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HomeMy WebLinkAboutNCG030535_DMR_20200427Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Resources General Permit No. NCG030000 Date submitted �/ -2 % a0,;20 CERTIFICATE OF COVERAGE NO. NCG03L 3 S FACILITY NAME ZF C 4 SS ��rno c.� c.z tS L t— C COUNTY _ CA TA w A,4 T — PERSON COLLECTING SAMPLES c., LABORATORY P CE Lab Cert. h dal ;2 7 yo Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD QC Jan -June July -Dec or ❑ Monthly'_ (month) DISCHARGING TO CLASS []ORW 0HQW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply FISA RECEI\/FD ®Other C, MAY 6V 2020REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL FILE .. • vLV 1 1. ,vv ulJU1u1 yC L111.� PtCr100! Outfall No. Date Sample i Collected 24-hour rainfall amount, Total Suspended Solids P H Copper Lead Zinc Non -Polar O&G/ Total Petroleum Total Toxic (mo/dd/yr) Inches Standard units Hydrocarbons Organicss Benchmarks =__> _ - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L - 16.1 D /Vl b 6, / Nb N .0) , .039rn �.,.," Y o 1'Hill 15 ,n'xcau ,., milli-amivaiI riiUSL uegilI wiui me secona consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3 The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." bl//I Name (Print name) Title (Print title) (Signature) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format "<XX me/L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Mote: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. Aln rlicrhnrnp fhic norin4.)2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =__> _ - 15 mg/L 106 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES Q NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one in the case of "No Discha this DMR, including all "No Discharge" reports, within 30 days o Division of Water Resources Attn: DWR Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 to: of the lab results at end of monitoring period YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 _ aceAnalytica(' www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 April 06, 2020 William Edens ZF Chassis Components LLC 1570 E. P St. Ext. Newton, NC 28658 RE: Project: STORMWATER SAMPLING Pace Project No.: 92471265 Dear William Edens: Enclosed are the analytical results for sample(s) received by the laboratory on March 26, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 /�e Analytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: STORMWATER SAMPLING Pace Project No.: 92471265 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 /71aceAnalyfical" www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: STORMWATER SAMPLING Pace Project No.: 92471265 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92471265001 3-2020 #1 A,B,C,D EPA 1664B WAM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 JNS 1 PASI-A EPA 9040C ECH 1 PASI-A 92471265002 3-2020 #2 A,B,C,D EPA 1664B WAM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 2540D-2011 JNS 1 PASI-A EPA 9040C ECH 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 ,��IaceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: STORMWATER SAMPLING Pace Project No.: 92471265 Sample: 3-2020 #1 A,B,C,D Lab ID: 92471265001 Collected: 03/25/20 10:30 Received: 03/26/20 10:47 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 03/31/20 09:50 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services - Asheville Copper ND mg/L 0.0050 1 04/02/20 01:31 04/02/20 22:49 7440-50-8 Lead ND mg/L 0.0050 1 04/02/20 01:31 04/02/20 22:49 7439-92-1 Zinc 0.028 mg/L 0.010 1 04/02/20 01:31 04/02/20 22:49 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 10 mg/L 4.4 1 04/01/20 11:27 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 6.1 Std. Units 0.10 1 04/05/20 14:17 H3 Date: 04/06/2020 03:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 14 1"'�e Analytical www.pactiabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: STORMWATER SAMPLING Pace Project No.: 92471265 Sample: 3-2020 #2 A,B,C,D Lab ID: 92471265002 Collected: 03/25/20 11:00 Received: 03/26/20 10:47 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Oil and Grease ND mg/L 5.0 1 03/31/20 09:50 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services -Asheville Copper ND mg/L 0.0050 1 04/02/20 01:31 04/02/20 22:52 7440-50-8 Lead ND mg/L 0.0050 1 04/02/20 01:31 04/02/20 22:52 7439-92-1 Zinc 0.039 mg/L 0.010 1 04/02/20 01:31 04/02/20 22:52 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services - Asheville Total Suspended Solids 4.4 mg/L 2.5 1 04/01/20 11:28 9040 pH Analytical Method: EPA 9040C Pace Analytical Services - Asheville pH at 25 Degrees C 6.4 Std. Units 0.10 1 04/05/20 14:22 H3 Date: 04/06/2020 03:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical www.patelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92471265 QC Batch: 533428 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92471265001, 92471265002 METHOD BLANK: 2847559 Matrix: Water Associated Lab Samples: 92471265001, 92471265002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 03/31/20 09:50 LABORATORY CONTROL SAMPLE: 2847560 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 35.4 88 78-114 MATRIX SPIKE SAMPLE: 2847561 2630482002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 35.2 87 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/06/2020 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 _�laceAnalXical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92471265 QC Batch: 533890 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92471265001, 92471265002 METHOD BLANK: 2849637 Associated Lab Samples: 92471265001, 92471265002 Parameter Units Copper mg/L Lead mg/L Zinc mg/L Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 04/02/20 22:25 ND 0.0050 04/02/20 22:25 ND 0.010 04/02/20 22:25 Qualifiers LABORATORY CONTROL SAMPLE: 2849638 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper mg/L 0.5 0.49 98 85-115 Lead mg/L 0.5 0.48 96 85-115 Zinc mg/L 0.5 0.47 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2849639 2849640 MS MSD 92471518001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND 0.5 0.5 0.51 0.50 103 100 70-130 2 Lead mg/L ND 0.5 0.5 0.50 0.49 100 98 70-130 2 Zinc mg/L 46.3 0.5 0.5 0.54 0.53 99 97 70-130 2 ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2849641 2849642 MS MSD 92471863003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Quaf Copper mg/L ND 0.5 0.5 0.59 0.57 117 114 70-130 3 Lead mg/L ND 0.5 0.5 0.52 0.50 103 100 70-130 3 Zinc mg/L ND 0.5 0.5 0.51 0.49 101 98 70-130 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/06/2020 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 n 71ac1�eAnalXical' r www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92471265 QC Batch: 533719 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92471265001, 92471265002 METHOD BLANK: 2848751 Matrix: Water Associated Lab Samples: 92471265001, 92471265002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/01/20 11:13 LABORATORY CONTROL SAMPLE: 2848752 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 246 98 90-110 SAMPLE DUPLICATE: 2848813 92471037001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 2460 2380 3 SAMPLE DUPLICATE: 2848814 92470717002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 1000 1400 33 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/06/2020 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 /71aceAnalXical" www.pacelabs.com i QUALITY CONTROL DATA Project: STORMWATER SAMPLING Pace Project No.: 92471265 QC Batch: 534419 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92471265001, 92471265002 SAMPLE DUPLICATE: 2852076 92471370001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.9 7.6 4 D6,H3 SAMPLE DUPLICATE: 2852077 92471437001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.1 7.2 1 H3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/06/2020 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 71aceAnalytical www.poesiabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: STORMWATER SAMPLING Pace Project No.: 92471265 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/06/2020 03:54 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 s 1�7aceAnalXical `� www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: STORMWATER SAMPLING Pace Project No.: 92471265 Lab ID Sample ID QC Batch Method QC Batch 92471265001 3-2020 #1 A,B,C,D EPA 1664B 533428 92471265002 3-2020 #2 A,B,C,D EPA 1664B 533428 92471265001 3-2020 #1 A,B,C,D EPA 200.7 Rev 4.4 1994 533890 92471265002 3-2020 #2 A,B,C,D EPA 200.7 Rev 4.4 1994 533890 92471265001 3-2020 #1 A,B,C,D SM 2540D-2011 533719 92471265002 3-2020 #2 A,B,C,D SM 2540D-2011 533719 92471265001 3-2020 #1 A,B,C,D EPA 9040C 534419 92471265002 3-2020 #2 A,B,C,D EPA 9040C 534419 Date: 04/06/2020 03:54 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch EPA 200.7 Rev 4.4 1994 533919 EPA 200.7 Rev 4.4 1994 533919 Page 11 of 14 J Document Name: Document Revised: February 7, 2018 b ace Analytical Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑' Ralelgh❑ Mechanicsville❑ • , ; Client Name: n Receipt Project # WO# : 9247126 5 i I,; , Courier: ❑Fed Ex ❑UPS ❑LISPS ❑Client ❑ Commercial 015ace ❑Other: 92471265 Custody Seal Present? ❑Yes ❑No Seals Intact? ❑Yes []No � P oats/Initials Parson Examining Contents: Packing Material: []Bubble Wrap ❑Bubble Bags ❑None ❑ Other Thermometer: Type of Ice: OG/et ❑slue ❑IR Gun ID: 92TO60 Cooler Tempj f ('C): `7 �> Correction Factor: Add/Subtract ('C) 0.0 Cooler Temp Corrected ('C)i USDA Regulated Soll ([Q�N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? nve• nu., Biological Tissue Frozen? [_—]Yes[]NO[]N/A❑None Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, cooling process hasbegun Did samples originate from a foreign source (internationally, inrllldine Hawaii and Puerto Rlcnl? 1—IYes nNo Comments/Discrepancy: 'chain of Custody Present? ` Yes ONO ❑N/A 1. Samples Arrived within Hold T"imel es ONO N/A 2. ;Short Hold Time Analysis <72hr.? ❑Yes o N/A 3. Rush Turn Around Time Requested? Yes ffNo N/A 4. Sufficient volume? es ONo N/A S. Correct Containers Used? -Pace Containers Used? [Yes [Yes ❑No ❑No ❑N/A ❑N/A 6. Containers Intact? Byes ONo N A 7. Dissolved analysis: Samples Field Filtered? Yes No 06/A 8. Sample Labels Match COC? QYes ❑No []N/A 9. -Includes Date/Time/ID/Analysis Matrix: Heads ace in VOA Vials (>S-6mm)? ❑Yes ❑No /A 10, Trip Blank Present? Trip Blank Custody Seals Present) ❑Yes OYes ❑No No (3k/A ' N/A 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers: Date/Time: Date: Date: Field Data Required? ❑Yes ❑No Page 12 of 14 . 1 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 �aceAnal�,trcal _ _ ------ -- y� Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check marls top half of be)( if pH and/or dechlorination is Project # © �� /1 S 26 verified and within the acceptance range for preservation samples. ppl: TIH Due Date: 04/09/20 Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 92-Memf ord `*Bottom half of box is to list number of bottle Z m aa, Z a, IU Z 2: a V di U V = v a p Z iv U ^ v `�. V Q Q, Z ry vv Z V n x a S Z ¢ Z 4 Y a n Z Z a, a, Z y n C a y n u or 0) G C .a. O !V S O Z = _ Q Z N u _n = p A Z L v a C U U c O O N qq O = E a Z -.. O ry 2 6 j 0 p d = o V1 l7 a ) .... m A C a _� Q. v N i Z rj a c Z) > c O a C u a E N m c E m a E O m (L v _ a E ✓l Nt%i n E n E LA a J E E ° v E a` E a` E o a E a v E a E o ,�.� m a O E a O E a O E a O E a a`, a N v N J E N m �n E r! m a of !n E a of O c ,n E O E J E Q E O m M m O N m � N m V m 2 M m N of m 67 O m u=. 3 O N a 2 - a O M a V, n a VI M a d M a 2 M c H M > 0 > Q1 o Q 4 o .y. � > 0 S Q ,n m > o a > cy > 7 o+ o t j i 2 - X I. 3 t. i a 4 5 6 \l 7 S 9 10 it pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot d Note: Whenever there is a discrepancy attesting Nor -in Laronna compnance samples, a copy o, m,5 w-- vrm tie 6enl to u!c k,.c. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 13 of 14 ll ' Paceafalyticaj" CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. At relevant fields must be completed accurately. ion A Section B Section C uired Client Information: Required Project Information: Invoice Information: P8 e ; 1 Of pant ZF Chassis - Newton Report To: WIIIIam Edens Attention ..r i ess 1570 East P Street Ext Copy To: Company Name: ,',j� ton, NC 28658 Address: IS' L — Rc ula ory Agency Il. apsharedservices@zf.com Purchase Order # Pace Quote: 1e (828)468-3340 Fax Project Name: Stormwater Sampling rnP 9tyriek.hooks Pace Project Manager pacelabs.eom. State Location jested Due Date: Project Pace P,Cfoe 4 3736-1 NC Re uested Analysis Filtered YJN) a 2 MATRIX CODE COLLECTED Preservatives > Drmkmg Wale, DW W.- WT o U Waste Wale, wW P.ed-t P y > emr J N SAMPLE ID o..Ir—, o� L? START END O > m One Character per box- W­ WP An w a w z y Q. AR IA Z 0.91, -) an„ oT O CLv Iu m m o = Sample Ids must be unique T,; ;,,,, T;; 0v a V OIs ss TIME DATE TIME Q d, Ni z z o — ODATE n ^ !% Alli 3 10: Z a D I x - W- 3 0 1 2 ADDITIONAL COMMENTS RELINQUISHED BY f AFFILIATION DATE TIME ACCEPTED 1 AFFILIATION DATE TIME SAMPLE CONDITIONS ry � )j��" Yet/' V� c/� 2 J ✓ C _- - % %' � 3 J 2({- ) ) ,,3V i SAMPLER NAME AND SIGNATURE G PRINT Name of SAMPLER: }} o SIGNATURE of SAMPLER: 00> DitTE Signed; �> G w IT m a-