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HomeMy WebLinkAboutWQ0004270_Monitoring - 08-2020_20200831hart '�4 hickman SMARTER ENVIRONMENTAL SOLUTIONS Via USPS August 19, 2020 NC DEQ - Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Semi -Annual Sprayfield Sampling Results A.B. Carter, Inc., Permit #WQ0004270 Gastonia, North Carolina H&H Job No. ABC.026 To Whom It May Concern: On behalf of A. B. Carter, Inc., enclosed are the results for the August 2020 sampling and analysis conducted at the above -referenced facility. The only constituent detected above standards was pH which was <6.5 in all wells. These pH levels are typical for this site and have been determined to be background for this facility. In accordance with the permit, the next sampling event will be conducted in February 2021. If you have any questions regarding the enclosed results, please feel free to give me a call at (919) 847-4241 or Lee Pennington of A.B. Carter at (704) 874-2754. Sincerely, Hart & Hickman, PC CX Z"M "'ee C . %' I o Ail _ Leonard C. Moretz, L.G. U Senior Project Manager Attachments Cc: Mr. Lee Pennington — A.B. Carter, Inc. (1 copy via email) 2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301 Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com 704.586.0007 main 919.847.4241 main GW-59A COMPLIANCE REPORT FORM Permit # W00004270 (.Submit one each monitoring period with GW-59 forms.) I Enter date monitoring results were due. (9-30-20) Will this monitoring report (GW-59 and GW-59A) be NO submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing NO identification plate, area overgrown, etc.)? If the answer is "Yes ", conincl the Regional Of,f ce for guidance. 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO" skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW-19: pH = 5.49, MW-20: pH = 4.91; MW-21: pH = 4.79 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO'; skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW-19: pH= <6.5 (8/2/18, 2/7/19, 8/13/19, 2/19/20) MW-20: pH= <6.5 (8/2/18, 217/19, 8/13/19, 2/19/20) MW-21: pH= <6.5 (8/2/18, 2/7/19, 8/13/19, 2/19/20) 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. pH has historically been low and this has been discussed with DEQ — determined to be background conditions. 7 Is the permittee implementing previously approved actions required by the Division involving this NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is havina at the review and compliance boundaries surroundina this facility, Failure to do so may subject the oermittee to a Notice of Violation fines, and/or penalties. 8 The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. Q August 19, 2020 Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: . • • DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: June 30. zozs Facility Name: A B Carter, Inc Non -Discharge W00004270 UIC Permit Name (if different). NPDES Other Facility Address: HWY 321 South Gastonia, NC 28053 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery County Gaston El Spray Field ® Remediation: Contact Person: Lee Pennington Telephone#: 704-865-1201 ❑ Rotary Distributor ® Land Application of Sludge Well Location/Site Name: Sprayfield/A.B. Carter No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-19 Date sample collected: 8-4-20 FIELD ANALYSES: WAS DRY Well Depth. 50 ft. Well Diameter: 2 in. pH 00400 5.49 units Temp. 000lo 18.2 oC at time of sampling, Depth to Water Level 82546. 37.59 ft. below measuring point Screened Interval: 40 ft. to 50 ft. Spec. Cond. 00094 459 uMhos check Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: 737.59 ft. Odor 00085 none here Volume of water pumped/bailed before sampling: 81 gallons Appearance clear Ll Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: [D YES ❑ NO LABORATORY INFORMATION Date sample analyzed: ea-20, 8-5-20, 8-6-20, ea-20, 8-10-20 Laboratory Name: waypoint Analytical Carolinas, Inc, Waypoint Analytical Tennessee LLC. Certification No, 402, 415 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 <50 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 Q CFU /100mL Nitrate (NO,) as N 00620 74 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.24 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 270 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1 00 mg/L Ca - Calcium oo916 mg/L Chloride 00940 19 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 110 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? El Yes (1) ❑ No (0) Specific Conductance 00095 uMhos K -Potassium 00937 mg/L method # Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH, as N. Ammonia Nitrogen. Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facility Name: A. B. Carter, Inc Permit Name (if different): Facility Address: HWY 321 South Gastonia, NC 2805: ntact Person: Lee Pennington !II Location/Site Name: Sprayfield/A.B. Carter Please Print Clearly or Type County Gaston Teleph one#: 704-865-1201 No. of wells to be sampled 3 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-1307-6306 PERMIT Number: Expiration Date: JuneK 2025 Non -Discharge W00004270 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation. Infiltration Gallery ID Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MW-20 Date sample collected: 8-4-20 Well Depth: 50 ft. Well Diameter: 2 in. Depth to Water Level 82546 44.34 ft. below measuring point Screened Interval: nodata ft. to n°data ft Measuring Point is 2,5 ft. above land surface Relative M.P. Elevation: no data ft. Volume of water pumped/bailed before sampling: 2.73 gallons Samples for metals were collected unfiltered '❑ YES ❑ NO and field acidified: 0 YES ❑ NO LABORATORY_ INFORMATION FIELD ANALYSES: pH 00400: 4.91 units Spec. Cond. 00094: 507.6 Odor 00085 none Appearance clear Date sample analyzed: 8A-20, 8-5-20. 8-6-20, ea-20. 8-10-20 Laboratory Name: Waypoint Analytical Carolinas, Inc. Waypoint Analytical Tennessee LLC PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Temp. 000lo: 18.1 °C uMhos Certification No. 402, 415 COD 00335 <50 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <2 CFU /100mL Nitrate (NO3) as N 00620 3.3 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 039 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 703oo 330 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC o0680 1,30 mg/L Ca - Calcium 00916 mg/L Chloride o094o 36 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC GC/MS HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 160 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? El Yes (1) ® No (0) Specific Conductance 00095 pMhos K - Potassium 00937 mg/L method # Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH, as N: Ammonia Nitrogen, Total) Mn - Manganese oloss ug/L .method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs mg/L VOC Removal% Leonard Moretz, Senior Project Manager - Hart & Hickman, PC Permittee (or Authorized Agent) Name and Title - Please print or type of Permittee for Authorized Age 8-19-20 (Date) If WELL WAS DRY at time of sampling, check here: GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: A. B. Carter. Inc Permit Name (if different). Facility Address: HWY 321 South Gastonia, NC 28053 act Person: Lee Pennington Location/Site Name: Sprayfield/A.B Carter SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-21 Well Depth 49 ft. Depth to Water Level 82546. 40.09 ft. below measuring point Measuring Point is 2.5 ft. above land surface Volume of water pumped/bailed before sampling: T2 Samples for metals were collected unfiltered: ❑ YES County Gaston Telep hone#. 704-865-1201 No. of wells to be sampled: 3 Date sample collected: 8-4-20 Well Diameter: 2 in Screened Interval: 40 ft. Relative M.P. Elevation: 754.91 to 50 ft. ft. gallons NO and field acidified: ED YES ❑ NO 1ARTMENT OF ENVIRONMENT & NATURAL RESOURCES 'ISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 91M07-6306 :RMIT Number: Expiration Date: Ame30.2025 n-Discharge W00004270 UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon Remediation. Infiltration Gallery Spray Field ® Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other FIELD ANALYSES: pH 00400. 4.79 units Spec Cond 00094 59.8 Odor 00085: None Appearance Clear WAS DRY Temp. 000lo 19.1 oC at time of uMhos sampling, rHer4 Date sample analyzed: 8-4-20, 8-5-20. 8-6-20, 8-7-20, 8-10-20 Laboratory Name: waypoint Analytical Carolinas, Inc. Waypoint Analytical Tennessee LLC. Certification No. 402, 0415 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 <50 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <2 CFU /100mL Nitrate (NO3) as N 0062o 2,7 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.20 mg/L (Note. Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units). Dissolved Solids:Total 703oo 62 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1.00 mg/L Ca - Calcium 00916 mg/L Chloride 0094o 6.7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS. HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <2.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) [13 No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L method # Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. NH, as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Leonard Moretz, Senior Project Manager - Hart & Hickman, PC Permittee (or Authorized Agent) Name and Title - Please print or type here: GW-59 Rev.8/2013 Case Narrative Waypoint ANALYTICAL Hart & Hickman (Charlotte) Leo Moretz 2923 South Tryon St. Ste 100 Charlotte, NC 28203 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: AB CarterABC.026 Project No.: ABC.026 Lab Submittal Date: 08/04/2020 Work Order: 0080033 8/12/20 9:52 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: TOC analysis was subcontracted to Waypoint Memphis. Laboratory report is attached. Please call if you have any questions relating to this analytical report. Respectfully, WAYPOINT ANALYTICAL a ---I Angela D. Overcash Senior Project Manager Data Qualifiers Key Reference: BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529.6364 - Fax: 704/525-0409 Page 1 of 20 Waypoint `- ANALYTICAL Client Sample ID Lab Sample ID Matrix MW-19 0080033-01 Water MW-20 0080033-02 Water MW-21 0080033-03 Water Samples were received in good condition at 5.5 degrees C unless otherwise noted. Sample Receipt Summary 08/12/2020 Work Order: 0080033 Date/Time Sampled 08/04/20 11:50 08/04/20 10:55 08/04/20 11:25 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704152"364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Date/Time Received 08/04/20 13:55 08/04/20 13:55 08/04/20 13:55 Page 2 of 20 Summary of Detections Waypoint 08/12/2020 Work ork Order: 0080033 Waypoint ID Client ID Parameter Method Result Units 0080033-01 MW-19 Chloride '9056A 19 mg/L 0080033-01 MW-19 Sulfate '9056A 110 mg/L 0080033-01 MW-19 Nitrate as N 'SM4500-NO3 F 7.4 mg/L 0080033-01 MW-19 Nitrate/Nitrite as N 'SM4500-NO3 F 7.4 mg-N/L 0080033-01 MW-19 Phosphorus -Total 'SM4500-P F 0.24 mg/L 0080033-01 MW-19 Total Dissolved Solids `SM2540 C 270 mg/L 0080033-02 MW-20 Chloride '9056A 36 mg/L 0080033-02 MW-20 Sulfate '9056A 160 mg/L 0080033-02 MW-20 Nitrate as N 'SM4500-NO3 F 3.3 mg/L 0080033-02 MW-20 Nitrate/Nitrite as N 'SM4500-NO3 F 3.3 mg -NIL 0080033-02 MW-20 Phosphorus -Total 'SM4500-P F 0.39 mg/L 0080033-02 MW-20 Total Dissolved Solids 'SM2540 C 330 mg/L 0080033-02 MW-20 TOC 'SM5310 C 1.30 mg/L 0080033-03 MW-21 Chloride '9056A 6.7 mg/L 0080033-03 MW-21 Nitrate as N 'SM4500-NO3 F 2.7 mg/L 0080033-03 MW-21 Nitrate/Nitrite as N 'SM4500-NO3 F 2.7 mg -NIL 0080033-03 MW-21 Phosphorus -Total 'SM4500-P F 0.20 mg/L 0080033-03 MW-21 Total Dissolved Solids 'SM2540 C 62 mg/L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 20 Waypoi nt ANALYTICAL Hart & Hickman (Charlotte) Attn: Leo Moretz 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: AB Carter ABC.026 Project No.: ABC.026 Sample Matrix: Water Laboratory Report 08/12/2020 Client Sample ID: MW-19 Sample ID: 0080033-01 Work Order: 0080033 Time Collected: 08/04/20 11:50 Time Submitted: 08/04/20 13:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anions by Ion Chromatography Chloride 19 mg/L 1.0 0.35 1 '9056A 8/6/20 21:23 BMS POH0081 Sulfate 110 mg/L 2.0 0.56 1 '9056A 8/6120 21:23 BMS POH0081 General Chemistry Parameters Nitrate as N 7.4 mg/L 0.50 0.32 5 'SM4500-NO3 F 817/20 12:49 BMS [CALC) Chemical Oxygen Demand BRL mg/L 50 11 1 •SM5220 D 8/6/20 13:27 BMS POH0042 Nitrate/Nitrite as N 7.4 mg-N/L 0.50 0.32 5 'SM4500-NO3 F 8/7/20 12:49 CLB POH0089 Nitrite as N BRL mg -NIL 0.010 0.0019 1 'SM4500-NO2 B 8/5/20 14:25 BMS POH0049 Phosphorus -Total 0.24 mg/L 0.10 0.048 1 'SM4500-P F 8/6120 8:58 CLB POH0048 Total Dissolved Solids 270 mg/L 50 31 1 'SM2540 C 8/6/20 16:52 SLS POH0095 Ammonia as N BRL mg-N/L 0.10 0.064 1 'SM4500-NH3 G 8/10/20 12:48 CLB POH0097 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 8/4/20 14:32 BMS POH0047 Subcontracted Analyses TOC BRL mg/L 1.00 0.498 1 "SM5310 C 8/10/20 19:28 SCD POH0113 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 4 of 20 F Waypoint ANALYTICAL Hart & Hickman (Charlotte) Attn: Leo Moretz 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: AB Carter ABC.026 Project No.: ABC.026 Sample Matrix: Water Laboratory Report 08/12/2020 Client Sample ID: MW-20 Sample ID: 0080033-02 Work Order: 0080033 Time Collected: 08/04/20 10:55 Time Submitted: 08/04/20 13:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anions by Ion Chromatography Chloride 36 mg/L 1.0 0.35 1 *9056A 8/6120 20:37 BMS PON0081 Sulfate 160 mg/L 2.0 0.56 1 *9056A 8l6/20 20:37 BMS POH0081 General Chemistry Parameters Nitrate as N 3.3 mg/L 0.10 0.065 1 *SM4500-NO3 F 817120 12:49 BMS [CALCI Chemical Oxygen Demand BRL mg/L 50 11 1 *SM5220 D 8/6/20 13:27 BMS POH0042 Nitrate/Nitrite as N 3.3 mg -NIL 0.10 0.065 1 *SM4500-NO3 F 8/7/20 12:49 CLB POH0089 Nitrite as N BRL mg-N/L 0.010 0.0019 1 *SM4500-NO2 B 8/5/20 14:25 BMS POH0049 Phosphorus -Total 0.39 mg/L 0.10 0.048 1 *SM4500-P F 816/20 8:58 CLB POH0048 Total Dissolved Solids 330 mg/L 50 31 1 *SM2540 C 816120 16:52 SLS POH0095 Ammonia as N BRL mg-N/L 0.10 0.064 1 *SM4500-NH3 G 8/10/20 12:48 CLB POH0097 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 *SM9222 D 8/4/20 14:32 BMS POH0047 Subcontracted Analyses TOC 1.30 mg/L 1.00 0.498 1 *SM5310 C 8/10120 20:06 SCD POH0113 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-0364 - Toll Free Number: 1-800/529-0364 - Fax: 7041525-0409 Page 5 of 20 iffl Laboratory Report • 08/12/2020 Waypoint ANALYTICAL Hart & Hickman (Charlotte) Project: AB Carter ABC.026 Client Sample ID: MW-21 Attn: Leo Moretz Sample ID: 0080033-03 2923 South Tryon St. Ste 100 Project No.: ABC.026 Work Order: 0080033 Charlotte, NC 28203 Sample Matrix: Water Time Collected: 08/04/20 11:25 Time Submitted: 08/04/20 13:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anions by Ion Chromatography Chloride 6.7 mg/L 1.0 0.35 1 `9056A 8/6120 21:38 BMS POH0081 Sulfate BRL mg/L 2.0 0.56 1 '9056A 8/6/20 21:38 BMS POH0081 General Chemistry Parameters Nitrate as N 2.7 mg/L 0.10 0.065 1 'SM4500-NO3 F 8/7/20 12:49 BMS ICALC] Chemical Oxygen Demand BRL mg/L 50 11 1 'SM5220 D 816/20 13:27 BMS POH0042 Nitrate/Nitrite as N 2.7 mg-N/L 0.10 0.065 1 'SM4500-NO3 F 8/7120 12:49 CLB POH0089 Nitrite as N BRL mg -NIL 0.010 0.0019 1 'SM4500-NO2 B 8/5/20 14:25 BMS POH0049 Phosphorus -Total 0.20 mg/L 0.10 0.048 1 `SM4500-P F 8/6/20 8:58 CLB POH0048 Total Dissolved Solids 62 mg/L 50 31 1 'SM2540 C 816/20 16:52 SLS POH0095 Ammonia as N BRL mg-N/L 0.10 0.064 1 'SM4500-NH3 G 8/10/20 12:48 CLB POH0097 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 8/4/20 14:32 BMS POH0047 Subcontracted Analyses TOC BRL mg/L 1.00 0.498 1 'SM5310 C 8/10/20 20:44 SCD POH0113 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 6 of 20 Waypoint r ANALYTICAL Hart & Hickman (Charlotte) Project: AB CarterABC.O26 Attn: Leo Moretz 2923 South Tryon St. Ste 100 Project No: ABC.O26 Charlotte, NC 28203 Anions by Ion Chromatography - Quality Control Level II QC Report 8/12/20 Work Order: 0080033 Time Submitted: 8/4/2020 1:55:O0PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POH0081 - NO PREP Blank (POH0081-BLK1) Prepared & Analyzed: 08/06/20 Chloride BRL 1.0 mg/L Sulfate BRL 2.0 mg/L LCS (POH0081-BS1) Prepared: 08/06/20 Analyzed: 08/07/20 Chloride 41.9 1.0 mg/L 40.00 105 80-120 Sulfate 44.0 2.1 mg/L 40.00 110 80-120 Matrix Spike (POH0081-MS1) Source: 0080033-02 Prepared &Analyzed: 08/06/20 Chloride 77.3 1.0 mg/L 40.00 36.0 103 80-120 Sulfate 197 2.1 mg/L 40.00 159 94 80-120 Matrix Spike Dup (POH0081-MSDi) Source: 0080033-02 Prepared & Analyzed: 08/06/20 Chloride 76.8 1.0 mg/L 40.00 36.0 102 80-120 0.7 15 Sulfate 197 2.1 mg/L 40.00 159 94 80-120 0.1 15 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 20 Waypoint(D ANALYTICAL Hart & Hickman (Charlotte) Project: AB CarterABC.026 Attn: Leo Moretz 2923 South Tryon St. Ste 100 Project No: ABC.026 Charlotte, NC 28203 General Chemistry Parameters - Quality Control Reporting Analyte Result Limit Units Batch POH0042 - NO PREP Level II QC Report 8/ 12/20 Work Order: 0080033 Time Submitted: 8/4/2020 1:55:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (POH0042-BLK1) Prepared &Analyzed: 08/06/20 Chemical Oxygen Demand BRL 50 mg/L LCS (POH0042-BSI) Prepared &Analyzed: 08/06/20 Chemical Oxygen Demand 495 50 mg/L 500.0 99 90-110 LCS (POH0042-BS2) Prepared & Analyzed: 08/06/20 Chemical Oxygen Demand 497 50 mg/L 500.0 99 90-110 LCS (POH0042-BS3) Prepared & Analyzed: 08/06/20 Chemical Oxygen Demand 496 50 mg/L 500.0 99 90-110 LCS (POH0042-BS4) Prepared & Analyzed: 08/06/20 Chemical Oxygen Demand 489 50 mg/L 500.0 98 90-110 Matrix Spike (POH0042-MS1) Source: 0080033-01 Prepared &Analyzed: 08/06/20 Chemical Oxygen Demand 490 50 mg/L 500.0 19.3 94 80-120 Matrix Spike Dup (POH0042-MSD1) Source: 0080033-01 Prepared & Analyzed: 08/06/20 Chemical Oxygen Demand 484 50 mg/L 500.0 19.3 93 80-120 1 20 Batch POH0048 - SM4500-PBS Blank (POH0048-BLK1) Prepared: 08/05/20 Analyzed: 08/06/20 Phosphorus -Total BRL 0.10 mg/L LCS (POH0048-BSI) Prepared: 08/05/20 Analyzed: 08/06/20 Phosphorus -Total 2.07 0.10 mg/L 2.000 104 90-110 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 8 of 20 Level II QC Report Waypoin8/12/20 t_ ANALYTICAL Hart & Hickman (Charlotte) Project: AB Carter ABC.026 Work Order: 0080033 Attn: Leo Moretz Time Submitted: 8/4/2020 1:55:OOPM 2923 South Tryon St. Ste 100 Project No: ABC.026 Charlotte, NC 28203 General Chemistry Parameters - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POH0049 - NO PREP Blank (POH0049-BLK1) Prepared & Analyzed: 08/05/20 Nitrite as N BRL 0.010 mg-N/L LCS (POH0049-BSI) Prepared & Analyzed: 08/05/20 Nitrite as N 0.105 0.010 mg-N/L 0.1000 105 90-110 Matrix Spike (POH0049-MS1) Source: 0080033-01 Prepared & Analyzed: 08/05/20 Nitrite as N 0.114 0.011 mg-N/L 0.1111 BRL 103 80-120 Matrix Spike Dup (POH0049-MSD1) Source: 0080033-01 Prepared & Analyzed: 08/05/20 Nitrite as N 0.116 0.011 mg-N/L 0.1111 BRL 104 80-120 1 20 Batch POH0089 - NO PREP Blank (POH0089-BLK1) Prepared &Analyzed: 08/07/20 Nitrate/Nitrite as N BRL 0.10 mg-N/L LCS (POH0089-BS1) Prepared &Analyzed: 08/07/20 Nitrate/Nitrite as N 0.966 0.10 mg-N/L 1.000 97 90-110 Matrix Spike (POH0089-MSI) Source: 0080033-01 Prepared & Analyzed: 08/07/20 Nitrate/Nitrite as N 8.38 0.50 mg-N/L 1.000 7.44 93 80-120 Matrix Spike Dup (POH0089-MSD1) Source: 0080033-01 Prepared & Analyzed: 08/07/20 Nitrate/Nitrite as N 8.37 0.50 mg-N/L 1.000 7.44 93 80-120 0.06 20 Batch POH0095 - NO PREP Blank (POH0095-BLK1) Prepared &Analyzed: 08/06/20 Total Dissolved Solids BRL 50 mg/L This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 9 of 20 Waypoint .. ANALYTICAL Hart & Hickman (Charlotte) Attn: Leo Moretz 2923 South Tryon St. Ste 100 Charlotte, NC 28203 General Chemistry Parameters - Quality Control Analyte Project: AB Carter ABC.026 Project No: ABC.026 Level II QC Report 8/12120 Work Order: 0080033 Time Submitted: 8/4/2020 1:55:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POH0095 - NO PREP LCS (POH0095-BS1) Prepared & Analyzed: 08/06/20 Total Dissolved Solids 968 50 mg/L 1000 97 90-110 Duplicate (POH0095-DUP1) Source: 0080033-02 Prepared &Analyzed: 08/06/20 Total Dissolved Solids 350 50 mg/L 328 6 10 Batch POH0097 - NO PREP Blank (POH0097-BLK1) Prepared & Analyzed: 08/10/20 Ammonia as N BRL 0.10 mg-N/L LCS (POH0097-BS1) Prepared &Analyzed: 08/10/20 Ammonia as N 2.46 0.10 mg-N/L 2.500 98 90-110 This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 20 Waypoint o ANALYTICAL Hart & Hickman (Charlotte) Attn: Leo Moretz 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Microbiological Parameters - Quality Control Analyte Project: AB Carter ABC.026 Project No: ABC.026 Level II QC Report 8/12/20 Work Order: 0080033 Time Submitted: 8/4/2020 1:55:00PM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Batch POH0047 - NO PREP Blank (POH0047-BLK1) Prepared & Analyzed: 08/04/20 Fecal Coliforms BRL 2 CFU/100 ml Sample Extraction Data Prep Method: SM4500-PB5 Lab Number Batch Initial Final OateMme 0080033-01 POH0048 50 mL 50 mL 08/05/20 13:19 0080033-02 POH0048 50 mL 50 mL 08/05/20 13:19 0080033-03 POH0048 50 mL 50 mL 08/05/20 13:19 Subcontracted Analyses The following analyses were subcontracted to Waypoint Analytical Lab Number Analysis 0080033-01 TOC (Sub) 0080033-02 TOC (Sub) 0080033-03 TOC (Sub) This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 -Toll Free Number: 1-800/529.6364 - Fax: 704/525-0409 Page 11 of 20 Waypoi nt . ANALYTICAL 449 Springbrook Road • Charlotte, NC 21217 Phone 7041529-6364 Fax: 70/4//525-0409 Client Company Name: cLr � 4- - Report To/Contact NameMcntC•-�aE�z RprtingAddress: 72-3 S -F, 4 loa /UL V 7.03 -- CHAIN OF CUSTODY RECORD PAGE OF QUOTE # TO ENSURE PROPER BILLING: - YES NO N/A � �� _ �� ` Samples INTACT upon arrival? Project Name: __ Received ON WET ICE? Short Hold Analysis (So (No) UST Project: (Yes) jf�_ PROPER PRESERVATIVES indicated? ! _ 'Please ATTACH any project specific reporting (QC LEVEL i If III IV) Received WITHIN HOLDING TIMES? provisions and/or QC Re uirements / CUSTODY SEALS INTACT? Invoice To: CGO�-t. q at Q t� c k �4 Hxo." VOLATILES recd W/OUT HEADSPACE? Address: PROPER CONTAINERS used? TEMP: Therm ID: _I I(L - r"I J Observed 57fC /Corr.l..-fl•Cl Phone: - Fa/x�(Yes)(No) Email Address: 1✓►1O rt{�c�'lo•i�11 FC�w�'!!L Purchase Order No./Billing Reference Cow,._ TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL EDD Type: PDFk Excel X Other Requested Due Date J 1 Day J 2 Days J 3 Days J 4 Days J 5 Days Rush Work Must Be Certification: NELAC____ _-_ FL ------ __ NC_ Working Days" J 6-9 Days J Standard 10 days J Pre Approved SC_.._ OTHER- NIA_______ Site Location Name: Samples received after 14:00 will be processed next business dayp Site Location Physical Address: Si c, &A/-- Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT) Sample Iced Upon Collection: YES NO — TIME MATRIX SAMPLE CONTAINER ANA IS REQUE§TED CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED MILITARY (SOIL, WATER, OR PRESERVA- TIVES mt/f'\S�� r p� REMARKS A l) J� li ID NO. 'TYPE NO. — SIZE HOURS SLUDGE) SEE BELOW It o-lcl g/Lf ZO P VOA I ' Ve,,,e, U ,: ,, x D 1 MW-ZO ( 0 5 5 X X S DOWN ;ect", FIRMLY 2 COPIES" Sampler's Signature ampled By (Print Name) _ ._ Affiliation Upon relinquishing, this Chain of Custody is your authorization for Waypoint Analytical to proceed with the analyses as requested above. Any changes must be . submitted in writing to the Waypoint Analytical Project Manager. There will be charges for any changes after analyses have been initialized. Relinquished By. (Sign ) Received By: (Signature) Date Military/Hours Additional Comments: Site Arrival Time: Relinquished By: (Signature) Received By (Signature] - / Date / Site Departure Time: --- -- Re"uished By: (Signature) Date Received For Waypoint Analytical By D Field Tech Fee - S Zv ) J $S Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRA SPOR ATION TO THE LA TORY. COC Group No, Mileage: SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABOR7ARY, Fed Ex U UPS J Hand4elivered J Waypoint Analy scat Field Service J Oiher______... __ _ __ - ._-_.—_-___ NPUES: UST. GROUNDWATER DRINKING WATER: SOLID WASTE: RCRA: BRWNFLD LANDFILL OTHER: UNCUSC JNC JSC IJNC JSC JNC -1 SC JNC JSC ANC JSC JNC JSC UNC JSC I JNC -1 SC UJ___ `I ---- -.._. J _ - _ _. _. -_.. -1 _ .- ___ --_- - J - - J -- .- - J — -- — J ----- 'CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) Page 12 of 20 Waypoint ANALYTICAL 8/11 /2020 Waypoint Analytical Charlotte Ms. Angela Overcash P.O. Box 240543 Charlotte, NC, 28224-0543 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Ref: Analytical Testing Lab Report Number: 20-219-0135 Client Project Description: Subcontract Order #0080033 Dear Ms. Angela Overcash: Waypoint Analytical, LLC. received sample(s) on 8/6/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, IJ4& A* 4jk Andrea R Brownfield Project manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. rLi Page 13 of 20 Page 1 of 8 Wayposintw ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2021 Arizona State Program AZ0816 08/30/2020 Arkansas State Program 88-0650 02/07/2021 California State Program 2904 05/10/2020 Florida State Program - NELAP E871157 06/30/2021 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2021 Illinois State Program - NELAP 200078 10/10/2020 Kentucky State Program 80215 06/30/2021 Kentucky State Program KY90047 12/31/2020 Louisiana State Program - NELAP LA037 12/31/2020 Louisiana State Program - NELAP 04015 06/30/2021 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2020 Oklahoma State Program 9311 08/31/2020 Pennsylvania State Program - NELAP 68-03195 05/31/2021 South Carolina State Program 84002 06/30/2021 South Carolina State Program 84002 06/30/2020 Tennessee State Program 02027 02/11/2023 Tennessee A21-A ISO 17025:2017 4313.01 10/31/2021 Texas State Program - NELAP T104704180 09/30/2020 Virginia State Program 00106 06/30/2021 Virginia State Program - NELAP 460181 09/14/2020 Page 1 of 1 00 Page 14 of 20 Page 2 of 8 (2) Waypoint, 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-219-0135 Client Project Description: Subcontract Order #0080033 Lab No Client Sample ID Matrix Date Collected Date Received 92714 MW-19 Aqueous 08/04/2020 11:50 08/06/2020 92715 MW-20 Aqueous 08/04/2020 10:55 08/06/2020 92716 MW-21 Aqueous 08/04/2020 11:25 08/06/2020 Page 15 of 20 Page 3 of 8 Waypoint,ANALYTICAL 25657 Waypoint Analytical Charlotte 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Ms. Angela Overcash Project Subcontract Order #0080033 P.O. Box 240543 Information Charlotte , NC 28224-0543 Report Number :20-219-0135 REPORT OFANAL YSIS Report Date : 08/11/2020 Received : 08/06/2020 Lab No : 92714 Matrix: Aqueous Sample ID: MW-19 Sampled: 8/4/2020 11:50 Analytical Method: 531OC-2011 Prep Batch(es): L505369 08/09/20 07:03 Prep Method: 531OC-2011 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch TOC 0.8051 mg/L 0.498 1.00 1 08/10/2019:28 DDB L505781 Lab No : 92715 Matrix: Aqueous Sample ID: MW-20 Sampled: 8/4/2020 10:55 Analytical Method: 531OC-2011 Prep Batch(es): L505369 08/09/20 07:03 Prep Method: 531OC-2011 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Batch TOC 1.30 mg/L 0.498 1.00 1 08/10/20 20:06 DDB L505781 Qualifiers/ DF Dilution Factor ) Estimated value Definitions MQL Method Quantitation Limit Page 16 of 20 Page 4 of 8 Waypoint2790 Whitten Road, Memphis, TN 38133 ,..'r Main 901.213.24001 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 25657 Waypoint Analytical Charlotte Ms. Angela Overcash Project Subcontract Order #0080033 P.O. Box 240543 Information Charlotte , NC 28224-0543 Report Number:20-219-0135 REPORT Of ANALYSIS Report Date : 08/11/2020 Received : 08/06/2020 Lab No : 92716 Matrix: Aqueous Sample ID: MW-21 Sampled: 8/4/2020 11:25 Analytical Method: 531OC-2011 Prep Method: 531OC-2011 Test Results TOC 0.8853 Prep Batch(es): L505369 08/09/20 07:03 Units MDL MQL DF Date / Time By Analytical Analyzed Batch mg/L 0.498 1.00 1 08/10/20 20:44 DDB L505781 Qualifiers/ DF Dilution Factor 3 Estimated value Definitions MQL Method Quantitation Limit Page 17 of 20 Page 5 of 8 a Waypoint . 279U Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Quality Control Data Client ID: Waypoint Analytical Charlotte Project Description: Subcontract Order #0080033 Report No: 20-219-0135 QC Prep: L505369 QC Analytical Batch(es): L505502 QC Prep Batch Method: 531OC-2011 Analysis Method: 531OC-2011 Analysis Description: Total Organic Carbon Lab Reagent Blank LRB-1-505369 Matrix: AQU Associated Lab Samples: 92714, 92715, 92716 Blank MDL MQL Analyzed Parameter Units Result TOC mg/L <0.498 0.498 1.00 08/09/20 20:13 Laboratory Control Sample LCS-1-505369 Spike LCS LCS %Rec °/a Rec Parameter Units Conc. Result Limits TOC mg/L 5.00 4.70 94.0 85-115 Matrix Spike & Matrix Spike Duplicate L 92881-MS-L505369 L 92881-MSD-L505369 MS Spike MSD MS Result MSD MS MSD %Rec Max Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD Conc. TOC mg/L 3040 5000 5000 6960 3520 78.0 10.0* 70-130 65.6* 20.0 * QC Fail Date: 08/11/2020 03:52 PM Page 18 of 20 Page 6 of 8 0 a Waypoint.. ANALYTICAL 2790 Whitten Road, Memphis, Thl 38133 Main 901.Z33.2400 ° Fax 901.213.2440 www.waypointanalytical.com Shipment Receipt Form Customer Number: 25657 Customer Name: Waypoint Analytical Charlotte Report Number: 20-219-0135 Shipping Method Fed Ex US Postal Lab Other : UPS Client Courier Thermometer ID: 100 Shipping container/cooler uncompromised? 0 Yes No Number of coolers/boxes received F 1 Custody seals intact on shipping container/cooler? Yes No Not Present Custody seals intact on sample bottles? Yes No Not Present Chain of Custody (COC) present? Yes No COC agrees with sample label(s)? Yes No COC properly completed Yes No Samples in proper containers? Yes No Sample containers intact? Yes No Sufficient sample volume for indicated test(s)? Yes No All samples received within holding time? Yes No Cooler temperature in compliance? Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Water - Sample containers properly preserved Yes No N/A Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Yes No N/A Soil VOA method 5035 — compliance criteria met Yes No N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Yes 0 No Comments Signature: Tory Phillips Date & Time: 08/06/2020 14:33:00 Page 19 of 20 Page 7 of 8 ���NN��1� NIN�i�I �II�II�I z 2020 Wavtxxnt Analvhcal Charlotte 1431 10 Waypoint Sumomtacl Omer a'G000033 ANALYi-ICAL SUBCONTRACT ORDER OLEQ Z y Z Certification: NEL.AC Waypoint Analytical NC x SCOther 0080033 si-ADING LABORATORY: RECEIVING LABORATORY: Waypoint Analytical Waypoint Analytical P. O. Box 240543 2790 Whitten Road Charlotte, NC 28224-0543 Memphis, TN 38133 Phone:800-529-6364 Phone :(901) 213-2400 Fax:704-525-0409 Fax: (901) 213-2440 Project Manager: Angela D. Overcash Need 3day TAT Analysis Due Expires Laboratory ID Comments Sample ID:0080033-01 Waler Sampled:08AN/2011:50 NIW-19 TOC (Sub) 09/01/20 11:50 Containers Xpplit� R j 4 r -T L ew( Sample ID: 0080033-02 1 Water Sampled:08/04/2010:55 MTV-20 TOC (Sub) Containers Supplied: Sample ID: 00801133-03 TOC (Sub) Containers SuNdied: 09/01 /20 10:55 N\aler Sampled:08/04/2011:25 NIW-21 09101 /20 11:25 5. 5 . Zo We X 2 4 oC tcctrnxu Gl� Q y vale nccctrcu o� aa�c Released By Date R °ivcd By Date Released By Date ce ed B� )ale &C=) : C)c Released 13% Date Rec 1**'wIT.N Date Paaelofl Iage 20 of 20 Page 8 of 8