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HomeMy WebLinkAboutNC0025135_PERMIT ISSUANCE_20020415WDE:; DOCYNEM'I' .;CAMMIMK COVER :;MEET NPDES Permit: NC0025135 Huffman Finishing WWTP Document Type: Permit Issuance Wasteload Allocation Authorization to Construct (AtC) Permit Modification Complete File - Historical Compliance Speculative Limits Instream Assessment (67b) Environmental Assessment (EA) Permit History Document Date: Aril 15, 2002 This document is printed on reuse paper - ignore any content orr the reverse side Mate of North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. Ross Jr., Secretary Gregory J. Thorpe, Ph.D., Acting Director Mr. Lee T. Huffman Huffman Finishing, Inc. P.O. Box 170 Granite Falls, North Carolina 28630 Dear Mr. Huffman: NCDENR April 15, 2002 Subject: Issuance of NPDES Permit NCO025135 Huffman Finishing, Inc. Caldwell County Division personnel have reviewed and approved your application for renewal of the subject permit. Accordingly, we are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the / requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection Agency dated May 9, 1994 (or as subsequently amended.) The following modifications have been made to the permit: • The antimony limit of 1.46 mg/L has been deleted based on data submitted. No values exceeded the allowable concentration and reasonable potential analysis (RPA) calculated that the maximum predicted values were less than the allowable concentration. The final permit contains quarterly monitoring only (no limit) for antimony. • Silver monitoring has been modified to quarterly instead of monthly. Effluent data showed all values below detection level and RPA calculated that the maximum predicted value was less than the allowable concentration. • A nickel limit of 261 µg/L has been added to permit. Evaluation of effluent data showed most values below detection level, however there was one reported value of 500 µg/L. A daily maximum limit of 261 µg/L has been implemented to protect the receiving stream from acute toxicity effects. After twelve months of sampling you may request a reevaluation of the nickel data to detemune if the effluent limit should be revised. • The existing quarterly acute toxicity test at 96% has been modified to a quarterly chronic toxicity test based on a revised DWQ procedure for whole toxicity tests. The instream waste concentration for Huffman Finishing is greater than 0.25% and DWQ now applies a chronic toxicity test for dischargers that meet that criterion. The revised toxicity test will be a quarterly chronic test using Ceriodaphnia and the limit will be 0.96%. The test months will remain March, June, September and December. • BOD5_ TSS COD and sulfide limits were modified based on updated production data provided by the permittee. Modified limits are as follows and are only slightly lower than the previous limits. BOD5 = 65 pounds/day (monthly average); COD = 759 pounds/day (monthly average); BOD5 = 132 pounds/day (daily maximum) COD = 1548 pounds/day (daily maximum) TSS = 278 pounds/day (monthly average); Sulfides = 2.5 pounds/day (monthly average); TSS = 565 pounds/day (daily maximum) Sulfides = 5.2 pounds/day (daily maximum) 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone 919-733-5083/FAX 919-733-0719 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper Permit NC0025135 If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the office of Administrative Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such'a demand is made, this permit shall be final and binding. Please take notice that this permit is not transferable. The Division may require modification or revocation and reissuance of the permit. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act, or any other Federal or Local governmental permits may be required. If you have any questions or need additional information, please contact its. Jacquelyn Nowell at telephone number (919) 733-5083, extension 512. Sincerely, priginal Signed BY David A. Goodrich Gregory J. Thorpe, Ph.D. cc: Central Files Asheville Regional Office / Water Quality Section Roosevelt Childress, EPA Region IV N_PDES.Uitit/,P,emut File - Aquatic Toxicology Unit Permit NCO025135 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY PERMTI TO DISCHARGE WASTEWATER UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Huffman Finishing Company, Inc. is hereby authorized to discharge wastewater from a facility located at the Huffman Finishing Company U.S. Highway 321 southeast of Granite Falls Caldwell County to receiving waters designated as the Catawba River (Lake Hickory) in the Catawba River Basin in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV hereof. This permit shall become effective May 1, 2002. This permit and authorization to discharge shall expire at midnight on March 31, 2005. Signed this day April 15, 2002. Original Signed By David A. Goodrich Gregory]. Thorpe, Ph.D., Acting Director Division of Water Quality By Authority of the Environmental Management Comtnission Permit No. NC0025135 SUPPLEMENT TO PERMIT COVER SHEET Huffman Finishing Company, Inc. is hereby authorized to: Continue to operate an existing 0.250 MGD wastewater treatment facility consisting of a manual lint screen, manual trash screen, a flow equalization basin with four floating aerators, lift pumps, an oxidation ditch, a circular clarifier, sludge recirculation pumps, a chlorine contact tank, ultrasonic flow measurement, chemical dechlorination, cascade post aeration, aerobic sludge digestor, sludge holding lagoon, sludge thickener, sludge drying beds and auxiliary power located at Huffman Finishing Company Wastewater Treatment Plant, a site on US Highway 321, southeast of Granite Falls, Caldwell County, and 2. Discharge from said treatment works at the location specified on the attached map into the Catawba River (Lake Hickory), which are classified WS-IV CA waters in the Catawba River Basin. LJ IRS !� i+ �... / � i` '. � 1 � `�//� tom! � � � �J � � •�\ •\\\, \\\ � �1 \' , � ^1', � l ,, i 1 i rJ I —i �i i r! 1+ J r � •Y(i . � y • � i �( \�:�— l :- 4 "yy\ \� 1 1 P)1 \ Facility Information Facility Latitude: 35045'34" Sub -Basin: 03-08-32 `' Location Longitude: 81023'49" Quad k: D13SW Stream Class: C NSW Huffman Inc. Receiving Stream: Catawba River (Lake Hickory) qqqq // NFinishing, C0025135 Per Flow: 0.250 MGD //o rth Caldwell County A. (1). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS -FINAL Permit No. NC0025135 During the period beginning upon the effective date of the permit and lasting until expiration, the Pennittee is authorized to discharge from outfall serial number 001. Such discharges shall be limited and monitored by the Pennittee as specified below: EFFLUENT CHARACTERISTICS LIMITS MONITORING REQUIREMENTS on y Average Daily Maximum Measurement Frequency Sample Type Sample Location FlowContinuous Recorder or ay, ay s ay —__-77VVe_eF— Total Suspendedo t s 278 lbsJday ay ee ra s ay s ay ee ompost e otal Chromium 1.3 lbsiday ay ee y ompost e Sulfides ay ay Weekly Urab Phenols ug ee y ra vecal colitorm (geometric mean m m ee ra otal Antimony ua ery ompost e otal Arsenic ----Qua ery ompost e _Wtal Barium ua ery ompost e -Total a mium ua e y ompost e -Chloride Uuarterly Composite -1 otal Copper ua e y Composite -1 otal Cyanide ua ery ra . - uon a ua e y ompost e jotal Leadua ery ompost e as on y ompost e otal Nickelug ee y ompost e pH3/Week Grab otal Silver on y Composite . o a inc ua ery ompost e otal Nitrogen + NO3+ on y ompost e otal Phosphorus on y omposi e Total esi uaChlorine on ra empera ure ee ra Chronic Toxicity ua ery ompost e Notes: r Sample locations: E - Effluent, I - Influent Y The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units. 3 Chronic toxicity (Ceriodaphnia) P/F@ 0.96%; March, June, September, and December. See Special Conditions A (2) of the Supplement to Effluent Limitations. There shall be no discharge of floating solids or foam in other than trace amounts. Permit No. NCO025135 ` SUPPLEMENT TO EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS SPECIAL CONDITIONS A (2). CHRONIC TOXICITY PERMIT LIMIT (QUARTERLY) The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to Cenodaphnia dubia at an effluent concentration of 0.96 %. The permit holder shall perform at a minimum, ouarrerlu monitoring using test procedures outlined in the "North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or "North Carolina Phase 11 Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. The tests will be performed during the months of March, June, September, and December. Effluent sampling for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes. If the test procedure performed as the fast test of any single quarter results in a failure or ChV below the permit limit, then multiple -concentration testing shall be performed at a minimum, in each of the two following months as described in "North Carolina Phase 11 Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. The chronic value for multiple concentration tests will be determined using the geometric mean of the highest concentration having no detectable impairment of reproduction or survival and the lowest concentration that does have a detectable impairment of reproduction or survival. The definition of "detectable impairment," .collection methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase 11 Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP313 for the pass/fail results and THP313 for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the following address: . Attention: Environmental Sciences Branch North Carolina Division of Water Quality 1621 Mail Service Center Raleigh, North Carolina 27699-1621 Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Branch no later than 30 days after the end of the reporting period for which the report is made. Test data shall be complete, accurate, include all supporting chemical/physical measurements and all concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Branch at the address cited above. Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be required during the following month. Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an invalid test and will require immediate follow-up testing to be completed no later than the last day of the month following the month of the initial monitoring. State of North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. Ross,.Jr.,.Secretary Gregory J. Thorpe, Ph.D.; Acting Director March 25, 2002 MEMORANDUM To: Jerry R. Freeman $?8 2S/ 083 NC DENR / DEH / Regional Engineer Asheville Regional Office From: Jackie Nowell NPDES Unit Subject: Review of Draft NPDES Permit NCO025135 Huffman Finishing Company Caldwell County ern NCDENR VI�DN(il)=N2Nd NAfRJ ED APA 1 ODU 202 DENR - WATER QUALITY POINT SOURCE BRANCH Please indicate below your agency's position or viewpoint on the draft permit and return this form by April 8, 2002. If you have any questions on the draft permit, please contact me at the telephone number or e-mail address listed at the bottom of this page. /W M/M�M�M//W /N//�/J/W/JJM/I�/J/N//JJ�/JM//�/J/JJNJrN///J/W/•/J�NM�M�NJNJM�M//W/�V//�//WIN//�/J/JJ/N//�/�IJJM/. /WNJM�M�/�N/WIW/JJM//W/W/JJM//W/JV/W/W/VJM/nN/�JNV/W/WM•IWM//NINJ/W//V/�/�///J/v`/NV/�/J/JJNJNJM•M� RESPONSE: (Check one) ❑Concur with the issuance of this permit provided the facility is operated and maintained properly, the stated effluent limits are met prior to discharge, and the discharge does not contravene the designated water quality standards. Concurs wh iss ante of he above permit, provided the follo in co ditions are met: �t � -r f s IN r YZ ❑ Opposes the issuance of the above permit, based on reasons stated below, or attached: Tuhii 9. P-urAuN •x pwq t `_ o .k.t:.� -1� �;(�� F ,I ��xP 5 n-.>�P w i,rw ��f� r �j,� , 16177M,ail Service Center Ralegh Nfarthcarolira 2 991617� {'� 919 733 5083je tension 512 a (faz) 919 733 9919 " * ' xVISR US ON THE INfERNET_fr ,,I/h20enr itatenc`iaMPDES"fw 1R2 aelue Navell �rrcmad nel A UNITED STATES ENVIRONMENTAL PROTECTION AGENCY <� hen yw REGION 4 ATLANTA FEDERAL CENTER 61 FORSYTH STREET �ir�( PROSE�4 ATLANTA, GEORGIA 30303-8960 FEB 0 8 2002 Mr. Dave Goodrich, Supervisor NPDES Unit Division of Water Quality North Carolina Department of Environment and Natural Resources 1617 Mail Service Center Raleigh, NC 27699-1617 SUBJ: NPDES Permit for Huffman Finishing Inc. Permit No. NCO025135 Dear Mr. Goodrich: p � 9 � p ' ID FEB 14 2ow Gc'•{-ER OtIALITY 1 P---_ G"tT_ SGURGE BRANCH In accordance with the EPAINCDENR MOA, we have completed our review of the draft permit referenced above and have no objections to the proposed permit conditions. We request that we be afforded an additional review opportunity only if significant changes are made to the permit prior to issuance, or if valid and significant comments to the permit are received. Otherwise, please send us one copy of the final permit when issued. If you have any questions, please call Ms. Dee Stewart at (404) 562-9334. Sincerely, Scott Gordon, Chief Permits, Grants and Technical Assistance Branch Water Management Division Internet Address (URL) a http://www.spa.gov RacyclodlRecyclable • Primed with Vegetable 01 Based Inks on Reqded Paper (Mlnknum 30% Postconsumer) [Fwd: 3 no comment letters are going out today to] Subject: ]Fwd: 3 no comment letters are going out today to] Date: Fri, 08 Feb 2002 13:35:30 -0500 From: Dave Goodrich <dave.goodrich@ncmail.net> To: Tom Belnick <Tom.Belnick@ncmai1.net>, Jackie Nowell <Jackie.Nowell@ncmail.net> Tom and Jackie - Please proceed with issuance of Erwin (Tom) and Huffman Finishing (Jackie). Thank you, Dave Subject: 3 no comment letters are going out today to Date: Fri, 08 Feb 2002 10:04:00 -0500 From: Flyatt.Marsball@epamail.epa.gov To: dave.goodrich@ncmail.net, mike.templeton@ncmail.net, mike.myers@ncmail.net, Susan.A.Wilson@ncmail.net either Dave or Tom Belnick for Huffman Finishing, Yorkshire Farms, and Erwin. I of 1 2/8/02 2:46 PM Comments on Huffman Finishing Subject: Comments on Huffman Finishing Date: Tue, 26 Feb 2002 15:33:05 -0500 From: Jackie Nowell <jackie.nowell@ncmail.net> Organization: NC DENR DWQ To: Jim Reid <Jim.Reid@ncmail.net> Hello Jim, Thanks for sending your comments on Huffman, however based on the information that was analyzed at the time of permit renewal, we are going to maintain the limits and monitoring frequencies originally recommended. Item #1 - ARO recommends no monitoring for antimony. NPDES has deleted the previous weekly limit for antimony based on the reasonable potential analyses which shows no potential for exceeding the standard instream. However, because there were detectable amounts of antimony in the effluent, we are recommending minimal quarterly monitoring so that there will be some data to evaluate at the next permit renewal. Item #2 - ARO recommends quarterly Ni monitoring. The results of the RPA indicated that a Ni limit should be given. There were 35 datapoints used in the analysis, with 13 hits for nickel,the highest value was 500 ug/l. We received no info that this was not a valid datapoint and it remained a part of the RPA. We recommend a nickel limit be placed in the permit. After twelve months of sampling, the facility may request that DWQ re-evaluate the nickel data and determine if a limit is still appropriate. The NPDES unit received approval from EPA on Feb. 14, 2002 to issue the Huffman permit with our recommended limits. 1 of 1 2/26/02 4:33 PM 02/13/2002 I1:19 4 INSTR AM MONITORING REOUIREMEN', InsLrt:a n monitoring is not required for t PAGE 01 Post -It' Fax Nole 7671 Date w of To C *i A,41 P From /r7 ca. c o Pho.w w rnm.; « y ��77 FAX �!` Fax PROM ED CHANGES: The fa lowing modifications have been made to the permit: I. W recommend antimonyUV* of 1.46 tag/1 be deleted based on data submitted. Re fewed 125 observations with oal91 7 valnea with detectable values. No values cx eeded the .allowable coaCsatr u n and reasonable• potenfial, analyslo (RPA) calculated that the maximum preddfeted values were less than the allowable concentration. Recommend quarterly monitoring for antimony. 2. Re'commend that silver be monitored auarterly instead of monthly. Evaluation of effluent data had all values below det all level and RPA Calculated that the max. predicted value was less than the �Ll>o�vable oonoentration. Recommend reduction in 3. Recommend that nickel limit of 26L UM/1 IEPA'o Ya FAVI be added to permit. Evaluation of effluent data had most values below detection lever, however there was one reported value of 500 ug/l. RPA calculated that the max. predicted value of 3605 ug/1 was greater than the allowable concentration of 2605 ug/1. Based on DWQ procellure of limits and monitoring for cyanide and metals (memo April 28, 1999) because the allowable concentration of 2605 ug/1 In greater than the Ya FAV, will roeorctuneud Ya FAV as the dilly maximum limit so that acute toxicity can be protepted instream. Rocommend a nlokel limit be added to the permit and be moni�ored weekly. 4. Recox aLmend modification Of limits for RODS, TSS, COD, and sulfide based on updated calculation of these limits from AppUcable eMuent guidelines are 40 CFR 410.92 (Subpart E, Knit Fabric). Modified limits are as follows and Huffman should be able comp y with limits, these limits am only slightly leas than the existing limits and exists ng effluent data indicates that Huffman in discharging well below the permitted limitz for BOD5; TSS'kiind COD. See effluent guldolinessection of faetsheet for actual = 65 lbs/day (mo. avg.); = 131.7 Ibs/day (da. mam) COD # 759 lbs/day (mo. avg-): COD $ 1548 lbs/day (da. max.) TS13 1 275.8 + 1.8 = 277.6 lba/day (mo. avg.); TSS 562.4 + 2.7 = 565.1 lbe/day (da. max.) = 0.1 * 25.3 - 2.5 lbs/day (mo. avg.); = 0.2 * 25.9 = 5.2 lbs/day (da. max.) PROPOSEO SCI IEDULE FOR PERMIT IS8UAN Dral'I Pcri�ut to Public Notice: 06/13/2001 PVT wit Scl4eduled to Issue: 0810612001 SPATE CO TAt.T: Ir ynu ha e any questions on any of the above information or on the attached permit, please contact J< ckie Nowell at (919) 733-5083 ext. 512. Herrman Finishing Inc. Fact SMaa. NPDES Re, newel P„ge 4 4 PAGE 02 02/13/2002 11:19 Dooj f r1l�ni�u2 'Coles 7gn��mo� �' f'��Cuov>.mCrUl�' '/Vj.. 4�—, >rr l o l Y7 e I U 6 wl fl y mO r7�: ti NAME" NPDRR RUPRP NAME.: e is La If Fini,hit) g Inc. FSC1!,tzo NPDES Renewal Page F. PUBLIC NOTICE �I NORTH CAROLINA, STATE OF 1 IORTH CAROLINA " CALDWELL COUNTY, -NVIRONMENTAL AFFIDAVIT OF PUBLICATION MANAUtmmml ti COMMISSION/. Before the undersigned, a Notary Public of said NPDES UNIT 1617 MAIL SERVICE) County and State, duly commissioned, qualified, and CENTER authorized by law to administer oaths, personally RALEIGH, NC 27699-1617 NOTIFICATION OF appeared ... Elaine .KUPfel. ................. that INTENT TO ISSUE I being first du ly sworn, deposes and says: A NPDES who WASTEWATER Advertising Director .. PERMIT , . , ... On the � basis of thor- staff review I he is ....................... . of Lenoir Newspapers, Inc., engaged in the publication ough And application of 1 General Statute 1 ub- of a newspaper known as Lenoir News -Topic, t class mail in the .NC 143.21, Public law 92-500 and other lished, issued, and entered as second in said County and State; that he is lawful standards City of Lenoir, this affidavit and sworn state - and regulations, the. authorized to make legal advertisement, a North Carolina Envi-' 1 ment; that the notice or other published ronmental Manage- true copy of which is attached hereto, was rrient Commission proposes to issue a 1 in Lenoir News -Topic on the following dates: 1'i National Pollutant Discharge Elimina- tion System June.19................................ (NPDES) Wastewa- ter discharge permit i.to the person(s) list- i ed below effective 1 45 days from .the and that the said newspaper in which such notice, publish date of this ! paper, document, or legal advertisement was published notice. was, at the time of each and every publication, a Written comments re- garding the pro- I newspaper meeting all of the requirements and quali- posed permit will be f Section 1-597 of the General Statutes of accepted until 30tications o I Idays after the pub- of North Carolina and was a qualified newspaper within lish date of this no-, the meaning of Section 1-597 of the General Statutes that date comments received to I of North Carolina. receivedd are Prior - �01 sidered in the finale .., determinations' re-� This .....19th.,....dayof .....June.... garding the pro- posed permit. TheG< 5?�`� Director of the NC 11, Division of Waterl may decide , ;, Sworn to and subscribed before me, this ...19th.... ZJ to P�.,joln a public' for the pro- June"' .. day of ............... ermit should w the Diviston receive a significant degree "' of public ir�lerest. Notary Public Copies of the ' draft FEB to '05 ............... „o.,,,,a,,,glyl.- -+��• My Commission expires: . DENR/ DWQ U FACT SHEET FOR NPDES PERMIT DEVELOPMENT NPDES No. NCO025135 Facility Information Applicant Facility Name: Huffman Finishing Company, Inc. Applicant Address: P.O. Box 170 Granite Falls, N.C. 28630 Facility Address: 4919 Hickory Boulevard Permitted Flow 0.250 MGD Type of Waste: Industrial and Domestic Facility/Permit Status: Renewal Facility Classification II County: Caldwell Miscellaneous Receiving Stream: Catawba River Lake Hickory) Regional Office: - Asheville Stream Classification: WS-IV CA USGS Topo Quad: D13SW/Granite Falls, N.C. 303 d Listed?: No Permit Writer: Jackie Nowell Subbasin: 03-08-32 Date: June 5, 2001 Drainage Area mil : 1090 " tE. Summer 7Q10 (cfs) 40 (min. inst. Release Winter 7Q10 (cfs): NA'ac Aver* e Flow (cfs): NA I % : 0.96 Primary SIC Code: 2252 Huffman Finishing Inc. is a textile plant that manufactures hosiery and has requested renewal of existing NPDES permit. Applicable effluent guidelines are 40 CFR 410.52 (Subpart E, Knit Fabric). The facility has a design flow of 0.250 MGD and its wastewater is 95% textile dye and bleach process and 5% domestic. The plant discharges into the Catawba River (Lake Hickory), approximately 2.5 miles below Rhodhiss Dam. This segment of the Catawba River (Lake Hickory) is a class WS-IV CA waterbody, in CTB32 subbasin. The relocation for direct discharge into Lake Hickory was effective April 1, 1997. The outfall is approximately one mile (-6000 ft.) downstream of the water supply intake for the City of Hickory. Prior to relocation, Huffman Finishing discharged into a small tributary to the Catawba River. Previous permits had effluent pages for both locations. This renewal will have limits and monitoring requirements for the Catawba River (Lake Hickory) location only. The Catawba River (Lake Hickory) is not listed on North Carolina's 2000 303(d) list. The use support rating for this segment (from Rhodhiss Dam to U. S. Highway 321) is fully supporting. Existine Effluent Limits for Huffman Finishin¢ Inc. At the Catawba River (Lake Hickory) discharge point Qw = 0.250 MOD BOD5 = 68.5 lbs/day (mo. avg.); 135.8 lbs/day (da. max.) COD = 790.0 lbs/day (mo. avg.); 1581.8 lbs/day (da. max.) TSS = 290.0 lbs/day (mo. avg.); 578.71bs/day (da. max.) Sulfides = 2.6 lbs/day (mo. avg.); 5.3 lbs/day (da. max.) Chromium = 1.3 lbs/day (mo. avg.); 2.6 lbs/day (da. max.) Phenols = 20.0 µg/l (daily max.) Antimony = 1.46 mg/l Fecal Coliform = 200/ 100ml (mo. avg.); 400/ 100ml (da. max.); pH = 6-9 SU Monthly monitoring for NH3, nickel, silver, TP and TN. Twice monthly monitoring for total residual chlorine. Huffman Finishing Inc. Fact Sheet NPDES Renewal Page I Quarterly monitoring for arsenic, barium, cadmium, chloride, copper, cyanide, fluoride, and lead. Acute Toxicity (Daphnid 48 hour) LC50 c@i 96%; March June September December DEVELOPMENT OF EFFLUENT GUIDELINES: Applicable effluent guidelines are 40 CFR 410.52 (Subpart E, Knit Fabric) Developed BPT limits using year 2000 production values of 25812 pounds for daily maximum value or 25.8 #/ 1000 lbs; monthly avg. value of 25340 pounds or 25.3 #/ 10001bs. (monthly avg. value derived by using highest monthly production value for past three years of 557,485 pounds per day/ 22 days of production in June 2000). Pounds of production for 1998, 1999, and 2000 was provided by Huffman Finishing. New effluent BPT guidelines developed were: BODS = 2.5 * 25.3 = 63.2 lbs/day (mo. avg.); BODS = 5.0 * 25.8 = 129 lbs/day (da. max.) Must add guidelines for sanitary wastewater for BODS Huffman Finishing has 5% sanitary wastewater and 95% industrial wastewater. Avg. wasteflow for 2000 was 0.1445 MGD, 5% _ 0.007225 MGD BODS = 30 mg/l * 8.34 * 0.007225 MGD = 1.8 lbs/day (mo. avg.); BODS = 45 mg/l * 8.34 * 0.007225 MGD = 2.7 lbs/day (da. max.l BODS = 63.2 + 1.8 = 65 lbs/day (mo. avg.); BODS = 129 + 2.7 = 131.7 lbs/day (da. max.) COD = 30 * 25.3 = 759 lbs/day (mo. avg.); COD = 60 * 25.8 = 1548 lbs/day (da. max.) TSS = 10.9 * 25.3 = 275.8 lbs/day (mo. avg.); TSS = 21.8 * 25.8 = 562.4lbs/day (da. max.) Must add guidelines for sanitary wastewater for TSS Huffman Finishing has 5% sanitary wastewater and 95% industrial wastewater. Avg. wasteflow for 2000 was 0.1445 MGD, 5% _ 0.007225 MGD TSS = 30 mg/l * 8.34 * 0.007225 MGD = 1.8 lbs/day (mo. avg.); TSS = 45 mg/l * 8.34 * 0.007225 MGD = 2.7 lbs/day Ida. max.) TSS = 275.8 + 1.8 = 277.6 lbs/day (mo. avg.); TSS = 562.4 + 2.7 = 565.1 lbs/day (da. max.) Sulfides = 0.1 * 25.3 = 2.5 lbs/day (mo. avg.); Sulfides = 0.2 * 25.8 = 5.2 Ibs/day (da. max.) Chromium = 0.05 * 25.3 = 1.3 lbs/day (mo. avg.); Chromium = 0.1 * 25.8 = 2.6 lbs/day (da. max.) Phenols = 0.05 * 25.3 = 1.3 lbs/day (mo. avg.); Phenols = 0.1 * 25.8 = 2.6 Ibs/day (da. max.) 1.3 lbs/day 18.3410.250 = 0.623 mg/l or 623 ugll 2.6 lbs/day 18.3410.250 = 1.247 mg/1 or 1247 ug/1 Allowable concentration of Phenols = 20.0 pg/l (daily max.) - based on protection of water quality standard ***Will recommend WQ based limit for phenols = 20 ug/l instead of effluent guideline REASONABLE POTENTIAL ANALYSIS: Analysis was performed on 1999 and 2000 data, antimony, arsenic, barium, cadmium, chloride, copper, cyanide, fluoride, lead, nickel, silver, zinc and phenols. Results indicated that only a nickel limit was needed based on maximum predicted concentration of 3650 ug/I was greater than the allowable concentration Of 2605 ug/l. All other parameters maximum predicted values were below the allowable concentrations and no limits are needed. 1) Will recommend antimony limit of 1.46 mg/l be deleted based on data submitted. Reviewed 125 observations with only 7 values with detectable values. None exceeded Huffman Finishing Inc. Fact Sheet NPDES Renewal Page 2 the allowable concentration and maximum predicted values were less than the allowable concentration. Recommend quarterly monitoring for antimony. 2) Will recommend continued quarterly monitoring for arsenic, barium, cadmium, chloride, copper, cyanide, fluoride, and lead. 3) Recommend that silver be monitored quarterly instead of monthly. 4) Recommend that nickel limit of 261 ug/1 jEPA's Y2 FAV) be added to permit. Evaluation of effluent data had most values below detection level, however there was one reported value of 500 ug/l. RPA calculated that the max. predicted value of 3605 ug/1 was greater than the allowable concentration of 2605 ug/l. Based on DWQ procedure of limits and monitoring for cyanide and metals (memo April 28, 1999) because the allowable concentration of 2605 ug/1 is greater than the Y2 FAV, will recommend Y2 FAV as the daily maximum limit so that acute toxicity can be protected instream. 5) Recommend continuation of phenols limit of 20 ug/l. The phenols limit is water quality based and was the limit at Huffman's old discharge point (UT Catawba River). Upon relocation to the current discharge point directly into Lake Hickory, the limit was maintained based on an agreement between DWQ and the Division of Environmental Health (DEH). There are two municipal water intakes located just downstream of Huffman's discharge. DEH believes special consideration is needed because of the complex hydraulics of Lake Hickory during various flow conditions and the uncertain impacts this may have on the two downstream intakes. TOXICITY TESTING: Current Requirement: Acute Toxicity (Daphnid 48 hour) LC50 n 96%; March June September December Recommended Requirement: Chronic Toxicity (Ceriodaphnial (i� 0.96%; March June September December per DWQ memo (August 1999) - per Whole Effluent Toxicity permit limits and monitoring requirements. If facility's IWC > 0.25%, the facility will perform the Chronic Whole Effluent Toxicity Test Procedure or subsequent versions on a quarterly basis. The limit will be stated as "shall at no time exhibit observable inhibition of reproduction or significant mortality" at the effluent concentration equivalent to the facility's IWC. Huffman had a toxicity problem in 1996 with seven FAILs of the limit. In 1997, there were four (4) PASS, two (2) FAILs and one "no report". Improvement started in July 1997 with no more FAILs until March 1999 which was followed by eight PASSes. In March 2001, there was a bad test. Tel 3F"J9r:NCeTD& krJiLiii•1 January through March 2001, Avg. Qw = 0. 1197 MGD (approximately 58% of capacity), BOD5=2.34 lbs/day, TSS=8.2 lbs/day, COD=56.5 lbs/day, TN=12.4 mg/ and TP=4.23 mg/l. There was sulfide violation in January. In 2000, Avg. Qw = 0. 1445 MGD (approximately 58% of capacity), BOD5=5.26 lbs/day, TSS=12.4 lbs/day, COD=108.4 lbs/day, TN=14.3 mg/ and TP=5.17 mg/l. There was sulfide violation in December. This was the first violation since 1998. In 1999, Avg. Qw = 0. 156 MGD (approximately 62% of capacity), BOD5=5.21lbs/day, TSS=15.8 lbs/day, COD=93.6 lbs/day, TN=13.8 mg/ and TP=6.72 mg/l. In 1998, Avg. Qw = 0. 1638 MGD (approximately 65% of capacity), BOD5=6.33 lbs/day, TSS=24.3 lbs/day, COD=143.6 lbs/day, TN=26.0 mg/ and TP=9.56 mg/l. There were four (4) sulfide violations in June, October, November and December. Correspondence File: 3/ 17/97 - Huffman Finishing completes extension of outfall directly to Lake Hickory 10/ 15/98 - ARO requests remission in amount of 50% of assessment as a result of factors beyond the permittee's control - sulfide violation, sample bottle broken, average based on 3 samples instead of 4 9/ 18/98 - NOV and civil assessment-$1153.00 - sulfide violation 5/22/98 - Compliance Sampling Inspection - In compliance Huffman Finishing Inc. Fact Sheet NPDES Renewal Page 3 INSTREAM MONITORING REQUIREMENTS: Instream monitoring is not required for this discharger. PROPOSED CHANGES: The following modifications have been made to the permit: 1. Will recommend antimony limit of 1.46 mg/l be deleted based on data submitted. Reviewed 125 observations with only 7 values with detectable values. No values exceeded the allowable concentration and reasonable potential analysis (RPA) calculated that the maximum predicted values were less than the allowable concentration. Recommend quarterly monitoring for antimony. 2. Recommend that silver be monitored quarterly instead of monthly. Evaluation of effluent data had all values below detection level and RPA calculated that the max. predicted value was less than the allowable concentration. Recommend reduction in monitoring frequency from monthly monitoring to quarterly monitoring for silver. Recommend that nickel limit of 261 ug/l (EPA's Y, FAV) be added to permit. Evaluation of effluent data had most values below detection level, however there was one reported value of 500 ug/l. RPA calculated that the max. predicted value of 3605 ug/l was greater than the allowable concentration of 2605 ug/l. Based on DWQ procedure of limits and monitoring for cyanide and metals (memo April 28, 1999) because the allowable concentration of 2605 ug/l is greater than the Y2 FAV, will recommend Y, FAV as the daily maximum limit so that acute toxicity can be protected instream. Recommend a nickel limit be added to the permit and be monitored weekly. 4. Recommend modification of limits for BOD5, TSS, COD, and sulfide based on updated calculation of these limits from Applicable effluent guidelines are 40 CPR 410.52 (Subpart E, Knit Fabric). Modified limits are as follows and Huffman should be able comply with limits, these limits are only slightly less than the existing limits and existing effluent data indicates that Huffman is discharging well below the permitted limits for BOD5, TSS, and COD. See effluent guidelines section of factsheet for actual calculation. BOD5 = 65 lbs/day (mo. avg.); BOD5 = 131.7 lbs/day (da. max.) COD = 759 lbs/day (mo. avg.); COD = 1548 lbs/day (da. max.) TSS = 275.8 + 1.8 = 277.6 lbs/day (mo. avg.); TSS = 562.4 + 2.7 = 565.1 lbs/day (da. max.) Sulfides = 0.1 * 25.3 = 2.5 lbs/day (mo. avg.); Sulfides = 0.2 * 25.8 = 5.2 lbs/day (da. max.) PROPOSED SCHEDULE FOR PERMIT ISSUANCE: Draft Permit to Public Notice: 0611312001 Permit Scheduled to Issue: 0810612001 STATE CONTACT: If you have any questions on any of the above information or on the attached permit, please contact Jackie Nowell at (919) 733-5083 ext. 512. NAMR-Jew,A 1 \ r)ATP- i0/IZ/b/ Finishing Inc. F NPDES Renewal Page 4 TOXICANT ANALYSIS acility Name huffman finishing NPDES # NC0025135 _ Qw (MGD) 0.25 _ 7Q10s (cts) 40 _ / WC (%) 0.96 _ c'ving Stream catawba Make hickory_ Stream Class WS-IV CA _ FINAL RESULTS Antimony _ ax. Pred Cw 189 ug/ Allowable Cw 1459.2 ug/ Max. Valuel 135 Arsenic _ ax. Pred Cw 222 ug/ Allowable Cw 5211.3 ug/ Max. Value 30 Barium __ ax. Pred Cw 65 ug/ Allowable Cw 104225.8 ug/ Max. Value 26 _ Cadmium ax. Pred Cw 29.4 ug/ Allowable Cw 208.5 ug/ Max. Value 6— Chloride ax. Pred Cw Allowable Cw 1080000 26056451.6 ug/ ug/ Max. Value 432000 Copper _ ax. Pred Cw 237.6 ug/ Allowable Cw 729.6 ug/ Max. Value 132 Cyanide _ ax. Pred Cw 2.5 ug/ Allowable Cw 521.1 ug/ Max. Value 2.5 Fluoride _ ax. Pred Cw 2550 _ ug/ Allowable Cw 187606.5 ug/ Max. Value 1700 Lead _ ax. Pred Cw 18.75 ug/ Allowable Cw 2605.6 ug/ Max. Value 7.5 Nickel _ -ax-Rred'Cw,) r-3650 _ ug/ Allowable Cw _ 2605.6 ug/ Max. Value 500 Silver _ ax. Pred Cw 3.3 ug/ Allowable Cw 6.3 ug/ Max. Value 3 Zinc _ ax. Pred Cw 1204.2 ug/ Allowable Cw 5211.3 ug/ / 2 , O Af, VAl".r/ µ/ v4vt alL7� ctl y 6✓inrot LkcLt!! a/lw..�lL c..,c, < odw�b/L N•6f. ladi$WLJL1ee#Y,/W�/ ,11k./ < 4/1.w,41' /L✓L/ llm5,, /✓.k.t okwL dtk /w nHc. 4 <, A«"L trLLa eYI"4 /*rot 4�c o41 !/wt. c, �qK, pvl. < 4l(•-.�h // 66-r,/ A4K, Aj./C A!/ ✓ 4L, 64/w�o�./W i�... // a(,{/ MAk�. < y(/w+fi It Lox, �ic d. < ���%i44L 9FEvdtAQ A 4 L/. Max. Value 669� ,i'o4r N// !it/— da% 6/7/01 TOXICANT ANALYSIS ammeter= Antimony P Standard= 14 pg/I n BDL=1/2DL tual Data RESULTS 1/00 1 12.6 <25 Std Dev. 12.552441 2 12.5 <25 Mean 14.856 3 12.5 <25 C.V. 0.84494083 4 12.5 <25 5 12.5 <25 l 6 12.5 <25 Mult Facto 1.4 7 12.5 <25 Max. Value 135 pg/ 8 12.5 <25 Max. Pred C 189 pg/ 9 12.5 <25 Allowable C 1459.16 pg/ 10 12.5 <25 11 12.5 <25 12 12.5 <25 13 12.5 <25 14 12.5 <25 15 12.5 <25 16 12.5 <25 17 12.5 <25 18 12.5 <25 19 12.5 <25 20 12.5 <25 21 12.5 <25 22 12S <25 23 12.5 c25 24 12.5 <25 25 12.5 <25 26 12.5 <25 27 12.5 <25 28 12.5 <25 29 12.5 <25 30 12.5 <25 31 12.5 <25 32 12.5 <25 33 12.5 <25 34 12.5 <25 35 12.5 -25 36 12.5 <25 37 12.5 <25 38 12.5 <25 39 12.5 <25 40 12.5 -25 41 12.5 <25 42 12.5 -25 43 12.5 <25 44 12.5 <25 45 12.5 <25 46 12.5 <25 47 12.5 25 J 48 12.5 - <25 - 49 12.5 <25 50 12.5 <25 51 12.5 -25 52 12.5 <25 12/99 53 12.5 25 54 12.5 <25 55 12.5 <25 56 12.5 <25 57 12.5 <25 58 12.5 <25 59 12.5 <25 60 12.5 <25 61 12.5 <25 62 12.5 <25 63 12.5 <25 64 125 <25 65 12.5 <25 66 12.5 <25 67 12.5 <25 68 12.5 <25 69 12.5 <25 70 12.5 <25 71 2.5 <25 72 2.5 <25 6r7101 TOXICANT ANALYSIS 73 12.5 <25 _ 74 12.5 <25 75 12.5 <25 76 1.5 <3 _ 77 12.5 <25 78 12.5 <25 79 12.5 <25 80 12.5 <25 81 12.5 <25 82 12.5 <25 83 2.5 <25 25 <50 25 <50 _ A86 12.5 <25 12.5 <25 12.5 <25 2.5 <25 492 12.5 <25 12.5 <25 12.5 <25 12.5 <25 94 10 <20 95 12.5 <25 96 12.5 <25 97 12.5 <25 98 12.5 <25 99 12.5 <25 100 12.5 <25 101 12.5 <25 102 12.5 <25 103 12.5 <25 104 12.5 <25 105 12.5 <25 106 30 30 107 27 27 108 31 31 109 66 66 110 31 <62 111 12.5 <25 112 32 32 113 31 31 4 135 135 115 12.5 <25 116 12.5 <25 117 12.5 <25 118 12.5 <25 119 12.5 <25 120 12.5 <25 _ 121 12.5 <25 122 12.5 <25 123 12.5 <25 124 12.5 <25 125 12.5 <25 6/7/01 TOXICANT ANALYSIS ameter=lArsenic Paramete, Barium I Parameter =lCadmium l Parameter -I Chloride) 11 1 P andard= 50 pglI _ I_'standard, = 1000 ygll Standard= 2 yg/I Standard= 25MW Pgn I I n DL=II2DItual Data RESULTS. n DL=12DIntual Dat RESU LTS-.' n DL=120C Gual 0at93ESULTS _ n DL=1/2DLctual Data RESULTS 1 2.5 <5 Std Dev. 8.23518 1 10 <20 Bid Dev. 6.351002071 1 11,2 Std De, 1.50755] 11 385000 W5000 Std D.,153471.9275 2 2.5 <5 Mean 5,727273 2 10 -20 Mean 111.79545451 2 ! 1 <2 Mean 1.454545 2 400000 400000 Mean 305936.3636 _ 3 2.5 <5 C.V. 1.437888 3 10 <20 C.V. 0.53842792 1 3 1 I< CM 1.036445 31 350000 350000 IC V. 0.50164657 4 2.5 <5 4 10 <20 1 1 4 1 <2 4 390000 390000 5 2.5 <5 1 S 10 <20 5 1 <2 5 365000 365000 6 2.5 a Mult Facto Z4 6 10 <20 Mutt Facto 2.5 4 6 1 <2 Mutt Facto 4.9 6 7400 7400 Mult Facto 2.5 7 8 8 Max. Value 30 pg0 7 20 1.25 20 <2.5 Max. Value 261pg4 Max. Pretl C 651p9A _ 1 7 8 1 <2 Max. Value 61 p911 1 ] 39M 3900 Max. Valu' 4320M _ pg/I 8 30 <60 Max. Pretl C 222 pgll 8 6 6 Max. Pretl C p98 8 274" 2741= Max. Pretl 1080000 pg/I 9 2.5 <5 Allowable C 5211.29 pgll 91 26 26 Allowable C 104225.81 p9ll 9 1 <2 Allowable C 20211445 pgAA 9 432000 432000 Allowable C26056451.61 pg0 10 2 5 <5 1 10 125 <25 10 1 <2 ! 10 380000 380000 11 5 <10 11 10 <20 11 1 <2 11 378000 378000 1 12 l 12 12 12 13 13 I 13 131 14 14 1 14 14 15 15 16 16 16 161 17 17 - 17 171 18 _ 18 18 1 181 19 19 19 19 20 20 1 20 20 21 21 21 211 I 22 1 22 22 - 2211 23 23 23 1 23 24 24 - 24 24 1 25 25 - 25 25 26 26 i 26 26 --1 27 28 27 28 i 27 28 27 28 1 11 29 30 _ 29 30 1 29 i 30 1y-- 291 30 311 1 31 1 I 1 1 31 31 32 32 1 32 32 33 _ 33 33 33 34 34 34 34 35 35 L ! 35 _ 35 36 37 36 37 ! 36 37 361 371 II 11 1 _ 38 1 38 1 38 38 39 40 39 7 1 40 1 1 I 39 I 40 39 40 W/01 TOXICANT ANALYSIS rame(er=lCopper 1 II 1 1 Parameter=lCyanide I I I Paramete,lPluoride I Parameter=lLead I I I I Parameter= andard= I 7 ygll II I I Standard = 1pi I Standard= 1 18001 pgn Standard= 1 251 pi Stand.rd= I I I 1 nl DL=l/2DLdual Data RESULTS n DL=12DI-dual Data RESULTS n DL=12DL dual Data RESULTS n DL=12DLdual Data. RESULTS n 1 76 76 Sic! Dev, 27.14541 1 25 <5 Sid Dev. 0 1 997 997 Sid Dev. 285.94771 1 2S <5 Std Dev. 1.5076 1 2 73 73 Mean ]7.4545 2 2.5 <5 Mean 25 2 1370 1370 Mean 1247.9091 2 2.5 <5 Mean 2.9545 2 3 84 84IIC.V. 0.35047 3 2.5 <5 1 C.V. 01 3 1200 1200 C.V. 0,2291415 3 2.5 <5 IC V. 0.5102 3 4 64 64 1 4 2.5 <5 i t 4 1150 1150 4 2S <5 4 5 59 59 S 2.5 <5 ! 5 1240 1240 51 2.5 <5 7100 6 62 62 Mott Facto 1.8 6 2.5 <5 Mutt Facto I 1 6 1530 1530 Mutt Facto 1.5 - 6 2.5 <5 Molt Facto 2S _ 6 ] 60 60 Max. Value 1321pgA 7 25 <5 Max. Value 251Ygfi 1 7 1000 1000 Max. Value 1700 P98 ] 2.5 <5 Max. Value ZS P44 7 8 43 43 Max. Prod C 237.6 Pgll 8 25 <5 Max. Pred C 25 P911 8 1700 17M Max. Pred C 2550 Pg11 B 7.5 <15 Max. Pred C 18.75 pg/l 8 - 9I 132 132 tAilow'able C 729.58ipgA 9 2S <5 AllmvableC 521.131Vgn 9 tOW 1000 Allowable C 187606.45 pgA - 9 2.5 <5 Allowable Q605.65 Pill 9 10 123 123 i j 10 2.5 <5 11 10 870 870 10 2.5 <5 10 11 76 76 11 25 b 11 16701 1670 11 2.5 <5 it 12 I1 12 II 12 12 12 13 1 13 13 13 13 14 14 14 14 14 15 15 15 151 15 16 16 II 16 tfi I - 16 171 17 17 171 i9199 17 18 18 I I 18 1 18 - 18 19 19 1 19 19 l i 19 zo !i 20 II 20 1 20 1 20 21 21 21 1 21 1 1 i 1 21 22 22 11 22 22 1 I 22 23 1 23 I 23 1 1 23 I 23 241 - 24 24 24 24 251 25 .I 251 25 jl 25 26 26 �i 26 26 26 27 27 El .� 27 27 1 27 28 28 21 28 1 28 291 29 29 29 29 30 30 30 _ 30 31 31 31 32 32 32 32 33 33 33 ft=3 33 34 34 34 I 3435 35 35 35 36 36 I 36 36 371 38 37 38 37 38 37 38 - - 37 38 39 39 li 39 39 39 40 40. 40 40 40 677101 TOXICANT ANALYSIS Nickel 1 Parameter =lSilver I I Parameter = I Zinc I I 25 pall Standard= 0.06 V_9ll 'Standard= 50 pgll DL=1/2DLdual Data RESULTS I n OL=1120Laual Data RESULTSi I n OL=12D1!aual Data RESULTS 2.5 <5 iStdDev. 1 83.86846 1 2.5 <5 Std Dev. 10117751 1 443 443 Sid Dev. 126.152 2.5 <5 Mean 20.01429 - 2 2.5 <5 Mean 2.52857 2 298 298 Mean 461727 2.5 <5 C.V. 1 4.19043 3 2.5 <5 C.V. 0,04657 3 391 391 C.V. 027322 2.5 <5 4 2.5 <5 4 375 375 37 37 -� -L 5 2.5 <5 5 466 466 2.5 <5 MuR Facto ].3 _ 6 2.5 <5 Mutt Facto 1. t 6 565 5651 Mutt Faao 1.8 2.5 <5 Max. Value 500 pgA 7 pg/I 8 2.5 <5 Max. Value 3 pgl1 7 345 350 669 6501 345 350 669 6501 Max. Value Max. Pred Allowable 669 12N 2 C 5211.29 pall pgll pall 34 34 Max. Pred C 3650 2.5 <5 Max. Pretl 3.3 pg4 8 25 <5 Allowable C 2605 65 pg8 9 2.5 2.5 <5 <5 Allowable C 6.25 pall 9 10 7 7 10 2.5 <5 11 2.5 <5 11 527 5271 2.5 <5 12 2.5 <5 12 2.5 <5 13 2.5 <5 13 2.5 <5 1 14 2.5 <5 14 7 7 1 15 2.5 <5 15 6 6 16 2.5 15 16 500 5 17 2.5 <5 _ 17 15 <5 18 2.5 <5 1 1 18 1 6 6 19 2.5 <5 19 I 5 "o 20 2.5 <5 20 2.5--5 21 2.5 <5 21 1 6 6 22 2.5 <5 ! 22 e 8 23 2.5 <5 23 7.5 <15 1 24 3 <6 24 7.5 <15 1 ! 25 3 <6 1 25 2.5 <5 I 26 25 <5 11 26 6 6 I 27 2.5 15 1I 27 2.5 <5 l 28 2.5 <5 28 6 6 29 2.5 <51 ! 29 -5 -5 ! 30 2.5 <511 1 1 30 2.5 15 _� 31 2.5 <5 I 1 31 51 5 32 2.5 <511 32 25 <5 33 2.5 <5 33 2.5 <5 _ 34 2.5 <5 34 2.5 <5 35 2.5 <5 35 36 gz 3637 3738 38 39 39 40 40 TOXICANT ANALYSIS ameter=lPhenols anear =OFgll -� n DL=12DLcWal Data RESULTS 1 25 <s 1 IStdDev. 1 0 2 2.5 <5 Mean 1 2.5 3 2.5 <5 C.V. 0 4 2.5 <5 _ 5 2.5 <5 6 2.5 <5 Malt Facto 1 _ 7 2.5 <5 Max. Value 2 5 Fg/I 8 2.5 <5 Max. Free 2.5 Fg/I 9 2.5 <5 Allowable 10423 Fg/I 10 2.5 <5 11 2.5 <5 12 2.5 <5 13 2.5 <5 14 2.5 <5 15 2.5 <5 _ 16 2.5 <5 17 2.5 <5 18 25 <5 19 2.5 <5 _ 20 2.5 <5 21 2.5 <5 22 2.5 <5 23 2.5 <5 24 2.5 <5 25 2.5 <5 26 2.5 <5 _ 27 25 <5 28 25 <5 29 2.5 <5 30 2.5 <5 31 2.5 <5 32 2.5 <5 33 2.5 <5 34 2 5 <5 35 2 5 <5mi--F-1 36 2 5 <537 2.5 <538 2.5 <539 2.5 <540 2.5 <541 2.5 <542 2.5 <543 2.5 <544 2.5 <545 25<547 48 50 fin/01 MA�-08-01 THU 07�25 AM HUFFMAN MILLS FAX N0, 8283964235 P.01 Facsimile Cover Sheet To: Jackie Nowell Company: NC/DENR Phone: 919-733-5083-512 Fax: 919-733-9919 From: Lee Huffman Company: Huffman Finishing Company, Inc. Phone: 828-396-1741 Fax: 828-396-4235 Date: 3/08/01 Pages including this cover page: 2 Comments: Attached are the monthly production figures and Daily maximums as requested. If you need any other information, please call. MRR-08-01 THU 07:26 AM HUFFMAN MILLS FAX N0, 8283964235 1. Huffman Finishing Company, Inc. Granite Falls, NC 28630 Pounds of Production Year Year Year M9n+h 2i?44 99 19M January 317443 331305 309145 February 352510 331811 328748 March 509999 358736 330502 April 453399 469453 365512 May 497600 426456 369023 June ,-557-4851 425628 425292 July 301319 439108 . 469576 August 41.4748 421957 407384 September 510641 417559 412514 October 476726 516250 483116-1 November 382657 410345 331135 December 416883 359762 315611 5191410 4908370 4547568 Daily Maximum 258 i 2 24937 24743 • E /4179LM.w � 9w = �.z�� Nc�) /9y8 SS 1'� (,7� �I��%�I S�/6 Zs o �G f.✓ Sr g 3 / �td /;,1�OVGrl r" S/I/9/0 508 370 �2 M f7if_ 93Z��7.S 9090.70.8 378/763, 16 /fF9 2-41YJ7 /yi4X/�.�%�✓ O /�O • -�//oo o �S.r /�'I. C�S�� Ur/[✓LV r.., �O C.+rJ[ca�7✓�C�j •.__YY�//OLi� /�1oj /Ov/ xws so z, s �� 6U•a ?o. 0 6,1 �f1 6-9 G-9 IN it(,• Ohl, ..0�, k : .�fi. f�. ,-... /��,Gf�X Coy 790. u /se,, e 75-9 isys 135 ,? o S'79,7 S, /.c r � 1.3 2. 6 ,. Z6 07- CASQtG.- i a�r r a�,�,c.. pn, � f 2`� dr-r'c�� �r.�' W..� .u.�-0 A 7t lin, wew �ia,�d.�c 9 i 74w A�w. III 7�- i�r �fl� �r~•� i..� , 11� I II! i f Y L11 II 'If �I `J I I i I il� II 1� ��3y7�Jw 1�'lr�� ���'�'^L ZUOU � S,�/7Y0��•✓�J 0p,.. d , e s,("7jiv 25.3 20a ,ZS3Yo da J 2- yo,,df /A) A f�/(�� y s, o 7or �S, 8 - / Z 9 /dr 0020 6U, a -X- ZS. 3o +r 2S, 3 = 7S9 /6/s 56 /o, 9 * eS,.3 = Z75777 a fi zs 8 - " /4 /Sr v. ZS.3 = o?,S3 /6s z, se /6s — o. s A& Zs 3 = ,. Z(o 15s, �j�f�v�,q./CN/n.,,,, o, LS, 9 = 2,5-9 /SS — o,ai K ,2f. 3 = /. ZGr X3 �# 6-9 6-9 Sy �v'S—= /z�f ,z.�/ /SJ = /3/. �� /65 G�.Zss-/.sod , �sos7/SJ TSS = rbz,It9 f-'71 /6s = sus./s/Ll II 7�-- Z000 Yv #. „&A 43z.6 17 /999 ;?Y.937 5/C., zt y09.03 /SS8 �Y.�y3 yE3.1/ 375.96 iS� �nnurTxr giy z 7s ;GPi) /yys oo: G?D -.74) ./2 A)ys- d.3 f�" , 007zzs-,#c0 = j d0% OId Mu.A 1 i3� &V e S.7fe ;9�0 s �,�� �� n no r l /.-so7,w4v AA, , .'7 2.. 7/ HUFFMAN FINISHING COMPANY POST OFFICE BOX 170 GRANITE FALLS, NORTH CAROLINA 28630 January 04, 2000 Mr. Charles H. Weaver, Jr. NC/DENR Water Quality / NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: Priority Pollutant Analysis Huffman Finishing Company NPDES Permit Renewal NPDES Permit No. NCO025135 Dear Mr. Weaver: Enclosed is three copies (3) of the priority analysis for Huffman Finishing Company. This should complete the NPDES renewal package for our facility. If additional information is required please contact Mr. Shuford Wise at (828) 396- 71 I 1 or myself at (828) 396-1741. 1 JAN DFNR - WATER OUALI7 POINT SOURCE PPV.:2_ Sincerely, vt q4,o Lee T. Huffman Huffman Finishing Company ' p� DEC - 3 1999 1 <NR <WunlE BRpNC AW 6 /70 tA &wuk A; eA4 nwkw 286-�0 November 23, 1999 Mr. Charles H. Weaver, Jr. NC/DENR Water Quality / NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: Request for NPDES Permit Renewal Huffman Finishing Company, Inc. Dear Mr. Weaver: Enclosed please find three (3) copies of the NPDES permit renewal application for the Huffman Finishing Company Wastewater Treatment Plant. Please advise if any additional information is required to process this permit application. Sincerely, Huffman Finishing Company, Inc. Lee T. Huffman Enclosures: Huffman Finishing Company W. W.T.P. NPDES 4 NCO025135 Narrative: Huffman Finishing Company operates an activated sludge oxidation ditch biological wastewater treatment plant as described below. Influent industrial waste consisting of 95% textile dye and bleach process and 5% domestic wastewater enters a mechanically aerated equalization basin (.25 MGD @ 24 hours detention time) Note: average influent flow .158 MG. 2. Influent wastewater is pumped from the equalization basin into a mechanically aerated oxidation ditch ( .25 MG @ 36 hours detention time, ditch volume .375 MG) Mixed liquor from the oxidation ditch enters a center feed clarifier for settling. (clarifier volume .063 MG) 4. Effluent from the clarifier is discharged to the chlorine contact tank (30 minutes detention time @ .25 MGD. 5. Chlorinated effluent enters a post aeration cascade where the effluent is dechlorinated with sodium sulfite and aerated prior to discharge. 6. Effluent from the aerated cascade travels approximately 1 mile to a post aeration tower where the effluent is reaerated and discharged into Lake Hickory (Catawba River) 7. Settled sludge from the clarifier is returned back to the oxidation ditch or wasted using a duplex pumping station. 8. Wasted sludge enters into 2 aerated lagoons for final digesting (total volume .178 MG) 9. Digested sludge (length of residuals storage >180 days) is pumped into tanker trucks and surface land applied to permitted land using a private biosolids contractor. Huffman Finishing Company W. W.T.P. NPDES # NCO025135 Statement of Potential Facility Changes: No planned upgrades/expansions/or major repairs are anticipated for the facility during the next five years. DECHLORINATION FACILITIES EQUALIZATION AERATION TANK CLARIFIER TANK (OXIDATION DITCH) INFLUENT EFFLUENT Ll SCREEN I_- .' v' _-_�— CHLORINE CASCADE POST I ! CONTACT AERATION I SLUDGE RECIRCULATION TANK ISLUDGE RECIRCULATION/ SLUDGE WASTE SLUDGE I WASTE PUMP STATION 1 DRYING DIGESTED SLUDGE T BEDS I - AEROBIC SLUDGE DIGESTION FACILITIES LEGEND BED UNDER DRAINAGE EXISTING FACILITIES NOTE: EITHER LIQUID OR DEWATERED STABILIZED SLUDGE WILL BE DISPOSED OF BY CONTRACT OPERATIONS, Cl PROPOSED FACILITIES lltlffnrtai Finishing Company, Inc. SCHEMATIC FLOW DIAGRAM Granite Falls, Caldwell County, N.C. NPDESIl NCO025135 Huffman Finishing Company W.W.T.P. NPDES # NC0025135 Production Rates 1997 n. Total Monthly Flow Avexage Daily.Flow— Average Daily BOD January 3.35 MG .124 MGD 3.50 LBS February 3.56 MG .127 MGD 3.62 LBS March 4.84 MG .156 MGD 8.641BS April 4.11 MG .137 MGD 7.51 LBS May 4.54 MG .151 MGD 6.41 LBS June 4.71 MG .188 MGD 5.23 1BS July 4.79 MG .218 MGD 9.95 LBS August 5.02 MG .239 MGD 12.62 LBS September 4.51 MG .215 MGD 8.14 LBS October 3.43 MG .149 MGD 5.19 LBS November 2.95 MG 148 MGD 5.79 LBS December 2.34 MG .130 MGD 9.49 LBS Huffman Finishing Company W.W.T.P. NPDES 4 NC0025135 Production Rates 1998 Total Monthly Flow Average Daily Flow Average Daily BOD January 2.46 MG .123 MGD 6.09 LBS February 2.94 MG .140 MGD 5.67 LBS March 3.20 MG .146 MGD 8.58 LBS April 2.85 MG .136 MGD 7.82 LBS May 3.47 MG .165 MGD 7.26 LBS June 3.85 MG .175 MGD 9.60 LBS July 3.98 MG .199 MGD 9.24 LBS August 3.59 MG .171 MGD 6.11 LBS September 3.46 MG .165 MGD 5.36 LBS October 3.32 MG .151 MGD 4.16 LBS November 3.02 MG .144 MGD 4.49 LBS December 2.20 MG .129 MGD 3.69 LBS January February March April May June July August September October November December Huffman Finishing Company W.W.T.P NPDES# NC0025135 Production Rates 1999 Total Monthly Flow 2.84 MG 2.61 MG 3.50 MG 3.23 MG 3.45 MG 4.39 MG 3.31 MG 3.60 MG 3.42 MG 3.84 MG Average Daily Flow .156 MGD .119 MGD .135 MGD .147 MGD .157 MGD .183 MGD .195 MGD .150 MGD .155 MGD .160 MGD Average Daily BOD 5.73 LBS 2.34 LBS 3.22 LBS 5.05 LBS 9.91 LBS 9.97 LBS 6.25 LBS 3.79 LBS 5.34 LBS 4.16 LBS Huffman Finishing Company W.W.T.P NPDES # NCO025135 Sludge Management Plan: Digested wastewater sludge is stored in two (2) aerated lagoons for period exceeding 180 days. The digested sludge is allowed to settle and the supernaught decanted to the head of the treatment facility. As needed the digested sludge is hauled and applied by a private bio-solids land application contractor under the provisions of our land application permit. Permit WQ0002431. Huffman Finishing Company W.W.T.P. NPDES # NCO025135 Priority Pollutant Analysis: The Priority Pollutant Analysis for Huffman Finishing Company is scheduled for the week of November 29, 1999. We will submit the results of the Priority Pollutant Analysis as soon as they are made available. NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations December 17, 1999 Huffman Finishing Highway 321 South P.O. Box 170 Granite Falls, NC 28630 Attention: Mr. Lee Huffman Enclosed please find the reports for your samples received 12/01/99, assigned to BRI Workorder 9L031. Please call if you have any questions. Thank you. J AN - 6 2000 i DENR - WATER QUALITY Burlington - Corporate Offices 1302 Belmont Street • Burlington, NC 27215-6935 Phone (336) 570-4661 • Fax (336) 570-4698 Sincerely, 'ON RESEARCH, INC. iLervices i61 Ext. 211 Eden 370 W. Meadow Road Eden, NC 27288 Phone (336) 623-8921 Fax (336) 623.5878 BR2U% .. .1 NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations BURLINGTON RESEARCH ANALYTICAL REPORT CUSTOMER: Huffman Finishing REPORT TO: Mr. Lee Huffman WORK ORDER #: 9LO31-001 RECEIVED: 12/01/99 REPORTED: 12/ 17/99 SAMPLE DESC: NOV. MONITORING SAMPLE TYPE: WASTEWATER, EFFLUENT COMP PO NUMBER: COLLECTED: 11/29/99 07:50 to 11/30/99 07:40 SITE: Effluent PARAMETER DATE/TIME/ANALYST MOL RESULT Base-Neutral/Acid Extractables Started 12/03/99 00:00 Attached EPA 625 Analyzed 12/09/99 by SAI at See attached Organo-chlorine Pesticides Started 12/03/99 00:00 Attached EPA 608 Analyzed 12/05/99 by SAI at See attached Antimony, Total by ICPMS Started 12/06/99 11:05 0.00002 0.0050 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Arsenic, Total by GF Started 12/06/99 11:05 0.005 <0.005 mg/L EPA 206.2 Analyzed 12/08/99 by SJH at BRI - Burlington rBeryllium; Total by ICPMS Started 12/06/99 11:05 0.00006 CO:000203mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Cadmium Total by ICPMS Started 12/06/99 11:05 0.00004 r0:000511 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Chromium, Total by ICPMS Started 12/06/99 11:05 0.0007 t0:044-',mg/l- EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Copper, Total by ICPMS Started 12/06/99 11:05 0.002 0.059 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Lead, Total by ICPMS Started 12/06/99 11:05 0.0002 0.0010 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Nickel, Total by ICPMS Started 12/06/99 11:05 0.002 0.003 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Silver, Total by ICPMS Started 12/06/99 11:05 0.00001 <0.00001 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Zinc, Total by ICPMS Started 12/06/99 11:05 0.005 0.35 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Burlington - Corporate Offices Eden 1302 Belmont Street • Burlington, NC 27215-6935 Page 1 370 W. Meadow Road Eden, NC 27288 Phone (336) 570-4661 • Fax (336) 570-4698 Phone (336) 623-8921 Fax (336) 623-5878 88 26'W NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations MQL = Minimum Quantitation Limit Burlington - Corporate Offices Eden 1302 Belmont Street • Burlington, NC 27215-6935 Page 2 370 W. Meadow Road Eden, NC 27288 Phone (336) 570-4661 • Fax (336) 570-4698 Phone (336) 623-8921 Fax (336) 623-5878 9R 2M SPECIALIZED ASSAYS, INC. 2960 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 A N A L Y T I C A L R [E P C3R T Phone 1-615-726-0177 GURLINGTON RESEARCH, INC 2100 Lab Number: 99-A182839 WAYNE- ALTHOUSE Sample ID: 9LO31-001 1302 BELMONT ST Sample Type: Water BURL.INGTON, NC 27215 Site ID: Date Collected: 11/30/99 Project: Time Collected: 7:40 F'T•o.ject Name: Date Received: 12/ 2/99 Sampler: SC Time Received: 9:00 Report Ruan Dil Analyte Result Units Limit Unit Factor Date Tlne Analyst Method Batch vEXTRACTAULE ORCARICSx Aoenaphthene RD u9/1 16. 10. 1 121 9199 20:21 M.Goodrich 625 2097 Arenaphthglene RD uq/1 10. 10. 1 171 9/99 10:21 H.Goodrich 625 2087 Ar,thracene RD u9/1 10. 10. 1 121 7/79 20:21 M.Goodrich 625 2937 I(enzidlne - RD uq/1 50. 50. 1 12/ 9199 20:21 M.Goodrich 625 2987 Benzo(a)ant hracehe RD ug/1 10. 10. 1 121 9199 20:21 M.Goodrich 625 7087 0enzo(a)pyrene r:D uq/1 10. 10. 1 12/ 7197 20:21 M.600drlch 625 2037 Gerao(b)Fluorarrthene RD uy/1 10. 10. 1 12/ 9/99 20:21 n.Goodrich 625 2087 Benzo(g,h,i)perylene RD uq/1 19. 10. 1 121 9/9? 20:21 H.Goodrich 625 2087 Denzo(k)fiuoranthene RD uq/l 10. 10. 1 121 9/99 29:21 M.Goodrich U5 2087 4-0ronophenylphenylether RD uq/1 10. 10, 1 .12/ 9197 20:21 M.Goodrich 625 208, Butglbenzylphthalate RD o9/1 I0. 10. 1 121 9/99 20:21 M.Goodrich 625 2087 4-Chlare-3-nethylpnenal RD ug/1 10. 10. 1 IV 7197 79:21 M.Goodrlch 625 2087 bis<2-ChloroethoxU)methane RD ug/L 10. 10. 1 12/ 9/79 20:21 M.Goodrich 625 206, b1s(2-Ch16roethgI)ether RD uq/I 10. 10. 1 12/ 7179 ZU:21 M.Goodrich 625 2087 bis(2-CblcrolsopropyDether RD u9/1 10. 19. 1 121 9/9? 20:11 M.600drich 625 Z087 2-Chloronaphthale he RD ug/l 10. 10. 1 12/ 7179 20:21 M.Goodrich 625 ZU87 2-Chlorophenol RD uy/1 10. 10. 1 171 9197 20:21 M.Goodrich 625 2087 4-Chloropheoylphe0glen,er RD uq/1 10. _ I0. 1 121 9/99 20:21 N.Goodrich 625 1u37 Chryss=ne RD 09/1 10. 10. 1 12/ 9199 20:21 M.Goodrich 625 2087 Dibenz(a,rJanthracene RD uq/1 10. 10. 1 12/ 9/99 20:71 1. Goodrich 625 2087 1,2-Dichlorobenzerne RD uq/1 10. 10. 1 £Z/ 7/77 20:21 M.Goodrich 625 2087 1,3-Dichloroben2ene RD uy/1 10. 10. 1 12/ 9/99 20:21 M.Goodrich 625 2087 1,4-Dichlorobenzene RD u9/1 10. 10. 1 12/ 7/99 20:21 M.Goodrich 625 2C87 3,Y -Dichiorobenzidlne RD ug/1 20. 20. 1 171 9/99 20:21 M.600drlch 625 2087 2,4-Dichloropheool RD uq/1 10. 10, 1 12/ 9199 20:21 M.Goodrich 625 2087 Diethylphthalate RO uq/l 10. 10. 1 12/ 9199 20:21 M.Goodrich 625 2087 2,4-Dinethylphenol RD ug/1 10. 10. 1 12/ 9199 "40:21 M.Goodrich 625 DUB Dinethylphthalate RD uq/1 10. 10. 1 12/ 9199 20:21 M.Goodrich 625 2087 Di-n-but9lphthalate RD uq/1 10. 10. 1 12/ 9199 20:21 M.Goodrich 625 2087 2,4-Dlnitrophehul RD ug/1 25. 75. 1 12/ 9197 20:21 M.Goodrich 625 2087 " 4-dinitrotoluene RD ug/1 Ia. 10. 1 12/ et" 20:21 M.Goodrlch 625 2087 2,5-DInItrotoluene RD uq/1 Ia. 10. 1 12/ 9/99 2U:21 11.600drieh 625 2087 of-n-octglphthalate RD uq/1 19. 10. 1 12/ 9/99 20:21 M.Goodrich 625 2087 Sahple report continued . . . COPY 1 SPECIALIZED ASSAYS, INC. r 2960 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 AIVHLYT I GAL F¢I=-F'OF2T Laboratory Number: 99-A1B2339 Sample ID: �FL031-001 Page 2 Report QUan DI1 Analyse Result Units Limit Limit factor Date Time Analyst Method Batch 1,2-D1pherylhydrazloe HD U911 Ia. 10. ---- 1 --------- 12/ 7179 ----- 20:21 -------- M. 6004rlch --------- 625 --'- 20U7 fluoraothene ND Ug/l 10. Ia. 1 12/ 7/99 20:21 n.Coodrich 625 2037 Fluore•ne MD U911 10. 10. 1 12/ 9179 70:21 M.600drich 625 2087 Hexachlorobenzene ND u9/1 Ia. 10. 1 12/ 7179 20:21 n.600drlch 625 2087 Hexachlorobutadiene ND U911 10. 1D. 1 IV 9197 20:21 n.600drich 625 2D87 Hexachloroogclopentadiene HD ug/1 10. 30. 1 121 9199 20:21 M.600dr1ch 625 2087 Hexachloroethane ND ug/1 10. 30. 1 12/ 7/79 70:71 n.Goodrich 625 7097 lnden6(1,2,3-ed)pgrene HD Ug/1 10. 10. 1 12/ 9/79 20:21 M. Goodrich 625 2097 1sophorone NO Ugil 10. 10. 1 12/ 9199 20:21 n.600drich 625 2037 2-nethyl-4,6-dinitrophenol HD ugil 50. 50. 1 121 4/49 20:21 M.600drich 625 2U37 Naphthalene ND ug/l 10. 10. 1 121 9199 20:21 M.Coodrich 625 2U87 Nitrobenzene ND Up/1 10. 10. 1 121 7199 20:21 M.600drich 625 2097 2-Altrophenol HD U911 10. Ia. 1 121 7179 20:21 M.600dr1ch 625 2087 4-4itrophenol ND Ug/1 25. 25. 1 12/ 9/99 20:21 M.600drich 625 2081 N-nitrosodi-n-p1•apylanine ND Ug/l 10. 10. 1 121 9/99 20:21 M.Coodrich 625 -Vol N-nitrosodlphenylanine ND ug/l 10, 10. 1 IV 9I99 20:21 n.Coodrich 625 2087 N-nitrosodinethylamine ND ug/1 10. 10. 1 12/ 9/99 20:21 n.Coodrich 625 2087 Pentachlorophenol ND ug/l 25. 25. 1 12/ 9199 20:21 M.600drich 625 2087 Phenanthrene ND Ug/1 10. 10. 1 12/ 9199 20:21 M.6oadrich 625 10"' Phenol ND u9/1 10. 10. 1 12/ 9/99 20:21 M.600drich 625 2081 Pyrenr ND Ug/l 10. 10. 1 12/ 9/99 20:21 M.Coodrich 625 2087 Bis(2-eth9lhexyllphthalate ND Ug/1 10. 10. 1 12/ 9199 20:21 M.Coodrich 625 2087 1,2,4-Triehlorobenzene HD ugll 19. 10. 1 12/ 9I99 20:21 M.600drich 625 2087 2,4,6-Trichloropheool ND Ug/1 10. 10. 1 12/ 9/97 20:21 n.600drich 625 2087 PESTICIDES/PCD's/HERBICIDESK Aldrin ND U911 0.05 0.05 1 121 5199 11:50 M. Cauthen 608 2258 Aroclor 1016 ND og/l 0.5D 0.50 1 12/ 7/99 19:45 n.Royers 608 2701 Aroclor 1221 HE, U911 0.50 0.50 1 121 7199 19:45 M.Rogers 608 2101 Aroclor 1132 HD 1jg/1 0.50 0.50 1 IV 7/99 19:45 M.Rogers 609 27U1 Aroclor 1142 ND U911 0.50 0.50 1 12/ 7177 19:45 M.Rogers 603 2701 Aroclor 1248 ND Ug/l 0.50 0.50 1 12/ 7/99 19:45 11.Rogers 608 2101 Aroclor i254 ND Ug/1 0.50 0.50 1 12/ 7199 19:45 n.Rogers 608 2701 Aroclor 1260 ND U9/1 0.50 0.50 1 12/ 7/97 19:45 M.Rogers 608 2701 a-LIHC ND Ug/l 0.05 0.05 1 12/ 5199 11:50 M. Cauthen 608 2258 b-:MC HD up/1 0.05 0.05 1 12/ 5199 11:50 M. Cauthen 608 2258 d-Mc ND Uy/1 0.05 0.05 1 12/ 5/99 11:50 M. Cauthen 608 2258 9-BHC, Lindane HD Ug/1 0.05 0.05 1 12/ 5199 11:50 M. Cauthen 608 2258 Chlordane ND Ugll 0.05 0.05 1 12/ 5/99 11:50 M. Cauthen 608 2258 4,4'-DDD ND Ug/1 0.10 0.10 1 12/ 5199 11:50 M. Cauthen 608 2258 4,4'-DDE ND ug/1 0.10 0.10 1 12/ 5179 11:50 M. Cauthen 600 2258 4,4'DDT HD Ug/l 0.10 0.10 1 121 5/99 11:50 M. Cauthen 608 2258 Dieldrin ND up/l 0.10 0.10 1 12/ 5199 11:50 M. Cauthen 608 2258 Sample report continued . . . COPY 1 SPECIALIZED ASSAYS, INC. 2960 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 Nnalyte Result Units ------------------------ Eadosulfan I ----------- RD ----- ug/l EiidosulFan II RD ug/l E[1dosulFan Sulfate RD ug/I Endrin RD u9/1 Endrin Aldehyde HD u9/1 Heptachlor RD ug/1 Heptachlor Epoxide RD U911 Tcxaphene RD ug/1 RD = Not detected at the report linit Sanple Extraction Data A14ALYTIGAIL HEEPORT Laboratory Number: 99-AlB2E339 Sample ID: 9LO31-001 Page 3 Report Ouan Dil Linit Linit factor Date Tine Analyst Method Batch ------ OAS ------- 0.05 ------ 1 -------- 12/ 5/99 ----- 11:50 ---------- M. Cauthen --------- 608 ----- 2258 0.10 0.10 1 12/ 5199 11:50 M. Cauthen 608 2258 0.10 0.10 1 12/ 5/99 11:50 M. Gauthen 609 2258 0.10 0.10 1 12/ 5/99 11:50 M. Cauthen 608 2258 0.10 0.10 1 12/ 5/99 11:50 M. Cauthen 608 2258 0.05 0.05 1 12/ 5/99 11:50 M. Cauthen 608 2258 0.05 0.05 1 121 5/99 11:50 M. Cauthen 608 2258 5.00 5.00 1 12/ 5/99 11:50 M. Cauthen 608 2258 Wt/Vol Paraneter ------------------ Extracted --------- Extract Vol ---------- Date -------- Analyst ---------- Method ------ DNA's 1010 nl 1.0 nl 121 3/99 C. Terry 3510 Pesticide, 500. nl 5.00 nl 121 3177 D.Yeager 3510 PCs's 500. nl 5.00 111 121 3/99 C. Terry 3510 Surrogate '/, Recovery Target Range Burr-Ritrohenzene-d5 72. 15. - 105. Burr-2-Fluorohiphen9l 76. 17. - 110. Burr-Terphenyl dia 57. 10. - 116. surr-Phenol d5 23. 10. - 100. Burr 2-Fluorophenel 34. 9. - 100. surr-Z,4,b-TriGronophenol 91. 15. - 134. pest surr-TCMY. 47. 20. - 121. surr-Dihutylchlorendate 53. 10. - 120. pest surr-DO 47. 10. - 120. Sanple report continued COPY 1 SPECIALIZED ASSAYS, INC. 2960 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 ANALYT I C AL H EP OR T Laboratory Number: 99—A182839 Sample ID: 9L031-001 Page 4 These results relate only to the items tested. This report shall not be reproduced except in full and With permission of the laboratory. Report Approved By: C_ �l.t�l A J Report Date: 12/15/99 Theodore J. Duello, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Services Eric Smith, Assistant Technical Director Gail A Lage, Technical Services Laboratory Certification Number: 387 End of Sample Report. COPY 1 NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations BURLINGTON RESEARCH ANALYTICAL REPORT CUSTOMER: Huffman Finishing REPORT TO: Mr. Lee Huffman SAMPLE DESC: NOV. MONITORING SAMPLE TYPE: WASTEWATER, EFFLUENT GRAB COLLECTED: 11/30/99 07:40 SITE: Effluent WORK ORDER #: 9LO31-002 PO NUMBER: RECEIVED: 12/01/99 REPORTED: 12/ 17/99 PARAMETER DATE/TIME/ANALYST MOIL RESULT Cyanide, Total Started 12/09/99 10:30 0.005 < 0.005 mg/L EPA 335.2 Analyzed 12/09/99 by MTT at BRI - Burlington Phenol, Total Started 12/02/99 08:30 0.005 <0.005 mg/L SM-5530C 18TH Analyzed 12/03/99 by TAR at BRI - Burlington Purgeable Organics, 624 Started 12/06/99 15:12 Attached EPA 624 Analyzed 12/06/99 by SAI at See attached MQL = Minimum Quantitation Limit Certifications: BRI - Burlington NC Chemistry: #85, Biomonitoring: #002, Drinking Water: #37743, Radiation License: #001-0904-OG VA SWCB ID: #000061, Drinking Water: #00018 SC Laboratory ID: #99042 EPA Chemistry Lab ID: NCO0137, Bioassay Lab ID: NC2721500 Burlington - Corporate Offices Eden 1302 Belmont Street • Burlington, NC 27215-6935 Page 3 370 W. Meadow Road Eden, NC 27288 Phone (336) 570-4661 • Fax (336) 570-4698 Phone (336) 623-8921 Fax (336) 623-5878 9R2G9 SPECIALIZED ASSAYS, INC. 2960 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 Phone 1.615-726-0177 ANALYTICAL F2;EP OR T 13URLINGTON RESEARCH, INC 2100 Lab Number: 99-A182840 WAYNE ALTHOUSE Sample ID: 9L031-002 1302 BELMONT ST Sample Type: Water SURLIP•iGTON, NC 27215 Site ID: Date Collected: 11/30/99 Project: Time Collected: 7:40 Project Name: Date Received: 12/ 2/99 Sampler: SC Time Received: 9:00 Report 0uan Dil Ahalyte -------`-------------- Fesult ----------- Units ------ Unit ------ Limit ------- Factor ------ Date -------- Tine ----- Analyst ---------- Method --------- Batch ----- 00LATILE DREP.RICSK Acrolein RD ug/1 10. 10. 1 121 6199 15:12 S. Mani 624 523 Acrylonitrile RD u9/1 10. 10. 1 12/ 6199 15:12 S. Mani 624 523 Benzene RD ug/l S. 5. 1 121 6179 15:12 S. Mani 624 523 Bronoforn RD u9/1 5. 5. 1 12/ 6199 15:11 S. Mani 624 523 Brononethane RD ug/l 5. 5. 1 12/ 6199 15:12 S. Mani 624 523 Carbon tetrachloride RD ug/1 5. J. 1 121 6199 15:1Z S. Mani 674 523 Chloroheraene RD ug/l S. 5. 1 121 6/97 15:12 S. Mani 624 523 C i'loro"ethane RD ug/l 10. J. 1 12/ 6199 15: 12 S. Mani 624 523 1-C hloroet bylui r,glet her RD ug/i 5. 5. 1 IZ/ 6199 15:12 S. Mani 6Z4 523 Chloroforn 12. ug/1 5. 5. 1 121 6199 15:12 S. Want 624 323 Chloronethane RD ug/1 5.. 5. 1 12/ 6/77 15:12 S. Man! 624 523 Di bronochloronethane RD ug/l 5. 5. 1 17/ 6/99 15:12 S. Mar.! 624 523 1,2-Dlchloroben7ene RD u911 5. 5. 1 121 6/79 15:12 S. Want 624 523 1,3-Dtchlorobenzeue RD ug/1 5. 5. - 1 12/ 6199 15:12 S. Mani 624 23 I,4-Dichlorobenzene RD u911 5. 5. 1 12/ 6177 15:12 S. Mani 624 523 DIchlorodifluoronethane RD ug/l 5. 5. 1 121 6/99 15:12 S. Rant 624 523 1,1-Dlchlaroethene RD ug/I 5. 5. 1 12/ 6199 15:12 S. Mani 624 523 1,2-D10hloroethane RD ug/l 5. 5. 1 12/ 6191 1J:12 S. Mani 624 523 1,1-Dl chloroethene RD ug/l 5. 5. 1 12/ 6/99 15: 12 S. Mani 624 J23 1,2-Dlchlaroethene (total) RD ug/1 5. 5. 1 121 6/99 15:12 S. Rant 624 523 1,2-Vtchloropropane RD ug/1 5. 5. 1 12/ 6197 15:12 S. Mani 624 523 cis-1,3-Dichloropropene RD 09/1 5. 5. 1 121 6/97 10:12 S. Mani 624 523 trans-1,3-Dichloropropere RD ug/1 5. 5. 1 121 6/99 15:12 S. Want 624 523 Ethylbenzene RD u911 5. S. i 121 6/99 15:12 S. Mani 624 523 nethgleoe chloride RD u911 10. 10. 1 121 6/99 15:12 S. Want 624 523 1,1,2,2-Tetrachloroethane RD ug/l 5. 5. 1 121 6/99 15:12 S. Want 624 513 Tetrachloroethene RD u9/1 5. 5. 1 121 6177 1J:12 S. Mani 624 523 Toluene RD ug/l 5. J. 1 121 6/99 15:12 S. Want 624 J23 1,1,1-Trichloroethane RD ug/l 5. 5. 1 121 6197 15:12 S. Mani 624 1073 1,1,2-Trichloroethane RD ug/1 5. 5. 1 121 6/99 15:12 S. Mani 624 523 Tricblornettrene RD u9/1 5. J. 1 12/ 6197 15:12 S. Want 624 523 Vinyl chloride RD u0/1 10. J. 1 12/ 6/99 15:12 S. Mani 624 513 Xylenes HE, ugll 3. 5. 1 12/ 6/99 15:122 S. Mani 624 523 Saiple report continued . . . COPY 1 SPECIALIZED ASSAYS, INC. 2960 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 AnAyte Result Units ----------------- '------- ----------- ------ DrOmedIchloromethane HD ug/l IrichlorofluoronethilH RD 69/1 HD = Hot detected at the report limit. AIYliLYTICAlL R3EF�OFRT Laboratory Number: 94—AI82640 Sample ID: 9LO31--002 Page 2 Report Auan oil Limit ' Limit Factor Date Time Analyst nethod [latch ------ 5. ------- ------ 5. 1 -------- --------------- 121 6197 15:12 S. Mani --------- ----- 624 523 5. 5. 1 11/ 6/97 15:12 S. Mani 624 523 Surrogate X Recovery Target Range VUR Surrogate, 1,2-Dichloroethane, d4 67. bo. - 138. VGA Surrogate, Toluene d8 lo4. 80. - 123. VGA Surrogate, 4-[r;onofluoroDenzene 71. 73. -.122. These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: (;� Report Date: 12/15/99 Theodore J. Duello, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Services Eric Smith, Assistant Technical Director Gail A Lage, Technical Services Laboratory Certification Humber: 387 Enid of Sample Report. COPY 1 �I XI 1302 Belmont Street 370 West Meadow Road Burlington, NC 27215-8935 Eden, NC 27288 BURLINGTON RESEARCH, INC. Faone(336)5336) 70-4698 0-4661 Fax (336)623-5878 ®Inne09 •-e CLIENT: Huffman Finishing Company SEND REPORT TO: Lee Huffman (go S. Wise) Facility/Site: Wastewater Treatment Plant Phone:—LB28) 396-1741 Fax: (8281 Z96_ Ramnlpr /Print) S. Wise (Signature) Purchase Order No.: Verbal Lee Huffman 100 East Gordon Street i Kinston. NC 28501 Phone (25:') 52Q-9921 Fax (252)520-9922 w� SAMPLE COLLECTION "' z Do4 SAMPLE TYPE LL or¢„ `Preservation Codes: "_ � - COMPOSITE GRAB SAMPLE ID z M m u w F J w a z m r w ANALYSIS REQUIRED w TEMP (4 -C) A Ice E= NaOH B HNO3 F. None •, STARTED ENDED DATE ........__.. DATE � � 2 <o a ? z o0 L�� a w N z C _' H2SO4 G = CUPRIC; TIME TIME u HAND AUTO z .. _'. D _ HCI'_ H =.HCHO .: . Yes No 11 /29/9 11 /30% 99 Q'd Cut l�h Pb - - - - Effluent A: 2.5 X 4 608, 625, Metals �. Yesl No 11 /R/99 11/3.0.[-9-9... 120 X CN, 624, Phenolics S, 5b,�'-- Effluent X: 5 , Yes: No i +- r. t-_ •:i i Yes; No i i i Yes: No _ Y Yes : No Yes: No i Yes; No g v - Was the sample dechlorinated at time of collection? Yes LXJ No LJ Will the results be used for regulatory monitoring purposes? Yes L-I No U OR CLIENT USE ONLY Relinquished by: (Si Date: amShipped by: (Sig.) Date: e:Huff TTime:11/30/10.35 /3D/Received by: (Sig.) Date: e: Method of Shipment UPS r USE ONLYf a 4 .vxF,OR{LJ16_ Received in �Lab FROM:*(Sig.) I. od otShIpment/ J- RE / /' •• / Samial ,- , eo. n 7.ae White - ORIGINAL - Forward to BRI - BRI will return to client with Final Report Canary - BRI - Laboratory Pink - BRI - Laboratory Goldenrod - Client - Copy NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations December 17, 1999 Huffman Finishing Highway 321 South P.O. Box 170 Granite Falls, NC 28630 Attention: Mr. Lee Huffman Enclosed please find the reports for your samples received 12/01/99, assigned to BRI Workorder 9L031. Please call if you have any questions. Thank you. it I JAIJ :-6 ' 1 I _ ... UENR - WATER OUALITY POINT SOUF.CE Fi?AhCH Burlington - Corporate Offices 1302 Belmont Street • Burlington. NC 27215-6935 Phone (336) 570-4661 • Fax (336) 570-4698 Sincerely, BURLINQTON RESEARCH, INC. ,rt Services Ext. 211 Eden 370 W. Meadow Road Ecen, NC 27288 Phone (336) 623-8921 Fax (336) 623-5878 5a 2 cv9 11 NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations BURLINGTON RESEARCH ANALYTICAL REPORT CUSTOMER: Huffman Finishing REPORT TO: Mr. Lee Huffman WORK ORDER #: 9LO31-001 RECEIVED: 12/01/99 REPORTED: 12/17/99 SAMPLE DESC: NOV. MONITORING SAMPLE TYPE: WASTEWATER, EFFLUENT COMP PO NUMBER: COLLECTED: 11/29/99 07:50 to 11/30/99 07:40 SITE: Effluent PARAMETER DATEMME/ANALYST MOIL RESULT Base-Neutral/Acid Extractables Started 12/03/99 00:00 Attached EPA 625 Analyzed 12/09/99 by SAI at See attached Organo-chlorine Pesticides Started 12/03/99 00:00 Attached EPA 608 Analyzed 12/05/99 by SAI at See attached Antimony, Total by ICPMS Started 12/06/99 11:05 0.00002 0.0050 ni EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Arsenic, Total by GF Started 12/06/99 11:05 0.005 <0.005 mg/L EPA 206.2 Analyzed 12/08/99 by SJH at BRI - Burlington Beryllium, Total by ICPMS Started 12/06/99 11:05 0.00006 0.00020 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Cadmium, Total by ICPMS Started 12/06/99 11:05 0.00004 0.00051 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Chromium, Total by ICPMS Started 12/06/99 11:05 0.0007 0.044 ri EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Copper, Total by ICPMS Started 12/06/99 11:05 0.002 0.059 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Lead, Total by ICPMS Started 12/06/99 11:05 0.0002 0.0010 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Nickel, Total by ICPMS Started 12/06/99 11:05 0.002 0.003 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Silver, Total by ICPMS Started 12/06/99 11:05 0,00001 <0.00001 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Zinc, Total by ICPMS Started 12/06/99 11:05 0.005 0.35 mg/L EPA 200.8 Analyzed 12/08/99 by RTW at BRI - Burlington Burlington - Corporate Offices Eden 1302 Belmont Street • Burlington, NO 27215-6935 Page 1 370 W. Meadow Road Eden, NO 27288 Phone (336) 570-4661 • Fax (336) 570-4698 Phone (336) 623-8921 Fax (336) 623-5878 bi 12 G99 11 NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations BURLINGTON RESEARCH MQL = Minimum Quantitation Limit Burlington - Corporate Offices Eden 1302 Belmont Street • Burlington, NC 27215-6935 Page 2 370 W. Meadow Road Eden, NC 27286 Phone (336) 570-4661 • Fax (336) 570-4698 Phone (336) 623-8921 Fax (336) 623-5376 91, 2,. 1 SPECIAIAZED ASSAYS, INC. 2960 Foster Creighton Dr. P.O. Box 40566 Nash\ fle, TN 37204-0566 Phone-615-726-0177 PE -SEARCH. INC 2 IDO UEL-NUINI �"'T -- V-Ij, I t 2 1 '4 , I -1� . ; 2 / " 11 14 oc"i r" 00% L- "Ir' -I- I (-- AL FZ JH F' OR -F Lab NurnbeT, ? 9 -- A 1 3 2 R 314 Sajult- ID: '7LO.51-001 sawn I e "r ij p ej.,, t j, r, S J. t E I D U, -i t e Coliected: 11/30/9'7' r i-, j T I M 2 is 0 1 1 E! C. t E d : 40 0 j2C 't' I I -i cu C- Da 1. E! R e c e i v e d 2 / V�:' 1 C Late Received 00 H,epurt qu ah D 11 Fp'.uit Units Limit Limit motor P'te line Rif 31 ti, 1, lt'tbod U a te h "HEficfLKE q/1 10. Ia. I I"/ q/79 20: 71 M, Goodi'lch 625 RceitahYrt'rlylerle Nil uq/1 IR Ia. 1 12" 7/99 20:21 M. Goo dr 10 h 625 1,'107 Arthl aoerle HD uQ,`I 10. ]'a. I I?/ 7191 20: 11.1 n' Goodrich: 625 2U37 ".15) u A 50. I V/ YM 20: 21 M. Coodrich 62' 21107 flzL'; -1 '-ft' iW-C VIR' u(VI 10. 10. .1 12/ 7/39 20: 71 M. Coo dr I c. h 625 20a7 v tvav' iiU _Q/1 I U. Ia. i 12/ 7 ! 3 7 20: 71 rj. t;ooJi,10, 625 121 9 197 20: 21 M. Goodrich 625 HP ljq!i 10. Ia. Ue' Fe'YY 20: 21 11. Goodrich 10 "aUl R.i Floor -jr, I u qp'l 10, Ili 1 12 Ff'7y "Q: ','I M. G"ou rich f25 7 aU7 1 1 !1 he wj 1. 0 t he r U uq/I aU. in. 1. I?f' 9IFY 20: 21. 11. C oo ej v i c I 1 62i 2081 i t: Ili. ble iI nI I p lt ij i I I o V., u 9 Ia. 1. 1�/ ?y 4 o: ?.I n. Goodr ic h 625 5 cp.:oro. l4. D uq/1 10. .10. 1 12( M�7 70: 71 11, goodrlOs 625 2087 z s 2 - C' h I a r u t: 4 c x lli i zen 111 oii Nl% Ia. 10. 1 U/ 9/79 '--'U: 21 M. 60odriCh 625 2ai7 gi et hf'r R) 10. 10. 1 12/ "7179 2U: 21 i'L Goodrich 625 2 0 a 71 20: '1 M. 6060101 12') il it ug"I 10, 10. 1 17, 1 V79 20: 21 n. Cc, od T, 1 o 1, 625 j 111817 ND uQ' 10. 10. 1 17/ 9/77 20: 21 n.Goodrich 62" 2 I'd 7 4- liq/1 H. M. 12l' '7'e"7 1; M 21 rj. �ot) ;rich i(V q/1 I U. 10, 1 7,T5 2T 21, n. Wou'r Lob 6"';j _ -Uot j fi, 1: F J(;v li�' F"') q/1 10. 10. .1 121 9/77 20: ZI It. U00dViCh 625 2087 '-Pieta oho le!o: i ug/I 10. ].a. 1 U/ VY9 70: ZI n. 600dvich 625 I087 "robeh'Ertw Ir" 10. 10. 1 12/ M? 20: 21 n.Goodrich 61, liqll 10. H. 1 12/ 9/93 21): 21 1. Goo V'r I c h 625 r? i (J: 1 uro !,i- TZ I fit- HD 2 U. 10. 1 17Il '11`77 "U: 21 M. Goodvlc h M 2.1187 7/99 10: 21, n. Goodrich6.2 'i 2087 uq/1 Ia. to, A I"Y 20 1 M, Goadv iL h 6 2 "1 0 No k!qll 10. 19. 1 12,' Q, M 2 0: 21 " it Goa d'vidt Q'- 7007 t it ll h A ;t'-� H U91/1 A. To. t 11" 91,99 2.9: '41 1 . Coo d p i c h 12 K, uqt'l 10. Ia. I 12t' 9/99 M 'I n. Goodr icii 62' 87 20 . 71y7 2U: 21 9. Uou, drlhh 625 f nitro uv U9.11 to. 10. 1 12." ?t""t Goo-Irl --h 625 20U7 No Ult"I 10. 10 17t, 5 70: 71 1. Ut)o,!y:Lofi 625 J: I'J"i to to. 5 20: .1. M raTeltrAl SPECIALIZED ASSAYS, INC. 2960 Foster Creighton D; P.O. Box 40566 Nashville, 'I'N 37204-0566 AIV ALYT 11 C AlL R 1EP OR T Phone 1.615-726.0177 Ldbaraturg Number: ?9-AIW.S3' Page 2 FPpGrt Wall DU R a lob? ROW Units Limit Limit Factor Date tine Analyst Method Gatti: 1,211 p6eoUlhudrW he RD Up 10. .10. 1 12/ 9179 20:21 M.Goodrlet, 625 Z087 Woranthene HD U911 10, 10. 1 121 9I9F ZU:21 M- Goodrich 625 2067 rl aore ne cD ugll 10. 10. 1 121 3199 ZD 21 R. Goodrich 625 2087 Heal aci;ler'idenzehe No uq/l 10. IU. i. 12/?; 9'i Z0: 21 M. Gcoill, l c,h 625 2U87 !i•:,:aehL)ruh:�tadieua HD ujil 10. 10. _ 12/ 9/99 20:21 M.Goodrlch 625 2087 Hea ac hlcmocurlohe r.Tzdirhe @D Ug"ll Ia. 10. 1 12/ 9/99 Z0: Z1 M. Goodrich 625 2087 .It a o0jlvroet:';ene i!0 uGii 10. 10. 1 12" 9/99 111 21 M. Goo dr ich 625 2037 ih de hot l;'2 is f p Urd'- an No Uyl Ia. 10. 1 12/ 9/9'i 2171 1Goodrlch 625 2087 C5oph7i'6na 8D w"'1 lU. 10. 1. .121 9199 20121 16wdHch 625 2 U8. _-it?th)l.'-!'/i 9iiutlOph,,iiGi ND Uq/1 M. M. 1 12i 9/99 271:-1 1.GuodPi6t 62"1 1i;67 'a7 hr ha le oe ?lD ;Igil 10. it). 1 11' 9/99 20:21. M.Gaodrich 625 2067 ii!truiPare r:a @D uG/1 10. 10. 1 121 MY 20: 21 n. Gondrich 625 208P/ i1D o!;'1 to. 10. 1 121 51199 M Z1 A. Goodrich U1 2n37 'HD ug;'l 25. 25. '1. 12/ 5195 20:21 M.Coo;rich 625 '21"U r{-r,itrosodi-n-p.opyl;rilnc HE. ugll 10. io. 1 12/ 9AP 20:;{1 M.Goodrir,1) 2267 itrc,odlphwnilardRe HD ugll 10. 1.0. 1. 11.' 9/99 20:21 n.Goodrich 625 21"67 R-nitrov),linetligl.ani.ne HD uq/l 10. 1.0. i. 12- 9i99 20:21 n.Goodrieh 625 2067 PantanhiUf Opj;etb.)1. HD ugil 25. 2S. i, 12e' 9/99 212.1 n.GOodrie.h 425 20W Pilenaothrene HE, Ugl1 10. 10. 1 12/ 9r'99 20:21 n.Goodrich 625 2087 00001 K" 0Cl/1 10. 10. 1 12/ 9/99 20:21 M.Goodrich 625 '2087 P;0•ene RD ug/1 10. 10. 1. 12/ 9/99 20:21 M. Which 625 2037 B; s?2-ethg0 he. ga>phthalate o[I bq/_ 10. 10. 1 12/ 9/99 2121 11.600drich 625 2087 .." �-iri,;hloroh?ncen� HD UVl 1U. i0. 1 IV 9r'99 2121 M.Goodrich 625 2067 ichiorophenol RD !iq",1 10. 10, 1 1219i99 2121 M.Gotabich 625 2087 iC1DL,,,/PlUcf. 'NcVItLf..?'1ESit ril drin HD oG/1 0.05 0.05 I L/ 5i99 i.t:SO M. Cauthen 608 2258 d! oc1,r 100 ilD ony'l 0.50 U.50 1 121 7197 OA5 M. Rogers 608 _701 Arocicr L221 HD w7 1 0.50 0.50 _ 121 N99 it45 1Rgers i,06 2701 ai�,oiar 113.1 8D uG/"1 0.50 0.50 1 1.2/ 799 19: 45 M. fingers No 2701 Aroeloi1247 RD Uq/; 150 BAD 1. 121 7/99 .IT45 n.Rogers 608 2701 arocinr 125E 1!D u9/1 0.50 0.50 1 12/ 7199 17:45 I1.Rogars No 2701 aroc:L,P 125. HD ocill ISO 150 1 12 i 7i99 OAT I Rgmw 603 2701 MCI. 060 HD ud/I G.to U.50 1 12/ 7/99 1195 n.6ogers 608 2701 e-!MC NU Un/d 0.05 0.05 1 121 5199 11:50 M Cauthen 608 2258 h';IHC No 09/1 11.05 WAS 1 121 5193 11.50 M. CauthPn Goo V56 HE HD U1111 0.05 0,05 1 121 5/99 1110 M. Cauthen No Z:'S8 I-BHC, Li;M-,mz HD uG• 1 0.01 U-US 1, 12/ 5199 1110 M. When NU U50 ;: i,Inr daue HD o:lil 0.0.5 U.0`i 1 12/ `ii 99 11:50YI. Cauthen HEM 45 WD RD o/l (),Ia 0.10 1 171 5i99 II: so A Cauthen 60 Mo 4g-CDC HE, ugil 0.10 0.10 1 121 ";/99 11:,`;0 11. Cauthen 6,08 2258 ,I•:a'D::%I HD Ug/1 0.10 0. 1U 1. 121 1/99 11:50 M. Cauthen 608 2756 Dle'l.drin R0 UVI I1.to KID 1 12/ 5/99 .HAD M. Cauthen No 2P53 . an cli: r V Ilort_ Lx,::; 1. rar d , . COPY 1 SPECIALIZED ASSAYS, INC 2960 Poster Creighton Or P.O. Box 40566 Nashville, IN 37204-0566 Phone 1-615-726-0177 AR';!.�ibr Roiult Units EnooStr..fan i. r;P ugr'i trdosulfan 11 i1C uQ/l c ndusti if an >ul"ate kD ua/1 L a6rin 80 ug:'1 C.ndria n3,deitgde 80 oil] He lti'3Chl or RD ogi'1 !Jrptacnli,r EimaSde 8C ugll Tm:apheRe •rt0 uge'l i?G < Nc:t dr=tected atthe rgiurt knit. Eahple btl'utlon Data RCYUd 4r aneie7 x rT?(;ied Est:i atA Vol DNA's `!..110 Hi 1..11 ril Pestic i4es 50i!. hl 5.00 tiL FIX, '; r;r,U. hi 5.00 r11 <orrogate ANALYTICAL RHPOFRT :-aboratory Number: 95-A182839 S �3 imp ie 1 D : S'LC31-ii C.1 P6ye 3 Report Ruch Oil. Lihit Utlit factor Date Time 9hily>t 11"thod Oatr:!i 0.05 0.05 1 12/ 5l99 11:50 it. Cauthen 608 7-'.8 0..10 0.10 1 12/ 5/97 11:J0 M. Cauthen 608 2258 0.10 1t. 10 7, 12/ 51199 11: 50 M. Gaut hen 603 M,8 11.10 0.19 i 12/ 5/99 i1: 50 n. Cauthen 609 22510 0.10 0.10 _ 12/ 5r99 11:50 n. Cauthen 608 2258 0.05 0.05 1 12/ J/99 11:00 n. cauthen 608 2258 O.OJ 0.05 1 121 '197 11:59 M. CButfRn 609 22J8 5.00 5.00 i 12r 5/99 11:50 M. Cauthen 608 2258 Date Analyst metiw,l I'll 3/99 P. Terry 3510 12/ 3/94 D.Yeager 8510 12r' 3/99 C. Terry 3519 Y. Eecuverg Target flange surr-kitriaen7one-dJ 72. Ili - 10J. .Oi•! .-FiUiir!iiipl'inlj? 7b. 17. 110. 5o+'r-tar�ilr:vnll dL9 Si. 1(1. - 1'i6. a1rr-i'henul. 65 surr-2-Fluorcgihenei 39. 9. - 100. t.;rr-2,4,6-';TitmoitGphri;G.i 91. 1.J. - 131. iir.t sur3-101% 5r. 20. " 122. sorr-!'ihut�;L:a?ioreneate 53. lrl. - M. COPY 1 SPEIClA[|2EDASSAYS, INC. 2wopw*Creighton Or xuBox 4o56^ wolnrocr*nuw��o^ � �P4 ^ L— -y' -F 1 L— ���(D�� Laboratory Number� 99—A1S2539 Sample ID: ?L031-001 Page 4 reia�e only �u the testetl. (ois /epnr( s:olL not L)e reprrduceU except In ful1 aod m{th permlss1on of the labaritorg- F,*p1., 4pp,eport nate: lZ,15/?9 71heodure J. Duello, Ph.D. , Lob Director Michaol H. Dunn, U.5. , Technical Director Johnny A. Mitchell, Dir Technical Services �r1c 3m1tk/ Assistant Technical Director 5ail 6 Laye/ Technical Services iabnrator9 Certification Number: 387 r"U o�* �;amp I keJ10ri 11 NPDES Analyses, Aquatic Toxicity Testing, Field Services, Infrastructure Evaluation, Chemical Product Environmental Assessments, Toxicity Reduction Evaluations BURLINGTON RESEARCH ANALYTICAL REPORT CUSTOMER: Huffman Finishing REPORT TO: Mr. Lee Huffman SAMPLE DESC: NOV. MONITORING SAMPLE TYPE: WASTEWATER, EFFLUENT GRAB COLLECTED: 11/30/9907:40 SITE: Effluent WORK ORDER #: 9LO31-002 RECEIVED: 12/01/99 REPORTED: 12/ 17/99 Ilil�l�L�l:3�:ii PARAMETER DATE/TIME/ANALYST MOIL RESULT Cyanide, Total Started 12/09/99 10:30 0.005 <0.005 mg/L EPA 335.2 Analyzed 12/09/99 by MTT at BRI - Burlington Phenol, Total Started 12/02/99 08:30 0.005 <0.005 mg/L SM-5530C 18TH Analyzed 12/03/99 by TAR at BRI - Burlington Purgeable Organics, 624 Started 12/06/99 15:12 Attached EPA 624 Analyzed 12/06/99 by SAI at See attached MQL = Minimum Quantitation Limit Certifications: BRI - Burlington NC Chemistry: #85, Biomonitoring: #002, Drinking Water: #37743, Radiation License: #001-0904-OG VA SWCB ID: #000061, Drinking Water: #00018 SC Laboratory ID: #99042 EPA Chemistry Lab ID: NCO0137, Bioassay Lab ID: NC2721500 Burlington -Corporate Offices Eden 1302 Belmont Street • Burlington, NC 27215-6935 Page 3 370 W. Meadow Road Eden, NC 27288 Phone (336) 570-4661 • Fax (336) 570-4698 Phone (336) 623.8921 Fax (336) 623-5878 09-2 c9') SPECIALIZED ASSAYS, INC. 2900 Foster Creighton Dr. P.O. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726-0177 .3i: PL I rNGTON RESEARCH, INC 2100 WAYNE ALTHOUSE !302 SELMON`f ST .., Jf'.:- l t':`J 'iJ ITV, 1'J G ['_ / 72 G 1 ... "Weat Name: _ampler S(1' Result Units J$,TLAIIL E 11KP.MCf:) ANALYTICAL RIEPORT Lab Number: 99-A1821340 Sample ID: VLO31-002 Sample Type: Water Site ID: Date Collected: 11/30/99 Time Collected: 7:40 Date Received: 3.2, 2;'99 Time Received: 9:OD Report San Dil Limit: Limit Factor MENU Hi) UPI 10. 10. dcrglonitriie RD Up/1 10. 10. leazehe RD UPI .. J. ;lru"oforh HD Ug/1 5. 5. ttPPmOmet h aw RD UPI J. 5. ua?bcn i[A.Tachlcride RD U4/1 5. 5. . Y.i E:rt:'JV 11iCIIC 131! IfV/1 J. ,A. Lacc,'cett:ai:e �:D up/1 1D. ;,. -C h I C F0(-t b Q V In filet lien' HD UPI .. 5. Ctll.oroforrc 12. Ug/I 5. 5. C h3.orowt.hfhe 'RD U:je'l :�: br0nmi hloromethihe 40 ogn 5. 5. ,2-D i c t110ro be o2e ne RD U9/1 5. 5. 1,3-Gechiorobenzene 8D ug/l J. 5. i ,9-UichlUrahen�e nE' 8D U9,'i 5. 5. Dichlcra d: Pluo:ronel:hahe RD Ugil 5. 5. i -Di'c!;lu,'oet:lai:e RD UPI 1 5. :-DiChiC'i'OeTtfane HD un/i .. J. .,.-Glctueroet barn: ND i !I 9. ,. 5. .7_Di,;hlcr/;etha na (rotai) HD ugll 5. 5. _,:. G 89 Ug/1 5. 5. :is •3-Dull ioprE'pehe HD Unil 'i. trans-I,?-D10h10rupropeo,; RD U4/I 5. 5. Cth9lbenzene RD Ugl1 1eeh9lene rAloridp HD ,gl1 10. l,U 1,2,2-1f'trac!aoroetItane RD UPI 5. J. fetr'achli,rotitherle 110 U9;1 5. '1 izd uene ND U4/1 .. 5. • 1': r' I u I'l ")roe t tl J l l:' FD u9/1 )'iiQ:dcrwth3ne ny: v4e'l uriie thE•i:i' ri7 U4/I .. ,. di L'�I uKr-1 de F-1 i'ti/I 10. ,.9 RM-, K% 0g:'1 5. 5. Date line 911al9st net'hod Dater, 1 12/ 6/99 15:12 S. Wani 624 52:3 I 12/ 6/79 15:12 S. Mani 624 523 1 12/ 6/79 1.J: 12 S. Want 624 523 1 IV 6/79 15:17 S. Mani 624 J73 .1 12/ a/99 1112 S. Wani 62q 527t 1 12,1 6/99 15:12 S. Wani 62q JZ_l 1 IV 6/9Y .15:17. S. Want 624 V1 1 1.2/ 6/99 15: 17 S. Wan 624 J73 1. iZ/ 6/99 15: 12 S. Want 624 523 I 12Z 6/99 15:12 S. Want 624 523 1 12/ 6/99 15: 12 S. Rani 619 573 1 12r 6197 15:12 S. Wane 624 523 1 12/ 6199 15:12 S. Wani 624 JZ3 1 12/ 6,/97 15:12 S. Wane 62q 523 1 1?/ 6.99 15:12 S. Ran! 624 S3 1 121 6r'99 15:12 S. Wane 624 523 1 121 6/99 1112 1 New 624 521 1 121 6/V9 15:17 .+. Wahl 624 li73 1 IV 6179 15: .11 S. Want 624 J23 .1 12/ 6/99 15:12 S. Want 629 523 1 12/ 6J95 15.12 Wahl 629 J23 1, 12/ 6/99 1S 12 J. Want 679 573 1. 12/ 601 1112 1 Wani 624 523 1 12/ 6/99 15:12 S. Wane 62:4 523 1 12/ 6/99 1512 S. Wane 629 523 1. 12/ 6/99 15:12 S. Wa111 671 J23 I. 12/ M 15:12 S. Wan.l 629 523 1 121 6/99 15:12 :. Wan! 624 J2-1 I i2/ 6/5'9 15:12 S. Wan! 629 523 1 12/ 6/9F 15:12 3. Want. 624 J23 1 121 6/99 15: 12 S. Want 62q JZ3 1 .17/ 6/'99 15:12 S. Wall 624 523 1 12r' b(99 3.5: 12 .:. Want 624 523 SPECIAIAZFD ASSAYS, INC 2960 Foster Creighton Dr. P. O. Box 40566 Nashville, TN 37204-0566 Phone 1-615-726.0177 .G5L- F:e�Ult Llliit5 �Irioo Co 41oronP•t ll ane HD u9il )riuMC'POHIocronetttarc- N.D ctg/1 A'•.7 : Hb)t 1, terteA it I -pa 1"f:pGi't limit. ;Ir cgal l'i)N iurrojAe, 7.,2-Uichl.oroethane, d4 !'i!N Sorrogcte, ?olueac• d0 VOR Siii'S'GgaCP, 4'Lii+;:ryGFiIiOPGhenLF nr P.IV AL YT=CAL RAP OR'T L-.a,ora tory Number: Yv—A 1821890 Sample iD: e7L031--00;' Page c RepuTt Buan PH LIHit Lltilt Factor Date flue Analyst tlet. hcd Batch 5. 0 1 121 6i99 15:12 S. Aani 624 523 ,.. .. 1 l2/ 6/99 15:12 5. Am 624 523 YL recovery 61. 104 71. Target Range 61). - 138. 80. 123, 73. 122, 'he results relate only to the items tested. This repc:rL shall not be reproduced except in full and .with permission of the laboratory. R-e poT t. +pprCvtri! 9t:1:'dt— a.�, __ Report Date: 1'2: 15; 99 Theodore J. Duello, Ph.D., Lab Director Michael H. Dunn, M.S., Technical Director Johnny A. Mitchell, Dir. Technical Services Eric Smith, Assistant Technical Director Gail A Lage, Technical Services Laboratory Certification iumbei: 387 L r: Ci •-0- Sample Rep Ot•t. COPY 1 •J 13023el ion c :: _j 370b,- IAe9f R, ! ®II L'INnqion. IJC -]569 he n NC72RP Phnnr.(l46)niU Iyi) 'no,1 (3fnt �lin'.I BURLlNGTON RESEARCH INC. Fax (3313)570 4GUS Fa Y (336)r 3 :37a • o 0EM o OI CLIENT: Huffman Finishing Company Facility/Site: Wastewater Treatment Plant_ Sampler: (Print) S . Wise (Signature)� J ;oo c, cnn s et Kin on t C ' 3J01 'Fnr ( K'')'i:°. I goo SENDREPORTTO: Lee Huffman (copy S._ Wise) --_ Phone:-_(_8.28-)_3.9.6_l-7_41 Fax:.(.828-)_396- Purchase Order No.: Verbal Lee Huffman SAMPLE ID w z o f rn x SAMPLE COLLECTION Q LL z D o 0 n" a,- J 1 O wQ0 SAMPLE TYPE o w w a z n z N M z. z� ANALYSIS REQUIRED -- 1�03� r w a w w _ z TEMP. 4o C ( ) Preservation Codes: A = Ice E = NaOH B= HNO3 F =None C=H2SO4 G=CUPRIC D = HCI H = HCHO COMPOSITE GRAB STARTED ENDED DATE - TIME DATE TIME HAND AUTO Effluent Yes No A: 11 /29/9 0Z5D_ l l /30/99 0730 2.5 X 4 41 CG; f+ vG 608, 625, Metals fJ Effluent Yes:No XI 11/30/99 1.1/30/99__ 120 X 5 CN, 624, Phenolics, GA Yes: No Yes: No Yes: No VesNo Yes: No Yes: No ._._..._.___._ ............ ...... ...... ....._...._.____ Yes; No Yes: No Was the sample dechlorinated at time of collection? Yes I1XJ No LJ Will the results be used for regulatory monitoring purposes? Yes LJ No U CLIENT USE ONLY Relinquished by: ISi JIFOR I Date: 11 30 99 Time: 10.35 am Shipped by: (Sig.) _ Huffman Received by: (-Sig.) — _ _ - __- ._ _ Date: __ll/30/-99_. Date: Time: — _ Tlme: Method of Shipment UPS Received in Lab FROM: (Sig.) Date: Time: ethod of Shipment L 2S 7 :Receiver L (Si .) g D�te� �j /,(,j a� 7� T/� Sampl Integrety Commet no r -'Ja White - ORIGINAL - For::ard to BRI - BRI will return to client v^,ith Final Report Canary - BRI - Labotatot, Pink - BRI - Laboiatory Goldenrod - Client - Copy Whole Effluent Toxicity Testing Self -Monitoring Summary May 16, 2001' FACILITY REQUIREMENT YEAR JAN FEB MAR APR MAY JUN JUL AUG SEP OCT NOV DEC Hay Sprlaas W WFP Pam cG lm: 90% 1997 _ _ — — _ _ _ NRM..a _ _ qra — NC0063U%001 Begm:3/111991 Frryuacy: Q PT + Feb May Aug Nov NmCo ar Smgk 1996 — NR1Paw• _ _ Pura _ _ Fee raw — Pw — Cwmry: Wabr Regina RRO Subbase. CPF02 INS _. Pecs — — Pre _— PF:0.5 Spew 20m _ Pas — — Fa Jab >100.>100 Pw — — has — 2Q10:00 IWC(%):IW aaw 2001 — Pre - Heeey.ve0latenamaal,laf, Peon 48M LC50 a lim: 9o%(Cerio or Daphnia) Im .10* — — -I% — 74.10 26]1 40M >100 -100 — — NC00018991001 Bagiml2/1/1996 Frequmcy:Q + Jw Apr JWOer + Nm(Cmp:S.We IM »m — — .100 — — 82.56>1m >10) — >100 — — Comfy : Clefaha , Region: RRO Subbaum CPFO'/ 19N 36A >100 — >100 — — .tm — — >100 _ _ FF: 0.244 spina 2000 »m — — >100,100 — — >t00 — — >IW — — 7Q10:e0 IWC(%)U.% Owe' "1 -125 12.5 a100 >100 H..e,weO latrnaOoeal, I.. Prom 241br W50 ae moil pis Md urab) INY _ _ _ .IN — _— N0001899/002 BegiwlVIII996 Froporcy:A N9nComp: 1106 — — -- >100 - — — — — — — — Comfy: Camara Region: RRO SWdaim CPF02 1599 _ _ — >1m — _. _ _ — — — _ FF: NA Sprrw$ 1000 — _ _. .100 —- 2Q10:0.0 IWq%)NA OWw: 2m1 — — — vim He,k Creek WWTP Perm cylim: I I%; if PM 075 chr IM la% IN2 — — Paw - — Pas — — P. — — Fee NOOal615/001 Begin:&1/1995 Frequncy:QP/F + Mu Jun Sp Da NmC_':Single 19% — — Pau -- — Pecs — — Paw — — Pw Comfy: Unaron Region: MRO Subbann: Cf935 1999 — — Pae — - Pass — — Pee - — B1 PF: 0.075 SMW 2m0 — Pw, Peary — — Pan _. _ Pus — — N". 7QI0'.092 IWC(%)'.I10 aan 2m1 — — Pw Heamaa F6YlaR Pam: Uhr LCM ae Iim 96% Y INY e12 S >N Nd — — fin •9. -NC.W25135N01 8egio:8/1/1W3 FrbWapa�:Q + Ma Jw Se Da nq: NmCa9lildp' 1990 — — .96 — — .96 - — >N Comfy: Caldwell Region: ARO 9i06aam CTB32 INS — — 26.Y >N — 1.6 -� — >96 — — NRVvN W-, 0.25 smai 2m0 am ... .tin — — .100 7Q1e 00 IWq%)O.% ()ore, 2ml — — Hyde Got, Fairfield Plus Perm cbr monk 9 . IN) NCOm8233A01 Begm.3/1/3001 Fre,aamy.Q Mal. S'D, r N..C.P:5.0, 1. — — — — — — — — — -- - — Comfy: Hyde Regym WARD Subima. TARO] INS PF: 0.10 spwul 2iw0 1QIO'. OU IWC(%):Ion (MYc 2001 — — Fail HY& Canary Pesar Pall Pmnchrmotul: WA IW2 _ NO077Y92/IJJl Hrgin:3/I4!00I Frequenry:Q Feb May Aug Nov + NwC.P:Sm B' 1995 — — — — — — — — — — — — County Hyde Regim: WARD Subbuin: TARO] 19% — — — — — — — — - -- - — PF: 0.109 Spew- 7Q10:0.0 HVC(%yw.o Order: 2m1 — — Fail HIP F.W. Perm chr run: WA 19BY Fw — — Pw _ _ lay Fr. — P. NOo0T1511001 Begmlll1/1996 Fmqurary:QF/F + Jan Apr JWW NoeC®p:Sbgk 1996 Pw — — Pw — — Pw — — Fall Par, — Comty Bad. Region: WIRO Subbef in: CPM 1999 Poaa _ _ Peary _ _ Pun _ _ P. PF: 0.65 SprW 2000 lay NRIF" Fed Fan .tin .tin 622 9,81 .Ion 919 — — 1QMBa IWC(%):IW 0&r: =I .tin — — ladotdal k A¢ricalmral Cbemleak PERM: 48M LC50 AC MONK CERIO OR DAPH (GRAB) S 1997 — — 20.1 — — NR/69.5 — — M — -- — NC000023N001 Begim2/I/19941 Frtquercy:2 R Seomeraal NmCmlp: I99B — — r125 — — — — — 504 - — - Cowry: Robeson Region FRO Su avwixr LUM INS — -12.5 — — — — — - — — — <13 5 PF: VAR sperW 2m0 113 NR 7QI0:0 IWC(%kNA ONw. 2ml — 0.125 — In¢eraB-lynNSchla¢a Corp. Peml-le, rim: WA(gmb) 1997 NR H N H NC0029221N01 Begin:&1/2m0 Foolmyry;Q Feb May Aug Nov + NmCorm:Sygle INS — H — — Fad Pw — Pace — — pass — Gwty: Naab Ragi0m RRO SWAasin: TM02 1999 _ Pre _ — Pae _ _ pan _ — Pm ff 0.124 SprW 2(ao _ Pee _ _ paa _ _ Pea _ _ P. — 2Q10:0.0 IWq%):IW.O Uaw. 2mt — Pass — Iolematlonal Papa Co. Porn cbr lan: 8% 1N, Faa — - Pra — — P. — — Pea — — NCO003298/ml Begin:3/1/1992 Frequency: Q P/F + Jan ApfJWOa + NmC=p:SitWe 199E Pr. — — Pee — — P. — — Pas — — Gun1y: Columbus Rcgima WIRO Subbasi. CPF11 19N P. — — P. — — Pw — — NRAWa 459 — PF: 50 spra 2000 Pw _ _ Faa — — Pw _ _ P. _ _ 2Q10: 8% IWC(%):8.3 nuke, 2mI Fw — — LEGEND: PMtM =Permit Rcquimnrnl LET= Adminoumvc Lmm- T3grf Frew.y= Mini" f".y. Puwler Qly; M- Mmlhly; BM- Bmxmbdy, SA-SemwnuallY; A- Alma y; OW Owm diw y wbhapyyp D- Dlacm0mm md aibmg nmgm creel BIW1CW.ftIocivm, uy low now ntrmim�m(cn) Paa/FWI�ACulemCMt= �nic nilenng- o Acly�MMmNslMt wring mug occur-ex.Jo, Apr, JuL Oct NonCmnp= Currni Cmlphame Reeluormnt PFp=Permitted flow MGD) PiF- Dam Nootbon f- Faa d Mimow; • - CeldodpMia sp.; my - Mysid sMr ; GV . Cl is valw; P. Morality of emend percmmge at Mglmal co10en"tiom at- Perfomwd by DWQ AqN c Toa UoiO M - Bed text Reporting Noudm: — - Dam sot mgWmd; NR - Nm manned Facility Aeuvity Sala:1- mauve, N -Newly laymIbT0 com6ua); H - Ar6ve bw sot dimharging 1-More dam available normal, in quesMn; • e ORC siglm m, vuedcd 26 Whole Effluent Toxicity Testing Self -Monitoring Summary December 18, 2000 FACRFFY REQUIREMENT VEAR IAN FEB MAR APR MAV JUN JUL AUU SEP OCf NOV DEC Has, RWee Iii Perm clor him: W14 (Grab) lme Fail FA Fall FY Fat Fat Pas Fan Fars - - Fail NC%25895N01 Bep.Wl/1996 Fr tfuerlcy: Q PT + Ma,/.Si NonComp:Svele IM Pat! Fall, Pra - - NR/Lela FIT Fa,l Gee Fan Fan Faa Country: Orlow Region: MR0 SubbaNn. CPF24 lm Pre - Pm - - Pre - -. Fee Fail F. Prat PF: 0.1 S uu 1BW - _ FJ FaY to lab Puri - Fan P— - Pau ]QIU: RO IWC(%):1W ana: 2000 - - Pat - - Fat >100 - Pan -- HuIly Sprlaea W W FP Pam ehr him: 9CF4. INN - _ - - _ _ - _ NC00610ti Begia:3/DIM Freq y: QPT a Feb May A, Nov NmhConhp:Smpe IN? - - _ _ _ _. - NPIPexx - _ Pau _ Comfy: Wake Repm: RRO Subtotal: CPFO] 1968 - NPLPa.• _ _ Pau - - Fail Palx -- Pau - PF: 0.5 saxw 1m Fan Pau Paw Pna - ]Q10:0.0 IWC(%):IW amer 20W - Par - - Fail 74.8 >1W11110 Faro - - NreeywcBlatraaOeaaLlx Perot 48hr LC50 ac have 90%(Caio or Daphnia) 1885 e125 w25 IF." >IW - - MAN 2P.0 03,05 -IN >hW - NCW01899Io01 BgativIllim Fogarmy:Q + I. Apr Jul Oct + NomC'amp'. Su181e 107 >1W - - >100 - 74,10 M.]t ally" a1W -IN - - Corty:Chatham Region: no Sabi CPFO] tllfa>IW - - IN - - Pt.511l >1W - IN FF: 0.244 SIxel 1659 0BA >1W - >100 - - >1W - - >1W - - 7Q10: W IWC(%)9.% area: tom >100 - - >1110,100 - - -IN - - IN Nraaywell lnemotil 4late. Pam 241r I.C50 r.1 Flair Obd(gab) 19W _ _ - IN - - - - - - - - NCgW1899IW2 BeginlV111996 Frmluamy:A NonComp: 107 - - - -IN - - - - - - - - Coady- Clhea b u Regular: RRO Subbaxi. CPFO] 1655 _ _ - >1 W _ - _ _ - - _ - PF: NA SPxltl I'm _ - - >1W - - - - _ _ 7Q10: 0.0 IWC(%):NA ada: 200K) _ - _ >I00 - _ - Hark Create WWIT Pamchrion ll%;if PF>0.0]5chrliml4% 1596 tale Pen Pas - - Pau - azs - - Pasc NCW41815A01 BI&VI/Plan Frequency-QPN + Marlbh Sep Dec NohConp: S'vhpe Iw] - - Poor - - Pat - -- Pass - - Pau County: Inhale Reglor, MRO Subba+m: M35 INS Pr Pasc - - I— - - Pass PF: 0.075 Swat IM Po Pass - - Pau - - 81 7Q10: 0.92 IWC(%):11.0 ceder: POW - Prx Prior _. Pea - - Pnsa -- Nalfmaa nalai Peorreabr LC50rlun96% y I998 NOW25115/WI Begin 95 V1119F1olm ury:Q + Marlun Sep Dec NohCa up Strafe IW1 t25 ag5 88 >5a - > - - Coma". Caldwell Region: ARO Subbaein: M32 rr >% e >98 - - >p5 PF: 0.25 speFial Im _ _ I6.1 >% - >g5 _ _. >95 - - momw 7Q10: 40 IWC(%).V+% arise-. AN _ _War >100 aIN - IBPFael. Pclmclrlim:W% I9118 Paaa - - Pan - - Pass - - Pacs - NCOaFF737A101 Bge:Il/l/1996 nequecry:QP/F + Ion AprlWOet Nauccan'Single I95P Prx - - Pas - - tale Pt Pass - - Co rty Dubw Region: WIRO Subbann: CPF23 1995 Per - - Pal - - Pat - - Fan Pass - PF:0.65 Faxul IM Prs - _ Pm - _ Pau - - P® 7Q10: 0.0 IWC(%):IW Order: 20W Ina NWFaa Fail Fat >1W IN eP] May >1W ".a IadanrW 4 ARricoRaral CSenitB PERM: 4101 LC50 AC MONK CERIO OR DAPH(GRADIS IM - - -115 - - - - - - - - -625 NC0000216IWI BeouVl1l9'N FFeP,F :2/VR SardemuW NonCcma 195J - - 21.1 - - NR/Sfl5 - - 51 Comty: ledbamn Region FRO Sulbtme LUM t886 - - a12.5 - _ _ - _ WA - - - PF: VAR Saeid IWB _ OZ5 etPS 7QI0:0 IWC(%):NA amen 2030 - - - - - - - - - - bgelteB-RtadISeWRe Care. P. clr lime 90% 1pab) 19% Par, Pohl - _ Law Pma - Pre _ _ Pat - NCUO]922]NOI 184.11IR000 FlatmeatiQ Feb May Aug Nov + NonCon'sawe 1597 - NR - - H - - H - - H - Colmty. Ntab Region: RRO Subbasin: TAR02 1598 - H - - FM Pet - Pas - - Pea - ff 0.124 i amw 1996 _ Foe - - Pax - _ Prat - - Par _- ]Q16.0A IWC(%fIW.o ceder 2oW - P. - - Par - - Po - - Iatersllpxtl Paper Co. Pam c)a him 8% 1925 Par - - Para - - Prx - - Per - '- NON032910101 Bepm Y1J199] Fromm: Q P/F + Jan AprJWM + NeoConPSiugle 1997 Prxa - - Par - - Pax - - Pas - - Cam1y. Colunlbm Rgo. WIRO Subbuin: CPFI] 1895 Paw - - Pa - - Po - - Pau - - PF:50 Spacial IM pre - - Para, _ _ Patte _ - W4Aah, 451 - 7QI0:856 IWC(%)B.J odx, 20W Pw - - Pm - - Pat - Pan IMerariral Paper Co. Perm cbr lim: D% 1695 N NCI BIM7N01 Bg.7/111ii Prefixal Q PIP + but Ape Jul Der + NmClanp:Smpe ISSI N C.". New Hour. Regan WIRO S1bba®: CPFI] 19% N PF: 0.05 Saeeid IM N ]QIe. 0.11 IWC(%)37 a9m 2000 N - - N - - N - - N N - - N - - N N - - N - - N N - - N - - N N - - N - - N LEGEND: PERM=Pmnit Requirement LET=Athninutrahive Later -Tugs Frequal- Modbrivg fmlatal Q- Quarterly;M- Mwthly; BM-BbmahIY: SA- Semi®mW1Y.A-Mwully, OW6 Only•'Lm diaclwgme;D- Drearmarom mortuaries requimrcnt Beg' - Fim month required ]QIO - Recetve, aveam low Oow From(e4) m - gtwaiy wldbnng horeaa to monthly upon Gilm m NR Month that extmg maw actor -ea Im, Apr, Juk Oct Nwa lamp = Carol Canplirce, Requirement PF=Permiued Dow(MGD) IWCK=Innrtm wase cohrenmtioo P/F=Paxi test AC=Acne MR -Chronic Dbz Noulien: F. Fathead Mirmmi • - Cmodephom sp.; my - Mysid MnW; CIV - Cluonic valuc; P - Morality of sued percentage at bight, eeoeamttim at- PerfomN by DWQ Apatc Tax Unit; N. Bad test Reaming NW4on:-=Ueu mirequirtd; NR-Not repmaW Facility ActivilYSubx: 1- frame. N-Newly ballet emtma); H - Active but mldi¢hrgine:]-Mom dab available formouth equoura. =ORC signafun needeJ 25 MAR-19-97 WED 10:58 TOWN OF GRANITE FALLS FAX N0. 7043863133 P,DI March 19,1997 TO: lames R. Reid Noah Carolina Department of Environment, Health & Natural Resources Division of Water Quality 59 Woodfin Place Asheville, North Carolina 28801 FROM. M.S. Wise HudFinan Finishing Company P.O. Box 170 Granite Falls, N.C. 28630 SUBJECT: Notification of Change in Effluent Discharge Location, NPDES Permit 9 NCO025135 -c �n rn Dear Mr Reid: x - Effective this date the Huffman Finishing Company Wastewater Treatment Plant k' i effluent discharge point has changed from a location approximately 100 feet from r� �• the treatment facility which discharges into a small tributary of the Catawba River a� to a location approximately one mile east of the treatment facility which discharges ; a directly into the Catawba River. Effective April 1, 1997 Huffman Finishing Company will monitor this discharge as stipulated in the final monitoring requirements of Cn their NPDES permit, (NC0025135) If you have any questions regarding this matter please feel free to contact me. Sincerely, Li MS. Wise MSWIsw cc: Lee Hufinan n' 9.