13110 01:09 106-93-4 Dibromomethane ND ug/L 1000 1000 10/13/10 01:09 74-95-3 1,2-Dichlorobenzene ND ug/L 1000 1000 "10/13110 01:09 95-50-1 1,3-Dichlorobenzene NID ug/L 1000 1000 10/13110 01:09 541-73-1 1,4-Dichlorobenzene ND ug/L 1000 1000 10/13/10 01:09 106-46-7 Dichlorodifluoromethane ND ug/L 1000 1000 10/13/10 01:09 75-71-8 1,1-Dichloroethane ND ug/L 1000 1000 10/13/10 01:09 75-34-3 1,2-Dichloroethane ND ug/L 1000 1000 10/13/10 01:09 107-06-2 1,1-Dichloroethene Nb ug/L 1000 1000 10/13/10 01:09 75-35-4 cis-1,2-Dichloroethene ND ug/L 1000 1000 10/13110 01:09 156-59-2 trans-1,2-Dichloroethene ND ug/L 1000 1000 10113/10 01:09 156-60-5 1,2-Dichloropropane ND ug/L 1000 1000 10/13/10 01:09 78-87-5 1,3-Dichloropropane ND ug/L 1000 1000 10/13/10 01:09 142-28-9 2,2-Dichloropropane ND ug/L 1000 1000 10/13/10 01:09 594-20-7 I,I-Dichloropropene ND ug/L 1000 1000 10/13/10 01:09 563-68-6 c7is-1,3-Dichloropropene ND ug/L 1000 1000 10/13/10 01:09 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1000 1000 10113110 01:09 10061-02-6 Diisopropyl ether ND ug/L 1000 1000 10113/10 01:09 108-20-3 i)ate: 10/ 15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS Page 3 of 28 This report shall not be reproduced, except In full, mfithout the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. . a ceAnalytical 2225 Riverside Dr. 9800 KinceyAve. Suite 100 wNwpacefabscom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Sample: MW-39 WT LabID: 9279170001 Collected: 10/06/10 11:14 Received: 10/06/10 14:48 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 1000 1000 10113/10 01:09 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1000 1000 1.0/13/10 01:09 87-68-3 2-Hexanone ND ug/L 5000 1000 10/13/10 01:09 591-78-6 p-Isopropyltoluene ND ug/L 1000 1000 10/13/10 01:09 99-87-6 Methylene Chloride 3470 ug/L 2000 1000 10/13/10 01:09 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5000 1000 10/13110 01:09 108-10-1 Methyl-tert-butyl ether ND ug/L 1000 1000 10113/10 01:09 1634-04-4 Naphthalene ND ug/L 1000 1000 10/13110 01:09 91-20-3 Styrene ND ug[L 1000 1000 10/13/10 01:09 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1000 1000 10/13/10 01:09 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1000 1000 10/13/10 01:09 79-34-5 Tetrachloroethene 1760-ug/L 1000 1000 10/13/10.01:09 127-18-4 Toluene 3670 ug/L* 1000 1000 10/13/10 01:09 108-88-3 1,2,3-T(ichlorobenzene ND ug/L 1000 1000 10/13110 01:09 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1000 1000 10/13/10 01:09 120-82-1 1,1,1-Trichlo*roethane 7700 ug/L 1000 1000 10113/10 01:09 71-55-6 1,1,2-Tr'ichloroethane ND ug/L 1000 1000 10/13110 01:09 79-00-5 Trichloroethene 116000 ug/L 1000 1000 10/13/10 01:09 79-01-6 Trichlorofluoromethane ND ug/L 1000 1000 10/13/10 01:09 75-69-4 1,2,3-Tr'ichloropropane ND ug/L 1000 1000 10/13110 01:09 96-18-4 Vinyl acetate ND ug[L 2000 1000 10/13/10 01:09 108-05-4 Vinyl chloride ND ug/L 1000� 1,000 10/13/1001:09 76-01-4 m&p-Xylene ND ug/L 2000 1000 10113110 01:09 179601-23-1 o-Xylene ND ug/L 1000 1000 10113/10 01:09 95-47 - 6 4-Bromofluorobenzene (S) 90 % 70-130 1000 10/13110 01:09 460-00-4 Dibromofluoromethane (S) 93 % 70-130 1000 10/13/10 01:09 1868-53-7 1,2-Dichloroethane-d4 (S) 91 % 70-130 1000 10/13110 01:09 17060-07-0 Toluene -dB (S) 86 % 70-130 1000 10/13/10 01:09 2037-26-5 2320B Alkalinity Analytical Method: SM 232bB Alkalinity, Total as CaCO3 17.8 mg/L 5.0 1 10/11/10 12:46 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 6.0 1 10/12/10 16:03 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 0.14 mg/L 0.10 1 10/06/10 17:28 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 10/12/10 12:44 16887-00-6 Date: 10/1512010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, , without the written consent of Pace Analytical Services, Inc.. Acca" A Page 4 of 28 Pace Analytical Services, Inc. Pace Analytical Services, Inc. /5a'ceAnalyficalcD 2225 Riverside Dr. 9800 KinceyAve. Suite 100 wwwpaWabs.- Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Sample: MW-40 WT Leib ID: 9279170002 Collected: 10/06/10 10:13 Received: 10/06/10 14:48 Matrix: Water Parameters 6010 MET ICP Arsenic Cadmium Chromium Copper Lead Zinc 7470 Mercury Mercury 8260 MSV Low Level Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform �Bromomethane 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chlorobth-ane Chloroform Chloromethane 2-Chlorotoluene .4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichlaroethene 1,2-Dichlo ropropahe 1,3-Dichloroptopane 2,2-Dichloropro pane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Date: 10/1512010 02:33 PM Results Units Report Limit DF Prepared Analyzed CAS No. Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 5.0 1 10107/10 12:30 10/10/10 02:58 7440-38-2 ND ug/L 1.0 1 10/07/10 12:30 10/10110 02:58 7440-43-9 89.3 ug/L 5.0 1 10/07/10 12:30 10/10/10 02:58 7440-47-3 32.5 ug/L .5.0 1 10/07/10 12:30 10/10110 02:58 7440-50-8 5.1 ug/L 5.0 1 10/07/10 12:30 10110/10 02:58 7439-92-1 41.6 ug/L 10.0 1 10107/10 12:30 10/10/10 02:58 7440-66-6 Analyfical Method: EPA 7470 Preparation Method: EPA 7470 ND ug/L 0.20 1 10107110 20:20 10/13/10 15:35 7439-97-6 Analytical Method: EPA 8260 ND ug/L 25.0 1 10/13/10 01:35 67-64-1 ND ug/L 1.0 1 10/13/10 01:35 71-43-2 ND ug/L 1.0 1 10/13/10 01:35 108-86-1 NO ug/L 1.0 1 10/13/10 01:35 74-97-5 ND ugil- 1.0 1 10/13110 01:35 75-27-4 ND ug/L 1.0 1 10/13110 01:35 75-25-2 ND ug/L 2.0 1 10/13110 01:35 74-83-9 ND ug/L 5.0 1 10113/10 01:35 78-93-3 ND ug/L 1.0 1 10/13/10 01:35 56-23-5 ND ug/L 1.0 1 10/13/10 01:35 108-90-7 ND ug/L 1.0 1 -10/13/10 01:35 -75-00-3 2.9 ug/L 1.0 1 10/13/10 01:35 67-66-3 ND ug/L ..1.0 1 10/13/10 01:35 74-87-3 ND ug/L 1.0 1 10/13/10 01:35 95-49-8 ND ug/L 1.0 1 10/13/10 01:36 106-43-4 ND ug/L 5.0 1 10/13110 01:35 96-12-8 ND ug/L 1.0 1 10/13/10 01:35 124-48-1 ND ug/L 1.0 1 10/13110 01:35 106-93-4 ND ug/L 1.0 1 10/13/10 01:35 74-95-3 ND ug/L 1.0 1 10/13/10 01:35 95-50-1 ND ug/L 1.0 1 10/13/10 01:35 541-73-1 ND ug/L 1.0 1 10/13/10 01:35 106-46-7 ND ug/L 1.0 1 10/13/10 01:35 75-71-8 ND ug/L 1.0 1 10/13/10 01:35 75-34-3 ND ug/L 1.0 1 10113110 01:35 107-06-2 ND ug/L 1.0 1 10/13/10 01:35 75-35-4 ND ug/L 1.0 1 10/13/10 01:35 156-59-2 ND ug/L 1.0 1 10/13/10 01:35 156-60-5 ND ug/L 1.0 1 10/13/10 01:35 78-87-5 ND ug/L 1.0 1 10/13/10 01:35 142-28-9 ND ug/L 1.0 1 10/13/10 01:35 594-20-7 ND ug/L 1.0 ' 1 10/131.10 01:35 563-58-6 ND ug/L 1.0 1 10/13/10 01:35 10061-01-5 ND ug/L 1.0 1 10/13/10 01:35 10061-02-6 ND ug/L 1.0 1 10/13/10 01:35 108-20-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Qual Page 5 of 28 a eAnalytical wwpaciWabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Sample: MW-40 WT Parameters 8260 MSV Low Level Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene Styrene M 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene - 1,2,3-Trichlorob enzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chlo-ride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (S) Tbluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate . 353.2 Nitrogen, N021NO3 unpres; Nitrogen, Nitrate 450 0 Chloride Chloride Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LabID: 9279170002 Collected: 10/06/10 10:13 Received: 10/06/10 14:48 Matrix: Water Results Units Report Limit DF Prepared Analyzed dAS No. Qual Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 3.7 ug/L ND ug/L ND ug/L ND ug/L ND- ug/L ND ug/L ND ug/L 98 % 90 % 95 % 91 % Analytical Method: SM 2320B 14.6 mg/L Analytical Method: EPA 300.0 ND mg/L Analytical Method: EPA 353.2 2.6 mg/L Analytical Method: SM 4500-CI-E ND mg/L 1.0 1 10/13/10 01:35 100-41-4 1.0 1 10/13/10 01:35 87-68-3 5.0 1 10/13/10 01:35 591-78-6 1.0 1 10/13/10 01:35 99-87-6 2.0 1 10/13/10 01:35 75-09-2 b.0 1 10113110 01:35 108-10-1 1.0 1 10/13/10 01:35 1634-04-4 1.0 1 10/13/10 01:35. 91-20-3 1.0 1 10/13/10 01:35 100-42-5 1.0 1 10/13/10 01:35 630-20-6 1.0 1 10/13/10 01:215 79-34-5 .1.0 1 10/13110 01:35 127-18-4 1.0 1 10/13/10 01:35 108-88-3 1.0 1 10/13/10 01:35 87-61-6 1.0 1 10113110 01:35 120-82-1 1.0 1 10/13/10 01:35 71-55-6 1.0 1 10/13/10 01:35 79-00-5 1.0 1 10/13110 01:35 79-01-6 1.0 1 10/13/10 01:35 75-69-4 1.0 1 10113110 01:35 96-18-4 2.0 1 10/13/10 01:35 108-05-4 1.0 1 10113/10 01:35 -75-0-1-4- 2.0 1 10/13/10 01:35 179601-23-1 1.0 1 10/13/10 01:35 95-47-6 70-130 1 10/13/10 01:35 460-00-4 70-130 1 10/13/10 01:35 1868-53-7 70-130 1 10113/10 01:35 17660-07-0 70-130 1 10/13/10 01:35 2037-26-5 5.0 1 10/11/10 12:46 5.0 1 10/12/10 16:26 14808-79-8 0.10 1 10/06/10 17:29 5.0 1 10/12110 12:44 16887-00-6 Date: 10115/2010 02:33 PM REPORT OF LABORATORY ANALYSIS Page 6 of 28 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. %% ceAnalyfical wwwpacelab&com Pace Analytical Services, Inc. . 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 980OKinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Sample: MW-41 WT LabID: 9279170003 Collected: 10/06110 09:14 Received: 10/06110-14:48 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET lCP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 10/07/10 12:30 10/10/10 03:05 7440-38-2 Cadmium ND ug/L 1.0 1 10/07/10 12:30 10/10/10 03:05 7440-43-9 Chromium 83.2 ug/L 5.0 1 10/07/10 12:30 10/10/10 03:05 7440-47-3 Copper 70.5 ug/L 5.0 1 10/07/10 12:30 10/10/10 03:05 7440-50-8 Lead 9.1 ug/L 5.0 1 10/07/10 12:30 10110/10 03:05 7439-92-1 Zinc 69.6 ug/L 10.0 1 10/07/10 12:30 10/10/10 03:05 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 10/07/10 20:20 10/13/10 15:43 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 - 1 10/1 W11 0 02:00 67-64-1 Benzene ND ug/L 1.0 1 10/13/10 02:00 71-43-2 Bromobenzene ND ugtL 1.0 1 10/13/10 02:00 '108-86-1 Bromochloromethane N D uglL 1.0 1 10/13/10 02:00 74-97-5 Bromodichloromethane N D ug/L 1.0 1 10/13/10 02:00 75-27-4 Bromoform ND ug/L 1.0 1 10/13110 02:00 75-25-2 �Bromomethane ND ug/L 2.0 1 10/13/10 02:00 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 10/13/10 02:00 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 10/13/10 02:00 66-23-5 Chlorobenzene ND ug/L 1.0 1 10/13/10 02:00 108-90-7 dhloroe-thine ND ug/L 1.0 1 10/13/10 02:00 75 -00-3 Chloroform . 3.6 ug/L 1.0 1 10/13/10 02:00 67-66-3 Chloromethane ND ug/L 1.0 1 10/13/10 02:00 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 10113/10 02:00 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 10/13/10 02:00 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 10/13/10 02:00 96-12-8 Dibromochloromethane ND ug/L 1.0 1 10/13/10 02:00 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 10/13/10 02:00 106-93-4 Dibromomethane ND ug/L 1.0 1 .10/13110 02:00 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 10113/10 02:00 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 10/13/10 02:00 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 10/13/10 02:00 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 10/13/10 02:00 76-71-8 1,1-Dichloroethane ND ug/L 1.0 1 10/13/10 02:00 76-34-3 1,2-Dichloroethane ND ug/L 1.0 1 10/13/10 02:00 107-06-2 1,1-Dichloroethene ND ug/L� 1.0 1 10/13/10 02:00 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 10/13/10 02:00 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 10/13/10 02:00 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 10/13/10 02:00 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 10/13/10 02:00 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 10/13/10 02:00 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 10/13/10 02:00 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 10113110 02:00 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 10/13/10 02:00 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 10/13/10 02:00 108-20-3 Date: 10115/2010 02:33 PM REPORT OF LABORATORY ANALYSIS Page 7 of 28 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. aoeAn4lyficalo 2225 Riverside Dr. www.pacelabs.com Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-41 WT Parameters LabID: 9279170003 Collected: 10/06/10 09:14 Results Units Report Limit DF Received: 10/06/10 14:48 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 1.0 1 10/13/10 02:00 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 10/13/10 02:00 87-68-3 2-Hexanone ND ug/L 5.0 1 10/13110 02:00 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 10/13/10 02:00 99-87-6 Methylene Chloride ND ug/L 2.0 1 10/13/10 02:00 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 10/13/10 02:00 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 10/13/10 02:00 1634-04-4 Naphthalene ND ugIL 1.0 1 10/13/10 02:00 91-20-3 Styrene ND ug/L 1.0 1 10/13/10 02:00 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 10/13/10 02:00 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 10/13/10 02:00 79-34-5 Tetrachloroethene ND ug/L 1.0 1 10/13/10 02:00 127-18-4 Toluene ND ug/L 1.0 1 10/13/10 02:00 108'88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 10/13/10 02:00 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 10113/10 02:00 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 10/13/10 02:00 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 10/13/10 02:00 79-00-5 Trichloroethene ND ug/L 1.0 1 10/13/10 02:00 79-01-6 trichlorofluoromethane Nb ug/L 1.0 1 10/13/10 02:00 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 10/13110 02:00 96-18-4 Vinyl acetate ND ug/L 2.0 1 10/13/10 02:00 108-05-4 Vinyl chloride ND -ug!L- 1.0 1 10/13/10 02:00 75-01-4 M&P-Xylene ND ug/L 2.0 1 10/13110 02:00 179601-23-1 o-Xylene ND ug�!- 1.0 1 10/13/10 02:00 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 1 10/13/10 02:00 460-00-4 Dibromofluoromethane (S) 91 % 70-130 1 10/13/10 02:00 1868-53-7 1,2-Dichloroethane-d4 (S) 95 % 70-130 1 10/13/10 02:00 17060-07-0 Toluene-d8 (S) 90 % 70-130 1 10/13/10 02:00 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 . 12.6 mg/L 5.0 1 10/11/10 12:47 300.0 I.0 Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5.0 1 10/12/10 16:50 14808-79-8 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 3.2 mg/L 0.10 1 10/06/10 17:38 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 1 10/12/10 12:45 16887-00-6 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 28 a AnalXimlv Ice ww.pacelab&com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: RW-6 LabID: 9279170004 Collected: 10/06/1012:13 Received: 10/06/10,14:48 Matflx:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 10/07/10 12:30 10110/10 03:08 7440-38-2 Cadmium ND ug/L '1.0 1 10/07/10 12:30 10/10/10 03:08 7440-43-9 Chromium 162 ug/L 6.0 1 10/07/10 12:30 10110/10 03:08 7440-47-3 Copper ND ug/L 5.0 1 10107/10 12:30 10/10110 03:08 7440-50-8 Lead ND ug/L 5.0 1 10/07/10 12:30 10/10/10 03:08 7439-92-1 Zinc ND ug/L 10.0 1 10/07/10 12:30 10/10110 03:08 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury 0.38 ug/L 0.20 1 10/07/10 20:20 10/1311.0 15:46 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone* ND ug/L 125 5 10/13/10 12:03 67-64-1 D3 Benzene ND uglL 5.0 5 10/13110 12:03 71-43-2 Bromobenzene ND ug/L 5.0 5 16/13110 12:03 108-86-1 Bromochloromethane ND ug/L 5.0 5 10/13/10 12:03 74-97-5 Bromodichloromethane ND ug/L 5.0 5 10/13110 12:03 75-27-4 Bromoform ND ug/L 5.0 5" 10113110 12:03. 75-25-2 �Bromomethane ND ug/L 10.0 5 10/13/10 12:03 74-83-9 2-Butanone (MEK) ND ug/L 25.0 5, 10/13110 12:03 78-93-3 Carbon tetrachloride ND ug/L 5.0 6 10/13110 12:03 56-23-5 Chlorobenzene ND ug/L 5.0 5 10/13110 12:03 108-90-7 Chloroethane ND ug[L -6.0 5 10/13110 12:03 7&00-3 Chloroform ND ug/L 5.0 5 10/13110 12:03 67-66-3 Chloromethane ND ug/L 5.0 5 10113/10 12:03 74-87-3 2-Chlorotoluene ND ug/L 5.0 5 10113110 12:03 95-49-8 4-Chlorotoluene ND ug/L 5.0 5 10/13/10 12:03 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 25.0 5 10113/10 12:03 96-12-8 Dibromochloromethane ND ug/L 5.0 5 10/13/10 12:03 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5.0 5 10/13/10 12:03 106-93-4 Dibromomethane ND ug/L 5.0 5 10/13/10 12:03 74-95-3 1,2-Dichiorobenzene ND ug/L 5.0 5 10/13110 12:03 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 5 10/13/10 12:03 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 5 10/13/10 12:03 106-46-7 Dichlorodifluoromethane ND ug1L 5.0 5 10/13/10 12:03 75-71-8 M-Dichloroethane ND ug/L 5.0 6 10/13/10 12:03 75-34-3 1,2-Dichloroethane ND ug/L 5.0 5 10113110 12:03 107-06-2 1,1.-Dichloroethene ND ug/L 5.0 5 10/13110 12:03 75-35-4 cis-1,2-Dichlo'roethene ND ug/L 5.0' 5 10/13110 12:03 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 5 10113/10 12:03 156-60-5 1,2-Dichloropropane ND ug/L 5.0 5 10/13110 12:03 78-87-5 1,3-Dichloropropane ND ug/L 5.0 5 10113/10 12:03 142-28-9 2,2-Dichloropropane ND ug/L 5.0 5 10/13/10 12:03 594-20-7 1 il -Dichloropropene ND ug/L 5.0 5 10/13/10 12:03 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 5 10/13/10 12:03 10061-01-5 trans-1,3-Dichloropropene ND ug/L 5.0 5 10/13/10 12:03 10061-02-6 Diisopropyl ether ND ug[L. 5.0 5 10113/10 12:03 108-20-3 ---,,,Date: 10/15/2010 02:33 . PM REPORT OF LABORATORY ANALYSIS Page 9 of 28 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc' AnalXicale 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.p6calabs.com Asheville; N C 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC; -FAIRVIEW PILOT TEST 1016 Pace Project No.: 9279170 Sample: RW-6 Lab ID: 9279170004 Collected: 10/06/10 12:13 Received: 10/06110 14:48 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 5.0 5 10/13/10 12:03 100-41-4 Hexachloro-1,3-butadiene ND ug/L 5.0 5 10/13/10 12:03 87-68-3 2-Hexanone ND ug/L 25.0 5 10/13/10 12:03 591-78-6 p-Isopropyltoluene ND ug/L 5.0 5 10/13/10 12:03 99-87-6 Methylene Chloride ND ug/L 10.0 5 10/13/10 12:03 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 25.0 5 10113/10 12:03 108-10-1 Methyl-tert-butyl ether ND ug/L 5.0 5 10/13/10 12:03 1634-04-4 Naphthalene ND ug/L 5.0 5 10/13/10 12:03 91-20-3 Styrene ND ug/L 5.0 5 10/13110 12:03 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 5 10/13/10 12:03 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 10/13110 12:03 �9-34-5 Tetrachloroethene ND ug/L 5.0 5 10/13/10 12:03 .127-18-4 Toluene ND ug/L 6.0 5 10/13/10 12:03 108-88-3 1,2,3-Trichlorobenze6e ND ug/L 5.0 5 10/13/10 12:03 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 5 10/13/10 12:03 120-82-'l 1,1,1-Trichloroethane ND ug/L 5.0 5 10/13/10 12:03 71-55-6 1,1,2-T(ichloroethane' ND ug/L 5.0 5 10/13/10'12:03 79-00-5 Trichloroethene ND ug/L 5.0 5 10/13/10 12:03 79-01-6 Trichlorofluoromethane ND ug/L 5.0 5 10/13/10 12:03 75-69-4 1,2,3-Trichloropropane ND ug/L 5.0 5 10/13/10-12:03 96-18-4 Vinyl acetate ND ug/L 10.0 5 10/13/10 12:03 108-05-4 Vinyl chloride ND ug/L 5.0 5_ 10/13/10 12:03 75701-4 m&p-Xylene ND ug/L 10.0 5 10/13/10 12:03 179601-23-1 o-Xylene ND ug/L 5.0 5 10/13/10 12:03 95-47-6 4-Bromofluorobenzene (S) 95 % 70-130 5 10/13/10 12:03 460-00-4 Dibromofluoromethane (S) 89 % 70-130 5 10113110 12:03 1868-53-7 1,2-Dichloroethane-d4 (S) 92 % 70-130 5 10/13/10 12:03 17060-07-0 Toluene-d8 (S) 89 % 70-130 5 10/13/10 12:03 2037-26-5 2320B Alkalinity Analytical Method.: SM 2320B Alkalinity, Total as CaCO3 41.8 mg/L 6.0 1 10/11/10 12:47 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5.0 1 10/12/10 17:13 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA353.2 Nitrogen, Nitrate 2.8 mg/L 0.20 2 10/06110 17:24 D3 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L . 60.0 10 10/12/10 12:47 16887-00-6 D3 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS Page10of28 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. Pace Analytical Services, Inc. Analytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 -/581ce. wmv.pacdabscom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: . TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Sample: RW-7 Parameters LabID: 9279170005 Collected: 10/06/1013:06 Results Units Report Limit DF Received: 10106/1014:48 Matdx:Water Prepared Analyzed CAS No. Qual 6010 MET lCP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 500 1 10/07110 12:30 10/10/10 03:11 7440-38-2 Cadmium ND ug/L 100 1 10/07/10 12:30 10/10/10 03:11 7440-43-9 Chromium 1400 ug/L 500 1 10/07/10 12:30 10/10/10 03:11 7440-47-3 Copper ND ug/L 500 1 10/07/10 12:30 10110/10 03:11 7440-50-8 Lead ND ug/L 500 1 10107/10 12:30 10/10110 03:11 7439-92-1 Zinc ND ug/L 1000 1 10107/10 12:30 10110110 03:11 7440-66-6 7470 Mercury Analytical Meth od: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 20.0 1 10107110 20:20 10/13/10 15:48 7439-97-6 D3 2320BAlkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 418 mg/L 250 50 10/11110 12A8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5.0 1 10/12/10 17:37 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical,Method: EPA 353.2 Nitrogen, Nitrate ND mg/L 20.0 200 10/06110 17:39 D3 4500 Chloride Analytical Method: SM 4500-CI-E Chlodde ND mg/L 25000 5000 10/112/10 12:47 16887-00-6 D3 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Acco. Page 11 of 28 c Analytical www.pacoabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Sample: TRIP BLANK LablD: 9279170006 Collected: 10/06/1000:00 Received: 10106/1014:48 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 10/12/10 23:02 67-64-1 Benzene ND ug/L 1.0 1 10/12/10 23:02 71-43-2 Bromobenzene ND ug/L 1.0 1 10/12/10 23:02 108-86-1 Bromochloromethane ND ug/L 1.0 1 10/12/10 23:02 74-97-5 Bromodichloromethane ND ug/L 1.0 1 10/12110 23:02 75-27-4 Bromoform ND ug/L 1.0 1 10/12110 23:02 75-25-2 Bromomethane ND ug/L 2.0 1 10/12/10 23:02 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 10/12/10 23:02 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 10/12/10 23:02 56-23-5 Chlorobenzene ND ug/L 1.0 1 10/12110 23:02 108-90-7 Chloroethane ND ug/L 1.0 1 10/12110 23:02 75-00-3 Chloroform ND ug/L 1.0 1 10/12/10 23:02 67-66-3 Chloromethane ND ug/L 1.0 1 10/12/10 23:02 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 10112/10 23:02 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 10/12/10 23:02 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 10/12/10 23:02 96-12-8 Dibromochloromethane . ND ug/L 1.0 1 10/12/10 23:02 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 10/12/10 23:02 106-93-4 Dibromomethane ND ug/L 1.0 1 10/12/10 23:02 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 10/12110 23:02 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 10/12/10 23:02 641-73-1 1,4-Dichlorobenzene ND ugIL 1.0 1 10112/10 23:02 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 10/12/10 23:02 75-71-8 M-Dichloroethane ND ug/L 1.0 1 10/12/10 23:02 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 10/12/10 23:02 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 10/12/10 23:02 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.b 1 10/12/10 23:02 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 10/12110 23:02 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 10/12/10 23:02 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 10/12/10 23:02 142-28-9 2,2-Dichloropropane ND ug/L. 1.0 1 10/12/10 23:02 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 10/12110 23:02 563-58-6 c7is-1,3-Dichloropropene ND ug/L 1.0 1 10/12/10 23M 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 10/12110 23:02 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 10/12/10 23:02 108-20-3 Ethylbenzene ND ug/L 1.0 1 10/12/10 23:02 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 10/12/10 23:02 87-68-3 2-Hexanone ND ug/L 5.0 1 10/12/10 23:02 591-78-6 p-isopropyltoluene ND ug/L 1.0 1 10/12/10 23:02 99-87-6 Methylene Chloride 2.0 ug/L 2.0 1 10/12/10 23:02 75-09-2 C9 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 10/12/10 23:02 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 10/12/10 23:02 1634-04-4 Naphthalene ND ug/L 1.0 1 10/12/10 23:02 91-20-3 Styrene ND ug/L 1.0 1 10/12/10 23:02 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 10/12/10 23:02 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 10/12/10 23:62 79-34-5 Tetrachloroethene N-D ug/L 1.0 1 10/12/10 23:02 127-18-4 Date: 10/1512010 02:33 PM REPORT OF LABORATORY ANALYSIS Page 12 of 28 . This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Aclo" 4nal ,oical -/5alce www-pacelaks-- Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800KInceyAve. Suite 100 Huntersville, NC 28078 (704)875-90W Sample: TRIP BLANK Parameters LabID: 9279170006 Collected: 10/06/10 00:00 Results Units Report Limit DF Received: 10106110 14:48 Matrix: Water Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1.0 1 10/12/10 �3:02 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 10/12/10 23:02 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 10/12/10 23:02 120-82-1 �1,1,1-Trichloroethane ND ug/L 1.0 1- 10112/10 23:02 71-55-6 1,1,2-Trichloroethane N * D ug/L 1.0 1 10/12/10 23:02 79-00-5 Trichloroethene ND ug/L 1.0 1 10/12/10 23:02 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/12110 23:02 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 10/12/10 23:02 96-18-4 Vinyl acetate ND ug[L 2.0 1 10/12/10 23:02 108-05-4 Vinyl chloride ND ug/L 1.0 1 10/12110 23:02 75-01-4 m&p-Xylene ND ug/L 2.0 1 10/12/10 23:02 179601-23-1 o-Xylene ND ug/L 1.0 1 10112/10 23:02 95-47-6 4-Bromofluorobenzene (S) 91 % 70-130 1 10/12110 23:02 460-00 -4 Dibrornofluoromethane (S) 93 % 70-130 1 10/12/10 23:02 1868-53-7 1,2-Dichloroethane-d4 (S) 91 % 70-130 ' 1 10/12/10 23:02 17060-07-0 Tbluene-d8 (S) 93 % 70-130 1 10/12/10 23:02 2037-26-5 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, Inc.. 1% ACCC*' Page 13 of 28 acmnalyficalo I www.pacdabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. ]Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MPRP/7193 Analysis Method: EPA6010 QC Batch Method: EPA3010 Analysis Description: 6010 MET Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 METHOD BLANK: 508488 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 Blank Reporting Parameter Units Result Limit Analyzed Arsenic ug/L ND 5.0 10110/10 02:44 Cadmium ug/L ND 1 . .0 10/10/10 02:44 Chromium ug/L ND 5.0. 10/10/10 02:44 Copper ug/L ND 5.0 10/10/10 02:44 Lead ug/L ND 5.0 10110/10 02:44 Zinc ug/L ND 10.0 10/10/10 02:44 LABORATORY CONTROL SAMPLE: 508489 Parameter Units Arsenic ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Zin c ug/L MATRIX SPIKE SAMPLE: 508490 Parameter Units Arsenic ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Zinc ug/L SAMPLE DUPLICATE: 508491 Parameter Units Arsenic ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Zinc ug/L Date: 10/15/2010 02:33 PM Qualifiers Spike LCS LCS % Rec Conc. Result % Rec Limits 500 530 106 80-120 500 528 106 80-120 500 528 106 80-120 500 525 105 80-120 500 536 107 80-120 500 533 107 80-120 9279170001 Spike Result Conc. ND 500 1.0 500 343 500 184 500 359 500 416 500 MS Result 370 399 769 633 740 853 MS % Rec 74 80 85 90 76 87 9279170002 Dup Result Result RPID Qualifiers ND ND ND ND 89.3 86.3 3 32.5 31.5 3 5.1 ND 41.6 39.6 5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACCQ,' Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Fluntersville, NC 28078 (704)875-9092 Qualifiers % Rec Limits Qualifiers 75-125 MO 75-125 75-125 75-125 75-125 75-125 Page 14 of 28 /5a'ceAna1yica1dD wwwpa6fabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA QC Batch: MERP/3055 Analysis Method: EPA 7470 QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 METHOD BLANK: 508585 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003,91279170004,9279170005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 10/13/10 14:39 LABORATORY CONTROL SAMPLE: 508586 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.3 91 80-120 MATRIX SPIKE& MATRIX SPIKE DUPLICATE: 608587 508588 MS MSD 9278860002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result . Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 2.1 2.1 84 83 75-125 1 MATRIX SPIKE& MATRIX SPIKE DUPLICATE: -508589 -508590 MS MSD 9278860003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L NO 2.5 2.5 2.1 2.4 85 94 75-125 10 10115/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 15 of 28 Pace Analytical Services, Inc. 2225 Riverside Dr. (�IaoeMaOcal Asheville, NC 28804 pacelabs-c9m (828)264-7176 QUALITY CONTROL DATA Project: TEC - FAIRVIEW PILOT TEST 1016 Pace Project No.: 9279170 QC Batch: MSW12597 Analysis Method: QC Batch Method: EPA 8260 Analysis Description: Associated Lab Samples: 9279170001,9279170002,9279170003,9279170006 EPA 8260 8260 MSV Low. Level METHOD BLANK: 510229 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003,9279170006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/12/10 22:36 1,1,1-Trichloroethane ug/L ND 1.0 10/12/10 22:36 1,1,2,2-T6trachloroethane ug/L ND 1.0 10/12110 22:36 1,1,2-Trichloroethane ug/L ND 1.0 10112/10 22:36 1,1-Dichloroethane ug/L ND 1.0 10/12/10 22:36 1,1-Dichloroethene ug/L ND 1.0 10/12110 22:36 1,1-Dichloropropene ug[L ND 1.0 10/12110 22:36 1,2,3-Trichlorobenzene ug/L ND 1.0 10/12/10 22:36 1,2,3-Trichloropropane ug/L ND 1.0 10/12/10 22:36 1,2,4-Tdchlorobenzene ug/L. ND 1.0 .10/12/10 22:36 1,2-Dibromo-3-chloropropane ug[L ND 5.0 10112/10 22:36 1,2-Dibromoethane (EDB) ug/L ND 1.0 10/12/10 22:36 1,2-bichlorobenzene ug/L ND 1.0 10/12/10 22:36 1,2-Dichloroethane ug/L ND 1.0 10112/10 22:36 1,2-Dichloropropane ug/L ND 1.0 10/12/10 22:36 1,3-Dichlorobenzene ug/L ND 1.0 10/12110 22:36 1,3-Dichloropropane ug/L ND 1.0 10/1.2/10 2�:36 1,4-Dichlorobenzene ug/L ND - -1.0 -10/12/10 22:36 2,2-Dichloropropane ug/L ND 1.0 10/12/10 22:36 2-Butanone (MEK) ug/L ND 5.0 10/12/10 22:36 2-Chlorotoluene ug/L ND 1.0 10/12/10 22:36 2 , Hexanone ug/L ND 5.0 10112/10 22:36 4-Chlorotoluene ug/L ND 1.0 10/12/10 22:36 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 10/12/10 22:36 Acetone ug/L ND 25.0 10/12/10 22:36 Benzene ug/L ND 1.0 10/12/10 22:36 Bromobenzene ug/L ND 1.0 10/12/10 22:36 Bromochloromethane ug/L ND 1.0 10/12/10 22:36 Bromodichloromethane ug/L ND 1.0 10/12/10 22:36 Bromoform ug/L ND 1.0 10/12/10 22:36 Bromomethane ug/L ND 2.0 10112/10 22:36 Carbon tetrachloride ug/L ND 1.0 10112/10 22:36 Chlorobenzene ug/L ND 1.0 10/12/10 M36 Chloroethane ug/L ND 1.0 10/12/10 22:36 Chloroform ug/L ND 1.0 10112/10 22:36 Chloromethane ug/L ND 1.0 10/12/10 22:36 cis-1,2-Dichloroethene ug/L ND 1.0 10/12/10 22:36 cis-1,3-Dichloropropene ug/L NIj 1.0 10/12/10 22:36 Dibromochloromethane ug/L ND 1.0 10/12/10 22:36 Dibromomethane ug/L ND 1.0 10/12/10 22:36 Dichlorodifluoromethane ug/L ND 1.0 10/12/10 22:36 Diisopropyl ether ug/L ND 1.b 10/12/10 22:36 Ethylbenzene ug/L ND 1.0 10/12110 22:36 Date: 10115/2010 02:33 PM REPORT -OF LABORATORY ANALYSIS . This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 28 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pacemolyficala 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pawabs.com Asheville, NC 28804 Huntersville, NC 28078 QUALITY CONTROL DATA Project: TEC - FAIRVIEW PILOT TEST 1016 Pace Project No.: 9279170 (828)254-7176 (704)875-9092 .METHOD BLANK: 510229 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003,'9279170006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0 10/12/10 22:36 m&p-Xylene ug/L ND 2.0 10/12110 22:36 Methyl-tert-butyl ether ug1L ND 1.0 10/12110 22:36 Methylene Chloride ug/L ND' 2.0 10/12110 22:36 Naphthalene ug/L ND 1.0 10/12110 22:36 o-Xylene ug/L ND 1.0 10/12/10 22:36 p-Isopropyltoluene ug/L ND 1.0 10/12/10 22:36 Styrene ug/L ND 1.0 10/12/10 22:36 Tetrachloroethene ug/L ND 1.0 10/12110 22:36 Toluene ug/L ND 1.0 10112/10 22:36 trans-1,2-Dichloroethene . ug/L ND 1.0 10/12/10 22:36 trans-1,3-Dichloropropene ug/L ND 1.0 10/12/10 22:36 Trichloroethene ug/L ND 1-0 10/12110 22:36 Trichlorofluoromethane ugil- ND 1.0 10/12/10 22:36 .Vinyl acetate ug/L ND 2.0 10/12/10 22:36 Vinyl chloride ug/L ND 1.0 10/12/10 22:36 1,2-Dichloroethane-d4 (S) % 91 70-130 10/12/10 22:36 4-Bromofldorobenzene (S) % 92 70-130 10/12/10 22:36 -'Dibromofluoromethane (S) % 90 70-130 10/12/10 22:36 Tbluene-d8 (S) % 93 70-130 10/12110 22:36 LABORATORY CONTROL SAMPLE: Parameter 610230 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 48.1 96 70-130 1,1,1-Trichloroethane ug/L 50 41.3 83 70-130 1,1,2,2-Tetrachloroethane ug/L 50 41.9 84 70-130 1,1,2-Trichloroethane ug/L 50 38.6 77 70-130 1,1-Dichloroethane ug/L 50 44.8 90 70-130 1,1-:Dichloroethene ug/L 50 44.1 88 70-132 1,1-Dichloropropene ug/L 50 37.7 75 70-130 1,2,3-Trichlorobenzene ug/L 60 49.0 .98 70-135 1,2,3-Trichloropropane ug/L 50 42.3 m 70-130 1,2,4-Trichlorobenzene ug/L 50 48.0 96 70-134 1,2-Dibromo-3-chloropropane ug/L 50 47.6 95 70-130 1,2-Dibromoethane (EDB) ug/L 50 45.4 91 .70-130 1,2-Dichlorobenzene uglL 50 46.5 93 70-130 1,2-Dichloroethane ug/L 50 43.0 86 70-130 1,2-Dichloropropane ug[L 50 38.0 76 70-130 1,3-Dichlorobenzene ug!L 50 45.5 91 70-130 1,3-Dichloropropane ug/L 50 45.9 92 70-130 1,4-Dichlorobenzene ug/L 50 48.0 96 70-130 2,2-Dichloropropane ug/L 60 42.0 84 58-145 2-Butanone (MEK) ug/L 100 72.1 72 70-145 2-Chlorotoluene ug/L 50 46.1 92 70-130 )Date: 10/15/2010 02:33 PIVI REPORT OF LABORATORY ANALYSIS Page 17 of 28 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. a eAnalytical ww.paWabs.ccm Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 LABORATORY CONTROL SAMPLE: Parameter 510230 Units 2 Hexanone ug/L 4-Chlorotoluene ug/L 4-Methyl-2-pentanone (MIBK) ug/L Acetone ug/L Benzene ug/L Bromobenzene ug/L Bromochloromethane ug/L Bromodichloromethane ug/L Bromoform ug/L Bromomethane ug/L Carbon tetrachloride ug/L Chlorobenzene ug/L Chloroethane ug/L Chloroform ug/L Chloromethane ug/L Cis-1,2-Dichloroethene ug/L cis-1,3-Dichloropropene ug/L Dibromochloromethane ug/L Dibromomethane ug/L Dichlorodifluorornethane ug/L Diisopropyl ether ug/L �thylbenzene ug/L Hexachloro-1,3-butadiene ug/L M&p-Xylene ug/L Methyl-tert-butyl ether ug/L Methylene Chloride ug/L Naphthalene ug/L o-Xylene ug/L p-Isopropyltoluene ug/L Styrene ug/L Tetrachloroethene ug/L Toluene ug/L trans-1,2-Dichloroethene ug/L trans-1,3-Dichloropropene ug/L Trichloroethene ug/L Trichlorofluoromethane ug/L Vinyl acetate ug/L Vinyl chloride ug/L 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Dibromofluoromethane (S) % Tbluene-d8 (S) % Date: 10/15/2010 02:33 PM Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 . (828)254-7176 QUALITY CONTROL DATA Spike Conc. LCS Result LCS % Rec % Rec Limits 100 93.4 93 70-144 50 48.9 98 70-130 100 83.3 83 70-140 100 77.4 77 50-175 50 44.9 90 70-130 50 43.3 87 70-130 50 43.7 87 70-130 50 40.0 80 70-130 50 43.0 86 70-1 W 50 43.6 87 54-130 50 44.1 88 70-132 50 46.4 93 70-130 50 42.8 86 64-134 50 43.8 88 70-130 50 37.6 75 64-130 50 42.6 85 70-131 50 40.4 81 70-130 50 44.6 89 70-130 50 42.2 84 70-131 50 38.1 76 56-130 60 45.5 91 70-130 50 49.8 100 70-130 50 45.0 90 70-130 100 98.5 98 70-130 50 43.5 87 70-130 50 38.9 78 63-130 50 53.1 106 70-138 50 49.8 100 70-130 50 48.5 97 70-130 50 47.9 96 70-130 50 51.8 104 70-130 50 43.6 87 70-130 50 43.3 87 70-130 50 39.7 79 70-132 50 44.6 89 70-130 50 46.3 93 62-133 100 94.3 94 66-157 50 40.6 81 69-130 87 70-130 96 70-130 86 70-130 91 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Acco, Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Hunter.sville, N C 28078 (704)875-9092 Qualifiers Page 18 of 28 p' 1�5a'ooAnalyfical" wwpacefabscom Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. � 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 510231 510232 MS MSD 9279055018 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Clual 1,1-Dichloroethene ug/L ND 50 50 46.6 52.6 93 105 70-166 12 Benzene ug/L ND 50 50 53.7 48.8 107 97 70-148 10 Chlorobenzene ug/L ND 50 50 55.1 52.9 110 106 70-146 4 Toluene ug/L ND 50 50 49.3 49.7 99 99 70-155 1 Trichloroethene ug/L ND 50 50 48.6 48.8 97 97 69-161 0 1,2-Dichloroethane-d4 (S) % 87 88 70-130 4-Bromofluorobenzene (S) % 92 90 70-130 Dibromofluorom,ethane (S) % 84 87 70-130 Toluene-d8 (S) % 89 88 70-130 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, m(ithout the written consent of Pace Analytical Services, Inc.. ACCo,' Page 19 of 28 WeAnaljftal MW.PaGwabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MSW12624 QC Batch Method: EPA 8260 Associated Lab Samples: 9279170004 Analysis Method: Analysis Description: EPA 8260 8260 MSV Low Level METHOD BLANK: 510996 Matrix: Water Associated Lab Samples: 9279170004 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/19/10 10:44 1,1,1-Trichloroethane ug/L ND 1.0 10/13/10 10:44 1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/13/10 10:44 1,1,2-Trichloroethane ug/L ND 1.0 10/13/10 10:44 M-Dichloroethane ug/L ND 1.0 10/13/10 10:44 IJ-Dichloroethene ug/L ND 1.0 10/13/10 10:44 1,1-Dichloropropene ug/L ND 1.0 10/13110 10:44 1,2,3-Trichlorobenzene ug/L ND 1.0 10/13/10 10:44 1,2,3-Trichloropropane ug/L ND 1.0 10/13/10 10:44 1,2,4-Trichlorobenzene ug/L ND 1.0 10/13/10 10:44 1,2-Dibromo-3-chloropropane ug/L ND 5.d 10/13/10 10:44 1,2-Dibromoethane (EDB) ug/L ND 1.0 10/13/10 10:44 1,2-Dichlorobenzene ug/L ND 1.0 10/13/10 10:44 1,2-Dichloroethane ug/L ND 1.0 10113/10 10:44 1,2-Dichloropropane ug/L ND 1.0 10/13/10 10:44 1,3-Dichlorobenzene ug/L ND 1.0 10/13110 10:44 1,3-Dichloropropane ug/L ND 1.0 10/13/10 10:44 1,47Dichlorobenzene ug/L ND 1.0 10/13/10 10:4.4 2,2-Dichloropropane ug/L ND 1.0 10113/10 10:44 2-Butanone (MEK) ug/L ND 5.0 10/13/10 10:44 2-Chlorotoluene ug/L ND 1.0 10/13/10 10:44 2-Hexanone ug/L ND 5.0 10/13/10 10:44 4-Chlorotoluene ug/L ND I * 0 10/13110 10:44 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 10/13/10 10:44 Acetone ug/L ND 25.0 10113110 10:44 Benzene ug/L ND 1.0 10113/10 10:44 Bromobenzene ug/L ND 1.0 10/13/10 10:44 Bromochloromethane ug/L NQ 1.0 10/13/10 10:44 Bromodichboromethane ug/L ND 1.0 10/13/10 10:44 Bromoform ug/L ND 1.0- 10/13/10 10:44 Bromomethane ug/L ND 2.0 10/13/10 10:44 Carbon tetrachloride ug/L ND 1.0 10/13/10 10:44 Chlorobenzene ug/L ND 1.0 10/13110 10:44 Chloroethane ug/L ND 1.0 10/13/10 10:44 Chloroform ug/L ND 1.0 10/13/10 10:44 Chloromethane ug/L ND 1.0 10/13/10 10:44 cis-1,2-Dichloroethene ug/L ND 1.0 10/13/10 10:44 Cis-1,3-Dichioropropene ug/L ND 1.0 10/13/10 10:44 Dibromochloromethane ug/L ND 1.0 10113/10 10:44 Dibromomethane ug/L ND 1.0 10/13/10 10:44 Dichlorodifluoromethane ug/L ND 1.0 10/13/10 10:44 Diisopropyl ether ug/L ND 1.0 10113/10 10:44 Ethylbenzene ug/L ND 1.0 10/13/10 10:44 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACCO, Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 28 Pace Analytical Services, Inc. 1�5a'cemal 2225 Riverside Dr. yical@ www.pacilabs.com Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: TEC - FAIRVIEW PILOT TEST 1016 Pace Project No.: 9279170 METHOD BLANK: 510996 Associated Lab Samples: Parameter 9279170004 Units Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 1.0 10/13/10 10:44 m&p-Xylene ug/L ND 2.0 10113/10 10:44 Methyl-tert-butyl ether ug/L ND 1.0 10/13110 10:44 Methylene Chloride ug/L ND 2.0 10/13110 10:44 Naphthalene ug/L ND 1.0 10/13110 10:44 o-Xylene ug/L ND 1.0 10/13/10 10:44 p-Isopropyltoluene ug/L ND 1.0 10/13/10 10:44 Styrene ug/L ND 1.0 10/13110 10:44 Tetrachloroethene ug/L ND 1.0 10/13/10 10:44 Toluene ug/L ND 1.0 10/13/10 10:44 trans-1,2-Dichloroethene ug/L ND 1.0 10/13/10 10:44 trans-1,3-Dichloropropene ug/L ND 1.0 10/13/10 10:44 Tdchloroethene ug/L ND 1.0 10/13/10 10:44 Trichloroflu oro methane ug/L ND 1.0 10/13/10 10:44 Vinyl acetate ug/L ND 2.0 10/13110 10:44 Vinyl chloride ug/L ND 1.0 10/13/10 10:44 1,2-Dichloroethane-d4 (S) 92 70-130 10/13110 10:44 4-Bromofluorobenzene (S) % 93 70-130 10/13/10 10:44 Dibromofluoromethane (S) % 95 70-130 10/13110 10:44 Tbluene-d8 (S) % 93 70-130 10/13/10 10:44 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: Parameter 510997 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 49.6 99 70-130 1,1,1-T(ichloroethane ug/L 60 45.1 90 70-130 1,1,2,2-Tetrachloroethane ug/L 50 45.4 91 70-130 1,1,2-Trichloroethane ug/L 50 41.4 83 70-130 1,1-Dichloroethane ug/L 50 47.1 94 70-130 1,1-Dichloroethene ug/L 50 47.1 94 70-132 1,1-Dichloropropene ug/L 50 42.2 84 70-130 1,2,3-Trichlorobenzene ug/L 50 49.8 100 70-135 1,2,3-Trichloropropane ug/L 50 47.4 95 70-130 1,2,4-Trichlorobenzene ug/L 50 48.6 97 70-134 1,2-Dibromo-3-chloropropane ug/L 50 4 8.9 98 70-130 1,2-Dibromoethane (EDB) ug/L 50 48.0 96 70-130 1,2-Dichlorobenzene ug/L 50 48.1 96 70-130 1,2-Dichloroethane ug/L 50 46.5 93 70-130 1,2-Dichloropropane ug/L. 50 38.1 76 70-130 1,3-Dichlorobenzene ug/L 60 46.0 92 70-130 1,3-Dichloropropane ug/L 50 47.5 95 70-130 1,4-Dichlorobenzene ug/L 50 48.2 96 70-130 2,2-Dichloropropane ug/L 50 38.1 76 58-145 2-Butanone (MEK) ug/L 100 83.9 84 70-145 2-Chlorotoluene ug/L 50 47.5 95 70-130 ---,,0ate: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Acco, Page 21 of 28 _� . I coAnalytical www.pacelabs.com Project: . TEC -FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800KInceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: Parameter 510997 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2-Hexanone ug/L 100 98.3 98 70-144 4-Chlorotoluene ug/L 50 50.6 _101 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 84.4 84 70-140 Acetone ug/L 100 77.9 78 50-175 Benzene ug/L 50 50.0 100 70-130 Bromobenzene ug/L 50 44.3 89 70-130 Bromochloromethane ug/L 50 45.2 90 70-130 Bromodichloromethane ug/L 50 40.6 81 70-130 Bromoform UgIL 50 45.9 92 70-130 Bro.momethane ug/L 50 45.3 91 54-130 Carbon tetrachloride ug/L 50 45.8 92 70-132 Chlorobenzene ug/L 60 49.4 99 70-130 Chloroethane ug/L 50 44.2 88 64-134 Chloroform ug/L 50 44.8 90 70-130 Chloromethane ug/L 50 39.9 80 64-130 cis-1,2-Dichloroethene ug/L 50 43.7 87 70-131 ds-1,3-Dichloropropene ug/L 60 39.9 80 70-130 Dibromochloromethane ug1L 50 47.0 94 70-130 Dibromomethane ug/L 50 43.7 87 70-131 Dichlorodifluoromethane ugiL 50 38.5 77 66-130 Diisopropyl ether ug/L 50 46.9 94 70-130 Ethylbenzene ug/L 50 52.5 105 70-130 ug/L 50 49.1 98 70-130 -Hexachloro-1,3-butadiene m&p-Xy_le ne - ' - - ug/L 100 103 103 70-i3O Methyl-tert-butyl ether ug/L 50 44.1 88 70-130 Methylene Chloride ug/L 50 39.9 80 63-130 Naphthalene ug/L 50 55.1 110 70-138 o-Xylene ug/L 50 51.2 102 70-130 P-Isopropyltoluene ug/L 50 50.0 100 70-130 Styrene , ug/L 50 47.6 95 70-130 Tetrachloroethene ug/L 50 54.5 109 70-130 Toluene ug/L 50 44.4 89 70-130 trans-1,2-Dichloroethene ug/L 50 44.6 89 70-130 trans-1,3-Dichloropropene ug/L 50 39.8 60 70-132 Trichloroethene ug/L 50 46.1 92 70-130 Trichlorofluoromethane ug/L 50 49.3 99 62-133 Vinyl acetate ug/L 100 90.7 91 66-157 Vinyl chloride ug/L 50 42.1 84 69-130 1,2-Dichloroethane-d4 (S) % 92 70-130 4-Bromofluorobenzene (S) % 97 70-130 Dibromofluoromethane (S) % 91 70-130 Tbluene-d8 (S) % 92 70-130 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 22 of 28 /Jo.e. Analytical wwwpacelab&cam Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 510998 510999 MS MSD 9279353012 Spike Spike MS MSD -MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual M-Dichloroethene ug/L 50.3 51.9 3 Benzene ug/L 3.0 50 50 52.1 53.3 98 101 70-148 2 Chlorobenzene ug/L ND 50 50 53.4 64.5 107 109 70-146 2 Toluene ug/L ND 50 50 50.9 50.7 102 101 70-155 0 Trichloroethene ug/L 48.1 49.7 3 1,2-Dichloroethane-d4 (S) % 90 89 70-130 4-Bromofluorobenzene (S) % 91 97 70-130 Dibromofluoromethane (S) % 90 86 70-130 Toluene -dB (S) % 90 89 70-130 \ Date: 10115/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACC,' Page 23 of 28 a eAnalytical www.pacWabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WET114053 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320B Alkalinity Associated Lab Samples: 9279170001,9279170002,92791700 03,9279170004,9279170005 METHOD BLANK: 509999 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L ND 5.0 10/11/10 12:39 Pace Analytical Services, Inc. 980.0 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 510000 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L 50 48.6 97 90-110 SAMPLE DUPLICATE: 510001 9278655001 Dup Parameter Units Result Result RPD Qualifiers Alkalinity, Total as CaCO3 mg/L 17.8 18.8 6 SAMPLE DUPLICATE: 510002 9279170001 Dup Parameter Units Result Result RPD Qualifiers Alkalinity, Total as CaCO3 mg/L 17.8 16.7 6 Date: 10/15/2010 02:33 PM REPORT OF LABORATORY A14ALYSIS This report shall not be reproduced, except in full, without the written consent of.Pace Analytical Services, Inc.. Page 24 of 28 Pace Analytical Services, Inc. AnalXical 2225 Riverside Dr.. /�?Cevyvmpac6labs.com Asheville, NG 28804 (828)254-7176 QUALITY CONTROL DATA Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 QC Batch: WETA/8345 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279i7OoO5 METHOD BLANK: 510116 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/L ND 5.0 10/12/1010:30 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 510117 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limit� Qualifiers Sulfate mg/L 30 28.5 95 MATRIX SPIKE SAMPLE: 510118 9279101001. Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mg/L 1210 30 1210 -4' Mo MATRIX SPIKE SAMPLE: 610120 9279101002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Sulfate mg/L 1340 30 1320 -56 Mo SAMPLE DUPLICATE: 510119 9279101001 Dup Parameter Units Result Result RPI) Qualifiers Sulfate mg/L 1210 1220 1 SAMPLE DUPLICATE: 510121 9279101002 Dup Parameter Units Result Result RPD Qualifiers Sulfate mg/L 1340 1330 1 Date: 10/1512010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except Ifi full, without the written consent of Pace Analytical Services, Inc.. ACCQ,' Page 25 of 28 Pace Analytical Services, Inc. ceAnalytical 2225 Riverside Dr. 7c, Asheville, NC 28804 �c wwwpacelabs com (828)254-7176 QUALITY CONTROL DATA Project: TEC - FAIRVIEW PILOT TEST 1016 Pace Project No.: 9279170 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: WETA18312 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 METHOD BLANK: 508198 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen', Nitrate mg/L ND 0.10 10/06/10 17:05 LABORATORY CONTROL SAMPLE: 508199 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 6 5.2 104 90-110 MATRIX SPIKE SAMPLE: 508200 9279102001 Spike MS MS 0/6 Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 0.66 5 5.5 97. 90-110 MATRIX SPIKE SAMPLE: 508201 9279102002, Spike MS MS % Rec Parameter Units Result Conc. Result Rec Limits Qualifiers Nitrogen, Nitrate . mg/L 1.2 5 6.1 97 90-110 SAMPLE DUPLICATE: 508202 9279102003 Dup- Parameter Units Result Result RPD Qualifiers Nitrogen, Nitrate mg/L ND ND SAMPLE DUPLICATE: 508203 9279102004 Dup' Parameter Units Result Result RPD Qualifiers Nitrogen, Nitrate mg/L 1.4. 1.4 0 - 'Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 26 of 28 acioAnalyfical" www.pacdabs.com Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETA/8348 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 9279170001,9279170002,9279170003,9279170004,9279170005 METHOD BLANK: 610321 Matrix: Water Associated Lab Samples: 9279170001,9279170002,9279170003.9279170004,9279176005 Blank Reporting Parameter Units Result Limit Analyzed Chloride mg/L ND 5.0 10/12/10 12:39 LABORATORY CONTROL SAMPLE: 510322 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 20.5 102 90-110 MATRIX SPIKE SAMPLE: Parameter Chloride 510323 9279113001 Spike MS MS % Rec Units Result Conc. Result % Rec Limits Qualifiers mg/L 6510 5000 10900 88 75-125 SAMPLE DUPLICATE: 510324 9279120001 Dup Parameter Units Result Result RPD. Qualifiers Chloride mg/L 234 247 5 / 0ate: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. %o ACco, Page 27 of 28 ceA nalyfical" ww.pacelabsxom QUALIFIERS Project: TEC - FAIRVIEW PILOT TEST 10/6 Pace Project No.: 9279170 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS , (D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. Date: 10/15/2010 02:33 PM REPORT OF LABORATORY ANALYSIS Page 28 of 28 This report shall not be reproduced, except in full, without the written c onsent of Pace Analytical Services, Inc.. ,1�!;ZeAna iTI .. It CHAIN -OF -CUSTODY /Analytical Request Document The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company; jr Report To: Attention: 2r JVr Z226g 61ft 4' 1464 1365589 Address�xm Copy To: Company Name: 9V REGIJILATORY 4PENCY Address: afr,,a r- NPDES rV-GROUND WATER r- DRINKING WATER F . LIST RCRA OTHER Purchase Order No.: Paw Quote Reference: Project Name; Pam Proj ct V Site Liocation Managers 1014� ... -` S TA T9. AJV— Requested Due DatarrAT: 4; C;p li Project Number: Pace Profile#: �:Riiiquiiitec!'Anilysis F11fdrid (YiN) Section D Matrix Codes Required Client Information MATRIX I CODE COLLECTED Preservatives Drinking Water DW 0 L) it z 2 Water WT Waste Water WW 0 ED COMPOSITE COMPOSITE Product P 7R ;� START ENDIGRAB Soll!Solld SIL Oil - OL SAMPLE ID I . 0 . 0 L) I I Wipe WP (A-Z, 0-9 1,-) Ar AR LU IL 40 0 Sample IDS MUST BE UNIQUE TIssue TS 0 U Lu Other OT X Lu W 0 0 a_ L) 0 CL 0 U) '6 1 -717 17 0 %Ze 'z cc CV > U) DATE TIME DATE TIME U) z z 0 -0 Project N..1 Lab I.D. 1 r4w- Wt wr C0 14(0110 1114 )H Y, Wh/ K Y I. I I I I 2 1H W - 40 Wr & It/Wila lors ) A, 11 1 $4 1 1 1 - 3 H V-r - H L Wr VJT G 10 �t S 7 -C7 r7a 4 VT 6. R -Ca X X, %/ 9TI V e7 f 7ell .,I 5 CUT 1. -91 —S 19-41-1K V, 1 17,0,0'a S Is, I e. e-' 7 8 9 10 111 121 ADDITIONAL COMMENTS RELINQUISHED BY tAFFILIATION DATE.. TIME ACCEPTED BY AFFILIAT ION DA�T TIME SAMPLE CONDITIONS. %6-4� S 'IV V SAMPL -.NAM .0 ORIQ'INAL o . "! -8z PRINT Name of SAMPLER, E n.T SIGNATURE of SAMPLER: DATE Signed (MMIDDIYY): E .Ir� late: By signing. this form you are accepting Pare's NET 30 day payment terms and agreeing to late charges of 1.5% per month, 1volces not �ald within 30 days. F-ALL-Q-020rev.07,, Y -ZOU7 I Sample Condition Upon Re Fice Analjftal' Client Name: Project #--!b 2 q f 70 1111here Received: El Huntersville P-Aiheville El Eden Courier: EJ Fed Ex EJ UPS 0 uspSe-ETICEr—lent EJ Commercial El Pace Other_ Custody Seal on Cooler/Box Present: El yes .2-In"o- Seals intact: El yes Packing Material: El Bubble Wrap 'E� 11ubble Bags El None E10ther Thermometer Usedt�522 / 14-648-44 Type of Ic Blue None Temp Correction Factor: Adil:14-1§jj�� 0. Optional ,p- �o Proi. Due Date: Proj. Name: P1<a—MP-111 on ice, cooling'process has begun Corrected Cooler Temp.: 5. 0 C Biological Tissue is Frozen: Yes No Da—teand Initia e m I Ining Temp should be above freezing to 60C Comments: contents Chain of Custody Present: ef<Yes ONo ON/A 1 Chain of Custody Filled Out: I Rfe—, ONo OWA 2. Chain of Custody Relinquished: PKe.' ONo ONIA 3.- Sampler Name & Signature on COC: No ON/A 4. Samples Arrived within Hold Time: R<e. ONo ONIA 5. Short Hold Time Analysis (<72hr): 42f.—, ONo ONIA 6. Rush Turn Around Time Requested: OYes Dwo--'ONZA 7. Sufficient Volume: J�Ke—. ONo ONIA 8. Correct Containers Used: 94-'s ONo ONIA 9. -Pace Containers Used: 9,!!!�s PNo ON/A .,,�ontainers Intact: ONo ONIA 10. Filtered volume received for Dissolved tests LK.-'[]No ONIA 11. Sample I Labels match COC: _Q*6-s'ONo 0 NhA 1�. -includes date/time/ID/Analysis Matrix: All containers needing preservation have been checked. X-'S' ONo ON/A 13. All containers needing preservation are found to be in compila;e recommendation. ONo El N/A - �wit 'P11"' except oliform, TOC, O&G, WI-DRO (water) J2 VeONo Initial when completed Samples checked for dechlorination: _Q*gs— ONo ON/A 14. Headspace in VOA Vials (>6mm): 21!e:s� E]No ONIA 15. Trip Blank Present: ��Yes ONo ON/A 16. Trip Blank Custody Seals Present 0. No ON/A. ,Pace Trip Blank Lot# (if purchased): Client Notification/ Resolution: Person, Contacted: Comments/ Resolution: Datefrime: Field Data Required? Y / N T-jCURF Reviewd 6a !Date: SRF Review: Uve 113ate: Note: Whenever there is a discrepancy affecting North Carolina comKiiance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) F-ASV-CS-03-Rev.02 L . a ceAnalytical wmpacilabs.com October 28, 2010 Mr. Chris Gilbert Altamont Environmental 231 Haywood Street Asheville, NC 28801 RE: Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Gilbert: Enclosed are the analytical results for sample(s) received by the laboratory on October 19, 2010. The results relate only to the samples included in this report. Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. I norganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwisefootnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Lord Patton lorri..pafton@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 25 a oAnalytical wmpacelabscom Project: TEC-Falrview Pilot Test 10/19 Pace Project No.: 9280078 Charlotte Certification lDs; 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/LELAP Certification #: 04034 New Jersey Certification #: NCO12 North Carolina Drinking Water Certification #: 37706 North Caroli na Field'Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pennsylvania Certification #: 68-00784 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. * 99006003 Virginia Certification #: 00213 Connecticut Certification#: PH-01 04 Florida/NELAP Certification* E87627 Kentucky UST Certification #: 84 Louisiana DHH Drinking Water * LA 100031 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC . 28804 North Carolina Drinking Water Certification #: 37712 Connecticut Certification#: PH-01 06 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 Pennsylvania Certification #: 68-03578 Massachusetts Certification #: M-NC030 South Carolina Bioassay Certification * 99030002 New Jersey Certification #: NC01 I ' South Carolina Certification #: 99030001 North Carolina Bioassay Certification #: 9 Virginia Certification #: 00072 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, ' except in full, without the written consent of Pace Analytical Services, Inc.. Acco" Page 2 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. ooAnalyfica( 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 wwwpaqvfabs.com (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test 10119 Pace Project No.: 9280078 Sample: MW-39 WT Lab ID: 9280078001 Collected: 10119/1011:14 Received: 10/1911015:25 Matrix: Water Parameters 6010 MET ICP Arsenic Cadmium Chromium Copper Lead Zinc 7470 Mercury Results Units Report Limit DF . Prepared Analyzed CAS No. Qual Analytical Method: EPA 6010 Preparation* Method: EPA 3010 ND ug/L 5.0 1 10/20/10 11:30 10/21/10 22:45 7440-38-2 6.0 ug/L 1.0 1 10/20/10 11:30 10/21/10 22:45 7440-43-9 418 ug/L 5.0 1 10/20/10 11:30 10/21/10 22:45 7440-47-3 218 ug/L 5.0 1 10120/10 11:30 10/21/10 22:45 7440-50-8 448 ug/L 5.0 1 10120/10 11:30 10/21/10 22:45 7439-92-1 493 ug/L 10.0 1 10/20/10 11:30 10/21/10 22:45 7440-66-6 Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury 0.26 ug/L 0.20 1 10/21/10 12:40 10122/10 13:16 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25000 1000 10/20/10 20:11 67-64-1 Benzene ND ug/L 1000 1000 10120/10 20:11 71-43-2 Bromobenzene ND ug/L 1000 1000 10/20/10 20:11 108-86-1 Bromochloromethane ND ug/L 1000 1000 10120/10 20:11 74-97-5 Bromodichloromethane ND ug/L 1000 1000 10/20/10 20:11 75-27-4 Bromoform ND ug/L 1000 1000 10/20/10 20:11 75-25-2 �Bromomethane ND ug/L 2000 1000 10/20/10 20:11 74-83-9 2-Butanone (MEK) 5610 ug/L 5000 1000 10120/10 20:11 78-93-3 Carbon tetrachloride ND ug/L 1000 1000 10120/10 20:11 56-23-5 Chlorobenzene ND ug/L 1000 1000 10/20/10 20:11 108-90-7 Chloroethane ND ug/L- *1000 1000 10/20/10-20-.11 75-00-3 Chloroform ND ug/L 1000' 1000 10/20/10 20:11 67-66-3 Chloromethane N D ug/L 1000 1000 10/20/10 20:11 74-87-3 2-Chlorotoluene ND ug/L 1000 1000 10120/10 20:11 95-49-8 4-Chlorotoluene ND ug/L 1000 1000 10/20110 20:11 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5000 1000 10/20/10 20:11 96-12-8 Dibromochloromethane ND ug/L 1000 1000 10/20/10 20:11 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1000 1000 10120/10 20:11 106-93-4 Dibromomethane ND ug/L 1000 1000 10/20/10 20:11 74-95-3 1,2-Dichlorobenzene ND ug/L 1000 1000 10/20/10 20:11 95-50-1 1,3-Dichlorobenzene ND ug/L i000 1000 10/26/10 20:11 541-73-1 1,4-Dichlorobenzene ND ug/L 1000 1000 10/20/10 20:11 106-46-7 Dichlorodifluoromethane ND ug/L 1000 1000 10/20/10 20:11 75-71-8 1,1-Dichloroethane ND ug/L 1000 1000 10/20/10 20:11 75-34-3 1,2-Dichloroethane ND ug[L 1000 1000 10/20/10 20:11 107-06-2 1,1-Dichloroethene ND ug/L 1000 1000 10/20/10 20:11 75-35-4 c7is-1,2-Dichloroethene ND ug/L 1000 1000 10/20/10 20:11 156-59-2 trans-1,2-Dichloroethene ND ug/L 1000 1000 10/20/10 20:11 156-60-5 1,2-Dichloropropane ND ug/L 1000 1000 10/20/10 20:11 78-87-5 1,3-Dichloropropane ND ug/L 1000 1000 10/20/10 20:11 142-28-9 2,2-Dichloropropane ND ug/L 1000 1000 10/20/10 20:11 594-20-7 IJ-Dichloropropene ND ug/L 1000 1000 10/20/10 20:11 563-6.8-6 cis-1,3-Dichloropropene ND ug/L 1000 1000 10/20/10 20:11 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1000 1000 10/201i 0 20:11 10061-02-6 Diisopropyl ether ND ug/L 1000 1000 10/20/10 20:11 108-20-3 /Date: 10/2812010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Acco'. Page 3of25 . 7 ci PaceAnalytical Services, Inc. Pace Analytical Services, Inc. maildicalo 2225 Riverside Dr. 9800,Kincey Ave. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test 10/19 Pace Project No.; 9280078 Sample: MW-39 WT Lab ID: 9280078001 Collected: 10/19/1011:14 Received: 10/19/1015:25 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 1000 1000 10120/10 20:11 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1000 1000. 10120110 20:11 87-68-3 2-Hexanone ND ug/L 5000 1000 10/20/10 20:11 591-78-6 p4sopropyltoluene ND ug/L 1000 1000 1 . 0120/10 20:11 99-87-6 Methylene Chloride ND ug/L 2000 1000 10/20110 20:11 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 6000 1000 10/20/10 20:11 108-10-1 Methyl-tert-butyl ether ND ug/L 1000 1000 10/20/10 20:11 1634-04-4 Naphthalene ND ug/L 1000 1000 10120/10 20:11 91-20-3 Styrene ND ug/L 1000 1000 10/20/10 20:11 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1000 1000 10120/10 20:11 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1000 1000 10/20/10 20:11 79-34-5 Tetrachloroethene 1540 ug/L 1000 1000 10/20/10 20:11 127-18-4 Toluene 4450 ug/L 1000 1000 10/20/10 20:11 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1000 1000 10120/10 20:11 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1000 1000 10/20/10 20:11 120-82-1 1,-1,1-Trichloroethane 10600 ug/L 1000 1000 10/20/10 20:11 71-55-6 1,1,2-Trichloroethane ND ug/L 1000 1000 10/20/10 20:11 79-00-5 Trichloroethene 156000 ug/L 1000 1000 10/20/10 20:11 79-01-6 Trichlorofluoromethane ND ug/L 1000 1000 10/20/1020:11 75-69-4 1,2,3-Trichloropropane ND ug/L 1000 1000 10/20/10 20:11 96-18-4 Vinyl acetate ND ug/L 2000 1000 10/20/10 20:11 108-05-4 Vinyl chloride ND ug/L 1000 1000 10/20/10 20:11 75-01-4 m&ia-Xylere ND ug/L 2000 1000 10/20/10"20:11 IT9661-231-1 o-Xylene ND ug/L 1000 1000 10/20110 20:11 95-47-6 4-Bromofluorobenzene (S) 101 % 10-130 1000 10/20/10 20:11 460-00-4 Dibromolluoromethane (S) 104 % 70-130 1000 10120/10 20:11 1868-53-7 1,2-Dichloroethane-d4 (S) 112 % 70-130 1000 10/20/10 20:11 17066-07-0 Tbluene-dS (S) 97 % 70-130 1000 10/20/10 20:11 2037-26-5 2320BAlkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 15.4 mg/L 5.0 1 10/26110 16:22 300.0 IQ Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5.0 1 10/22/10 03:00 14808-79-8 363.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate. 0.34 mg/L 0.10 1 10/20/10 10:42 M1 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 1 10/20110 13:59 16887-00-6 Date: 10/2812010 10:32 AM REPORT OF LABORATORY ANALYSIS Page 4 of 25 This report -shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ACCQ,� 1/56aeAnalyfical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Sample: MW-40 WT LabID: 9280078002 Collected: 10/1911010:16 Received: 10/19/1015:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 . 1 10/20/10 11:30 10/21/10 22:58 7440-38-2 Cadmium ND ug/L 1.0 1 10/20110 11:30 10/21110 22:58 7440-43-9 Chromium 92.3 ug/L 5.0 1 10120/10 11:30 10/21/10 22:58 7440-47-3 Copper 31.7 ug/L 5.0 1 10/20/10 11:30 10/21/10 22:58 7440-50-8 Lead ND ug/L 5.0 1 10/20110 11:30 10121/10 22:58 7439-92-1 Zinc 58.9 ug/L 10.0 1 10120110 11:30 10/21/10 22:58 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 10121/10 12:40 10/22110 13:24 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 10/20/10 20:37 67-64-1 Benzene ND ug/L 1.0 1 10/20110 20:37 71-43-2 Bromobenzene ND ug/L 1.0 1 10/20110 20:37 108-86-1 Bromochloromethane ND ug/L 1.0 1 10/20/10 20:37 74-97-5 Bromodichloromethane ND ug/L 1.0 1 10/20110 20:37 75-27-4 Bromoform ND ug/L 1.0 1 10120110 20:37 75-25-2 'Bromomethane ND ug/L 2.0 1 10120/10 20:37 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 10/20110 20:37 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 10/20/10 20:37 56-23-5 Chlorobenzene ND ug/L 1.0 1 10/20/10 20:37 108-90-7 Chloroethane ND ug/L Iwo 1 10120110 20:37 75-00-3 Chloroform 3.4 ug/L 1.0 1 10120/10 20:37 67-66-3 Chloromethane ND ug/L 1.0 1 10/20/10 20:37 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 10/20/16 20:37 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 10/20110 20:37 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 10/20/10 20:37 96-12-8 Dibromochloromethane ND ug/L 1.0 1 10/20/10 20:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 11.0 - 1 10/20110 20:37 106-93-4 Dibromomethane ND ugIL 1.0 1 10/20/10 20:37 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1� 10/20/10 20:37 96-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 10120/10 20:37 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 10/20110 20:37 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 10120/10 20:37 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 10/20/10 20:37 75.-34-3 1,2-Dichloroethane ND ug/L 1.0 1 10/20/10 20:37 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 10/20/10 20:37 75-35-4 c7is-1,2-Dichloroethene ND ug/L 1.0 1 10/20/10 20:37 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 10/20/10 20:37 156-60-5 1,2-Dichloropropane ND ug[L 1.0 1 10/20110 20:37 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 10120/10 20:37 .142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 10/20/10 20:37 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 10/20/10 20:37 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 10/20/10 20:37 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 10/20/10 20:37 10061-02-6 Dilsopropyl ether ND ug/L 1.0 1 10/20/10 20:37 108-20-3 )Date: 1012812010 10:32 AM REPORT OF LABORATORY ANALYSIS Page 5of26 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc ACCO,. a eAnalj6dal ww.pacelabsxom Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)876-9092 Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Sample: MW-40 WT Lab ID., 9280078002 Collected: 10/1911010:16 Received: 10/19/1615:25 -Matrix:Water Parameters Results Un its Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 1.0 1 10/20/10 20:37 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 10/20/10 20:37 87-68-3 2-Hexanone ND ug/L 5.0 1 10/20/10 20:37 591-78-6 p-lsopropyltoluene ND ug/L 1.0 1 .10120/10 20:37 99-87-6 Methylene Chloride ND ug/L 2.0 '1 10120/10 20:37 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 10120/10 20:37 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 10/20110 20:37 1634-04-4 Naphthalene ND ug/L 1.0 1 10/20/10 20:37 91-20-3 Styrene ND ug/L 1.0 1 10/20/10 20:37 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 10/20/10 20:37 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L .1.0 1 10/20/10 20:37 79-34-5 Tetrachloroethene ND ug/L 1.0 1 10/20/10 20:37 127-18-4 Toluene ND ug/L 1.0 1 10/20/10 20:37 108-88-3 1,2,3-Tdchlorobenzene ND ug/L 1.0 1 10/20110 20:37 87-61-6 1,2,4-Tdchlorobenzene. ND ug1L 1.0 1 10/20/10 20:37 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 10/20/10 20:37 71-55-6 1,1,2-Tdchloroethane ND ug/L 1.0 1 10/20/10 20:37 79-00-5 Trickloroethene 2.9 ug/L 1.0 1 10/20/10 20:37 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/20/10 20:37 75-69-4 1,2,3-Tdchloropropane ND ug/L 1.0 1 10/20/10 20:37 96-18-4 Vinyl acetate ND ug/L 2.0 1 10/20/10 20:37 108-05-4 Vinyl chloride ND ug/L' 1.0 1 10/20110 20:37 75-01-4 m&p-Xylene Nb uglL 2.0 1 1 mbli 0 2b: 37 176601-23-1 o-Xylene ND ug/L 1.0 1 10120/10 20:37 95-47-6 4-Bromofluorobenzene (S) 97 % 70-130 1 10/20/10 20:37 460-00-4 Dibromofluoromethane (S) 107 % 70-130 1� 10/20/10 20:37 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 170-130 1 10/20/10 20:37 17060-07-0 Toluene-d8 (S) 99 % �0-1 30 1 10/20/10 20:37 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 10.2 mg/L 5.0 1 10/26/10 16:22 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5:0 1 10/22/10 04:11 14808-79-8 353.2 Nitrogen, NO2/H03 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 2.7 mg/L 0.10 1 10120110 10:45 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 1 10/20110 13:59 16887-00-6 Date: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of PaceAnalytical Services, Inc.. AccoR Page. 6 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. oeAnalyficalo 2225 Riverside Dr. 9800 KinceyAve. Suite too wwwpacelabscom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Sample: MW-41 WT Parameters Lab ID: 9280078003 Collected: 10/19/1009:24 Results Units Report Limit DF Received: 10/19/1015:25 Matrix:Water Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3010 Arsenic ND ug/L 5.0 1 10/20/10 11:30 10/21110 23:06 7440-38-2 Cadmium ND ug/L 1.0 1 10120/10 11:30 10/21/10 23:06 7440-43-9 Chromium 7.1 ug/L 5.0 1 10/20/10 11:30 10/21/10 23:06 7440-47-3 Copper ND ug/L 5.0 1 10120/10 11:30 10/21110 23:06 7440-50-8 Lead ND ug/L 5.0 1 10/20/10 11:30 10/21/10 23:06 7439-92-1 Zinc ND ug/L 10.0 1 10/20/10 11:30 10/21/10 23:06 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 10/21/10 12:40 10/22/10 13:31 7439-97-6 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 10120/10 21:02 67-64-1 Benzene ND ug/L 1.0 1 10/20/10 21:02 71-43-2 Bromobenzene ND ug/L 1.0 1 10/20/10 21:02 108-86-1 Bromochloromethane ND ug/L 1.0 1 10120/10 21:02 74-97-5 Bromodichloromethane ND ug/L 1.0 1 10/20/10 21:02 75-27-4 13romoform ND ug/L 1.0 1 10/20110 21:02 75-25-2 Nb ug/L 2.0 1 10120110 21:02 74-83-9 �2_Butanone (MEK) ND ug/L 5.0 1 10120/10 21:02 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 10120110 21:02 56-23-5 Chlorobenzene ND ug/L 1.0 1 10/20/10 21:02 108-90-7 Chloroethane ND ug/L -1.0 1 10/20/10 21:02 75-00-3 Chloroform .6.0 ug/L 1.0 1 10/20/10 21:02 67-66-3 Chloromethane ND ug/L 1.0 1 10/20/10 21:02 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 10/20/10 21:02 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 10/20/10 21:02 106-43-4 1,2-Dibromo-3-chloro propane ND ug/L 5.0 1 10/20110 21:02 96-12-8 Dibromochloromethane ND ug/L 1.0 1 1 0/20h 0 21:02 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 10/20/10 21:02 106-93-4 Dibromomethane ND ug/L 1.0 1 10120/10 21:02 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 10/20/10 21:02 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 10/20/10 21:02 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 10/20/10 21:02 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 10/20/10 21:02 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 10/20/10 21:02 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 10/20/10 21:02 107-06-2 1, 1 -Diehl oroethene ND ug/L 1.0 1 10/20/10 21:02 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 10/20/10 21:02 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 10/20/10 21:02 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 10/20110 21:02 78-87-5 .1,3-Dichloropropane ND ug/L 1.0 1 10/20/10 21:02 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 10/20/10 21:02 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 10/20110 21:02 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 10/20/10 21:02 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 10/20/10 21:02 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 10/20110 21:02 108-20-3 ;)ate: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS Page 7 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc acieAnalyficalo www.pac�ldbs.com Project: TEC-Fairview Pilot Test 10/19 Pace Project No.:' 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-41 WT Parameters Lab ID: 9280078003 Collected: 10/19/1009:24 Results Units Report Limit DF Received: 10/1911015:25 Matrix: Water P.repared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 1.0 1 10/20/10 21:02 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 10/20/10 21:02 87-68-3 2-Hexanone ND ug/L 5.0 1 10120/10 21:02 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 10/20/10 21:02 99-87-6 Methylene Chloride ND ug/L 2.0 1 10/20/10 21:02 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 10/20110 21:02 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 10120/10 21:02 1634-04-4 Naphthalene ND ug/L 1.0 1 10/20110 21:02 91-20-3 Styrene ND ug/L 1.0 1 10/20/10 21:02 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 10/20110 21:02 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 10120/10 21:02 79-34-5 ' Tetrachloroethene ND ug/L 1.0 1 10/20/10 21:02 - 127-18-4 Toluene ND ug/L 1.0 1 10/20/10 21:02 108-88-3 1,2,3-Trichlorobenzene Nb ug/L 1.0 1 10/20/10 21:02 87-61-6 1,2,4-Trichlorobenzene N D ug/L 1.0 1 10/20/10 21:02 120-82-1 1, 1, 1 -Trichloroethane ND ug/L 1.0 1 10/20/10 21:02 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 10/20/10 21:02 79-00-5 Trichloroethene N D ug/L 1.0 1 10/20110 21:02 79-01-6 Trichlorofluoromethane N D ug/L 1.0 1 10/20/10 21:02 75-69-4 1,2,3-Tr'ichloropropafie ND ug/L 1.0 1 10/20/10 21:02 96-18-4 Vinyl acetate ND ug/L 2.0 1 10/20/10 21:02 108-05-4 Vinyl chloride ND ug/L 1.0 1 1012011.0 21:02 75-01-4 m&p-Xylene ND ug/L 2.0 1 10/20110 21:02 179601-23-1 o-Xylene ND ug/L 1.0 1 10/20/10 21:02 95-47-6 4-Bromofluorobenzene (S) 100 % 70-130 1 1.0/20/10 21:02 460-00-4 Dibromofluoromethane (S) 104 % 70-130 1 10/20/10 21:02 1868-53-7 1,2-Dichloroethane-d4 (S) ill % 70-130 1 10/20/10 21:02 17b6O-O7-0 Tbluene-d8 (S) 98 % 70-130 1 10120/10 21:02 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaCO3 10.2 mg/L 5.0 1 10126110 16:22 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 S ulfate ND mg/L 5.0 1 10/22/10 04:34 14808-79-8 353.2 Nitrogen, N021NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 3.3 mg/L 0.10 1 10120110 10:48 4500 Chloride Analytical Method: SM 4500-CI-E Chloride ND mg/L 5.0 1 10120110 13:59 16.887-00-6 Date: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. AccQ# .-J iac� Page 8 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. Xical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 eMal /5ao www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Sample:'RW-6 Lab ID: 9280078004 Collected: 10/19/10 12:13 Received: 10/19/10 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 5.0 1 10/20/10 11:30 10/21/10 23:25 7440-38-2 Cadmium ND ug/L 1.0 1 10/20/10 11:30 10121110 23:25 7440-43-9 Chromium 117 ug/L 5.0 1 10/20/10 11:30 10/21/10 23:25 7440-47-3 Copper ND ug/L 5.0 1 10/20/10 11:30 10121/10 23:25 7440-50-8 Lead ND ugil- 6.0 1 10120/10 11:30 10/21/10 23:25 7439-92-1 Zinc 17.4 ug/L 10.0 1 10/20/10 11:30 10/21/10 23:25 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 10121/10 12:40 10/22/10 13:34 7439-97-6 .8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 250 10 10/20/10 21:27 67-64-1 Benzene ND ug/L 10.0 10 10/20/10 21:27 71-43-2 Bromobenzene ND ug/L 10.0 10 10/20110 21:27 108-86-1 Bromochloromethane ND ug/L 10.0 10 10120/10 21:27 74-97-5 Bromodichloromethane ND ug/L 10.0 10 10/20/10 21:27 75-27-4 9romoform NID ug/L 10.0 10 10/20/10 21:27 75-25-2 �3romomethane ND ug/L 20.0 10 10/20/10 21:27 74-83-9 ---�O-Butanone (MEK) ND ug/L 50.0 10 10120110 21:27 78-93-3 Carbon tetrachloride ND ug/L 10.0 10 10/20/10 21:27 56-23-5 Chlorobenzene ND ug/L 10.0 10 10120/10 21:27 108-90-7 Chloroethane ND ug/L 10.0 10 10/20/10 21:27 75-00-3 Chloroform ND ug/L 10.0 10 1 0120h 0 21:27 67-66-3 Chloromethane ND ug/L 10.0 10 10/20/10 21:27 74-87-3 2-Chlorotoluene ND ug/L 10.0 10 10/20/10 21:27 95-49-8 4-Chlorotoluene ND ug/L 10.0 10 10/20/10 21:27 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 60.0 10 10/20/10 21:27 96-12-8 Dibromochloromethane ND ug/L 10.0 10 10120110 21:27 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 10.0 10 10/20/10 21:27 106-93-4 Dibromomethane ND ug/L 10.0 10 10120/10 �1:27 74-95-3 1,2-Dichlorobenzene ND ug/L 10.0 10 10/20110 21:27 95-50-1 1,3-Dichlorobenzene ND ug/L 10.0 10 10/20110 21:27 541-73-1 1,4-Dichloro6enzene NID ug/L 10.0 10 10/20/10 21:27 106-46-7 Dichlorodifluoromethane ND ug/L 10.0 10 10/20110 21:27 75-71-8 1,1-Dichloroethane NIJ ug/L 10.0 10 10/20110 21:27 75-34-3 1,2-Dichloroethane ND ug/L 10.0 10 10/20/10 21:27 107-06*-2 1,1-Dichloroethene ND ug/L 10.0 10 10/20/10 21:27 75-35-4 cis-1,2-Dichloroethene ND ug/L 10.0 10 10/20/10 21:97 156-59-2 trans-1,2-Dichloroethene ND ug/L 10.0 10 10120/10 21:27 166-60-5 1,2-Dichloropropane ND ug/L 10.0 10 10/20/10 21:27 78-87-5 1,3-Dichloropropane ND ug/L 10.0 10 10120110 21:27 142-28-9 2,2-Dichloropropane ND ug/L 10.0 10 10/20/10 21:27 594-20-7 1,1-Dichloropropene NID ug/L 10.0 10 10/20/10 21:27 563-58-6 cis-1,3-Dichloropropene ND ug/L 10.0 10. 10/20/10 21:27 10061-01-5 trans-1,3-Dichloropropene ND ug/L 10.0 10 10120/10 21:27 -10061-02-6 Dilsopropyl ether NID ug/L 10.0 10 10/20110 21:27 108-20-3 1)ate: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. D3 Page 9 of 25 acloAnalyfical www.paqe1ahs.cain Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9900 Kincey Ave. Suite 1 ' 00 Ftuntersville, NC 28078 (704)875-9092 Project: TEC-Fairview Pilot Test 10119 Pace Project No.: 9280078 Sample: RW-6 LablD: 9280078004 Collected: 10/19/1012:13 Received: 10/19/1015:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Analytical Method: EPA 8260 Ethylbenzene ND ug/L 10.0 10 Hexachloro-1,3-butadiene ND ug/L 10.0 10 2-Hexanone ND ug/L 50.0 10 p-Isopropyltoluene ND ug/L 10.0 10 Methylene Chloride ND ug/L 20.0 10 4-Methyl-2-pentanone (MIBK) ND ug/L 50.0 10 Methyl-tert-butyl ether ND ug/L 10.0 10 Naphthalene ND ug/L 10.0 10 Styrene ND ug/L 10.0 10 1,1,1,2-Tetrachloroethane ND ug/L 10.0 10 1,1,2,2-Tetrachloroethane ND ug/L 10.0 10 Tetrachloroethene ND ug/L 10.0 10 Toluene ND ug/L 10.0 10 1,2,3-Trichlorobenzene ND ug/L 10.0 10 1,2,4-Trichlorobenzene ND ug/L 10.0 10 1,1,1-Trich.loroethane ND ug/L 10.0 10 1,1,2-Trichloroethane ND ug/L 10.0 10 Trichloroethene ND ug/L 10.0 10 Tr'ichlorofluoromethane ND ug/L 10.0 10 1,2,3-Trichloropropane ND ug/L 10.0 10 Vinyl acetate ND ug/L 20.0 10 Vinyl chloride ND ug/L 10.0 10 m&p-Xylene ND ugll- 20.0 10 o-Xylene ND ug]L 10.0 10 4-Bromofluorobenzene (S) 100 % 70-130 10 Dibromofluoromethane (S) 105 % 70-130 10 1,2-Dichloroethane-d4 (S) III % 70-130 10 Toluene -dB (S) 99 % 70-130 10 2320B Alkalinity Analytical Method: SM 2320B Alkalinity, Total as CaC 03 42.0 mg/L 5.0 1 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Sulfate ND mg/L 5.0 1 363.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Nitrogen, Nitrate 3.2 mg/L 0.10 1 4500 Chloride Analytical Method: SM 4500-CI-E Chloride 6.0 mg/L 5.0 1 Date: 10/2812010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 10/20/10 21:27 100-41-4 10/20/10 21:27 87-68-3 10120/10 21:27 591-78-6 10120/10 21:27 99-87-6 10/20/10 21:27 75-09-2 10/20/10 21:27 108-10-1 10/20/10 21:27 1634-04-4 10/20/10 21:27 91-20-3 10/20/10 21:27 100-42-5 10/20110 21:27 630-20-6 10/20/10 21:27 79-34-5 10120110 21:27 127-18-4 10/20/10 21:27 108-88-3 10120/10 21:27 87-61-6 10/20/10 21:27 120-82-1 10/20/10 21:27 71-55-6 10/20/10 21:27 79-00-5 10/20/10 21:27 79-01-6 10/20/10 21:27 75-69-4 10/20/10 21:27 96-18-4 10/20/10 21:27 108-05-4 10/20/10 21:27 75-01-4 10/20/10 21:27 179601-23-1 10/20/10 21:27 95-47-6 10/20/10 21:27 460-00-4 10/20/10 21:27 1868-53-7 10/20/10 21:27 17060-07-0 10/20/10 21:27 2037-26-5 10126/10 16:23 10/22/10 04:58 14808-79-8 10120110 10:49 10/24/10 15:11 16887-00-6 Page10of25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. AnalXical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 1�5alce Asheville, NC 288 . 04 Huntersville, NC 28078 (828)254-7176 (704)876-9092 ANALYTICAL RESULTS Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Sample: RW-7 LablD: 9280078006 Collected: 10/19/1013:03 Received: 10/19/1015:25 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND ug/L 500 1 10/20110 11:30 10121/10 23:28 7440-38-2 Cadmium NO ug/L 100 1 10/20110 11:36 10/21/10 23:28 7440-43-9 Chromium 768 ug/L 500 1 10/20/10 11:30 10/21/10 23:28 7440-47-3 Copper ND ug/L 500 1 10/20/10 11:30 10/21/10 23:28 7440-50-8 Lead ND ug/L 500 1 10/20/10 11:30 10/21/10 23:28 7439-92-1 Zinc ND ug/L 1000 1 10/20/10 11:30 10/21/10 23:28 7440-66-6 7470 Mercury Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 2.0 1 - 10/21?10 12:40 10/22/10 13:42 7439-97-6 D3 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 125000 5000 10/20/10 21:63 67-64-1 D3 Benzene ND ug/L 5000 5000 10/20/10 21:53 71-43-2 Bromobenzene ND ug/L 5000 5000 10120/10 21:53 108-86-1 Bromochloromethane ND ug/L 5000 5000 10/20110 21:53 74-97-5 Bromodichloromethane ND ug/L 5000 5000 10/20/10 21:53 75-27-4 13romoform ND ug/L 5000 5000 10/20/10 21:53 75-25-2 'Bromomethane ND ug/L 10000 5000 10/20/10 21:53 74-83-9 2-Butanone (MEK) ND ug/L 25000 5000 10/20110 21:53 78-93-3 Carbon tetrachloride ND ug/L 5000 5000 10120/10 21:53 56-23-5 Chlorobenzene ND ug/L 5000 5000 10/20/10 21:53 108-90-7 Chloroethane ND ug/L 5000- 5000 10/20/10 21:53 76-00-3 Chloroform ND ug/L 5000 5000 10120/10 21:53 67-66-3 Chloromethane ND ug/L 5000 5000 10/20/10 21:53 74-87-3 2-Chlorotoluene ND ug/L 5000 5000 10/20/10 21:53 95-49-8 4-Chlorotoluene ND ug/L 5000 5000 10/20/10 21:53 106-43-4 1,2-Dibromo-3-chloro propane ND ug/L 25000 5000 10/20/10 21:53 96-12-8 Dibromochloromethane ND ug/L 5000 5000. 10/20/10 21:53 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 5000 5000 10120/10 21:53 106-93-4 Dibromomethane ND ug/L 5000 5000 10/20/10 21:53 74-95-3 1,2-Dichlorobenzene NID ug/L 5000 5000 10120/10 21:53 95-50-1 1,3-Dichlorobenzene ND ug/L 5000 5000 10/20110 21:53 541-73-1 1,4-Dichlorobenzene ND ug/L 5000 5000 10/20/10 21:53 106-46-7 Dichlorodifluoromethane ND ug/L 5000 5000 10/20/10 21:53 75-71-8 I,I-Dichloroethane NO ug/L 5000 5000 10120/10 21:53 75-34-3 1,2-Dichloroethane ND ug/L 5000 5000 10/20/10 21:53 107-06-2 IJ-Dichloroethene ND ug/L 5000 5000 10/20110 21:53 75-35-4 cis-1,2-Dichloroethene NID ug/L 5000 5000 10120/10 21:53 156-59-2 trans-1,2-Dichloroethene ND ug/L 5000 5000 16/20/10 21:53 156-60-5 1,2-Dichloropropane NO ug/L 6000 5000 10/20/10 21:53 78-87-5 1,3-Dichloropropane ND ug/L 5000 5000 10120/10 21:53 142-28-9 2,2-Dichloropropane ND ug/L 5600 5000 10/20/10 21:53 594-20-7 1,1-Dichloropropene NID ug/L 5000 5000 10/20/10 21:63 563-58-6 cis-1,3-Dichloropropene ND ug/L 5000 5000 10/20110 21:53 10061-01-5 tran's-1,3-Dichloropropene ND ug/L 5000 5000 10/20/10 21:53 10061-02-6 Diisopropyl ether NID ug/L 5000 5000 10120/10 21:53 108-20-3 ,Date: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS Page 11 of 25 This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. 0 1 a eAnal . yfical ww.pacelabs.com Project: Pace Project No. Sample: RW-7 TEC-Fairview Pilot Test 10/19 9280078 Parameters 8260 MSV Low Level Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4mlvlethyl-2-pentanone (MlBK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Tr'ichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloro6thene Trichlor-ofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chlor ide m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (S) Tbluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 300.0 IC Anions 28 Days Sulfate 353.2 Nitrogen, NO2/NO3 unpres; Nitrogen, Nitrate 4600 Chloride Chloride Date: 10/28/2010 10:32 AM Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)2544176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab!D: 9280078005 Collected: 10/19/10 13:03 Received: 10/19/10 15:25 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qua] Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND'ug/L ND ug/L NQ ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug[L ND ug/L ND ug/L ND ug/ L ND ug/L ND ug/L 100 % 109 % 113 % 98 % Analytical Method: SM 2320B ND mg/L Analytical Method: EPA 300.0 ND mg/L Analytical Method: EPA 353.2 ND mg/L Analytical Method: SM 4500-CI-E ND mg/L 5000 5000 10/20/10 21:53 100-41-4 5000 5000 10/20/10 21:53 87-68-3 25000 5000 10/20/10 21:53 591-78-6 5000 5000 10/20/10 21:53 99-87-6 10000 5000 10/20/10 21:53 75-09-2 25000 5000 10/20/10 21:53 108-10-1 5000 5000 10/20/10 21:53 1634-04-4 '5000 5000 10/20/10 21:53 91-20-3 5000 5000 10120110 21:53 100-42-5 5000 5000 10/20/10 21:53 630-20-6 5000 5000 10/20/10 21:53 79-34-5 5000 5000 10/20/10 21:53 127-18-4 6000 5000 10/20/10 21:53 108-88-3 5000 5000 10120110 21:53 87-61-6 6000 5000 10/20/10 21:53 120-82-1 5000 5000 10/2M 0 21:53 71-55-6 5000 5000 10120/10 21:53 79-00-5 5000 5000 10/20/10 21:53 79-01-6 5000 5000 10/20/10 21:53 75-69-4 5000 5000 10/20110 21:53 96-18-4 10000 5000 10/20/10 21:53 108-05-4 6000 5000 10/20/10 21:53 75-01-4 10000 5000 10/20/10 21:53 179601-23-1 5000 5000 10120110 21:53 95-47-6 70-130 5000 10/20/10 21:53 460-00-4 70-130 5000 10120110 21:53 1868-53-7 70-130 5000 10/20/10 21:53 17060-07-0 70-130 5000 10/20/10 21:53 2037-26-5 25000 5000 10/26/10 16:23 5000 1000 1 10/22/10 05:22 14808-79-8 D3 10.0 100 10/20/10 11:11 5000 1000 10124/10 15:11 16887-00-6 D3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, with out th e vaitten consent of Pace Analytical Services, Inc.. Page 12 of 25 1�5a.'peAnalyfical ID www.pacelabs.com Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Trip Blank Parameters LablID: 9280078006 Collected: 10/19/1000:00 Results Units Repprt Limit DF Received: 10/19/1015:25 Matdx:Water Prepared Analyzed CAS No. 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 25.0 1 10/20/10 19:46 67-64-1 Benzene ND ug/L 1.0 1 10/20/10 19:46 71-43-2 Bromobenzene NID ug/L 1.0 1 10/20/10 19:46 108-86-1 Bromochloromethane ND ug/L 1.0 1 10120/10 19:46 74-97-5 Bromodichloromethane ND ug/L 1.0 1 10/20/10 19:46 75-27-4 Bromoform ND ug/L 1.0 1 10/20/10 19:46 75-25-2 Bromomethane NID ug/L 2.0 1 10/20/10 19:46 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 10/20/10 19:46 78-93-3 Carbon tetrachloride NID ug/L 1.0 1 10/20/10 19:46 56-23-5 Chlorobenzene ND ug/L 1.0 1 10/20/10 19:46 108-90-7 Chloroethane ND ug/L 1.0 1 10/20/10 19:46 75-00-3 Chloroform ND ug/L 1.0 1 10/20/10 19:46 67-66-3 Chloromethane NID ug/L 1.0 1 10/20/10 19:46 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 10/20/10 19:46 95-49-8 4-Chlorotoluene NID ug/L 1.0 1 10/20/10 19:46 106-43-4 1,2-Dibromo-3-chloropropane NID ug/L 5.0 1 10120110 19:46 96-12-8 Dibromochlo romethane ND ug/L 1.0 1 10/20/101 9:46 124-48-1 ,,2-Dibromoethane (EDB) ND ug/L 1.0 1 -10/20/10 19:46 106-93-4 -!)ibromomethane NID ug/L 1.0 1 10120/10 19:46 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 10/20/10 19:46 95-50-1 1,3-Dichlorobenzene NID ug/L 1.0 1 10/20/10 19:46 541-73-1 1,4-Dic-hl-orobenzene NID ug/L 1.0 1 10/20110 19:46 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 10/20/110 19:46 75-71-8 M-Dichloroethane ND ug/L 1.0 1 10/20/10 19:46 75-214-3 1,2-Dichloroethane ND ug/L 1.0 1 10/20/10 19:46 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 10/20/10 19:46 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 10/20/10 19:46 156-59-2 trans-1,2-Dichloroethene NID ug/L 1.0 1 10120/1019 :46 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 10/20/10 19:46 78-8T5 1,3-Dichloropropane ND ug/L 1.0 1 10/20/10 19:46 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 10/20/10 19:46 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 10/20/10 19:46 563-58-6 cis-1,3-Dichloropropene NID ug/L 1.0 1 10/20/10 19:46 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 10120/10 19:46 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 10/20/10 19:46 108-20-3 Ethylbenzene ND ug/L 1.0 1 10/20/10 19:46 100-41-4 Hexachloro-1,3-butadiene ND ug/L 1.0 1 10/20/10 19:46 87-68-3 2-Hexanone ND ug/L 5.0 1 10/20/10 19:46 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 10/20110 19:46 99-87-6 Methylene Chloride NID ug/L 2.0 1 10/20/1619:46 75-09-2 4-Methyl-2-pentanone (MIBK) NID ug/L 5.0 1 10/20110 19:46 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 10/20/10 19:46 1634-04-4 Naphthalene NID ug/L 1.0 1 10/20110 19:46 91-20-3 Styrene ND ug/L 1.0 1 10/20/10 19:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L .1.0 1 10/20/10 19:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 10/20110 19:46 79-34-5 Tetrachloroethene ND ug/L 1.0 1 10/20/10 19:46 127-18-4 .late: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Page 13 of 25 acieAnaliftal www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Me. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TEC-Falrview Pilot Test 10/19 Pace Project No.: 9280078 Sample: Trip Blank LablD: 9280078006 Collected: 10/19/1000:00 Received: 10/19/1015:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,11 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl a(cetate Vinyl chloride m&p-Xylene o-Xylene 4-Bromofluorobenzene (S) Dibromofluoromethane (S) 1,2-Dichloroethane-d4 (S) Tbluene-d8 (S) Analytical Method: EPA 8260 ND ug/L 1.0 1 10/20/10 19:46 108-88-3 ND ug/L 1.0 1 10/20/10 19:46 87-61-6 ND ug/L 1.0 1 10/20/10 19:46 120-82-1 �D ug/L 1.0 1 10/20/10 19:46 71-55-6 ND ug/L 1.0 1 10/20/10 19:46 79-00-5. ND ug/L 1.0 1 10/20/10 19:46 79-01-6 ND ug/L 1.0 1 10/20/10 19:46 75-69-4 ND ug/L 1.0 1 10/20/10 19:46 96-18-4 ND ug/L 2.0 1 10/20/10 19:46 108-05-4 ND ug/L 1.0 1 10/20/10 19:46 75-01-4 ND ug/L 2.0 1 10/20/10 19:46 179601-23-1 ND ug/L 1.0 1 10120/10 19:46 95-47-6 98 % 70-130 1 10/20/10 19:46 460-00-4 106 % 70-130 1 10/20/10 19:46 1868-53-7 109 % 70-130 1 10/20/10 19:46 17060-07-0 98 % 70-130 1 10/20/10 19:46 2037-26-5 Date: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, withoutthe written consent of Pace Analytical Services, Inc.. Page 14 of.25 /581cAnalytical e www.pac�tbs.com Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MPRP/7267 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 9280,078001,9280078002,9280078003,9280078004,9280078005 METHOD BLANK: 514297 Matrix: Water Associated Lab Samples: 9280078001,9280078002,9280078003,9280078004,9280078005 Blank Reporting Parameter Units Result Limit Analyzed Arsenic ug/L ND 5.0 10/21110 22:38 Cadmium ug/L ND 1.0 10/21110 22:38 Chromium ug/L ND 6.0 10/21/10 22:38 Copper ug/L ND 5.0 10/21110 22:38 Lead ug/L ND 5.0 10121110 22:38 Zinc ug/L ND 10.0 10/21/10 22:38 LABORATORY CONTROL SAMPLE: 514298 Parameter Units Arsenic ug/L Cadmium ug/L -'Chromium ug/L Copper ug/L Lead ug/L Zinc ug/L MATRIX SPIKE SAMPLE: .514299 Parameter Units Arsenic ug/L Cadmium ug/L Chromium ug/L Copper ug/L Lead ug/L Zinc ug/L SAMPLE DUPLICATE: 514300 Parameter Arsenic Cadmium Chromium Copper Lead Zinc Date: 10128/2010 10:32 AM Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 500 484 97 80-120 500 493 99 80-120 500 495 99 80-120 500 483 97 80-120. 600 492 98 80-120 500 476 95 80-120 9280078001 Spike MS IVIS % Rec Result Conc. Result % Rec Limits Qualifiers ND 500 300 60 75-125 MO 6.0 500 362 71 75-125 MO 418 500 789 74 75-125 MO 218 500 601 77 75-125 448 500 750 60 75-125 MO 493 500 843 .70 75-125 MO Units 9280078002 Result Dup Result RPD Qualifiers ug/L ND ND' ug/L ND ND ug/L 92.3 92.3 0 ug/L 31.7 32.1 1 ug/L ND 4.6J ug/L 58.9 59.0 0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc:. %% ACC04. Page 15 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. ,�aoeAnalyfical 2225 Riverside Dr. 9800 KinceyAve. Suite 100 www.pacelabs.com Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 QC Batch: MERP/3086 Analysis Method: EPA 7470 QC. Batch Method: EPA 7470 Analysis Description: 7470 Mercury Associated Lab Samples: 9280078001,9280078002,9280078003,9280078004"9280078005 METHOD BLANK: 515156 Matrix: Water Associated Lab Samples: 9280078001,9280078002,9280078003,9280078004,9280078005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND- 0.20 10/22/10 13:07 LABORATORY CONTROL SAMPLE: 515157 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers. Mercury ug/L 2.5 2.1 83 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 515158 515159 IVIS MSID 9280078001 Spike Spike IVIS MSD IVIS MSD % Rec Parameter Units' Result Conc. Conc. Result Result % Rec % Rec Limits RPD. Qual Mercury ug/L 0.26 2.5 2.5 2.3 2.3 81 130 75-125. 1 MATRIX SPIKE& MATRIX SPIKE DUPLICATE: 515160 515161 IVIS MSD 9280078002 Spike Spike MS MSD IVIS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPID Qual Mercury ug/L ND 2.5 2.5 2.2 2.2 89 87 75-125 2 Date: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 25 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA . Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 QG Batch: MSW12728 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Associated Lab Samples: 9280078001,9280078002,9280078003,9280078004,9280078005,9280078006 METHOD BLANK: 514488 Associated Lab Samples: Parameter Matrix: Water 9280078001,9280078002,9280078003,9280078004,9280078005,9280078006 Blank Reporting Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane 1,11,11-Trichloroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,11-Dichloroethane M-Dichloroethene 1,1-Dichloropropene 1,2,3-trichlorobenzene 1,2,3-Tr'ichloropropane 1,2,4-Trichlorobenzene .1,2-Dibromd-3-chloropropane 1,2-Dibromoethane (EDB) I i2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3-Dichlorobenzene 1,3-Dichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butanone (MEK) 2-Chlorotoluene 2-Hexanone, 4-Chlorotoluene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Bromobenzene Bromochloromethane Bro mod ichlorom ethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromachloromethane Dibromomethane DiGhlorodifluoromethane Diisopropyl ether Ethylbenzene I Date: 10/28/2010 10:32 AM ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug[L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L. ug/L ug/L ug/L ug/L ug/L ug[L u6/1- ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND - ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 5.0 1.0 5.0 25.0 1.0 1.0 1�0 1.0 1.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 10/20/10 12:27 10120110 12:27 10120110 12:27 10/20/10 12:27 10120/10 12:27 10/20110 12:27 10/20/10 12:27 10/20/10 12:27 10/20110 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20110 12:27 10/20/10 12:27 10/20/10 12:27 10/20110 12:27 10/20/10 12:27 10/20/10 12:27 10/20110 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20/10 12:27 10/20110 12:27 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 25 eAnalytical www.pacelabs.com Project: TEC-FaIrview Pilot Test 10/19 Pace Project No.: 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 METHODBLANK: 514488 Matrix: Water Associated Lab Samples: 9280078001,9280078002,9280078003,9280078004,9280078005,9280078006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butad.iene ug/L ND 1.0 10120110 12:27 m&p-Xylene ug/L ND 2.0 10/20/10 12:27 Methyl-tert-butyl ether ug/L ND 1.0 10/20/10 12:27 Methylene Chloride ug/L ND 2.0 10/20/10 12:27 Naphthalene ug/L ND 1.0 10/20/10 12:27 o-Xylene ug/L ND 1.0 10/20/10 12:27 p-Isopropyltoluene ug/L ND 1.0 10/20/10 12:27 Styrene ug/L ND 1.0 10/20/10 12:27 Tetrachloroethene ug/L ND 1.0 10120/10 12:27 Toluene ug/L ND 1.0 10/20/10 12:27 trans-1,2-Dichlor oethene ug/L ND 1.0 10/20/10 12:27 trans-1,3-Dichloropropene ug/L ND 1.0 10/20/10 12:27 Trichloroethene ug/L ND 1.0 10/20/10 12:27 Trichlorofluoromethane ug/L ND 1.0 10120110 12:27 Vinyl acetate ug/L ND 2.0 10120/10 12:27 Vinyl chloride ug/L ND 1.0 10/20/10 12:27 1,2-Dichloroethane-d4 (S) % 108 70-130 10/20/10 12:27 4-Bromofluorobenzene (S) % 98 70-130 10/20110 12:27 Dibromofluoromethane (S) % 105 70-130 10/20/10 12:27 Tbluene-d8 (S) % 97 70-130 10/20/10 12:27 LABORATORY CONTROL SAMPLE: 514489 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2'Tetrachloroethane ug/L 50 55.6 'I'll 70-130 1,1,1-Trichloroethane ug/L 50 54.7 109 70-130 1,1,2,2-Tetrachloroethane ug/L 50 52.0 104 70-130 1,12-Trichloroethane ug/L 50 54 ' 1 108 70-130 1,1-Dichloroethane ug/L 50 51.8 104 70-130 M-Dichloro6thene ug/L 50 50.6 101 70-132 1,1-Dichloropropene ug/L 50 50.6 101 70-130 1,2,3-Trichlorobenzene ug/L 50 52.0 104 70-135 1,2,3-Trichloropropane ug/L 50 50.9 102 70-130 1,2,4-Trichlorobenzene ug/L 50 54.0 108 70-134 1,2-Dibromo-3-chloropropane ug/L 50 50.7 101 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.7 105 70-130 1,2-Dichlorobenzene ug/L 56 52.0 104 70-130 1,2-Dichloroethane ug/L 50 54.0 108 70-130 1,2-Dichloropropane ug/L 50 50.8 102 70-130 1,3-Dichlorobenzene ug/L 50 50.8 102 70-130 1,3-Dichloropropane ug/L 50 50.6 101 70-130 1,4-Dichlorobenzene ug/L 50 51.8 104 70-130 2,2-Dichloropropane ug/L 50 56.6 113 58-145 2-Butanone (MEK) ug/L 100 97.2 97 70-145 2-Chlorotoluene ug/L 50 52.2 104 7.0-130 Date: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 18 of 26 Pace Analytical Services, Inc. /581CeAna1Xic'a1` 2225 Riverside Dr. www.pa*celabs.com Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 LABORATORY CONTROL SAMPLE: 614489 Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2-Hexanone ug/L 100 91.8 92 70-144 4-Chlorotoluene ug/L 50 54.4 109 70-130 4-Methyl-2-pentanone (MlBK) ug/L 100 10� 103 70-140 Acetone ug/L 100 102 102 50-175 Benzene ug/L 50 50.7 101 70-130 Bromobenzene. ug/L 50 51.6 103 70-130 Bromochloromethane ug/L 50 53.2 106 70-130 Bromodichloromethane ug/L 50 55.8 112 70-130 Bromoform ug/L 50 49.7 99 70-130 Bromomethane ug/L 50 55.6 ill 54-130 Carbon tetrachloride ug/L -50 58.4 117 70-132 Chlorobenzene ug/L 50 52.0 104 70-130 Chloroethane ug/L 56 49.2 98 64�134 .Chloroform ug/L 50 53.9 108 70-130 Chloromethane ug/L 50 46.8 94 64-130 cis:1,2-Dichloroethene ug/L 50 50.8 102 70-131 cis-1,3-Dichloropropene ug/L 50 56.1 112 70-130 Dibromochloromethane ug/L 50 54.7 109 70-130 Dibromomethane ug/L 50 55.5 ill 70-131 Dichlorodifluoromethane ug/L 50 55.7 ill 56-130 Diisopropyl ether ug/L 60 50.7 101 70-130 Ethylbenzene ug/L 50 53.5 107 70-130 Hexachloro-1,3-butadiene ug/L 50 53.9 108 70-130 M&P-Xylene ug/L 100 110 110 70-130 Methyl-tert-butyl ether ug/L 50 52.4 105 70-130 Methylene Chloride ug/L 50 46.4 93 63-130 Naphthalene ug/L 50 53.7 107 70-138 o-Xylene ug/L 50 54.9 110 70-130 p-lsopropyltoluene ug/L 50 54.5 109 70-130 Styrene ug/L 50 �5.5 Ill 70-130 Tetrachloroethene ug/L 50 53.6 107 70-130 Toluene ug/L 50 52.8 106 70-130 trans-1,2-Dichloroethene ug/L 50 50.2 100 70-130 trans-1,3-Dichloropfopene ug/L 50 49.8 100 70-132 Trichloroethene ug/L -50 53.1 106 70-130 Tdchlorofluoromethane ug/L 50 51.4 103 62-133 Vinyl acetate ug/L 100 120 120 66-157 Vinyl chloride ug/L 50 54.5 109 69-130 1,2-Dichloroethane-d4 (S) % 101 70-130 4-Bromofluorobenzene (S) % 104 70-130 Dibromofluoromethane (S) % 100 70-130 toluene-d8 (S) % 99 70-130 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 Qualifiers (704)875-9092 _;)ate: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS Page 19 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ACCo, oAnalyfical www.pacelabs.com Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WET114216 Analysis Method: SM 2320B QC Batch Method: SM 2320B Analysis Description: 2320B Alkalinity Associated Lab Samples: 9280078001,9280078002,9280078003,9280078004,9280078005 METHOD BLANK: 517833 Matrix: Water Associated Lab'Samples: 9280078001,9280078002,9280078003,9280078004,9280078005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 mg/L ND 6.0 10/26/10 16:20 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 517834 Spike L6S LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 mg/L - 50 50.7 101 90-110 SAMPLE DUPLICATE: 517835 9280078001 Dup Parameter Units Result Result RPD Qualifiers Alkalinity, Total as CaCO3 mg1L 15.4 15.4 0 Date: 10/2812010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. A Page 20 of 25 aceftlyfical" www.pacelabs.com Project: TEC-Fairview Pilot Test 10119 Pace Project No.: 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETA/8402 Analysis Method: EPA 300.0 QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions Associated Lab Samples: 9280078001,9280078002,9280078003,9280078004,9280078005 METHOD BLANK: 514393 Matrix: Water Associated Lab Samples: 9280078001,9260078002,9280078003,9280078004,928Oo78005 . . Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate mg/L ND 5.0 10/21/10 07:46 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 514394 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate mg/L 30 28.3 94 MATRIX'SPIKE SAMPLE: 514395 9279510005 Spike IVIS MS % Rec Parameter Units Result Conc. Result % Rec Limits Sulfate mg/L NO 30 27.1 90 MATRIX SPIKE SAMPLE: 514397 9279510006 Spike MS Parameter Units Result Conc. Result Sulfate mg/L ND 30 27.3 SAMPLE DUPLICATE: 514396 9279510005 Dup Parameter Units Result Result RPD Sulfate mg/L. ND ND SAMPLE DUPLICATE: 514398 Parameter Sulfate bate: 10/28/2.010 10:32 AM 9279510006 Dup Units Result Result mg/L ND ND Qualifiers MS % Rec % Rec Limits Qualifiers 91 Qualifiers RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. %% 1cco'* Page 21 of 25 Pace Analytical Services, Inc. 2225 Riverside Dr. aaeMalyfical Asheville, NC 28804 mvwpacefabs.com (828)254-7176 QUALITY CONTROL DATA Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: WETA/8398 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. As6ociated Lab Samples: 9280078001,9280078002,9280078003,9280078004,9280078005 METHOD BLANK: 514324 Matrix: Water Associated Lab Samples: 9280078001, 9280078002, 9280078003, 9280078004, 9280078005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.10 10/20/10 10:38 LABORATORY CONTROL SAMPLE: 514325 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 5 5.1 102 90-110 MATRIX SPIKE SAMPLE: 514326 9280078001 Spike IVIS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 6.34 5 6.2 117 90-110 M1 SAMPLE DUPLICATE: 514327 9280078002 Dup- Parameter Units Result Result RPD Qualifiers Nitrogen, Nitrate mg/L 2.7 2.7 Date: 10128/2010 10:32 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. ACCC�� Page 22 of 25 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 1�;a'ciemalyfical wwwpacelaftcom Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: T.EC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 QC Batch: WETA18403 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 9280078001,9280078002,9280078003 METHOD BLANK: 514506 Matrix: Water Associated Lab Samples: 9280078001,9280078002,9280078003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers. Chloride mg/L ND 5.0 10/20/10 13:55 LABORATORY CONTROL SAMPLE: 514507 Spike LCS LCS % Rec Parameter Units Conc. Result 61. Rec Limits Qualifiers Chloride mg/L 20 20.4 102 . 90-110 MATRIX SPIKE SAMPLE: Parameter Chloride SAMPLE DUPLICATE: 514511 Parameter Chloride Date: 10128/2010 10:32 AM 514510 9279760004 Spike Units Result Conc. mg/L 21.8 20 ..9279760004 Dup Units Result Result mg/L 21.8 21.8 IVIS MS Result % Rec 38.0 81 RPD Qualifiers 0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. % Rec Limits Qualifiers 75-125 Page 23 of 25 aneAnalytical wmpat:Wabs com Project:. TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETA/8429 Analysis Method: SM 4500-CI-E QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride Associated Lab Samples: 9280078004,9280078005 METHOD BLANK: 516946 Matrix: Water Associated Lab Samples: 9280078004,9280078005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 5.0 10/24/10 15:11 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 516947 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 21.3 107 90-110 MATRIX SPIKE SAMPLE: 516949, 9279674001 Spike MS IVIS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Chloride mg/L ND 20 24.4 107 . 75-125 SAMPLE DUPLICATE: 516948 9279674001 Dup Parameter Units Result Result Chloride mg/L ND ND Date: 10/2812010 10:32 AM RPD Qualifiers REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 24 of 25 Pace Analytical Services, Inc. 1�5a'ceAnayicalp_ 2225 Riverside Dr. www.pac0abs.com Asheville, NC 28804 (828)254-7176 QUALIFIERS Project: TEC-Fairview Pilot Test 10/19 Pace Project No.: 9280078 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if r ' eported, represents the factor applied to.the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) IVIS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference. NC - Not Calculable. U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. ANALYTE QUALIFIERS D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. ,Date: 10/28/2010 10:32 AM REPORT OF LABORATORY ANALYSIS Page 25 of 25 This report shali not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Acca" CHAIWOF'CUS'� I.Analytical'Request Document J, t fields must be completed accurately. The Chain-cf-Custody Is a LEGAL DOCUMENT. All relevan Page: of Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: 5744 Company: Report To: Attention: Qm4ew -Sit, � 1136 Addresb�j�*' C Copy To: Company Name: REGULATORY AGENCY Address: NPDES OtROUNDWATER I— DRINKING WATER LIST RCRA OTHER Email o* Purchase Order No.: Pace Quote Refere ce: AAA a ame: 713,-- tAxy4w Pace act 7roi Manager. 3t on Avh— Ph Fam. o;69_a&-*1 Requested 13UG DatOFIFAT: JProject Number Pace Profile StATE. 4 TC. 4ilte Re4q6ited.Arialysis F Co Section D matrix des E, COLLECTED Preservatives I RoquireclCileni Information MATRIX I CODE U Drinking Water DW 2 0 11 z Water WT Waste Water WW L) COMPOSME STAFt'r composrr� ENDIGRAS uJ rod P P uct Soil/Solld SL oil OL a) SAMPLE ID Wipe WP Lu z 0 (A-Z 0-9 1,-) Ar AR LL, 0 ul 0_ V a) C1 94MO-715 Sample IDs MUST BE UNIQUE Tissue TS Other OT 0 6 (L ul, z (1) , 6 %1) X IR ui Lu _1 0 0 M X: 0 N q Cc — 0 :2 _i IL ,E 0 CL 0 U) (5 z 0 to Cn 9 J� a) a) :S (2 Pace Project No./ Lab I.D. t= �C) DATE I TIME DATE TIME 7:. X z z 2 0 Id ")Q %ky, X WT WO& I A141,01 101(� 1.r+ -1 X -41 3 1 Mw Lit w-T wal i. 101,11b 99R 1k -L 1� 1111D pis .117- 7 — 41 Rw__ (0 5 !2w— 6 :191!z INAsiv- I L 9 ]10. 12 ADDITIONAL COMMENTS RELINQUISHED BY DATE TIME. ACCEPTEDBY �.AFFILIATtON DATE TIME SAMPLE CONDITIONS /10/,V Z /S-.2 r :SAMPLtA �.N . 4MEA EYSI 0 — 6. ORIGINAL z -082 Z PRINT Name of SAMPLER: E DATE Signed 12 U.2 L) M a, E Ca SIGNATURE of SAMPLER: (MMIDDNY): 'Important Note: By signing this form you am accepting Pace�s NET 30 day payment terms and agreeing to late charges of 1.5% per month for any InvolcedQfpsid .1thin 30 days. F-ALL-Q-020rev.07,15-May-2007 ---Sampre-C—onditron Upon Me-c-eipt-1 _.FkeAna1jdka1` Client Name: AAI&Ko&.J� —Project # q9 M) 7 Where Received: Huntersville XAsheviile El Eden Courier: E] Fed Ex [] UPS [] USPSXClient D Commercial El Pace OtheL Optional Custody Seal on Cooler/Box Present: 0 yes 21*'no Seals intact: El yes El no Proj. Due Date: Packing Material- E] Bubble Wrap oubble Bags D None DOther— Proj. Narne:— Thermometer Usedo�R3 ��un#1 4-648-44 Type of Ice: (S Blue None 10 Samples on ice, cooling process has begun Temp Correction Factor: Add rftbta�c �Q,�C Corrected Cooler Temp.: C Temp should be above freezing to M Biological Tissue is Frozen: Yes No Comments: Date and Initial geyson examining contents: Chain of Custody Present: Yryes 1:1 No El N/A 1 . Chain of Custody Filled Out: 2�es 0 No ONIA 2. Chain of Custody Relinquished: PTYes ONo ON/A 3. Sampler Name & Signature on COC: gryes ONo El NIA 4. Samples Arrived within Hold Time: Yfyes ONo El N/A 5. Short Hold Time Analysis (<72hr): /eyes ONo ON/A Rush Turn Around Time Requested: - OYesoNo ON/A 7. Sufficient Volume: ;Aes ONo ON/A 8. Correct Containers Used: -Pace Containers Used: /01yes ONo Xes ONo ON/A 0 N/A 9. Containers Intact: 7 /Yes ONo OWA 10. Filtered volume received for Dissolved tests . OYes ONo /ETN/A 11. Sample Labels match COC: Fely'es ONo ON/A -Includes date/time/ID/Analysis Matrix: - 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coliform,TOC, O&G, WI-DRO (water) /Yes ONo Zyes ONo OYes ;2N'o El N/A ON/A 13, Initial when completed Samples checked for dechlorination:_ "eyes DNo EINIA 14. Headspace in VOA Vials (>6mm): OYes/N. >(41 Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): 'X-s ON. ZeYes ONo NIA kNIA Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Date/Time: Comments/ Resolution: SCURF Reviewd �0 1—.1 IDate: SRIF Review: L �ZE —]Date: V Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) F-ASV-CS-03-Rev.02 APPENDIX F Photographs Pilot Test Groundwater Coloration Recovery Well RW-07