NCG080431_2019 DMR_20201014 (4)

�VMICROBACR
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9H0284
Carolina Tank Lines, Inc. Project Name: Stormwater sample - Semiannual
Mr. Ron Goras Project / PO Number: N/A
Post Office Box 2827 Received: 08/20/2019
Burlington, NC 27216-2827 Reported: 08/29/2019
Case Narrative
Qualitative Field Monitoring (by client)
Color: Clear
Odor: None
Clarity: Clear
Floating Solids:None
Suspended Solids: None
Foam: None
Oil Sheen: None
Erosion at outfall:
Other: None
Rainfall:
Sample Summary Report
Sample Name Laboratory ID Client Matrix Sample Type Sample Begin
Stormwater, grab K9H0284-01 Aqueous Grab
Sample Taken Lab Received
08/19/19 09:00 08/20/19 08:38
Page 2of7

MICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9H0284
Project Description
Stormwater sample - Semiannual
For:
Mr. Ron Goras
Carolina Tank Lines, Inc.
Post Office Box 2827
—� Burlington, NC 27216-2827
Client Relationship Specialist, Environmental
Jeanne Overstreet
Thursday, August 29, 2019
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require
further assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil
samples are reported on a 'dry -weight' basis unless specified otherwise. Analytical results for water and wastes are reported on
a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This
laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported
results are related only to the samples analyzed as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 1 of 7

�VMICROBAC`p
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9H0284
ialvtical Testing Parameters
Client Sample ID: Stormwater, grab
Sample Matrix: Aqueous Collected By: Goras
Lab Sample ID: K9H0284-01 Collection Date: 08/19/2019 9:00
Wet Chemistry
EPA 1664 Rev. B
Oil & Grease (SGT-HEM)
SM 2540 D-2011
Total Suspended Solids
SM 2540 F-2011
Settleable Solids
SM 4500 H+B-2011
pH at 25 °C
Result
RL
Units
Dilution Note
<5.00
5.00
mg/L
1
51.2
6.25
mg/L
1
0.80
0.10
mUL
1
6.5
1.0
pH Units
1 H
Prepared Analyzed Analyst
08/27/19 1133 TBM
08/22/19 1047 CLB
08/20/19 0931 CLB
08/20/19 1450 CLB
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 7

�MICROBAC:`
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9H0284
Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville
Spike Source
%REC RPD
Wet Chemistry Result
RL
Units Level Result %REC
Limits RPD Limit Notes
Batch KH90192 - Wet Chem Aqueous - SM 2540 D-2011
Blank (KH90192-BLK1)
Prepared &Analyzed: 08/22/2019
Total Suspended Solids <2.50
2.50
mg/L
Blank (KH90192-BLK2)
Prepared &Analyzed: 08/22/2019
-
Total Suspended Solids <2.50
2.50
mg/L
Blank (KH90192-BLK3)
Prepared & Analyzed: 08/22/2019
Total Suspended Solids <2.50
2.50
mg/L
LCS (KH90192-BSI)
Prepared &Analyzed08/22/2019
-
Total Suspended Solids 29.2
2.50
mg/L
94.5-105.4
Batch KH90264 - Wet Chem Aqueous - EPA 1664 Rev. B
Blank (KH90264-BLK1)
Prepared & Analyzed: 08/27/2019
Oil & Grease (SGT-HEM) <5.00
5.00
mg/L
LCS (KH90264-BSI)
Prepared &Analyzed: 08/27/2019
Oil & Grease (SGT-HEM) 20.2
5.00
mg/L 20.4 99
64-114
,atrix Spike (KH90264-MS1) Source: K91-10284-01
Prepared &Analyzed: 08/27/2019
Oil & Grease (SGT-HEM) 19.8
5.00
mg/L 21.9 1.86 82
78-114
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 7

�MICROBACp
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9H0284
Definitions
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
RL: Reporting Limit
Cooler Receipt Log
Cooler ID: Default Cooler
Cooler Inspection Checklist
Ice Present or not required?
Custody seals intact or not required?
COC includes customer information?
Sample collector identified on COC?
Correct type of Containers Received
Containers Intact?
Enough sample volume for indicated tests received?
Samples arrived within hold time?
Chemical preservations checked or not required?
VOA vials have zero headspace, or not recd.?
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
Report Comments
Temp: 25.2°C
No
Shipping containers sealed or not required?
Yes
Yes
Chain of Custody (COC) Present?
Yes
Yes
Relinquished and received signature on COC?
Yes
Yes
Sample type identified on COC?
Yes
Yes
Correct number of containers listed on COC?
Yes
Yes
COC includes requested analyses?
Yes
Yes
Sample labels match COC (Name, Date & Time?)
Yes
Yes
Correct preservatives on COC or not required?
Yes
Yes
Preservation checks meet method requirements?
Yes
Yes
North Carolina DENR NPDES
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to/��L/tom �/L+�iLd2 e
applicable accreditation standard unless otherwise noted. �j/(
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated Jeanne Overstreet
in the footnote are present and an authorized signature is included. Client Relationship Specialist, Environmental
Reported: 08/29/2019 09:04
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 7

<!�)MJCROBAC- Fayetteville Division 2592 Hope Mills Road - F,
aeville, NC 28306 [phone] / 884-8774 fax
CHAIN OF CUSTODY RECORD
,K9HO284*
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C�IENT NAME& ADDRESS,
Carolina Tank Lines
3255 Maple Ave.
Burlington, NC
PO4
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CONTACTPERSON:
Mr. Ron Goras
PKONE:
336 -2 26-7039 ext 219
DATEIMETHOI)OF SHIPMENT:
LAB ID
SAMPLE
TYPE
"n
TIME 0
cosip
GRAB
PH
11.-
TEIII
CHLORINE
SULFIDE
Stormwater
41-7
X
2
C
I
A
LED injuais—*
Turnaround time: REGULAR
. 1•
'.X -I
TI
F,
2
Rdlp*fsh� by.
R—N,d by: (SIgnWura)
TI..
3
4
Rellnqulshad by.
Dal.
T1—
R—Ivad by: (319nal—)
LW�
TI.,
PH t-leld :
Temp Field:
Field Chlorine; Orc
by-O vw
RUSH
Dala Comments or SDecial Hazards:
on ia'
IS DATA FOR REG. COMPLIANCE PURPOSE?
NO YES WHICH: C� _ rec' r (':U
51;,D /) � . 'Wirg
Page

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"K9HO284-
STORM WATER - QUALITATIVE MONITORING - CAROLINA TANK ,111111h
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STORM
SITE #
DATE
SAMPLED
COLOR
ODOR
CLARITY
FLOATING
SOLIDS
SUSPENDED
SOLIDS
FOAM
OIL SHEEN
EROSION OR
DEPOSITION AT
THE OUTFALL
OTHER OBVIOUS
INDICATORS OF
STORMWATER
POLLUTION
2
3
TOTAL RAINFALL (inches):
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