WQ0036881_Monitoring (Report)_20180228

JV01MMHOR GF?L1MJW�4JV
Date: 28 February 2018
To: John Johnston
U. S. Environmental Protection Agency
Atlanta Federal Center
61 Forsyth Street, SW
Atlanta, GA 30303-8960
cc: Rob McDaniel
North Carolina Department of
Environment and Natural Resources
Hazardous Waste Section, Suite 150
401 Oberlin Road
Raleigh, NC 27605-1358
Groundwater Protection Branch
Water Quality Regional Operations Section
1636 Mail Service Center
Raleigh, NC 27699-1636
From: Michael D. Shannon
Northrop Grumman Corporation
on behalf of Northrop Grumman
Guidance and Electronics Company, Inc.
101 Continental Boulevard
MS: D12/XE6D21
El Segundo, CA 90245
Subject/Title:
TRANSMITTAL
Kurt Batsel
The Dextra Group, Inc.
1205 Johnson Ferry Road, Suite # 136-446
Marietta, GA 30068
Water Quality Regional Operations Section
Asheville Regional Office
2090 U.S. Highway 70
Swannanoa, NC 28778
Phone: [phone]
Email: [e-mail]
Corrective Action Monitoring Report — October 2017 Semiannual Event
Former Clifton Precision Site, Murphy, NC
EPA ID No. NCD 044 438 406
We are sending you the above referenced document(s):
For your review and comment
XX For your information and file
For your approval
For your signature
Total number of copies sent:
Remarks:
Please find attached the October 2017 Semiannual Event Corrective Action Monitoring Report for the former
Clifton Precision Site.
If you have any questions or comments, please do not hesitate to call me at the number shown above or Kurt
Batsel at [phone].

MONTMAVOP GAWIMMAAF
Former Clifton Precision Site
Murphy, North Carolina
Corrective Action Monitoring Report
October 2017 Semiannual Event
February 2018

Contents
Section1 Introduction ......................................................................................................................... 1
Section 2 Monitoring Summary ...................................................................................................... 1
Section3 Results ..................................................................................................................................... 1
Section 4 Summary of Results ......................................................................................................... 2
4.1 Groundwater ......................................................................................................................................... 2
4.2 Surface Water ........................................................................................................................................ 2
4.3 Private Wells and Spring .................................................................................................................. 3
Section 5 Potentiometric Surface Mapping and Trend Analysis ................................... 3
5.1 Regolith/Transition Zone ................................................................................................................. 3
5.2 Bedrock Zone ......................................................................................................................................... 3
Section 6 Groundwater Recovery .................................................................................................. 3
Section7 References .................................................................................................................. 4
Figures
Figure 1
Site Location Map
Figure 2a
Corrective Action Monitoring Locations
Figure 2b
Onsite Well Locations
Figure 3
Regolith/Transition Zone Potentiometric Surface Map
Figure 4
Bedrock Zone Potentiometric Surface Map
Figure 5
Groundwater Recovery Volumes
Tables
Table 1
Corrective Action Monitoring Schedule
Table 2
Summary of Hydrogeologic Zones
Table 3
Well Construction and Water Level Data
Table 4
Regolith/Transition Zone Groundwater Data Summary
Table 5
Bedrock Zone Groundwater Data Summary
Table 6
Surface Water Data Summary
Table 7
Private Well and Spring Data Summary
Table 8
Quality Assurance/ Quality Control Data Summary
Table 9
12 Month Groundwater Recovery Data Summary
Appendices
Appendix A Laboratory Reports (Electronic Only)
Appendix B Field Notes

Corrective Action Monitoring Report
October 2017 Semiannual Event
1 Introduction
This Corrective Action Monitoring Report presents the results of groundwater and
surface water monitoring performed during the October 2017 semiannual event at the
Former Clifton Precision Site (site) located near Murphy, North Carolina (Figure 1). This
event was conducted during the period of 23 October 2017 through 30 October 2017.
The event followed the monitoring plan prescribed in the latest revision of the Corrective
Action Monitoring Plan (CDM Smith, April 2009; modified June 9,2014). Details
regarding the site history and background are available in the Resource Conservation
and Recovery Act (RCRA) Facility Investigation Report (CDM Smith, August 2013).
While mobilized for the October 2017 sampling event, field crews completed additional
sampling in support of the upcoming bioremediation interim measure. However, this
report presents only the results associated with the routine Corrective Action Monitoring
Program (CAMP). The results from the additional sampling for the bioremediation
interim measure will be summarized and submitted separately.
2 Monitoring Summary
During this monitoring event, 23 monitoring wells, 4 groundwater recovery wells, 3
surface water stations, 3 creek monitoring points, 1 spring location, and 1 private well
location were sampled. Water levels were measured in each of the sampled monitoring
wells, the 4 recovery wells, and an additional 23 monitoring wells. The monitoring
locations are shown on Figures 2a and 2b, and the monitoring schedule is presented as
Table 1. A summary of the hydrogeologic zones referenced in Table 1 is presented as
Table 2.
The work performed in implementing the monitoring program is consistent with the
Field Branches Quality System and Technical Procedures, EPA Region 4, Science and
Ecosystem Support Division (SESD), Athens, Georgia. The data collection adhered to the
latest revision of the following SESD Operating Procedures (SESDPROC): SESDPROC- 010
(Logbooks), SESDPROC-005 (Sample and Evidence Management), SESDPROC-100 (Field
pH Measurement), SESDPROC-101 (Field Specific Conductance Measurement),
SESDPROC-102 (Field Temperature Measurement), SESDPROC-105 (Groundwater Level
and Well Depth Measurement), SESDPROC-201 (Surface Water Sampling), SESDPROC-
203 (Pump Operation), SESDPROC-205 (Field Equipment Cleaning and
Decontamination), and SESDPROC-301 (Groundwater Sampling).
Collected samples were analyzed for volatile organic compounds (VOCs) by TestAmerica
Laboratories in Savannah, Georgia and Nashville, Tennessee, according to SW-846
Method 8260B. The VOC list reported for this monitoring event is a site -specific list
containing 49 VOCs. In addition to the groundwater and surface water samples, duplicate
samples were collected at a frequency of 10% and submitted to the laboratory as blind
duplicates.
Field work for this event was performed by Environmental Monitoring Services, LLC, and
reporting was done by CDM Smith Inc.

Corrective Action Monitoring Report
October 2017 Semiannual Event
3 Results
The results for the October 2017 semiannual monitoring event are presented in Tables 3
through 8 as outlined below:
• Table 3 presents a summary of water level measurements and calculated
groundwater elevations.
• Table 4 presents a summary of detected compounds for regolith/transition zone
groundwater wells.
• Table 5 presents a summary of detected compounds for bedrock zone
groundwater wells.
• Table 6 presents a summary of detected compounds for surface water stations.
• Table 7 presents a summary of detected compounds for the private well and
spring location sampled during this event.
• Table 8 presents a summary of detected compounds for quality
assurance/quality control samples, including the blind field duplicates.
Complete laboratory reports for the October 2017 semiannual monitoring event are
included in a CD format as Appendix A. In addition to groundwater monitoring well
sampling, operational data were collected for the three groundwater recovery wells (RW-
3, RW-4, and RW-5) in service. Groundwater recovery data collected from November
2016 to October 2017 for these wells are summarized in Table 9.
4 Summary of Results
4.1 Groundwater
Concentrations detected in onsite and offsite monitoring wells this event are consistent
with recent and historical events. In general, monitoring wells show either a stable or
declining VOC trend. Several wells show improving conditions as a result of groundwater
reinjection, which was started in April 2015. For example, the following decreasing
concentrations of trichloroethene (TCE) have been observed:
• MW-13
1,300 micrograms per liter (�tg/L) in April 2013 and now 120 ug/L
• MW-28
1,700 Vg/L in April 2013 and now 22 [tg/L
• MW-35
Steady around 40 [tg/L from April 2013 to April 2014, now 15 Vg/L
• MW-60
Between 25 and 41 �tg/L from April 2013 to April 2015, now 7.3 �tg/L
0 MW-61
Between 33 and 45 Vg/L from April 2013 to April 2015, now 15 [tg/L.
4.2 Surface Water
TCE was detected at concentrations above the practical quantification limit (PQL) but
below the MCL of 5 �Lg/L at CMP-3 (4.3 �tg/L), CMP-4 (2.3 �tg/L), and SW-3 (1.9 �Lg/L).
The results at CMP-3 are lower than the previous 7.2 Vg/L detected during the sampling
event in April 2017. These values are also significantly below the applicable North

Corrective Action Monitoring Report
October 2017 Semiannual Event
Carolina surface water quality standard of 30 �tg/L, based on human health criteria and
Class C surface water use.
1, 1, 1 -Trichlo ro ethane (1.1 [tg/L) was also detected at a concentration above the PQL but
below the MCL of 200 �Lg/l, at CMP-3. No other compounds were detected at the surface
water locations.
4.3 Private Wells and Spring
In August 2012, EPA approved revisions to the Corrective Action Monitoring Plan that
adjusted the private well and spring sampling plan. One private well (PW-16) and one
spring location (SP-26) were sampled during this event. TCE and Freon 113 were
detected above PQL but below the MCL at SP-26 (1.9 ug/L and 1.5 respectively) during
this event. No compounds were detected in the sample collected at PW-16.
5 Potentiornetric Surface Mapping
5.1 Regolith / Transition Zone
A potentiometric surface map representing the regolith/transition zone is presented as
Figure 3.
The groundwater flow patterns in the regolith zone for this event are generally
consistent with the flow patterns observed during the RCRA Facility Investigation (RFI).
The direction of groundwater flow is to the north and northwest across the site and
toward Slow Creek and the alluvial valley. Groundwater flow in the alluvial valley is to
the west. The effect of the recovery wells on groundwater flow is evident by the
drawdown cone observed in the northwest portion of the site and extending off site to
the north.
5.2 Bedrock Zone
A potentiometric surface map representing the conditions in the bedrock zone is
presented as Figure 4.
The direction of groundwater flow is to the north and northwest across the site and
toward Slow Creek and the alluvial valley. Groundwater flow in the alluvial valley is to
the west. The groundwater flow patterns in the bedrock zone for this event show a
pronounced influence across the north portion of the site and extending off site due to
the ongoing operation of the onsite recovery wells.
6 Groundwater Recovery
Figure 5 presents the monthly groundwater recovery volumes for the currently used
groundwater recovery wells for the last eight years.
The TCE concentration in recovered groundwater from RW-3 has remained low and
relatively stable since the historical high concentration (8,700 �tg/L) was detected in
October 2008. The TCE concentration detected during this monitoring event was
3

Corrective Action Monitoring Report
October 2017 Semiannual Event
270 Vg/L. The average flow rate for RW-3 was 1.00 gallons per minute (gpm) over the
period of October 2016 through October 2017.
The TCE concentration in recovered groundwater from RW-4 for this monitoring event
was 397 Vg/L. This concentration is within the historical range for this well.
The average flow rate for RW-4 was 22.6 gpm over the period of October 2016 through
October 2017.
Historical TCE concentrations in recovered groundwater from RW-5 have ranged from a
low of 570 �tg/L (October 2016) to a high of 5,300 �tg/L (October 2014). The
concentration reported during this monitoring event was 1,400 �Lg/L. The average flow
rate for RW-5 was 3.2 gpm over the period of October 2016 through July 2017.
7 References
Corrective Action Monitoring Plan, CDM Smith, April 2009; modified 9 June 2014.
Resource Conservation andRecoveryAct (RCRA) Facility Investigation Report. CDM Smith,
August 2013.
Field Branches Quality System and Technical Procedures: SESDPROC- 010 (Logbooks). EPA
Region 4, Science and Ecosystem Support Division, Athens, Georgia, 30 May 2013.
Field Branches Quality System and Technical Procedures: SESDPROC- 005 (Sample and
Evidence Management). EPA Region 4, Science and Ecosystem Support Division, Athens,
Georgia, 29 January 2013.
Field Branches Quality System and Technical Procedures: SESDPROC- 100 (Field pH
Measurement). EPA Region 4, Science and Ecosystem Support Division, Athens, Georgia,
16 December 2016.
Field Branches Quality System and Technical Procedures: SESDPROC- 101 (Field Specific
Conductance Measurement). EPA Region 4, Science and Ecosystem Support Division,
Athens, Georgia, 13 July 2016.
Field Branches Quality System and Technical Procedures: SESDPROC- 102 (Field
Temperature Measurement). EPA Region 4, Science and Ecosystem Support Division,
Athens, Georgia, 23 October 2014.
Field Branches Quality System and Technical Procedures: SESDPROC- 105 (Groundwater
Level and Well Depth Measurement). EPA Region 4, Science and Ecosystem Support
Division, Athens, Georgia, 03 November 2016.
Field Branches Quality System and Technical Procedures: SESDPROC- 201 (Surface Water
Sampling). EPA Region 4, Science and Ecosystem Support Division, Athens, Georgia, 16
December 2016.
4

Corrective Action Monitoring Report
October 2017 Semiannual Event
Field Branches Quality System and Technical Procedures: SESDPROC- 203 (Pump
Operation). EPA Region 4, Science and Ecosystem Support Division, Athens, Georgia, 12
September 2013.
Field Branches Quality System and Technical Procedures: SESDPROC- 205 (Field Equipment
Cleaning and Decontamination). EPA Region 4, Science and Ecosystem Support Division,
Athens, Georgia, 18 December 2015.
Field Branches Quality System and Technical Procedures: SESDPROC- 301 (Groundwater
Sampling). EPA Region 4, Science and Ecosystem Support Division, Athens, Georgia, 16
April 2017.
Method 8260B: Volatile Organic Compounds by Gas ChromatographylMass Spectrometry
(GCIMS), part of Test Methodsfor Evaluating Solid Waste, Physical/Chemical Methods. US
Environmental Protection Agency, December 1996.
5

Corrective Action Monitoring Report
October 2017 Semiannual Event
Figures

Topographic Contour Interval
National Geodic Vertical Datui
1" = 11800'
900 Feet 0 1,800
Town of Murphy
Former Clifton
Prescision Site
CDN1
Smith
�7
Forrn�r Clifton
5�i toe
Precision Site
N
W E
S
Figure 1
Site Location Map
ier 2017 Semiannual Event
n. Action Monitoring Report
)rmer Clifton Precision Site
Murphy, North Carolina

MW-44
E
MW-47
Ilk
MW-41-*
Le W-63 A
t r-
At
MW MW-62 MW-50
MW-40
MW-61 V
fSW-3 CM
CM
AV
00
MW-14R
;w*_ 4 3
IL
MC-37
V4 . . . -
MW-53
'AA 44 .1 4
't J KW-38
SW-6 A
See Figure 2 L
4
+ MW-39
L
'to
bb
MW-17
MW_19R
V
Y MW_
-*MWM55
SW-1q &I
IP it
AN!
* Regolith Monitor Well (f) Regolith Recovery Well Regolith Re -Injection Well A RFI Surface Water Station Annual VOC Sampling Figure 2a
* Bedrock Monitor Well Bedrock Recovery Well Bedrock Re -Injection Well Spring 0 Water Level Only Scale in Feet Corrective Action Monitoring Locations
* Transition Monitor Well Bedrock Supply Well A Creek Monitoring Point Semi -Annual VOC Sampling October 2017 Semiannual Event
125 0 250 Co rrective Act ion M o n ito ri ng Repo rt
CDM water levels will also be collected from all well sampling locations. Former Clifton Precision Site
Smith All monitoring wells are shown but only those surface water stations and residential wells that have historically been sampled are shown. Murphy, North Carolina

N
W E MW-11
MW-2R +*
RW-3 MW-10
S G G)
MW-29 + MW-30
RW- 2 (D * _* MW-28
MW-36 MW-31
(D Rw-s
MW-32
MW-12
MW-8
MW-7
+ Regolith Monitor Well
Semi -Annual VOC Sampling
Bedrock Monitor Well
Annual VOC Sampling
Transition Monitor Well
0 Water Level Only
(D Regolith Recovery Well
Water levels will also be collected
EE) Bedrock Recovery Well
from all well sampling locations.
CDNI
Smith
44k^
MW-21+ MW-20
MW-22
Scale in Feet
32.5 0 65
Figure 2b
Onsite Well Locations
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina

CDM
smith
MW-46 (1612.58) r
AK C'
-do -7
IMesser/
Creek 10
A4
8) T
.041
S w Creek ir� I
k.
Ile
Foil Clifton IF.
I sion SiLe V
16 0 %
ql�nl .7
P
c_.X 4
!T 000" h A
4P Facility -Owned
f Parcel Lines
Properties
Coarse -Grained
A Alluvium Data Point 0
d Spring
d.
Groundwater
Reinjection Well
RegolithfTransition Zone Potentiometric Surface
23 October 2017
49-
06/" North American VertIcal Datum 1988
6 —1,610— 2-Foot Interval
Dashed contours inferred
based on professional judgement
Artesian - Water level not included
a 1. in potomiometric surfnm mapping.
N
Scale in Fect
0 300 600 900 1200
Figure 3: Regolith/Transition Zone
Potentiometric Surface Map
October 2017 CAMP Event
Former Clifton Precision Site
Murphy, Cherokee County, North Carolina

i".
;ser
ek
V,
r
t 1'r-ecision Site
rsp-26
'00,1
161%s
'00.
OOOP
100,
kL00,
.1 Ole .0'
�116 �e -
CDN1
Smith
Scale in Feet
I
0 300 600 900 1200
7,
Parcel Lines Facility -Owned
Properties
Coarse -Grained
Alluvium Data Point 0
Groundwater V Spring
Reinjection Wells
Bedrock Zone Potentiometric Surface
23 October 2017
North American Vertical Datum 1988
—1,610-5-Foot Interval
Dashed contours inferred
based on professio n al jud gerne rit
Figure 4: Bedrock Zone
Potentiometric Surface Map
October 2017 CAMP Event
Former Clifton Precision Site
Murphy, Cherokee County, North Carolina

"Id
WXIIIJ
WIIIIJ
X 800
M
600
a
IAIIIIJ
alid
—*--RW-2/RW-5 —0—RW-3
RW-4
Groundwater reinjection and thermal
remediation interim measures initiated -
RW-4 & RW-S extraction system shut down for a temporary
brought online period
A
V
nn A
New groundwater
r]
treatment system
AV'I Y-
I I
brought online.
A
A
0 --�
12/09
12/10 12/11 12/12 12/13 12/14 12/15 12/16 12/17
Figure 5: Groundwater
Recovery Volumes
October 2017 CAMP Event
CDNI Former Clifton Precision Site
Smith Murphy, North Carolina

Corrective Action Monitoring Report
October 2017 Semiannual Event
Tables

Table 1: Corrective Action Monitoring Schedule
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Station
Code
MW-9
Station Type
Screened Regolith
Station Location
Onsite, east site boundary
Monitoring Rationale
Potentionnetric surface mapping
vocs
Water
Level
x
MW-10
Screened Regolith
Onsite, north downgradient site boundary
Containment monitoring
x
x
MW-11
Open Bore PWR/Bedrock
Onsite, north downgradient site boundary
Containment monitoring
x
x
MW-12
Screened Regolith
Onsite, site interior, downgradient of source area
Source status monitoring
x
x
MW-13
Screened Regolith
Onsite, northwest downgradient site boundary
Containment monitoring
x
x
MW-14R
Bore Bedrock
Onsite, northwest downgradient site boundary
Potentionnetric surface mapping
x
_Open
MW-17
Screened PWR
Onsite, southwest upgradient site boundary
Sentinel well
X*
x
MW-18
IScreened Regolith
Onsite, southeast upgradient site boundary
Potentionnetric surface mapping
x
MW-19R
Open Bore Bedrock
Onsite, southeast upgradient site boundary
Potentiometric surface mapping
x
MW-20
Screened Regolith
Onsite, site interior
VOCs historically unstable
x
x
MW-22
Open Bore PWR/Bedrock
Onsite, site interior
Potentiometric surface mapping
x
MW-23
Screened Regolith
Offsite, northern flow area
Potentionnetric surface mapping
x
MW-25
Open Bore PWR/Bedrock
Offsite, northern flow area
Potentiometric surface mapping
x
MW-27
Screened Regolith
Onsite, east upgradient
Potentionnetric surface mapping
x
MW-28
Screened Regolith
Onsite, north downgradient site boundary
Containment monitoring
x
x
MW-29
Screened Regolith
Onsite, north downgradient site boundary
Potentionnetric surface mapping
x
MW-30
Screened Regolith/PWR
Onsite, north downgradient site boundary
Potentiometric surface mapping
x
MW-31
Screened Regolith/PWR
Onsite, site interior, downgradient of source area
Potentionnetric surface mapping
x
MW-32
Screened Regolith/PWR
Onsite, site interior, downgradient of source area
Source status monitoring
x
x
MW-33
Screened Regolith
Offsite, northwestern flow area
Offsite status monitoring
x
x
MW-34
Screened Regolith
Offsite, northern flow area
Offsite status monitoring
X*
x
MW-35
Screened Regolith
Offsite, northwestern flow area
Offsite status monitoring
x
x
MW-36
Screened Bedrock
Onsite, north downgradient site boundary
Source status monitoring
x
x
MW-37
Screened Bedrock
Onsite, west downgradient site boundary
Source status monitoring
x
x
MW-38
Screened Bedrock
Onsite, west site boundary
Potentiometric surface mapping
x
MW-39
Screened Bedrock
Onsi te, west site boundary
Potentionnetric surface mapping
x
MW-40
Screened Bedrock
Offsite, northwestern flow area
Reinjection monitoring
x
x
MW-41
Screened Bedrock
Offsite, northern flow area
Offsite status monitoring
X*
x
MW-42
Screened Regolith
Offsite, northwestern flow area
Offsite status monitoring
X*
x
MW-43
Screened Bedrock
Offsite, northwestern flow area
Offsite status monitoring
X*
x
MW-44
Screened Bedrock
Offsite, northwestern flow area
Potentiometric surface mapping
x
I MW-45
Screened Bedrock
southwest upgradient site boundary
Sentinel well
X*
x
I MW-46
_40nsite,
IScreened Regolith
10ffsite, northern flow area
Potentionnetric surface mapping
x
I MW-47
IScreened Bedrock
10ffsite, northern flow area
Sentinel well
X*
x
PWR - Partially weathered rock (transition zone) RFI - RCRA Facility Investigation Annual Monitoring in October
VOCs - Volatile organic compounds RCRA - Resource Conservation and Recovery Act
Page 1 of 2

Table 1: Corrective Action Monitoring Schedule
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Station
Code
MW-49
� Station Type
Screened Regolith
Station Location
Onsite, north siteTo—unTa—ry
Monitoring Rationale
Potentiometric surface mapping
vocs
Water
Level
MW-50
Screened Bedrock
Onsite, north site boundary
Potentiometric surface mapping
x
MW-51
Screened Bedrock
Offsite, western stream valley
Potentiometric surface mapping
x
MW-52
Screened Regolith
Offsite, western stream valley
Potentiometric surface mapping
x
MW-53
Screened Bedrock
Offsite, western stream valley
Potentiometric surface mapping
x
MW-54
Screened Regolith
Offsite, southwestern area
Potentiometric surface mapping
x
MW-55
IScreened Bedrock
Offsite, southwestern area
Potentiometric surface mapping
x
MW-56
Screened Transition
Onsite, west site boundary
Potentiometric surface mapping
x
MW-57
Screened Transition
Onsite, west site boundary
Potentiometric surface mapping
x
MW-60
Screened Regolith/Transition
Offsite, northwestern flow area
Offsite status monitoring
x
x
MW-61
Screened Bedrock
Offsite, northwestern flow area
Offsite status monitoring
x
x
MW-62
Screened Regolith/Transition
Offsite, northern flow area
Offsite status monitoring_
x
x
MW-63
Screened Bedrock
Offsite, northern flow area
Offsite status monitoring
x
x
RW-2
Screened Regolith Recovery
Onsite, recovery system
Containment monitorin
x
x
RW-3
Screened Regolith Recovery
Onsite, recovery system
Containment monitoring
x
x
RW-4
Screened Regolith Recovery
Onsite, recovery system
Containment monitoring
x
x
RW-5
Screened Bedrock Recovery
Onsite, recovery system
Containment monitoring
x
x
CMP-1
Creek Monitoring Point
Slow Creek upstream of site
Background
x
CMP-3
lCreek Monitoring Point
Slow Creek adjacent to site
Containment monitoring
x
CMP-4
Creek Monitoring Point
Slow Creek downstream of site
Containment monitoring
x
SW-3
RFI Surface Water Station
Slow Creek downstream of site
Offsite status monitoring
x
SW-6
RFI Surface Water Station
Slow Creek downstream of site
Offsite status monitoring
x
SW-10
RFI Surface Water Station
Slow Creek downstream of site
Sentinel station
x
PW-16
Bedrock Supply Well
Offsite, western flow area
Offsite status monitorinq
X*
x
SP-26
Spring
10ffsite, western stream valley
10ffsite status monitoring
X*
PWR - Partially weathered rock (transition zone) RFI - RCRA Facility Investigation Annual Monitoring in October
VOCs - Volatile organic compounds RCRA - Resource Conservation and Recovery Act
Page 2 of 2

Table 2: Summary of Hydrogeologic Zones
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
* - Rock types are listed from most to least frequently observed and are commonly interlayered.

Table 3: Well Construction and Water Level Data
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Well Code iWell Type
MW-9 Onsite Screened Regolith
Date
LstalleJ
Apr-87
Iopen
Diameter Total Depth Elevation I
Inches I Feet BGS I TOC Feet
2 25 1623.21
interval Water Surface
R I Feet (10-23-2017)
F -From I To I Depth IlElevation
5 25 5.61 1,617.60
MW-10
Onsite Screened Regolith
Mar-87
2
40
1620.35
17.5
37.5
7.44
1,612.91
MW-11
Onsite Open Bore PWR/Bedrock
Apr-87
4
73.5
1620.83
27
73.5
8.06
1,612.77
MW-12
Onsite Screened Regolith
Nov-88
2
29.5
1633.79
19
29
22.50
1,611.29
MW-13
Onsite Screened Regolith
Nov-88
2
29.8
1619.08
9.8
29.8
7.54
1,611.54
MW-14R
Onsite Open Bore Bedrock
Dec-88
6
78
1620.08
42
78
9.49
1,610.59
MW-17
Onsite Screened PWR
Nov-88
2
49.5
1631.76
29.5
49.5
9.18
1,622.58
MW-18
Onsite Screened Regolith
Nov-88
2
64
1633.79
44
64
15.14
1,618.65
MW-19R
Onsite Open Bore Bedrock
Dec-88
6
74.5
1632.00
66.5
74.5
14.92
1,617.08
MW-20
Onsite Screened Regolith
Nov-88
2
15.5
1621.77
5.5
15.5
7.18
1,614.59
MW-22
Onsite Open Bore PWR/Bedrock
Dec-88
6
52
1622.07
32
52
7.27
1,614.80
MW-23
Ciffsite Screened Regolith
Mar-91
2
21
1614.56
10
20
8.03
1,606.53
MW-25
Ciffsite Screened PWR/Bedrock
Mar-91
2
41
1615.02
28
38
7.56
1,607.46
MW-27
Onsite Screened Regolith
Jul-96
4
72
1636.21
62
72
18.16
1,618.05
MW-28
Onsite Screened Regolith
Jul-96
4
36
1618.38
26
36
4.10
1,614.28
MW-29
Onsite Screened Regolith
Jun-00
2
30
1620.32
20
30
9.14
1,611.18
MW-30
Onsite Screened Regolith/PWR
Jun-00
2
24
1617.80
14
24
Dest ed
MW-31
Onsite Screened Regolith/PWR
Jun-00
2
25
1619.58
15
25
6.67
1,612.91
MW-32
Onsite Screened Regolith/PWR
Jun-00
2
32
1620.90
22
32
8.65
1,612.25
MW-33
Ciffsite Screened Regolith
Jul-06
2
75
1610.85
70
75
0.00
1,610.85
MW-34
Ciffsite Screened Regolith
Jul-06
2
41
1619.36
36
41
5.39
1,613.97
MW-35
Ciffsite Screened Regolith
Jul-06
2
91
1619.22
86
91
7.15
1,612.07
MW-36
Onsite Screened Bedrock
Jun-06
2
70
1620.77
65
70
32.02
1,588.75
MW-37
Onsite Screened Bedrock
Jun-06
2
108
1630.60
101
106
21.87
1,608.73
MW-38
Onsite Screened Bedrock
Jun-06
2
101
1653.92
96
101
44.12
1,609.80
MW-39
Onsite Screened Bedrock
Jul-06
2
161
1650.79
151
161
37.69
1,613.10
MW-40
Ciffsite Screened Bedrock
Jul-06
2
161.5
1610.95
146.5
156.5
0.51
1,610.44
MW-41
Ciffsite Screened Bedrock
Jul-06
2
159
1618.93
149
159
5.15
1,613.78
MW-42
Ciffsite Screened Regolith
May-07
2
28
1610.19
18
28
3.98
1,606.21
MW-43
Ciffsite Screened Bedrock
Jun-07
2
83
1622.64
78
83
17.32
1,605.32
MW-44
Ciffsite Screened Bedrock
May-07
2
73
1618.35
68
73
7.26
1,611.09
MW-45
Onsite Screened Bedrock
Nov-07
2
95
1631.02
72.5
77.5
. 10.12
1,620.90.
MW-46
Ciffsite Screened Regolith
May-07
2
53
1626.19
43
53
13.61
1,612.58
MW-47
Ciffsite Screened Bedrock
May-07
2
83
1626.46
78
83
13.64
1,612.82
MW-49
Onsite Screened Regolith
May-07
2
12
1620.62
7
12
5.17
1,615.45
MW-50
Onsite Screened Bedrock
3un-07
2
82
1620.59
77
82
5.09
1,615.50
MW-51
Ciffsite Screened Bedrock
Nov-07
2
115.5
1602.66
105.5
115.5
1.86
1,600.80
MW-52
Ciffsite Screened Regolith
Nov-07
2
42
1604.88
32
42
1.70
1,603.18
MW-53
Ciffsite Screened Bedrock
Nov-07
2
52
1604.93
47
52
0.88
1,604.05
MW-54
Ciffsite Screened Regolith
Jan-08
2
38
1637.61
28
38
19.31
1,618.30,
MW-55
Ciffsite Screened Bedrock
Jan-08
2
110
1637.41
105
110
18.45
11618.96
MW-56
Onsite Screened Transition
Sep-11
2
76.5
1644.97
61.5
76.5
18.68
1,626.29
MW-57
Onsite Screened Transition
Sep-11
2
90
1640.86
80
90
25.25
1,615.61
MW-60
Ciffsite Screened Regolith/Transition
Sep-11
2
48
1611.26
38
1 48
0.00
1,611.26
MW-61
Ciffsite Screened Bedrock
Sep-11
2
90
1611.58
80
90
0.00
1,611.58
MW-62
Ciffsite Screened Regolith/Transition
Sep-11
2
43.5
1614.87
33.5
43.5
1.18
1,613.69
MW-63
Ciffsite Screened Bedrock
Sep-11
2
4
1615.17
74
84
0.00
1,615.17
RW-2
Screened Regolith Recovery
Aug-00
4
42
1624.71
17
0.00
1,624.71
RW-3
Screened Regolith Recovery
Aug-00
4
42
1620.99
17
37
30.01
1,590.98
RW-4
Screened Regolith Recovery
Oct-08
6
65
1627.49
30
g37
60
24.91
1,602.58
RW-5
Screened Bedrock Recovery
Oct-08
6
119
1623.7 ,
64
114!
10
10704!4
1,516.26,
BGS - Below ground surface
TOC - Top of casing
PWR - Partially weathered rock (transition zone)
Elevation is National Geodic Vertical Datum, 1929
Page 1 of 1

Table 4: Regolith/Transition Zone Groundwater Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
SampleCodej
Description I
Sample Date
Compound MCL(pg/L)
MW-10
-
10/24/2017
I MW-12
10/27/2017
I MW-13
I MW-17
I MW-20
I MW-28
I MW-32
I MW-33
I MW-34
10/24/2017
9
10/24/2017
ND
10/24/201
ND
10/24/2017
1
10/30/2017
72
10/25/2017
ND
10/25/2017
ND
1, 1, 1 -Trichloroethane 200
ND
136
1, 1,2-Trichloro-1,2,2-trifluoroethane IN E
NID
376
5
ND
1
1
76
ND
ND
1,1-Dichloroethane NE
ND
105
2
ND
ND
7
27
ND
ND
1,1-Dichloroethene 7
NID
219
4
NID
NID
2
91
NID
NID
1,4-Dichlorobenzene 75
ND
ND
ND
ND
ND
ND
ND
ND
ND
2-Butanone NE
NID
NID
NID
ND
NID
ND
ND
ND
ND
Acetone NE
NID
NID
NID
ND
ND
ND
ND
ND
ND
Bromodichloromethane 80*
IND
0.218
ND
ND
ND
ND
IND
ND
ND
Carbon disulfide NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
Chloroform 80*
10
13
NID
NID
NID
ND
6.2
ND
IND
Chloromethane NE
ND
ND
ND
ND
ND
ND
ND
ND
ND
cis-1,2-Dichloroethene 70
1.0
388
7
NID
39
3
76
NID
NID
Dichlorodifluoromethane (CFC-12) NE
ND
60
ND
ND
ND
ND
ND
ND
ND
Methyl tert-butyl ether NE
NID
NID
NID
NID
NID
NID
ND
ND
ND
Methylene Chloride 5
ND
ND
ND
ND
ND
ND
ND
ND
ND
Tetrachloroethene 5
NID
176
4
NID
NID
7
99
NID
NID
Toluene 1,000
NID
ND
ND
ND
ND
ND
ND
ND
ND
trans- 1,2-Dichloroethene 100
NID
ND
ND
ND
ND
ND
ND
ND
ND
Trichloroethene 5
34
1690
120
NID
1.6
22
334
5.7
2.8
Vinyl chloride 2
NID
3.8
NID
NID
NID
14
0.7
NID
NID
pg/L - Micrograms per liter. * - Total trilhalomethanes (chloroform + bromodichloromethane + clibromochloromethane + bromoform).
MCL - Federal Maximum Contaminant Level. B - This compound was also detected in a corresponding method blank or trip blank at a reportable level.
NE - MCL not established. J - Estimated result, result is less than the RL.
No - Not detected, result is below reporting limit (RL). D - Diluted sample was analyzed because undiluted sample result exceeded calibration range
PWR - Partially weathered rock (transition zone) H - Sample was prepped or analyzed beyond specified holding time
NM - Not measured Samples analyzed for 49 volatile organic compounds (VOCs) by Method 8260B.
E - Result exceeded calibration range
Compounds listed in this table are the VOCs reported above the RL in any sample reported during the RCRA Facility Investigation or subsequent testing.
NIS - Not Sampled Bold indicates the detected concentration was greater than the MCL.
Page 1 of 2

Table 4: Regolith/Transition Zone Groundwater Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Sample Codel
Description I
Sample Date
Compound MCL(pg/L)
MW-35
Offsite
Regolith
10/24/2017
I MW-42
Offsite
Regolith
10/24/2017
I MW-60
Offsite
Regolith
I MW-62
Offsite
Regolith
I RW-2 '
Regolith
Monitoring Well
I RW-3
Regolith Recovery
Well
I RW-4
Regolith
Recovery Well
10/25/2017
ND
10/25/2017
ND
10/26/2017
ND
10/26/2017
59
10/27/2017
39
1, 1, 1 -Trichloroethane 200
ND
ND
1, 1,2-Trichloro-1,2,2-trifluoroethane NE
NID
NID
NID
ND
ND
91
232
1,1-Dichloroethane NE
ND
ND
ND
ND
ND
4.8
10.5
1,1-Dichloroethene 7
NID
NID
NID
ND
ND
44
40.1
1,4-Dichlorobenzene 75
ND
ND
ND
ND
ND
ND
ND
2-Butanone NE
NID
NID
NID
NID
NID
ND
ND
Acetone NE
NID
NID
NID
ND
ND
ND
ND
Bromodichloromethane 80*
NID
NID
ND
ND
ND
ND
IND
Carbon disulfide NE
ND
ND
ND
ND
ND
ND
ND
Chloroform 80*
NID
NID
NID
NID
NID
11
3.52
Chloromethane NE
ND
ND
ND
ND
ND
ND
ND
cis-1,2-Dichloroethene 70
1.2
NID
NID
5.4
ND
7.9
24.8
Dichlorodifluoromethane (CFC-12) NE
ND
ND
ND
ND
ND
ND
4.91
Methyl tert-butyl ether NE
NID
NID
NID
NID
NID
IND
ND
Methylene Chloride 5
ND
ND
ND
ND
ND
ND
ND
Tetrachloroethene 5
NID
NID
NID
NID
ND
39
36
Toluene 1,000
NID
ND
ND
ND
ND
ND
ND
trans- 1,2-Dichloroethene 100
NID
ND
ND
ND
ND
ND
IND
Frichloroethene 5
15
ND
7.3
4.7
6.5
270
397
IVinyl chloride 2
NID
ND
IND
IND
1.4
ND
pg/L - Micrograms per liter * - Total trilhalomethanes (chloroform + bromodichloromethane + dibromochloromethane + bromoform).
MCL - Federal Maximum Contaminant Level B - This compound was also detected in a corresponding method blank or trip blank at a reportable level.
NE - MCL not established J - Estimated result, result is less than the RL.
No - Not detected, result is below reporting limit (RL). D - Diluted sample was analyzed because undiluted sample result exceeded calibration range
PWR - Partially weathered rock (transition zone) H - Sample was prepped or analyzed beyond specified holding time
NM - No measurement Samples analyzed for 49 volatile organic compounds (VOCs) by Method 8260B
E - Result exceeded calibration range
Compounds listed in this table are the VOCs reported above the RL in any sample reported during the RCRA Facility Investigation or subsequent testing.
NIS - Not Sampled Bold indicates the detected concentration was greater than the MCL
1 Recovery well RW-2 converted to monitoring well and replaced with Recovery Well RW-5.
Page 2 of 2

Table 5: Bedrock Zone Groundwater Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
SampleCode MW-11 MW-36 MW-37 MW-40 MW-41
Description / Onsite PWR - Onsite Onsite Offsite Offsite
Sample Datel Bedrock Bedrock Bedrock Bedrock Bedrock
Compound MCL(pg/L) 10/24/2017 10/25/2017 10/27/2017 10/25/2017 10/25/2017
1, 1, 1 -Trichloroethane 200 ND 13 17 ND ND
MW-43 MW-45
Offste Onsite
Bedrock Bedrock
10/24/2017
ND ND
1, 1,2-Trichloro-1,2,2-trifluoroethane NE
ND
20
20.8
ND
ND
ND
ND
1, 1 -Dichloroethane NE
3.2
19
224
ND
ND
ND
ND
1, 1 -Dichloroethene 7
7.6
55
ill
ND
13
ND
ND
1,4-Dichlorobenzene 75
ND
ND
ND
ND
ND
ND
ND
2-Butanone NE
ND
ND
ND
ND
ND
ND
ND
Acetone NE
ND
ND
ND
ND
ND
ND
ND
Bromodichloromethane 80*
ND
ND
ND
ND
ND
ND
ND
Carbon disulficle NE
ND
ND
0.309
ND
ND
ND
ND
Carbon Tetrachloride 5
ND
ND
ND
ND
ND
ND
ND
Chloroform 80*
ND
4.7
0.361
ND
ND
ND
ND
Chloromethane NE
ND
ND
ND
ND
ND
ND
ND
cis-1,2-Dichloroethene 70
46
49
1550
ND
230
ND
ND
Dichlorodifluoromethane (CFC-12) NE
ND
ND
13.7
ND
ND
ND
ND
Methyl tert-butyl ether NE
ND
ND
ND
ND
ND
ND
ND
Methylene Chloride 5
ND
ND
ND
ND
ND
ND
ND
Tetrachloroethene 5
5.5
45
253
ND
11
ND
ND
Toluene 1,000
ND
ND
0.448
ND
ND
ND
ND
trans-1,2-Dichloroethene 100
ND
ND
5.41
ND
ND
ND
ND
Trichloroethene 5
120
320
10,700
ND
920
4.5
ND
Vinyl chloride 2
ND
1.2
39.6
ND
56
ND
ND
pg/L - Micrograms per liter. * - Total trilhalomethanes (chloroform + bromodichloromethane + dibromochloromethane + bromoform).
MCL - Federal Maximum Contaminant Level. B - This compound was also detected in a corresponding method blank or trip blank at a reportable level.
NE - MCL not established. J - Estimated result, result is less than the RL.
ND - Not detected, result is below reporting limit (RIL). Samples analyzed for 49 volatile organic compounds (VOCs) by Method 8260B.
PWR - Partially weathered rock (transition zone) Compounds listed in this table are the VOCs reported above the RL in any sample reported during the RCRA Facility Investigation
or subsequent testing.
NS - Not Sampled Bold indicates the detected concentration was greater than the MCL.
Page 1 of 2

Table 5: Bedrock Zone Groundwater Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Sample Codel
Descriptiorfi���
Sample Da
MW-47
I MW-61
I MW-63
I RW-5'
—
Compound MCL(pg/L)
1, 1, 1 -Trichloroethane 200
10/25/2017
ND
10/25/2017
ND
10/27/2017
IND
10/26/2017
110
1, 1,2-Trichloro-1,2,2-trifluoroethane NE
ND
ND
ND
ND
1, 1 -Dichloroethane NE
ND
ND
ND
180
1, 1 -Dichloroethene 7
ND
ND
ND
64
1,4-Dichlorobenzene 75
ND
ND
ND
ND
2-Butanone NE
ND
ND
ND
ND
Acetone NE
ND
ND
ND
ND
Bromodichloromethane 80*
ND
ND
ND
ND
Carbon disulfide NE
ND
ND
ND
ND
Carbon Tetrachloride 5
ND
ND
ND
ND
Chloroform 80*
ND
ND
ND
ND
Chloromethane NE
ND
ND
ND
ND
cis-1,2-Dichloroethene 70
ND
ND
12
160
Dichlorodifluoromethane (CFC-12) NE
ND
ND
ND
ND
Methyl tert-butyl ether NE
ND
ND
ND
ND
Methylene Chloride 5
ND
ND
ND
ND
Tetrachloroethene 5
ND
ND
ND
74
Toluene 1,000
ND
ND
ND
ND
trans-1,2-Dichloroethene 100
ND
ND
ND
ND
Trichloroethene 5
ND
15
13
1400
lVinyl chloride 2
1 IND
I ND
I ND
I ND
pg/L - Micrograms per liter. * - Total trilhalomethanes (chloroform + bromodichloromethane + dibromochloromethane + bromoform).
MCL - Federal Maximum Contaminant Level. B - This compound was also detected in a corresponding method blank or trip blank at a reportable level.
NE - MCL not established. J - Estimated result, result is less than the RL.
ND - Not detected, result is below reporting limit (RIL). Samples analyzed for 49 volatile organic compounds (VOCs) by Method 8260B.
PWR - Partially weathered rock (transition zone) Compounds listed in this table are the VOCs reported above the RL in any sample reported during the RCRA Facility Investigation
or subsequent testing.
Bold indicates the detected concentration was greater than the MCL.
1 Recovery well RW-2 converted to monitoring well and replaced with Recovery Well RW-5.
Page 2 of 2

Table 6: Surface Water Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Sample Code
Description /
Sample Date
Compound MCL(pg/L)
1,1,1-Trichloroethane 200
CMP-1
Surface
Water
CMP-3
Surface
Water
CMP-4
Surface
Water
SW-3
Surface
Water
SW-6
Surface
Water
SW-1 0
Surface
Water
10/27/2017
IND
10/27/2017
1.1
10/27/2017
IND
10/27/2017
IND
10/27/2017
IND
10/27/2017
IND
1,1,2-Trichloro-1,2,2-trifluoroethane NE
ND
ND
IND
IND
IND
IND
1,1-Dichloroethane NE
ND
ND
ND
ND
IND
IND
1,1-Dichloroethene 7
ND
ND
ND
IND
IND
IND
1,4-Dichlorobenzene 75
ND
ND
IND
IND
IND
ND
2-Butanone NE
ND
ND
ND
ND
ND
ND
Acetone NE
ND
ND
ND
ND
ND
ND
Bromodichloromethane 80*
ND
ND
IND
IND
IND
ND
Bromomethane NE
ND
ND
ND
ND
ND
IND
Carbon disulfide NE
ND
ND
ND
ND
IND
IND
Chloroform 80*
ND
ND
ND
ND
ND
IND
Chloromethane NE
ND
ND
ND
ND
IND
IND
cis-1,2-Dichloroethene 70
ND
ND
IND
IND
IND
ND
Dichlorodifluoromethane (CFC-12) NE
IND
IND
IND
ND
ND
ND
Methyl tert-butyl ether NE
ND
ND
ND
ND
ND
ND
Methylene Chloride 5
ND
ND
ND
IND
IND
IND
Tetrachloroethene 5
ND
ND
ND
ND
IND
IND
Toluene 1,000
ND
ND
ND
ND
ND
IND
trans- 1,2-Dichloroethene 100
ND
IND
IND
IND
ND
ND
Trichloroethene 5
ND
4.3
2.3
1.9
ND
ND
,Vinyl chloride 2
ND
ND
ND
ND
IND
IND
pg/L - Micrograms per liter. * - Total trilhalomethanes (chloroform + bromodichloromethane + clibromochloromethane + bromoform).
MCL - Federal Maximum Contaminant Level. B - This compound was also detected in a corresponding method blank or trip blank at a reportable level.
NE - MCL not established. J - Estimated result, result is less than the RL.
ND - Not detected, result is below reporting limit (RL). Samples analyzed for 49 volatile organic compounds (VOCs) by Method 8260B.
NIS - Not Sampled Compounds listed in this table are the VOCs reported above the RL in any sample reported during the RCRA Facility
Investigation or subsequent testing.
Bold indicates the detected concentration was greater than the MCL.
Page 1 of 1

Table 7: Private Well and Spring Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Sample Code
Description /
Sample Datel
Compound MCL(pg/L)
PWA 6
Bedrock
Supply Well
10/27/2017
SP-26
Spring
I
10/27/2017
1,1,1-Trichloroethane 200
ND
ND
1,1,2-Trichloro-1,2,2-trifluoroethane NE
ND
1.5
1,1-Dichloroethane NE
ND
ND
1,1-Dichloroethene 7
ND
ND
1,4-Dichlorobenzene 75
ND
ND
2-Butanone NE
ND
ND
Acetone NE
ND
ND
Bromodichloromethane 80*
ND
ND
Carbon disulfide NE
ND
ND
Chloroform 80*
ND
ND
Chloromethane NE
ND
ND
cis- 1,2-Dich loroethene 70
ND
ND
Dichlorodifluoromethane (CFC-12) NE
ND
ND
Methyl tert-butyl ether NE
ND
ND
Methylene Chloride 5
ND
ND
Tetrachloroethene 5
ND
ND
Toluene 1,000
ND
ND
trans- 1,2-Dich loroethene 100
ND
ND
Trichloroethene 5
ND
1.9
,Vinyl chloride 2
ND
ND
pg/L - Micrograms per liter. * - Total trihalomethanes (chloroform + bromodichloromethane + dibromochloromethane + bromoform).
MCL - Federal Maximum Contaminant Level. B - This compound was also detected in a corresponding method blank or trip blank at a reportable level.
NE - MCL not established. J - Estimated result, result is less than the RL.
No - Not detected, result is below reporting limit (RL). Samples analyzed for 49 volatile organic compounds (VOCs) by Method 8260B.
NS - Not Sampled Compounds listed in this table are the VOCs reported above the RL in any sample reported during the RCRA Facility Investigation or subsequent testing.
Bold indicates the detected concentration was greater than the MCL.
Page I of I

Table 8: Quality Assurance/Quality Control Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
Sample Codel
Description /I
Sample Date
Compound MCL(pg/L)
MW-20
Onsite I
Regolith
I DUP-1
MW-20
Duplicate
MW-35
Offsite
Bedrock
I DUP-2
MW-35
Duplicate
I MW-33 DUP-3
Offsite MW-33_
Regolith I, d r�t
MW-61
Offsite
R-dr-Hc
DUP-4
iiiiiiiiiiiii!m'
NMM I =
10/24/2017
ND
10/24/2017
ND
10/24/2017
ND
10/24/2017
ND
10/25/2017 10/25/2017
ND ND
�5/201�7
ND
10/25/2017
ND
1, 1, 1 -Trichloroethane 200
1, 1,2-Trichloro-1,2,2-trifluoroethane N E
1.4
1.7
N D
N D
ND
ND
ND
ND
1, 1 -Dichloroethane N E
ND
ND
N D
N D
ND
ND
ND
47
1, 1 -Dichloroethene 7
ND
ND
N D
N D
ND
ND
ND
8.8
1,4-Dichlorobenzene 75
ND
ND
N D
N D
ND
ND
ND
ND
2-Butanone N E
ND
ND
N D
N D
ND
ND
ND
ND
Acetone N E
ND
ND
N D
N D
ND
ND
ND
ND
Bromodichloromethane 80*
ND
ND
N D
N D
ND
ND
ND
ND
Carbon disulfide NE
ND
ND
ND
ND
ND
ND
ND
ND
Carbon Tetrachloride 5
ND
ND
ND
ND
ND
ND
ND
ND
Chloroform 80*
ND
ND
ND
ND
ND
ND
ND
23
Chloromethane NE
ND
ND
ND
ND
ND
ND
ND
ND
cis- 1,2-Dich loroethene 70
39
39
1.2
1
ND
ND
ND
6.6
Dichlorodifluoromethane (CFC-12) NE
ND
ND
ND
ND
ND
ND
ND
ND
Methyl tert-butyl ether NE
ND
ND
ND
ND
ND
ND
ND
ND
Methylene Chloride 5
ND
ND
ND
ND
ND
ND
ND
ND
Tetrachloroethene 5
ND
ND
ND
ND
ND
ND
ND
45
Toluene 1,000
ND
ND
ND
ND
ND
ND
ND
110
trans- 1, 2-Dich loroethene 100
ND
ND
ND
ND
ND
ND
ND
ND
Trichloroethene 5
1.6
1.9
15
15
5.7
5.7
15
91
Vinyl chloride 2
ND
ND
ND
ND
ND
ND
ND
13
pg/L - Micrograms per liter. * - Total trihalomethanes (chloroform + bromodichloromethane + dibromochloromethane + bromoform).
MCL - Federal Maximum Contaminant Level. B - This compound was also detected in a corresponding method blank or trip blank at a reportable level.
NE - MCL not established. J - Estimated result, result is less than the RL.
ND - Not detected, result is below reporting limit (RL). Samples analyzed for 49 volatile organic compounds (VOCs) by Method 8260B.
PWR - Partially weathered rock Compounds listed in this table are the VOCs reported above the RL in any sample reported during the RCRA Facility Investigation
or subsequent testing.
Bold indicates the detected concentration was greater than the MCL.
Page 1 of 1

Table 9: Groundwater Recovery Data Summary
October 2017 Semiannual Event
Corrective Action Monitoring Report
Former Clifton Precision Site
Murphy, North Carolina
RW-1S
RW-1D
Operation Ceased in October 2014
Operation Ceased September 2010
Recovery WeL
RW-3
RW-4
Days Average Flowl
Days Average Flowl
MonthNear
Total Gallons
Operated
gpm
Remarks
Total Gallons
Operated
gpm
Remarks
November 2016
67,093
30
1.55
11/3/16 - System Login Fixed. Data reporting again.
944,421
30
21.86
11/3/16 - System Login Fixed. Data reporting again
December 2016
57,253
31
1.28
994,305
31
22.27
January 2017
90,794
31
2.03
966,170
31
21.64
February 2017
31,686
28
0.79
914,556
28
22.68
March 2017
30,914
31
0.69
1,027,746
31
23.02
April 2017
26,834
30
0.62
1,004,988
30
23.26
May 2017
29,940
31
0.67
1,022,246
31
22.90
June 2017
30,848
30
0.71
6112/17 - System shutdown to fix cracked fitting near SP-3.
1,008,900
30
23.35
611 2/17 - System shutdown to fix cracked fitting near SP-
10:00 System returned to service.
3. 10:00 System returned to service.
July 2017
40,396
31
0.90
1,041,705
31
23.34
8125/17 - Facility Power Outage. System restarted however
8125/17 - Facility Power Outage. System restarted
IRW-4 not communicating.
however RW-4 not communicating.
August 2017
35,677
29
0.85
934,645
29
22.38
8128/17 - System returned to normal operat on. RW4 still
8128/17 - System returned to normal operation. RW4 still
not communicating, however pump is running.
not communicating, however pump is running.
9/5/17. Facility Power Outage.
9/5/17. Facility Power Outage.
9/7/17 - System restarted at 09:30am. Communication with
9/7/17 - System restarted at 09:30am. Communication
September 2017
28,455
29
0.68
IRW-4 re-established, however well is not responding to
951,688
29
22.79
with IRW-4 re-established, however well is not responding
changes in inputs from remote operator.
to changes in inputs from remote operator.
9/15/17 - Full communications and operator control have
9/15/17 - Full communications and operator control have
been restored to RW-4 at 13:30.
been restored to RW-4 at 13:30.
October 2017
j 51,345
j 31
1.15
989,852
31
1 22.17
1.00
November 2016
0
0
1�!116 - System Login Fixed. Data reporting again,
- 'x
December 2016
0
0 0.00
7RW-5Communication
January 2017
97,891
2672.61
11'5'11'7 - _ Commu c error fixed.
February 2017
113,598
28 2.82
March 2017
168,094
31 3.77
April 2017
151,945
30 3.52
May 2017
131,166
26 3.50
June 2017
135,817
3.14
112/17 - System shutdown to fix cracked fitting near SP-3,
30
10:00 System returned to service.
July 2017
130,833
31 2.93
8125/17 - Facility Power Outage. System restarted however
IRW-4 not communicating,
August 2017
139,674
29
3.34
8128/17 - System returned to normal operation. RW4 still
not communicating, however pump is running.
915/17 - Facility Power Outage.
917/17 - System restarted at 09:30am. Communication with
September 2017
143,808
29
3.44
IRW-4 re-established, however well is not responding to
changes in inputs from remote operator,
9115/17 - Full communications and operator control have
been restored to RW-4 at 13:30.
lOctober 2017
141,064
31 3.16
gpm - gallons per minute
Page 1 of 1

Corrective Action Monitoring Report
October 2017 Semiannual Event
Appendix A
(CD Format Only)

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
TestAmerica Job ID: 680-144889-1
Client Project/Site: Murphy. NC, October 2017
Foi
GHD Services Inc.
2055 Niagara Falls Blvd., Suite 3
Niagara Falls, New York 14304
Attn: Ms. Sue Scrocchi
_)LJ"' C'_
Authorized for release by.-
1111012017 8:23:33 AM
Keaton Conner, Project Manager 1
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestAmerica Job ID: 680-144889-1
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3
Sample Summary .........................................
5
Method Summary .........................................
6
Definitions...............................................
7
Detection Summary ........................................
8
Client Sample Results ......................................
13
Surrogate Summary .......................................
93
QC Sample Results ........................................
95
Chronicle................................................
131
Chain of Custody ..........................................
138
Certification Summary ......................................
142
Page 2 of 142
TestArnerica Savannah
11/10/2017

Case Narrative
Client: GHID Services Inc. TestAmerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Job ID: 680-144889-1
Laboratory: TestArnerica Savannah
Narrative L
CASE NARRATIVE
Client: GHD Services Inc.
Project: Murphy. NC, October 2017
Report Number: 680-144889-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT I
The samples were received on 10/28/2017; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 5.3 C.
VOLATILE ORGANIC COMPOUNDS (GC -MS)
Samples J1 155-MW-1 0-102417 (680-144889-1), J1 155-MW-1 1-102417 (680-144889-2), J1 155-MW-1 3-102417 (680-144889-3),
J1 155-MW-1 7-102417 (680-144889-4), J1 155-MW-20-102417 (680-144889-5), J1 155-MW-28-102417 (680-144889-6),
J1 155-MW-33-102517 (680-144889-7), J1 155-MW-34-102517 (680-144889-8), J1 155-MW-35-102417 (680-144889-9),
J1 155-MW-36-102517 (680-144889-10), J1 155-MW-40-102517 (680-144889-11), J1 155-MW-41-102517 (680-144889-12),
J1 155-MW-42-102417 (680-144889-13), J1 155-MW-43-102417 (680-144889-14), J1 155-MW-45-102417 (680-144889-15),
J1 155-MW-47-102517 (680-144889-16), J1 155-MW-60-102517 (680-144889-17), J1 155-MW-61-102517 (680-144889-18),
J1 155-MW-62-102517 (680-144889-19), J1 155-MW-63-102717 (680-144889-20), J1 155-PW-1 6-102717 (680-144889-21),
J1 155-SP-26-102717 (680-144889-22), J1 155-CMP-1-1 02717 (680-144889-23), J1 155-CMP-3-102717 (680-144889-24),
J1 155-CMP-4-102717 (680-144889-25), J1 155-SW-3-102717 (680-144889-26), J1 155-SW-6-102717 (680-144889-27),
J1 155-SW-10-102717 (680-144889-28), J1 155-RW-2-102617 (680-144889-29), J1 155-RW-3-102617 (680-144889-30),
J1 155-RW-5-102617 (680-144889-31), J1 155-DUP-1-102417 (680-144889-32), J1 155-DUP-2-102417 (680-144889-33),
J1 155-DUP-3-102517 (680-144889-34), J1 155-DUP-4-102517 (680-144889-35), J1 155-EB-01-102417 (680-144889-36),
J1 155-EB-02-102517 (680-144889-37), J1 155-EB-03-102617 (680-144889-38), J1 155-EB-04-102717 (680-144889-39) and
J1 155-TB-1 02417 (680-144889-40) were analyzed for Volatile Organic Compounds (GC -MS) in accordance with EPA SW-846 Method
8260B. The samples were analyzed on 11/03/2017, 11/04/2017, 11/05/2017, 11/06/2017, 11/07/2017, 11/08/2017 and 11/09/2017.
Samples J1 155-MW-36-102517 (680-144889-10)[2X], J1 155-MW-41-102517 (680-144889-12)[10X], J1 155-RW-3-102617
(680-144889-30)[2X], J1 155-RW-5-102617 (680-144889-31)[10X] and J1 155-RW-5-102617 (680-144889-31)[20X] required dilution prior
to analysis. The reporting limits have been adjusted accordingly.
Dibromofluoromethane (Surr) recovered high for LCSID 680-501395/4.
Methyl acetate recovered low for LCS 680-501326/6 and LCS 680-501359/3.
1,2,4-Trichlorobenzene recovered high for LCS 680-501694/3.
Dibromochloromethane, Tetrachloroethene and Toluene recovered high for LCS 680-501730/3.
1,2,4-Trichlorobenzene recovered high for LCS 680-501749/4, LCSD 680-501694/4 and LCSD 680-501749/5.
2-Hexanone, Methyl acetate and Tetrahydrofuran recovered low for LCSID 680-501326/7.
TestAmerica Savannah
Page 3 of 142 11/10/2017

Case Narrative
Client: GHID Services Inc. TestAmerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Job ID: 680-144889-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
2-Hexanone, 4-Methyl-2-pentanone, Methyl acetate and Tetrahydrofuran recovered low for LCSD 680-501359/4.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 4 of 142 11/10/2017

Sample Summary
Client: GHID Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy.
NC, October 2017
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
680-144889-1
A 155-MW-10-102417
Water
10/24/17 08:53
10/28/17 10:40
680-144889-2
A 155-MW-1 1-102417
Water
10/24/17 09:33
10/28/17 10:40
680-144889-3
A 155-MW-13-102417
Water
10/24/17 10:39
10/28/17 1 0:40
680-144889-4
J1 155-MW-17-102417
Water
10/24/17 13:53
10/28/17 10:40
680-144889-5
J1 155-MW-20-102417
Water
10/24/17 10:07
10/28/17 10:40
680-144889-6
J 1 155-MW-28-102417
Water
10/24/17 15:09
10/28/17 10:40
680-144889-7
J 1 155-MW-33-102517
Water
10/25/17 09:19
10/28/17 10:40
680-144889-8
J 1 155-MW-34-102517
Water
10/25/17 14:41
10/28/17 10:40
680-144889-9
J 1 155-MW-35-102417
Water
10/24/17 11:39
10/28/17 1 0:40
680-144889-10
J 1 155-MW-36-102517
Water
10/25/17 08:28
10/28/17 10:40
680-144889-11
J 1 155-MW-40-102517
Water
10/25/17 10:05
10/28/17 1 0:40
680-144889-12
J 1 155-MW-41-102517
Water
10/25/17 14:05
10/28/17 10:40
680-144889-13
J 1 155-MW-42-102417
Water
10/24/17 13:05
10/28/17 10:40
680-144889-14
J 1 155-MW-43-102417
Water
10/24/17 12:30
10/28/17 10:40
680-144889-15
J 1 155-MW-45-102417
Water
10/24/17 14:32
10/28/17 10:40
680-144889-16
J I 155-MW-47-102517
Water
10/25/17 13:22
10/28/17 10:40
680-144889-17
J1 155-MW-60-102517
Water
10/25/17 11:39
10/28/17 10:40
680-144889-18
J 1 155-MW-61-102517
Water
10/25/17 10:56
10/28/17 10:40
680-144889-19
J 1 155-MW-62-102517
Water
10/25/17 12:21
10/28/17 10:40
680-144889-20
J 1 155-MW-63-102717
Water
10/27/17 09:09
10/28/17 1 0:40
680-144889-21
J1 155-PW-16-102717
Water
10/27/17 10:35
10/28/17 10:40
680-144889-22
J1 155-SP-26-102717
Water
10/27/17 11:29
10/28/17 10:40
680-144889-23
J1 155-CMP-1-102717
Water
10/27/17 09:35
10/28/17 10:40
680-144889-24
J1 155-CMP-3-102717
Water
10/27/17 11:47
10/28/17 10:40
680-144889-25
J1 155-CMP-4-102717
Water
10/27/17 09:21
10/28/17 10:40
680-144889-26
J 1 155-SW-3-102717
Water
10/27/17 09:48
10/28/17 10:40
680-144889-27
J 1 155-SW-6-102717
Water
10/27/17 11:09
10/28/17 10:40
680-144889-28
J1 155-SW-10-102717
Water
10/27/17 10:47
10/28/17 10:40
680-144889-29
J 1 155-RW-2-102617
Water
10/26/17 16:49
10/28/17 10:40
680-144889-30
J 1 155-RW-3-102617
Water
10/26/17 16:56
10/28/17 10:40
680-144889-31
A 155-RW-5-102617
Water
10/26/17 16:38
10/28/17 10:40
680-144889-32
A 155-DUP-1-102417
Water
10/24/17 16:00
10/28/17 10:40
680-144889-33
A 155-DUP-2-102417
Water
10/24/17 16:10
10/28/17 10:40
680-144889-34
J1 155-DUP-3-102517
Water
10/25/17 16:00
10/28/17 10:40
680-144889-35
J1 155-DUP-4-102517
Water
10/25/17 16:10
10/28/17 10:40
680-144889-36
J1 155-EB-01-102417
Water
10/24/17 15:32
10/28/17 10:40
680-144889-37
J1 155-EB-02-102517
Water
10/25/17 15:53
10/28/17 10:40
680-144889-38
J1 155-EB-03-102617
Water
10/26/17 16:40
10/28/17 10:40
680-144889-39
J1 155-EB-04-102717
Water
10/27/17 13:55
10/28/17 10:40
680-144889-40
J1 155-TB-102417
Water
10/24/17 08:00
10/28/17 10:40
TestArnerica Savannah
Page 5 of 142 11/10/2017

Method Summary
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL SAV
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestArnerica Savannah
Page 6 of 142 11/10/2017

Definitions/Glossary
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Qualifiers
GC/IVIS VOA
Qualifier Qualifier Description
LCS or LCSD is outside acceptance limits.
X Surrogate is outside control limits
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
rl Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestArnerica Savannah
Page 7 of 142 11/10/2017

Detection Summary
Client: GHID Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample 11): J1155-MW-10-102417
Lab Sample ID: 680-144889-1
Analyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
Chloroform 10
1.0
dg-/L
-1 8260B Total/NA
cis- 1,2-Dichloroethene 1.0
1.0
ug/L
1 8260B Tota /NA
Trichloroethene 34
1.0
ug/L
1 8260B Tota�/NA
Client Sample 11): A 155-MW-11-102417
Lab Sample 11): 680-144889-2
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis- 1,2-Dichloroethene 46
1.0
ug/L
1 8260B Tota /NA
1,1-Dichloroethane 3.2
1.0
ug/L
1 8260B Tota�/NA
1,1-Dichloroethene 7.6
1.0
ug/L
1 8260B Tota /NA
Tetrachloroethene 5.5
1.0
ug/L
I 8260B Tota�/NA
Trichloroethene 120
1.0
ug/L
I 8260B Total/NA
Client Sample ID: A 155-MW-1 3-102417
Lab Sample ID: 680-144889-3
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis- 1,2-Dichloroethene 6.5
1.0
ug/L
1 8260B Total/NA
1,1-Dichloroethane 1.8
1.0
ug/L
1 8260B Total/NA
1,1-Dichloroethene 4.2
1.0
ug/L
1 8260B Tota /NA
Tetrachloroethene 4.0
1.0
ug/L
1 8260B Tota�/NA
1, 1, 1 -Trichloroethane 9.2
1.0
ug/L
1 8260B Total/NA
Trichloroethene 120
1.0
ug/L
1 8260B Total/NA
1, 1,2-Trichloro-1,2,2-trifluoroethane 5.3
1.0
ug/L
1 8260B Total/NA
Client Sample ID: A 155-MW-1 7-102417
Lab Sample ID: 680-144889-4
1 No Detections.
Client Sample 11): A 155-MW-20-102417
Lab Sample 11): 680-144889-5
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis- 1,2-Dichloroethene 39
1.0
ug/L
1 8260B Total/NA
Trichloroethene 1.6
1.0
ug/L
1 8260B Total/NA
1,1,2-Trichloro-1,2,2-trifluoroethane 1.4
1.0
ug/L
1 8260B Total/NA
Client Sample 11): A 155-MW-28-102417
Lab Sample 11): 680-144889-6
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis- 1,2-Dich loroethene 2.5
1.0
ug/L
1 8260B Total/NA
1,1-Dichloroethane 6.9
1.0
ug/L
1 8260B Total/NA
1,1-Dichloroethene 2.2
1.0
ug/L
1 8260B Total/NA
Tetrachloroethene 6.7
1.0
ug/L
1 8260B Total/NA
1,1,1-Trichloroethane 1.1
1.0
ug/L
1 8260B Total/NA
Trichloroethene 22
1.0
ug/L
1 8260B Total/NA
1,1,2-Trichloro-1,2,2-trifluoroethane 1.0
1.0
ug/L
I 8260B Total/NA
Vinyl chloride 14
1.0
ug/L
I 8260B Total/NA
Client Sample ID: A 155-MW-33-102517
Lab Sample 11): 680-144889-7
Fnalyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
LTrichloroethene 5.7
1.0
ug/L
1 8260B Total/NA
This Detection Summary does not include radiochernical test results.
TestArnerica Savannah
Page 8 of 142 11/10/2017

Detection Summary
Client: GHID Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample 11): A 155-MW-34-102517
Lab Sample ID: 680-144889-8
1 No Detections.
Client Sample ID: A 155-MW-35-10241
Lab Sample ID: 680-144889-9
Analyte Result Qualifier
RL
MDL Unit
DilFac D Method Prep Type
cis-1,2-Dichloroethene 1.2
1.0
ug/L
1 8260B Total/NA
—Trichloroethene 15
1.0
ug/L
1 8260B Total/NA
Client Sample ID: A 155-MW-36-102517
Lab Sample ID: 680-144889-10
Analyte Result Qualifier
RL
MDL Unit
Dil Fac D Method Prep Type
Benzene 1.2
1.0
ug/L
I 8260B Total/NA
Chloroform 4.7
1.0
ug/L
I 8260B Total/NA
cis- 1,2-Dichloroethene 49
1.0
ug/L
I 8260B Total/NA
1,1-Dichloroethane 19
1.0
ug/L
I 8260B Total/NA
1,1-Dichloroethene 55
1.0
ug/L
1 8260B Total/NA
Tetrachloroethene 45
1.0
ug/L
I 8260B Total/NA
1,1,1-Trichloroethane 13
1.0
ug/L
1 8260B Total/NA
1,1,2-Trichloro-1,2,2-trifluoroethane 20
1.0
ug/L
1 8260B Total/NA
Vinyl chloride 1.2
1.0
ug/L
1 8260B Tota�/NA
Trichloroethene - DL 320
2.0
ug/L
2 8260B Tota /NA
Client Sample ID: A 155-MW-40-102517
Lab Sample ID: 680-144889-11
ENo Detections.
Client Sample 11): A 155-MW-41-102517
Lab Sample ID: 680-144889-12
Analyte Result Qualifier
RL
MDL Unit
Dil Fac D Method Prep Type
cis- 1,2-Dichloroethene 230
1,1-Dichloroethene 13
Tetrachloroethene 11
Trichloroethene 920
Vinyl chloride 56
Client Sample ID: J1155-MW-42-102417
10
10
10
10
10
ug/L
ug/L
ug/L
ug/L
ug/L
10 8260B Total/NA
10 8260B Total/NA
10 8260B Total/NA
10 8260B Total/NA
10 8260B Total/NA
Lab Sample ID: 680-144889-13
ENo Detections.
Client Sample 11): A 155-MW-43-102417
Lab Sample ID: 680-144889-14
Analyte Result Qualifier
RL
MDL Unit
DilFac D Method Prep Type
Trichloroethene 4.5
1.0
ug/L
1 8260B Total/NA
Client Sample ID: J1155-MW-45-102417
Lab Sample ID: 680-144889-15
ENo Detections.
Client Sample 11): A 155-MW-47-102517
Lab Sample ID: 680-144889-16
INo Detections
This Detection Summary does not include radiochernical test results.
TestArnerica Savannah
Page 9 of 142 11/10/2017

Detection Summary
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample 11): A 155-MW-60-102517
Lab Sample ID: 680-144889-17
nalyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
LTrichloroethene 7.3
1.0
dg-/—L
—1 — 8260B Total/NA
Client Sample 11): A 155-MW-61-102517
Lab Sample ID: 680-144889-18
Fnalyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
LTrichloroethene 15
1.0
ug/L
1 8260B Total/NA
Client Sample ID: A 155-MW-62-102517
Lab Sample ID: 680-144889-19
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis-1,2-Dichloroethene 54
1.0
1 8260B Total/NA
Trichloroethene 4.7
1.0
ug/L
1 8260B Total/NA
Client Sample ID: A 155-MW-63-102717
Lab Sample ID: 680-144889-20
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis- 1,2-Dichloroethene 12
1.0
ug/L
1 8260B Total/NA
Trichloroethene 13
1.0
ug/L
1 8260B Total/NA
Client Sample ID: A 155-PW-1 6-102717
Lab Sample ID: 680-144889-21
Analyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
Tetrahydrofuran 35
10
ug/L
I 8260B Total/NA
Client Sample 11): A 155-SP-26-102717
Lab Sample ID: 680-144889-22
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Trichloroethene 1.9
1.0
ug/L
1 8260B Total/NA
1,1,2-Trichloro-1,2,2-trifluoroethane 1.5
1.0
ug/L
1 8260B Total/NA
Client Sample 11): J1155-CMP-1-102717
Lab Sample ID: 680-144889-23
ENo Detections.
Client Sample ID: A 155-CMP-3-102717
Lab Sample ID: 680-144889-24
Analyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
1,1,1-Trichloroethane 1.1
1.0
ug/L
I 8260B Total/NA
Trichloroethene 4.3
1.0
ug/L
1 8260B Total/NA
Client Sample 11): A 155-CMP-4-102717
Lab Sample ID: 680-144889-25
Inalyte Result Qualifier
A
RL
MDL
Unit
Dil Fac D Method Prep Type
—
LTrichloroethene 2.3
1.0
ug/L
— — — —
1 8260B Total/NA
Client Sample ID: A 155-SW-3-102717
Lab Sample ID: 680-144889-26
nalyte Result Qualifier
F�
RL
MDL
Unit
DilFac D Method Prep Type
LTrichloroethene 1.9
1.0
ug/L
1 8260B Total/NA
This Detection Summary does not include radiochernical test results.
TestArnerica Savannah
Page 10 of 142 11/10/2017

Detection Summary
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Client Sample 11): A 155-SW-6-102717
INo Detections.
TestArnerica Job ID: 680-144889-1
Lab Sample ID: 680-144889-27
Client Sample ID: A 155-SW-1 0-102717
Lab Sample ID: 680-144889-28
INo Detections.
Client Sample ID: A 155-RW-2-102617
Lab Sample ID: 680-144889-29
Analyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
Trichloroethene 6.5
1.0
ug/L
1 8260B Total/NA
Vinyl chloride 1.4
1.0
ug/L
1 8260B Total/NA
Client Sample ID: A 155-RW-3-102617
Lab Sample ID: 680-144889-30
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
Chloroform 11
2.0
ug/L
2 8260B Total/NA
cis- 1,2-Dichloroethene 7.9
2.0
ug/L
2 8260B Total/NA
1,1-Dichloroethane 4.8
2.0
ug/L
2 8260B Total/NA
1,1-Dichloroethene 44
2.0
ug/L
2 8260B Total/NA
Tetrachloroethene 39
2.0
ug/L
2 8260B Tota�/NA
1,1,1-Trichloroethane 59
2.0
ug/L
2 8260B Tota /NA
Trichloroethene 270
2.0
ug/L
2 8260B Total/NA
1, 1,2-Trichloro-1,2,2-trifluoroethane 91
2.0
ug/L
2 8260B Total/NA
Client Sample ID: A 155-RW-5-102617
Lab Sample ID: 680-144889-31
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis- 1,2-Dichloroethene 160
10
ug/L
10 8260B Total/NA
1,1-Dichloroethane 180
10
ug/L
10 8260B Total/NA
1,1-Dichloroethene 64
10
ug/L
10 8260B Total/NA
Tetrachloroethene 74
10
ug/L
10 8260B Total/NA
1,1,1-Trichloroethane 110
10
ug/L
10 8260B Total/NA
Trichloroethene - DL 1400
20
ug/L
20 8260B Total/NA
Client Sample 11): A 155-DUP-1-1 02417
Lab Sample ID: 680-144889-32
Analyte Result Qualifier
RL
MDL
Unit
Dil Fac D Method Prep Type
cis- 1,2-Dichloroethene 39
1.0
ug/L
1 8260B Total/NA
Trichloroethene 1.9
1.0
ug/L
1 8260B Total/NA
1,1,2-Trichloro-1,2,2-trifluoroethane 1.7
1.0
ug/L
1 8260B Total/NA
Client Sample ID: J1155-DUP-2-102417
Lab Sample ID: 680-144889-33
Analyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
cis- 1,2-Dichloroethene 1.0
1.0
ug/L
I 8260B Total/NA
Trichloroethene 15
1.0
ug/L
1 8260B Total/NA
Client Sample 11): A 155-DUP-3-102517
Lab Sample ID: 680-144889-34
nalyte Result Qualifier
RL
MDL
Unit
DilFac D Method Prep Type
LTrichloroethene 5.7
1.0
ug/[--
-1 8260B Total/NA
This Detection Summary does not include radiochemical test results.
TestArnerica Savannah
Page 11 of 142 11/10/2017

Detection Summary
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
F
TestArnerica Job ID: 680-144889-1
Client Sample 11): A 155-DUP-4-102517
Lab Sample ID: 680-144889-35
Analyte Result Qualifier
RL
MDL Unit
Dil Fac D Method Prep Type
-
Benzene 5.2
1.0
ug-/L
-
1 8260B Total/NA
Chloroform 23
1.0
ug/L
1 8260B Tota�/NA
cis- 1,2-Dichloroethene 6.6
1.0
ug/L
1 8260B Tota /NA
1,1-Dichloroethane 47
1.0
ug/L
1 8260B Total/NA
1,1-Dichloroethene 8.8
1.0
ug/L
1 8260B Total/NA
Ethylbenzene 2.6
1.0
ug/L
1 8260B Tota�/NA
Tetrachloroethene 45
1.0
ug/L
1 8260B Tota /NA
Toluene 110
1.0
ug/L
1 8260B Tota /NA
Trichloroethene 91
1.0
ug/L
1 8260B Tota�/NA
Vinyl chloride 13
1.0
ug/L
I 8260B Tota�/NA
Xylenes, Total 9.4
1.0
ug/L
I 8260B Tota /NA
Client Sample 11): A 155-EB-01 -102417
Lab Sample ID: 680-144889-36
- No Detections.
Client Sample 11): A 155-EB-02-102517
Lab Sample ID: 680-144889-37
1 No Detections.
Client Sample ID: J1155-EB-03-102617
Lab Sample ID: 680-144889-38
ENo Detections.
Client Sample 11): A 155-EB-04-102717
Lab Sample ID: 680-144889-39
ENo Detections.
Client Sample 11): A 155-TB-1 02417
Lab Sample ID: 680-144889-40
ENo Detections
This Detection Summary does not include radiochernical test results.
TestArnerica Savannah
Page 12 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-10-102417
Lab Sample ID: 680-144889-1
Date Collected: 10/24/17 08:53
Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/03/17 19:31
1
Benzene
ND
1.0
ug/L
11/03/17 19:31
1
Bromodichloromethane
ND
1.0
ug/L
11/03/17 19:31
1
Brornoform
ND
1.0
ug/L
11/03/17 19:31
1
Brornornethane
ND
5.0
ug/L
11/03/17 19:31
1
2-Butanone
ND
10
ug/L
11/03/17 19:31
1
Carbon disulfide
ND
2.0
ug/L
11/03/17 19:31
1
Carbon tetrachloride
ND
1.0
ug/L
11/03/17 19:31
1
Chlorobenzene
ND
1.0
ug/L
11/03/17 19:31
1
Chloroethane
ND
5.0
ug/L
11/03/17 19:31
1
Chloroform
10
1.0
ug/L
11/03/17 19:31
1
Chloromethane
ND
1.0
ug/L
11/03/17 19:31
1
cis-1,2-Dichloroethene
1.0
1.0
ug/L
11/03/17 19:31
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/03/17 19:31
1
Cyclohexane
ND
1.0
ug/L
11/03/17 19:31
1
Dibromochloromethane
ND
1.0
ug/L
11/03/17 19:31
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/03/17 19:31
1
1,2-Dibromoethane
ND
1.0
ug/L
11/03/17 19:31
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/03/17 19:31
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/03/17 19:31
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/03/17 19:31
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/03/17 19:31
1
1,1-Dichloroethane
ND
1.0
ug/L
11/03/17 19:31
1
1,2-Dichloroethane
ND
1.0
ug/L
11/03/17 19:31
1
1,1-Dichloroethene
ND
1.0
ug/L
11/03/17 19:31
1
1,2-Dichloropropane
ND
1.0
ug/L
11/03/17 19:31
1
Ethylbenzene
ND
1.0
ug/L
11/03/17 19:31
1
2-Hexanone
ND
10
ug/L
11/03/17 19:31
1
1 sopropyl benzene
ND
1.0
ug/L
11/03/17 19:31
1
Methyl acetate
ND
5.0
ug/L
11/03/17 19:31
1
Methylcyclohexane
ND
1.0
ug/L
11/03/17 19:31
1
Methylene Chloride
ND
5.0
ug/L
11/03/17 19:31
1
4-Methyl-2-pentanone
ND
10
ug/L
11/03/17 19:31
1
Methyl tert-butyl ether
ND
10
ug/L
11/03/17 19:31
1
Styrene
ND
1.0
ug/L
11/03/17 19:31
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/03/17 19:31
1
Tetrachloroethene
ND
1.0
ug/L
11/03/17 19:31
1
Tetrahydrofuran
ND
10
ug/L
11/03/17 19:31
1
Toluene
ND
1.0
ug/L
11/03/17 19:31
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/03/17 19:31
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/03/17 19:31
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/03/17 19:31
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/03/17 19:31
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/03/17 19:31
1
Trichloroethene
34
1.0
ug/L
11/03/17 19:31
1
Trichlorofluoromethane
ND
1.0
ug/L
11/03/17 19:31
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/03/17 19:31
1
Vinyl chloride
ND
1.0
ug/L
11/03/17 19:31
1
Xylenes, Total
ND
1.0
ug/L
11/03/17 19:31
1
a
F
TestArnerica Savannah
Page 13 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-10-102417 Lab Sample ID: 680-144889-1
Date Collected: 10/24/17 08:53 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 89 80-120 11103117 19:31 ,
Dibromofluoromethane (Surr) 96 80-122 11103117 19:31 1
1,2-Dichloroethane-d4 (Surr) 96 73-131 11103117 19:31 1
Toluene-d8 (Surr) 104 80-120 11103117 19:31 1
a
F
TestArnerica Savannah
Page 14 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-11-102417 Lab Sample ID: 680-144889-2
Date Collected: 10/24/17 09:33 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/03/17 19:55
1
Benzene
ND
1.0
ug/L
11/03/17 19:55
1
Bromodichloromethane
ND
1.0
ug/L
11/03/17 19:55
1
Bromoform
ND
1.0
ug/L
11/03/17 19:55
1
Bromomethane
ND
5.0
ug/L
11/03/17 19:55
1
2-Butanone
ND
10
ug/L
11/03/17 19:55
1
Carbon disulfide
ND
2.0
ug/L
11/03/17 19:55
1
Carbon tetrachloride
ND
1.0
ug/L
11/03/17 19:55
1
Chlorobenzene
ND
1.0
ug/L
11/03/17 19:55
1
Chloroethane
ND
5.0
ug/L
11/03/17 19:55
1
Chloroform
ND
1.0
ug/L
11/03/17 19:55
1
Chloromethane
ND
1.0
ug/L
11/03/17 19:55
1
cis-1,2-Dichloroethene
46
1.0
ug/L
11/03/17 19:55
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/03/17 19:55
1
Cyclohexane
ND
1.0
ug/L
11/03/17 19:55
1
Dibromochloromethane
ND
1.0
ug/L
11/03/17 19:55
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/03/17 19:55
1
1,2-Dibromoethane
ND
1.0
ug/L
11/03/17 19:55
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/03/17 19:55
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/03/17 19:55
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/03/17 19:55
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/03/17 19:55
1
11,11-Dichloroethane
3.2
1.0
ug/L
11/03/17 19:55
1
1,2-Dichloroethane
ND
1.0
ug/L
11/03/17 19:55
1
1,1-Dichloroethene
7.6
1.0
ug/L
11/03/17 19:55
1
1,2-Dichloropropane
ND
1.0
ug/L
11/03/17 19:55
1
Ethylbenzene
ND
1.0
ug/L
11/03/17 19:55
1
2-Hexanone
ND
10
ug/L
11/03/17 19:55
1
1 sopropyl benzene
ND
1.0
ug/L
11/03/17 19:55
1
Methyl acetate
ND
5.0
ug/L
11/03/17 19:55
1
Methylcyclohexane
ND
1.0
ug/L
11/03/17 19:55
1
Methylene Chloride
ND
5.0
ug/L
11/03/17 19:55
1
4-Methyl-2-pentanone
ND
10
ug/L
11/03/17 19:55
1
Methyl tert-butyl ether
ND
10
ug/L
11/03/17 19:55
1
Styrene
ND
1.0
ug/L
11/03/17 19:55
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/03/17 19:55
1
Tetrachloroethene
5.5
1.0
ug/L
11/03/17 19:55
1
Tetrahydrofuran
ND
10
ug/L
11/03/17 19:55
1
Toluene
ND
1.0
ug/L
11/03/17 19:55
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/03/17 19:55
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/03/17 19:55
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/03/17 19:55
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/03/17 19:55
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/03/17 19:55
1
Trichloroethene
120
1.0
ug/L
11/03/17 19:55
1
Trichlorofluoromethane
ND
1.0
ug/L
11/03/17 19:55
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/03/17 19:55
1
Vinyl chloride
ND
1.0
ug/L
11/03/17 19:55
1
Xylenes, Total
ND
1.0
ug/L
11/03/17 19:55
1
a
F
TestArnerica Savannah
Page 15 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-11-102417 Lab Sample ID: 680-144889-2
Date Collected: 10/24/17 09:33 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 89 80-120 11103117 19:55 ,
Dibromofluoromethane (Surr) 96 80-122 11103117 19:55 1
1,2-Dichloroethane-d4 (Surr) 94 73-131 11103117 19:55 1
Toluene-d8 (Surr) 102 80-120 11103117 19:55 1
a
F
TestArnerica Savannah
Page 16 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: A 155-MW-1 3-102417 Lab Sample ID: 680-144889-3
Date Collected: 10/24/17 10:39 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
cis-1,2-Dichloroethene
6.5
cis- 1,3-Dichloropropene
ND
Cyclohexane
ND
Dibromochloromethane
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
11,11-Dichloroethane
1.8
1,2-Dichloroethane
ND
1,1-Dichloroethene
4.2
1,2-Dichloropropane
ND
Ethylbenzene
ND
2-Hexanone
ND
I sopropyl benzene
ND
Methyl acetate
ND
Methylcyclohexane
ND
Methylene Chloride
ND
4-Methyl-2-pentanone
ND
Methyl tert-butyl ether
ND
Styrene
ND
1,1,2,2-Tetrachloroethane
ND
Tetrachloroethene
4.0
Tetrahydrofuran
ND
Toluene
ND
trans- 1,2-Dich loroethene
ND
trans- 1, 3-Dich loropropene
ND
1,2,4-Trichlorobenzene
ND
1,1,1-Trichloroethane
9.2
1,1,2-Trichloroethane
ND
Trichloroethene
120
Trichlorofluoromethane
ND
1 1 2-Trichloro-1 2 2-trifluoroetha
5.3
I I I I
ne
Vinyl chloride ND
RL
MDL Unit
D Prepared Analyzed
Dil Fac
10
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
5.0
ug/L
11/07/17 18:03
1
10
ug/L
11/07/17 18:03
1
2.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
5.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
5.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
10
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
5.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
5.0
ug/L
11/07/17 18:03
1
10
ug/L
11/07/17 18:03
1
10
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
10
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
5.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
1.0
ug/L
11/07/17 18:03
1
a
F
TestArnerica Savannah
Page 17 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: A 155-MW-1 3-102417
Lab Sample ID: 680-144889-3
Date Collected: 10/24/17 10:39
Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Xylenes, Total ND
1.0 ug/L
11/07/17 18:03 --1
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
4-Bromofluorobenzene FSu-rr) 87
80-120
111071171 1
Dibromofluoromethane (Surr) 91
80-122
11107117 18:03 1
1,2-Dichloroethane-d4 (Surr) 91
73-131
11107117 18:03
Toluene-d8 (Surr) 101
80-120
11107117 18:03 1
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TestArnerica Savannah
Page 18 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: A 155-MW-1 7-102417
Lab Sample ID: 680-144889-4
Date Collected: 10/24/17 13:53
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/03/17 20:20
1
Benzene
ND
1.0
ug/L
11/03/17 20:20
1
Bromodichloromethane
ND
1.0
ug/L
11/03/17 20:20
1
Bromoform
ND
1.0
ug/L
11/03/17 20:20
1
Bromomethane
ND
5.0
ug/L
11/03/17 20:20
1
2-Butanone
ND
10
ug/L
11/03/17 20:20
1
Carbon disulfide
ND
2.0
ug/L
11/03/17 20:20
1
Carbon tetrachloride
ND
1.0
ug/L
11/03/17 20:20
1
Chlorobenzene
ND
1.0
ug/L
11/03/17 20:20
1
Chloroethane
ND
5.0
ug/L
11/03/17 20:20
1
Chloroform
ND
1.0
ug/L
11/03/17 20:20
1
Chloromethane
ND
1.0
ug/L
11/03/17 20:20
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/03/17 20:20
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/03/17 20:20
1
Cyclohexane
ND
1.0
ug/L
11/03/17 20:20
1
Dibromochloromethane
ND
1.0
ug/L
11/03/17 20:20
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/03/17 20:20
1
1,2-Dibromoethane
ND
1.0
ug/L
11/03/17 20:20
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/03/17 20:20
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/03/17 20:20
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/03/17 20:20
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/03/17 20:20
1
1,1-Dichloroethane
ND
1.0
ug/L
11/03/17 20:20
1
1,2-Dichloroethane
ND
1.0
ug/L
11/03/17 20:20
1
1,1-Dichloroethene
ND
1.0
ug/L
11/03/17 20:20
1
1,2-Dichloropropane
ND
1.0
ug/L
11/03/17 20:20
1
Ethylbenzene
ND
1.0
ug/L
11/03/17 20:20
1
2-Hexanone
ND
10
ug/L
11/03/17 20:20
1
1 sopropyl benzene
ND
1.0
ug/L
11/03/17 20:20
1
Methyl acetate
ND
5.0
ug/L
11/03/17 20:20
1
Methylcyclohexane
ND
1.0
ug/L
11/03/17 20:20
1
Methylene Chloride
ND
5.0
ug/L
11/03/17 20:20
1
4-Methyl-2-pentanone
ND
10
ug/L
11/03/17 20:20
1
Methyl tert-butyl ether
ND
10
ug/L
11/03/17 20:20
1
Styrene
ND
1.0
ug/L
11/03/17 20:20
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/03/17 20:20
1
Tetrachloroethene
ND
1.0
ug/L
11/03/17 20:20
1
Tetrahydrofuran
ND
10
ug/L
11/03/17 20:20
1
Toluene
ND
1.0
ug/L
11/03/17 20:20
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/03/17 20:20
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/03/17 20:20
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/03/17 20:20
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/03/17 20:20
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/03/17 20:20
1
Trichloroethene
ND
1.0
ug/L
11/03/17 20:20
1
Trichlorofluoromethane
ND
1.0
ug/L
11/03/17 20:20
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/03/17 20:20
1
Vinyl chloride
ND
1.0
ug/L
11/03/17 20:20
1
Xylenes, Total
ND
1.0
ug/L
11/03/17 20:20
1
a
F
TestArnerica Savannah
Page 19 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: A 155-MW-1 7-102417 Lab Sample ID: 680-144889-4
Date Collected: 10/24/17 13:53 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 91 80-120 11103117 20:20 ,
Dibromofluoromethane (Surr) 94 80-122 11103117 20:20 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11103117 20:20 1
Toluene-d8 (Surr) 102 80-120 11103117 20:20 1
a
F
TestArnerica Savannah
Page 20 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-20-102417 Lab Sample ID: 680-144889-5
Date Collected: 10/24/17 10:07 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
cis-1,2-Dichloroethene
39
cis- 1,3-Dichloropropene
ND
Cyclohexane
ND
Dibromochloromethane
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
1,1-Dichloroethene
ND
1,2-Dichloropropane
ND
Ethylbenzene
ND
2-Hexanone
ND
I sopropyl benzene
ND
Methyl acetate
ND
Methylcyclohexane
ND
Methylene Chloride
ND
4-Methyl-2-pentanone
ND
Methyl tert-butyl ether
ND
Styrene
ND
1,1,2,2-Tetrachloroethane
ND
Tetrachloroethene
ND
Tetrahydrofuran
ND
Toluene
ND
trans- 1,2-Dich loroethene
ND
trans- 1, 3-Dich loropropene
ND
1,2,4-Trichlorobenzene
ND
1,1,1-Trichloroethane
ND
1,1,2-Trichloroethane
ND
Trichloroethene
1.6
Trichlorofluoromethane
ND
1 1 2-Trichloro-1 2 2-trifluoroetha
1.4
I I I I
ne
Vinyl chloride ND
RL
MDL Unit
D Prepared Analyzed
Dil Fac
10
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
5.0
ug/L
11/05/17 15:08
1
10
ug/L
11/05/17 15:08
1
2.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
5.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
5.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
10
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
5.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
5.0
ug/L
11/05/17 15:08
1
10
ug/L
11/05/17 15:08
1
10
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
10
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
5.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
1.0
ug/L
11/05/17 15:08
1
a
F
TestArnerica Savannah
Page 21 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-20-102417
Lab Sample ID: 680-144889-5
Date Collected: 10/24/17 10:07
Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Xylenes, Total ND
1.0 ug/L
11/05/17 15:06 --1
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
4-Bromofluorobenzene FSu-rr) 104
80-120
111051171 1
Dibromofluoromethane (Surr) 112
80-122
11105117 15:08 1
1,2-Dichloroethane-d4 (Surr) 112
73-131
11105117 15:08
Toluene-d8 (Surr) 111
80-120
11105117 15:08 1
F
TestArnerica Savannah
Page 22 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-28-102417 Lab Sample ID: 680-144889-6
Date Collected: 10/24/17 15:09 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
cis-1,2-Dichloroethene
2.5
cis- 1,3-Dichloropropene
ND
Cyclohexane
ND
Dibromochloromethane
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
11,11-Dichloroethane
6.9
1,2-Dichloroethane
ND
1,1-Dichloroethene
2.2
1,2-Dichloropropane
ND
Ethylbenzene
ND
2-Hexanone
ND
I sopropyl benzene
ND
Methyl acetate
ND
Methylcyclohexane
ND
Methylene Chloride
ND
4-Methyl-2-pentanone
ND
Methyl tert-butyl ether
ND
Styrene
ND
1,1,2,2-Tetrachloroethane
ND
Tetrachloroethene
6.7
Tetrahydrofuran
ND
Toluene
ND
trans- 1,2-Dich loroethene
ND
trans- 1, 3-Dich loropropene
ND
1,2,4-Trichlorobenzene
ND
11,11,11-Trichloroethane
1.1
1,1,2-Trichloroethane
ND
Trichloroethene
22
Trichlorofluoromethane
ND
1 1 2-Trichloro-1 2 2-trifluoroetha
1.0
I I I I
ne
Vinyl chloride 14
RL
MDL Unit
D Prepared Analyzed
Dil Fac
10
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
5.0
ug/L
11/05/17 14:46
1
10
ug/L
11/05/17 14:46
1
2.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
5.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
5.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
10
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
5.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
5.0
ug/L
11/05/17 14:46
1
10
ug/L
11/05/17 14:46
1
10
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
10
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
5.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
1.0
ug/L
11/05/17 14:46
1
a
F
TestArnerica Savannah
Page 23 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-28-102417
Lab Sample ID: 680-144889-6
Date Collected: 10/24/17 15:09
Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Xylenes, Total ND
1.0 ug/L
11/05/17 14:46 --1
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
4-Bromofluorobenzene FSu-rr) 108
80-120
111051171 1
Dibromofluoromethane (Surr) 115
80-122
11105117 14:46 1
1,2-Dichloroethane-d4 (Surr) 116
73-131
11105117 14:46
Toluene-d8 (Surr) 111
80-120
11105117 14:46 1
F
TestArnerica Savannah
Page 24 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-33-102517 Lab Sample ID: 680-144889-7
Date Collected: 10/25/17 09:19 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 15:22
1
Benzene
ND
1.0
ug/L
11/04/17 15:22
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 15:22
1
Bromoform
ND
1.0
ug/L
11/04/17 15:22
1
Bromomethane
ND
5.0
ug/L
11/04/17 15:22
1
2-Butanone
ND
10
ug/L
11/04/17 15:22
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 15:22
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 15:22
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 15:22
1
Chloroethane
ND
5.0
ug/L
11/04/17 15:22
1
Chloroform
ND
1.0
ug/L
11/04/17 15:22
1
Chloromethane
ND
1.0
ug/L
11/04/17 15:22
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 15:22
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 15:22
1
Cyclohexane
ND
1.0
ug/L
11/04/17 15:22
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 15:22
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 15:22
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 15:22
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 15:22
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 15:22
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 15:22
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 15:22
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 15:22
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 15:22
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 15:22
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 15:22
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 15:22
1
2-Hexanone
ND *
10
ug/L
11/04/17 15:22
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 15:22
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 15:22
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 15:22
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 15:22
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 15:22
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 15:22
1
Styrene
ND
1.0
ug/L
11/04/17 15:22
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 15:22
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 15:22
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 15:22
1
Toluene
ND
1.0
ug/L
11/04/17 15:22
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 15:22
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 15:22
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 15:22
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 15:22
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 15:22
1
Trichloroethene
5.7
1.0
ug/L
11/04/17 15:22
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 15:22
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 15:22
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 15:22
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 15:22
1
a
F
TestArnerica Savannah
Page 25 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-33-102517 Lab Sample ID: 680-144889-7
Date Collected: 10/25/17 09:19 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 105 80-120 11104117 15:22 ,
Dibromofluoromethane (Surr) 104 80-122 11104117 15:22 1
1,2-Dichloroethane-d4 (Surr) 102 73-131 11104117 15:22 1
Toluene-d8 (Surr) 101 80-120 11104117 15:22 1
a
F
TestArnerica Savannah
Page 26 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-34-102517
Lab Sample ID: 680-144889-8
Date Collected: 10/25/17 14:41
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 15:47
1
Benzene
ND
1.0
ug/L
11/04/17 15:47
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 15:47
1
Bromoform
ND
1.0
ug/L
11/04/17 15:47
1
Bromomethane
ND
5.0
ug/L
11/04/17 15:47
1
2-Butanone
ND
10
ug/L
11/04/17 15:47
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 15:47
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 15:47
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 15:47
1
Chloroethane
ND
5.0
ug/L
11/04/17 15:47
1
Chloroform
ND
1.0
ug/L
11/04/17 15:47
1
Chloromethane
ND
1.0
ug/L
11/04/17 15:47
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 15:47
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 15:47
1
Cyclohexane
ND
1.0
ug/L
11/04/17 15:47
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 15:47
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 15:47
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 15:47
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 15:47
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 15:47
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 15:47
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 15:47
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 15:47
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 15:47
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 15:47
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 15:47
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 15:47
1
2-Hexanone
ND *
10
ug/L
11/04/17 15:47
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 15:47
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 15:47
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 15:47
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 15:47
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 15:47
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 15:47
1
Styrene
ND
1.0
ug/L
11/04/17 15:47
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 15:47
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 15:47
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 15:47
1
Toluene
ND
1.0
ug/L
11/04/17 15:47
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 15:47
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 15:47
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 15:47
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 15:47
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 15:47
1
Trichloroethene
ND
1.0
ug/L
11/04/17 15:47
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 15:47
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 15:47
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 15:47
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 15:47
1
a
F
TestArnerica Savannah
Page 27 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-34-102517 Lab Sample ID: 680-144889-8
Date Collected: 10/25/17 14:41 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 103 80-120 11104117 15:47 ,
Dibromofluoromethane (Surr) 103 80-122 11104117 15:47 1
1,2-Dichloroethane-d4 (Surr) 96 73-131 11104117 15:47 1
Toluene-d8 (Surr) 102 80-120 11104117 15:47 1
a
F
TestArnerica Savannah
Page 28 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-35-102417 Lab Sample ID: 680-144889-9
Date Collected: 10/24/17 11:39 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 15:30
1
Benzene
ND
1.0
ug/L
11/05/17 15:30
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 15:30
1
Bromoform
ND
1.0
ug/L
11/05/17 15:30
1
Bromomethane
ND
5.0
ug/L
11/05/17 15:30
1
2-Butanone
ND
10
ug/L
11/05/17 15:30
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 15:30
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 15:30
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 15:30
1
Chloroethane
ND
5.0
ug/L
11/05/17 15:30
1
Chloroform
ND
1.0
ug/L
11/05/17 15:30
1
Chloromethane
ND
1.0
ug/L
11/05/17 15:30
1
cis-1,2-Dichloroethene
1.2
1.0
ug/L
11/05/17 15:30
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 15:30
1
Cyclohexane
ND
1.0
ug/L
11/05/17 15:30
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 15:30
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 15:30
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 15:30
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 15:30
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 15:30
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 15:30
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 15:30
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 15:30
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 15:30
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 15:30
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 15:30
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 15:30
1
2-Hexanone
ND
10
ug/L
11/05/17 15:30
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 15:30
1
Methyl acetate
ND
5.0
ug/L
11/05/17 15:30
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 15:30
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 15:30
1
4-Methyl-2-pentanone
ND
10
ug/L
11/05/17 15:30
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 15:30
1
Styrene
ND
1.0
ug/L
11/05/17 15:30
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 15:30
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 15:30
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 15:30
1
Toluene
ND
1.0
ug/L
11/05/17 15:30
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 15:30
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 15:30
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 15:30
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 15:30
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 15:30
1
Trichloroethene
15
1.0
ug/L
11/05/17 15:30
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 15:30
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 15:30
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 15:30
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 15:30
1
a
F
TestArnerica Savannah
Page 29 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-35-102417 Lab Sample ID: 680-144889-9
Date Collected: 10/24/17 11:39 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 101 80-120 11105117 15:30 ,
Dibromofluoromethane (Surr) 122 80-122 11105117 15:30 1
1,2-Dichloroethane-d4 (Surr) 119 73-131 11105117 15:30 1
Toluene-d8 (Surr) 115 80-120 11105117 15:30 1
a
F
TestArnerica Savannah
Page 30 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-36-102517 Lab Sample ID: 680-144889-10
Date Collected: 10/25/17 08:28 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
1.2
Bromodichloromethane
ND
Brornoform
ND
Brornornethane
ND
2-Butanone
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
4.7
Chloromethane
ND
cis-1,2-Dichloroethene
49
cis- 1,3-Dichloropropene
ND
Cyclohexane
ND
Dibromochloromethane
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
19
1,2-Dichloroethane
ND
11,11-Dichloroethene
55
1,2-Dichloropropane
ND
Ethylbenzene
ND
2-Hexanone
ND
I sopropyl benzene
ND
Methyl acetate
ND
Methylcyclohexane
ND
Methylene Chloride
ND
4-Methyl-2-pentanone
ND
Methyl tert-butyl ether
ND
Styrene
ND
1,1,2,2-Tetrachloroethane
ND
Tetrachloroethene
45
Tetrahydrofuran
ND
Toluene
ND
trans- 1,2-Dich loroethene
ND
trans- 1, 3-Dich loropropene
ND
1,2,4-Trichlorobenzene
ND
11,11,11-Trichloroethane
13
1,1,2-Trichloroethane
ND
Trichlorofluoromethane
ND
1,1,2-Trichloro-1,2,2-trifluoroetha
20
ne
Vinyl chloride
1.2
Xylenes, Total
ND
RL
MDL Unit
D Prepared Analyzed
Dil Fac
10
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
5.0
ug/L
11/04/17 16:11
1
10
ug/L
11/04/17 16:11
1
2.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
5.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
5.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
10
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
5.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
5.0
ug/L
11/04/17 16:11
1
10
ug/L
11/04/17 16:11
1
10
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
10
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
5.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
1.0
ug/L
11/04/17 16:11
1
a
F
TestArnerica Savannah
Page 31 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
F
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-36-102517 Lab Sample ID: 680-144889-10
Date Collected: 10/25/17 08:28 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
115
80-120
Dibromofluoromethane (Surr)
106
80-122
1,2-Dichloroethane-d4 (Surr)
100
73-131
Toluene-d8 (Surr)
105
80-120
Method: 8260B - Volatile Organic
Compounds (GC/MS) - DIL
Analyte
Result Qualifier
RL
Trichloroethene
320
2.0
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
116
80-120
Dibromofluoromethane (Surr)
109
80-122
1,2-Dichloroethane-d4 (Surr)
105
73-131
Toluene-d8 (Surr)
108
80-120
Prepared Analyzed
DY Fac
L
11104117 16:11
,
11104117 16:11
1
11104117 16:11
1
11104117 16:11
1
MDL Unit D Prepared
ug/L
Prepared
Analyzed
Dil Fac
a
11/06/17 13:58
-
2
Analyzed
Dil Fac
11106117 13:58
2
11106117 13:58
2
11106117 13:58
2
11106117 13:58
2
TestArnerica Savannah
Page 32 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-40-102517
Lab Sample ID: 680-144889-11
Date Collected: 10/25/17 10:05
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 16:36
1
Benzene
ND
1.0
ug/L
11/04/17 16:36
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 16:36
1
Bromoform
ND
1.0
ug/L
11/04/17 16:36
1
Bromomethane
ND
5.0
ug/L
11/04/17 16:36
1
2-Butanone
ND
10
ug/L
11/04/17 16:36
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 16:36
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 16:36
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 16:36
1
Chloroethane
ND
5.0
ug/L
11/04/17 16:36
1
Chloroform
ND
1.0
ug/L
11/04/17 16:36
1
Chloromethane
ND
1.0
ug/L
11/04/17 16:36
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 16:36
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 16:36
1
Cyclohexane
ND
1.0
ug/L
11/04/17 16:36
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 16:36
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 16:36
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 16:36
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 16:36
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 16:36
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 16:36
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 16:36
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 16:36
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 16:36
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 16:36
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 16:36
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 16:36
1
2-Hexanone
ND *
10
ug/L
11/04/17 16:36
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 16:36
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 16:36
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 16:36
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 16:36
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 16:36
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 16:36
1
Styrene
ND
1.0
ug/L
11/04/17 16:36
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 16:36
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 16:36
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 16:36
1
Toluene
ND
1.0
ug/L
11/04/17 16:36
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 16:36
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 16:36
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 16:36
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 16:36
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 16:36
1
Trichloroethene
ND
1.0
ug/L
11/06/17 14:20
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 16:36
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 16:36
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 16:36
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 16:36
1
a
F
TestArnerica Savannah
Page 33 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: A 155-MW-40-102517
Lab Sample ID: 680-144889-11
Date Collected: 10/25/17 10:05
Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 113
80-120
11104117 16:36 1
4-Bromofluorobenzene (Surr) 107
80-120
11106117 14:20 1
Dibromofluoromethane (Surr) 106
80-122
11104117 16:36 1
Dibromofluoromethane (Surr) 111
80-122
11106117 14:20 1
1,2-Dichloroethane-d4 (Surr) 101
73-131
11104117 16:36 1
1,2-Dichloroethane-d4 (Surr) 110
73-131
11106117 14:20 1
Toluene-d8 (Surr) 113
80-120
11104117 16:36 1
—Toluene-d8 (Surr) 112
80-120
11106117 14:20 1
a
F
TestArnerica Savannah
Page 34 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-41-102517 Lab Sample ID: 680-144889-12
Date Collected: 10/25/17 14:05 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
100
ug/L
11/08/17 18:40
10
Benzene
ND
10
ug/L
11/08/17 18:40
10
Bromodichloromethane
ND
10
ug/L
11/08/17 18:40
10
Bromoform
ND
10
ug/L
11/08/17 18:40
10
Bromomethane
ND
50
ug/L
11/08/17 18:40
10
2-Butanone
ND
100
ug/L
11/08/17 18:40
10
Carbon disulfide
ND
20
ug/L
11/08/17 18:40
10
Carbon tetrachloride
ND
10
ug/L
11/08/17 18:40
10
Chlorobenzene
ND
10
ug/L
11/08/17 18:40
10
Chloroethane
ND
50
ug/L
11/08/17 18:40
10
Chloroform
ND
10
ug/L
11/08/17 18:40
10
Chloromethane
ND
10
ug/L
11/08/17 18:40
10
cis-1,2-Dichloroethene
230
10
ug/L
11/08/17 18:40
10
cis- 1,3-Dichloropropene
ND
10
ug/L
11/08/17 18:40
10
Cyclohexane
ND
10
ug/L
11/08/17 18:40
10
Dibromochloromethane
ND
10
ug/L
11/08/17 18:40
10
1,2-Dibromo-3-Chloropropane
ND
50
ug/L
11/08/17 18:40
10
1,2-Dibromoethane
ND
10
ug/L
11/08/17 18:40
10
1,2-Dichlorobenzene
ND
10
ug/L
11/08/17 18:40
10
1,3-Dichlorobenzene
ND
10
ug/L
11/08/17 18:40
10
1,4-Dichlorobenzene
ND
10
ug/L
11/08/17 18:40
10
Dichlorodifluoromethane
ND
10
ug/L
11/08/17 18:40
10
1,1-Dichloroethane
ND
10
ug/L
11/08/17 18:40
10
1,2-Dichloroethane
ND
10
ug/L
11/08/17 18:40
10
1,1-Dichloroethene
13
10
ug/L
11/08/17 18:40
10
1,2-Dichloropropane
ND
10
ug/L
11/08/17 18:40
10
Ethylbenzene
ND
10
ug/L
11/08/17 18:40
10
2-Hexanone
ND
100
ug/L
11/08/17 18:40
10
I sopropyl benzene
ND
10
ug/L
11/08/17 18:40
10
Methyl acetate
ND
50
ug/L
11/08/17 18:40
10
Methylcyclohexane
ND
10
ug/L
11/08/17 18:40
10
Methylene Chloride
ND
50
ug/L
11/08/17 18:40
10
4-Methyl-2-pentanone
ND
100
ug/L
11/08/17 18:40
10
Methyl tert-butyl ether
ND
100
ug/L
11/08/17 18:40
10
Styrene
ND
10
ug/L
11/08/17 18:40
10
1,1,2,2-Tetrachloroethane
ND
10
ug/L
11/08/17 18:40
10
Tetrachloroethene
11
10
ug/L
11/08/17 18:40
10
Tetrahydrofuran
ND
100
ug/L
11/08/17 18:40
10
Toluene
ND
10
ug/L
11/08/17 18:40
10
trans- 1,2-Dich loroethene
ND
10
ug/L
11/08/17 18:40
10
trans- 1, 3-Dich loropropene
ND
10
ug/L
11/08/17 18:40
10
1,2,4-Trichlorobenzene
ND
50
ug/L
11/08/17 18:40
10
1,1,1-Trichloroethane
ND
10
ug/L
11/08/17 18:40
10
1,1,2-Trichloroethane
ND
10
ug/L
11/08/17 18:40
10
Trichloroethene
920
10
ug/L
11/08/17 18:40
10
Trichlorofluoromethane
ND
10
ug/L
11/08/17 18:40
10
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
10
ug/L
11/08/17 18:40
10
Vinyl chloride
56
10
ug/L
11/08/17 18:40
10
Xylenes, Total
ND
10
ug/L
11/08/17 18:40
10
a
TestArnerica Savannah
Page 35 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-41-102517
Lab Sample ID: 680-144889-12
Date Collected: 10/25/17 14:05
Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
4-Bromofluorobenzene (Surr) 89
80-120
11108117 18:40 io
Dibromofluoromethane (Surr) 101
80-122
11108117 18:40 10
1,2-Dichloroethane-d4 (Surr) 110
73-131
11108117 18:40 10
Toluene-d8 (Surr) 91
80-120
11108117 18:40 10
a
F
TestArnerica Savannah
Page 36 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-42-102417
Lab Sample ID: 680-144889-13
Date Collected: 10/24/17 13:05
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 15:52
1
Benzene
ND
1.0
ug/L
11/05/17 15:52
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 15:52
1
Bromoform
ND
1.0
ug/L
11/05/17 15:52
1
Bromomethane
ND
5.0
ug/L
11/05/17 15:52
1
2-Butanone
ND
10
ug/L
11/05/17 15:52
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 15:52
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 15:52
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 15:52
1
Chloroethane
ND
5.0
ug/L
11/05/17 15:52
1
Chloroform
ND
1.0
ug/L
11/05/17 15:52
1
Chloromethane
ND
1.0
ug/L
11/05/17 15:52
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/05/17 15:52
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 15:52
1
Cyclohexane
ND
1.0
ug/L
11/05/17 15:52
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 15:52
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 15:52
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 15:52
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 15:52
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 15:52
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 15:52
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 15:52
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 15:52
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 15:52
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 15:52
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 15:52
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 15:52
1
2-Hexanone
ND
10
ug/L
11/05/17 15:52
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 15:52
1
Methyl acetate
ND
5.0
ug/L
11/05/17 15:52
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 15:52
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 15:52
1
4-Methyl-2-pentanone
ND
10
ug/L
11/05/17 15:52
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 15:52
1
Styrene
ND
1.0
ug/L
11/05/17 15:52
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 15:52
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 15:52
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 15:52
1
Toluene
ND
1.0
ug/L
11/05/17 15:52
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 15:52
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 15:52
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 15:52
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 15:52
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 15:52
1
Trichloroethene
ND
1.0
ug/L
11/05/17 15:52
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 15:52
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 15:52
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 15:52
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 15:52
1
a
F
TestArnerica Savannah
Page 37 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-42-102417 Lab Sample ID: 680-144889-13
Date Collected: 10/24/17 13:05 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 107 80-120 11105117 15:52 ,
Dibromofluoromethane (Surr) 107 80-122 11105117 15:52 1
1,2-Dichloroethane-d4 (Surr) 109 73-131 11105117 15:52 1
Toluene-d8 (Surr) 110 80-120 11105117 15:52 1
a
F
TestArnerica Savannah
Page 38 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-43-102417
Lab Sample ID: 680-144889-14
Date Collected: 10/24/17 12:30
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 16:14
1
Benzene
ND
1.0
ug/L
11/05/17 16:14
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 16:14
1
Bromoform
ND
1.0
ug/L
11/05/17 16:14
1
Bromomethane
ND
5.0
ug/L
11/05/17 16:14
1
2-Butanone
ND
10
ug/L
11/05/17 16:14
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 16:14
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 16:14
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 16:14
1
Chloroethane
ND
5.0
ug/L
11/05/17 16:14
1
Chloroform
ND
1.0
ug/L
11/05/17 16:14
1
Chloromethane
ND
1.0
ug/L
11/05/17 16:14
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/05/17 16:14
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 16:14
1
Cyclohexane
ND
1.0
ug/L
11/05/17 16:14
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 16:14
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 16:14
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 16:14
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:14
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:14
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:14
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 16:14
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 16:14
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 16:14
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 16:14
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 16:14
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 16:14
1
2-Hexanone
ND
10
ug/L
11/05/17 16:14
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 16:14
1
Methyl acetate
ND
5.0
ug/L
11/05/17 16:14
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 16:14
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 16:14
1
4-Methyl-2-pentanone
ND
10
ug/L
11/05/17 16:14
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 16:14
1
Styrene
ND
1.0
ug/L
11/05/17 16:14
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 16:14
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 16:14
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 16:14
1
Toluene
ND
1.0
ug/L
11/05/17 16:14
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 16:14
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 16:14
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 16:14
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 16:14
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 16:14
1
Trichloroethene
4.5
1.0
ug/L
11/05/17 16:14
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 16:14
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 16:14
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 16:14
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 16:14
1
a
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TestArnerica Savannah
Page 39 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-43-102417 Lab Sample ID: 680-144889-14
Date Collected: 10/24/17 12:30 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 115 80-120 11105117 16:14 ,
Dibromofluoromethane (Surr) 113 80-122 11105117 16:14 1
1,2-Dichloroethane-d4 (Surr) 107 73-131 11105117 16:14 1
Toluene-d8 (Surr) 109 80-120 11105117 16:14 1
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TestArnerica Savannah
Page 40 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-45-102417 Lab Sample ID: 680-144889-15
Date Collected: 10/24/17 14:32 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 16:36
1
Benzene
ND
1.0
ug/L
11/05/17 16:36
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 16:36
1
Bromoform
ND
1.0
ug/L
11/05/17 16:36
1
Bromomethane
ND
5.0
ug/L
11/05/17 16:36
1
2-Butanone
ND
10
ug/L
11/05/17 16:36
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 16:36
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 16:36
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 16:36
1
Chloroethane
ND
5.0
ug/L
11/05/17 16:36
1
Chloroform
ND
1.0
ug/L
11/05/17 16:36
1
Chloromethane
ND
1.0
ug/L
11/05/17 16:36
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/05/17 16:36
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 16:36
1
Cyclohexane
ND
1.0
ug/L
11/05/17 16:36
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 16:36
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 16:36
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 16:36
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:36
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:36
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:36
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 16:36
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 16:36
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 16:36
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 16:36
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 16:36
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 16:36
1
2-Hexanone
ND
10
ug/L
11/05/17 16:36
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 16:36
1
Methyl acetate
ND
5.0
ug/L
11/05/17 16:36
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 16:36
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 16:36
1
4-Methyl-2-pentanone
ND
10
ug/L
11/05/17 16:36
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 16:36
1
Styrene
ND
1.0
ug/L
11/05/17 16:36
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 16:36
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 16:36
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 16:36
1
Toluene
ND
1.0
ug/L
11/05/17 16:36
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 16:36
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 16:36
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 16:36
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 16:36
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 16:36
1
Trichloroethene
ND
1.0
ug/L
11/05/17 16:36
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 16:36
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 16:36
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 16:36
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 16:36
1
a
F
TestArnerica Savannah
Page 41 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-45-102417 Lab Sample ID: 680-144889-15
Date Collected: 10/24/17 14:32 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 104 80-120 11105117 16:36 1
Dibromofluoromethane (Surr) 115 80-122 11105117 16:36 1
1,2-Dichloroethane-d4 (Surr) 114 73-131 11105117 16:36 1
Toluene-d8 (Surr) 111 80-120 11105117 16:36 1
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TestArnerica Savannah
Page 42 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-47-102517
Lab Sample ID: 680-144889-16
Date Collected: 10/25/17 13:22
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 19:04
1
Benzene
ND
1.0
ug/L
11/08/17 19:04
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 19:04
1
Bromoform
ND
1.0
ug/L
11/08/17 19:04
1
Bromomethane
ND
5.0
ug/L
11/08/17 19:04
1
2-Butanone
ND
10
ug/L
11/08/17 19:04
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 19:04
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 19:04
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 19:04
1
Chloroethane
ND
5.0
ug/L
11/08/17 19:04
1
Chloroform
ND
1.0
ug/L
11/08/17 19:04
1
Chloromethane
ND
1.0
ug/L
11/08/17 19:04
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 19:04
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 19:04
1
Cyclohexane
ND
1.0
ug/L
11/08/17 19:04
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 19:04
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 19:04
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 19:04
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 19:04
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 19:04
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 19:04
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 19:04
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 19:04
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 19:04
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 19:04
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 19:04
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 19:04
1
2-Hexanone
ND
10
ug/L
11/08/17 19:04
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 19:04
1
Methyl acetate
ND
5.0
ug/L
11/08/17 19:04
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 19:04
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 19:04
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 19:04
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 19:04
1
Styrene
ND
1.0
ug/L
11/08/17 19:04
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 19:04
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 19:04
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 19:04
1
Toluene
ND
1.0
ug/L
11/08/17 19:04
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 19:04
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 19:04
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 19:04
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 19:04
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 19:04
1
Trichloroethene
ND
1.0
ug/L
11/08/17 19:04
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 19:04
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 19:04
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 19:04
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 19:04
1
a
F
TestArnerica Savannah
Page 43 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: A 155-MW-47-102517 Lab Sample ID: 680-144889-16
Date Collected: 10/25/17 13:22 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 88 80-120 11108117 19:04 ,
Dibromofluoromethane (Surr) 93 80-122 11108117 19:04 1
1,2-Dichloroethane-d4 (Surr) 91 73-131 11108117 19:04 1
Toluene-d8 (Surr) 101 80-120 11108117 19:04 1
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TestArnerica Savannah
Page 44 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-60-102517
Lab Sample ID: 680-144889-17
Date Collected: 10/25/17 11:39
Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 17:01
1
Benzene
ND
1.0
ug/L
11/04/17 17:01
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 17:01
1
Bromoform
ND
1.0
ug/L
11/04/17 17:01
1
Bromomethane
ND
5.0
ug/L
11/04/17 17:01
1
2-Butanone
ND
10
ug/L
11/04/17 17:01
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 17:01
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 17:01
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 17:01
1
Chloroethane
ND
5.0
ug/L
11/04/17 17:01
1
Chloroform
ND
1.0
ug/L
11/04/17 17:01
1
Chloromethane
ND
1.0
ug/L
11/04/17 17:01
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 17:01
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 17:01
1
Cyclohexane
ND
1.0
ug/L
11/04/17 17:01
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 17:01
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 17:01
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 17:01
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:01
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:01
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:01
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 17:01
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 17:01
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 17:01
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 17:01
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 17:01
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 17:01
1
2-Hexanone
ND *
10
ug/L
11/04/17 17:01
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 17:01
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 17:01
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 17:01
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 17:01
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 17:01
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 17:01
1
Styrene
ND
1.0
ug/L
11/04/17 17:01
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 17:01
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 17:01
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 17:01
1
Toluene
ND
1.0
ug/L
11/04/17 17:01
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 17:01
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 17:01
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 17:01
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 17:01
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 17:01
1
Trichloroethene
7.3
1.0
ug/L
11/04/17 17:01
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 17:01
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 17:01
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 17:01
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 17:01
1
a
F
TestArnerica Savannah
Page 45 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-60-102517 Lab Sample ID: 680-144889-17
Date Collected: 10/25/17 11:39 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 116 80-120 11104117 17:01 ,
Dibromofluoromethane (Surr) 98 80-122 11104117 17:01 1
1,2-Dichloroethane-d4 (Surr) 96 73-131 11104117 17:01 1
Toluene-d8 (Surr) 100 80-120 11104117 17:01 1
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TestArnerica Savannah
Page 46 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-61-102517 Lab Sample ID: 680-144889-18
Date Collected: 10/25/17 10:56 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 17:25
1
Benzene
ND
1.0
ug/L
11/04/17 17:25
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 17:25
1
Bromoform
ND
1.0
ug/L
11/04/17 17:25
1
Bromomethane
ND
5.0
ug/L
11/04/17 17:25
1
2-Butanone
ND
10
ug/L
11/04/17 17:25
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 17:25
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 17:25
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 17:25
1
Chloroethane
ND
5.0
ug/L
11/04/17 17:25
1
Chloroform
ND
1.0
ug/L
11/04/17 17:25
1
Chloromethane
ND
1.0
ug/L
11/04/17 17:25
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 17:25
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 17:25
1
Cyclohexane
ND
1.0
ug/L
11/04/17 17:25
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 17:25
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 17:25
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 17:25
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:25
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:25
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:25
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 17:25
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 17:25
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 17:25
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 17:25
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 17:25
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 17:25
1
2-Hexanone
ND *
10
ug/L
11/04/17 17:25
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 17:25
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 17:25
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 17:25
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 17:25
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 17:25
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 17:25
1
Styrene
ND
1.0
ug/L
11/04/17 17:25
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 17:25
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 17:25
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 17:25
1
Toluene
ND
1.0
ug/L
11/04/17 17:25
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 17:25
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 17:25
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 17:25
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 17:25
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 17:25
1
Trichloroethene
15
1.0
ug/L
11/04/17 17:25
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 17:25
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 17:25
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 17:25
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 17:25
1
a
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TestArnerica Savannah
Page 47 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-61-102517 Lab Sample ID: 680-144889-18
Date Collected: 10/25/17 10:56 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 116 80-120 11104117 17:25 ,
Dibromofluoromethane (Surr) 106 80-122 11104117 17:25 1
1,2-Dichloroethane-d4 (Surr) 96 73-131 11104117 17:25 1
Toluene-d8 (Surr) 110 80-120 11104117 17:25 1
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TestArnerica Savannah
Page 48 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-62-102517 Lab Sample ID: 680-144889-19
Date Collected: 10/25/17 12:21 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 17:50
1
Benzene
ND
1.0
ug/L
11/04/17 17:50
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 17:50
1
Bromoform
ND
1.0
ug/L
11/04/17 17:50
1
Bromomethane
ND
5.0
ug/L
11/04/17 17:50
1
2-Butanone
ND
10
ug/L
11/04/17 17:50
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 17:50
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 17:50
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 17:50
1
Chloroethane
ND
5.0
ug/L
11/04/17 17:50
1
Chloroform
ND
1.0
ug/L
11/04/17 17:50
1
Chloromethane
ND
1.0
ug/L
11/04/17 17:50
1
cis-1,2-Dichloroethene
5.4
1.0
ug/L
11/04/17 17:50
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 17:50
1
Cyclohexane
ND
1.0
ug/L
11/04/17 17:50
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 17:50
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 17:50
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 17:50
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:50
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:50
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 17:50
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 17:50
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 17:50
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 17:50
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 17:50
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 17:50
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 17:50
1
2-Hexanone
ND *
10
ug/L
11/04/17 17:50
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 17:50
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 17:50
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 17:50
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 17:50
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 17:50
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 17:50
1
Styrene
ND
1.0
ug/L
11/04/17 17:50
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 17:50
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 17:50
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 17:50
1
Toluene
ND
1.0
ug/L
11/04/17 17:50
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 17:50
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 17:50
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 17:50
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 17:50
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 17:50
1
Trichloroethene
4.7
1.0
ug/L
11/04/17 17:50
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 17:50
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 17:50
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 17:50
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 17:50
1
a
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TestArnerica Savannah
Page 49 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-62-102517 Lab Sample ID: 680-144889-19
Date Collected: 10/25/17 12:21 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 105 80-120 11104117 17:50 ,
Dibromofluoromethane (Surr) 97 80-122 11104117 17:50 1
1,2-Dichloroethane-d4 (Surr) 95 73-131 11104117 17:50 1
Toluene-d8 (Surr) 105 80-120 11104117 17:50 1
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TestArnerica Savannah
Page 50 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-MW-63-102717 Lab Sample ID: 680-144889-20
Date Collected: 10/27/17 09:09 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 01:22
1
Benzene
ND
1.0
ug/L
11/08/17 01:22
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 01:22
1
Bromoform
ND
1.0
ug/L
11/08/17 01:22
1
Bromomethane
ND
5.0
ug/L
11/08/17 01:22
1
2-Butanone
ND
10
ug/L
11/08/17 01:22
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 01:22
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 01:22
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 01:22
1
Chloroethane
ND
5.0
ug/L
11/08/17 01:22
1
Chloroform
ND
1.0
ug/L
11/08/17 01:22
1
Chloromethane
ND
1.0
ug/L
11/08/17 01:22
1
cis-1,2-Dichloroethene
12
1.0
ug/L
11/08/17 01:22
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 01:22
1
Cyclohexane
ND
1.0
ug/L
11/08/17 01:22
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 01:22
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 01:22
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 01:22
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 01:22
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 01:22
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 01:22
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 01:22
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 01:22
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 01:22
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 01:22
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 01:22
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 01:22
1
2-Hexanone
ND
10
ug/L
11/08/17 01:22
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 01:22
1
Methyl acetate
ND
5.0
ug/L
11/08/17 01:22
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 01:22
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 01:22
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 01:22
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 01:22
1
Styrene
ND
1.0
ug/L
11/08/17 01:22
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 01:22
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 01:22
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 01:22
1
Toluene
ND
1.0
ug/L
11/08/17 01:22
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 01:22
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 01:22
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 01:22
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 01:22
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 01:22
1
Trichloroethene
13
1.0
ug/L
11/08/17 01:22
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 01:22
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 01:22
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 01:22
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 01:22
1
a
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TestArnerica Savannah
Page 51 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-MW-63-102717 Lab Sample ID: 680-144889-20
Date Collected: 10/27/17 09:09 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 87 80-120 11108117 01:22 ,
Dibromofluoromethane (Surr) 97 80-122 11108117 01:22 1
1,2-Dichloroethane-d4 (Surr) 92 73-131 11108117 01:22 1
Toluene-d8 (Surr) 100 80-120 11108117 01:22 1
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TestArnerica Savannah
Page 52 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: A 155-PW-1 6-102717
Lab Sample ID: 680-144889-21
Date Collected: 10/27/17 10:35
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 01:44
1
Benzene
ND
1.0
ug/L
11/08/17 01:44
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 01:44
1
Bromoform
ND
1.0
ug/L
11/08/17 01:44
1
Bromomethane
ND
5.0
ug/L
11/08/17 01:44
1
2-Butanone
ND
10
ug/L
11/08/17 01:44
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 01:44
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 01:44
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 01:44
1
Chloroethane
ND
5.0
ug/L
11/08/17 01:44
1
Chloroform
ND
1.0
ug/L
11/08/17 01:44
1
Chloromethane
ND
1.0
ug/L
11/08/17 01:44
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 01:44
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 01:44
1
Cyclohexane
ND
1.0
ug/L
11/08/17 01:44
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 01:44
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 01:44
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 01:44
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 01:44
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 01:44
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 01:44
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 01:44
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 01:44
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 01:44
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 01:44
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 01:44
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 01:44
1
2-Hexanone
ND
10
ug/L
11/08/17 01:44
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 01:44
1
Methyl acetate
ND
5.0
ug/L
11/08/17 01:44
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 01:44
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 01:44
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 01:44
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 01:44
1
Styrene
ND
1.0
ug/L
11/08/17 01:44
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 01:44
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 01:44
1
Tetrahydrofuran
35
10
ug/L
11/08/17 01:44
1
Toluene
ND
1.0
ug/L
11/08/17 01:44
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 01:44
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 01:44
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 01:44
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 01:44
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 01:44
1
Trichloroethene
ND
1.0
ug/L
11/08/17 01:44
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 01:44
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 01:44
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 01:44
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 01:44
1
a
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TestArnerica Savannah
Page 53 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: A 155-PW-1 6-102717 Lab Sample ID: 680-144889-21
Date Collected: 10/27/17 10:35 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 88 80-120 11108117 01:44 ,
Dibromofluoromethane (Surr) 99 80-122 11108117 01:44 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11108117 01:44 1
Toluene-d8 (Surr) 99 80-120 11108117 01:44 1
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TestArnerica Savannah
Page 54 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-SP-26-102717 Lab Sample ID: 680-144889-22
Date Collected: 10/27/17 11:29 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
cis- 1,2-Dichloroethene
ND
cis- 1,3-Dichloropropene
ND
Cyclohexane
ND
Dibromochloromethane
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
1,1-Dichloroethene
ND
1,2-Dichloropropane
ND
Ethylbenzene
ND
2-Hexanone
ND
I sopropyl benzene
ND
Methyl acetate
ND
Methylcyclohexane
ND
Methylene Chloride
ND
4-Methyl-2-pentanone
ND
Methyl tert-butyl ether
ND
Styrene
ND
1,1,2,2-Tetrachloroethane
ND
Tetrachloroethene
ND
Tetrahydrofuran
ND
Toluene
ND
trans- 1,2-Dich loroethene
ND
trans- 1, 3-Dich loropropene
ND
1,2,4-Trichlorobenzene
ND
1,1,1-Trichloroethane
ND
1,1,2-Trichloroethane
ND
Trichloroethene
1.9
Trichlorofluoromethane
ND
1 1 2-Trichloro-1 2 2-trifluoroetha
1.5
I I I I
ne
Vinyl chloride ND
RL
MDL Unit
D Prepared Analyzed
Dil Fac
10
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
5.0
ug/L
11/08/17 02:06
1
10
ug/L
11/08/17 02:06
1
2.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
5.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
5.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
10
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
5.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
5.0
ug/L
11/08/17 02:06
1
10
ug/L
11/08/17 02:06
1
10
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
10
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
5.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
1.0
ug/L
11/08/17 02:06
1
a
F
TestArnerica Savannah
Page 55 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-SP-26-102717
Lab Sample ID: 680-144889-22
Date Collected: 10/27/17 11:29
Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Xylenes, Total ND
1.0 ug/L
11/08/17 02:06 -1
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
4-Bromofluorobenzene FSu-rr) 88
80-120
111081170 1
Dibromofluoromethane (Surr) 97
80-122
11108117 02:06 1
1,2-Dichloroethane-d4 (Surr) 93
73-131
11108117 02:06
Toluene-d8 (Surr) 99
80-120
11108117 02:06 1
F
TestArnerica Savannah
Page 56 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-CMP-1-102717
Lab Sample ID: 680-144889-23
Date Collected: 10/27/17 09:35
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 02:28
1
Benzene
ND
1.0
ug/L
11/08/17 02:28
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 02:28
1
Bromoform
ND
1.0
ug/L
11/08/17 02:28
1
Bromomethane
ND
5.0
ug/L
11/08/17 02:28
1
2-Butanone
ND
10
ug/L
11/08/17 02:28
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 02:28
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 02:28
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 02:28
1
Chloroethane
ND
5.0
ug/L
11/08/17 02:28
1
Chloroform
ND
1.0
ug/L
11/08/17 02:28
1
Chloromethane
ND
1.0
ug/L
11/08/17 02:28
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 02:28
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 02:28
1
Cyclohexane
ND
1.0
ug/L
11/08/17 02:28
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 02:28
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 02:28
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 02:28
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 02:28
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 02:28
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 02:28
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 02:28
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 02:28
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 02:28
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 02:28
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 02:28
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 02:28
1
2-Hexanone
ND
10
ug/L
11/08/17 02:28
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 02:28
1
Methyl acetate
ND
5.0
ug/L
11/08/17 02:28
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 02:28
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 02:28
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 02:28
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 02:28
1
Styrene
ND
1.0
ug/L
11/08/17 02:28
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 02:28
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 02:28
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 02:28
1
Toluene
ND
1.0
ug/L
11/08/17 02:28
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 02:28
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 02:28
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 02:28
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 02:28
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 02:28
1
Trichloroethene
ND
1.0
ug/L
11/08/17 02:28
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 02:28
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 02:28
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 02:28
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 02:28
1
a
F
TestArnerica Savannah
Page 57 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-CMP-1-102717 Lab Sample ID: 680-144889-23
Date Collected: 10/27/17 09:35 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 88 80-120 11108117 02:28 ,
Dibromofluoromethane (Surr) 97 80-122 11108117 02:28 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11108117 02:28 1
Toluene-d8 (Surr) 99 80-120 11108117 02:28 1
a
F
TestArnerica Savannah
Page 58 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-CMP-3-102717 Lab Sample ID: 680-144889-24
Date Collected: 10/27/17 11:47 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 02:50
1
Benzene
ND
1.0
ug/L
11/08/17 02:50
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 02:50
1
Bromoform
ND
1.0
ug/L
11/08/17 02:50
1
Bromomethane
ND
5.0
ug/L
11/08/17 02:50
1
2-Butanone
ND
10
ug/L
11/08/17 02:50
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 02:50
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 02:50
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 02:50
1
Chloroethane
ND
5.0
ug/L
11/08/17 02:50
1
Chloroform
ND
1.0
ug/L
11/08/17 02:50
1
Chloromethane
ND
1.0
ug/L
11/08/17 02:50
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 02:50
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 02:50
1
Cyclohexane
ND
1.0
ug/L
11/08/17 02:50
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 02:50
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 02:50
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 02:50
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 02:50
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 02:50
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 02:50
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 02:50
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 02:50
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 02:50
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 02:50
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 02:50
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 02:50
1
2-Hexanone
ND
10
ug/L
11/08/17 02:50
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 02:50
1
Methyl acetate
ND
5.0
ug/L
11/08/17 02:50
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 02:50
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 02:50
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 02:50
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 02:50
1
Styrene
ND
1.0
ug/L
11/08/17 02:50
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 02:50
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 02:50
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 02:50
1
Toluene
ND
1.0
ug/L
11/08/17 02:50
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 02:50
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 02:50
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 02:50
1
1,1,1-Trichloroethane
1.1
1.0
ug/L
11/08/17 02:50
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 02:50
1
Trichloroethene
4.3
1.0
ug/L
11/08/17 02:50
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 02:50
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 02:50
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 02:50
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 02:50
1
a
F
TestArnerica Savannah
Page 59 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-CMP-3-102717 Lab Sample ID: 680-144889-24
Date Collected: 10/27/17 11:47 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 88 80-120 11108117 02:50 ,
Dibromofluoromethane (Surr) 98 80-122 11108117 02:50 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11108117 02:50 1
Toluene-d8 (Surr) 100 80-120 11108117 02:50 1
a
F
TestArnerica Savannah
Page 60 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-CMP-4-102717
Lab Sample ID: 680-144889-25
Date Collected: 10/27/17 09:21
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 03:12
1
Benzene
ND
1.0
ug/L
11/08/17 03:12
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 03:12
1
Bromoform
ND
1.0
ug/L
11/08/17 03:12
1
Bromomethane
ND
5.0
ug/L
11/08/17 03:12
1
2-Butanone
ND
10
ug/L
11/08/17 03:12
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 03:12
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 03:12
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 03:12
1
Chloroethane
ND
5.0
ug/L
11/08/17 03:12
1
Chloroform
ND
1.0
ug/L
11/08/17 03:12
1
Chloromethane
ND
1.0
ug/L
11/08/17 03:12
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 03:12
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 03:12
1
Cyclohexane
ND
1.0
ug/L
11/08/17 03:12
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 03:12
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 03:12
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 03:12
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:12
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:12
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:12
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 03:12
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 03:12
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 03:12
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 03:12
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 03:12
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 03:12
1
2-Hexanone
ND
10
ug/L
11/08/17 03:12
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 03:12
1
Methyl acetate
ND
5.0
ug/L
11/08/17 03:12
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 03:12
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 03:12
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 03:12
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 03:12
1
Styrene
ND
1.0
ug/L
11/08/17 03:12
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 03:12
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 03:12
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 03:12
1
Toluene
ND
1.0
ug/L
11/08/17 03:12
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 03:12
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 03:12
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 03:12
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 03:12
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 03:12
1
Trichloroethene
2.3
1.0
ug/L
11/08/17 03:12
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 03:12
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 03:12
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 03:12
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 03:12
1
a
F
TestArnerica Savannah
Page 61 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-CMP-4-102717 Lab Sample ID: 680-144889-25
Date Collected: 10/27/17 09:21 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 89 80-120 11108117 03:12 ,
Dibromofluoromethane (Surr) 98 80-122 11108117 03:12 1
1,2-Dichloroethane-d4 (Surr) 92 73-131 11108117 03:12 1
Toluene-d8 (Surr) 101 80-120 11108117 03:12 1
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TestArnerica Savannah
Page 62 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-SW-3-102717
Lab Sample ID: 680-144889-26
Date Collected: 10/27/17 09:48
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 03:34
1
Benzene
ND
1.0
ug/L
11/08/17 03:34
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 03:34
1
Bromoform
ND
1.0
ug/L
11/08/17 03:34
1
Bromomethane
ND
5.0
ug/L
11/08/17 03:34
1
2-Butanone
ND
10
ug/L
11/08/17 03:34
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 03:34
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 03:34
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 03:34
1
Chloroethane
ND
5.0
ug/L
11/08/17 03:34
1
Chloroform
ND
1.0
ug/L
11/08/17 03:34
1
Chloromethane
ND
1.0
ug/L
11/08/17 03:34
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 03:34
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 03:34
1
Cyclohexane
ND
1.0
ug/L
11/08/17 03:34
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 03:34
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 03:34
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 03:34
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:34
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:34
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:34
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 03:34
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 03:34
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 03:34
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 03:34
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 03:34
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 03:34
1
2-Hexanone
ND
10
ug/L
11/08/17 03:34
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 03:34
1
Methyl acetate
ND
5.0
ug/L
11/08/17 03:34
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 03:34
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 03:34
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 03:34
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 03:34
1
Styrene
ND
1.0
ug/L
11/08/17 03:34
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 03:34
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 03:34
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 03:34
1
Toluene
ND
1.0
ug/L
11/08/17 03:34
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 03:34
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 03:34
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 03:34
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 03:34
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 03:34
1
Trichloroethene
1.9
1.0
ug/L
11/08/17 03:34
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 03:34
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 03:34
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 03:34
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 03:34
1
a
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TestArnerica Savannah
Page 63 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-SW-3-102717 Lab Sample ID: 680-144889-26
Date Collected: 10/27/17 09:48 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 88 80-120 11108117 03:34 ,
Dibromofluoromethane (Surr) 99 80-122 11108117 03:34 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11108117 03:34 1
Toluene-d8 (Surr) 98 80-120 11108117 03:34 1
a
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TestArnerica Savannah
Page 64 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-SW-6-102717
Lab Sample ID: 680-144889-27
Date Collected: 10/27/17 11:09
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 03:56
1
Benzene
ND
1.0
ug/L
11/08/17 03:56
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 03:56
1
Bromoform
ND
1.0
ug/L
11/08/17 03:56
1
Bromomethane
ND
5.0
ug/L
11/08/17 03:56
1
2-Butanone
ND
10
ug/L
11/08/17 03:56
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 03:56
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 03:56
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 03:56
1
Chloroethane
ND
5.0
ug/L
11/08/17 03:56
1
Chloroform
ND
1.0
ug/L
11/08/17 03:56
1
Chloromethane
ND
1.0
ug/L
11/08/17 03:56
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 03:56
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 03:56
1
Cyclohexane
ND
1.0
ug/L
11/08/17 03:56
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 03:56
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 03:56
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 03:56
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:56
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:56
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 03:56
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 03:56
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 03:56
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 03:56
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 03:56
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 03:56
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 03:56
1
2-Hexanone
ND
10
ug/L
11/08/17 03:56
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 03:56
1
Methyl acetate
ND
5.0
ug/L
11/08/17 03:56
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 03:56
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 03:56
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 03:56
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 03:56
1
Styrene
ND
1.0
ug/L
11/08/17 03:56
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 03:56
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 03:56
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 03:56
1
Toluene
ND
1.0
ug/L
11/08/17 03:56
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 03:56
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 03:56
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 03:56
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 03:56
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 03:56
1
Trichloroethene
ND
1.0
ug/L
11/08/17 03:56
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 03:56
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 03:56
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 03:56
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 03:56
1
a
F
TestArnerica Savannah
Page 65 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-SW-6-102717 Lab Sample ID: 680-144889-27
Date Collected: 10/27/17 11:09 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 88 80-120 11108117 03:56 ,
Dibromofluoromethane (Surr) 99 80-122 11108117 03:56 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11108117 03:56 1
Toluene-d8 (Surr) 99 80-120 11108117 03:56 1
a
F
TestArnerica Savannah
Page 66 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-SW-10-102717 Lab Sample ID: 680-144889-28
Date Collected: 10/27/17 10:47 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 11:28
1
Benzene
ND
1.0
ug/L
11/08/17 11:28
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 11:28
1
Bromoform
ND
1.0
ug/L
11/08/17 11:28
1
Bromomethane
ND
5.0
ug/L
11/08/17 11:28
1
2-Butanone
ND
10
ug/L
11/08/17 11:28
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 11:28
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 11:28
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 11:28
1
Chloroethane
ND
5.0
ug/L
11/08/17 11:28
1
Chloroform
ND
1.0
ug/L
11/08/17 11:28
1
Chloromethane
ND
1.0
ug/L
11/08/17 11:28
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 11:28
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 11:28
1
Cyclohexane
ND
1.0
ug/L
11/08/17 11:28
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 11:28
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 11:28
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 11:28
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 11:28
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 11:28
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 11:28
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 11:28
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 11:28
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 11:28
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 11:28
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 11:28
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 11:28
1
2-Hexanone
ND
10
ug/L
11/08/17 11:28
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 11:28
1
Methyl acetate
ND
5.0
ug/L
11/08/17 11:28
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 11:28
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 11:28
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 11:28
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 11:28
1
Styrene
ND
1.0
ug/L
11/08/17 11:28
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 11:28
1
Tetrachloroethene
ND *
1.0
ug/L
11/08/17 11:28
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 11:28
1
Toluene
ND *
1.0
ug/L
11/08/17 11:28
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 11:28
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 11:28
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 11:28
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 11:28
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 11:28
1
Trichloroethene
ND
1.0
ug/L
11/08/17 11:28
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 11:28
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 11:28
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 11:28
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 11:28
1
a
F
TestArnerica Savannah
Page 67 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-SW-10-102717 Lab Sample ID: 680-144889-28
Date Collected: 10/27/17 10:47 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 107 80-120 11108117 11:28 ,
Dibromofluoromethane (Surr) 104 80-122 11108117 11:28 1
1,2-Dichloroethane-d4 (Surr) 106 73-131 11108117 11:28 1
Toluene-d8 (Surr) 108 80-120 11108117 11:28 1
a
F
TestArnerica Savannah
Page 68 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-RW-2-102617 Lab Sample ID: 680-144889-29
Date Collected: 10/26/17 16:49 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 20:30
1
Benzene
ND
1.0
ug/L
11/05/17 20:30
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 20:30
1
Bromoform
ND
1.0
ug/L
11/05/17 20:30
1
Bromomethane
ND
5.0
ug/L
11/05/17 20:30
1
2-Butanone
ND
10
ug/L
11/05/17 20:30
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 20:30
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 20:30
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 20:30
1
Chloroethane
ND
5.0
ug/L
11/05/17 20:30
1
Chloroform
ND
1.0
ug/L
11/05/17 20:30
1
Chloromethane
ND
1.0
ug/L
11/05/17 20:30
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/05/17 20:30
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 20:30
1
Cyclohexane
ND
1.0
ug/L
11/05/17 20:30
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 20:30
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 20:30
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 20:30
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 20:30
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 20:30
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 20:30
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 20:30
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 20:30
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 20:30
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 20:30
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 20:30
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 20:30
1
2-Hexanone
ND *
10
ug/L
11/05/17 20:30
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 20:30
1
Methyl acetate
ND *
5.0
ug/L
11/05/17 20:30
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 20:30
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 20:30
1
4-Methyl-2-pentanone
ND *
10
ug/L
11/05/17 20:30
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 20:30
1
Styrene
ND
1.0
ug/L
11/05/17 20:30
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 20:30
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 20:30
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 20:30
1
Toluene
ND
1.0
ug/L
11/05/17 20:30
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 20:30
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 20:30
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 20:30
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 20:30
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 20:30
1
Trichloroethene
6.5
1.0
ug/L
11/05/17 20:30
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 20:30
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 20:30
1
Vinyl chloride
1.4
1.0
ug/L
11/05/17 20:30
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 20:30
1
a
F
TestArnerica Savannah
Page 69 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-RW-2-102617 Lab Sample ID: 680-144889-29
Date Collected: 10/26/17 16:49 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 116 80-120 11105117 20:30 ,
Dibromofluoromethane (Surr) 100 80-122 11105117 20:30 1
1,2-Dichloroethane-d4 (Surr) 94 73-131 11105117 20:30 1
Toluene-d8 (Surr) 101 80-120 11105117 20:30 1
a
F
TestArnerica Savannah
Page 70 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-RW-3-102617 Lab Sample ID: 680-144889-30
Date Collected: 10/26/17 16:56 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
ND
Bromodichloromethane
ND
Brornoform
ND
Brornornethane
ND
2-Butanone
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
11
Chloromethane
ND
cis-1,2-Dichloroethene
7.9
cis- 1,3-Dichloropropene
ND
Cyclohexane
ND
Dibromochloromethane
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
11,11-Dichloroethane
4.8
1,2-Dichloroethane
ND
1,1-Dichloroethene
44
1,2-Dichloropropane
ND
Ethylbenzene
ND
2-Hexanone
ND
I sopropyl benzene
ND
Methyl acetate
ND
Methylcyclohexane
ND
Methylene Chloride
ND
4-Methyl-2-pentanone
ND
Methyl tert-butyl ether
ND
Styrene
ND
1,1,2,2-Tetrachloroethane
ND
Tetrachloroethene
39
Tetrahydrofuran
ND
Toluene
ND
trans- 1,2-Dich loroethene
ND
trans- 1, 3-Dich loropropene
ND
1,2,4-Trichlorobenzene
ND
11,11,11-Trichloroethane
59
1,1,2-Trichloroethane
ND
Trichloroethene
270
Trichlorofluoromethane
ND
1 1 2-Trichloro-1 2 2-trifluoroetha
91
I I I I
ne
Vinyl chloride ND
RL
MDL Unit
D Prepared Analyzed
Dil Fac
20
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
10
ug/L
11/05/17 20:54
2
20
ug/L
11/05/17 20:54
2
4.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
10
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
10
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
20
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
10
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
10
ug/L
11/05/17 20:54
2
20
ug/L
11/05/17 20:54
2
20
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
20
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
10
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
2.0
ug/L
11/05/17 20:54
2
a
TestArnerica Savannah
Page 71 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-RW-3-102617 Lab Sample ID: 680-144889-30
Date Collected: 10/26/17 16:56 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Xylenes, Total ND 2.0 ug/L 11/05/17 20:54 -2
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
4-Bromofluorobenzene FSu-rr) 107 80-120 111051172 2
Dibromofluoromethane (Surr) 104 80-122 11105117 20:54 2
1,2-Dichloroethane-d4 (Surr) 98 73-131 11105117 20:54 2
Toluene-d8 (Surr) 116 80-120 11105117 20:54 2
F
TestArnerica Savannah
Page 72 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-RW-5-102617 Lab Sample ID: 680-144889-31
Date Collected: 10/26/17 16:38 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
100
ug/L
11/07/17 17:14
10
Benzene
ND
10
ug/L
11/07/17 17:14
10
Bromodichloromethane
ND
10
ug/L
11/07/17 17:14
10
Bromoform
ND
10
ug/L
11/07/17 17:14
10
Bromomethane
ND
50
ug/L
11/07/17 17:14
10
2-Butanone
ND
100
ug/L
11/07/17 17:14
10
Carbon disulfide
ND
20
ug/L
11/07/17 17:14
10
Carbon tetrachloride
ND
10
ug/L
11/07/17 17:14
10
Chlorobenzene
ND
10
ug/L
11/07/17 17:14
10
Chloroethane
ND
50
ug/L
11/07/17 17:14
10
Chloroform
ND
10
ug/L
11/07/17 17:14
10
Chloromethane
ND
10
ug/L
11/07/17 17:14
10
cis-1,2-Dichloroethene
160
10
ug/L
11/07/17 17:14
10
cis- 1,3-Dichloropropene
ND
10
ug/L
11/07/17 17:14
10
Cyclohexane
ND
10
ug/L
11/07/17 17:14
10
Dibromochloromethane
ND
10
ug/L
11/07/17 17:14
10
1,2-Dibromo-3-Chloropropane
ND
50
ug/L
11/07/17 17:14
10
1,2-Dibromoethane
ND
10
ug/L
11/07/17 17:14
10
1,2-Dichlorobenzene
ND
10
ug/L
11/07/17 17:14
10
1,3-Dichlorobenzene
ND
10
ug/L
11/07/17 17:14
10
1,4-Dichlorobenzene
ND
10
ug/L
11/07/17 17:14
10
Dichlorodifluoromethane
ND
10
ug/L
11/07/17 17:14
10
11,11-Dichloroethane
180
10
ug/L
11/07/17 17:14
10
1,2-Dichloroethane
ND
10
ug/L
11/07/17 17:14
10
1,1-Dichloroethene
64
10
ug/L
11/07/17 17:14
10
1,2-Dichloropropane
ND
10
ug/L
11/07/17 17:14
10
Ethylbenzene
ND
10
ug/L
11/07/17 17:14
10
2-Hexanone
ND
100
ug/L
11/07/17 17:14
10
I sopropyl benzene
ND
10
ug/L
11/07/17 17:14
10
Methyl acetate
ND
50
ug/L
11/07/17 17:14
10
Methylcyclohexane
ND
10
ug/L
11/07/17 17:14
10
Methylene Chloride
ND
50
ug/L
11/07/17 17:14
10
4-Methyl-2-pentanone
ND
100
ug/L
11/07/17 17:14
10
Methyl tert-butyl ether
ND
100
ug/L
11/07/17 17:14
10
Styrene
ND
10
ug/L
11/07/17 17:14
10
1,1,2,2-Tetrachloroethane
ND
10
ug/L
11/07/17 17:14
10
Tetrachloroethene
74
10
ug/L
11/07/17 17:14
10
Tetrahydrofuran
ND
100
ug/L
11/07/17 17:14
10
Toluene
ND
10
ug/L
11/07/17 17:14
10
trans- 1,2-Dich loroethene
ND
10
ug/L
11/07/17 17:14
10
trans- 1, 3-Dich loropropene
ND
10
ug/L
11/07/17 17:14
10
1,2,4-Trichlorobenzene
ND
50
ug/L
11/07/17 17:14
10
1,1,1-Trichloroethane
110
10
ug/L
11/07/17 17:14
10
1,1,2-Trichloroethane
ND
10
ug/L
11/07/17 17:14
10
Trichlorofluoromethane
ND
10
ug/L
11/07/17 17:14
10
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
10
ug/L
11/07/17 17:14
10
Vinyl chloride
ND
10
ug/L
11/07/17 17:14
10
Xylenes, Total
ND
10
ug/L
11/07/17 17:14
10
a
TestArnerica Savannah
Page 73 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
F
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-RW-5-102617 Lab Sample ID: 680-144889-31
Date Collected: 10/26/17 16:38 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
90
80-120
Dibromofluoromethane (Surr)
102
80-122
1,2-Dichloroethane-d4 (Surr)
102
73-131
Toluene-d8 (Surr)
100
80-120
Method: 8260B - Volatile Organic
Compounds (GC/MS) - DIL
Analyte
Result Qualifier
RL
Trichloroethene
1400
20
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
106
80-120
Dibromofluoromethane (Surr)
105
80-122
1,2-Dichloroethane-d4 (Surr)
105
73-131
Toluene-d8 (Surr)
107
80-120
Prepared Analyzed
Dil Fac
L
11/07/17 17:14
io
11/07/17 17:14
10
11/07/17 17:14
10
11/07/17 17:14
10
MDL Unit D Prepared
ug/L
Prepared
Analyzed
Dil Fac
a
11/09/17 12:46
-
20
Analyzed
Dil Fac
11109117 12:46
20
11109117 12:46
20
11109117 12:46
20
11109117 12:46
20
TestArnerica Savannah
Page 74 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-DUP-1-102417 Lab Sample ID: 680-144889-32
Date Collected: 10/24/17 16:00 Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
Acetone
ND
Benzene
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
cis-1,2-Dichloroethene
39
cis- 1,3-Dichloropropene
ND
Cyclohexane
ND
Dibromochloromethane
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
1,1-Dichloroethene
ND
1,2-Dichloropropane
ND
Ethylbenzene
ND
2-Hexanone
ND
I sopropyl benzene
ND
Methyl acetate
ND
Methylcyclohexane
ND
Methylene Chloride
ND
4-Methyl-2-pentanone
ND
Methyl tert-butyl ether
ND
Styrene
ND
1,1,2,2-Tetrachloroethane
ND
Tetrachloroethene
ND
Tetrahydrofuran
ND
Toluene
ND
trans- 1,2-Dich loroethene
ND
trans- 1, 3-Dich loropropene
ND
1,2,4-Trichlorobenzene
ND
1,1,1-Trichloroethane
ND
1,1,2-Trichloroethane
ND
Trichloroethene
1.9
Trichlorofluoromethane
ND
1 1 2-Trichloro-1 2 2-trifluoroetha
1.7
I I I I
ne
Vinyl chloride ND
RL
MDL Unit
D Prepared Analyzed
Dil Fac
10
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
5.0
ug/L
11/05/17 16:58
1
10
ug/L
11/05/17 16:58
1
2.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
5.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
5.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
10
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
5.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
5.0
ug/L
11/05/17 16:58
1
10
ug/L
11/05/17 16:58
1
10
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
10
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
5.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
1.0
ug/L
11/05/17 16:58
1
a
F
TestArnerica Savannah
Page 75 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-DUP-2-102417 Lab Sample ID: 680-144889-33
Date Collected: 10/24/17 16:10 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 21:00
1
Benzene
ND
1.0
ug/L
11/05/17 21:00
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 21:00
1
Bromoform
ND
1.0
ug/L
11/05/17 21:00
1
Bromomethane
ND
5.0
ug/L
11/05/17 21:00
1
2-Butanone
ND
10
ug/L
11/05/17 21:00
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 21:00
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 21:00
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 21:00
1
Chloroethane
ND
5.0
ug/L
11/05/17 21:00
1
Chloroform
ND
1.0
ug/L
11/05/17 21:00
1
Chloromethane
ND
1.0
ug/L
11/05/17 21:00
1
cis-1,2-Dichloroethene
1.0
1.0
ug/L
11/05/17 21:00
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 21:00
1
Cyclohexane
ND
1.0
ug/L
11/05/17 21:00
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 21:00
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 21:00
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 21:00
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 21:00
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 21:00
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 21:00
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 21:00
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 21:00
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 21:00
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 21:00
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 21:00
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 21:00
1
2-Hexanone
ND
10
ug/L
11/05/17 21:00
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 21:00
1
Methyl acetate
ND
5.0
ug/L
11/05/17 21:00
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 21:00
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 21:00
1
4-Methyl-2-pentanone
ND
10
ug/L
11/05/17 21:00
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 21:00
1
Styrene
ND
1.0
ug/L
11/05/17 21:00
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 21:00
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 21:00
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 21:00
1
Toluene
ND
1.0
ug/L
11/05/17 21:00
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 21:00
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 21:00
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 21:00
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 21:00
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 21:00
1
Trichloroethene
15
1.0
ug/L
11/05/17 21:00
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 21:00
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 21:00
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 21:00
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 21:00
1
a
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Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-DUP-1-102417
Lab Sample ID: 680-144889-32
Date Collected: 10/24/17 16:00
Matrix: Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Xylenes, Total ND
1.0 ug/L
11/05/17 16:56 -1
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
4-Bromofluorobenzene FSu-rr) 95
80-120
111051171 1
Dibromofluoromethane (Surr) 110
80-122
11105117 16:58 1
1,2-Dichloroethane-d4 (Surr) 118
73-131
11105117 16:58
Toluene-d8 (Surr) 101
80-120
11105117 16:58 1
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TestArnerica Savannah
Page 76 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-DUP-2-102417 Lab Sample ID: 680-144889-33
Date Collected: 10/24/17 16:10 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 108 80-120 11105117 21:00 1
Dibromofluoromethane (Surr) 107 80-122 11105117 21:00 1
1,2-Dichloroethane-d4 (Surr) 111 73-131 11105117 21:00 1
Toluene-d8 (Surr) 107 80-120 11105117 21:00 1
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TestArnerica Savannah
Page 78 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-DUP-3-102517
Lab Sample ID: 680-144889-34
Date Collected: 10/25/17 16:00
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 18:15
1
Benzene
ND
1.0
ug/L
11/04/17 18:15
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 18:15
1
Bromoform
ND
1.0
ug/L
11/04/17 18:15
1
Bromomethane
ND
5.0
ug/L
11/04/17 18:15
1
2-Butanone
ND
10
ug/L
11/04/17 18:15
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 18:15
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 18:15
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 18:15
1
Chloroethane
ND
5.0
ug/L
11/04/17 18:15
1
Chloroform
ND
1.0
ug/L
11/04/17 18:15
1
Chloromethane
ND
1.0
ug/L
11/04/17 18:15
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 18:15
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 18:15
1
Cyclohexane
ND
1.0
ug/L
11/04/17 18:15
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 18:15
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 18:15
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 18:15
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 18:15
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 18:15
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 18:15
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 18:15
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 18:15
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 18:15
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 18:15
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 18:15
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 18:15
1
2-Hexanone
ND *
10
ug/L
11/04/17 18:15
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 18:15
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 18:15
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 18:15
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 18:15
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 18:15
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 18:15
1
Styrene
ND
1.0
ug/L
11/04/17 18:15
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 18:15
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 18:15
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 18:15
1
Toluene
ND
1.0
ug/L
11/04/17 18:15
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 18:15
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 18:15
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 18:15
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 18:15
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 18:15
1
Trichloroethene
5.7
1.0
ug/L
11/04/17 18:15
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 18:15
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 18:15
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 18:15
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 18:15
1
a
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TestArnerica Savannah
Page 79 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-DUP-3-102517 Lab Sample ID: 680-144889-34
Date Collected: 10/25/17 16:00 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 106 80-120 11104117 18:15 ,
Dibromofluoromethane (Surr) 91 80-122 11104117 18:15 1
1,2-Dichloroethane-d4 (Surr) 89 73-131 11104117 18:15 1
Toluene-d8 (Surr) 106 80-120 11104117 18:15 1
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TestArnerica Savannah
Page 80 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-DUP-4-102517 Lab Sample ID: 680-144889-35
Date Collected: 10/25/17 16:10 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 16:20
1
Benzene
5.2
1.0
ug/L
11/08/17 16:20
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 16:20
1
Brornoform
ND
1.0
ug/L
11/08/17 16:20
1
Brornornethane
ND
5.0
ug/L
11/08/17 16:20
1
2-Butanone
ND
10
ug/L
11/08/17 16:20
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 16:20
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 16:20
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 16:20
1
Chloroethane
ND
5.0
ug/L
11/08/17 16:20
1
Chloroform
23
1.0
ug/L
11/08/17 16:20
1
Chloromethane
ND
1.0
ug/L
11/08/17 16:20
1
cis-1,2-Dichloroethene
6.6
1.0
ug/L
11/08/17 16:20
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 16:20
1
Cyclohexane
ND
1.0
ug/L
11/08/17 16:20
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 16:20
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 16:20
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 16:20
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 16:20
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 16:20
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 16:20
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 16:20
1
11,11-Dichloroethane
47
1.0
ug/L
11/08/17 16:20
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 16:20
1
1,1-Dichloroethene
8.8
1.0
ug/L
11/08/17 16:20
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 16:20
1
Ethylbenzene
2.6
1.0
ug/L
11/08/17 16:20
1
2-Hexanone
ND
10
ug/L
11/08/17 16:20
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 16:20
1
Methyl acetate
ND
5.0
ug/L
11/08/17 16:20
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 16:20
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 16:20
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 16:20
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 16:20
1
Styrene
ND
1.0
ug/L
11/08/17 16:20
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 16:20
1
Tetrachloroethene
45
1.0
ug/L
11/08/17 16:20
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 16:20
1
Toluene
110
1.0
ug/L
11/08/17 16:20
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 16:20
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 16:20
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 16:20
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 16:20
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 16:20
1
Trichloroethene
91
1.0
ug/L
11/08/17 16:20
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 16:20
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 16:20
1
Vinyl chloride
13
1.0
ug/L
11/08/17 16:20
1
Xylenes, Total
9.4
1.0
ug/L
11/08/17 16:20
1
a
F
TestArnerica Savannah
Page 81 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-DUP-4-102517 Lab Sample ID: 680-144889-35
Date Collected: 10/25/17 16:10 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 89 80-120 11108117 16:20 ,
Dibromofluoromethane (Surr) 102 80-122 11108117 16:20 1
1,2-Dichloroethane-d4 (Surr) 99 73-131 11108117 16:20 1
Toluene-d8 (Surr) 96 80-120 11108117 16:20 1
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TestArnerica Savannah
Page 82 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-EB-01-102417
Lab Sample ID: 680-144889-36
Date Collected: 10/24/17 15:32
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/03/17 17:52
1
Benzene
ND
1.0
ug/L
11/03/17 17:52
1
Bromodichloromethane
ND
1.0
ug/L
11/03/17 17:52
1
Bromoform
ND
1.0
ug/L
11/03/17 17:52
1
Bromomethane
ND
5.0
ug/L
11/03/17 17:52
1
2-Butanone
ND
10
ug/L
11/03/17 17:52
1
Carbon disulfide
ND
2.0
ug/L
11/03/17 17:52
1
Carbon tetrachloride
ND
1.0
ug/L
11/03/17 17:52
1
Chlorobenzene
ND
1.0
ug/L
11/03/17 17:52
1
Chloroethane
ND
5.0
ug/L
11/03/17 17:52
1
Chloroform
ND
1.0
ug/L
11/03/17 17:52
1
Chloromethane
ND
1.0
ug/L
11/03/17 17:52
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/03/17 17:52
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/03/17 17:52
1
Cyclohexane
ND
1.0
ug/L
11/03/17 17:52
1
Dibromochloromethane
ND
1.0
ug/L
11/03/17 17:52
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/03/17 17:52
1
1,2-Dibromoethane
ND
1.0
ug/L
11/03/17 17:52
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/03/17 17:52
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/03/17 17:52
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/03/17 17:52
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/03/17 17:52
1
1,1-Dichloroethane
ND
1.0
ug/L
11/03/17 17:52
1
1,2-Dichloroethane
ND
1.0
ug/L
11/03/17 17:52
1
1,1-Dichloroethene
ND
1.0
ug/L
11/03/17 17:52
1
1,2-Dichloropropane
ND
1.0
ug/L
11/03/17 17:52
1
Ethylbenzene
ND
1.0
ug/L
11/03/17 17:52
1
2-Hexanone
ND
10
ug/L
11/03/17 17:52
1
1 sopropyl benzene
ND
1.0
ug/L
11/03/17 17:52
1
Methyl acetate
ND
5.0
ug/L
11/03/17 17:52
1
Methylcyclohexane
ND
1.0
ug/L
11/03/17 17:52
1
Methylene Chloride
ND
5.0
ug/L
11/03/17 17:52
1
4-Methyl-2-pentanone
ND
10
ug/L
11/03/17 17:52
1
Methyl tert-butyl ether
ND
10
ug/L
11/03/17 17:52
1
Styrene
ND
1.0
ug/L
11/03/17 17:52
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/03/17 17:52
1
Tetrachloroethene
ND
1.0
ug/L
11/03/17 17:52
1
Tetrahydrofuran
ND
10
ug/L
11/03/17 17:52
1
Toluene
ND
1.0
ug/L
11/03/17 17:52
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/03/17 17:52
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/03/17 17:52
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/03/17 17:52
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/03/17 17:52
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/03/17 17:52
1
Trichloroethene
ND
1.0
ug/L
11/03/17 17:52
1
Trichlorofluoromethane
ND
1.0
ug/L
11/03/17 17:52
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/03/17 17:52
1
Vinyl chloride
ND
1.0
ug/L
11/03/17 17:52
1
Xylenes, Total
ND
1.0
ug/L
11/03/17 17:52
1
a
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TestArnerica Savannah
Page 83 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-EB-01-102417 Lab Sample ID: 680-144889-36
Date Collected: 10/24/17 15:32 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 92 80-120 11103117 17:52 ,
Dibromofluoromethane (Surr) 95 80-122 11103117 17:52 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11103117 17:52 1
Toluene-d8 (Surr) 104 80-120 11103117 17:52 1
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TestArnerica Savannah
Page 84 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-EB-02-102517
Lab Sample ID: 680-144889-37
Date Collected: 10/25/17 15:53
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/04/17 18:39
1
Benzene
ND
1.0
ug/L
11/04/17 18:39
1
Bromodichloromethane
ND
1.0
ug/L
11/04/17 18:39
1
Bromoform
ND
1.0
ug/L
11/04/17 18:39
1
Bromomethane
ND
5.0
ug/L
11/04/17 18:39
1
2-Butanone
ND
10
ug/L
11/04/17 18:39
1
Carbon disulfide
ND
2.0
ug/L
11/04/17 18:39
1
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 18:39
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 18:39
1
Chloroethane
ND
5.0
ug/L
11/04/17 18:39
1
Chloroform
ND
1.0
ug/L
11/04/17 18:39
1
Chloromethane
ND
1.0
ug/L
11/04/17 18:39
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 18:39
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 18:39
1
Cyclohexane
ND
1.0
ug/L
11/04/17 18:39
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 18:39
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 18:39
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 18:39
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 18:39
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 18:39
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 18:39
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 18:39
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 18:39
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 18:39
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 18:39
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 18:39
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 18:39
1
2-Hexanone
ND *
10
ug/L
11/04/17 18:39
1
1 sopropyl benzene
ND
1.0
ug/L
11/04/17 18:39
1
Methyl acetate
ND *
5.0
ug/L
11/04/17 18:39
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 18:39
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 18:39
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 18:39
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 18:39
1
Styrene
ND
1.0
ug/L
11/04/17 18:39
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 18:39
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 18:39
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 18:39
1
Toluene
ND
1.0
ug/L
11/04/17 18:39
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 18:39
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 18:39
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 18:39
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 18:39
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 18:39
1
Trichloroethene
ND
1.0
ug/L
11/04/17 18:39
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 18:39
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 18:39
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 18:39
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 18:39
1
a
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TestArnerica Savannah
Page 85 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-EB-02-102517 Lab Sample ID: 680-144889-37
Date Collected: 10/25/17 15:53 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 105 80-120 11104117 18:39 ,
Dibromofluoromethane (Surr) 102 80-122 11104117 18:39 1
1,2-Dichloroethane-d4 (Surr) 99 73-131 11104117 18:39 1
Toluene-d8 (Surr) 100 80-120 11104117 18:39 1
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Page 86 of 142 11/10/2017

Client Sample Results
Client: GHD Services Inc.
TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-EB-03-102617
Lab Sample ID: 680-144889-38
Date Collected: 10/26/17 16:40
Matrix:
Water
Date Received: 10/28/17 10:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 16:23
1
Benzene
ND
1.0
ug/L
11/05/17 16:23
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 16:23
1
Bromoform
ND
1.0
ug/L
11/05/17 16:23
1
Bromomethane
ND
5.0
ug/L
11/05/17 16:23
1
2-Butanone
ND
10
ug/L
11/05/17 16:23
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 16:23
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 16:23
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 16:23
1
Chloroethane
ND
5.0
ug/L
11/05/17 16:23
1
Chloroform
ND
1.0
ug/L
11/05/17 16:23
1
Chloromethane
ND
1.0
ug/L
11/05/17 16:23
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/05/17 16:23
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 16:23
1
Cyclohexane
ND
1.0
ug/L
11/05/17 16:23
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 16:23
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 16:23
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 16:23
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:23
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:23
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 16:23
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 16:23
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 16:23
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 16:23
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 16:23
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 16:23
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 16:23
1
2-Hexanone
ND *
10
ug/L
11/05/17 16:23
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 16:23
1
Methyl acetate
ND *
5.0
ug/L
11/05/17 16:23
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 16:23
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 16:23
1
4-Methyl-2-pentanone
ND *
10
ug/L
11/05/17 16:23
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 16:23
1
Styrene
ND
1.0
ug/L
11/05/17 16:23
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 16:23
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 16:23
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 16:23
1
Toluene
ND
1.0
ug/L
11/05/17 16:23
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 16:23
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 16:23
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 16:23
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 16:23
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 16:23
1
Trichloroethene
ND
1.0
ug/L
11/05/17 16:23
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 16:23
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 16:23
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 16:23
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 16:23
1
a
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TestArnerica Savannah
Page 87 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-EB-03-102617 Lab Sample ID: 680-144889-38
Date Collected: 10/26/17 16:40 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 119 80-120 11105117 16:23 ,
Dibromofluoromethane (Surr) 100 80-122 11105117 16:23 1
1,2-Dichloroethane-d4 (Surr) 93 73-131 11105117 16:23 1
Toluene-d8 (Surr) 114 80-120 11105117 16:23 1
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Page 88 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: J1155-EB-04-102717 Lab Sample ID: 680-144889-39
Date Collected: 10/27/17 13:55 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/07/17 21:19
1
Benzene
ND
1.0
ug/L
11/07/17 21:19
1
Bromodichloromethane
ND
1.0
ug/L
11/07/17 21:19
1
Bromoform
ND
1.0
ug/L
11/07/17 21:19
1
Bromomethane
ND
5.0
ug/L
11/07/17 21:19
1
2-Butanone
ND
10
ug/L
11/07/17 21:19
1
Carbon disulfide
ND
2.0
ug/L
11/07/17 21:19
1
Carbon tetrachloride
ND
1.0
ug/L
11/07/17 21:19
1
Chlorobenzene
ND
1.0
ug/L
11/07/17 21:19
1
Chloroethane
ND
5.0
ug/L
11/07/17 21:19
1
Chloroform
ND
1.0
ug/L
11/07/17 21:19
1
Chloromethane
ND
1.0
ug/L
11/07/17 21:19
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/07/17 21:19
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/07/17 21:19
1
Cyclohexane
ND
1.0
ug/L
11/07/17 21:19
1
Dibromochloromethane
ND
1.0
ug/L
11/07/17 21:19
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/07/17 21:19
1
1,2-Dibromoethane
ND
1.0
ug/L
11/07/17 21:19
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/07/17 21:19
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/07/17 21:19
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/07/17 21:19
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/07/17 21:19
1
1,1-Dichloroethane
ND
1.0
ug/L
11/07/17 21:19
1
1,2-Dichloroethane
ND
1.0
ug/L
11/07/17 21:19
1
1,1-Dichloroethene
ND
1.0
ug/L
11/07/17 21:19
1
1,2-Dichloropropane
ND
1.0
ug/L
11/07/17 21:19
1
Ethylbenzene
ND
1.0
ug/L
11/07/17 21:19
1
2-Hexanone
ND
10
ug/L
11/07/17 21:19
1
1 sopropyl benzene
ND
1.0
ug/L
11/07/17 21:19
1
Methyl acetate
ND
5.0
ug/L
11/07/17 21:19
1
Methylcyclohexane
ND
1.0
ug/L
11/07/17 21:19
1
Methylene Chloride
ND
5.0
ug/L
11/07/17 21:19
1
4-Methyl-2-pentanone
ND
10
ug/L
11/07/17 21:19
1
Methyl tert-butyl ether
ND
10
ug/L
11/07/17 21:19
1
Styrene
ND
1.0
ug/L
11/07/17 21:19
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/07/17 21:19
1
Tetrachloroethene
ND
1.0
ug/L
11/07/17 21:19
1
Tetrahydrofuran
ND
10
ug/L
11/07/17 21:19
1
Toluene
ND
1.0
ug/L
11/07/17 21:19
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/07/17 21:19
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/07/17 21:19
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/07/17 21:19
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/07/17 21:19
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/07/17 21:19
1
Trichloroethene
ND
1.0
ug/L
11/07/17 21:19
1
Trichlorofluoromethane
ND
1.0
ug/L
11/07/17 21:19
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/07/17 21:19
1
Vinyl chloride
ND
1.0
ug/L
11/07/17 21:19
1
Xylenes, Total
ND
1.0
ug/L
11/07/17 21:19
1
a
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TestArnerica Savannah
Page 89 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Client Sample ID: J1155-EB-04-102717 Lab Sample ID: 680-144889-39
Date Collected: 10/27/17 13:55 Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier Limits Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 87 80-120 11/07/17 21:19 ,
Dibromofluoromethane (Surr) 98 80-122 11/07/17 21:19 1
1,2-Dichloroethane-d4 (Surr) 91 73-131 11/07/17 21:19 1
Toluene-d8 (Surr) 100 80-120 11/07/17 21:19 1
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Page 90 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: A 155-TB-1 02417 Lab Sample ID: 680-144889-40
Date Collected: 10/24/17 08:00 Matrix: Water
Date Received: 10/28117 10:40
F
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/03/17 17:27
1
Benzene
ND
1.0
ug/L
11/03/17 17:27
1
Bromodichloromethane
ND
1.0
ug/L
11/03/17 17:27
1
Bromoform
ND
1.0
ug/L
11/03/17 17:27
1
Bromomethane
ND
5.0
ug/L
11/03/17 17:27
1
2-Butanone
ND
10
ug/L
11/03/17 17:27
1
Carbon disulfide
ND
2.0
ug/L
11/03/17 17:27
1
Carbon tetrachloride
ND
1.0
ug/L
11/03/17 17:27
1
Chlorobenzene
ND
1.0
ug/L
11/03/17 17:27
1
Chloroethane
ND
5.0
ug/L
11/03/17 17:27
1
Chloroform
ND
1.0
ug/L
11/03/17 17:27
1
Chloromethane
ND
1.0
ug/L
11/03/17 17:27
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/03/17 17:27
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/03/17 17:27
1
Cyclohexane
ND
1.0
ug/L
11/03/17 17:27
1
Dibromochloromethane
ND
1.0
ug/L
11/03/17 17:27
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/03/17 17:27
1
1,2-Dibromoethane
ND
1.0
ug/L
11/03/17 17:27
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/03/17 17:27
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/03/17 17:27
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/03/17 17:27
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/03/17 17:27
1
1,1-Dichloroethane
ND
1.0
ug/L
11/03/17 17:27
1
1,2-Dichloroethane
ND
1.0
ug/L
11/03/17 17:27
1
1,1-Dichloroethene
ND
1.0
ug/L
11/03/17 17:27
1
1,2-Dichloropropane
ND
1.0
ug/L
11/03/17 17:27
1
Ethylbenzene
ND
1.0
ug/L
11/03/17 17:27
1
2-Hexanone
ND
10
ug/L
11/03/17 17:27
1
1 sopropyl benzene
ND
1.0
ug/L
11/03/17 17:27
1
Methyl acetate
ND
5.0
ug/L
11/03/17 17:27
1
Methylcyclohexane
ND
1.0
ug/L
11/03/17 17:27
1
Methylene Chloride
ND
5.0
ug/L
11/03/17 17:27
1
4-Methyl-2-pentanone
ND
10
ug/L
11/03/17 17:27
1
Methyl tert-butyl ether
ND
10
ug/L
11/03/17 17:27
1
Styrene
ND
1.0
ug/L
11/03/17 17:27
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/03/17 17:27
1
Tetrachloroethene
ND
1.0
ug/L
11/03/17 17:27
1
Tetrahydrofuran
ND
10
ug/L
11/03/17 17:27
1
Toluene
ND
1.0
ug/L
11/03/17 17:27
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/03/17 17:27
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/03/17 17:27
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/03/17 17:27
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/03/17 17:27
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/03/17 17:27
1
Trichloroethene
ND
1.0
ug/L
11/03/17 17:27
1
Trichlorofluoromethane
ND
1.0
ug/L
11/03/17 17:27
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/03/17 17:27
1
Vinyl chloride
ND
1.0
ug/L
11/03/17 17:27
1
Xylenes, Total
ND
1.0
ug/L
11/03/17 17:27
1
a
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TestArnerica Savannah
Page 91 of 142 11/10/2017

Client Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: A 155-TB-1 02417
Lab Sample ID: 680-144889-40
Date Collected: 10/24/17 08:00
Matrix: Water
Date Received: 10/28/17 10:40
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed DY Fac
4-Bromofluorobenzene (Surr) 91
80-120
11103117 17:27 ,
Dibromofluoromethane (Surr) 98
80-122
11103117 17:27 1
1,2-Dichloroethane-d4 (Surr) 96
73-131
11103117 17:27 1
Toluene-d8 (Surr) 102
80-120
11103117 17:27 1
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Page 92 of 142 11/10/2017

Surrogate Summary
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS)
Matrix: Water
Lab Sample ID
680-144889-1
680-144889-2
680-144889-3
680-144889-4
680-144889-5
680-144889-6
680-144889-7
680-144889-8
680-144889-9
680-144889-10
680-144889-10 - DL
680-144889-11
680-144889-11
680-144889-12
680-144889-13
680-144889-14
680-144889-15
680-144889-16
680-144889-17
680-144889-18
680-144889-19
680-144889-20
680-144889-21
680-144889-22
680-144889-23
680-144889-24
680-144889-25
680-144889-26
680-144889-27
680-144889-28
680-144889-29
680-144889-30
680-144889-31
680-144889-31 - DL
680-144889-32
680-144889-33
680-144889-34
680-144889-35
680-144889-36
680-144889-37
680-144889-38
680-144889-39
680-144889-40
LCS 680-501188/4
LCS 680-501326/6
LCS 680-501355/3
LCS 680-501359/3
LCS 680-501395/3
LCS 680-501564/4
Client Sample ID
Jl 155-MW-10-102417
Jl 155-MW-1 1-102417
J 1 155-MW-1 3-102417
J 1 155-MW-1 7-102417
Jl 155-MW-20-102417
Jl 155-MW-28-102417
Jl 155-MW-33-102517
Jl 155-MW-34-102517
Jl 155-MW-35-102417
J I 155-MW-36-102517
J I 155-MW-36-102517
J I 155-MW-40-102517
J I 155-MW-40-102517
J I 155-MW-41-102517
J I 155-MW-42-102417
Jl 155-MW-43-102417
Jl 155-MW-45-102417
Jl 155-MW-47-102517
Jl 155-MW-60-102517
Jl 155-MW-61-102517
Jl 155-MW-62-102517
Jl 155-MW-63-102717
J 1 155-PW-1 6-102717
Jl 155-SP-26-102717
J I 155-CMP-1-102717
JI 155-CMP-3-102717
JI 155-CMP-4-102717
Jl 155-SW-3-102717
Jl 155-SW-6-102717
Jl 155-SW-10-1 02717
Jl 155-RW-2-102617
Jl 155-RW-3-102617
Jl 155-RW-5-102617
Jl 155-RW-5-102617
Jl 155-DUP-1-1 02417
Jl 155-DUP-2-102417
Jl 155-DUP-3-102517
Jl 155-DUP-4-102517
Jl 155-EB-01-1 02417
JI 155-EB-02-102517
Jl 155-EB-03-102617
JI 155-EB-04-102717
Jl 155-TB-1 02417
Lab Control Sample
Lab Control Sample
Lab Control Sample
Lab Control Sample
Lab Control Sample
Lab Control Sample
TestArnerica Job ID: 680-144889-1
Prep Type: Total/NA
BFB
(80-120)
Percent Surrogate Recovery (Acceptance Limits)
DBFM 12DCE TOL
(80-122) (73-131) (80-120)
89
96
96
104
89
96
94
102
87
91
91
101
91
94
93
102
104
112
112
ill
108
115
116
ill
105
104
102
101
103
103
96
102
101
122
119
115
115
106
100
105
116
109
105
108
113
106
101
113
107
ill
110
112
89
101
110
91
107
107
109
110
115
113
107
109
104
115
114
ill
88
93
91
101
116
98
96
100
116
106
96
110
105
97
95
105
87
97
92
100
88
99
93
99
88
97
93
99
88
97
93
99
88
98
93
100
89
98
92
101
88
99
93
98
88
99
93
99
107
104
106
108
116
100
94
101
107
104
98
116
90
102
102
100
106
105
105
107
95
110
118
101
108
107
ill
107
106
91
89
106
89
102
99
96
92
95
93
104
105
102
99
100
119
100
93
114
87
98
91
100
91
98
96
102
84
97
94
99
113
105
95
108
ill
108
116
104
118
105
104
115
ill
110
117
109
89
102
95
100
Page 93 of 142
TestArnerica Savannah
11/10/2017

Surrogate Summary
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Matrix: Water Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
Lab Sample ID
Client Sample ID
BFIB
(80-120)
DlBFM
(80-122)
12DCE
(73-131)
TOL
(80-120)
LCS 680-501694/3
Lab Control Sample
89
101
93
99
LCS 680-501727/4
Lab Control Sample
85
98
95
97
LCS 680-501730/3
Lab Control Sample
105
114
116
115
LCS 680-501749/4
Lab Control Sample
90
103
95
100
LCS 680-501874/3
Lab Control Sample
105
110
ill
109
LCSD 680-501188/5
Lab Control Sample Dup
83
99
95
98
LCSD 680-501326/7
Lab Control Sample Dup
100
97
90
103
LCSD 680-501355/4
Lab Control Sample Dup
ill
104
105
ill
LCSD 680-501359/4
Lab Control Sample Dup
98
98
99
100
LCSD 680-501395/4
Lab Control Sample Dup
102
129 X
125
106
LCSD 680-501564/5
Lab Control Sample Dup
85
100
96
97
LCSD 680-501694/4
Lab Control Sample Dup
88
102
93
99
LCSD 680-501727/5
Lab Control Sample Dup
85
97
92
98
LCSD 680-501730/4
Lab Control Sample Dup
107
108
103
110
LCSD 680-501749/5
Lab Control Sample Dup
86
100
93
96
LCSD 680-501874/4
Lab Control Sample Dup
106
118
108
106
MB 680-501188/9
Method Blank
90
94
91
104
MB 680-501326/11
Method Blank
107
100
102
117
MB 680-501355/8
Method Blank
102
100
101
110
MB 680-501359/9
Method Blank
106
100
98
112
MB 680-501395/8
Method Blank
105
108
104
ill
MB 680-501564/9
Method Blank
89
92
91
101
MB 680-501694/9
Method Blank
88
96
91
99
MB 680-501727/9
Method Blank
88
95
92
102
MB 680-501730/8
Method Blank
112
109
105
114
MB 680-501749/9
Method Blank
88
97
91
98
MB 680-501874/8
Method Blank
104
103
102
108
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr)
DBFM Dibromofluoromethane (Surr)
12DCE 1,2-Dichloroethane-d4 (Surr)
TOL = Toluene-d8 (Surr)
TestArnerica Savannah
Page 94 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 680-501188/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501188
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
N D
-
10
d9-/ -L
11/03/17 12:55
1
Benzene
N D
1.0
ug/L
11/03/17 12:55
1
Bromodichloromethane
N D
1.0
ug/L
11/03/17 12:55
1
Bromoform
N D
1.0
ug/L
11/03/17 12:55
1
Bromomethane
N D
5.0
ug/L
11/03/17 12:55
1
2-Butanone
N D
10
ug/L
11/03/17 12:55
1
Carbon disulfide
ND
2.0
ug/L
11/03/17 12:55
1
Carbon tetrachloride
ND
1.0
ug/L
11/03/17 12:55
1
Chlorobenzene
ND
1.0
ug/L
11/03/17 12:55
1
Chloroethane
ND
5.0
ug/L
11/03/17 12:55
1
Chloroform
ND
1.0
ug/L
11/03/17 12:55
1
Chloromethane
ND
1.0
ug/L
11/03/17 12:55
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/03/17 12:55
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/03/17 12:55
1
Cyclohexane
ND
1.0
ug/L
11/03/17 12:55
1
Dibromochloromethane
ND
1.0
ug/L
11/03/17 12:55
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/03/17 12:55
1
1,2-Dibromoethane
ND
1.0
ug/L
11/03/17 12:55
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/03/17 12:55
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/03/17 12:55
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/03/17 12:55
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/03/17 12:55
1
1,1-Dichloroethane
ND
1.0
ug/L
11/03/17 12:55
1
1,2-Dichloroethane
ND
1.0
ug/L
11/03/17 12:55
1
1,1-Dichloroethene
ND
1.0
ug/L
11/03/17 12:55
1
1,2-Dichloropropane
ND
1.0
ug/L
11/03/17 12:55
1
Ethylbenzene
ND
1.0
ug/L
11/03/17 12:55
1
2-Hexanone
ND
10
ug/L
11/03/17 12:55
1
1 sopropyl benzene
ND
1.0
ug/L
11/03/17 12:55
1
Methyl acetate
ND
5.0
ug/L
11/03/17 12:55
1
Methylcyclohexane
ND
1.0
ug/L
11/03/17 12:55
1
Methylene Chloride
ND
5.0
ug/L
11/03/17 12:55
1
4-Methyl-2-pentanone
ND
10
ug/L
11/03/17 12:55
1
Methyl tert-butyl ether
ND
10
ug/L
11/03/17 12:55
1
Styrene
ND
1.0
ug/L
11/03/17 12:55
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/03/17 12:55
1
Tetrachloroethene
ND
1.0
ug/L
11/03/17 12:55
1
Tetrahydrofuran
ND
10
ug/L
11/03/17 12:55
1
Toluene
ND
1.0
ug/L
11/03/17 12:55
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/03/17 12:55
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/03/17 12:55
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/03/17 12:55
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/03/17 12:55
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/03/17 12:55
1
Trichloroethene
ND
1.0
ug/L
11/03/17 12:55
1
Trichlorofluoromethane
ND
1.0
ug/L
11/03/17 12:55
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/03/17 12:55
1
Vinyl chloride
ND
1.0
ug/L
11/03/17 12:55
1
TestArnerica Savannah
Page 95 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50118819
Matrix: Water
Analysis Batch: 501188
Analyte
MB
Result
MB
Qualifier
RL MDL Unit
Xylenes, Total
ND
1.0 ug/L
MB
MB
Surrogate %Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr)
90
80-120
Dibromofluoromethane (Surr)
94
80-122
1,2-Dichloroethane-d4 (Surr)
91
73-131
Toluene-d8 (Surr)
104
80-120
Lab Sample ID: LCS 680-501188/4
Matrix: Water
Analysis Batch: 501188
F
TestArnerica Job ID: 680-144889-1
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
11/03/17 12:55 1
Prepared Analyzed Dil Fac
11103117 12:55
11103117 12:55 1
11103117 12:55
1
11103117 12:55
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Acetone
250
286
ug/L
115
68-132
Benzene
50.0
51.8
ug/L
104
80-120
Bromodichloromethane
50.0
51.5
ug/L
103
80-120
Bromoform
50.0
49.4
ug/L
99
52-122
Bromomethane
50.0
53.7
ug/L
107
43-146
2-Butanone
250
305
ug/L
122
79-125
Carbon disulfide
50.0
47.6
ug/L
95
77-129
Carbon tetrachloride
50.0
45.1
ug/L
90
67-125
Chlorobenzene
50.0
51.6
ug/L
103
80-120
Chloroethane
50.0
54.4
ug/L
109
48-145
Chloroform
50.0
48.4
ug/L
97
80-120
Chloromethane
50.0
40.7
ug/L
81
76-149
cis- 1,2-Dichloroethene
50.0
47.7
ug/L
95
80-120
cis- 1,3-Dichloropropene
50.0
52.4
ug/L
105
80-129
Cyclohexane
50.0
49.5
ug/L
99
80-132
Dibromochloromethane
50.0
51.6
ug/L
103
68-120
1,2-Dibromo-3-Chloropropane
50.0
48.2
ug/L
96
74-120
1,2-Dibromoethane
50.0
51.3
ug/L
103
75-126
1,2-Dichlorobenzene
50.0
48.6
ug/L
97
80-120
1,3-Dichlorobenzene
50.0
48.3
ug/L
97
80-120
1,4-Dichlorobenzene
50.0
48.0
ug/L
96
80-120
Dichlorodifluoromethane
50.0
39.5
ug/L
79
70-137
1,1-Dichloroethane
50.0
48.2
ug/L
96
80-120
1,2-Dichloroethane
50.0
50.4
ug/L
101
72-128
1,1-Dichloroethene
50.0
46.8
ug/L
94
80-120
1,2-Dichloropropane
50.0
53.5
ug/L
107
80-120
Ethylbenzene
50.0
50.8
ug/L
102
80-120
2-Hexanone
250
256
ug/L
102
80-131
1 sopropyl benzene
50.0
51.6
ug/L
103
79-126
Methyl acetate
250
235
ug/L
94
73-139
Methylcyclohexane
50.0
55.2
ug/L
110
80-138
Methylene Chloride
50.0
51.9
ug/L
104
80-120
4-Methyl-2-pentanone
250
256
ug/L
102
80-134
Methyl tert-butyl ether
50.0
52.4
ug/L
105
80-122
Styrene
50.0
55.2
ug/L
110
80-126
TestArnerica Savannah
Page 96 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501188/4
Matrix: Water
Analysis Batch: 501188
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
1,1,2,2-Tetrachloroethane
50.0
56.1
ug/L
112
76-126
Tetrachloroethene
50.0
51.9
ug/L
104
71-123
Tetrahydrofuran
100
94.0
ug/L
94
70-133
Toluene
50.0
52.5
ug/L
105
80-120
trans- 1,2-Dich loroethene
50.0
50.3
ug/L
101
80-120
trans- 1, 3-Dich loropropene
50.0
51.8
ug/L
104
80-128
1,2,4-Trichlorobenzene
50.0
51.3
ug/L
103
71-126
1,1,1-Trichloroethane
50.0
45.8
ug/L
92
80-120
1,1,2-Trichloroethane
50.0
54.2
ug/L
108
80-120
Trichloroethene
50.0
48.9
ug/L
98
80-120
Trichlorofluoromethane
50.0
48.2
ug/L
96
58-127
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
47.8
ug/L
96
75-128
ne
Vinyl chloride
50.0
45.4
ug/L
91
80-129
Xylenes, Total
100
102
ug/L
102
80-120
LCS LCS
Surrogate
%Recovety Qualifier
Limits
4-Bromofluorobenzene (Surr)
84
80-120
Dibromofluoromethane (Surr)
97
80-122
1,2-Dichloroethane-d4 (Surr)
94
73-131
Toluene-d8 (Surr)
99
80-120
Lab Sample ID: LCSID 680-501188/5
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501188
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
Acetone
250
300
ug/L
120
68-132
5
30
Benzene
50.0
51.3
ug/L
103
80-120
1
20
Bromodichloromethane
50.0
51.8
ug/L
104
80-120
1
20
Bromoform
50.0
51.4
ug/L
103
52-122
4
20
Bromomethane
50.0
54.3
ug/L
109
43-146
1
20
2-Butanone
250
311
ug/L
124
79-125
2
20
Carbon disulfide
50.0
46.3
ug/L
93
77-129
3
20
Carbon tetrachloride
50.0
44.8
ug/L
90
67-125
1
20
Chlorobenzene
50.0
52.5
ug/L
105
80-120
2
20
Chloroethane
50.0
52.9
ug/L
106
48-145
3
20
Chloroform
50.0
49.4
ug/L
99
80-120
2
20
Chloromethane
50.0
39.4
ug/L
79
76-149
3
30
cis- 1,2-Dichloroethene
50.0
47.7
ug/L
95
80-120
0
20
cis- 1,3-Dichloropropene
50.0
52.8
ug/L
106
80-129
1
20
Cyclohexane
50.0
47.4
ug/L
95
80-132
4
20
Dibromochloromethane
50.0
52.1
ug/L
104
68-120
1
20
1,2-Dibromo-3-Chloropropane
50.0
51.8
ug/L
104
74-120
7
20
1,2-Dibromoethane
50.0
53.4
ug/L
107
75-126
4
20
1,2-Dichlorobenzene
50.0
48.8
ug/L
98
80-120
1
20
1,3-Dichlorobenzene
50.0
48.5
ug/L
97
80-120
0
20
1,4-Dichlorobenzene
50.0
48.6
ug/L
97
80-120
1
20
TestArnerica Savannah
Page 97 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501188/5
Matrix: Water
Analysis Batch: 501188
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Dichlorodifluoromethane
50.0
38.0
ug/L
76
70-137
4
40
1,1-Dichloroethane
50.0
48.0
ug/L
96
80-120
0
20
1,2-Dichloroethane
50.0
51.0
ug/L
102
72-128
1
50
1,1-Dichloroethene
50.0
46.3
ug/L
93
80-120
1
20
1,2-Dichloropropane
50.0
53.7
ug/L
107
80-120
0
20
Ethylbenzene
50.0
50.7
ug/L
101
80-120
0
20
2-Hexanone
250
263
ug/L
105
80-131
3
20
1 sopropyl benzene
50.0
51.5
ug/L
103
79-126
0
20
Methyl acetate
250
246
ug/L
98
73-139
4
20
Methylcyclohexane
50.0
52.2
ug/L
104
80-138
6
20
Methylene Chloride
50.0
53.7
ug/L
107
80-120
3
20
4-Methyl-2-pentanone
250
261
ug/L
104
80-134
2
20
Methyl tert-butyl ether
50.0
54.4
ug/L
109
80-122
4
20
Styrene
50.0
55.2
ug/L
110
80-126
0
20
1,1,2,2-Tetrachloroethane
50.0
56.6
ug/L
113
76-126
1
20
Tetrachloroethene
50.0
50.7
ug/L
101
71-123
2
20
Tetrahydrofuran
100
98.0
ug/L
98
70-133
4
30
Toluene
50.0
51.9
ug/L
104
80-120
1
20
trans- 1,2-Dich loroethene
50.0
49.9
ug/L
100
80-120
1
20
trans- 1, 3-Dich loropropene
50.0
52.5
ug/L
105
80-128
1
30
1,2,4-Trichlorobenzene
50.0
52.2
ug/L
104
71-126
2
20
1,1,1-Trichloroethane
50.0
45.3
ug/L
91
80-120
1
20
1,1,2-Trichloroethane
50.0
55.6
ug/L
111
80-120
2
20
Trichloroethene
50.0
48.1
ug/L
96
80-120
2
20
Trichlorofluoromethane
50.0
46.5
ug/L
93
58-127
4
20
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
46.4
ug/L
93
75-128
3
20
ne
Vinyl chloride
50.0
43.9
ug/L
88
80-129
3
20
Xylenes, Total
100
102
ug/L
102
80-120
1
20
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
83
80-120
Dibromofluoromethane (Surr)
99
80-122
1,2-Dichloroethane-d4 (Surr)
95
73-131
Toluene-d8 (Surr)
98
80-120
Lab Sample ID: MB 680-501326/11
Matrix: Water
Analysis Batch: 501326
Analyte
MB MB
Result Qualifier
Acetone
ND
Benzene
ND
Bromodichloromethane
ND
Brornoform
ND
Brornornethane
ND
2-Butanone
ND
Carbon disulfide
ND
RL
MDL Unit D
10
ug/L
1.0
ug/L
1.0
ug/L
1.0
ug/L
5.0
ug/L
10
ug/L
2.0
ug/L
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed
Dil Fac
11/04/17 14:57
1
11/04/17 14:57
1
11/04/17 14:57
1
11/04/17 14:57
1
11/04/17 14:57
1
11/04/17 14:57
1
11/04/17 14:57
1
Page 98 of 142
TestArnerica Savannah
11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-501326/11
Matrix: Water
Analysis Batch: 501326
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
Carbon tetrachloride
ND
1.0
ug/L
11/04/17 14:57
1
Chlorobenzene
ND
1.0
ug/L
11/04/17 14:57
1
Chloroethane
ND
5.0
ug/L
11/04/17 14:57
1
Chloroform
ND
1.0
ug/L
11/04/17 14:57
1
Chloromethane
ND
1.0
ug/L
11/04/17 14:57
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/04/17 14:57
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/04/17 14:57
1
Cyclohexane
ND
1.0
ug/L
11/04/17 14:57
1
Dibromochloromethane
ND
1.0
ug/L
11/04/17 14:57
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/04/17 14:57
1
1,2-Dibromoethane
ND
1.0
ug/L
11/04/17 14:57
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/04/17 14:57
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/04/17 14:57
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/04/17 14:57
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/04/17 14:57
1
1,1-Dichloroethane
ND
1.0
ug/L
11/04/17 14:57
1
1,2-Dichloroethane
ND
1.0
ug/L
11/04/17 14:57
1
1,1-Dichloroethene
ND
1.0
ug/L
11/04/17 14:57
1
1,2-Dichloropropane
ND
1.0
ug/L
11/04/17 14:57
1
Ethylbenzene
ND
1.0
ug/L
11/04/17 14:57
1
2-Hexanone
ND
10
ug/L
11/04/17 14:57
1
Isopropylbenzene
ND
1.0
ug/L
11/04/17 14:57
1
Methyl acetate
ND
5.0
ug/L
11/04/17 14:57
1
Methylcyclohexane
ND
1.0
ug/L
11/04/17 14:57
1
Methylene Chloride
ND
5.0
ug/L
11/04/17 14:57
1
4-Methyl-2-pentanone
ND
10
ug/L
11/04/17 14:57
1
Methyl tert-butyl ether
ND
10
ug/L
11/04/17 14:57
1
Styrene
ND
1.0
ug/L
11/04/17 14:57
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/04/17 14:57
1
Tetrachloroethene
ND
1.0
ug/L
11/04/17 14:57
1
Tetrahydrofuran
ND
10
ug/L
11/04/17 14:57
1
Toluene
ND
1.0
ug/L
11/04/17 14:57
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/04/17 14:57
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/04/17 14:57
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/04/17 14:57
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/04/17 14:57
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/04/17 14:57
1
Trichloroethene
ND
1.0
ug/L
11/04/17 14:57
1
Trichlorofluoromethane
ND
1.0
ug/L
11/04/17 14:57
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/04/17 14:57
1
Vinyl chloride
ND
1.0
ug/L
11/04/17 14:57
1
Xylenes, Total
ND
1.0
ug/L
11/04/17 14:57
1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
107
80-120
11104117 14:57
1
Dibromofluoromethane (Surr)
100
80-122
11104117 14:57
1
1,2-Dichloroethane-d4 (Surr)
102
73-131
11104117 14:57
1
Toluene-d8 (Surr)
117
80-120
11104117 14:57
1
TestArnerica Savannah
Page 99 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Lab Sample ID: LCS 680-501326/6
Matrix: Water
Analysis Batch: 501326
Analyte
Spike
Added
LCS LCS
Result Qualifier
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
Unit D %Rec Limits
Acetone
250
206
ug/L
82
68-132
Benzene
50.0
52.3
ug/L
105
80-120
Bromodichloromethane
50.0
47.5
ug/L
95
80-120
Bromoform
50.0
37.3
ug/L
75
52-122
Bromomethane
50.0
56.1
ug/L
112
43-146
2-Butanone
250
214
ug/L
86
79-125
Carbon disulfide
50.0
54.7
ug/L
109
77-129
Carbon tetrachloride
50.0
52.5
ug/L
105
67-125
Chlorobenzene
50.0
49.6
ug/L
99
80-120
Chloroethane
50.0
63.4
ug/L
127
48-145
Chloroform
50.0
53.3
ug/L
107
80-120
Chloromethane
50.0
59.3
ug/L
119
76-149
cis- 1,2-Dichloroethene
50.0
54.3
ug/L
109
80-120
cis- 1,3-Dichloropropene
50.0
53.0
ug/L
106
80-129
Cyclohexane
50.0
54.2
ug/L
108
80-132
Dibromochloromethane
50.0
43.2
ug/L
86
68-120
1,2-Dibromo-3-Chloropropane
50.0
37.3
ug/L
75
74-120
1,2-Dibromoethane
50.0
47.6
ug/L
95
75-126
1,2-Dichlorobenzene
50.0
50.9
ug/L
102
80-120
1,3-Dichlorobenzene
50.0
53.0
ug/L
106
80-120
1,4-Dichlorobenzene
50.0
51.4
ug/L
103
80-120
Dichlorodifluoromethane
50.0
67.9
ug/L
136
70-137
1,1-Dichloroethane
50.0
52.8
ug/L
106
80-120
1,2-Dichloroethane
50.0
48.7
ug/L
97
72-128
1,1-Dichloroethene
50.0
49.8
ug/L
100
80-120
1,2-Dichloropropane
50.0
47.8
ug/L
96
80-120
Ethylbenzene
50.0
53.8
ug/L
108
80-120
2-Hexanone
250
210
ug/L
84
80-131
1 sopropyl benzene
50.0
55.1
ug/L
110
79-126
Methyl acetate
250
157
ug/L
63
73-139
Methylcyclohexane
50.0
62.6
ug/L
125
80-138
Methylene Chloride
50.0
53.6
ug/L
107
80-120
4-Methyl-2-pentanone
250
206
ug/L
83
80-134
Methyl tert-butyl ether
50.0
46.4
ug/L
93
80-122
Styrene
50.0
53.1
ug/L
106
80-126
1,1,2,2-Tetrachloroethane
50.0
37.8
ug/L
76
76-126
Tetrachloroethene
50.0
57.7
ug/L
115
71-123
Tetrahydrofuran
100
74.8
ug/L
75
70-133
Toluene
50.0
53.6
ug/L
107
80-120
trans- 1,2-Dich loroethene
50.0
51.2
ug/L
102
80-120
trans- 1, 3-Dich loropropene
50.0
54.6
ug/L
109
80-128
1,2,4-Trichlorobenzene
50.0
43.1
ug/L
86
71-126
1,1,1-Trichloroethane
50.0
59.6
ug/L
119
80-120
1,1,2-Trichloroethane
50.0
50.5
ug/L
101
80-120
Trichloroethene
50.0
53.5
ug/L
107
80-120
Trichlorofluoromethane
50.0
57.2
ug/L
114
58-127
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
50.6
ug/L
101
75-128
ne
Vinyl chloride
50.0
61.3
ug/L
123
80-129
Xylenes, Total
100
110
ug/L
110
80-120
TestArnerica Savannah
Page 100 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501326/6 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501326
LCS LCS
Surrogate %Recovety Qualifier Limits
4-Bromofluorobenzene (Surr) 113 80-120
Dibromofluoromethane (Surr) 105 80-122
1,2-Dichloroethane-d4 (Surr) 95 73-131
Toluene-d8 (Surr) 108 80-120
Lab Sample ID: LCSID 680-501326/7 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501326
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Acetone
250
196
ug/L
78
68-132
5
30
Benzene
50.0
49.6
ug/L
99
80-120
5
20
Bromodichloromethane
50.0
49.0
ug/L
98
80-120
3
20
Bromoform
50.0
40.6
ug/L
81
52-122
8
20
Bromomethane
50.0
47.9
ug/L
96
43-146
16
20
2-Butanone
250
197
ug/L
79
79-125
8
20
Carbon disulfide
50.0
52.1
ug/L
104
77-129
5
20
Carbon tetrachloride
50.0
48.0
ug/L
96
67-125
9
20
Chlorobenzene
50.0
52.2
ug/L
104
80-120
5
20
Chloroethane
50.0
58.6
ug/L
117
48-145
8
20
Chloroform
50.0
48.4
ug/L
97
80-120
10
20
Chloromethane
50.0
56.2
ug/L
112
76-149
5
30
cis- 1,2-Dichloroethene
50.0
49.7
ug/L
99
80-120
9
20
cis- 1,3-Dichloropropene
50.0
53.4
ug/L
107
80-129
1
20
Cyclohexane
50.0
48.7
ug/L
97
80-132
11
20
Dibromochloromethane
50.0
40.4
ug/L
81
68-120
7
20
1,2-Dibromo-3-Chloropropane
50.0
37.9
ug/L
76
74-120
1
20
1,2-Dibromoethane
50.0
44.6
ug/L
89
75-126
6
20
1,2-Dichlorobenzene
50.0
50.9
ug/L
102
80-120
0
20
1,3-Dichlorobenzene
50.0
53.5
ug/L
107
80-120
1
20
1,4-Dichlorobenzene
50.0
51.7
ug/L
103
80-120
1
20
Dichlorodifluoromethane
50.0
62.5
ug/L
125
70-137
8
40
1,1-Dichloroethane
50.0
47.8
ug/L
96
80-120
10
20
1,2-Dichloroethane
50.0
47.0
ug/L
94
72-128
3
50
1,1-Dichloroethene
50.0
47.0
ug/L
94
80-120
6
20
1,2-Dichloropropane
50.0
46.5
ug/L
93
80-120
3
20
Ethylbenzene
50.0
55.2
ug/L
110
80-120
3
20
2-Hexanone
250
194 *
ug/L
78
80-131
8
20
1 sopropyl benzene
50.0
57.7
ug/L
115
79-126
5
20
Methyl acetate
250
152 *
ug/L
61
73-139
3
20
Methylcyclohexane
50.0
61.0
ug/L
122
80-138
3
20
Methylene Chloride
50.0
50.8
ug/L
102
80-120
5
20
4-Methyl-2-pentanone
250
201
ug/L
80
80-134
3
20
Methyl tert-butyl ether
50.0
44.6
ug/L
89
80-122
4
20
Styrene
50.0
54.3
ug/L
109
80-126
2
20
1,1,2,2-Tetrachloroethane
50.0
45.0
ug/L
90
76-126
17
20
Tetrachloroethene
50.0
52.5
ug/L
105
71-123
10
20
Tetrahydrofuran
100
68.9
ug/L
69
70-133
8
30
TestArnerica Savannah
Page 101 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501326/7 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501326
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Toluene
50.0
50.8
ug/L
102
80-120 5
20
trans- 1,2-Dich loroethene
50.0
48.3
ug/L
97
80-120 6
20
trans- 1, 3-Dich loropropene
50.0
48.9
ug/L
98
80-128 11
30
1,2,4-Trichlorobenzene
50.0
43.7
ug/L
87
71-126 1
20
1,1,1-Trichloroethane
50.0
53.1
ug/L
106
80-120 12
20
1,1,2-Trichloroethane
50.0
46.1
ug/L
92
80-120 9
20
Trichloroethene
50.0
52.9
ug/L
106
80-120 1
20
Trichlorofluoromethane
50.0
53.8
ug/L
108
58-127 6
20
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
48.9
ug/L
98
75-128 4
20
ne
Vinyl chloride
50.0
56.3
ug/L
113
80-129 8
20
Xylenes, Total
100
ill
ug/L
111
80-120 1
20
LCSD
LCSD
Surrogate %Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr) 100
80-120
Dibromofluoromethane (Surr) 97
80-122
1,2-Dichloroethane-d4 (Surr) 90
73-131
Toluene-d8 (Surr) 103
80-120
Lab Sample ID: MB 680-501355/8
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501355
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 14:02
1
Benzene
ND
1.0
ug/L
11/05/17 14:02
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 14:02
1
Bromoform
ND
1.0
ug/L
11/05/17 14:02
1
Bromomethane
ND
5.0
ug/L
11/05/17 14:02
1
2-Butanone
ND
10
ug/L
11/05/17 14:02
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 14:02
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 14:02
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 14:02
1
Chloroethane
ND
5.0
ug/L
11/05/17 14:02
1
Chloroform
ND
1.0
ug/L
11/05/17 14:02
1
Chloromethane
ND
1.0
ug/L
11/05/17 14:02
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/05/17 14:02
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 14:02
1
Cyclohexane
ND
1.0
ug/L
11/05/17 14:02
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 14:02
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 14:02
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 14:02
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 14:02
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 14:02
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 14:02
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 14:02
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 14:02
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 14:02
1
TestArnerica Savannah
Page 102 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50135518
Matrix: Water
Analysis Batch: 501355
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 14:02
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 14:02
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 14:02
1
2-Hexanone
ND
10
ug/L
11/05/17 14:02
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 14:02
1
Methyl acetate
ND
5.0
ug/L
11/05/17 14:02
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 14:02
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 14:02
1
4-Methyl-2-pentanone
ND
10
ug/L
11/05/17 14:02
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 14:02
1
Styrene
ND
1.0
ug/L
11/05/17 14:02
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 14:02
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 14:02
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 14:02
1
Toluene
ND
1.0
ug/L
11/05/17 14:02
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 14:02
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 14:02
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 14:02
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 14:02
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 14:02
1
Trichloroethene
ND
1.0
ug/L
11/05/17 14:02
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 14:02
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 14:02
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 14:02
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 14:02
1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
102
80-120
11105117 14:02
1
Dibromofluoromethane (Surr)
100
80-122
11105117 14:02
1
1,2-Dichloroethane-d4 (Surr)
101
73-131
11105117 14:02
1
Toluene-d8 (Surr)
110
80-120
11105117 14:02
1
Lab Sample ID: LCS 680-501355/3
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501355
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Acetone
250
274
ug/L
110
68-132
Benzene
50.0
55.1
ug/L
110
80-120
Bromodichloromethane
50.0
55.9
ug/L
112
80-120
Bromoform
50.0
47.0
ug/L
94
52-122
Bromomethane
50.0
43.5
ug/L
87
43-146
2-Butanone
250
287
ug/L
115
79-125
Carbon disulfide
50.0
55.1
ug/L
110
77-129
Carbon tetrachloride
50.0
56.1
ug/L
112
67-125
Chlorobenzene
50.0
46.7
ug/L
93
80-120
Chloroethane
50.0
49.5
ug/L
99
48-145
Chloroform
50.0
57.1
ug/L
114
80-120
TestArnerica Savannah
Page 103 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501355/3 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501355
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Chloromethane
50.0
51.1
ug/L
102
76-149
cis- 1,2-Dichloroethene
50.0
55.8
ug/L
112
80-120
cis- 1,3-Dichloropropene
50.0
51.5
ug/L
103
80-129
Cyclohexane
50.0
50.5
ug/L
101
80-132
Dibrornochloromethane
50.0
57.9
ug/L
116
68-120
1,2-Dibromo-3-Chloropropane
50.0
53.5
ug/L
107
74-120
1,2-Dibromoethane
50.0
56.3
ug/L
113
75-126
1,2-Dichlorobenzene
50.0
53.5
ug/L
107
80-120
1,3-Dichlorobenzene
50.0
53.7
ug/L
107
80-120
1,4-Dichlorobenzene
50.0
53.3
ug/L
107
80-120
Dichlorodifluoromethane
50.0
59.3
ug/L
119
70-137
1,1-Dichloroethane
50.0
58.0
ug/L
116
80-120
1,2-Dichloroethane
50.0
56.8
ug/L
114
72-128
1,1-Dichloroethene
50.0
56.4
ug/L
113
80-120
1,2-Dichloropropane
50.0
50.3
ug/L
101
80-120
Ethylbenzene
50.0
49.0
ug/L
98
80-120
2-Hexanone
250
294
ug/L
117
80-131
1 sopropyl benzene
50.0
50.8
ug/L
102
79-126
Methyl acetate
250
296
ug/L
118
73-139
Methylcyclohexane
50.0
59.1
ug/L
118
80-138
Methylene Chloride
50.0
54.9
ug/L
110
80-120
4-Methyl-2-pentanone
250
297
ug/L
119
80-134
Methyl tert-butyl ether
50.0
54.1
ug/L
108
80-122
Styrene
50.0
50.5
ug/L
101
80-126
1,1,2,2-Tetrachloroethane
50.0
52.6
ug/L
105
76-126
Tetrachloroethene
50.0
60.5
ug/L
121
71-123
Tetrahydrofuran
100
115
ug/L
115
70-133
Toluene
50.0
52.0
ug/L
104
80-120
trans- 1,2-Dich loroethene
50.0
56.4
ug/L
113
80-120
trans- 1, 3-Dich loropropene
50.0
52.3
ug/L
105
80-128
1,2,4-Trichlorobenzene
50.0
51.8
ug/L
104
71-126
1,1,1-Trichloroethane
50.0
59.4
ug/L
119
80-120
1,1,2-Trichloroethane
50.0
47.2
ug/L
94
80-120
Trichloroethene
50.0
46.7
ug/L
93
80-120
Trichlorofluoromethane
50.0
51.2
ug/L
102
58-127
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
50.6
ug/L
101
75-128
ne
Vinyl chloride
50.0
54.3
ug/L
109
80-129
Xylenes, Total
100
98.7
ug/L
99
80-120
LCS LCS
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 111 80-120
Dibromofluoromethane (Surr) 108 80-122
1,2-Dichloroethane-d4 (Surr) 116 73-131
Toluene-d8 (Surr) 104 80-120
TestArnerica Savannah
Page 104 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 680-50135514
Matrix: Water
Analysis Batch: 501355
Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
I sopropyl benzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone
Methyl tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dich loroethene
trans- 1, 3-Dich loropropene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Spike
LCSD LCSD
Added
Result Qualifier
250
238
50.0
50.1
50.0
51.5
50.0
46.3
50.0
43.6
250
243
50.0
52.1
50.0
55.8
50.0
53.7
50.0
50.1
50.0
52.9
50.0
49.0
50.0
54.5
50.0
50.7
50.0
44.9
50.0
52.6
50.0
55.3
50.0
50.5
50.0
55.4
50.0
52.7
50.0
52.4
50.0
56.4
50.0
52.1
50.0
54.3
50.0
52.7
50.0
47.2
50.0
54.5
250
266
50.0
52.9
250
271
50.0
52.9
50.0
53.2
250
269
50.0
50.1
50.0
55.1
50.0
52.8
50.0
57.4
100
101
50.0
51.2
50.0
51.7
50.0
52.0
50.0
51.7
50.0
55.1
50.0
47.2
50.0
49.2
50.0
46.3
50.0
47.4
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
ug-/L
-95
68- 13-2
-14
-30
ug/L
100
80-120
9
20
ug/L
103
80-120
8
20
ug/L
93
52-122
2
20
ug/L
87
43-146
0
20
ug/L
97
79-125
17
20
ug/L
104
77-129
6
20
ug/L
112
67-125
1
20
ug/L
107
80-120
14
20
ug/L
100
48-145
1
20
ug/L
106
80-120
8
20
ug/L
98
76-149
4
30
ug/L
109
80-120
2
20
ug/L
101
80-129
2
20
ug/L
90
80-132
12
20
ug/L
105
68-120
10
20
ug/L
ill
74-120
3
20
ug/L
101
75-126
11
20
ug/L
111
80-120
3
20
ug/L
105
80-120
2
20
ug/L
105
80-120
2
20
ug/L
113
70-137
5
40
ug/L
104
80-120
11
20
ug/L
109
72-128
5
50
ug/L
105
80-120
7
20
ug/L
94
80-120
6
20
ug/L
109
80-120
10
20
ug/L
106
80-131
10
20
ug/L
106
79-126
4
20
ug/L
108
73-139
9
20
ug/L
106
80-138
11
20
ug/L
106
80-120
3
20
ug/L
108
80-134
10
20
ug/L
100
80-122
8
20
ug/L
110
80-126
9
20
ug/L
106
76-126
0
20
ug/L
115
71-123
5
20
ug/L
101
70-133
13
30
ug/L
102
80-120
1
20
ug/L
103
80-120
9
20
ug/L
104
80-128
1
30
ug/L
103
71-126
0
20
ug/L
110
80-120
7
20
ug/L
94
80-120
0
20
ug/L
98
80-120
5
20
ug/L
93
58-127
10
20
ug/L
95
75-128
7
20
Page 105 of 142
TestArnerica Savannah
11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501355/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501355
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D %Rec Limits RPD Limit
Vinyl chloride
50.0
52.4
ug/L
105 80-129 4 20
Xylenes, Total
100
104
ug/L
104 80-120 5 20
LCSD
LCSD
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr)
111
80-120
Dibromofluoromethane (Surr)
104
80-122
1,2-Dichloroethane-d4 (Surr)
105
73-131
Toluene-d8 (Surr)
111
80-120
Lab Sample ID: MB 680-501359/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501359
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/05/17 14:44
1
Benzene
ND
1.0
ug/L
11/05/17 14:44
1
Bromodichloromethane
ND
1.0
ug/L
11/05/17 14:44
1
Bromoform
ND
1.0
ug/L
11/05/17 14:44
1
Bromomethane
ND
5.0
ug/L
11/05/17 14:44
1
2-Butanone
ND
10
ug/L
11/05/17 14:44
1
Carbon disulfide
ND
2.0
ug/L
11/05/17 14:44
1
Carbon tetrachloride
ND
1.0
ug/L
11/05/17 14:44
1
Chlorobenzene
ND
1.0
ug/L
11/05/17 14:44
1
Chloroethane
ND
5.0
ug/L
11/05/17 14:44
1
Chloroform
ND
1.0
ug/L
11/05/17 14:44
1
Chloromethane
ND
1.0
ug/L
11/05/17 14:44
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/05/17 14:44
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/05/17 14:44
1
Cyclohexane
ND
1.0
ug/L
11/05/17 14:44
1
Dibromochloromethane
ND
1.0
ug/L
11/05/17 14:44
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/05/17 14:44
1
1,2-Dibromoethane
ND
1.0
ug/L
11/05/17 14:44
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/05/17 14:44
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/05/17 14:44
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/05/17 14:44
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/05/17 14:44
1
1,1-Dichloroethane
ND
1.0
ug/L
11/05/17 14:44
1
1,2-Dichloroethane
ND
1.0
ug/L
11/05/17 14:44
1
1,1-Dichloroethene
ND
1.0
ug/L
11/05/17 14:44
1
1,2-Dichloropropane
ND
1.0
ug/L
11/05/17 14:44
1
Ethylbenzene
ND
1.0
ug/L
11/05/17 14:44
1
2-Hexanone
ND
10
ug/L
11/05/17 14:44
1
1 sopropyl benzene
ND
1.0
ug/L
11/05/17 14:44
1
Methyl acetate
ND
5.0
ug/L
11/05/17 14:44
1
Methylcyclohexane
ND
1.0
ug/L
11/05/17 14:44
1
Methylene Chloride
ND
5.0
ug/L
11/05/17 14:44
1
4-Methyl-2-pentanone
ND
10
ug/L
11/05/17 14:44
1
Methyl tert-butyl ether
ND
10
ug/L
11/05/17 14:44
1
TestArnerica Savannah
Page 106 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50135919
Matrix: Water
Analysis Batch: 501359
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
Styrene
ND
1.0
ug/L
11/05/17 14:44
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/05/17 14:44
1
Tetrachloroethene
ND
1.0
ug/L
11/05/17 14:44
1
Tetrahydrofuran
ND
10
ug/L
11/05/17 14:44
1
Toluene
ND
1.0
ug/L
11/05/17 14:44
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/05/17 14:44
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/05/17 14:44
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/05/17 14:44
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/05/17 14:44
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/05/17 14:44
1
Trichloroethene
ND
1.0
ug/L
11/05/17 14:44
1
Trichlorofluoromethane
ND
1.0
ug/L
11/05/17 14:44
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/05/17 14:44
1
Vinyl chloride
ND
1.0
ug/L
11/05/17 14:44
1
Xylenes, Total
ND
1.0
ug/L
11/05/17 14:44
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed DR Fac
4-Bromofluorobenzene FSu-rr)
106
80-120
111051171 1
Dibromofluoromethane (Surr)
100
80-122
11105117 14:44 1
1,2-Dichloroethane-d4 (Surr)
98
73-131
11105117 14:44 1
Toluene-d8 (Surr)
112
80-120
11105117 14:44 1
Lab Sample ID: LCS 680-501359/3
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501359
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
250
208
ug/L
83
68-132
Benzene
50.0
55.3
ug/L
111
80-120
Bromodichloromethane
50.0
50.5
ug/L
101
80-120
Bromoform
50.0
38.7
ug/L
77
52-122
Bromomethane
50.0
49.5
ug/L
99
43-146
2-Butanone
250
210
ug/L
84
79-125
Carbon disulfide
50.0
52.1
ug/L
104
77-129
Carbon tetrachloride
50.0
51.5
ug/L
103
67-125
Chlorobenzene
50.0
49.3
ug/L
99
80-120
Chloroethane
50.0
60.9
ug/L
122
48-145
Chloroform
50.0
53.5
ug/L
107
80-120
Chloromethane
50.0
54.3
ug/L
109
76-149
cis- 1,2-Dichloroethene
50.0
51.7
ug/L
103
80-120
cis- 1,3-Dichloropropene
50.0
57.7
ug/L
115
80-129
Cyclohexane
50.0
52.9
ug/L
106
80-132
Dibromochloromethane
50.0
43.3
ug/L
87
68-120
1,2-Dibromo-3-Chloropropane
50.0
37.5
ug/L
75
74-120
1,2-Dibromoethane
50.0
48.9
ug/L
98
75-126
1,2-Dichlorobenzene
50.0
52.4
ug/L
105
80-120
1,3-Dichlorobenzene
50.0
53.8
ug/L
108
80-120
1,4-Dichlorobenzene
50.0
52.3
ug/L
105
80-120
TestArnerica Savannah
Page 107 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501359/3
Matrix: Water
Analysis Batch: 501359
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
Dichlorodifluoromethane
50.0
59.5
ug/L
119
70-137
1,1-Dichloroethane
50.0
51.9
ug/L
104
80-120
1,2-Dichloroethane
50.0
53.2
ug/L
106
72-128
1,1-Dichloroethene
50.0
48.3
ug/L
97
80-120
1,2-Dichloropropane
50.0
47.1
ug/L
94
80-120
Ethylbenzene
50.0
54.2
ug/L
108
80-120
2-Hexanone
250
219
ug/L
88
80-131
1 sopropyl benzene
50.0
54.6
ug/L
109
79-126
Methyl acetate
250
150
ug/L
60
73-139
Methylcyclohexane
50.0
62.4
ug/L
125
80-138
Methylene Chloride
50.0
52.0
ug/L
104
80-120
4-Methyl-2-pentanone
250
223
ug/L
89
80-134
Methyl tert-butyl ether
50.0
45.6
ug/L
91
80-122
Styrene
50.0
53.1
ug/L
106
80-126
1,1,2,2-Tetrachloroethane
50.0
38.1
ug/L
76
76-126
Tetrachloroethene
50.0
56.9
ug/L
114
71-123
Tetrahydrofuran
100
75.1
ug/L
75
70-133
Toluene
50.0
57.8
ug/L
116
80-120
trans- 1,2-Dich loroethene
50.0
49.5
ug/L
99
80-120
trans- 1, 3-Dich loropropene
50.0
55.4
ug/L
ill
80-128
1,2,4-Trichlorobenzene
50.0
47.4
ug/L
95
71-126
1,1,1-Trichloroethane
50.0
58.4
ug/L
117
80-120
1,1,2-Trichloroethane
50.0
50.5
ug/L
101
80-120
Trichloroethene
50.0
54.9
ug/L
110
80-120
Trichlorofluoromethane
50.0
53.5
ug/L
107
58-127
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
49.5
ug/L
99
75-128
ne
Vinyl chloride
50.0
55.8
ug/L
112
80-129
Xylenes, Total
100
110
ug/L
110
80-120
LCS LCS
Surrogate
%Recovety Qualifier
Limits
4-Bromofluorobenzene (Surr)
118
80-120
Dibromofluoromethane (Surr)
105
80-122
1,2-Dichloroethane-d4 (Surr)
104
73-131
Toluene-d8 (Surr)
115
80-120
Lab Sample ID: LCSID 680-501359/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501359
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
Acetone
250
-
198
- ug -/L
-79
-(�8-- 13-2
- -5
-30
Benzene
50.0
51.6
ug/L
103
80-120
7
20
Bromodichloromethane
50.0
48.7
ug/L
97
80-120
4
20
Brornoform
50.0
40.5
ug/L
81
52-122
5
20
Brornornethane
50.0
44.6
ug/L
89
43-146
10
20
2-Butanone
250
203
ug/L
81
79-125
3
20
Carbon disulfide
50.0
49.8
ug/L
100
77-129
5
20
TestArnerica Savannah
Page 108 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501359/4 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501359
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Carbon tetrachloride
50.0
49.6
ug/L
99
67-125
4
20
Chlorobenzene
50.0
50.3
ug/L
101
80-120
2
20
Chloroethane
50.0
56.9
ug/L
114
48-145
7
20
Chloroform
50.0
51.5
ug/L
103
80-120
4
20
Chloromethane
50.0
52.6
ug/L
105
76-149
3
30
cis- 1,2-Dichloroethene
50.0
51.0
ug/L
102
80-120
1
20
cis- 1,3-Dichloropropene
50.0
52.7
ug/L
105
80-129
9
20
Cyclohexane
50.0
51.9
ug/L
104
80-132
2
20
Dibromochloromethane
50.0
39.0
ug/L
78
68-120
10
20
1,2-Dibromo-3-Chloropropane
50.0
38.3
ug/L
77
74-120
2
20
1,2-Dibromoethane
50.0
43.6
ug/L
87
75-126
12
20
1,2-Dichlorobenzene
50.0
52.4
ug/L
105
80-120
0
20
1,3-Dichlorobenzene
50.0
53.9
ug/L
108
80-120
0
20
1,4-Dichlorobenzene
50.0
51.5
ug/L
103
80-120
1
20
Dichlorodifluoromethane
50.0
57.4
ug/L
115
70-137
4
40
1,1-Dichloroethane
50.0
46.7
ug/L
93
80-120
11
20
1,2-Dichloroethane
50.0
51.0
ug/L
102
72-128
4
50
1,1-Dichloroethene
50.0
47.5
ug/L
95
80-120
2
20
1,2-Dichloropropane
50.0
44.8
ug/L
90
80-120
5
20
Ethylbenzene
50.0
53.9
ug/L
108
80-120
1
20
2-Hexanone
250
193 *
ug/L
77
80-131
13
20
Isopropylbenzene
50.0
56.3
ug/L
113
79-126
3
20
Methyl acetate
250
151 *
ug/L
60
73-139
1
20
Methylcyclohexane
50.0
60.2
ug/L
120
80-138
4
20
Methylene Chloride
50.0
49.1
ug/L
98
80-120
6
20
4-Methyl-2-pentanone
250
198 *
ug/L
79
80-134
12
20
Methyl tert-butyl ether
50.0
43.7
ug/L
87
80-122
4
20
Styrene
50.0
52.3
ug/L
105
80-126
2
20
1,1,2,2-Tetrachloroethane
50.0
40.3
ug/L
81
76-126
6
20
Tetrachloroethene
50.0
51.4
ug/L
103
71-123
10
20
Tetrahydrofuran
100
69.0
ug/L
69
70-133
8
30
Toluene
50.0
49.2
ug/L
98
80-120
16
20
trans- 1,2-Dich loroethene
50.0
47.7
ug/L
95
80-120
4
20
trans- 1, 3-Dich loropropene
50.0
47.9
ug/L
96
80-128
15
30
1,2,4-Trichlorobenzene
50.0
48.7
ug/L
97
71-126
3
20
1,1,1-Trichloroethane
50.0
54.6
ug/L
109
80-120
7
20
1,1,2-Trichloroethane
50.0
43.7
ug/L
87
80-120
14
20
Trichloroethene
50.0
52.9
ug/L
106
80-120
4
20
Trichlorofluoromethane
50.0
51.1
ug/L
102
58-127
5
20
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
49.1
ug/L
98
75-128
1
20
ne
Vinyl chloride
50.0
54.7
ug/L
109
80-129
2
20
Xylenes, Total
100
109
ug/L
109
80-120
1
20
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr) 98
80-120
Dibromofluoromethane (Surr) 98
80-122
1,2-Dichloroethane-d4 (Surr) 99
73-131
TestArnerica Savannah
Page 109 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
F
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501359/4 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501359 LCSD LCSD L
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 100 80 - f2—O
Lab Sample ID: MB 680-501395/8 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501395
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Trichloroethene ND
1.0
ug/L 11/06/17 10:58 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
4-Bromofluorobenzene (Surr) 105
80-120
11106117 10:58 1
Dibromofluoromethane (Surr) 108
80-122
11106117 10:58 1
1,2-Dichloroethane-d4 (Surr) 104
73-131
11106117 10:58 1
Toluene-d8 (Surr) 111
80-120
11106117 10:58 1
Lab Sample ID: LCS 680-501395/3
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501395
Spike
LCS LCS %Rec.
Analyte
Added
Result Qualifier Unit D %Rec Limits
Trichloroethene
50.0
49.6 ug/L 99 80-120
LCS LCS
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr) 111
80-120
Dibromofluoromethane (Surr) 110
80-122
1,2-Dichloroethane-d4 (Surr) 117
73-131
Toluene-d8 (Surr) 109
80-120
Lab Sample ID: LCSID 680-501395/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501395
Spike
LCSD LCSD %Rec. RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
Trichloroethene
50.0
53.8 ug/L 108 80-120 8 20
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr) 102
80-120
Dibromofluoromethane (Surr) 129 X
80-122
1,2-Dichloroethane-d4 (Surr) 125
73-131
Toluene-d8 (Surr) 106
80-120
Lab Sample ID: MB 680-501564/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501564
MB MB
Analyte Result Qualifier
RL
MDL Unit D Prepared Analyzed Dil Fac
Acetone ND
10
ug/L 11/07/17 11:29 1
TestArnerica Savannah
Page 110 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50156419
Matrix: Water
Analysis Batch: 501564
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
Benzene
ND
1.0
ug/L
11/07/17 11:29
1
Bromodichloromethane
ND
1.0
ug/L
11/07/17 11:29
1
Bromoform
ND
1.0
ug/L
11/07/17 11:29
1
Bromomethane
ND
5.0
ug/L
11/07/17 11:29
1
2-Butanone
ND
10
ug/L
11/07/17 11:29
1
Carbon disulfide
ND
2.0
ug/L
11/07/17 11:29
1
Carbon tetrachloride
ND
1.0
ug/L
11/07/17 11:29
1
Chlorobenzene
ND
1.0
ug/L
11/07/17 11:29
1
Chloroethane
ND
5.0
ug/L
11/07/17 11:29
1
Chloroform
ND
1.0
ug/L
11/07/17 11:29
1
Chloromethane
ND
1.0
ug/L
11/07/17 11:29
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/07/17 11:29
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/07/17 11:29
1
Cyclohexane
ND
1.0
ug/L
11/07/17 11:29
1
Dibromochloromethane
ND
1.0
ug/L
11/07/17 11:29
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/07/17 11:29
1
1,2-Dibromoethane
ND
1.0
ug/L
11/07/17 11:29
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/07/17 11:29
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/07/17 11:29
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/07/17 11:29
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/07/17 11:29
1
1,1-Dichloroethane
ND
1.0
ug/L
11/07/17 11:29
1
1,2-Dichloroethane
ND
1.0
ug/L
11/07/17 11:29
1
1,1-Dichloroethene
ND
1.0
ug/L
11/07/17 11:29
1
1,2-Dichloropropane
ND
1.0
ug/L
11/07/17 11:29
1
Ethylbenzene
ND
1.0
ug/L
11/07/17 11:29
1
2-Hexanone
ND
10
ug/L
11/07/17 11:29
1
1 sopropyl benzene
ND
1.0
ug/L
11/07/17 11:29
1
Methyl acetate
ND
5.0
ug/L
11/07/17 11:29
1
Methylcyclohexane
ND
1.0
ug/L
11/07/17 11:29
1
Methylene Chloride
ND
5.0
ug/L
11/07/17 11:29
1
4-Methyl-2-pentanone
ND
10
ug/L
11/07/17 11:29
1
Methyl tert-butyl ether
ND
10
ug/L
11/07/17 11:29
1
Styrene
ND
1.0
ug/L
11/07/17 11:29
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/07/17 11:29
1
Tetrachloroethene
ND
1.0
ug/L
11/07/17 11:29
1
Tetrahydrofuran
ND
10
ug/L
11/07/17 11:29
1
Toluene
ND
1.0
ug/L
11/07/17 11:29
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/07/17 11:29
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/07/17 11:29
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/07/17 11:29
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/07/17 11:29
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/07/17 11:29
1
Trichloroethene
ND
1.0
ug/L
11/07/17 11:29
1
Trichlorofluoromethane
ND
1.0
ug/L
11/07/17 11:29
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/07/17 11:29
1
Vinyl chloride
ND
1.0
ug/L
11/07/17 11:29
1
Xylenes, Total
ND
1.0
ug/L
11/07/17 11:29
1
TestArnerica Savannah
Page 111 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50156419
Matrix: Water
Analysis Batch: 501564
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
4-Bromofluorobenzene (Surr)
89
80-120
11107117 11:29 1
Dibromofluoromethane (Surr)
92
80-122
11107117 11:29 1
1,2-Dichloroethane-d4 (Surr)
91
73-131
11107117 11:29 1
Toluene-d8 (Surr)
101
80-120
11107117 11:29 1
Lab Sample ID: LCS 680-501564/4
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501564
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
250
296
ug/L
118
68-132
Benzene
50.0
52.0
ug/L
104
80-120
Bromodichloromethane
50.0
50.5
ug/L
101
80-120
Bromoform
50.0
48.8
ug/L
98
52-122
Bromomethane
50.0
71.9
ug/L
144
43-146
2-Butanone
250
305
ug/L
122
79-125
Carbon disulfide
50.0
50.8
ug/L
102
77-129
Carbon tetrachloride
50.0
46.8
ug/L
94
67-125
Chlorobenzene
50.0
50.9
ug/L
102
80-120
Chloroethane
50.0
62.3
ug/L
125
48-145
Chloroform
50.0
49.9
ug/L
100
80-120
Chloromethane
50.0
50.0
ug/L
100
76-149
cis- 1,2-Dichloroethene
50.0
49.1
ug/L
98
80-120
cis- 1,3-Dichloropropene
50.0
52.8
ug/L
106
80-129
Cyclohexane
50.0
51.5
ug/L
103
80-132
Dibromochloromethane
50.0
52.0
ug/L
104
68-120
1,2-Dibromo-3-Chloropropane
50.0
51.3
ug/L
103
74-120
1,2-Dibromoethane
50.0
51.9
ug/L
104
75-126
1,2-Dichlorobenzene
50.0
50.2
ug/L
100
80-120
1,3-Dichlorobenzene
50.0
48.9
ug/L
98
80-120
1,4-Dichlorobenzene
50.0
49.0
ug/L
98
80-120
Dichlorodifluoromethane
50.0
60.1
ug/L
120
70-137
1,1-Dichloroethane
50.0
50.0
ug/L
100
80-120
1,2-Dichloroethane
50.0
51.4
ug/L
103
72-128
1,1-Dichloroethene
50.0
50.8
ug/L
102
80-120
1,2-Dichloropropane
50.0
53.1
ug/L
106
80-120
Ethylbenzene
50.0
50.8
ug/L
102
80-120
2-Hexanone
250
259
ug/L
104
80-131
1 sopropyl benzene
50.0
51.8
ug/L
104
79-126
Methyl acetate
250
249
ug/L
100
73-139
Methylcyclohexane
50.0
58.0
ug/L
116
80-138
Methylene Chloride
50.0
53.2
ug/L
106
80-120
4-Methyl-2-pentanone
250
255
ug/L
102
80-134
Methyl tert-butyl ether
50.0
53.7
ug/L
107
80-122
Styrene
50.0
54.7
ug/L
109
80-126
1,1,2,2-Tetrachloroethane
50.0
55.1
ug/L
110
76-126
Tetrachloroethene
50.0
51.4
ug/L
103
71-123
Tetrahydrofuran
100
95.4
ug/L
95
70-133
TestArnerica Savannah
Page 112 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501564/4
Matrix: Water
Analysis Batch: 501564
Analyte
Toluene
tra ns- 1, 2- D ich loroeth e ne
trans- 1, 3-Dich loropropene
1, 2,4-Trich lorobe nzene
1, 1, 1 -Trichloroethane
1, 1,2-Trich loroethane
Trichloroethene
Trichlorofluoromethane
1, 1,2-Trich loro-1,2,2-trifluoroetha
ne
Vinyl chloride
Xylenes, Total
LCS LCS
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surr) 89
Dibromofluoromethane (Surr) 102
1,2-Dichloroethane-d4 (Surr) 95
Toluene-d8 (Surr) 100
Lab Sample ID: LCSD 680-50156415
Matrix: Water
Analysis Batch: 501564
Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
50.0
52.0
ug/L
104
80-120
50.0
51.3
ug/L
103
80-120
50.0
51.7
ug/L
103
80-128
50.0
53.7
ug/L
107
71-126
50.0
48.2
ug/L
96
80-120
50.0
56.2
ug/L
112
80-120
50.0
49.9
ug/L
100
80-120
50.0
55.0
ug/L
110
58-127
50.0
53.0
ug/L
106
75-128
50.0
54.6
ug/L
109
80-129
100
102
ug/L
102
80-120
Limits
80-120
80-122
73-131
80-120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec.
RPD
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
250
299
ug/L
120
68-132
1
30
50.0
51.6
ug/L
103
80-120
1
20
50.0
52.3
ug/L
105
80-120
4
20
50.0
49.9
ug/L
100
52-122
2
20
50.0
69.7
ug/L
139
43-146
3
20
250
302
ug/L
121
79-125
1
20
50.0
49.6
ug/L
99
77-129
2
20
50.0
46.3
ug/L
93
67-125
1
20
50.0
51.1
ug/L
102
80-120
0
20
50.0
60.4
ug/L
121
48-145
3
20
50.0
50.2
ug/L
100
80-120
0
20
50.0
49.6
ug/L
99
76-149
1
30
50.0
48.6
ug/L
97
80-120
1
20
50.0
52.3
ug/L
105
80-129
1
20
50.0
50.3
ug/L
101
80-132
3
20
50.0
51.8
ug/L
104
68-120
0
20
50.0
49.6
ug/L
99
74-120
3
20
50.0
53.6
ug/L
107
75-126
3
20
50.0
48.9
ug/L
98
80-120
3
20
50.0
47.1
ug/L
94
80-120
4
20
50.0
48.7
ug/L
97
80-120
1
20
50.0
58.7
ug/L
117
70-137
2
40
50.0
48.9
ug/L
98
80-120
2
20
50.0
51.2
ug/L
102
72-128
0
50
Page 113 of 142
TestArnerica Savannah
11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501564/5
Matrix: Water
Analysis Batch: 501564
Analyte
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
I sopropyl benzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone
Methyl tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dich loroethene
trans- 1, 3-Dich loropropene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Vinyl chloride
Xylenes, Total
LCSD LCSD
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surr) 85
Dibromofluoromethane (Surr) 100
1,2-Dichloroethane-d4 (Surr) 96
Toluene-d8 (Surr) 97
Lab Sample ID: MB 680-501694/9
Matrix: Water
Analysis Batch: 501694
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec.
RPD
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
50.0
49.2
ug/L
98
80-120
3
20
50.0
52.9
ug/L
106
80-120
0
20
50.0
50.4
ug/L
101
80-120
1
20
250
263
ug/L
105
80-131
1
20
50.0
51.0
ug/L
102
79-126
1
20
250
250
ug/L
100
73-139
1
20
50.0
56.1
ug/L
112
80-138
3
20
50.0
53.4
ug/L
107
80-120
0
20
250
257
ug/L
103
80-134
1
20
50.0
54.1
ug/L
108
80-122
1
20
50.0
53.4
ug/L
107
80-126
2
20
50.0
55.2
ug/L
110
76-126
0
20
50.0
50.5
ug/L
101
71-123
2
20
100
98.4
ug/L
98
70-133
3
30
50.0
51.7
ug/L
103
80-120
1
20
50.0
50.6
ug/L
101
80-120
1
20
50.0
52.5
ug/L
105
80-128
2
30
50.0
52.5
ug/L
105
71-126
2
20
50.0
47.4
ug/L
95
80-120
2
20
50.0
55.1
ug/L
110
80-120
2
20
50.0
49.1
ug/L
98
80-120
2
20
50.0
53.7
ug/L
107
58-127
2
20
50.0
51.8
ug/L
104
75-128
2
20
50.0
53.3
ug/L
107
80-129
2
20
100
100
ug/L
100
80-120
1
20
Limits
80-120
80-122
73-131
80-120
Client Sample ID: Method Blank
Prep Type: Total/NA
MlB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/07/17 20:34
1
Benzene
ND
1.0
ug/L
11/07/17 20:34
1
Bromodichloromethane
ND
1.0
ug/L
11/07/17 20:34
1
Brornoform
ND
1.0
ug/L
11/07/17 20:34
1
Brornornethane
ND
5.0
ug/L
11/07/17 20:34
1
2-Butanone
ND
10
ug/L
11/07/17 20:34
1
Carbon disulfide
ND
2.0
ug/L
11/07/17 20:34
1
Carbon tetrachloride
ND
1.0
ug/L
11/07/17 20:34
1
Chlorobenzene
ND
1.0
ug/L
11/07/17 20:34
1
Chloroethane
ND
5.0
ug/L
11/07/17 20:34
1
Page 114 of 142
TestArnerica Savannah
11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50169419
Matrix: Water
Analysis Batch: 501694
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
Chloroform
ND
1.0
ug/L
11/07/17 20:34
1
Chloromethane
ND
1.0
ug/L
11/07/17 20:34
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/07/17 20:34
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/07/17 20:34
1
Cyclohexane
ND
1.0
ug/L
11/07/17 20:34
1
Dibromochloromethane
ND
1.0
ug/L
11/07/17 20:34
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/07/17 20:34
1
1,2-Dibromoethane
ND
1.0
ug/L
11/07/17 20:34
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/07/17 20:34
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/07/17 20:34
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/07/17 20:34
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/07/17 20:34
1
1,1-Dichloroethane
ND
1.0
ug/L
11/07/17 20:34
1
1,2-Dichloroethane
ND
1.0
ug/L
11/07/17 20:34
1
1,1-Dichloroethene
ND
1.0
ug/L
11/07/17 20:34
1
1,2-Dichloropropane
ND
1.0
ug/L
11/07/17 20:34
1
Ethylbenzene
ND
1.0
ug/L
11/07/17 20:34
1
2-Hexanone
ND
10
ug/L
11/07/17 20:34
1
1 sopropyl benzene
ND
1.0
ug/L
11/07/17 20:34
1
Methyl acetate
ND
5.0
ug/L
11/07/17 20:34
1
Methylcyclohexane
ND
1.0
ug/L
11/07/17 20:34
1
Methylene Chloride
ND
5.0
ug/L
11/07/17 20:34
1
4-Methyl-2-pentanone
ND
10
ug/L
11/07/17 20:34
1
Methyl tert-butyl ether
ND
10
ug/L
11/07/17 20:34
1
Styrene
ND
1.0
ug/L
11/07/17 20:34
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/07/17 20:34
1
Tetrachloroethene
ND
1.0
ug/L
11/07/17 20:34
1
Tetrahydrofuran
ND
10
ug/L
11/07/17 20:34
1
Toluene
ND
1.0
ug/L
11/07/17 20:34
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/07/17 20:34
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/07/17 20:34
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/07/17 20:34
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/07/17 20:34
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/07/17 20:34
1
Trichloroethene
ND
1.0
ug/L
11/07/17 20:34
1
Trichlorofluoromethane
ND
1.0
ug/L
11/07/17 20:34
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/07/17 20:34
1
Vinyl chloride
ND
1.0
ug/L
11/07/17 20:34
1
Xylenes, Total
ND
1.0
ug/L
11/07/17 20:34
1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
88
80-120
11/07/17 20:34
1
Dibromofluoromethane (Surr)
96
80-122
11/07/17 20:34
1
1,2-Dichloroethane-d4 (Surr)
91
73-131
11/07/17 20:34
1
Toluene-d8 (Surr)
99
80-120
11/07/17 20:34
1
TestArnerica Savannah
Page 115 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID:
Matrix: Water
Analysis Batch
LCS 680-501694/3
501694
Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
I sopropyl benzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone
Methyl tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dich loroethene
trans- 1, 3-Dich loropropene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Spike
LCS LCS
Added
Result Qualifier
250
240
50.0
50.1
50.0
53.2
50.0
56.7
50.0
54.4
250
229
50.0
52.8
50.0
52.5
50.0
50.1
50.0
55.6
50.0
50.5
50.0
51.6
50.0
51.8
50.0
53.8
50.0
51.7
50.0
50.0
50.0
52.0
50.0
49.8
50.0
50.7
50.0
50.0
50.0
49.0
50.0
55.3
50.0
51.0
50.0
48.8
50.0
51.1
50.0
50.1
50.0
50.6
250
249
50.0
52.1
250
253
50.0
53.8
50.0
52.1
250
251
50.0
48.5
50.0
51.9
50.0
47.4
50.0
51.6
100
94.2
50.0
49.6
50.0
52.3
50.0
51.9
50.0
64.6
50.0
52.2
50.0
48.6
50.0
50.9
50.0
55.2
50.0
56.8
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
Unit
D %Rec
Limits
dg-/ -L
-96
68-132
ug/L
100
80-120
ug/L
106
80-120
ug/L
113
52-122
ug/L
109
43-146
ug/L
91
79-125
ug/L
106
77-129
ug/L
105
67-125
ug/L
100
80-120
ug/L
111
48-145
ug/L
101
80-120
ug/L
103
76-149
ug/L
104
80-120
ug/L
108
80-129
ug/L
103
80-132
ug/L
100
68-120
ug/L
104
74-120
ug/L
100
75-126
ug/L
101
80-120
ug/L
100
80-120
ug/L
98
80-120
ug/L
111
70-137
ug/L
102
80-120
ug/L
98
72-128
ug/L
102
80-120
ug/L
100
80-120
ug/L
101
80-120
ug/L
99
80-131
ug/L
104
79-126
ug/L
101
73-139
ug/L
108
80-138
ug/L
104
80-120
ug/L
100
80-134
ug/L
97
80-122
ug/L
104
80-126
ug/L
95
76-126
ug/L
103
71-123
ug/L
94
70-133
ug/L
99
80-120
ug/L
105
80-120
ug/L
104
80-128
ug/L
129
71-126
ug/L
104
80-120
ug/L
97
80-120
ug/L
102
80-120
ug/L
110
58-127
ug/L
114
75-128
Page 116 of 142
TestArnerica Savannah
11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501694/3
Matrix: Water
Analysis Batch: 501694
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
Vinyl chloride
50.0
54.1
ug/L
108
80-129
Xylenes, Total
100
102
ug/L
102
80-120
LGS LCS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
89
80-120
Dibromofluoromethane (Surr)
101
80-122
1,2-Dichloroethane-d4 (Surr)
93
73-131
Toluene-d8 (Surr)
99
80-120
Lab Sample ID: LCSID 680-501694/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501694
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
Acetone
250
240
ug/L
96
68-132
0
30
Benzene
50.0
50.2
ug/L
100
80-120
0
20
Bromodichloromethane
50.0
53.6
ug/L
107
80-120
1
20
Bromoform
50.0
55.8
ug/L
112
52-122
2
20
Bromomethane
50.0
59.0
ug/L
118
43-146
8
20
2-Butanone
250
237
ug/L
95
79-125
4
20
Carbon disulfide
50.0
53.6
ug/L
107
77-129
1
20
Carbon tetrachloride
50.0
52.8
ug/L
106
67-125
1
20
Chlorobenzene
50.0
49.6
ug/L
99
80-120
1
20
Chloroethane
50.0
55.8
ug/L
112
48-145
0
20
Chloroform
50.0
50.6
ug/L
101
80-120
0
20
Chloromethane
50.0
51.9
ug/L
104
76-149
1
30
cis- 1,2-Dichloroethene
50.0
51.7
ug/L
103
80-120
0
20
cis- 1,3-Dichloropropene
50.0
53.2
ug/L
106
80-129
1
20
Cyclohexane
50.0
51.4
ug/L
103
80-132
0
20
Dibromochloromethane
50.0
50.0
ug/L
100
68-120
0
20
1,2-Dibromo-3-Chloropropane
50.0
53.5
ug/L
107
74-120
3
20
1,2-Dibromoethane
50.0
50.3
ug/L
101
75-126
1
20
1,2-Dichlorobenzene
50.0
50.1
ug/L
100
80-120
1
20
1,3-Dichlorobenzene
50.0
50.2
ug/L
100
80-120
0
20
1,4-Dichlorobenzene
50.0
49.3
ug/L
99
80-120
0
20
Dichlorodifluoromethane
50.0
54.1
ug/L
108
70-137
2
40
1,1-Dichloroethane
50.0
51.5
ug/L
103
80-120
1
20
1,2-Dichloroethane
50.0
48.9
ug/L
98
72-128
0
50
1,1-Dichloroethene
50.0
50.0
ug/L
100
80-120
2
20
1,2-Dichloropropane
50.0
50.2
ug/L
100
80-120
0
20
Ethylbenzene
50.0
50.5
ug/L
101
80-120
0
20
2-Hexanone
250
255
ug/L
102
80-131
3
20
1 sopropyl benzene
50.0
52.2
ug/L
104
79-126
0
20
Methyl acetate
250
257
ug/L
103
73-139
1
20
Methylcyclohexane
50.0
54.1
ug/L
108
80-138
1
20
Methylene Chloride
50.0
52.2
ug/L
104
80-120
0
20
4-Methyl-2-pentanone
250
259
ug/L
103
80-134
3
20
Methyl tert-butyl ether
50.0
49.5
ug/L
99
80-122
2
20
TestArnerica Savannah
Page 117 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501694/4
Matrix: Water
Analysis Batch: 501694
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits RPD
Limit
Styrene
50.0
51.5
ug/L
103
80-126 1
20
1,1,2,2-Tetrachloroethane
50.0
47.7
ug/L
95
76-126 1
20
Tetrachloroethene
50.0
51.9
ug/L
104
71-123 1
20
Tetrahydrofuran
100
96.1
ug/L
96
70-133 2
30
Toluene
50.0
49.7
ug/L
99
80-120 0
20
trans- 1,2-Dich loroethene
50.0
52.7
ug/L
105
80-120 1
20
trans- 1, 3-Dich loropropene
50.0
52.5
ug/L
105
80-128 1
30
1,2,4-Trichlorobenzene
50.0
66.6
ug/L
133
71-126 3
20
1,1,1-Trichloroethane
50.0
52.9
ug/L
106
80-120 1
20
1,1,2-Trichloroethane
50.0
48.1
ug/L
96
80-120 1
20
Trichloroethene
50.0
51.5
ug/L
103
80-120 1
20
Trichlorofluoromethane
50.0
55.4
ug/L
111
58-127 0
20
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
56.2
ug/L
112
75-128 1
20
ne
Vinyl chloride
50.0
54.5
ug/L
109
80-129 1
20
Xylenes, Total
100
102
ug/L
102
80-120 0
20
LCSD
LCSD
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr)
88
80-120
Dibromofluoromethane (Surr)
102
80-122
1,2-Dichloroethane-d4 (Surr)
93
73-131
Toluene-d8 (Surr)
99
80-120
Lab Sample ID: MB 680-501727/9
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501727
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 12:29
1
Benzene
ND
1.0
ug/L
11/08/17 12:29
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 12:29
1
Bromoform
ND
1.0
ug/L
11/08/17 12:29
1
Bromomethane
ND
5.0
ug/L
11/08/17 12:29
1
2-Butanone
ND
10
ug/L
11/08/17 12:29
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 12:29
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 12:29
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 12:29
1
Chloroethane
ND
5.0
ug/L
11/08/17 12:29
1
Chloroform
ND
1.0
ug/L
11/08/17 12:29
1
Chloromethane
ND
1.0
ug/L
11/08/17 12:29
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 12:29
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 12:29
1
Cyclohexane
ND
1.0
ug/L
11/08/17 12:29
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 12:29
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 12:29
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 12:29
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 12:29
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 12:29
1
TestArnerica Savannah
Page 118 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50172719
Matrix: Water
Analysis Batch: 501727
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 12:29
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 12:29
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 12:29
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 12:29
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 12:29
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 12:29
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 12:29
1
2-Hexanone
ND
10
ug/L
11/08/17 12:29
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 12:29
1
Methyl acetate
ND
5.0
ug/L
11/08/17 12:29
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 12:29
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 12:29
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 12:29
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 12:29
1
Styrene
ND
1.0
ug/L
11/08/17 12:29
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 12:29
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 12:29
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 12:29
1
Toluene
ND
1.0
ug/L
11/08/17 12:29
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 12:29
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 12:29
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 12:29
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 12:29
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 12:29
1
Trichloroethene
ND
1.0
ug/L
11/08/17 12:29
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 12:29
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 12:29
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 12:29
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 12:29
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
4-Bromofluorobenzene Fsu-rr)
88
80-120
111081171 1
Dibromofluoromethane (Surr)
95
80-122
11108117 12:29 1
1,2-Dichloroethane-d4 (Surr)
92
73-131
11108117 12:29 1
Toluene-d8 (Surr)
102
80-120
11108117 12:29 1
Lab Sample ID: LCS 680-501727/4
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501727
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
250
301
ug/L
120
68-132
Benzene
50.0
51.2
ug/L
102
80-120
Bromodichloromethane
50.0
51.1
ug/L
102
80-120
Brornoform
50.0
49.0
ug/L
98
52-122
Brornornethane
50.0
68.5
ug/L
137
43-146
2-Butanone
250
310
ug/L
124
79-125
Carbon disulfide
50.0
47.6
ug/L
95
77-129
TestArnerica Savannah
Page 119 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501727/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501727
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Carbon tetrachloride
50.0
45.1
ug/L
90
67-125
Chlorobenzene
50.0
50.4
ug/L
101
80-120
Chloroethane
50.0
58.1
ug/L
116
48-145
Chloroform
50.0
48.3
ug/L
97
80-120
Chloromethane
50.0
47.2
ug/L
94
76-149
cis- 1,2-Dichloroethene
50.0
48.2
ug/L
96
80-120
cis- 1,3-Dichloropropene
50.0
51.9
ug/L
104
80-129
Cyclohexane
50.0
50.4
ug/L
101
80-132
Dibromochloromethane
50.0
50.5
ug/L
101
68-120
1,2-Dibromo-3-Chloropropane
50.0
49.0
ug/L
98
74-120
1,2-Dibromoethane
50.0
52.9
ug/L
106
75-126
1,2-Dichlorobenzene
50.0
47.2
ug/L
94
80-120
1,3-Dichlorobenzene
50.0
46.3
ug/L
93
80-120
1,4-Dichlorobenzene
50.0
47.2
ug/L
94
80-120
Dichlorodifluoromethane
50.0
55.3
ug/L
111
70-137
1,1-Dichloroethane
50.0
48.2
ug/L
96
80-120
1,2-Dichloroethane
50.0
50.0
ug/L
100
72-128
1,1-Dichloroethene
50.0
45.8
ug/L
92
80-120
1,2-Dichloropropane
50.0
53.3
ug/L
107
80-120
Ethylbenzene
50.0
48.7
ug/L
97
80-120
2-Hexanone
250
266
ug/L
106
80-131
Isopropylbenzene
50.0
49.7
ug/L
99
79-126
Methyl acetate
250
247
ug/L
99
73-139
Methylcyclohexane
50.0
55.8
ug/L
112
80-138
Methylene Chloride
50.0
53.0
ug/L
106
80-120
4-Methyl-2-pentanone
250
266
ug/L
106
80-134
Methyl tert-butyl ether
50.0
54.9
ug/L
110
80-122
Styrene
50.0
50.6
ug/L
101
80-126
1,1,2,2-Tetrachloroethane
50.0
56.2
ug/L
112
76-126
Tetrachloroethene
50.0
49.8
ug/L
100
71-123
Tetrahydrofuran
100
101
ug/L
101
70-133
Toluene
50.0
50.4
ug/L
101
80-120
trans- 1,2-Dich loroethene
50.0
50.4
ug/L
101
80-120
trans- 1, 3-Dich loropropene
50.0
50.9
ug/L
102
80-128
1,2,4-Trichlorobenzene
50.0
51.2
ug/L
102
71-126
1,1,1-Trichloroethane
50.0
46.2
ug/L
92
80-120
1,1,2-Trichloroethane
50.0
55.8
ug/L
112
80-120
Trichloroethene
50.0
48.1
ug/L
96
80-120
Trichlorofluoromethane
50.0
51.0
ug/L
102
58-127
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
49.9
ug/L
100
75-128
ne
Vinyl chloride
50.0
50.7
ug/L
101
80-129
Xylenes, Total
100
97.7
ug/L
98
80-120
LCS LCS
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr) 85
80-120
Dibromofluoromethane (Surr) 98
80-122
1,2-Dichloroethane-d4 (Surr) 95
73-131
TestArnerica Savannah
Page 120 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501727/4 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501727
LCS LCS
Surrogate %Recovety Qualifier Limits
Toluene-d8 (Surr) 97 80 - f2O
Lab Sample ID: LCSD 680-501727/5 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501727
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Acetone
250
277
ug/L
111
68-132
8
30
Benzene
50.0
50.8
ug/L
102
80-120
1
20
Bromodichloromethane
50.0
49.4
ug/L
99
80-120
3
20
Bromoform
50.0
46.8
ug/L
94
52-122
5
20
Bromomethane
50.0
68.3
ug/L
137
43-146
0
20
2-Butanone
250
291
ug/L
116
79-125
6
20
Carbon disulfide
50.0
47.1
ug/L
94
77-129
1
20
Carbon tetrachloride
50.0
45.0
ug/L
90
67-125
0
20
Chlorobenzene
50.0
50.0
ug/L
100
80-120
1
20
Chloroethane
50.0
57.1
ug/L
114
48-145
2
20
Chloroform
50.0
47.5
ug/L
95
80-120
2
20
Chloromethane
50.0
47.2
ug/L
94
76-149
0
30
cis- 1,2-Dichloroethene
50.0
47.6
ug/L
95
80-120
1
20
cis- 1,3-Dichloropropene
50.0
50.5
ug/L
101
80-129
3
20
Cyclohexane
50.0
49.6
ug/L
99
80-132
2
20
Dibromochloromethane
50.0
48.1
ug/L
96
68-120
5
20
1,2-Dibromo-3-Chloropropane
50.0
48.6
ug/L
97
74-120
1
20
1,2-Dibromoethane
50.0
49.7
ug/L
99
75-126
6
20
1,2-Dichlorobenzene
50.0
48.4
ug/L
97
80-120
3
20
1,3-Dichlorobenzene
50.0
46.9
ug/L
94
80-120
1
20
1,4-Dichlorobenzene
50.0
48.0
ug/L
96
80-120
2
20
Dichlorodifluoromethane
50.0
55.7
ug/L
ill
70-137
1
40
1,1-Dichloroethane
50.0
47.4
ug/L
95
80-120
2
20
1,2-Dichloroethane
50.0
48.5
ug/L
97
72-128
3
50
1,1-Dichloroethene
50.0
46.9
ug/L
94
80-120
2
20
1,2-Dichloropropane
50.0
52.2
ug/L
104
80-120
2
20
Ethylbenzene
50.0
48.9
ug/L
98
80-120
0
20
2-Hexanone
250
248
ug/L
99
80-131
7
20
1 sopropyl benzene
50.0
49.2
ug/L
98
79-126
1
20
Methyl acetate
250
232
ug/L
93
73-139
6
20
M ethyl cyclohexa ne
50.0
55.4
ug/L
111
80-138
1
20
Methylene Chloride
50.0
51.7
ug/L
103
80-120
3
20
4-Methyl-2-pentanone
250
247
ug/L
99
80-134
7
20
Methyl tert-butyl ether
50.0
52.6
ug/L
105
80-122
4
20
Styrene
50.0
51.6
ug/L
103
80-126
2
20
1,1,2,2-Tetrachloroethane
50.0
55.4
ug/L
111
76-126
1
20
Tetrachloroethene
50.0
48.9
ug/L
98
71-123
2
20
Tetrahydrofuran
100
93.5
ug/L
93
70-133
8
30
Toluene
50.0
49.6
ug/L
99
80-120
2
20
trans- 1,2-Dich loroethene
50.0
50.5
ug/L
101
80-120
0
20
trans- 1, 3-Dich loropropene
50.0
49.0
ug/L
98
80-128
4
30
TestArnerica Savannah
Page 121 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 680-501727/5 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501727 Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
1,2,4-Trichlorobenzene
50.0
51.8
ug/L
104
71-126 1
20
1,1,1-Trichloroethane
50.0
46.2
ug/L
92
80-120 0
20
1,1,2-Trichloroethane
50.0
52.9
ug/L
106
80-120 5
20
Trichloroethene
50.0
47.9
ug/L
96
80-120 0
20
Trichlorofluoromethane
50.0
51.0
ug/L
102
58-127 0
20
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
49.9
ug/L
100
75-128 0
20
ne
Vinyl chloride
50.0
50.3
ug/L
101
80-129 1
20
Xylenes, Total
100
98.0
ug/L
98
80-120 0
20
LCSD
LCSD
Surrogate %Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr) 85
80-120
Dibromofluoromethane (Surr) 97
80-122
1,2-Dichloroethane-d4 (Surr) 92
73-131
Toluene-d8 (Surr) 98
80-120
Lab Sample ID: MB 680-501730/8
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501730
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 10:34
1
Benzene
ND
1.0
ug/L
11/08/17 10:34
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 10:34
1
Bromoform
ND
1.0
ug/L
11/08/17 10:34
1
Bromomethane
ND
5.0
ug/L
11/08/17 10:34
1
2-Butanone
ND
10
ug/L
11/08/17 10:34
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 10:34
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 10:34
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 10:34
1
Chloroethane
ND
5.0
ug/L
11/08/17 10:34
1
Chloroform
ND
1.0
ug/L
11/08/17 10:34
1
Chloromethane
ND
1.0
ug/L
11/08/17 10:34
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 10:34
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 10:34
1
Cyclohexane
ND
1.0
ug/L
11/08/17 10:34
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 10:34
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 10:34
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 10:34
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 10:34
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 10:34
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 10:34
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 10:34
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 10:34
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 10:34
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 10:34
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 10:34
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 10:34
1
TestArnerica Savannah
Page 122 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50173018
Matrix: Water
Analysis Batch: 501730
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
2-Hexanone
ND
10
ug/L
11/08/17 10:34
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 10:34
1
Methyl acetate
ND
5.0
ug/L
11/08/17 10:34
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 10:34
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 10:34
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 10:34
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 10:34
1
Styrene
ND
1.0
ug/L
11/08/17 10:34
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 10:34
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 10:34
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 10:34
1
Toluene
ND
1.0
ug/L
11/08/17 10:34
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 10:34
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 10:34
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 10:34
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 10:34
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 10:34
1
Trichloroethene
ND
1.0
ug/L
11/08/17 10:34
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 10:34
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 10:34
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 10:34
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 10:34
1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
112
80-120
11108117 10:34
1
Dibromofluoromethane (Surr)
109
80-122
11108117 10:34
1
1,2-Dichloroethane-d4 (Surr)
105
73-131
11108117 10:34
1
Toluene-d8 (Surr)
114
80-120
11108117 10:34
1
Lab Sample ID: LCS 680-501730/3
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501730
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Acetone
-
250
280
ug-/L
-112
68- 13-2
Benzene
50.0
58.5
ug/L
117
80-120
Bromodichloromethane
50.0
59.7
ug/L
119
80-120
Bromoform
50.0
48.8
ug/L
98
52-122
Bromomethane
50.0
46.9
ug/L
94
43-146
2-Butanone
250
282
ug/L
113
79-125
Carbon disulfide
50.0
54.1
ug/L
108
77-129
Carbon tetrachloride
50.0
58.0
ug/L
116
67-125
Chlorobenzene
50.0
54.8
ug/L
110
80-120
Chloroethane
50.0
52.0
ug/L
104
48-145
Chloroform
50.0
60.1
ug/L
120
80-120
Chloromethane
50.0
53.8
ug/L
108
76-149
cis- 1,2-Dichloroethene
50.0
59.2
ug/L
118
80-120
cis- 1,3-Dichloropropene
50.0
55.5
ug/L
ill
80-129
TestArnerica Savannah
Page 123 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501730/3
Matrix: Water
Analysis Batch: 501730
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Cyclohexane
50.0
51.9
ug/L
104
80-132
Dibromochloromethane
50.0
62.0
ug/L
124
68-120
1,2-Dibromo-3-Chloropropane
50.0
51.5
ug/L
103
74-120
1,2-Dibromoethane
50.0
58.1
ug/L
116
75-126
1,2-Dichlorobenzene
50.0
52.7
ug/L
105
80-120
1,3-Dichlorobenzene
50.0
52.5
ug/L
105
80-120
1,4-Dichlorobenzene
50.0
53.7
ug/L
107
80-120
Dichlorodifluoromethane
50.0
61.6
ug/L
123
70-137
1,1-Dichloroethane
50.0
58.1
ug/L
116
80-120
1,2-Dichloroethane
50.0
62.5
ug/L
125
72-128
1,1-Dichloroethene
50.0
56.4
ug/L
113
80-120
1,2-Dichloropropane
50.0
51.5
ug/L
103
80-120
Ethylbenzene
50.0
57.4
ug/L
115
80-120
2-Hexanone
250
312
ug/L
125
80-131
1 sopropyl benzene
50.0
56.8
ug/L
114
79-126
Methyl acetate
250
311
ug/L
124
73-139
Methylcyclohexane
50.0
59.1
ug/L
118
80-138
Methylene Chloride
50.0
59.8
ug/L
120
80-120
4-Methyl-2-pentanone
250
302
ug/L
121
80-134
Methyl tert-butyl ether
50.0
58.7
ug/L
117
80-122
Styrene
50.0
56.6
ug/L
113
80-126
1,1,2,2-Tetrachloroethane
50.0
58.9
ug/L
118
76-126
Tetrachloroethene
50.0
62.1 *
ug/L
124
71-123
Tetrahydrofuran
100
115
ug/L
115
70-133
Toluene
50.0
60.5 *
ug/L
121
80-120
trans- 1,2-Dich loroethene
50.0
57.3
ug/L
115
80-120
trans- 1, 3-Dich loropropene
50.0
57.5
ug/L
115
80-128
1,2,4-Trichlorobenzene
50.0
48.0
ug/L
96
71-126
1,1,1-Trichloroethane
50.0
58.6
ug/L
117
80-120
1,1,2-Trichloroethane
50.0
53.9
ug/L
108
80-120
Trichloroethene
50.0
51.2
ug/L
102
80-120
Trichlorofluoromethane
50.0
49.5
ug/L
99
58-127
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
51.5
ug/L
103
75-128
ne
Vinyl chloride
50.0
57.9
ug/L
116
80-129
Xylenes, Total
100
ill
ug/L
111
80-120
LCS LCS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
105
80-120
Dibromofluoromethane (Surr)
114
80-122
1,2-Dichloroethane-d4 (Surr)
116
73-131
Toluene-d8 (Surr)
115
80-120
TestArnerica Savannah
Page 124 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 680-50173014
Matrix: Water
Analysis Batch: 501730
Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
I sopropyl benzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone
Methyl tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dich loroethene
trans- 1, 3-Dich loropropene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Spike
LCSD LCSD
Added
Result Qualifier
250
247
50.0
54.3
50.0
55.3
50.0
48.8
50.0
48.1
250
255
50.0
53.1
50.0
53.4
50.0
53.6
50.0
47.7
50.0
55.6
50.0
52.8
50.0
54.5
50.0
49.2
50.0
49.6
50.0
56.6
50.0
48.6
50.0
52.6
50.0
51.7
50.0
54.3
50.0
56.1
50.0
59.2
50.0
56.5
50.0
55.3
50.0
53.5
50.0
46.8
50.0
53.3
250
261
50.0
55.8
250
267
50.0
57.5
50.0
53.1
250
267
50.0
52.5
50.0
55.2
50.0
52.1
50.0
54.7
100
103
50.0
54.7
50.0
56.2
50.0
54.9
50.0
51.4
50.0
52.9
50.0
49.2
50.0
48.3
50.0
49.4
50.0
48.7
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
ug A
-99
-(�8-- 13-2
-13
-30
ug/L
109
80-120
7
20
ug/L
ill
80-120
8
20
ug/L
98
52-122
0
20
ug/L
96
43-146
2
20
ug/L
102
79-125
10
20
ug/L
106
77-129
2
20
ug/L
107
67-125
8
20
ug/L
107
80-120
2
20
ug/L
95
48-145
9
20
ug/L
111
80-120
8
20
ug/L
106
76-149
2
30
ug/L
109
80-120
8
20
ug/L
98
80-129
12
20
ug/L
99
80-132
5
20
ug/L
113
68-120
9
20
ug/L
97
74-120
6
20
ug/L
105
75-126
10
20
ug/L
103
80-120
2
20
ug/L
109
80-120
3
20
ug/L
112
80-120
4
20
ug/L
118
70-137
4
40
ug/L
113
80-120
3
20
ug/L
111
72-128
12
50
ug/L
107
80-120
5
20
ug/L
94
80-120
10
20
ug/L
107
80-120
7
20
ug/L
105
80-131
18
20
ug/L
112
79-126
2
20
ug/L
107
73-139
15
20
ug/L
115
80-138
3
20
ug/L
106
80-120
12
20
ug/L
107
80-134
13
20
ug/L
105
80-122
11
20
ug/L
110
80-126
3
20
ug/L
104
76-126
12
20
ug/L
109
71-123
13
20
ug/L
103
70-133
11
30
ug/L
109
80-120
10
20
ug/L
112
80-120
2
20
ug/L
110
80-128
5
30
ug/L
103
71-126
7
20
ug/L
106
80-120
10
20
ug/L
98
80-120
9
20
ug/L
97
80-120
6
20
ug/L
99
58-127
0
20
ug/L
97
75-128
5
20
Page 125 of 142
TestArnerica Savannah
11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501730/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501730
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D %Rec Limits RPD Limit
Vinyl chloride
50.0
55.0
ug/L
110 80-129 5 20
Xylenes, Total
100
107
ug/L
107 80-120 3 20
LCSD
LCSD
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr)
107
80-120
Dibromofluoromethane (Surr)
108
80-122
1,2-Dichloroethane-d4 (Surr)
103
73-131
Toluene-d8 (Surr)
110
80-120
Lab Sample ID: MB 680-501749/9
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501749
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
10
ug/L
11/08/17 12:39
1
Benzene
ND
1.0
ug/L
11/08/17 12:39
1
Bromodichloromethane
ND
1.0
ug/L
11/08/17 12:39
1
Bromoform
ND
1.0
ug/L
11/08/17 12:39
1
Bromomethane
ND
5.0
ug/L
11/08/17 12:39
1
2-Butanone
ND
10
ug/L
11/08/17 12:39
1
Carbon disulfide
ND
2.0
ug/L
11/08/17 12:39
1
Carbon tetrachloride
ND
1.0
ug/L
11/08/17 12:39
1
Chlorobenzene
ND
1.0
ug/L
11/08/17 12:39
1
Chloroethane
ND
5.0
ug/L
11/08/17 12:39
1
Chloroform
ND
1.0
ug/L
11/08/17 12:39
1
Chloromethane
ND
1.0
ug/L
11/08/17 12:39
1
cis- 1,2-Dichloroethene
ND
1.0
ug/L
11/08/17 12:39
1
cis- 1,3-Dichloropropene
ND
1.0
ug/L
11/08/17 12:39
1
Cyclohexane
ND
1.0
ug/L
11/08/17 12:39
1
Dibromochloromethane
ND
1.0
ug/L
11/08/17 12:39
1
1,2-Dibromo-3-Chloropropane
ND
5.0
ug/L
11/08/17 12:39
1
1,2-Dibromoethane
ND
1.0
ug/L
11/08/17 12:39
1
1,2-Dichlorobenzene
ND
1.0
ug/L
11/08/17 12:39
1
1,3-Dichlorobenzene
ND
1.0
ug/L
11/08/17 12:39
1
1,4-Dichlorobenzene
ND
1.0
ug/L
11/08/17 12:39
1
Dichlorodifluoromethane
ND
1.0
ug/L
11/08/17 12:39
1
1,1-Dichloroethane
ND
1.0
ug/L
11/08/17 12:39
1
1,2-Dichloroethane
ND
1.0
ug/L
11/08/17 12:39
1
1,1-Dichloroethene
ND
1.0
ug/L
11/08/17 12:39
1
1,2-Dichloropropane
ND
1.0
ug/L
11/08/17 12:39
1
Ethylbenzene
ND
1.0
ug/L
11/08/17 12:39
1
2-Hexanone
ND
10
ug/L
11/08/17 12:39
1
1 sopropyl benzene
ND
1.0
ug/L
11/08/17 12:39
1
Methyl acetate
ND
5.0
ug/L
11/08/17 12:39
1
Methylcyclohexane
ND
1.0
ug/L
11/08/17 12:39
1
Methylene Chloride
ND
5.0
ug/L
11/08/17 12:39
1
4-Methyl-2-pentanone
ND
10
ug/L
11/08/17 12:39
1
Methyl tert-butyl ether
ND
10
ug/L
11/08/17 12:39
1
TestArnerica Savannah
Page 126 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 680-50174919
Matrix: Water
Analysis Batch: 501749
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
Styrene
ND
1.0
ug/L
11/08/17 12:39
1
1,1,2,2-Tetrachloroethane
ND
1.0
ug/L
11/08/17 12:39
1
Tetrachloroethene
ND
1.0
ug/L
11/08/17 12:39
1
Tetrahydrofuran
ND
10
ug/L
11/08/17 12:39
1
Toluene
ND
1.0
ug/L
11/08/17 12:39
1
trans- 1,2-Dich loroethene
ND
1.0
ug/L
11/08/17 12:39
1
trans- 1, 3-Dich loropropene
ND
1.0
ug/L
11/08/17 12:39
1
1,2,4-Trichlorobenzene
ND
5.0
ug/L
11/08/17 12:39
1
1,1,1-Trichloroethane
ND
1.0
ug/L
11/08/17 12:39
1
1,1,2-Trichloroethane
ND
1.0
ug/L
11/08/17 12:39
1
Trichloroethene
ND
1.0
ug/L
11/08/17 12:39
1
Trichlorofluoromethane
ND
1.0
ug/L
11/08/17 12:39
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
ug/L
11/08/17 12:39
1
Vinyl chloride
ND
1.0
ug/L
11/08/17 12:39
1
Xylenes, Total
ND
1.0
ug/L
11/08/17 12:39
1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed DR Fac
4-Bromofluorobenzene FSu-rr)
88
80-120
111081171 1
Dibromofluoromethane (Surr)
97
80-122
11108117 12:39 1
1,2-Dichloroethane-d4 (Surr)
91
73-131
11108117 12:39 1
Toluene-d8 (Surr)
98
80-120
11108117 12:39 1
Lab Sample ID: LCS 680-501749/4
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 501749
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
250
259
ug/L
104
68-132
Benzene
50.0
51.7
ug/L
103
80-120
Bromodichloromethane
50.0
54.2
ug/L
108
80-120
Bromoform
50.0
56.9
ug/L
114
52-122
Bromomethane
50.0
65.9
ug/L
132
43-146
2-Butanone
250
255
ug/L
102
79-125
Carbon disulfide
50.0
52.8
ug/L
106
77-129
Carbon tetrachloride
50.0
53.8
ug/L
108
67-125
Chlorobenzene
50.0
51.4
ug/L
103
80-120
Chloroethane
50.0
57.0
ug/L
114
48-145
Chloroform
50.0
51.9
ug/L
104
80-120
Chloromethane
50.0
52.7
ug/L
105
76-149
cis- 1,2-Dichloroethene
50.0
52.6
ug/L
105
80-120
cis- 1,3-Dichloropropene
50.0
55.9
ug/L
112
80-129
Cyclohexane
50.0
52.5
ug/L
105
80-132
Dibromochloromethane
50.0
50.7
ug/L
101
68-120
1,2-Dibromo-3-Chloropropane
50.0
55.3
ug/L
111
74-120
1,2-Dibromoethane
50.0
52.8
ug/L
106
75-126
1,2-Dichlorobenzene
50.0
51.2
ug/L
102
80-120
1,3-Dichlorobenzene
50.0
50.9
ug/L
102
80-120
1,4-Dichlorobenzene
50.0
49.8
ug/L
100
80-120
TestArnerica Savannah
Page 127 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 680-501749/4
Matrix: Water
Analysis Batch: 501749
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Dichlorodifluoromethane
50.0
55.9
ug/L
112
70-137
1,1-Dichloroethane
50.0
53.0
ug/L
106
80-120
1,2-Dichloroethane
50.0
51.0
ug/L
102
72-128
1,1-Dichloroethene
50.0
52.7
ug/L
105
80-120
1,2-Dichloropropane
50.0
52.5
ug/L
105
80-120
Ethylbenzene
50.0
51.6
ug/L
103
80-120
2-Hexanone
250
275
ug/L
110
80-131
1 sopropyl benzene
50.0
53.8
ug/L
108
79-126
Methyl acetate
250
275
ug/L
110
73-139
Methylcyclohexane
50.0
53.9
ug/L
108
80-138
Methylene Chloride
50.0
54.0
ug/L
108
80-120
4-Methyl-2-pentanone
250
275
ug/L
110
80-134
Methyl tert-butyl ether
50.0
51.5
ug/L
103
80-122
Styrene
50.0
53.2
ug/L
106
80-126
1,1,2,2-Tetrachloroethane
50.0
49.7
ug/L
99
76-126
Tetrachloroethene
50.0
52.7
ug/L
105
71-123
Tetrahydrofuran
100
104
ug/L
104
70-133
Toluene
50.0
51.4
ug/L
103
80-120
trans- 1,2-Dich loroethene
50.0
53.7
ug/L
107
80-120
trans- 1, 3-Dich loropropene
50.0
55.3
ug/L
ill
80-128
1,2,4-Trichlorobenzene
50.0
66.3
ug/L
133
71-126
1,1,1-Trichloroethane
50.0
54.0
ug/L
108
80-120
1,1,2-Trichloroethane
50.0
51.0
ug/L
102
80-120
Trichloroethene
50.0
52.7
ug/L
105
80-120
Trichlorofluoromethane
50.0
56.0
ug/L
112
58-127
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
56.1
ug/L
112
75-128
ne
Vinyl chloride
50.0
56.1
ug/L
112
80-129
Xylenes, Total
100
105
ug/L
105
80-120
LCS LCS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
90
80-120
Dibromofluoromethane (Surr)
103
80-122
1,2-Dichloroethane-d4 (Surr)
95
73-131
Toluene-d8 (Surr)
100
80-120
Lab Sample ID: LCSID 680-501749/5
Matrix: Water
Analysis Batch: 501749
Analyte
Acetone
Benzene
Bromodichloromethane
Brornoform
Brornornethane
2-Butanone
Carbon disulfide
Spike
Added
LCSD LCSD
Result Qualifier
250
240
50.0
49.3
50.0
51.3
50.0
55.3
50.0
64.8
250
234
50.0
52.0
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
ug -/L
-96
-(�8-- 13-2
-8
-30
ug/L
99
80-120
5
20
ug/L
103
80-120
6
20
ug/L
111
52-122
3
20
ug/L
130
43-146
2
20
ug/L
93
79-125
9
20
ug/L
104
77-129
2
20
Page 128 of 142
TestArnerica Savannah
11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501749/5 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 501749
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Carbon tetrachloride
50.0
49.5
ug/L
99
67-125
8
20
Chlorobenzene
50.0
49.3
ug/L
99
80-120
4
20
Chloroethane
50.0
54.6
ug/L
109
48-145
4
20
Chloroform
50.0
49.8
ug/L
100
80-120
4
20
Chloromethane
50.0
50.6
ug/L
101
76-149
4
30
cis- 1,2-Dichloroethene
50.0
50.3
ug/L
101
80-120
4
20
cis- 1,3-Dichloropropene
50.0
53.2
ug/L
106
80-129
5
20
Cyclohexane
50.0
49.2
ug/L
98
80-132
6
20
Dibromochloromethane
50.0
47.7
ug/L
95
68-120
6
20
1,2-Dibromo-3-Chloropropane
50.0
50.3
ug/L
101
74-120
9
20
1,2-Dibromoethane
50.0
50.4
ug/L
101
75-126
5
20
1,2-Dichlorobenzene
50.0
49.1
ug/L
98
80-120
4
20
1,3-Dichlorobenzene
50.0
48.8
ug/L
98
80-120
4
20
1,4-Dichlorobenzene
50.0
48.0
ug/L
96
80-120
4
20
Dichlorodifluoromethane
50.0
51.9
ug/L
104
70-137
7
40
1,1-Dichloroethane
50.0
50.0
ug/L
100
80-120
6
20
1,2-Dichloroethane
50.0
49.1
ug/L
98
72-128
4
50
1,1-Dichloroethene
50.0
50.2
ug/L
100
80-120
5
20
1,2-Dichloropropane
50.0
50.3
ug/L
101
80-120
4
20
Ethylbenzene
50.0
49.2
ug/L
98
80-120
5
20
2-Hexanone
250
251
ug/L
100
80-131
9
20
Isopropylbenzene
50.0
51.6
ug/L
103
79-126
4
20
Methyl acetate
250
253
ug/L
101
73-139
8
20
Methylcyclohexane
50.0
50.6
ug/L
101
80-138
6
20
Methylene Chloride
50.0
52.2
ug/L
104
80-120
3
20
4-Methyl-2-pentanone
250
253
ug/L
101
80-134
9
20
Methyl tert-butyl ether
50.0
49.3
ug/L
99
80-122
4
20
Styrene
50.0
52.3
ug/L
105
80-126
2
20
1,1,2,2-Tetrachloroethane
50.0
46.5
ug/L
93
76-126
7
20
Tetrachloroethene
50.0
50.1
ug/L
100
71-123
5
20
Tetrahydrofuran
100
95.7
ug/L
96
70-133
8
30
Toluene
50.0
49.1
ug/L
98
80-120
5
20
trans- 1,2-Dich loroethene
50.0
51.1
ug/L
102
80-120
5
20
trans- 1, 3-Dich loropropene
50.0
52.0
ug/L
104
80-128
6
30
1,2,4-Trichlorobenzene
50.0
65.0
ug/L
130
71-126
2
20
1,1,1-Trichloroethane
50.0
51.0
ug/L
102
80-120
6
20
1,1,2-Trichloroethane
50.0
48.3
ug/L
97
80-120
5
20
Trichloroethene
50.0
49.7
ug/L
99
80-120
6
20
Trichlorofluoromethane
50.0
53.1
ug/L
106
58-127
5
20
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
52.7
ug/L
105
75-128
6
20
ne
Vinyl chloride
50.0
53.9
ug/L
108
80-129
4
20
Xylenes, Total
100
101
ug/L
101
80-120
4
20
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr) 86
80-120
Dibromofluoromethane (Surr) 100
80-122
1,2-Dichloroethane-d4 (Surr) 93
73-131
TestArnerica Savannah
Page 129 of 142 11/10/2017

QC Sample Results
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 680-501749/5
Matrix: Water
Analysis Batch: 501749
LCSD LCSD
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 96 80 - f2O
Lab Sample ID: MB 680-501874/8
Matrix: Water
Analysis Batch: 501874
Analyte
MB MB
Result Qualifier
Trichloroethene
ND
MB MB
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surr)
104
Dibromofluoromethane (Surr)
103
1,2-Dichloroethane-d4 (Surr)
102
Toluene-d8 (Surr)
108
Lab Sample ID: LCS 680-501874/3
Matrix: Water
Analysis Batch: 501874
Analyte
Trichloroethene
LCS LCS
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surr) 105
Dibromofluoromethane (Surr) 110
1,2-Dichloroethane-d4 (Surr) III
Toluene-d8 (Surr) 109
Lab Sample ID: LCSID 680-501874/4
Matrix: Water
Analysis Batch: 501874
Analyte
Trichloroethene
RL
1.0
F
TestArnerica Job ID: 680-144889-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Client Sample ID: Method Blank
Prep Type: Total/NA
MDL Unit D Prepared Analyzed Dil Fac
ug/L 11/09/17 10:07 1
Limits Prepared Analyzed Dil Fac
80-120 11109117 10:07 1
80-122 11109117 10:07 1
73-131 11109117 10:07 1
80-120 11109117 10:07 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
50.0 45.9 ug/L 92 80-120
Limits
80-120
80-122
73-131
80-120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
50.0 47.3 ug/L 95 80-120 3 20
LCSD LCSD
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 106 80-120
Dibromofluoromethane (Surr) 118 80-122
1,2-Dichloroethane-d4 (Surr) 108 73-131
Toluene-d8 (Surr) 106 80-120
Page 130 of 142
TestArnerica Savannah
11/10/2017

Lab Chronicle
Client: GHID Services Inc.
Project/Site: Murphy. NC, October 2017
Client Sample ID: A 155-MW-1 0-102417
Date Collected: 10/24/17 08:53
Date Received: 10/28/17 10:40
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analysis
8260B
Client Sample ID: J1155-MW-11-102417
Date Collected: 10/24/17 09:33
Date Received: 10/28/17 10:40
Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
Client Sample ID: A 155-MW-1 3-102417
Date Collected: 10/24/17 10:39
Date Received: 10/28/17 10:40
Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
Client Sample ID: A 155-MW-1 7-102417
Date Collected: 10/24/17 13:53
Date Received: 10/28/17 10:40
Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
TestArnerica Job ID: 680-144889-1
Lab Sample ID: 680-144889-1
Matrix: Water
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab
1 501188 11/03/17 19:31 CMB TAL SAV
Lab Sample ID: 680-144889-2
Matrix: Water F
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab E:
1 501188 11/03/17 19:55 CMB TAIL SAV
Lab Sample ID: 680-144889-3
Matrix: Water Im
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab
1 501564 11/07/17 18:03 CMB TALSAV
Lab Sample ID: 680-144889-4
Matrix: Water
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab
1 501188 11/03/17 20:20 CMB TALSAV
Client Sample ID: J1155-MW-20-102417 Lab Sample ID: 680-144889-5
Date Collected: 10/24/17 10:07 Matrix: Water
Date Received: 10/28/17 10:40
F Batch Batch Dilution
Prep Type Type Method Run Factor
Total/NA Analysis 8260B 1
Client Sample ID: J1155-MW-28-102417
Date Collected: 10/24/17 15:09
Date Received: 10/28/17 10:40
Batch Prepared
Number or Analyzed Analyst Lab
501355 11/05/17 15:08 CMB TAL SAV
Lab Sample ID: 680-144889-6
Matrix: Water
Batch
Prep Type Type
Batch
Method
Dilution
Run Factor
Batch
Number
Prepared
or Analyzed Analyst Lab
Total/NA An��
8260B
1
501355
11/05/17 14:46 CMB TALSAV
Page 131 of 142
TestArnerica Savannah
11/10/2017

Lab Chronicle
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
Client Sample 11): A 155-MW-33-102517
Date Collected: 10/25/17 09:19
Date Received: 10/28/17 10:40
Batch
Prep Type Type
Total/NA Analysis
Batch
Method Run
8260B
TestArnerica Job ID: 680-144889-1
Lab Sample ID: 680-144889-7
Matrix: Water
Dilution Batch Prepared
Factor Number orAnalyzed Analyst Lab
1 501326 11/04/1715:22 CMB TAL SAV
Client Sample ID: J1155-MW-34-102517 Lab Sample ID: 680-144889-8
Date Collected: 10/25/17 14:41 Matrix: Water
Date Received: 10/28/17 10:40
F Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
Client Sample 11): A 155-MW-35-102417
Date Collected: 10/24/17 11:39
Date Received: 10/28/17 10:40
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab
1 501326 11/04/17 15:47 CMB TAL SAV
Batch Batch Dilution
Prep Type Type Method Run Factor
Total/NA Analysis 8260B 1
Lab Sample ID: 680-144889-9
Matrix: Water M
Batch Prepared
Number or Analyzed Analyst Lab F-
501355 11/05/17 15:30 CMB TALSAV
Client Sample ID: J1155-MW-36-102517
Lab Sample ID: 680-144889-10
Date Collected: 10/25/17 08:28
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed Analyst Lab
Total/NA Analysis 8260B DL
2
501395
11/06/17 13:58 CMB TAL SAV
Total/NA Analysis 8260B
1
501326
11/04/17 16:11 CMB TAL SAV
Client Sample ID: A 155-MW-40-102517
Lab Sample ID: 680-144889-11
Date Collected: 10/25/17 10:05
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed Analyst Lab
Total/NA Analysis 8260B
1
501395
11/06/17 14:20 CMB TAL SAV
Total/NA Analysis 8260B
1
501326
11/04/17 16:36 CMB TAL SAV
Client Sample ID: A 155-MW-41-102517
Lab Sample ID: 680-144889-12
Date Collected: 10/25/17 14:05
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed Analyst Lab
Total/NA Analysis 8260B
10
501727
11/08/17 18:40 CMB TAL SAV
Page 132 of 142
TestArnerica Savannah
11/10/2017

Lab Chronicle
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
Client Sample 11): A 155-MW-42-102417
Date Collected: 10/24/17 13:05
Date Received: 10/28/17 10:40
Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
TestArnerica Job ID: 680-144889-1
Lab Sample ID: 680-144889-13
Matrix: Water
Dilution Batch Prepared
Factor Number orAnalyzed Analyst
1 501355 11/05/1715:52 CMB
Lab
TAL SAV
Client Sample ID: A 155-MW-43-102417 Lab Sample ID: 680-144889-14
Date Collected: 10/24/17 12:30 Matrix: Water
Date Received: 10/28/17 10:40
F Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
Client Sample ID: J1155-MW-45-102417
Date Collected: 10/24/17 14:32
Date Received: 10/28/17 10:40
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab
1 501355 11/05/17 16:14 CMB TAL SAV
Batch Batch Dilution
Prep Type Type Method Run Factor
LTotal/NA Analysis 8260B 1
Lab Sample ID: 680-144889-15
Matrix: Water M
Batch Prepared
Number or Analyzed Analyst Lab F-
501355 11/05/17 16:36 CMB TALSAV
Client Sample ID: J1155-MW-47-102517
Lab Sample ID: 680-144889-16
Date Collected: 10/25/17 13:22
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
orAnalyzed
Analyst Lab
Total/NA Analysis 8260B
1
501727
11/08/17 19:04 CMB TAL SAV
Client Sample ID: A 155-MW-60-102517
Lab Sample ID: 680-144889-17
Date Collected: 10/25/17 11:39
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501326
11/04/17 17:01
CMB TAL SAV
Client Sample ID: J1155-MW-61-102517
Lab Sample ID: 680-144889-18
Date Collected: 10/25/17 10:56
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501326
11/04/17 17:25 CMB TALSAV
Page 133 of 142
TestArnerica Savannah
11/10/2017

Lab Chronicle
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample 11): A 155-MW-62-102517
Lab Sample ID: 680-144889-19
Date Collected: 10/25/17 12:21
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
orAnalyzed
Analyst Lab
Total/NA Analysis 8260B
1
501326
11/04/1717:50 CMB TAL SAV
Client Sample ID: A 155-MW-63-102717
Lab Sample ID: 680-144889-20
Date Collected: 10/27/17 09:09
Matrix: Water
Date Received: 10/28/17 10:40
F Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501694
11/08/1701:22 CMB TAL SAV
Client Sample ID: A 155-PW-1 6-102717
Lab Sample ID: 680-144889-21
Date Collected: 10/27/17 10:35
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501694
11/08/17 01:44 CMB TALSAV
Client Sample ID: J1155-SP-26-102717
Lab Sample ID: 680-144889-22
Date Collected: 10/27/17 11:29
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
orAnalyzed
Analyst Lab
Total/NA Analysis 8260B
1
501694
11/08/1702:06 CMB TAL SAV
Client Sample ID: A 155-CMP-1 -102717
Lab Sample ID: 680-144889-23
Date Collected: 10/27/17 09:35
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501694
11/08/17 02:28 CMB TAL SAV
Client Sample ID: J1155-CMP-3-102717
Lab Sample ID: 680-144889-24
Date Collected: 10/27/17 11:47
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501694
11/08/17 02:50 CMB TALSAV
TestArnerica Savannah
Page 134 of 142 11/10/2017

Lab Chronicle
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
Client Sample ID: A 155-CMP-4-102717
Date Collected: 10/27/17 09:21
Date Received: 10/28/17 10:40
Batch
Prep Type Type
Total/NA Analysis
Batch
Method Run
8260B
TestArnerica Job ID: 680-144889-1
Lab Sample ID: 680-144889-25
Matrix: Water
Dilution Batch Prepared
Factor Number orAnalyzed Analyst
1 501694 11/08/1703:12 CMB
Lab
TAL SAV
Client Sample 11): J1155-SW-3-102717 Lab Sample ID: 680-144889-26
Date Collected: 10/27/17 09:48 Matrix: Water
Date Received: 10/28/17 10:40
F Batch Batch
Prep Type Type Method Run
Total/NA Analysis 8260B
Client Sample 11): A 155-SW-6-102717
Date Collected: 10/27/17 11:09
Date Received: 10/28/17 10:40
Dilution Batch Prepared
Factor Number or Analyzed Analyst Lab
1 501694 11/08/17 03:34 CMB TAL SAV
Batch Batch Dilution
Prep Type Type Method Run Factor
Total/NA Analysis 8260B 1
I
Lab Sample 11): 680-144889-27
Matrix: Water M
Batch Prepared
Number or Analyzed Analyst Lab F-
501694 11/08/17 03:56 CMB TALSAV
Client Sample 11): J1155-SW-10-102717
Lab Sample ID: 680-144889-28
Date Collected: 10/27/17 10:47
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
orAnalyzed
Analyst Lab
Total/NA Analysis 8260B
1
501730
11/08/17 11:28 CMB TAL SAV
Client Sample 11): A 155-RW-2-102617
Lab Sample 11): 680-144889-29
Date Collected: 10/26/17 16:49
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501359
11/05/17 20:30 CMB TAL SAV
Client Sample ID: J1155-RW-3-102617
Lab Sample ID: 680-144889-30
Date Collected: 10/26/17 16:56
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
2
501359
11/05/17 20:54 CMB TALSAV
Page 135 of 142
TestArnerica Savannah
11/10/2017

Lab Chronicle
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
TestArnerica Job ID: 680-144889-1
Client Sample ID: A 155-RW-5-102617
Lab Sample ID: 680-144889-31
Date Collected: 10/26/17 16:38
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed Analyst Lab
Total/NA Analysis 8260B b—L
20
501874
11/09/17 12:46 CMB TAL SAV
Total/NA Analysis 8260B
10
501564
11/07/17 17:14 CMB TALSAV
Client Sample ID: J1155-DUP-1-102417
Lab Sample ID: 680-144889-32
Date Collected: 10/24/17 16:00
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
F
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501355
11/05/17 16:58 CMB TAL SAV
Client Sample ID: J1155-DUP-2-102417
Lab Sample ID: 680-144889-33
Date Collected: 10/24/17 16:10
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501355
11/05/17 21:00 CMB TALSAV
Client Sample ID: J1155-DUP-3-102517
Lab Sample ID: 680-144889-34
Date Collected: 10/25/17 16:00
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501326
11/04/17 18:15 CMB TALSAV
Client Sample ID: A 155-DUP-4-102517
Lab Sample ID: 680-144889-35
Date Collected: 10/25/17 16:10
Matrix: Water
Date Received: 10/28/17 10:40
r Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501749
11/08/17 16:20 CMB TAL SAV
Client Sample ID: J1155-EB-01-102417
Lab Sample ID: 680-144889-36
Date Collected: 10/24/17 15:32
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501188
11/03/17 17:52 CMB TALSAV
TestArnerica Savannah
Page 136 of 142 11/10/2017

Lab Chronicle
Client: GHD Services Inc.
Project/Site: Murphy. NC, October 2017
F
TestArnerica Job ID: 680-144889-1
Client Sample 11): A 155-EB-02-102517
Lab Sample ID: 680-144889-37
Date Collected: 10/25/17 15:53
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
orAnalyzed
Analyst Lab
Total/NA Analysis 8260B
1
501326
11/04/1718:39 CMB TAL SAV
Client Sample ID: J1155-EB-03-102617
Lab Sample ID: 680-144889-38
Date Collected: 10/26/17 16:40
Matrix: Water
Date Received: 10/28/17 10:40
F
F Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501359
11/05/17 16:23 CMB TAL SAV
Client Sample ID: J1155-EB-04-102717
Lab Sample ID: 680-144889-39
Date Collected: 10/27117 13:55
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
or Analyzed
Analyst Lab
Total/NA Analysis 8260B
1
501694
11/07/17 21:19 CMB TALSAV
Client Sample ID: A 155-TB-1 02417
Lab Sample ID: 680-144889-40
Date Collected: 10/24/17 08:00
Matrix: Water
Date Received: 10/28/17 10:40
Batch Batch
Dilution
Batch
Prepared
Prep Type Type Method Run
Factor
Number
orAnalyzed
Analyst Lab
Total/NA Analysis 8260B
1
501188
11/03/1717:27 CMB TAL SAV
Laboratory References:
TAL SAV = TestArnerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
TestArnerica Savannah
Page 137 of 142 11/10/2017

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11/10/2017

Accreditation/Certification Summary
Client: GHID Services Inc. TestArnerica Job ID: 680-144889-1
Project/Site: Murphy. NC, October 2017
Laboratory: TestArnerica Savannah
The accreditations/certifications listed below are applicable to this report
I Authority Program EPA Region Identification Number Expiration Date
L North Carolina (DW) State Program 4 13701 07-31-18
TestArnerica Savannah
Page 142 of 142 11/10/2017

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-139553-1
Client Project/Site: NGC-Murphy NC
For-
CDM Smith, Inc.
9420 Bunsen Parkway
Suite 225
Louisville, Kentucky 40220
Attn: Mr. Phillip Hendershot
R"0_44U� 6"rv:s
Authorized for release by.-
1111012017 3:32:24 PM
Roxanne Cisneros, Senior Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Table of Contents
TestAmerica Job ID: 490-139553-1
CoverPage ..............................................
1
Table of Contents .........................................
2
Sample Summary .........................................
3
Case Narrative ...........................................
4
Definitions...............................................
6
Client Sample Results ......................................
8
QC Sample Results ........................................
28
QC Association ...........................................
52
Chronicle................................................
58
Method Summary .........................................
62
Certification Summary ......................................
63
Chain of Custody ..........................................
64
Receipt Checklists .........................................
69
TestAmerica Nashville
Page 2 of 70 11/10/2017

Sample Summary
Client: CIDIVI Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
490-139553-1
J 1 155-MW-1 2-102617
Water
10/26/17 09:01
10/27/17 09:45
490-139553-2
J 1 155-MW-37-102617
Water
10/26/17 10:02
10/27/17 09:45
490-139553-3
A 155-PM-3S-102617
Water
10/26/17 12:49
10/27/17 09:45
490-139553-4
J1 155-PM-3D-102617
Water
10/26/17 11:34
10/27/17 09:45
490-139553-5
J 1 155-PM-7D-1 02617
Water
10/26/17 14:00
10/27/17 09:45
490-139553-6
J1 155-RW-4-102617
Water
10/26/17 14:10
10/27/17 09:45
490-139553-7
J 1 155-DU P-1 -102617
Water
10/26/17 16:00
10/27/17 09:45
TestAmerica Nashville
Page 3 of 70 11/10/2017

Case Narrative
Client: CIDM Smith, Inc.
Project/Site: NGC-Murphy NC
Job ID: 490-139553-1
Laboratory: TestArnerica Nashville
Narrative
ob Narrative
490-139553-1
Comments
No additional comments.
TestAmerica Job ID: 490-139553-1
Receipt
The samples were received on 10/27/2017 9:45 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 0.21 C, 1.41 C and 4.51 C.
GC/IVIS VOA
Method(s) 8260B: The laboratory control sample (LCS) for analytical batch 490-471321 recovered outside control limits for Methyl acetate.
This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data have been reported.
Method(s) 8260B: The RPID of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for batch analytical
batch 490-471321 recovered outside control limits for the following analytes: Dichlorobromomethane, 2-Hexanone,
cis- 1, 3-Dichloropropene, 1,2,4-Trichlorobenzene, trans- 1, 3-Dich loropropene, cis- 1,2-Dichloroethene, Toluene, 1,1,2-Trichloroethane,
Isopropylbenzene, 4-Methyl-2-pentanone (MIBK), Tetrachloroethene, 1,2-Dibromo-3-Chloropropane, Methylcyclohexane and
1,2-Dichloropropane.
Method(s) 8260B: The laboratory control sample duplicate (LCSD) for analytical batch 490-472139 recovered outside control limits for the
following analytes: 1,2-Dichloroethane, cis-1,3-Dichloropropene . These analytes were biased high in the LCSD and were not detected in
the associated samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/IVIS Semi VOA
Method(s) 8270D: The continuing calibration verification (CCVIS) analyzed in batch 490-471924 was outside the method criteria for the
following analyte(s): 1,4-Dioxane. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to
be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is
considered estimated.
Method(s) 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-471651 and analytical batch 490-471924.
Method(s) 8270D: The following samples was diluted to bring the concentration of target analytes within the calibration range:
J1155-MW-12-102617 (490-139553-1) and J1155-PM-7D-102617 (490-139553-5). Elevated reporting limits (RI-s) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
HPLC/IC
Method(s) 300.0: The following samples was diluted due to the nature of the sample matrix: J1 155-MW-37-102617 (490-139553-2),
J1155-PM-3S-102617 (490-139553-3) and J1155-PM-3D-102617 (490-139553-4), and J1155-PM-7D-102617 (490-139553-5). Elevated
reporting limits (RLs) are provided.
Method(s) VFA-IC: The following samples was diluted due to odor: J1 155-MW-12-102617 (490-139553-1), J1 155-MW-37-102617
(490-139553-2), J1 155-PM-3S-1 02617 (490-139553-3), J1 155-PM-3D-102617 (490-139553-4), J1 155-PM-7D-102617 (490-139553-5)
and J1155-RW-4-102617 (490-139553-6). Elevated reporting limits (RL) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method(s) RSK-1 75: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-473602.
a
L
TestAmerica Nashville
Page 4 of 70 11/10/2017

Case Narrative
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Job ID: 490-139553-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals L
Method(s) 200.8: The matrix spike / matrix spike duplicate / sample duplicate (MS/MSD/DUP) precision for preparation batch 490-472038
and 490-472422 and analytical batch 490-472734 was outside control limits. Sample matrix interference and/or non -homogeneity are
suspected because the associated laboratory control sample / laboratory control sample duplicate (LCS/LCSD) and post dilution spike
(PDS) precision was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
General Chemistry
Method(s) SM 4500 P E: The initial calibration blank and continuing calibration blank for analytical batch 490-471764 contained
Orthophosphate as P above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore,
re -extraction and/or re -analysis of samples was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
Method(s) 351OC: The following samples formed emulsions during the extraction procedure: J1 155-MW-12-102617 (490-139553-1),
J1 155-MW-37-102617 (490-139553-2), A 155-PM-3S-102617 (490-139553-3), J1 155-PM-3D-102617 (490-139553-4),
J1155-PM-7D-102617 (490-139553-5) and J1155-RW-4-102617 (490-139553-6). The emulsions were broken up using centrifugation.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica Nashville
Page 5 of 70 11/10/2017

Definitions/Glossary
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
yuaimers
GUMS VOA
TestAmerica Job ID: 490-139553-1
Qualifier Qualifier Description
F2 MS/MSD RPD exceeds control limits
RPD of the LCS and LCSD exceeds the control limits
F1 MS and/or MSD Recovery is outside acceptance limits.
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
LCS or LCSD is outside acceptance limits.
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
E Result exceeded calibration range.
GC/MS Semi VOA
Qualifier Qualifier Description
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC VOA
Qualifier Qualifier Description
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
HPLC/lC
Qualifier Qualifier Description _F_
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
F 1 MS and/or MSD Recovery is outside acceptance limits.
Metals
Qualifier Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
F1 MS and/or MSD Recovery is outside acceptance limits.
F3 Duplicate RPD exceeds the control limit
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
12 Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
VIDA Minimum Detectable Activity (Radiochemistry)
VIDC Minimum Detectable Concentration (Radiochemistry)
VIDL Method Detection Limit
VIL Minimum Level (Dioxin)
TestAmerica Nashville
Page 6 of 70 11/10/2017

Definitions/Glossary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Glossary (Continued)
Abbreviation These commonly used abbreviations may or may not be present in this report.
NC
Not Calculated
IND
Not Detected at the reporting limit (or MDL or EDL if shown)
PQL
Practical Quantitation Limit
QC
Quality Control
RER
Relative Error Ratio (Radiochemistry)
RL
Reporting Limit or Requested Limit (Radiochemistry)
RPD
Relative Percent Difference, a measure of the relative difference between two points
TEF
Toxicity Equivalent Factor (Dioxin)
TEQ
Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 7 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1155-MW-12-102617 Lab Sample ID: 490-139553-1
Date Collected: 10/26/17 09:01 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/27/17 18:12
1
Benzene
1.46
0.500
0.200
ug/L
10/27/17 18:12
1
Bromodichloromethane
0.218 J*
0.500
0.170
ug/L
10/27/17 18:12
1
Brornoform
ND
0.500
0.290
ug/L
10/27/17 18:12
1
Brornornethane
ND
0.500
0.350
ug/L
10/27/17 18:12
1
2-Butanone (MEK)
ND F1 F2
50.0
2.64
ug/L
10/27/17 18:12
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/27/17 18:12
1
Carbon tetrachloride
ND F2
0.500
0.180
ug/L
10/27/17 18:12
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/27/17 18:12
1
Chloroethane
ND F1
0.500
0.360
ug/L
10/27/17 18:12
1
Chloroform
12.5 F2
0.500
0.230
ug/L
10/27/17 18:12
1
Chloromethane
ND F1
0.500
0.360
ug/L
10/27/17 18:12
1
cis-1,2-Dichloroethene
388 * F2
0.500
0.210
ug/L
10/27/17 18:12
1
cis- 1,3-Dichloropropene
ND *
0.500
0.170
ug/L
10/27/17 18:12
1
Cyclohexane
ND
1.00
0.130
ug/L
10/27/17 18:12
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/27/17 18:12
1
1,2-Dibromo-3-Chloropropane
ND *
5.00
0.940
ug/L
10/27/17 18:12
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/27/17 18:12
1
1,2-Dichlorobenzene
0.721
0.500
0.190
ug/L
10/27/17 18:12
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/27/17 18:12
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/27/17 18:12
1
Dichlorodifluoromethane
59.5
0.500
0.170
ug/L
10/27/17 18:12
1
1,1-Dichloroethane
105
0.500
0.240
ug/L
10/27/17 18:12
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/27/17 18:12
1
1,1-Dichloroethene
219
2.50
1.25
ug/L
10/31/17 13:33
5
1,2-Dichloropropane
ND *
0.500
0.250
ug/L
10/27/17 18:12
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/27/17 18:12
1
2-Hexanone
ND *
5.00
1.28
ug/L
10/27/17 18:12
1
1 sopropyl benzene
ND *
1.00
0.330
ug/L
10/27/17 18:12
1
Methyl acetate
ND *
10.0
0.580
ug/L
10/27/17 18:12
1
Methylcyclohexane
ND *
0.500
0.0900
ug/L
10/27/17 18:12
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/27/17 18:12
1
4-Methyl-2-pentanone (MIBK)
ND *
5.00
0.810
ug/L
10/27/17 18:12
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/27/17 18:12
1
Styrene
ND
0.500
0.280
ug/L
10/27/17 18:12
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/27/17 18:12
1
Tetrachloroethene
176 *
0.500
0.140
ug/L
10/27/17 18:12
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/27/17 18:12
1
Toluene
ND *
0.500
0.170
ug/L
10/27/17 18:12
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/27/17 18:12
1
trans- 1, 3-Dich loropropene
ND *
0.500
0.170
ug/L
10/27/17 18:12
1
1,2,4-Trichlorobenzene
ND *
0.500
0.200
ug/L
10/27/17 18:12
1
11,11,11-Trichloroethane
136 F2
0.500
0.190
ug/L
10/27/17 18:12
1
1,1,2-Trichloroethane
1.53
0.500
0.190
ug/L
10/27/17 18:12
1
Trichloroethene
1690
2.50
1.00
ug/L
10/31/17 13:33
5
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/27/17 18:12
1
1,1,2-Trichloro-1,2,2-trifluoroetha
376
1.00
0.150
ug/L
10/27/17 18:12
1
ne
Vinyl chloride
3.79 F1
0.500
0.180
ug/L
10/27/17 18:12
1
M
TestAmerica Nashville
Page 8 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Client Sample ID: J1155-MW-12-102617
Lab Sample
ID: 490-139553-1
Date Collected: 10/26/17 09:01
Matrix:
Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Xylenes, Total
ND
1.50
0.580 ug/L
10/27/17 18:12
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene Fsu-rr)
90
70-130
10127117 18:12
1
4-Bromofluorobenzene (Surr)
94
70-130
10131117 13:33
5
Dibromofluoromethane (Surr)
108
70-130
10127117 18:12
Dibromofluoromethane (Surr)
86
70-130
10131117 13:33
5
1,2-Dichloroethane-d4 (Surr)
116
70-130
10127117 18:12
'
1,2-Dichloroethane-d4 (Surr)
109
70-130
10131117 13:33
5
Toluene-d8 (Surr)
103
70-130
10127117 18:12
1
Toluene-d8 (Surr)
103
70-130
10131117 13:33
5
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
47.7
18.5
11.3 ug/L
10/28/17 20:55
10/30/17 16:14
2
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
81
10-120
10128117 20:55
10130117 16:14
2
2-Fluorobiphenyl (Surr)
79
29-120
10128117 20:55
10130117 16:14
2
2-Fluorophenol (Surr)
67
10-120
10128117 20:55
10130117 16:14
2
Nitrobenzene-d5 (Surr)
82
27-120
10128117 20:55
10130117 16:14
2
Phenol-d5 (Surr)
49
10-120
10128117 20:55
10130117 16:14
2
Terphenyl-d14 (Surr)
95
13-120
10128117 20:55
10130117 16:14
2
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Ethane
ND
0.00500
0.00270 mg/L
11/06/17 12:18
1
Ethylene
0.00333 J
0.00500
0.00220 mg/L
11/06/17 12:18
1
Methane
0.0982
0.00500
0.00170 mg/L
11/06/17 12:18
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Acetylene (Surr)
96
62-124
11106117 12:18
1
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chloride
8.62
1.00
0.700 mg/L
10/27/17 16:14
1
Nitrate as N
0.0586 J
0.100
0.0500 mg/L
10/27/17 16:14
1
Sulfate
15.2
1.00
0.600 mg/L
10/27/17 16:14
1
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Iron
ND
0.100
0.0500
mg/L
11/01/1707:32
11/02/1702:40
1
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.261
F1
0.00400
0.00150
mg/L
11/01/1707:37
11/01/1716:12
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
0.0828
0.0500
0.0500
mg/L
11/01/17 11:12
1
Sulfide
ND
5.00
0.700
mg/L
11/01/17 13:00
11/01/17 15:00
1
Total Organic Carbon
0.563
J
1.00
0.500
mg/L
11/08/17 19:17
1
TestAmerica Nashville
Page 9 of 70 11/10/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-MW-1
2-102617
Lab Sample ID: 490-139553-1
Date Collected: 10/26/17 09:01
Matrix: Water
Date Received: 10/27/17 09:45
General Chemistry (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Alkalinity
138
10.0
5.00
mg/L
11/08/17 11:13 1
Total Dissolved Solids
250
10.0
7.00
mg/L
11/01/17 19:09 1
Orthophosphate as P
ND
0.100
0.0500
mg/L
10/27/17 17:13 1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 07:37 5
Formic -acid
ND
5.00
1.30
mg/L
11/07/17 07:37 5
Lactic acid
ND
5.00
1.55
mg/L
11/07/17 07:37 5
n-Butyric Acid
ND
5.00
1.30
mg/L
11/07/17 07:37 5
Propionic acid
ND
5.00
1.75
mg/L
11/07/17 07:37 5
Pyruvic Acid
ND
7.50
1.85
mg/L
11/07/17 07:37 5
TestAmerica Nashville
Page 10 of 70
11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1155-MW-37-102617 Lab Sample ID: 490-139553-2
Date Collected: 10/26/17 10:02 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/27/17 18:38
1
Benzene
ND
0.500
0.200
ug/L
10/27/17 18:38
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/27/17 18:38
1
Brornoform
ND
0.500
0.290
ug/L
10/27/17 18:38
1
Brornornethane
ND
0.500
0.350
ug/L
10/27/17 18:38
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/27/17 18:38
1
Carbon disulficle
0.309 J
0.500
0.220
ug/L
10/27/17 18:38
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/27/17 18:38
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/27/17 18:38
1
Chloroethane
ND
0.500
0.360
ug/L
10/27/17 18:38
1
Chloroform
0.361 J
0.500
0.230
ug/L
10/27/17 18:38
1
Chloromethane
ND
0.500
0.360
ug/L
10/27/17 18:38
1
cis-1,2-Dichloroethene
1550
25.0
10.5
ug/L
10/31/17 15:15
50
cis- 1,3-Dichloropropene
ND *
0.500
0.170
ug/L
10/27/17 18:38
1
Cyclohexane
ND
1.00
0.130
ug/L
10/27/17 18:38
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/27/17 18:38
1
1,2-Dibromo-3-Chloropropane
ND *
5.00
0.940
ug/L
10/27/17 18:38
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/27/17 18:38
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/27/17 18:38
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/27/17 18:38
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/27/17 18:38
1
Dichlorodifluoromethane
13.7
0.500
0.170
ug/L
10/27/17 18:38
1
1,1-Dichloroethane
224
0.500
0.240
ug/L
10/27/17 18:38
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/27/17 18:38
1
1,1-Dichloroethene
ill
0.500
0.250
ug/L
10/27/17 18:38
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/27/17 18:38
1
Ethylbenzene
0.224 J
0.500
0.190
ug/L
10/27/17 18:38
1
2-Hexanone
ND *
5.00
1.28
ug/L
10/27/17 18:38
1
lsopropyl benzene
0.582 J
1.00
0.330
ug/L
10/27/17 18:38
1
Methyl acetate
ND *
10.0
0.580
ug/L
10/27/17 18:38
1
Methylcyclohexane
ND *
0.500
0.0900
ug/L
10/27/17 18:38
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/27/17 18:38
1
4-Methyl-2-pentanone (MIBK)
ND *
5.00
0.810
ug/L
10/27/17 18:38
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/27/17 18:38
1
Styrene
ND
0.500
0.280
ug/L
10/27/17 18:38
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/27/17 18:38
1
Tetrachloroethene
253 *
0.500
0.140
ug/L
10/27/17 18:38
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/27/17 18:38
1
Toluene
0.448 J
0.500
0.170
ug/L
10/27/17 18:38
1
trans-1,2-Dichloroethene
5.41
0.500
0.230
ug/L
10/27/17 18:38
1
trans- 1, 3-Dich loropropene
ND *
0.500
0.170
ug/L
10/27/17 18:38
1
1,2,4-Trichlorobenzene
ND *
0.500
0.200
ug/L
10/27/17 18:38
1
11,11,11-Trichloroethane
17.1
0.500
0.190
ug/L
10/27/17 18:38
1
1,1,2-Trichloroethane
ND *
0.500
0.190
ug/L
10/27/17 18:38
1
Trichloroethene
10700
25.0
10.0
ug/L
10/31/17 15:15
50
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/27/17 18:38
1
1,1,2-Trichloro-1,2,2-trifluoroetha
20.8
1.00
0.150
ug/L
10/27/17 18:38
1
ne
Vinyl chloride
39.6
0.500
0.180
ug/L
10/27/17 18:38
1
M
TestAmerica Nashville
Page 11 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Client Sample ID: J1155-MW-37-102617
Lab Sample
ID: 490-139553-2
Date Collected: 10/26/17 10:02
Matrix:
Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Xylenes, Total
ND
1.50
0.580 ug/L
10/27/17 18:38
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene Fsu-rr)
98
70-130
10127117 18:38
1
4-Bromofluorobenzene (Surr)
118
70-130
10131117 15:15
50
Dibromofluoromethane (Surr)
106
70-130
10127117 18:38
Dibromofluoromethane (Surr)
106
70-130
10131117 15:15
50
1,2-Dichloroethane-d4 (Surr)
109
70-130
10127117 18:38
'
1,2-Dichloroethane-d4 (Surr)
117
70-130
10131117 15:15
50
Toluene-d8 (Surr)
104
70-130
10127117 18:38
1
Toluene-d8 (Surr)
104
70-130
10131117 15:15
50
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
ND
9.26
5.65 ug/L
10/28/17 20:55
10/30/17 14:29
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
60
10-120
10128117 20:55
10130117 14:29
1
2-Fluorobiphenyl (Surr)
62
29-120
10128117 20:55
10130117 14:29
1
2-Fluorophenol (Surr)
49
10-120
10128117 20:55
10130117 14:29
1
Nitrobenzene-d5 (Surr)
62
27-120
10128117 20:55
10130117 14:29
1
Phenol-d5 (Surr)
37
10-120
10128117 20:55
10130117 14:29
1
Terphenyl-d14 (Surr)
74
13-120
10128117 20:55
10130117 14:29
1
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Ethane
0.00724
0.00500
0.00270 mg/L
11/06/17 12:23
1
Ethylene
0.0748
0.00500
0.00220 mg/L
11/06/17 12:23
1
Methane
0.00886
0.00500
0.00170 mg/L
11/06/17 12:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Acetylene (Surr)
92
62-124
11106117 12:23
1
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chloride
19.3
1.00
0.700 mg/L
10/27/17 16:24
1
Nitrate as N
ND
0.500
0.250 mg/L
10/27/17 17:42
5
Sulfate
32.5
5.00
3.00 mg/L
10/27/17 17:42
5
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Iron
ND
0.100
0.0500
mg/L
11/01/1707:32
11/02/1703:16
1
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.144
0.00400
0.00150
mg/L
11/01/1707:37
11/01/1716:33
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
0.128
0.0500
0.0500
mg/L
11/01/17 11:13
1
Sulfide
ND
5.00
0.700
mg/L
11/01/17 13:00
11/01/17 15:00
1
Total Organic Carbon
ND
1.00
0.500
mg/L
11/08/17 20:44
1
TestAmerica Nashville
Page 12 of 70 11/10/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1155-MW-37-102617
Lab Sample ID: 490-139553-2
Date Collected: 10/26/17 10:02
Matrix: Water
Date Received: 10/27/17 09:45
General Chemistry (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Alkalinity
143
10.0
5.00
mg/L
11/08/17 11:20 1
Total Dissolved Solids
279
10.0
7.00
mg/L
11/01/17 19:09 1
Orthophosphate as P
0.153
0.100
0.0500
mg/L
10/27/17 17:18 1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 08:06 5
Formic -acid
ND
5.00
1.30
mg/L
11/07/17 08:06 5
Lactic acid
ND
5.00
1.55
mg/L
11/07/17 08:06 5
n-Butyric Acid
ND
5.00
1.30
mg/L
11/07/17 08:06 5
Propionic acid
ND
5.00
1.75
mg/L
11/07/17 08:06 5
Pyruvic Acid
ND
7.50
1.85
mg/L
11/07/17 08:06 5
TestAmerica Nashville
Page 13 of 70
11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-3S-1 02617 Lab Sample ID: 490-139553-3
Date Collected: 10/26/17 12:49 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/27/17 19:03
1
Benzene
214
5.00
2.00
ug/L
10/31/17 14:49
10
Bromodichloromethane
ND
0.500
0.170
ug/L
10/27/17 19:03
1
Bromoform
ND
0.500
0.290
ug/L
10/27/17 19:03
1
Bromomethane
ND
0.500
0.350
ug/L
10/27/17 19:03
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/27/17 19:03
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/27/17 19:03
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/27/17 19:03
1
Chlorobenzene
6.22
0.500
0.180
ug/L
10/27/17 19:03
1
Chloroethane
ND
0.500
0.360
ug/L
10/27/17 19:03
1
Chloroform
ND
0.500
0.230
ug/L
10/27/17 19:03
1
Chloromethane
ND
0.500
0.360
ug/L
10/27/17 19:03
1
cis- 1,2-Dichloroethene
ND
5.00
2.10
ug/L
10/31/17 14:49
10
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/27/17 19:03
1
Cyclohexane
ND
1.00
0.130
ug/L
10/27/17 19:03
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/27/17 19:03
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/27/17 19:03
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/27/17 19:03
1
1,2-Dichlorobenzene
0.469 J
0.500
0.190
ug/L
10/27/17 19:03
1
1,3-Dichlorobenzene
0.874
0.500
0.180
ug/L
10/27/17 19:03
1
1,4-Dichlorobenzene
0.603
0.500
0.170
ug/L
10/27/17 19:03
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/27/17 19:03
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/27/17 19:03
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/27/17 19:03
1
1,1-Dichloroethene
0.396 J
0.500
0.250
ug/L
10/27/17 19:03
1
1,2-Dichloropropane
ND *
0.500
0.250
ug/L
10/27/17 19:03
1
Ethylbenzene
0.262 J
0.500
0.190
ug/L
10/27/17 19:03
1
2-Hexanone
ND *
5.00
1.28
ug/L
10/27/17 19:03
1
1 sopropyl benzene
ND *
1.00
0.330
ug/L
10/27/17 19:03
1
Methyl acetate
ND *
10.0
0.580
ug/L
10/27/17 19:03
1
Methylcyclohexane
ND *
0.500
0.0900
ug/L
10/27/17 19:03
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/27/17 19:03
1
4-Methyl-2-pentanone (MIBK)
ND *
5.00
0.810
ug/L
10/27/17 19:03
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/27/17 19:03
1
Styrene
ND
0.500
0.280
ug/L
10/27/17 19:03
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/27/17 19:03
1
Tetrachloroethene
0.226 J
0.500
0.140
ug/L
10/27/17 19:03
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/27/17 19:03
1
Toluene
2.68 *
0.500
0.170
ug/L
10/27/17 19:03
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/27/17 19:03
1
trans- 1, 3-Dich loropropene
ND *
0.500
0.170
ug/L
10/27/17 19:03
1
1,2,4-Trichlorobenzene
ND *
0.500
0.200
ug/L
10/27/17 19:03
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/27/17 19:03
1
1,1,2-Trichloroethane
ND *
0.500
0.190
ug/L
10/27/17 19:03
1
Trichloroethene
10.1
5.00
2.00
ug/L
10/31/17 14:49
10
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/27/17 19:03
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.150
ug/L
10/27/17 19:03
1
Vinyl chloride
ND
0.500
0.180
ug/L
10/27/17 19:03
1
Xylenes, Total
ND
1.50
0.580
ug/L
10/27/17 19:03
1
M
TestAmerica Nashville
Page 14 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Client Sample ID: A 155-PM-3S-1 02617
Lab Sample
ID: 490-139553-3
Date Collected: 10/26/17 12:49
Matrix:
Water
Date Received: 10/27/17 09:45
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
98
70-130
10127117 19:03
1
4-Bromofluorobenzene (Surr)
98
70-130
10131117 14:49
10
Dibromofluoromethane (Surr)
85
70-130
10127117 19:03
1
Dibromofluoromethane (Surr)
83
70-130
10131117 14:49
10
1,2-Dichloroethane-d4 (Surr)
115
70-130
10127117 19:03
1
1,2-Dichloroethane-d4 (Surr)
117
70-130
10131117 14:49
Toluene-d8 (Surr)
102
70-130
10127117 19:03
1
Toluene-d8 (Surr)
123
70-130
10131117 14:49
lo
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
27.2
8.77
5.35 ug/L
10/28/17 20:55
10/30/17 14:50
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
DY Fac
2,4,6-Tribromophenol (Surr)
67
10-120
10128117 20:55
10130117 14:50
1
2-Fluorobiphenyl (Surr)
60
29-120
10128117 20:55
10130117 14:50
1
2-Fluorophenol (Surr)
47
10-120
10128117 20:55
10130117 14:50
1
Nitrobenzene-d5 (Surr)
63
27-120
10128117 20:55
10130117 14:50
1
Phenol-d5 (Surr)
33
10-120
10128117 20:55
10130117 14:50
1
Terphenyl-d14 (Surr)
78
13-120
10128117 20:55
10130117 14:50
1
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Ethane
--"6456 J-
ObO600
ObUM mgiL�
1��
1
Ethylene
0.00625
0.00500
0.00220 mg/L
11/06/17 12:30
1
Methane
0.00463 J
0.00500
0.00170 mg/L
11/06/17 12:30
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Acetylene (Surr)
100
62-124
11106117 12:30
1
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chloride
145
10.0
7.00 mg/L
10/27/17 17:52
10
Nitrate as N
2.66
0.100
0.0500 mg/L
10/27/17 16:33
1
Sulfate
104
10.0
6.00 mg/L
10/27/17 17:52
10
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Iron
ND
0.100
0.0500 mg/L
11/01/1707:32
11/02/1703:21
1
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.0494
0.00400
0.00150
mg/L
11/01/17 07:37
11/01/17 16:36
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
1.67
0.0500
0.0500
mg/L
11/01/17 11:14
1
Sulfide
ND
5.00
0.700
mg/L
11/01/17 13:00
11/01/17 15:00
1
Total Organic Carbon
5.08
1.00
0.500
mg/L
11/08/17 21:12
1
Alkalinity
40.4
10.0
5.00
mg/L
11/08/17 11:27
1
Total Dissolved Solids
474
10.0
7.00
mg/L
11/01/17 19:09
1
Orthophosphate as P
ND
0.100
0.0500
mg/L
10/27/17 17:19
1
TestAmerica Nashville
Page 15 of 70 11/10/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-3S-1 02617 Lab Sample ID: 490-139553-3
Date Collected: 10/26/17 12:49 Matrix: Water
Date Received: 10/27/17 09:45
General Chemistry (Continued)
Analyte
Acetic acid
Formic -acid
Lactic acid
n-Butyric Acid
Propionic acid
Pyruvic Acid
Result Qualifier
RL
MDL
Unit D
6.17
5.00
1.45
mg/L
ND
5.00
1.30
mg/L
ND
5.00
1.55
mg/L
ND
5.00
1.30
mg/L
ND
5.00
1.75
mg/L
ND
7.50
1.85
mg/L
Prepared
Analyzed
11/07/17 08:35
11/07/17 08:35
11/07/17 08:35
11/07/17 08:35
11/07/17 08:35
11/07/17 08:35
Dil Fac
5
5 E.
5
5
5
5 E
E
TestAmerica Nashville
Page 16 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-3D-1 02617 Lab Sample ID: 490-139553-4
Date Collected: 10/26/17 11:34 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
10.5
5.00
2.66
ug/L
10/31/17 13:07
1
Benzene
2.13
0.500
0.200
ug/L
10/31/17 13:07
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/31/17 13:07
1
Bromoform
ND
0.500
0.290
ug/L
10/31/17 13:07
1
Bromomethane
ND
0.500
0.350
ug/L
10/31/17 13:07
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/31/17 13:07
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/31/17 13:07
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/31/17 13:07
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/31/17 13:07
1
Chloroethane
ND
0.500
0.360
ug/L
10/31/17 13:07
1
Chloroform
ND
0.500
0.230
ug/L
10/31/17 13:07
1
Chloromethane
ND
0.500
0.360
ug/L
10/31/17 13:07
1
cis- 1,2-Dichloroethene
ND
0.500
0.210
ug/L
10/31/17 13:07
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/31/17 13:07
1
Cyclohexane
ND
1.00
0.130
ug/L
10/31/17 13:07
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/31/17 13:07
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/31/17 13:07
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/31/17 13:07
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/31/17 13:07
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/31/17 13:07
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/31/17 13:07
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/31/17 13:07
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/31/17 13:07
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/31/17 13:07
1
1,1-Dichloroethene
0.775
0.500
0.250
ug/L
10/31/17 13:07
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/31/17 13:07
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/31/17 13:07
1
2-Hexanone
ND
5.00
1.28
ug/L
10/31/17 13:07
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/31/17 13:07
1
Methyl acetate
ND
10.0
0.580
ug/L
10/31/17 13:07
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/31/17 13:07
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/31/17 13:07
1
4-Methyl-2-pentanone (MIBK)
4.04 J
5.00
0.810
ug/L
10/31/17 13:07
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/31/17 13:07
1
Styrene
ND
0.500
0.280
ug/L
10/31/17 13:07
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/31/17 13:07
1
Tetrachloroethene
0.382 J
0.500
0.140
ug/L
10/31/17 13:07
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/31/17 13:07
1
Toluene
0.249 J
0.500
0.170
ug/L
10/31/17 13:07
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/31/17 13:07
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/31/17 13:07
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/31/17 13:07
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/31/17 13:07
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/31/17 13:07
1
Trichloroethene
10.8
0.500
0.200
ug/L
10/31/17 13:07
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/31/17 13:07
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.150
ug/L
10/31/17 13:07
1
Vinyl chloride
ND
0.500
0.180
ug/L
10/31/17 13:07
1
Xylenes, Total
ND
1.50
0.580
ug/L
10/31/17 13:07
1
TestAmerica Nashville
Page 17 of 70 11/10/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-3D-1 02617 Lab Sample ID: 490-139553-4
Date Collected: 10/26/17 11:34 Matrix: Water
Date Received: 10/27/17 09:45
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
100
70-130
Dibromofluoromethane (Surr)
92
70-130
1,2-Dichloroethane-d4 (Surr)
118
70-130
Toluene-d8 (Surr)
98
70-130
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
1,4-Dioxane
5.94 J_
9.43
Surrogate
%Recovery Qualifier
2,4,6-Tribromophenol (Surr)
52
2-Fluorobiphenyl (Surr)
50
2-Fluorophenol (Surr)
39
Nitrobenzene-d5 (Surr)
50
Phenol-d5 (Surr)
30
Terphenyl-d14 (Surr)
72
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
Ethane
ND
Ethylene
ND
Methane
ND
Surrogate
%Recovery Qualifier
Acetylene (Surr)
96
Method: 300.0 - Anions,
Ion Chromatography
Analyte
Result Qualifier
Chloride
51.1
Nitrate as N
1.88
Sulfate
83.3
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
Iron
ND
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result Qualifier
Manganese
0.0445
General Chemistry
Analyte
Ammonia (as N)
Sulfide
Total Organic Carbon
Alkalinity
Total Dissolved Solids
Orthophosphate as P
Acetic acid
Formic -acid
Lactic acid
n-Butyric Acid
Limits
10-120
29-120
10-120
27-120
10-120
13-120
Prepared Analyzed Dil Fac
10131117 13:07 1
10131117 13:07
1
10131117 13:07
10131117 13:07 1
MDL Unit D Prepared Analyzed Dil Fac F
5.75 ug/L TO/28/17 20:55 TO/30/17 15:11 1
Prepared Analyzed Dil FacE
10128117 20:55
10130117 15:11 1
10128117 20:55
10130117 15:11 1
10128117 20:55
10130117 15:11 1
10128117 20:55
10130117 15:11 1
10128117 20:55
10130117 15:11 1
10128117 20:55
10130117 15:11 1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
F
-b--0-0500
-6-0-02-70
m_g/L_
11/06/17 12:33
1
0.00500
0.00220
mg/L
11/06/17 12:33
1
0.00500
0.00170
mg/L
11/06/17 12:33
1
Limits
Prepared
Analyzed
Dil Fac
62-124
11106117 12:33
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
10.0
7.00
mg/L
10/27/17 18:01
10
0.100
0.0500
mg/L
10/27/17 16:43
1
10.0
6.00
mg/L
10/27/17 18:01
10
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
0.100
0.0500
mg/L
11/01/17 07:32
11/02/17 03:26
1
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
-b--0-0400
0­00-150
mg -IL
-
11/01/1707:37
11/01/1716:39
1
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
-6.141
0.0500
0.0500
mg/L
11/01/17 11:15
1
ND
5.00
0.700
mg/L
11/01/17 13:00 11/01/17 15:00
1
5.20
1.00
0.500
mg/L
11/08/17 21:41
1
7.87 J
10.0
5.00
mg/L
11/08/17 11:34
1
326
10.0
7.00
mg/L
11/01/17 19:09
1
ND
0.100
0.0500
mg/L
10/27/17 17:24
1
ND
5.00
1.45
mg/L
11/07/17 09:04
5
ND
5.00
1.30
mg/L
11/07/17 09:04
5
ND
5.00
1.55
mg/L
11/07/17 09:04
5
ND
5.00
1.30
mg/L
11/07/17 09:04
5
Page 18 of 70
TestAmerica Nashville
11/10/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
F
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-3D-1 02617 Lab Sample ID: 490-139553-4
Date Collected: 10/26/17 11:34 Matrix: Water
Date Received: 10/27/17 09:45
General Chemistry (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Propionic acid ND 5.00 1.75 mg/L 11/07/17 09:04 5
Pyruvic Acid ND F1 7.50 1.85 mg/L 11/07/17 09:04 5
TestAmerica Nashville
Page 19 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-7D-1 02617 Lab Sample ID: 490-139553-5
Date Collected: 10/26/17 14:00 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
24.5
5.00
2.66
ug/L
10/27/17 19:54
1
Benzene
0.207 J
0.500
0.200
ug/L
10/27/17 19:54
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/27/17 19:54
1
Bromoform
ND
0.500
0.290
ug/L
10/27/17 19:54
1
Bromomethane
ND
0.500
0.350
ug/L
10/27/17 19:54
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/27/17 19:54
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/27/17 19:54
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/27/17 19:54
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/27/17 19:54
1
Chloroethane
ND
0.500
0.360
ug/L
10/27/17 19:54
1
Chloroform
ND
0.500
0.230
ug/L
10/27/17 19:54
1
Chloromethane
ND
0.500
0.360
ug/L
10/27/17 19:54
1
cis-1,2-Dichloroethene
0.509
0.500
0.210
ug/L
10/27/17 19:54
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/27/17 19:54
1
Cyclohexane
ND
1.00
0.130
ug/L
10/27/17 19:54
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/27/17 19:54
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/27/17 19:54
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/27/17 19:54
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/27/17 19:54
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/27/17 19:54
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/27/17 19:54
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/27/17 19:54
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/27/17 19:54
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/27/17 19:54
1
1,1-Dichloroethene
0.374 J
0.500
0.250
ug/L
10/27/17 19:54
1
1,2-Dichloropropane
ND *
0.500
0.250
ug/L
10/27/17 19:54
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/27/17 19:54
1
2-Hexanone
ND *
5.00
1.28
ug/L
10/27/17 19:54
1
1 sopropyl benzene
ND *
1.00
0.330
ug/L
10/27/17 19:54
1
Methyl acetate
ND *
10.0
0.580
ug/L
10/27/17 19:54
1
Methylcyclohexane
ND *
0.500
0.0900
ug/L
10/27/17 19:54
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/27/17 19:54
1
4-Methyl-2-pentanone (MIBK)
2.88 J *
5.00
0.810
ug/L
10/27/17 19:54
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/27/17 19:54
1
Styrene
ND
0.500
0.280
ug/L
10/27/17 19:54
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/27/17 19:54
1
Tetrachloroethene
0.436 J *
0.500
0.140
ug/L
10/27/17 19:54
1
Tetrahydrofuran
12.6
5.00
0.820
ug/L
10/27/17 19:54
1
Toluene
ND *
0.500
0.170
ug/L
10/27/17 19:54
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/27/17 19:54
1
trans- 1, 3-Dich loropropene
ND *
0.500
0.170
ug/L
10/27/17 19:54
1
1,2,4-Trichlorobenzene
ND *
0.500
0.200
ug/L
10/27/17 19:54
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/27/17 19:54
1
1,1,2-Trichloroethane
ND *
0.500
0.190
ug/L
10/27/17 19:54
1
Trichloroethene
51.9
0.500
0.200
ug/L
10/27/17 19:54
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/27/17 19:54
1
1,1,2-Trichloro-1,2,2-trifluoroetha
0.572 J
1.00
0.150
ug/L
10/27/17 19:54
1
ne
Vinyl chloride
ND
0.500
0.180
ug/L
10/27/17 19:54
1
M
TestAmerica Nashville
Page 20 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-7D-1 02617 Lab Sample ID: 490-139553-5
Date Collected: 10/26/17 14:00 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared
Xylenes, Total ND 1.50 0.580 ug/L
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene Fsu-rr)
100
70-130
Dibromofluoromethane (Surr)
111
70-130
1,2-Dichloroethane-d4 (Surr)
117
70-130
Toluene-d8 (Surr)
103
70-130
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
1,4-Dioxane
74.5
43.9
Surrogate
%Recovery Qualifier
2,4,6-Tribromophenol (Surr)
72
2-Fluorobiphenyl (Surr)
69
2-Fluorophenol (Surr)
51
Nitrobenzene-d5 (Surr)
68
Phenol-d5 (Surr)
34
Terphenyl-d14 (Surr)
90
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
Ethane
ND
Ethylene
0.00349 J
Methane
0.00896
Surrogate
%Recovery Qualifier
Acetylene (Surr)
98
Method: 300.0 - Anions,
Ion Chromatography
Analyte
Result Qualifier
Chloride
18.9
Nitrate as N
ND
Sulfate
1.01
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
Iron
0.559
Method: 200.8 - Metals (ICP/MS) - Dissolved
Prepared
Analyzed Dil Fac
10/27/17 19:54
1
Analyzed
Dil Fac
10127117 19:54
1
10127117 19:54
1
10127117 19:54
10127117 19:54
1
MDL Unit D Prepared Analyzed Dil Fac
26.8 ug/L 10/28/17 20:55 10/30/17 16:35 5
Limits
Prepared
Analyzed
Dil Fac
10-120
10128117 20:55
10130117 16:35
5
29-120
10128117 20:55
10130117 16:35
5
10-120
10128117 20:55
10130117 16:35
5
27-120
10128117 20:55
10130117 16:35
5
10-120
10128117 20:55
10130117 16:35
5
13-120
10128117 20:55
10130117 16:35
5
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.00500
0.00270
mg/L
11/06/17 12:36
1
0.00500
0.00220
mg/L
11/06/17 12:36
1
0.00500
0.00170
mg/L
11/06/17 12:36
1
Limits
62-124
Prepared Analyzed Dil Fac
111061171 1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
10.0
7.00
mg/L
10/28/17 18:38
10
0.500
0.250
mg/L
10/27/17 18:31
5
1.00
0.600
mg/L
10/27/17 16:53
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.100
0.0500
mg/L
11/01/1707:32
11/02/1703:31
1
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.309
0.00400
0.00150
mg/L
11/01/17 07:37
11/01/17 16:42
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
0.939
0.0500
0.0500
mg/L
11/01/17 11:16
1
Sulfide
ND
5.00
0.700
mg/L
11/01/17 13:00
11/01/17 15:00
1
Total Organic Carbon
2.24
1.00
0.500
mg/L
11/08/17 22:10
1
Alkalinity
12.8
10.0
5.00
mg/L
11/08/17 11:40
1
Total Dissolved Solids
89.0
10.0
7.00
mg/L
11/01/17 19:09
1
Orthophosphate as P
0.0550 1
0.100
0.0500
mg/L
10/27/17 17:25
1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 11:30
5
TestAmerica Nashville
Page 21 of 70 11/10/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
F
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-PM-7D-1 02617 Lab Sample ID: 490-139553-5
Date Collected: 10/26/17 14:00 Matrix: Water
Date Received: 10/27/17 09:45
General Chemistry (Continued)
Analyte
Formic -acid
Lactic acid
n-Butyric Acid
Propionic acid
Pyruvic Acid
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
ND
5.00
1.30
mg/L
11/07/17 11:30
5
ND
5.00
1.55
mg/L
11/07/17 11:30
5
ND
5.00
1.30
mg/L
11/07/17 11:30
5
ND
5.00
1.75
mg/L
11/07/17 11:30
5
ND
7.50
1.85
mg/L
11/07/17 11:30
5
F
F
TestAmerica Nashville
Page 22 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1155-RW-4-102617 Lab Sample ID: 490-139553-6
Date Collected: 10/26/17 14:10 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/27/17 20:20
1
Benzene
0.360 J
0.500
0.200
ug/L
10/27/17 20:20
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/27/17 20:20
1
Brornoform
ND
0.500
0.290
ug/L
10/27/17 20:20
1
Brornornethane
ND
0.500
0.350
ug/L
10/27/17 20:20
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/27/17 20:20
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/27/17 20:20
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/27/17 20:20
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/27/17 20:20
1
Chloroethane
ND
0.500
0.360
ug/L
10/27/17 20:20
1
Chloroform
3.52
0.500
0.230
ug/L
10/27/17 20:20
1
Chloromethane
ND
0.500
0.360
ug/L
10/27/17 20:20
1
cis-1,2-Dichloroethene
24.8
0.500
0.210
ug/L
10/27/17 20:20
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/27/17 20:20
1
Cyclohexane
ND
1.00
0.130
ug/L
10/27/17 20:20
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/27/17 20:20
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/27/17 20:20
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/27/17 20:20
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/27/17 20:20
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/27/17 20:20
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/27/17 20:20
1
Dichlorodifluoromethane
4.91
0.500
0.170
ug/L
10/27/17 20:20
1
1,1-Dichloroethane
10.5
0.500
0.240
ug/L
10/27/17 20:20
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/27/17 20:20
1
1,1-Dichloroethene
40.1
0.500
0.250
ug/L
10/27/17 20:20
1
1,2-Dichloropropane
ND *
0.500
0.250
ug/L
10/27/17 20:20
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/27/17 20:20
1
2-Hexanone
ND *
5.00
1.28
ug/L
10/27/17 20:20
1
1 sopropyl benzene
ND *
1.00
0.330
ug/L
10/27/17 20:20
1
Methyl acetate
ND *
10.0
0.580
ug/L
10/27/17 20:20
1
Methylcyclohexane
ND *
0.500
0.0900
ug/L
10/27/17 20:20
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/27/17 20:20
1
4-Methyl-2-pentanone (MIBK)
ND *
5.00
0.810
ug/L
10/27/17 20:20
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/27/17 20:20
1
Styrene
ND
0.500
0.280
ug/L
10/27/17 20:20
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/27/17 20:20
1
Tetrachloroethene
36.0 *
0.500
0.140
ug/L
10/27/17 20:20
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/27/17 20:20
1
Toluene
ND *
0.500
0.170
ug/L
10/27/17 20:20
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/27/17 20:20
1
trans- 1, 3-Dich loropropene
ND *
0.500
0.170
ug/L
10/27/17 20:20
1
1,2,4-Trichlorobenzene
ND *
0.500
0.200
ug/L
10/27/17 20:20
1
11,11,11-Trichloroethane
38.9
0.500
0.190
ug/L
10/27/17 20:20
1
1,1,2-Trichloroethane
0.233 J
0.500
0.190
ug/L
10/27/17 20:20
1
Trichloroethene
397
0.500
0.200
ug/L
10/27/17 20:20
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/27/17 20:20
1
1,1,2-Trichloro-1,2,2-trifluoroetha
232
1.00
0.150
ug/L
10/27/17 20:20
1
ne
Vinyl chloride
ND
0.500
0.180
ug/L
10/27/17 20:20
1
M
TestAmerica Nashville
Page 23 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Client Sample ID: J1155-RW-4-102617
Lab Sample
ID: 490-139553-6
Date Collected: 10/26/17 14:10
Matrix:
Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Xylenes, Total
ND
1.50
0.580
ug/L
10/27/17 20:20
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene Fsu-rr)
100
70-130
10127117 20:20
1
Dibromofluoromethane (Surr)
108
70-130
10127117 20:20
1
1,2-Dichloroethane-d4 (Surr)
116
70-130
10127117 20:20
Toluene-d8 (Surr)
110
70-130
10127117 20:20
1
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,4-Dioxane
6.32 J
8.93
5.45
ug/L
10/28/17 20:55
10/30/17 15:53
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
95
10-120
10128117 20:55
10130117 15:53
1
2-Fluorobiphenyl (Surr)
95
29-120
10128117 20:55
10130117 15:53
1
2-Fluorophenol (Surr)
75
10-120
10128117 20:55
10130117 15:53
1
Nitrobenzene-d5 (Surr)
91
27-120
10128117 20:55
10130117 15:53
Phenol-d5 (Surr)
54
10-120
10128117 20:55
10130117 15:53
1
Terphenyl-d14 (Surr)
108
13-120
10128117 20:55
10130117 15:53
1
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Ethane
ND
0.00500
0.00270
mg/L
11/06/17 12:45
1
Ethylene
ND
0.00500
0.00220
mg/L
11/06/17 12:45
1
Methane
ND
0.00500
0.00170
mg/L
11/06/17 12:45
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Acetylene (Surr)
95
62-124
111061171
1
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Chloride
3.63
1.00
0.700
mg/L
10/27/17 17:03
1
Nitrate as N
0.460
0.100
0.0500
mg/L
10/27/17 17:03
1
Sulfate
10.8
1.00
0.600
mg/L
10/27/17 17:03
1
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Iron
ND
0.100
0.0500
mg/L
11/01/17 07:32
11/02/17 03:36
1
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Manganese
0.00228 J
0.00400
0.00150
mg/L
11/01/17 07:37
11/01/17 16:45
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Ammonia (as N)
ND
0.0500
0.0500
mg/L
11/01/17 11:17
1
Sulfide
ND
5.00
0.700
mg/L
11/01/17 13:00
11/01/17 15:00
1
Total Organic Carbon
ND
1.00
0.500
mg/L
11/08/17 22:39
1
Alkalinity
113
10.0
5.00
mg/L
11/08/17 11:46
1
Total Dissolved Solids
233
10.0
7.00
mg/L
11/01/17 19:09
1
Orthophosphate as P
ND
0.100
0.0500
mg/L
10/27/17 17:26
1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 11:59
5
TestAmerica Nashville
Page 24 of 70 11/10/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
F
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1155-RW-4-102617 Lab Sample ID: 490-139553-6
Date Collected: 10/26/17 14:10 Matrix: Water
Date Received: 10/27/17 09:45
General Chemistry (Continued)
Analyte
Formic -acid
Lactic acid
n-Butyric Acid
Propionic acid
Pyruvic Acid
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
ND
5.00
1.30
mg/L
11/07/17 11:59
5
ND
5.00
1.55
mg/L
11/07/17 11:59
5
ND
5.00
1.30
mg/L
11/07/17 11:59
5
ND
5.00
1.75
mg/L
11/07/17 11:59
5
ND
7.50
1.85
mg/L
11/07/17 11:59
5
F
F
TestAmerica Nashville
Page 25 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1155-DUP-1-102617 Lab Sample ID: 490-139553-7
Date Collected: 10/26/17 16:00 Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
26.3
5.00
2.66
ug/L
10/27/17 20:45
1
Benzene
0.259 J
0.500
0.200
ug/L
10/27/17 20:45
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/27/17 20:45
1
Bromoform
ND
0.500
0.290
ug/L
10/27/17 20:45
1
Bromomethane
ND
0.500
0.350
ug/L
10/27/17 20:45
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/27/17 20:45
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/27/17 20:45
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/27/17 20:45
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/27/17 20:45
1
Chloroethane
ND
0.500
0.360
ug/L
10/27/17 20:45
1
Chloroform
ND
0.500
0.230
ug/L
10/27/17 20:45
1
Chloromethane
ND
0.500
0.360
ug/L
10/27/17 20:45
1
cis-1,2-Dichloroethene
0.491 J*
0.500
0.210
ug/L
10/27/17 20:45
1
cis- 1,3-Dichloropropene
ND *
0.500
0.170
ug/L
10/27/17 20:45
1
Cyclohexane
ND
1.00
0.130
ug/L
10/27/17 20:45
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/27/17 20:45
1
1,2-Dibromo-3-Chloropropane
ND *
5.00
0.940
ug/L
10/27/17 20:45
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/27/17 20:45
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/27/17 20:45
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/27/17 20:45
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/27/17 20:45
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/27/17 20:45
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/27/17 20:45
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/27/17 20:45
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/27/17 20:45
1
1,2-Dichloropropane
ND *
0.500
0.250
ug/L
10/27/17 20:45
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/27/17 20:45
1
2-Hexanone
ND *
5.00
1.28
ug/L
10/27/17 20:45
1
1 sopropyl benzene
ND *
1.00
0.330
ug/L
10/27/17 20:45
1
Methyl acetate
ND *
10.0
0.580
ug/L
10/27/17 20:45
1
Methylcyclohexane
ND *
0.500
0.0900
ug/L
10/27/17 20:45
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/27/17 20:45
1
4-Methyl-2-pentanone (MIBK)
2.94 J
5.00
0.810
ug/L
10/27/17 20:45
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/27/17 20:45
1
Styrene
ND
0.500
0.280
ug/L
10/27/17 20:45
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/27/17 20:45
1
Tetrachloroethene
0.556 *
0.500
0.140
ug/L
10/27/17 20:45
1
Tetrahydrofuran
13.4
5.00
0.820
ug/L
10/27/17 20:45
1
Toluene
ND *
0.500
0.170
ug/L
10/27/17 20:45
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/27/17 20:45
1
trans- 1, 3-Dich loropropene
ND *
0.500
0.170
ug/L
10/27/17 20:45
1
1,2,4-Trichlorobenzene
ND *
0.500
0.200
ug/L
10/27/17 20:45
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/27/17 20:45
1
1,1,2-Trichloroethane
ND *
0.500
0.190
ug/L
10/27/17 20:45
1
Trichloroethene
46.7
0.500
0.200
ug/L
10/27/17 20:45
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/27/17 20:45
1
1,1,2-Trichloro-1,2,2-trifluoroetha
0.726 J
1.00
0.150
ug/L
10/27/17 20:45
1
ne
Vinyl chloride
ND
0.500
0.180
ug/L
10/27/17 20:45
1
M
TestAmerica Nashville
Page 26 of 70 11/10/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1155-DUP-1-102617
Lab Sample ID: 490-139553-7
Date Collected: 10/26/17 16:00
Matrix: Water
Date Received: 10/27/17 09:45
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Xylenes, Total
ND
1.50 0.580 ug/L
10/27/17 20:45 1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed Dif Fac
4-Bromofluorobenzene FSu-rr)
101
70-130
101271172 -1
Dibromofluoromethane (Surr)
105
70-130
10127117 20:45 1
1,2-Dichloroethane-d4 (Surr)
115
70-130
10127117 20:45
Toluene-d8 (Surr)
111
70-130
10127117 20:45 1
F
TestAmerica Nashville
Page 27 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 490-471321/8
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471321
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
TO-/27/1716-55
1
Benzene
ND
0.500
0.200
ug/L
10/27/17 16:55
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/27/17 16:55
1
Bromoform
ND
0.500
0.290
ug/L
10/27/17 16:55
Bromomethane
ND
0.500
0.350
ug/L
10/27/17 16:55
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/27/17 16:55
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/27/17 16:55
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/27/17 16:55
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/27/17 16:55
1
Chloroethane
ND
0.500
0.360
ug/L
10/27/17 16:55
1
Chloroform
ND
0.500
0.230
ug/L
10/27/17 16:55
1
Chloromethane
ND
0.500
0.360
ug/L
10/27/17 16:55
1
cis- 1,2-Dichloroethene
ND
0.500
0.210
ug/L
10/27/17 16:55
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/27/17 16:55
1
Cyclohexane
ND
1.00
0.130
ug/L
10/27/17 16:55
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/27/17 16:55
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/27/17 16:55
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/27/17 16:55
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/27/17 16:55
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/27/17 16:55
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/27/17 16:55
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/27/17 16:55
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/27/17 16:55
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/27/17 16:55
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/27/17 16:55
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/27/17 16:55
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/27/17 16:55
1
2-Hexanone
ND
5.00
1.28
ug/L
10/27/17 16:55
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/27/17 16:55
1
Methyl acetate
ND
10.0
0.580
ug/L
10/27/17 16:55
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/27/17 16:55
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/27/17 16:55
1
4-Methyl-2-pentanone (MlBK)
ND
5.00
0.810
ug/L
10/27/17 16:55
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/27/17 16:55
1
Styrene
ND
0.500
0.280
ug/L
10/27/17 16:55
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/27/17 16:55
1
Tetrachloroethene
ND
0.500
0.140
ug/L
10/27/17 16:55
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/27/17 16:55
1
Toluene
ND
0.500
0.170
ug/L
10/27/17 16:55
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/27/17 16:55
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/27/17 16:55
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/27/17 16:55
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/27/17 16:55
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/27/17 16:55
1
Trichloroethene
ND
0.500
0.200
ug/L
10/27/17 16:55
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/27/17 16:55
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.150
ug/L
10/27/17 16:55
1
Vinyl chloride
ND
0.500
0.180
ug/L
10/27/17 16:55
1
TestAmerica Nashville
Page 28 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 490-47132118
Matrix: Water
Analysis Batch: 471321
MB MB
Analyte Result Qualifier RL MDL Unit
Xylenes, Total ND 1.50 0.580 ug/L
MB MB
F
TestAmerica Job ID: 490-139553-1
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
10/27/17 16:55 1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
4-Bromofluorobenzene (Surr)
100
70-130
10127117 16:55
Dibromofluoromethane (Surr)
102
70-130
10127117 16:55
1,2-Dichloroethane-d4 (Surr)
116
70-130
10127117 16:55
Toluene-d8 (Surr)
118
70-130
10127117 16:55
Lab Sample ID: LCS 490-471321/3
Matrix: Water
Analysis Batch: 471321
Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
I sopropyl benzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MlBK)
Methyl tert-butyl ether
Styrene
Dil Fac 9
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
100
148.3
ug/L
148
39-150
20.0
18.37
ug/L
92
70-130
20.0
21.59
ug/L
108
70-130
20.0
21.78
ug/L
109
70-137
20.0
16.90
ug/L
85
53-150
100
109.6
ug/L
110
55-143
20.0
20.24
ug/L
101
64-135
20.0
21.90
ug/L
109
70-147
20.0
19.69
ug/L
98
70-130
20.0
23.88
ug/L
119
60-138
20.0
25.37
ug/L
127
70-130
20.0
22.41
ug/L
112
33-150
20.0
24.58
ug/L
123
70-130
20.0
15.45
ug/L
77
70-133
20.0
17.17
ug/L
86
70-134
20.0
21.57
ug/L
108
70-133
20.0
15.08
ug/L
75
45-138
20.0
20.13
ug/L
101
70-130
20.0
19.30
ug/L
96
70-130
20.0
20.53
ug/L
103
70-130
20.0
20.82
ug/L
104
70-130
20.0
26.27
ug/L
131
48-150
20.0
21.40
ug/L
107
70-130
20.0
21.25
ug/L
106
70-130
20.0
19.96
ug/L
100
70-132
20.0
20.09
ug/L
100
70-130
20.0
18.78
ug/L
94
70-130
100
82.72
ug/L
83
54-142
20.0
17.67
ug/L
88
70-131
40.0
56.55
ug/L
141
56-136
20.0
21.40
ug/L
107
70-132
20.0
22.48
ug/L
112
70-130
100
85.64
ug/L
86
60-137
20.0
18.60
ug/L
93
70-130
20.0
18.16
ug/L
91
70-130
TestAmerica Nashville
Page 29 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-471321/3
Matrix: Water
Analysis Batch: 471321
TestAmerica Job ID: 490-139553-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,1,2,2-Tetrachloroethane
20.0
22.03
ug/L
110
69-131
Tetrachloroethene
20.0
17.58
ug/L
88
70-130
Tetrahydrofuran
40.0
40.89
ug/L
102
51-136
Toluene
20.0
15.72
ug/L
79
70-130
trans- 1,2-Dich loroethene
20.0
19.83
ug/L
99
70-130
trans- 1, 3-Dich loropropene
20.0
15.08
ug/L
75
63-142
1,2,4-Trichlorobenzene
20.0
14.80
ug/L
74
58-147
1,1,1-Trichloroethane
20.0
20.41
ug/L
102
70-135
1,1,2-Trichloroethane
20.0
16.31
ug/L
82
70-130
Trichloroethene
20.0
19.14
ug/L
96
70-130
Trichlorofluoromethane
20.0
25.88
ug/L
129
59-150
1,1,2-Trichloro-1,2,2-trifluoroetha
20.0
24.75
ug/L
124
69-145
ne
Vinyl chloride
20.0
21.67
ug/L
108
57-137
Xylenes, Total
40.0
36.26
ug/L
91
70-132
LCS LCS
Surrogate
%Recovety Qualifier
Limits
4-Bromofluorobenzene (Surr)
102
70-130
Dibromofluoromethane (Surr)
105
70-130
1,2-Dichloroethane-d4 (Surr)
120
70-130
Toluene-d8 (Surr)
83
70-130
Lab Sample ID: LCSID 490-471321/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471321
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Acetone
100
130.8
ug/L
131
39-150
13
23
Benzene
20.0
19.84
ug/L
99
70-130
8
12
Bromodichloromethane
20.0
17.65
ug/L
88
70-130
20
14
Bromoform
20.0
22.40
ug/L
112
70-137
3
14
Bromomethane
20.0
14.93
ug/L
75
53-150
12
19
2-Butanone (MEK)
100
100.1
ug/L
100
55-143
9
19
Carbon disulfide
20.0
18.13
ug/L
91
64-135
11
16
Carbon tetrachloride
20.0
23.05
ug/L
115
70-147
5
16
Chlorobenzene
20.0
20.19
ug/L
101
70-130
3
12
Chloroethane
20.0
21.19
ug/L
106
60-138
12
15
Chloroform
20.0
23.36
ug/L
117
70-130
8
14
Chloromethane
20.0
20.16
ug/L
101
33-150
11
20
cis- 1,2-Dichloroethene
20.0
17.11
ug/L
86
70-130
36
15
cis- 1,3-Dichloropropene
20.0
19.48
ug/L
97
70-133
23
15
Cyclohexane
20.0
19.24
ug/L
96
70-134
11
16
Dibromochloromethane
20.0
22.72
ug/L
114
70-133
5
13
1,2-Dibromo-3-Chloropropane
20.0
19.06
ug/L
95
45-138
23
19
1,2-Dibromoethane (EDB)
20.0
21.53
ug/L
108
70-130
7
13
1,2-Dichlorobenzene
20.0
20.44
ug/L
102
70-130
6
12
1,3-Dichlorobenzene
20.0
20.97
ug/L
105
70-130
2
13
1,4-Dichlorobenzene
20.0
20.92
ug/L
105
70-130
0
12
TestAmerica Nashville
Page 30 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-471321/4
Matrix: Water
Analysis Batch: 471321
TestAmerica Job ID: 490-139553-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Dichlorodifluoromethane
20.0
23.76
ug/L
119
48-150
10
16
1,1-Dichloroethane
20.0
20.96
ug/L
105
70-130
2
17
1,2-Dichloroethane
20.0
23.67
ug/L
118
70-130
11
13
1,1-Dichloroethene
20.0
17.42
ug/L
87
70-132
14
20
1,2-Dichloropropane
20.0
16.27 *
ug/L
81
70-130
21
15
Ethylbenzene
20.0
19.22
ug/L
96
70-130
2
12
2-Hexanone
100
104.0 *
ug/L
104
54-142
23
17
1 sopropyl benzene
20.0
22.09 *
ug/L
110
70-131
22
13
Methyl acetate
40.0
50.94
ug/L
127
56-136
10
18
Methylcyclohexane
20.0
16.19 *
ug/L
81
70-132
28
17
Methylene Chloride
20.0
19.75
ug/L
99
70-130
13
15
4-Methyl-2-pentanone (MIBK)
100
110.8 *
ug/L
111
60-137
26
21
Methyl tert-butyl ether
20.0
16.76
ug/L
84
70-130
10
16
Styrene
20.0
18.71
ug/L
94
70-130
3
12
1,1,2,2-Tetrachloroethane
20.0
22.46
ug/L
112
69-131
2
15
Tetrachloroethene
20.0
21.56 *
ug/L
108
70-130
20
17
Tetrahydrofuran
40.0
45.02
ug/L
113
51-136
10
20
Toluene
20.0
20.07 *
ug/L
100
70-130
24
13
trans- 1,2-Dich loroethene
20.0
17.73
ug/L
89
70-130
11
15
trans- 1, 3-Dich loropropene
20.0
19.84 *
ug/L
99
63-142
27
13
1,2,4-Trichlorobenzene
20.0
18.15 *
ug/L
91
58-147
20
15
1,1,1-Trichloroethane
20.0
22.31
ug/L
112
70-135
9
15
1,1,2-Trichloroethane
20.0
20.67 *
ug/L
103
70-130
24
13
Trichloroethene
20.0
16.99
ug/L
85
70-130
12
14
Trichlorofluoromethane
20.0
23.55
ug/L
118
59-150
9
22
1,1,2-Trichloro-1,2,2-trifluoroetha
20.0
22.16
ug/L
111
69-145
11
16
ne
Vinyl chloride
20.0
19.84
ug/L
99
57-137
9
15
Xylenes, Total
40.0
37.85
ug/L
95
70-132
4
11
LCSD LCSD
Surrogate
%Recovety Qualifier
Limits
4-Bromofluorobenzene (Surr)
107
70-130
Dibromofluoromethane (Surr)
105
70-130
1,2-Dichloroethane-d4 (Surr)
120
70-130
Toluene-d8 (Surr)
101
70-130
Lab Sample ID: 490-139553-1 MS
Matrix: Water
Analysis Batch: 471321
Analyte
Sample
Result
Sample
Qualifier
Acetone
ND
Benzene
1.46
Bromodichloromethane
0.218
J*
Brornoform
ND
Brornornethane
ND
2-Butanone (MEK)
ND
F1 F2
Carbon disulfide
ND
Spike
Added
MS MS
Result Qualifier
100
108.1
20.0
22.99
20.0
21.53
20.0
22.07
20.0
16.71
100
109.3
20.0
26.59
Client Sample ID: J1 155-MW-1 2-102617
Prep Type: Total/NA
Unit
D %Rec
%Rec.
Limits
ug/L
108
39-150
ug/L
108
55-147
ug/L
107
70-140
ug/L
110
53-150
ug/L
84
30-150
ug/L
109
50-143
ug/L
133
35-150
TestAmerica Nashville
Page 31 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139553-1 MS
Matrix: Water
Analysis Batch: 471321
Analyte
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dich loroethene
trans- 1, 3-Dich loropropene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1 155-MW-1 2-102617
Prep Type: Total/NA
Sample Sample
Spike
MS
MS
%Rec.
Result Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
ND F2
20.0
20.53
ug/L
103
56-150
ND
20.0
22.79
ug/L
114
70-130
ND Fl
20.0
23.48
ug/L
117
58-141
12.5 F2
20.0
29.05
ug/L
83
66-138
ND Fl
20.0
22.37
ug/L
112
10-150
388 * F2
20.0
301.2
4
ug/L
-436
68-131
ND *
20.0
22.48
ug/L
112
70-133
ND
20.0
19.23
ug/L
96
48-150
ND
20.0
23.53
ug/L
118
66-140
ND *
20.0
19.10
ug/L
96
38-138
ND
20.0
22.58
ug/L
113
65-137
0.721
20.0
23.17
ug/L
112
70-130
ND
20.0
22.98
ug/L
115
68-131
ND
20.0
23.42
ug/L
117
70-130
59.5
20.0
70.41
ug/L
55
10-150
105
20.0
98.46
4
ug/L
-32
61-139
ND
20.0
24.33
ug/L
122
64-136
255 E
20.0
223.7
E 4
ug/L
-155
54-150
ND *
20.0
21.56
ug/L
108
67-130
ND
20.0
22.60
ug/L
113
65-139
ND *
100
111.0
ug/L
ill
44-150
ND *
20.0
21.95
ug/L
110
70-137
ND *
40.0
46.36
ug/L
116
42-136
ND *
20.0
22.23
ug/L
111
59-150
ND
20.0
21.70
ug/L
108
64-130
ND *
100
115.5
ug/L
115
50-140
ND
20.0
19.60
ug/L
98
55-141
ND
20.0
21.65
ug/L
108
70-130
ND
20.0
21.72
ug/L
109
56-145
176 *
20.0
163.3
4
ug/L
-64
57-138
ND
40.0
30.78
ug/L
77
40-136
ND *
20.0
24.17
ug/L
121
64-136
ND
20.0
22.17
ug/L
111
59-143
ND *
20.0
21.56
ug/L
108
63-142
ND *
20.0
18.25
ug/L
91
47-147
136 F2
20.0
120.0
4
ug/L
-80
68-144
1.53 *
20.0
23.52
ug/L
110
70-130
1430 E
20.0
1170
E 4
ug/L
-1323
63-135
ND
20.0
24.42
ug/L
122
44-150
376
20.0
308.3
4
ug/L
-339
63-150
3.79 Fl
20.0
24.37
ug/L
103
57-150
ND
40.0
43.73
ug/L
109
69-132
MS MS
%Recovery Qualifier
Limits
103
70-130
79
70-130
104
70-130
TestAmerica Nashville
Page 32 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139553-1 MS Client Sample ID: J1 155-MW-1 2-102617
Matrix: Water Prep Type: Total/NA
Analysis Batch: 471321
MS MS
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 105 70-130
Lab Sample ID: 490-139553-1 MSD Client Sample ID: J1 155-MW-1 2-102617
Matrix: Water Prep Type: Total/NA
Analysis Batch: 471321
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Acetone
ND
100
124.5
ug/L
125
39-150
14
28
Benzene
1.46
20.0
22.60
ug/L
106
55-147
2
22
Bromodichloromethane
0.218 J*
20.0
21.73
ug/L
108
70-140
1
196
Bromoform
ND
20.0
21.35
ug/L
107
53-150
3
20
Bromomethane
ND
20.0
21.94
ug/L
110
30-150
27
44
2-Butanone (MEK)
ND Fl F2
100
148.3
Fl F2
ug/L
148
50-143
30
28
Carbon disulfide
ND
20.0
20.38
ug/L
102
35-150
26
34
Carbon tetrachloride
ND F2
20.0
26.33
F2
ug/L
132
56-150
25
18
Chlorobenzene
ND
20.0
22.23
ug/L
ill
70-130
2
15
Chloroethane
ND Fl
20.0
29.14
Fl
ug/L
146
58-141
22
31
Chloroform
12.5 F2
20.0
38.05
F2
ug/L
128
66-138
27
21
Chloromethane
ND Fl
20.0
30.42
Fl
ug/L
152
10-150
31
43
cis- 1,2-Dichloroethene
388 * F2
20.0
404.0
E 4 F2
ug/L
78
68-131
29
21
cis- 1,3-Dichloropropene
ND *
20.0
23.20
ug/L
116
70-133
3
19
Cyclohexane
ND
20.0
22.73
ug/L
114
48-150
17
22
Dibromochloromethane
ND
20.0
25.21
ug/L
126
66-140
7
19
1,2-Dibromo-3-Chloropropane
ND *
20.0
18.15
ug/L
91
38-138
5
26
1,2-Dibromoethane (EDB)
ND
20.0
23.61
ug/L
118
65-137
4
21
1,2-Dichlorobenzene
0.721
20.0
23.04
ug/L
112
70-130
1
15
1,3-Dichlorobenzene
ND
20.0
23.78
ug/L
119
68-131
3
14
1,4-Dichlorobenzene
ND
20.0
23.19
ug/L
116
70-130
1
14
Dichlorodifluoromethane
59.5
20.0
88.93
ug/L
147
10-150
23
50
1,1-Dichloroethane
105
20.0
121.8
4
ug/L
84
61-139
21
23
1,2-Dichloroethane
ND
20.0
24.07
ug/L
120
64-136
1
22
1,1-Dichloroethene
255 E
20.0
267.1
E 4
ug/L
61
54-150
18
24
1,2-Dichloropropane
ND *
20.0
20.63
ug/L
103
67-130
4
19
Ethylbenzene
ND
20.0
22.03
ug/L
110
65-139
3
18
2-Hexanone
ND *
100
108.1
ug/L
108
44-150
3
21
1 sopropyl benzene
ND *
20.0
21.57
ug/L
108
70-137
2
17
Methyl acetate
ND *
40.0
49.93
ug/L
125
42-136
7
26
M ethyl cyclohexa ne
ND *
20.0
21.61
ug/L
108
59-150
3
20
Methylene Chloride
ND
20.0
25.21
ug/L
126
64-130
15
22
4-Methyl-2-pentanone (MIBK)
ND *
100
118.7
ug/L
119
50-140
3
24
Methyl tert-butyl ether
ND
20.0
22.55
ug/L
113
55-141
14
24
Styrene
ND
20.0
20.73
ug/L
104
70-130
4
16
1,1,2,2-Tetrachloroethane
ND
20.0
21.44
ug/L
107
56-145
1
19
Tetrachloroethene
176 *
20.0
174.6
4
ug/L
-7
57-138
7
17
Tetrahydrofuran
ND
40.0
40.43
ug/L
101
40-136
27
27
Toluene
ND *
20.0
23.08
ug/L
115
64-136
5
18
trans- 1,2-Dich loroethene
ND
20.0
26.92
ug/L
135
59-143
19
25
trans- 1, 3-Dich loropropene
ND *
20.0
22.01
ug/L
110
63-142
2
18
TestAmerica Nashville
Page 33 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139553-1 MSD
Matrix: Water
Analysis Batch: 471321
Analyte
1, 2,4-Trich lorobe nzene
1, 1, 1 -Trichloroethane
1, 1,2-Trich loroethane
Trichloroethene
Trichlorofluoromethane
1, 1,2-Trich loro-1,2,2-trifluoroetha
ne
Vinyl chloride
Xylenes, Total
Client Sample ID: J1 155-MW-1 2-102617
Prep Type: Total/NA
Sample Sample
Result Qualifier
Spike
Added
MSD
Result
MSD
Qualifier
Unit
D %Rec
%Rec.
Limits
RPD
ND *
20.0
19.15
ug/L
96
47-147
5
136 F2
20.0
150.7
4 F2
ug/L
74
68-144
23
1.53 *
20.0
25.80
ug/L
121
70-130
9
1430 E
20.0
1318
E 4
ug/L
-583
63-135
12
ND
20.0
30.03
ug/L
150
44-150
21
376
20.0
372.9
4
ug/L
-15
63-150
19
3.79 F1
ND
MSD MSD
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surr) 102
Dibromofluoromethane (Surr) 76
1,2-Dichloroethane-d4 (Surr) 107
Toluene-d8 (Surr) 105
Lab Sample ID: MB 490-472139/7
Matrix: Water
Analysis Batch: 472139
20.0 34.62 F1 ug/L
40.0 42.66 ug/L
Limits
70-130
70-130
70-130
70-130
154 57-150 35
107 69-132 2
RPD
Limit
24
17
18
17
32
22
37
17
Client Sample ID: Method Blank
Prep Type: Total/NA
Analyte
MlB MB
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/31/17 11:25
1
Benzene
ND
0.500
0.200
ug/L
10/31/17 11:25
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/31/17 11:25
1
Bromoform
ND
0.500
0.290
ug/L
10/31/17 11:25
1
Bromomethane
ND
0.500
0.350
ug/L
10/31/17 11:25
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/31/17 11:25
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/31/17 11:25
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/31/17 11:25
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/31/17 11:25
1
Chloroethane
ND
0.500
0.360
ug/L
10/31/17 11:25
1
Chloroform
ND
0.500
0.230
ug/L
10/31/17 11:25
1
Chloromethane
ND
0.500
0.360
ug/L
10/31/17 11:25
1
cis- 1,2-Dichloroethene
ND
0.500
0.210
ug/L
10/31/17 11:25
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/31/17 11:25
1
Cyclohexane
ND
1.00
0.130
ug/L
10/31/17 11:25
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/31/17 11:25
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/31/17 11:25
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/31/17 11:25
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/31/17 11:25
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/31/17 11:25
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/31/17 11:25
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/31/17 11:25
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/31/17 11:25
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/31/17 11:25
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/31/17 11:25
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/31/17 11:25
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/31/17 11:25
1
Page 34 of 70
TestAmerica Nashville
11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 490-47213917
Matrix: Water
Analysis Batch: 472139
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
2-Hexanone
ND
5.00
1.28
ug/L
10/31/17 11:25
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/31/17 11:25
1
Methyl acetate
ND
10.0
0.580
ug/L
10/31/17 11:25
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/31/17 11:25
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/31/17 11:25
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/31/17 11:25
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/31/17 11:25
1
Styrene
ND
0.500
0.280
ug/L
10/31/17 11:25
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/31/17 11:25
1
Tetrachloroethene
ND
0.500
0.140
ug/L
10/31/17 11:25
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/31/17 11:25
1
Toluene
ND
0.500
0.170
ug/L
10/31/17 11:25
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/31/17 11:25
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/31/17 11:25
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/31/17 11:25
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/31/17 11:25
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/31/17 11:25
1
Trichloroethene
ND
0.500
0.200
ug/L
10/31/17 11:25
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/31/17 11:25
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.150
ug/L
10/31/17 11:25
1
Vinyl chloride
ND
0.500
0.180
ug/L
10/31/17 11:25
1
Xylenes, Total
ND
1.50
0.580
ug/L
10/31/17 11:25
1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
107
70-130
10131117 11:25
1
Dibromofluoromethane (Surr)
96
70-130
10131117 11:25
1
1,2-Dichloroethane-d4 (Surr)
115
70-130
10131117 11:25
1
Toluene-d8 (Surr)
109
70-130
10131117 11:25
1
Lab Sample ID: LCS 490-472139/4
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472139
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
100
-
85.71
ug A
-86
-:�9-- 15-0
Benzene
20.0
17.56
ug/L
88
70-130
Bromodichloromethane
20.0
19.93
ug/L
100
70-130
Bromoform
20.0
19.81
ug/L
99
70-137
Bromomethane
20.0
14.58
ug/L
73
53-150
2-Butanone (MEK)
100
81.05
ug/L
81
55-143
Carbon disulfide
20.0
15.82
ug/L
79
64-135
Carbon tetrachloride
20.0
20.84
ug/L
104
70-147
Chlorobenzene
20.0
19.28
ug/L
96
70-130
Chloroethane
20.0
19.50
ug/L
98
60-138
Chloroform
20.0
20.33
ug/L
102
70-130
Chloromethane
20.0
17.11
ug/L
86
33-150
cis- 1,2-Dichloroethene
20.0
18.30
ug/L
92
70-130
cis- 1,3-Dichloropropene
20.0
20.39
ug/L
102
70-133
TestAmerica Nashville
Page 35 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-472139/4
Matrix: Water
Analysis Batch: 472139
TestAmerica Job ID: 490-139553-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Cyclohexane
20.0
15.68
ug/L
78
70-134
Dibromochloromethane
20.0
21.32
ug/L
107
70-133
1,2-Dibromo-3-Chloropropane
20.0
16.60
ug/L
83
45-138
1,2-Dibromoethane (EDB)
20.0
19.09
ug/L
95
70-130
1,2-Dichlorobenzene
20.0
18.90
ug/L
95
70-130
1,3-Dichlorobenzene
20.0
19.94
ug/L
100
70-130
1,4-Dichlorobenzene
20.0
19.43
ug/L
97
70-130
Dichlorodifluoromethane
20.0
16.07
ug/L
80
48-150
1,1-Dichloroethane
20.0
18.16
ug/L
91
70-130
1,2-Dichloroethane
20.0
22.28
ug/L
111
70-130
1,1-Dichloroethene
20.0
17.31
ug/L
87
70-132
1,2-Dichloropropane
20.0
18.36
ug/L
92
70-130
Ethylbenzene
20.0
18.02
ug/L
90
70-130
2-Hexanone
100
83.15
ug/L
83
54-142
1 sopropyl benzene
20.0
17.49
ug/L
87
70-131
Methyl acetate
40.0
42.54
ug/L
106
56-136
Methylcyclohexane
20.0
16.98
ug/L
85
70-132
Methylene Chloride
20.0
19.54
ug/L
98
70-130
4-Methyl-2-pentanone (MIBK)
100
91.06
ug/L
91
60-137
Methyl tert-butyl ether
20.0
18.25
ug/L
91
70-130
Styrene
20.0
17.38
ug/L
87
70-130
1,1,2,2-Tetrachloroethane
20.0
17.80
ug/L
89
69-131
Tetrachloroethene
20.0
20.52
ug/L
103
70-130
Tetrahydrofuran
40.0
29.48
ug/L
74
51-136
Toluene
20.0
19.02
ug/L
95
70-130
trans- 1,2-Dich loroethene
20.0
20.02
ug/L
100
70-130
trans- 1, 3-Dich loropropene
20.0
18.11
ug/L
91
63-142
1,2,4-Trichlorobenzene
20.0
15.95
ug/L
80
58-147
1,1,1-Trichloroethane
20.0
19.37
ug/L
97
70-135
1,1,2-Trichloroethane
20.0
18.65
ug/L
93
70-130
Trichloroethene
20.0
19.18
ug/L
96
70-130
Trichlorofluoromethane
20.0
20.76
ug/L
104
59-150
1,1,2-Trichloro-1,2,2-trifluoroetha
20.0
20.47
ug/L
102
69-145
ne
Vinyl chloride
20.0
16.89
ug/L
84
57-137
Xylenes, Total
40.0
35.24
ug/L
88
70-132
LCS LCS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
98
70-130
Dibromofluoromethane (Surr)
92
70-130
1,2-Dichloroethane-d4 (Surr)
114
70-130
Toluene-d8 (Surr)
104
70-130
TestAmerica Nashville
Page 36 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-47213915
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472139
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier Unit
D %Rec
Limits
RPD
Limit
Acetone
100
91.11
dg-/L
9 -1
39-150
6
23
Benzene
20.0
18.55
ug/L
93
70-130
5
12
Bromodichloromethane
20.0
17.95
ug/L
90
70-130
10
14
Bromoform
20.0
22.84
ug/L
114
70-137
14
14
Bromomethane
20.0
15.66
ug/L
78
53-150
7
19
2-Butanone (MEK)
100
86.54
ug/L
87
55-143
7
19
Carbon disulfide
20.0
14.77
ug/L
74
64-135
7
16
Carbon tetrachloride
20.0
21.38
ug/L
107
70-147
3
16
Chlorobenzene
20.0
18.95
ug/L
95
70-130
2
12
Chloroethane
20.0
18.99
ug/L
95
60-138
3
15
Chloroform
20.0
21.68
ug/L
108
70-130
6
14
Chloromethane
20.0
17.31
ug/L
87
33-150
1
20
cis- 1,2-Dichloroethene
20.0
20.00
ug/L
100
70-130
9
15
cis- 1,3-Dichloropropene
20.0
17.29
ug/L
86
70-133
16
15
Cyclohexane
20.0
16.82
ug/L
84
70-134
7
16
Dibromochloromethane
20.0
20.63
ug/L
103
70-133
3
13
1,2-Dibromo-3-Chloropropane
20.0
16.11
ug/L
81
45-138
3
19
1,2-Dibromoethane (EDB)
20.0
17.94
ug/L
90
70-130
6
13
1,2-Dichlorobenzene
20.0
17.64
ug/L
88
70-130
7
12
1,3-Dichlorobenzene
20.0
19.78
ug/L
99
70-130
1
13
1,4-Dichlorobenzene
20.0
19.69
ug/L
98
70-130
1
12
Dichlorodifluoromethane
20.0
16.08
ug/L
80
48-150
0
16
1,1-Dichloroethane
20.0
19.31
ug/L
97
70-130
6
17
1,2-Dichloroethane
20.0
18.84
ug/L
94
70-130
17
13
1,1-Dichloroethene
20.0
18.09
ug/L
90
70-132
4
20
1,2-Dichloropropane
20.0
17.66
ug/L
88
70-130
4
15
Ethylbenzene
20.0
18.69
ug/L
93
70-130
4
12
2-Hexanone
100
77.56
ug/L
78
54-142
7
17
1 sopropyl benzene
20.0
19.34
ug/L
97
70-131
10
13
Methyl acetate
40.0
43.01
ug/L
108
56-136
1
18
Methylcyclohexane
20.0
16.98
ug/L
85
70-132
0
17
Methylene Chloride
20.0
18.96
ug/L
95
70-130
3
15
4-Methyl-2-pentanone (MlBK)
100
83.46
ug/L
83
60-137
9
21
Methyl tert-butyl ether
20.0
18.27
ug/L
91
70-130
0
16
Styrene
20.0
18.18
ug/L
91
70-130
5
12
1,1,2,2-Tetrachloroethane
20.0
18.34
ug/L
92
69-131
3
15
Tetrachloroethene
20.0
18.93
ug/L
95
70-130
8
17
Tetrahydrofuran
40.0
30.84
ug/L
77
51-136
5
20
Toluene
20.0
17.58
ug/L
88
70-130
8
13
trans- 1,2-Dich loroethene
20.0
19.19
ug/L
96
70-130
4
15
trans- 1, 3-Dich loropropene
20.0
17.84
ug/L
89
63-142
2
13
1,2,4-Trichlorobenzene
20.0
14.27
ug/L
71
58-147
11
15
1,1,1-Trichloroethane
20.0
20.33
ug/L
102
70-135
5
15
1,1,2-Trichloroethane
20.0
17.82
ug/L
89
70-130
5
13
Trichloroethene
20.0
18.47
ug/L
92
70-130
4
14
Trichlorofluoromethane
20.0
20.68
ug/L
103
59-150
0
22
1,1,2-Trichloro-1,2,2-trifluoroetha
20.0
20.04
ug/L
100
69-145
2
16
ne
TestAmerica Nashville
Page 37 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-472139/5
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472139
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D %Rec Limits RPD Limit
Vinyl chloride
20.0
16.97
ug/L
85 57-137 0 15
Xylenes, Total
40.0
35.30
ug/L
88 70-132 0 11
LCSD LCSD
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 96 70-130
Dibromofluoromethane (Surr) 100 70-130
1,2-Dichloroethane-d4 (Surr) 117 70-130
Toluene-d8 (Surr) 97 70-130
Lab Sample ID: 490-139553-1 MS
Matrix: Water
Analysis Batch: 472139
Client Sample ID: J1 155-MW-1 2-102617
Prep Type: Total/NA
Analyte
Sample Sample
Result Qualifier
Spike
Added
MS
Result
MS
Qualifier
Unit
D %Rec
%Rec.
Limits
Acetone
39.5
500
569.4
ug/L
106
39-150
Benzene
1.56 J
100
104.8
ug/L
103
55-147
Bromodichloromethane
ND
100
102.6
ug/L
103
70-140
Bromoform
ND
100
103.9
ug/L
104
53-150
Bromomethane
ND
100
81.10
ug/L
81
30-150
2-Butanone (MEK)
ND
500
523.5
ug/L
105
50-143
Carbon disulfide
ND
100
68.40
ug/L
68
35-150
Carbon tetrachloride
ND
100
123.1
ug/L
123
56-150
Chlorobenzene
ND
100
100.0
ug/L
100
70-130
Chloroethane
ND
100
110.8
ug/L
111
58-141
Chloroform
12.4
100
134.9
ug/L
123
66-138
Chloromethane
ND
100
93.79
ug/L
94
10-150
cis- 1,2-Dichloroethene
356
100
503.2
F1
ug/L
147
68-131
cis- 1,3-Dichloropropene
ND
100
103.9
ug/L
104
70-133
Cyclohexane
ND
100
99.60
ug/L
100
48-150
Dibromochloromethane
ND
100
109.8
ug/L
110
66-140
1,2-Dibromo-3-Chloropropane
ND
100
79.85
ug/L
80
38-138
1,2-Dibromoethane (EDB)
ND
100
95.02
ug/L
95
65-137
1,2-Dichlorobenzene
1.05 J
100
98.98
ug/L
98
70-130
1,3-Dichlorobenzene
ND
100
99.94
ug/L
100
68-131
1,4-Dichlorobenzene
ND
100
100.4
ug/L
100
70-130
Dichlorodifluoromethane
48.3
100
124.4
ug/L
76
10-150
1,1-Dichloroethane
88.4
100
207.4
ug/L
119
61-139
1,2-Dichloroethane
ND
100
113.9
ug/L
114
64-136
1,1-Dichloroethene
219
100
238.7
F1
ug/L
20
54-150
1,2-Dichloropropane
ND
100
92.47
ug/L
92
67-130
Ethylbenzene
ND
100
96.22
ug/L
96
65-139
2-Hexanone
ND
500
429.5
ug/L
86
44-150
1 sopropyl benzene
ND
100
92.96
ug/L
93
70-137
Methyl acetate
ND
200
180.4
ug/L
90
42-136
Methylcyclohexane
ND
100
93.45
ug/L
93
59-150
Methylene Chloride
ND
100
107.7
ug/L
108
64-130
4-Methyl-2-pentanone (MlBK)
21.9 J
500
501.0
ug/L
96
50-140
Methyl tert-butyl ether
ND
100
98.05
ug/L
98
55-141
TestAmerica Nashville
Page 38 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139553-1 MS Client Sample ID: J1 155-MW-1 2-102617
Matrix: Water Prep Type: Total/NA
Analysis Batch: 472139
Sample Sample Spike MS MS %Rec.
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits
Styrene
ND
100
91.94
ug/L
92
70-130
1,1,2,2-Tetrachloroethane
ND
100
90.52
ug/L
91
56-145
Tetrachloroethene
139
100
272.1
ug/L
133
57-138
Tetrahydrofuran
4.82
J
200
148.1
ug/L
72
40-136
Toluene
1.22
J
100
117.6
ug/L
116
64-136
trans- 1,2-Dich loroethene
2.49
J
100
111.5
ug/L
109
59-143
trans- 1, 3-Dich loropropene
ND
100
104.7
ug/L
105
63-142
1,2,4-Trichlorobenzene
ND
100
71.80
ug/L
72
47-147
1,1,1-Trichloroethane
134
100
257.4
ug/L
124
68-144
1,1,2-Trichloroethane
1.44
J
100
111.7
ug/L
110
70-130
Trichloroethene
1690
100
1800
4
ug/L
106
63-135
Trichlorofluoromethane
ND
100
129.1
ug/L
129
44-150
1,1,2-Trichloro-1,2,2-trifluoroetha
322
100
364.0
F1
ug/L
42
63-150
ne
Vinyl chloride
ND
100
99.28
ug/L
99
57-150
Xylenes, Total
ND
200
183.0
ug/L
91
69-132
MS
MS
Surrogate
%Recovety
Qualifier
Limits
4-Bromofluorobenzene (Surr)
93
70-130
Dibromofluoromethane (Surr)
110
70-130
1,2-Dichloroethane-d4 (Surr)
125
70-130
Toluene-d8 (Surr)
113
70-130
Lab Sample ID: 490-139553-1 MSD
Client Sample ID:
J1 155-MW-1 2-102617
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472139
Sample
Sample
Spike
MSD
MSD
%Rec.
RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
RPD
Limit
Acetone
39.5
-
500
-
529.7
wg-/L
-98
-3-9-- 15-0
-7
-28
Benzene
1.56
J
100
89.15
ug/L
88
55-147
16
22
Bromodichloromethane
ND
100
99.24
ug/L
99
70-140
3
196
Bromoform
ND
100
97.22
ug/L
97
53-150
7
20
Bromomethane
ND
100
78.37
ug/L
78
30-150
3
44
2-Butanone (MEK)
ND
500
408.6
ug/L
82
50-143
25
28
Carbon disulfide
ND
100
79.97
ug/L
80
35-150
16
34
Carbon tetrachloride
ND
100
111.0
ug/L
111
56-150
10
18
Chlorobenzene
ND
100
93.86
ug/L
94
70-130
6
15
Chloroethane
ND
100
102.6
ug/L
103
58-141
8
31
Chloroform
12.4
100
115.9
ug/L
104
66-138
15
21
Chloromethane
ND
100
84.35
ug/L
84
10-150
11
43
cis- 1,2-Dichloroethene
356
100
448.0
ug/L
92
68-131
12
21
cis- 1,3-Dichloropropene
ND
100
85.97
ug/L
86
70-133
19
19
Cyclohexane
ND
100
83.50
ug/L
83
48-150
18
22
Dibromochloromethane
ND
100
101.2
ug/L
101
66-140
8
19
1,2-Dibromo-3-Chloropropane
ND
100
81.72
ug/L
82
38-138
2
26
1,2-Dibromoethane (EDB)
ND
100
89.15
ug/L
89
65-137
6
21
1,2-Dichlorobenzene
1.05
1
100
104.4
ug/L
103
70-130
5
15
1,3-Dichlorobenzene
ND
100
93.49
ug/L
93
68-131
7
14
TestAmerica Nashville
Page 39 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139553-1 MSD
Matrix: Water
Analysis Batch: 472139
TestAmerica Job ID: 490-139553-1
Client Sample ID: J1 155-MW-1 2-102617
Prep Type: Total/NA
Sample
Sample
Spike
MSD
MSD
%Rec.
RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits RPD
Limit
1,4-Dichlorobenzene
ND
100
97.25
ug/L
97
70-130
3
14
Dichlorodifluoromethane
48.3
100
118.0
ug/L
70
10-150
5
50
1,1-Dichloroethane
88.4
100
195.6
ug/L
107
61-139
6
23
1,2-Dichloroethane
ND
100
97.41
ug/L
97
64-136
16
22
1,1-Dichloroethene
219
100
280.8
ug/L
62
54-150
16
24
1,2-Dichloropropane
ND
100
91.88
ug/L
92
67-130
1
19
Ethylbenzene
ND
100
90.78
ug/L
91
65-139
6
18
2-Hexanone
ND
500
391.1
ug/L
78
44-150
9
21
1 sopropyl benzene
ND
100
87.69
ug/L
88
70-137
6
17
Methyl acetate
ND
200
185.6
ug/L
93
42-136
3
26
Methylcyclohexane
ND
100
88.90
ug/L
89
59-150
5
20
Methylene Chloride
ND
100
98.70
ug/L
99
64-130
9
22
4-Methyl-2-pentanone (MIBK)
21.9
J
500
422.5
ug/L
80
50-140
17
24
Methyl tert-butyl ether
ND
100
89.57
ug/L
90
55-141
9
24
Styrene
ND
100
87.95
ug/L
88
70-130
4
16
1,1,2,2-Tetrachloroethane
ND
100
91.96
ug/L
92
56-145
2
19
Tetrachloroethene
139
100
242.6
ug/L
104
57-138
11
17
Tetrahydrofuran
4.82
J
200
161.4
ug/L
78
40-136
9
27
Toluene
1.22
J
100
93.65
F2
ug/L
92
64-136
23
18
trans- 1,2-Dich loroethene
2.49
J
100
104.4
ug/L
102
59-143
7
25
trans- 1, 3-Dich loropropene
ND
100
85.22
F2
ug/L
85
63-142
21
18
1,2,4-Trichlorobenzene
ND
100
81.08
ug/L
81
47-147
12
24
1,1,1-Trichloroethane
134
100
224.3
ug/L
91
68-144
14
17
1,1,2-Trichloroethane
1.44
J
100
92.50
F2
ug/L
91
70-130
19
18
Trichloroethene
1690
100
1788
4
ug/L
94
63-135
1
17
Trichlorofluoromethane
ND
100
117.5
ug/L
117
44-150
9
32
1,1,2-Trichloro-1,2,2-trifluoroetha
322
100
352.4
F1
ug/L
30
63-150
3
22
ne
Vinyl chloride
ND
100
90.78
ug/L
91
57-150
9
37
Xylenes, Total
ND
200
173.1
ug/L
87
69-132
6
17
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr)
100
70-130
Dibromofluoromethane (Surr)
95
70-130
1,2-Dichloroethane-d4 (Surr)
119
70-130
Toluene-d8 (Surr)
102
70-130
Method: 8270D - Semivolatile Organic Compounds
(GC/MS)
Lab Sample ID: MB 490-471651/1-A
Client Sample ID: Method
Blank
Matrix: Water
Prep Type:
Total/NA
Analysis Batch: 471924
Prep Batch: 471651
MB MB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
ND
10.0
6.10 ug/L
10/28/17 20:55
10/30/17 12:24
1
TestAmerica Nashville
Page 40 of 70 11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 8270D - Sernivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 490-471651/1-A
Matrix: Water
Analysis Batch: 471924
MB MB
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
76
10-120
2-Fluorobiphenyl (Surr)
80
29-120
2-Fluorophenol (Surr)
66
10-120
Nitrobenzene-d5 (Surr)
78
27-120
Phenol-d5 (Surr)
48
10-120
Terphenyl-d14 (Surr)
96
13-120
Lab Sample ID: LCS 490-471651/2-A
Matrix: Water
Analysis Batch: 471924
Spike LCS LCS
Analyte
Added Result Qualifier
1,4-Dioxane
----40b
13.80
LCS
LCS
Surrogate
%Recovery
Qualifier
Limits
2,4,6-Tribromophenol (Surr)
71
10-120
2-Fluorobiphenyl (Surr)
67
29-120
2-Fluorophenol (Surr)
54
10-120
Nitrobenzene-d5 (Surr)
69
27-120
Phenol-d5 (Surr)
40
10-120
Terphenyl-d14 (Surr)
77
13-120
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 471651
Prepared
Analyzed Dil Fac
10128117 20:55
101301171 1
10128117 20:55
10130117 12:24 1
10128117 20:55
10130117 12:24 1
10128117 20:55
10130117 12:24
10128117 20:55
10130117 12:24 1
10128117 20:55
10130117 12:24 '
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 471651
%Rec.
Unit D %Rec Limits
ug/L — 34 —10 - M
Lab Sample ID: LCSID 490-471651/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471924
Prep Batch: 471651
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier Unit
D %Rec Limits RPD Limit
1,4-Dioxane
40.0
11.01 ug/L
28 10-110 22 33
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr) 74
10-120
2-Fluorobiphenyl (Surr) 68
29-120
2-Fluorophenol (Surr) 49
10-120
Nitrobenzene-d5 (Surr) 65
27-120
Phenol-d5 (Surr) 36
10-120
L Terphenyl-d14 (Surr) 76
13-120
Method: RSK-175 - Dissolved Gases (GC)
F
Lab Sample ID: MB 490-473602/5
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 473602
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Ethane ND
0.00500
0.00270 mg/L
11/06/17 11:14 1
Ethylene ND
0.00500
0.00220 mg/L
11/06/17 11:14 1
Methane ND
0.00500
0.00170 mg/L
11/06/17 11:14 1
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Page 41 of 70 11/10/2017

QC Sample Results
Client: CIDM Smith, Inc.
ProjecVSite: NGC-Murphy NC
Method: RSK-175 - Dissolved Gases (GC) (Continued)
Lab Sample ID: MB 490-473602/5
Matrix: Water
Analysis Batch: 473602
MB MB
Surrogate %Recovery Qualifier Limits
Acetylene (Surr) 89 62-124
Lab Sample ID: LCS 490-473602/6
Matrix: Water
Analysis Batch: 473602
TestAmerica Job ID: 490-139553-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed DR Fac
11106117 11:14 1
Client Sample ID: Lab Control Sample 9
Prep Type: Total/NA F
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Ethane
-
0.527
- -
0.5101
rrig/L
97
60-120
Ethylene
0.493
0.4898
mg/L
99
80-120
Methane
0.287
0.2792
mg/L
97
80-120
LCS LCS
Surrogate %Recovery Qualifier Limits
Acetylene (Surr) 91 62-124
Lab Sample ID: LCSID 490-47360217
Matrix: Water
Analysis Batch: 473602
Analyte
Ethane
Ethylene
Methane
LCSD LCSD
Surrogate %Recovery Qualifier
Acetylene (Surr) 90
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec.
RPD
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
0.527
0.5020
mg/L
95
80-120
2
30
0.493
0.4745
mg/L
96
80-120
3
29
0.287
0.2762
mg/L
96
80-120
1
33
Limits
62-124
Method: 300.0 - Anions, Ion Chromatography
Lab Sample ID: MB 490-471357/3
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471357
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Chloride ND
1.00 0.700 mg/L
10/27/17 15:45 1
Sulfate ND
1.00 0.600 mg/L
10/27/17 15:45 1
Lab Sample ID: LCS 490-471357/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471357
Spike
LCS LCS
%Rec.
Analyte Added
Result Qualifier
Unit D %Rec Limits
Chloride 10.0
- -
10.94
m-g/L -109 --90 - 1-10
Sulfate 10.0
10.57
mg/L 106 90-110
Page 42 of 70
TestAmerica Nashville
11/10/2017

QC Sample Results
Client: CDIVI Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Method: 300.0 - Anions, Ion Chromatography (Continued)
Lab Sample ID: LCSD 490-47135715
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471357
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Chloride
10.0
10.89
mg/L
109 90-110 0 20
Sulfate
10.0
10.42
mg/L
104 90-110 1 20
Lab Sample ID: 490-139557-A-1 MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471357
Sample
Sample
Spike
ms
ms
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Chloride 11.7
2.00
12.14
4—
rrig—/L
— —21 —6-0-- 12-0
Sulfate 1.93
2.00
4.166
mg/L
112 80-120
Lab Sample ID: 490-139557-A-1 MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471357
Sample
Sample
Spike
MSD
MSD
%Rec. RPD
Analyte Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Chloride 11.7
2.00
11.61
4
mg/L
-6 80-120 4 20
Sulfate 1.93
2.00
4.190
mg/L
113 80-120 1 20
Lab Sample ID: MB 490-471358/3
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471358
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Nitrate as N
ND
0.100
0.0500 mg/L
10/27/17 15:45 1
Lab Sample ID: LCS 490-471358/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471358
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Nitrate as N
1.00
1.071
mg/L
107 90-110
Lab Sample ID: LCSD 490-47135815
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471358
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Nitrate as N
1.00
1.081
mg/L
108 90-110 1 20
Lab Sample ID: 490-139557-A-1 MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471358
Sample
Sample
Spike
ms
ms
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Nitrate as N 0.0863
J F1
0.200
0.1556
F-1—
mg—/L
—35 --60--120
TestAmerica Nashville
Page 43 of 70 11/10/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 300.0 - Anions, Ion Chromatography (Continued)
Lab Sample ID: 490-139557-A-1 MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471358
Sample
Sample
Spike
IMSID IMSID
%Rec. RPID
Analyte Result
Qualifier
Added
Result Qualifier
Unit D %Rec Limits RPID Limit
Nitrate as N 0.0863
J F1
0.200
0. 1694 V1 —
rng--/L —41 1-20 — 9 —20
Lab Sample ID: MB 490-471599/3
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471599
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Chloride
IND
1.00 0.700 mg/L
10/28/17 17:47 1
Sulfate
IND
1.00 0.600 mg/L
10/28/17 17:47 1
Lab Sample ID: LCS 490-471599/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471599
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Chloride
—
10.0
10.78
-Fn-g—lL —108 96- 11-0
Sulfate
10.0
10.98
mg/L 110 90-110
Lab Sample ID: LCSD 490-471599/5
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471599
Spike
LCSID
LCSID %Rec. RPID
Analyte
Added
Result
Qualifier Unit D %Rec Limits RPID Limit
Chloride
10.0
10.76
mg/L 107 90-110 0 20
Sulfate
10.0
10.94
mg/L 109 90-110 0 20
Method: 200.7 Rev 4.4 - Metals (ICP)
Lab Sample ID: MB 490-472037/1-B
Matrix: Water
Analysis Batch: 472726
IMB M13
Analyte Result Qualifier
Iron IND
Lab Sample ID: LCS 490-472037/2-B
Matrix: Water
Analysis Batch: 472920
Analyte
Iron
FLab Sample ID: 490-139553-1 MS
Matrix: Water
Analysis Batch: 472726
IAnalyte
Iron
Sample Sample
Result Qualifier
ND
Client Sample ID: Method Blank
Prep Type: Dissolved
Prep Batch: 472418
RL MIDIL Unit D Prepared Analyzed Dil Fac
0.100 0.0500 mg/L 11/01/1707:K2 11/02/1702:30 1
Client Sample ID: Lab Control Sample
Prep Type: Dissolved
Prep Batch: 472418
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
— -Fn-g—lL —102 85--115
1.00 1.023
Client Sample ID: J1155-MW-12-102617
Prep Type: Dissolved
Prep Batch: 472418
Spike IVIS IVIS %Rec.
Added Result Qualifier Unit D %Rec Limits
1.00 0.8653 mg/L 87 70-130
TestAmerica Nashville
Page 44 of 70 11/10/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 200.7 Rev 4.4 - Metals (ICP) (Continued)
TestAmerica Job ID: 490-139553-1
Lab Sample ID: 490-139553-1 MSD Client Sample ID: J11 155-MW-1 2-102617
Matrix: Water Prep Type: Dissolved
Analysis Batch: 472726 Prep Batch:472418
Sample Sample Spike IVISD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPID Limit
Iron ND 1.00 0.8859 mg/L 89 70-130 2 20
Method: 200.8 - Metals (ICP/MS) 9
Lab Sample ID: MB 490-472038/1-B Client Sample ID: Method Blank F-
Matrix: Water Prep Type: Dissolved
Analysis Batch: 472734 Prep Batch: 472422 F
IVIB IVIB
Analyte Result Qualifier
RL
IVIDL Unit
D Prepared Analyzed Dil Fac
L Manganese
ND
--b-.-00-400
O-DOO-150 m—g&—
— 11/01/17 07:37 11/01/17 16:06 1
Lab Sample ID: LCS 490-472038/2-B
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472734
Prep Batch: 472422
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Manganese
0.100
0.09639
mg/L 96 85-115
Lab Sample ID: 490-139553-1 MS
Client Sample ID: J1 155-MW-12-102617
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472734
Prep Batch: 472422
Sample
Sample
Spike
IVIS
MS
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier
Unit D %Rec Limits
Manganese 0.261
F1
0.100
0.3490
mg/L 88 70-130
Lab Sample ID: 490-139553-1 MSD Client Sample ID: J1155-MW-12-102617
Matrix: Water Prep Type: Dissolved
Analysis Batch: 472734 Prep Batch: 472422
Sample Sample Spike IVISD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPID Limit
L Manganese 0.261 F1 0.100 0.2912 F1 mg/L 30 70-130 18 20
Method: 350.1 - Nitrogen, Ammonia
Lab Sample ID: MB 490-472555/5
Matrix: Water
Analysis Batch: 472555
MB MB
Analyte Result Qualifier
Ammonia (as N) ND
Lab Sample ID: LCS 490-472555/6
Matrix: Water
Analysis Batch: 472555
Client Sample ID: Method Blank
Prep Type: Total/NA
RL IVIDL Unit D Prepared Analyzed Dil Fac
0.0500 0.0500 mg/L 11/01/17 11:07 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
LAmmonia (as N) 5.00 5.420 mg/L 108 90-110
Page 45 of 70
TestAmerica Nashville
11/10/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 350.1 - Nitrogen, Ammonia (Continued)
TestAmerica Job ID: 490-139553-1
Lab Sample ID: LCSD 490-472555/7
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472555
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits RPD Limit
Ammonia (as N)
5.00
5.410
mg/L
108 90-110 0 20
Lab Sample ID: 490-139626-C-1 MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472555
Sample
Sample
Spike
IVIS
IVIS
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Ammonia (as N) ND
5.00
5.240
mg/L
105 90-110
Lab Sample ID: 490-139745-0-4 MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472555
Sample
Sample
Spike
IVIS
IVIS
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec Limits
Ammonia (as N) ND
5.00
5.250
mg/L
105 90-110
Method: 9034 - Sulfide, Acid soluble and
Insoluble (Titrimetric)
Lab Sample ID: MB 490-473647/1-A
Matrix: Water
Analysis Batch: 473706
MB MB
Analyte Result Qualifier
Sulfide ND
Lab Sample ID: LCS 490-473647/2-A
Matrix: Water
Analysis Batch: 473706
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 473647
RL MDL Unit D Prepared Analyzed Dil Fac
5.00 0.700 mg/L 11/01/17 13:00 11/01/17 15:06 —1
Client Sample ID: Lab Control Sample
Spike
LCS
LCS
Analyte
Added
Result
Qualifier
Unit
Sulfide
20.0
19.63
mg/L
Lab Sample ID: 490-139537-D-2-B MS
Matrix: Water
Analysis Batch: 473706
Sample Sample
Spike
ms
ms
Result Qualifier
Added
Result
Qualifier
Unit
L�Anlalyte
Su fide ND
20.0
19.16
mg/L
Lab Sample ID: 490-139537-D-2-C MSD
Matrix: Water
Analysis Batch: 473706
Sample Sample
Analyte Result Qualifier
Lsulfide ND
Prep Type: Total/NA
Prep Batch: 473647
%Rec.
D %Rec Limits
— — --T— — —
98 0-130
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 473647
%Rec.
D %Rec Limits
96 70-130
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 473647
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 19.32 mg/L 96 70-130 1 10
Page 46 of 70
TestAmerica Nashville
11/10/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 490-139626-D-3-B DU
Matrix: Water
Analysis Batch: 473706
Sample Sample DU DU
Analyte Result Qualifier Result Qualifier Unit D
Sulfide ND ND mg/L
Client Sample ID: Duplicate
Prep Type: Total/NA
Prep Batch:473647
RPD
RPD Limit
NC 20
Method: 9060A - Organic Carbon, Total (TOC)
Lab Sample ID: MB 490-474798/2 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 474798
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Organic Carbon ND 1.00 0.500 mg/L 11/08/17 16:53 1
Lab Sample ID: LCS 490-474798/6
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474798
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Total Organic Carbon
10.0
10.15
mg/L 102 90-110
Lab Sample ID: 490-139553-1 MS
Client Sample ID: J1155-MW-12-102617
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474798
Sample
Sample
Spike
MS
MS
%Rec.
Analyte Result
Qualifier
Added
Result
Qualifier
Unit D %Rec Limits
Total Organic Carbon 0.563
J
20.0
20.92
m-g—/L 102 —75---122
Lab Sample ID: 490-139553-1 MSD
Client Sample ID: J1155-MW-12-102617
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474798
Sample
Sample
Spike
MSD
MSD
%Rec. RPD
Analyte Result
Organic Carbon 0.563
Qualifier
J
Added
20.0
Result
21.08
Qualifier
Unit D %Rec Limits RPD Limit
mg/L 103 75-122 1 20
LTotal
Lab Sample ID: 490-139626-H-5 MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474798
Sample
Sample
Spike
ms
ms
%Rec.
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
Total Organic Carbon
ND
20.0
20.60
mg/L
103
75-122
Lab Sample ID: 490-139626-H-5
MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474798
Sample
Sample
Spike
MSD
MSD
%Rec. RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits RPD Limit
LTotal Organic Carbon
ND
20.0
20.76
mg/L
104
75-122 1 20
TestAmerica Nashville
Page 47 of 70 11/10/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: SM 2320B - Alkalinity
Lab Sample ID: MB 490-474401/54
Matrix: Water
Analysis Batch: 474401
MB MB
Analyte Result Qualifier
Alkalinity ND
Lab Sample ID: LCS 490-474401/55
Matrix: Water
Analysis Batch: 474401
Analyte
Alkalinity
Lab Sample ID: LCSD 490-474401/77
Matrix: Water
Analysis Batch: 474401
Analyte
Alkalinity
F
Lab Sample ID: 490-139565-G-1 DU
Matrix: Water
Analysis Batch: 474401
Sample Sample
Analyte Result Qualifier
LAlkalinity 128
RL MDL Unit D
10.0 5.00 mg/L
TestAmerica Job ID: 490-139553-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed Dil Fac
11/08/17 10:26 -1
Client Sample ID: Lab Control Sample 9
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
- - - -Fn-g-lL -100 9-0---110
100 99.72
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
100 98.89 mg/L 99 90-110 1 20
Client Sample ID: Duplicate
Prep Type: Total/NA
Method: SM 2540C - Solids, Total Dissolved (TDS)
Lab Sample ID: MB 490-472517/1
Matrix: Water
Analysis Batch: 472517
Analyte
Total Dissolved Solids
Lab Sample ID: LCS 490-472517/2
Matrix: Water
Analysis Batch: 472517
I Analyte
LTotal Dissolved Solids
Lab Sample ID: LCSD 490-472517/3
Matrix: Water
Analysis Batch: 472517
IAnalyte
LTotal Dissolved Solids
DU DU RPD
Result Qualifier Unit D RPD Limit
31.11 F3 mg/L 122 20
MB MB
Result Qualifier RL MDL Unit
ND 10.0 7.00 mg/L
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
11/01/17 19:09 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
100 106.0 mg/L 106 90-110
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
- - - -FngIL 9-- -
100 104.0 104 0-110 2 20
TestAmerica Nashville
Page 48 of 70 11/10/2017

QC Sample Results
Client: CDM Smith, Inc. TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Method: SM 2540C - Solids, Total Dissolved (TDS) (Continued)
Lab Sample ID: 490-139538-B-1 DU
Matrix: Water
Analysis Batch: 472517
Sample Sample DU DU
Analyte Result Qualifier Result Qualifier Unit
Total Dissolved Solids 310 316.0 mg/L
Lab Sample ID: 490-139740-E-1 DU
Matrix: Water
Analysis Batch: 472517
Client Sample ID: Duplicate
Prep Type: Total/NA
RPD
D RPD Limit
2 20
Sample Sample DU DU
Analyte Result Qualifier Result Qualifier Unit D
Total Dissolved Solids 2120 2226 mg/L
Method: SM 4500 P E - Orthophosphate
Lab Sample ID: MB 490-471764/3
Matrix: Water
Analysis Batch: 471764
MB MB
Analyte Result Qualifier
Orthophosphate as P ND
Lab Sample ID: LCS 490-471764/4
Matrix: Water
Analysis Batch: 471764
Client Sample ID: Duplicate a
Prep Type: Total/NA
RPD
RPD Limit
5 20
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
0.100 0.0500 mg/L 10/27/17 17:11 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
Orthophosphate as P
0.500
0.5180
mg/L
104
90-110
Lab Sample ID: 490-139553-1 MS
Client Sample ID:
J1155-MW-12-102617
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471764
Sample Sample
Spike
ms
ms
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
Orthophosphate as P ND
0.500
0.5250
mg/L
105
72-129
Lab Sample ID: 490-139553-1 MSD
Matrix: Water
Analysis Batch: 471764
Sample
Sample
Analyte
Result
Qualifier
L Orthophosphate as P
ND
Lab Sample ID: 490-139553-1
DU
Matrix: Water
Analysis Batch: 471764
Sample
Sample
Analyte
Result
Qualifier
L Orthophosphate as P
ND
Client Sample ID: J1155-MW-12-102617
Prep Type: Total/NA
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.500 0.5330 mg/L 107 T2 - 1-29 — 2 20
Client Sample ID: J1155-MW-12-102617
Prep Type: Total/NA
DU DU
Result Qualifier Unit D
ND mg/L
RPD
RPD Limit
NC 20
Page 49 of 70
TestAmerica Nashville
11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: VFA-IC - Volatile Fatty Acids, Ion Chromatography
Lab Sample ID: MB 480-385877/28
Matrix: Water
Analysis Batch: 385877
MB MB
Analyte
Result Qualifier
Acetic acid
ND
Formic -acid
ND
Lactic acid
ND
n-Butyric Acid
ND
Propionic acid
ND
Pyruvic Acid
ND
Lab Sample ID: LCS 480-385877/27
Matrix: Water
Analysis Batch: 385877
Analyte
Acetic acid
Formic -acid
Lactic acid
n-Butyric Acid
Propionic acid
Pyruvic Acid
Lab Sample ID: 490-139553-4 MS
Matrix: Water
Analysis Batch: 385877
Analyte
Sample Sample
Result Qualifier
Acetic acid
ND
Formic -acid
ND
Lactic acid
ND
n-Butyric Acid
ND
Propionic acid
ND
Pyruvic Acid
ND F1
Lab Sample ID: 490-139553-4 MSD
Matrix: Water
Analysis Batch: 385877
Sample Sample
Analyte
Result Qualifier
Acetic acid
ND
Formic -acid
ND
Lactic acid
ND
n-Butyric Acid
ND
Propionic acid
ND
Pyruvic Acid
ND F1
Lab Sample ID: 490-139745-H-2 MS
Matrix: Water
Analysis Batch: 385877
Analyte
Acetic acid
TestAmerica Job ID: 490-139553-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
1.00
0.290
mg/L
11/07/17 06:09 1
1.00
0.260
mg/L
11/07/17 06:09 1
1.00
0.310
mg/L
11/07/17 06:09 1
1.00
0.260
mg/L
11/07/17 06:09
1.00
0.350
mg/L
11/07/17 06:09 1
1.50
0.370
mg/L
11/07/17 06:09 1
Client Sample ID:
Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
D %Rec
Limits
1 Ob
_10.
ff
-
rn��
- 1U
-80
10.0
8.531
mg/L
85
80-120
10.0
10.14
mg/L
101
80-120
10.0
10.26
mg/L
103
80-120
10.0
9.815
mg/L
98
80-120
10.0
9.414
mg/L
94
80-120
Client Sample ID: J1 155-PM-3D-102617
Prep Type: Total/NA
Spike
Added
MS MS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
50.0
50.46
mg/L
101
80-120
50.0
42.01
mg/L
84
80-120
50.0
49.87
mg/L
100
80-120
50.0
51.57
mg/L
103
80-120
50.0
48.39
mg/L
97
80-120
50.0
36.25 F1
mg/L
73
80-120
Client Sample ID: J1 155-PM-3D-102617
Prep Type: Total/NA
Spike
MSD MSD
Added
Result Qualifier
Unit
50.0
- -
51.66
rrig/L
50.0
42.85
mg/L
50.0
50.83
mg/L
50.0
51.24
mg/L
50.0
47.49
mg/L
50.0
36.56 F1
mg/L
Sample Sample Spike MS MS
Result Qualifier Added Result Qualifier Unit
ND 50.0 49.51 mg/L
D %Rec
%Rec.
Limits
RPD
RPD
Limit
103
-120
2
20
86
80-120
2
20
102
80-120
2
20
102
80-120
1
20
95
80-120
2
20
73
80-120
1
20
Client Sample ID: Matrix Spike
Prep Type: Total/NA
%Rec.
D %Rec Limits
99 80-120
Page 50 of 70
TestAmerica Nashville
11/10/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
F
TestAmerica Job ID: 490-139553-1
Method: VFA-lC - Volatile Fatty Acids, Ion Chromatography (Continued)
Lab Sample ID: 490-139745-H-2 MS
Client Sample
ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 385877
Sample Sample
Spike
MS MS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Formic -acid ND
50.0
40.95
mg/L
82
80-120
Lactic acid ND
50.0
48.76
mg/L
98
80-120
n-Butyric Acid ND
50.0
49.91
mg/L
100
80-120
Propionic acid ND
50.0
48.76
mg/L
98
80-120
Pyruvic Acid ND
50.0
43.91
mg/L
88
80-120
TestAmerica Nashville
Page 51 of 70 11/10/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
GC/MS VOA
Analysis Batch: 471321
TestAmerica Job ID: 490-139553-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
8260B
490-139553-2
A 155-MW-37-102617
Total/NA
Water
8260B
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
8260B
490-139553-5
J I 155-PM-7D-1 02617
Total/NA
Water
8260B
490-139553-6
A 155-RW-4-102617
Total/NA
Water
8260B
490-139553-7
A 155-DUP-1 -102617
Total/NA
Water
8260B
MB 490-471321/8
Method Blank
Total/NA
Water
8260B
LCS 490-471321/3
Lab Control Sample
Total/NA
Water
8260B
LCSD 490-471321/4
Lab Control Sample Dup
Total/NA
Water
8260B
490-139553-1 MS
J 1 155-MW- 12-102617
Total/NA
Water
8260B
490-139553-1 MSD
J 1 155-MW- 12-102617
Total/NA
Water
8260B
Analysis Batch: 472139
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
8260B
490-139553-2
A 155-MW-37-102617
Total/NA
Water
8260B
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
8260B
490-139553-4
J I 155-PM-3D-1 02617
Total/NA
Water
8260B
MB 490-472139/7
Method Blank
Total/NA
Water
8260B
LCS 490-472139/4
Lab Control Sample
Total/NA
Water
8260B
LCSD 490-472139/5
Lab Control Sample Dup
Total/NA
Water
8260B
490-139553-1 MS
J 1 155-MW-1 2-102617
Total/NA
Water
8260B
490-139553-1 MSD
J 1 155-MW-1 2-102617
Total/NA
Water
8260B
GUMS Semi VOA
Prep Batch: 471651
Lab Sample ID
490-139553-1
490-139553-2
490-139553-3
490-139553-4
490-139553-5
490-139553-6
M B 490-471651 /1 -A
LCS 490-471651/2-A
LCSD 490-471651/3-A
Analysis Batch: 471924
Lab Sample ID
490-139553-1
490-139553-2
490-139553-3
490-139553-4
490-139553-5
490-139553-6
M B 490-471651 /1 -A
LCS 490-471651/2-A
LCSD 490-471651/3-A
Prep Batch
Prep Batch
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
J 1 155-MW- 12-102617
Total/NA
Water
351 OC
J I 155-MW-37-102617
Total/NA
Water
351 OC
J I 155-PM-3S- 102617
Total/NA
Water
351 OC
J 1 155-PM-3D-1 02617
Total/NA
Water
351 OC
J 1 155-PM-7D-1 02617
Total/NA
Water
351 OC
A 155-RW-4-102617
Total/NA
Water
351 OC
Method Blank
Total/NA
Water
351 Oc
Lab Control Sample
Total/NA
Water
351 Oc
Lab Control Sample Dup
Total/NA
Water
351 Oc
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
J I 155-MW- 12-102617
Total/NA
Water
8270D
471651
J I 155-MW-37-102617
Total/NA
Water
8270D
471651
A 155-PM-3S-1 02617
Total/NA
Water
8270D
471651
J I 155-PM-3D-1 02617
Total/NA
Water
8270D
471651
J I 155-PM-7D-1 02617
Total/NA
Water
8270D
471651
J I 155-RW-4-102617
Total/NA
Water
8270D
471651
Method Blank
Total/NA
Water
8270D
471651
Lab Control Sample
Total/NA
Water
8270D
471651
Lab Control Sample Dup
Total/NA
Water
8270D
471651
a
F
Page 52 of 70
TestAmerica Nashville
11/10/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
GC VOA
Analysis Batch: 473602
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
RSK-175
490-139553-2
A 155-MW-37-102617
Total/NA
Water
RSK-175
490-139553-3
A 155-PM-3S-102617
Total/NA
Water
RSK-175
490-139553-4
J I 155-PM-3D-1 02617
Total/NA
Water
RSK-175
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
RSK-175
490-139553-6
A 155-RW-4-102617
Total/NA
Water
RSK-175
MB 490-473602/5
Method Blank
Total/NA
Water
RSK-175
LCS 490-473602/6
Lab Control Sample
Total/NA
Water
RSK-175
LCSD 490-473602/7
Lab Control Sample Dup
Total/NA
Water
RSK-175
HPLCAC
Analysis Batch: 471357
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J I 155-MW- 12-102617
Total/NA
Water
300.0
490-139553-2
J I 155-MW-37-102617
Total/NA
Water
300.0
490-139553-2
J I 155-MW-37-102617
Total/NA
Water
300.0
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
300.0
490-139553-4
J 1 155-PM-3D-1 02617
Total/NA
Water
300.0
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
300.0
490-139553-6
A 155-RW-4-102617
Total/NA
Water
300.0
MB 490-471357/3
Method Blank
Total/NA
Water
300.0
LCS 490-471357/4
Lab Control Sample
Total/NA
Water
300.0
LCSD 490-471357/5
Lab Control Sample Dup
Total/NA
Water
300.0
490-139557-A-1 MS
Matrix Spike
Total/NA
Water
300.0
490-139557-A-1 MSD
Matrix Spike Duplicate
Total/NA
Water
300.0
Analysis Batch: 471358
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J I 155-MW- 12-102617
Total/NA
Water
300.0
490-139553-2
J I 155-MW-37-102617
Total/NA
Water
300.0
490-139553-3
A 155-PM-3S-102617
Total/NA
Water
300.0
490-139553-4
J 1 155-PM-3D-1 02617
Total/NA
Water
300.0
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
300.0
490-139553-6
A 155-RW-4-102617
Total/NA
Water
300.0
MB 490-471358/3
Method Blank
Total/NA
Water
300.0
LCS 490-471358/4
Lab Control Sample
Total/NA
Water
300.0
LCSD 490-471358/5
Lab Control Sample Dup
Total/NA
Water
300.0
490-139557-A-1 MS
Matrix Spike
Total/NA
Water
300.0
490-139557-A-1 MSD
Matrix Spike Duplicate
Total/NA
Water
300.0
Analysis Batch: 471599
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
300.0
MB 490-471599/3
Method Blank
Total/NA
Water
300.0
LCS 490-471599/4
Lab Control Sample
Total/NA
Water
300.0
LCSD 490-471599/5
Lab Control Sample Dup
Total/NA
Water
300.0
TestAmerica Nashville
Page 53 of 70 11/10/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Metals
Filtration Batch: 472037
TestAmerica Job ID: 490-139553-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-1
J 1 155-MW- 12-102617
Dissolved
Water
Filtration
490-139553-2
A 155-MW-37-102617
Dissolved
Water
Filtration
490-139553-3
A 155-PM-3S-1 02617
Dissolved
Water
Filtration
490-139553-4
J I 155-PM-3D-1 02617
Dissolved
Water
Filtration
490-139553-5
J 1 155-PM-7D-1 02617
Dissolved
Water
Filtration
490-139553-6
A 155-RW-4-102617
Dissolved
Water
Filtration
M B 490-472037/1 -B
Method Blank
Dissolved
Water
Filtration
LCS 490-472037/2-B
Lab Control Sample
Dissolved
Water
Filtration
490-139553-1 MS
J 1 155-MW-1 2-102617
Dissolved
Water
Filtration
490-139553-1 MSD
J 1 155-MW-1 2-102617
Dissolved
Water
Filtration
Filtration Batch: 472038
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-1
J 1 155-MW- 12-102617
Dissolved
Water
Filtration
490-139553-2
A 155-MW-37-102617
Dissolved
Water
Filtration
490-139553-3
A 155-PM-3S-1 02617
Dissolved
Water
Filtration
490-139553-4
J I 155-PM-3D-1 02617
Dissolved
Water
Filtration
490-139553-5
J I 155-PM-7D-1 02617
Dissolved
Water
Filtration
490-139553-6
J I 155-RW-4-102617
Dissolved
Water
Filtration
M B 490-472038/1 -B
Method Blank
Dissolved
Water
Filtration
LCS 490-472038/2-B
Lab Control Sample
Dissolved
Water
Filtration
490-139553-1 MS
J 1 155-MW-1 2-102617
Dissolved
Water
Filtration
490-139553-1 MSD
J 1 155-MW- 12-102617
Dissolved
Water
Filtration
Prep Batch: 472418
Prep Batch
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J 1 155-MW- 12-102617
Dissolved
Water
200.7
472037
490-139553-2
A 155-MW-37-102617
Dissolved
Water
200.7
472037
490-139553-3
A 155-PM-3S-1 02617
Dissolved
Water
200.7
472037
490-139553-4
J I 155-PM-3D-1 02617
Dissolved
Water
200.7
472037
490-139553-5
J I 155-PM-7D-1 02617
Dissolved
Water
200.7
472037
490-139553-6
J I 155-RW-4-102617
Dissolved
Water
200.7
472037
M B 490-472037/1 -B
Method Blank
Dissolved
Water
200.7
472037
LCS 490-472037/2-B
Lab Control Sample
Dissolved
Water
200.7
472037
490-139553-1 MS
J 1 155-MW-1 2-102617
Dissolved
Water
200.7
472037
490-139553-1 MSD
J 1 155-MW- 12-102617
Dissolved
Water
200.7
472037
Prep Batch: 472422
Lab Sample ID
490-139553-1
490-139553-2
490-139553-3
490-139553-4
490-139553-5
490-139553-6
M B 490-472038/1 -B
LCS 490-472038/2-B
490-139553-1 MS
490-139553-1 MSD
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
J 1 155-MW- 12-102617
Dissolved
Water
200.8
472038
A 155-MW-37-102617
Dissolved
Water
200.8
472038
A 155-PM-3S-1 02617
Dissolved
Water
200.8
472038
J I 155-PM-3D-1 02617
Dissolved
Water
200.8
472038
J I 155-PM-7D-1 02617
Dissolved
Water
200.8
472038
J I 155-RW-4-102617
Dissolved
Water
200.8
472038
Method Blank
Dissolved
Water
200.8
472038
Lab Control Sample
Dissolved
Water
200.8
472038
J 1 155-MW-1 2-102617
Dissolved
Water
200.8
472038
J 1 155-MW-1 2-102617
Dissolved
Water
200.8
472038
a
F
TestAmerica Nashville
Page 54 of 70 11/10/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Metals (Continued)
Analysis Batch: 472726
TestAmerica Job ID: 490-139553-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J 1 155-MW- 12-102617
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-2
A 155-MW-37-102617
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-3
A 155-PM-3S-1 02617
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-4
J I 155-PM-3D-1 02617
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-5
J 1 155-PM-7D-1 02617
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-6
A 155-RW-4-102617
Dissolved
Water
200.7 Rev 4.4
472418
M B 490-472037/1 -B
Method Blank
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-1 MS
J 1 155-MW- 12-102617
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-1 MSD
J 1 155-MW-1 2-102617
Dissolved
Water
200.7 Rev 4.4
472418
Analysis Batch: 472734
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J 1 155-MW- 12-102617
Dissolved
Water
200.8
472422
490-139553-2
A 155-MW-37-102617
Dissolved
Water
200.8
472422
490-139553-3
A 155-PM-3S-1 02617
Dissolved
Water
200.8
472422
490-139553-4
J 1 155-PM-3D-1 02617
Dissolved
Water
200.8
472422
490-139553-5
J 1 155-PM-7D-1 02617
Dissolved
Water
200.8
472422
490-139553-6
A 155-RW-4-102617
Dissolved
Water
200.8
472422
M B 490-472038/1 -B
Method Blank
Dissolved
Water
200.8
472422
LCS 490-472038/2-B
Lab Control Sample
Dissolved
Water
200.8
472422
490-139553-1 MS
J I 155-MW- 12-102617
Dissolved
Water
200.8
472422
490-139553-1 MSD
J 1 155-MW-1 2-102617
Dissolved
Water
200.8
472422
Analysis Batch: 472920
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCS 490-472037/2-B
Lab Control Sample
Dissolved
Water
200.7 Rev 4.4
472418
General Chemistry
Analysis Batch: 385877
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
VFA-lC
490-139553-2
A 155-MW-37-102617
Total/NA
Water
VFA-lC
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
VFA-lC
490-139553-4
J 1 155-PM-3D-1 02617
Total/NA
Water
VFA-lC
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
VFA-lC
490-139553-6
A 155-RW-4-102617
Total/NA
Water
VFA-lC
MB 480-385877/28
Method Blank
Total/NA
Water
VFA-lC
LCS 480-385877/27
Lab Control Sample
Total/NA
Water
VFA-lC
490-139553-4 MS
J I 155-PM-3D-1 02617
Total/NA
Water
VFA-lC
490-139553-4 MSD
J I 155-PM-3D-1 02617
Total/NA
Water
VFA-lC
490-139745-H-2 MS
Matrix Spike
Total/NA
Water
VFA-lC
Analysis Batch: 471764
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
SM 4500 P E
490-139553-2
A 155-MW-37-102617
Total/NA
Water
SM 4500 P E
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
SM 4500 P E
490-139553-4
J 1 155-PM-3D-1 02617
Total/NA
Water
SM 4500 P E
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
SM 4500 P E
a
TestAmerica Nashville
Page 55 of 70 11/10/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
General Chemistry (Continued)
Analysis Batch: 471764 (Continued)
TestAmerica Job ID: 490-139553-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-6
A 155-RW-4-102617
Total/NA
Water
SM 4500 P E
MB 490-471764/3
Method Blank
Total/NA
Water
SM 4500 P E
LCS 490-471764/4
Lab Control Sample
Total/NA
Water
SM 4500 P E
490-139553-1 MS
J 1 155-MW- 12-102617
Total/NA
Water
SM 4500 P E
490-139553-1 MSD
J I 155-MW- 12-102617
Total/NA
Water
SM 4500 P E
490-139553-1 DU
J I 155-MW- 12-102617
Total/NA
Water
SM 4500 P E
Analysis Batch: 472517
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
SM 2540C
490-139553-2
A 155-MW-37-102617
Total/NA
Water
SM 2540C
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
SM 2540C
490-139553-4
J 1 155-PM-3D-1 02617
Total/NA
Water
SM 2540C
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
SM 2540C
490-139553-6
A 155-RW-4-102617
Total/NA
Water
SM 2540C
MB 490-472517/1
Method Blank
Total/NA
Water
SM 2540C
LCS 490-472517/2
Lab Control Sample
Total/NA
Water
SM 2540C
LCSD 490-472517/3
Lab Control Sample Dup
Total/NA
Water
SM 2540C
490-139538-B-1 DU
Duplicate
Total/NA
Water
SM 2540C
490-139740-E-1 DU
Duplicate
Total/NA
Water
SM 2540C
Analysis Batch: 472555
Lab Sample ID
Client Sample ID
490-139553-1
J 1 155-MW- 12-102617
490-139553-2
A 155-MW-37-102617
490-139553-3
A 155-PM-3S-1 02617
490-139553-4
J 1 155-PM-3D-1 02617
490-139553-5
J 1 155-PM-7D-1 02617
490-139553-6
A 155-RW-4-102617
MB 490-472555/5
Method Blank
LCS 490-472555/6
Lab Control Sample
LCSD 490-472555/7
Lab Control Sample Dup
490-139626-C-1 MS
Matrix Spike
490-139745-0-4 MS
Matrix Spike
Prep Batch: 473647
Lab Sample ID
Client Sample ID
490-139553-1
J 1 155-MW- 12-102617
490-139553-2
A 155-MW-37-102617
490-139553-3
A 155-PM-3S-1 02617
490-139553-4
J 1 155-PM-3D-1 02617
490-139553-5
J 1 155-PM-7D-1 02617
490-139553-6
A 155-RW-4-102617
M B 490-473647/1 -A
Method Blank
LCS 490-473647/2-A
Lab Control Sample
490-139537-D-2-B MS
Matrix Spike
490-139537-D-2-C MSD
Matrix Spike Duplicate
490-139626-D-3-B DU
Duplicate
Prep Type
Matrix
Method
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Total/NA
Water
350.1
Prep Type
Matrix
Method
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Total/NA
Water
9030B
Prep Batch
a
Prep Batch F
Prep Batch
Prep Batch
TestAmerica Nashville
Page 56 of 70 11/10/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
General Chemistry (Continued)
Analysis Batch: 473706
TestAmerica Job ID: 490-139553-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
9034
473647
490-139553-2
A 155-MW-37-102617
Total/NA
Water
9034
473647
490-139553-3
A 155-PM-3S-102617
Total/NA
Water
9034
473647
490-139553-4
J I 155-PM-3D-1 02617
Total/NA
Water
9034
473647
490-139553-5
J 1 155-PM-7D-1 02617
Total/NA
Water
9034
473647
490-139553-6
A 155-RW-4-102617
Total/NA
Water
9034
473647
M B 490-473647/1 -A
Method Blank
Total/NA
Water
9034
473647
LCS 490-473647/2-A
Lab Control Sample
Total/NA
Water
9034
473647
490-139537-D-2-B MS
Matrix Spike
Total/NA
Water
9034
473647
490-139537-D-2-C MSD
Matrix Spike Duplicate
Total/NA
Water
9034
473647
490-139626-D-3-B DU
Duplicate
Total/NA
Water
9034
473647
Analysis Batch: 474401
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-1
J1 155-MW-1 2-102617
Total/NA
Water
SM 2320B
490-139553-2
A 155-MW-37-102617
Total/NA
Water
SM 2320B
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
SM 2320B
490-139553-4
J I 155-PM-3D-1 02617
Total/NA
Water
SM 2320B
490-139553-5
J I 155-PM-7D-1 02617
Total/NA
Water
SM 2320B
490-139553-6
J I 155-RW-4-102617
Total/NA
Water
SM 2320B
MB 490-474401/54
Method Blank
Total/NA
Water
SM 2320B
LCS 490-474401/55
Lab Control Sample
Total/NA
Water
SM 2320B
LCSD 490-474401/77
Lab Control Sample Dup
Total/NA
Water
SM 2320B
490-139565-G-1 DU
Duplicate
Total/NA
Water
SM 2320B
Analysis Batch: 474798
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139553-1
J 1 155-MW- 12-102617
Total/NA
Water
9060A
490-139553-2
A 155-MW-37-102617
Total/NA
Water
9060A
490-139553-3
A 155-PM-3S-1 02617
Total/NA
Water
9060A
490-139553-4
J I 155-PM-3D-1 02617
Total/NA
Water
9060A
490-139553-5
J I 155-PM-7D-1 02617
Total/NA
Water
9060A
490-139553-6
J I 155-RW-4-102617
Total/NA
Water
9060A
MB 490-474798/2
Method Blank
Total/NA
Water
9060A
LCS 490-474798/6
Lab Control Sample
Total/NA
Water
9060A
490-139553-1 MS
J 1 155-MW-1 2-102617
Total/NA
Water
9060A
490-139553-1 MSD
J 1 155-MW- 12-102617
Total/NA
Water
9060A
490-139626-H-5 MS
Matrix Spike
Total/NA
Water
9060A
490-139626-H-5 MSD
Matrix Spike Duplicate
Total/NA
Water
9060A
Prep Batch
Prep Batch
a
TestAmerica Nashville
Page 57 of 70 11/10/2017

Lab Chronicle
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample ID: A 155-MW-1 2-102617
Lab Sample ID: 490-139553-1
Date Collected:
10/26/17 09:01
Matrix: Water
Date Received: 10/27/17 09:45
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
8266B
1
--TO -
mL
--TO mL
471321
TO/27/17 18:12
ClA
TAL NSH
Total/NA
Analysis
8260B
5
10 mL
10 mL
472139
10/31/17 13:33
TCT
TAL NSH
Total/NA
Prep
3510C
270 mL
1 mL
471651
10/28/17 20:55
JKG
TAL NSH
Total/NA
Analysis
8270D
2
471924
10/30/17 16:14
KME
TAL NSH
Total/NA
Analysis
RSK-175
1
21 mL
21 mL
473602
11/06/17 12:18
AAB
TAL NSH
Total/NA
Analysis
300.0
1
5 mL
1.0 mL
471357
10/27/17 16:14
JML
TAL NSH
Total/NA
Analysis
300.0
1
471358
10/27/17 16:14
JML
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
Dissolved
Prep
200.7
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NSH
Dissolved
Analysis
200.7 Rev 4.4
1
472726
11/02/17 02:40
LCS
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
Dissolved
Prep
200.8
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
Dissolved
Analysis
200.8
1
472734
11/01/17 16:12
BLG
TAL NSH
Total/NA
Analysis
350.1
1
50 mL
50 mL
472555
11/01/17 11:12
GRIM
TAL NSH
Total/NA
Prep
9030B
50 mL
50 mL
473647
11/01/17 13:00
REM
TAL NSH
Total/NA
Analysis
9034
1
473706
11/01/17 15:00
REM
TAL NSH
Total/NA
Analysis
9060A
1
50 mL
50 mL
474798
11/08/17 19:17
RN
TAL NSH
Total/NA
Analysis
SM 2320B
1
35 mL
35 mL
474401
11/08/17 11:13
BMC
TAL NSH
Total/NA
Analysis
SM 2540C
1
100 mL
100 mL
472517
11/01/17 19:09
BMC
TAL NSH
Total/NA
Analysis
SM 4500 P E
1
10 mL
10 mL
471764
10/27/17 17:13
BLM
TAL NSH
Total/NA
Analysis
VFA-IC
5
385877
11/07/17 07:37
DMIR
TAL BUF
Client Sample ID: J1155-MW-37-102617
Lab Sample ID: 490-139553-2
Date Collected:
10/26/17 10:02
Matrix: Water
Date Received: 10/27/17 09:45
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
10 mL
10 mL
471321
10/27/17 18:38
ClA
TAL NSH
Total/NA
Analysis
8260B
50
10 mL
10 mL
472139
10/31/17 15:15
TCT
TAL NSH
Total/NA
Prep
3510C
270 mL
1 mL
471651
10/28/17 20:55
JKG
TAL NSH
Total/NA
Analysis
8270D
1
471924
10/30/17 14:29
KME
TAL NSH
Total/NA
Analysis
RSK-175
1
21 mL
21 mL
473602
11/06/17 12:23
AAB
TAL NSH
Total/NA
Analysis
300.0
1
5 mL
1.0 mL
471357
10/27/17 16:24
JML
TAL NSH
Total/NA
Analysis
300.0
5
5 mL
1.0 mL
471357
10/27/17 17:42
JML
TAL NSH
Total/NA
Analysis
300.0
5
5 mL
1.0 mL
471358
10/27/17 17:42
JML
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
Dissolved
Prep
200.7
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NISH
Dissolved
Analysis
200.7 Rev 4.4
1
472726
11/02/17 03:16
LCS
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
Dissolved
Prep
200.8
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
Dissolved
Analysis
200.8
1
472734
11/01/17 16:33
BLG
TAL NSH
Total/NA
Analysis
350.1
1
50 mL
50 mL
472555
11/01/17 11:13
GRIM
TAL NSH
TestAmerica Nashville
Page 58 of 70 11/10/2017

Lab Chronicle
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
F
TestAmerica Job ID: 490-139553-1
Client Sample 11): A 155-MW-37-102617
Date Collected: 10/26/17 10:02
Date Received: 10/27/17 09:45
Batch Batch
Prep Type Type Method Run
Dil
Factor
Initial
Amount
Final
Amount
Lab Sample ID: 490-139553-2
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
Total/NA Prep 9030B
50 mL
50 mL
473647
11/01/17 13:00
REM TAL NSH
Total/NA Analysis 9034
1
473706
11/01/17 15:00
REM TAL NSH
Total/NA Analysis 9060A
1
50 mL
50 mL
474798
11/08/17 20:44
RN TAL NSH
Total/NA Analysis SM 2320B
1
35 mL
35 mL
474401
11/08/17 11:20
BMC TAL NSH
Total/NA Analysis SM 2540C
1
100 mL
100 mL
472517
11/01/17 19:09
BMC TAL NSH
Total/NA Analysis SM 4500 P E
1
10 mL
10 mL
471764
10/27/17 17:18
BLM TAL NSH
Total/NA Analysis VFA-IC
5
385877
11/07/17 08:06
DMR TAL BUF
Client Sample ID: A 155-PM-3S-1 02617
Lab Sample ID: 490-139553-3
Date Collected: 10/26/17 12:49
Matrix: Water
Date Received: 10/27/17 09:45
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
10 mL
10 mL
471321
10/27/17 19:03
ClA
TAL NSH
Total/NA
Analysis
8260B
lo
10 mL
10 mL
472139
10/31/17 14:49
TCT
TAL NSH
Total/NA
Prep
3510C
285 mL
1 mL
471651
10/28/17 20:55
JKG
TAL NSH
Total/NA
Analysis
8270D
1
471924
10/30/17 14:50
KME
TAL NSH
Total/NA
Analysis
RSK-175
1
21 mL
21 mL
473602
11/06/17 12:30
AAB
TAL NSH
Total/NA
Analysis
300.0
1
471358
10/27/17 16:33
JML
TAL NSH
Total/NA
Analysis
300.0
10
5 mL
1.0 mL
471357
10/27/17 17:52
JML
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
Dissolved
Prep
200.7
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NSH
Dissolved
Analysis
200.7 Rev 4.4
1
472726
11/02/17 03:21
LCS
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
Dissolved
Prep
200.8
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
Dissolved
Analysis
200.8
1
472734
11/01/17 16:36
BLG
TAL NSH
Total/NA
Analysis
350.1
1
50 mL
50 mL
472555
11/01/17 11:14
GRM
TAL NSH
Total/NA
Prep
9030B
50 mL
50 mL
473647
11/01/17 13:00
REM
TAL NSH
Total/NA
Analysis
9034
1
473706
11/01/17 15:00
REM
TAL NSH
Total/NA
Analysis
9060A
1
50 mL
50 mL
474798
11/08/17 21:12
RN
TAL NSH
Total/NA
Analysis
SM 2320B
1
35 mL
35 mL
474401
11/08/17 11:27
BMC
TAL NSH
Total/NA
Analysis
SM 2540C
1
100 mL
100 mL
472517
11/01/17 19:09
BMC
TAL NSH
Total/NA
Analysis
SM 4500 P E
1
10 mL
10 mL
471764
10/27/17 17:19
BLM
TAL NSH
Total/NA
Analysis
VFA-IC
5
385877
11/07/17 08:35
DMR
TAL BUF
Client Sample ID: A 155-PM-3D-1 02617
Lab Sample ID: 490-139553-4
Date Collected:
10/26/17 11:34
Matrix: Water
Date Received: 10/27/17 09:45
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
82601B-
--16-rnL
16-rnL
47�
-10� 13:07
TCT
TAL NSH
Total/NA
Prep
3510C
265 mL
1 mL
471651
10/28/17 20:55
XG
TAL NSH
TestAmerica
Nashville
Page 59 of 70 11/10/2017

Lab Chronicle
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139553-1
Client Sample 11): A 155-PM-3D-1 02617
Date Collected: 10/26/17 11:34
Date Received: 10/27/17 09:45
Batch Batch
Prep Type Type Method Run
Dil
Factor
Initial
Amount
Final
Amount
Lab Sample ID: 490-139553-4
Matrix: Water
Batch Prepared
Number or Analyzed Analyst Lab
Total/NA
Analysis
8270D
---1
-
-
-4719
24
-
10/30/17 15:11
KME
TAL NSH
Total/NA
Analysis
RSK-175
1
21 mL
21 mL
473602
11/06/17 12:33
AAB
TAL NSH
Total/NA
Analysis
300.0
1
471358
10/27/17 16:43
JML
TAL NSH
Total/NA
Analysis
300.0
10
5 mL
1.0 mL
471357
10/27/17 18:01
JML
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472037
10/30/17 15:32
JU
TAL NSH
Dissolved
Prep
200.7
50 mL
50 mL
472418
11/01/17 07:32
JU
TAL NSH
Dissolved
Analysis
200.7 Rev 4.4
1
472726
11/02/17 03:26
LCS
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472038
10/30/17 15:34
JU
TAL NSH
Dissolved
Prep
200.8
50 mL
50 mL
472422
11/01/17 07:37
JU
TAL NSH
Dissolved
Analysis
200.8
1
472734
11/01/17 16:39
BLG
TAL NSH
Total/NA
Analysis
350.1
1
50 mL
50 mL
472555
11/01/17 11:15
GRM
TAL NSH
Total/NA
Prep
9030B
50 mL
50 mL
473647
11/01/17 13:00
REM
TAL NSH
Total/NA
Analysis
9034
1
473706
11/01/17 15:00
REM
TAL NSH
Total/NA
Analysis
9060A
1
50 mL
50 mL
474798
11/08/17 21:41
RN
TAL NSH
Total/NA
Analysis
SM 2320B
1
35 mL
35 mL
474401
11/08/17 11:34
BMC
TAL NSH
Total/NA
Analysis
SM 2540C
1
100 mL
100 mL
472517
11/01/17 19:09
BMC
TAL NSH
Total/NA
Analysis
SM 4500 P E
1
10 mL
10 mL
471764
10/27/17 17:24
BLM
TAL NSH
Total/NA
Analysis
VFA-IC
5
385877
11/07/17 09:04
DMR
TAL BUF
Client Sample ID: A 155-13M-713-1 02617
Date Collected: 10/26117 14:00
Date Received: 10/27/17 09:45
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analys�
8260B
Total/NA
Prep
351 OC
Total/NA
Analysis
8270D
Total/NA
Analysis
RSK-175
Total/NA
Analysis
300.0
Total/NA
Analysis
300.0
Total/NA
Analysis
300.0
Dissolved
Filtration
Filtration
Dissolved
Prep
200.7
Dissolved
Analysis
200.7 Rev 4.4
Dissolved
Filtration
Filtration
Dissolved
Prep
200.8
Dissolved
Analysis
200.8
Total/NA
Analysis
350.1
Total/NA
Prep
9030B
Total/NA
Analysis
9034
Total/NA
Analysis
9060A
Total/NA
Analysis
SM 2320B
Lab Sample ID: 490-139553-5
Matrix: Water
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
1
10 mL
10 mL
471321
10/27/17 19:54
ClA
TAL NSH
285 mL
1 mL
471651
10/28/17 20:55
JKG
TAL NSH
5
471924
10/30/17 16:35
KME
TAL NSH
1
21 mL
21 mL
473602
11/06/17 12:36
AAB
TAL NSH
1
471357
10/27/17 16:53
JML
TAL NSH
5
5 mL
1.0 mL
471358
10/27/17 18:31
JML
TAL NSH
10
10 mL
1.0 mL
471599
10/28/17 18:38
JML
TAL NSH
50 mL
50 mL
472037
10/30/17 15:32
JU
TAL NSH
50 mL
50 mL
472418
11/01/17 07:32
JU
TAL NSH
1
472726
11/02/17 03:31
LCS
TAL NSH
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
1
472734
11/01/17 16:42
BLG
TAL NSH
1
50 mL
50 mL
472555
11/01/17 11:16
GRM
TAL NSH
50 mL
50 mL
473647
11/01/17 13:00
REM
TAL NSH
1
473706
11/01/17 15:00
REM
TAL NSH
1
50 mL
50 mL
474798
11/08/17 22:10
RN
TAL NSH
1
35 mL
35 mL
474401
11/08/17 11:40
BMC
TAL NSH
Page 60 of 70
TestAmerica Nashville
11/10/2017

Lab Chronicle
Client: CDIVI Smith, Inc. TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Client Sample 11): A 155-PM-7D-1 02617 Lab Sample ID: 490-139553-5
Date Collected: 10/26/17 14:00 Matrix: Water
Date Received: 10/27/17 09:45
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
SM 25��
— I
—166-mL
—166-mL
472�
-11� 19:09
BMC
TAL NSH
Total/NA
Analysis
SM 4500 P E
1
10 mL
10 mL
471764
10/27/17 17:25
BLM
TAL NSH
Total/NA
Analysis
VFA-IC
5
385877
11/07/17 11:30
DMR
TAL BUF
Client Sample ID: J1155-RW-4-102617
Lab Sample ID: 490-139553-6
Date Collected:
10/26/17 14:10
Matrix: Water
Date Received: 10/27/17 09:45
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
10 mL
10 mL
471321
10/27/17 20:20
ClA
TAL NSH
Total/NA
Prep
3510C
280 mL
1 mL
471651
10/28/17 20:55
JKG
TAL NSH
Total/NA
Analysis
8270D
1
471924
10/30/17 15:53
KME
TAL NSH
Total/NA
Analysis
RSK-175
1
21 mL
21 mL
473602
11/06/17 12:45
AAB
TAL NSH
Total/NA
Analysis
300.0
1
471357
10/27/17 17:03
JML
TAL NSH
Total/NA
Analysis
300.0
1
471358
10/27/17 17:03
JML
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
Dissolved
Prep
200.7
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NSH
Dissolved
Analysis
200.7 Rev 4.4
1
472726
11/02/17 03:36
LCS
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
Dissolved
Prep
200.8
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
Dissolved
Analysis
200.8
1
472734
11/01/17 16:45
BLG
TAL NSH
Total/NA
Analysis
350.1
1
50 mL
50 mL
472555
11/01/17 11:17
GRM
TAL NSH
Total/NA
Prep
9030B
50 mL
50 mL
473647
11/01/17 13:00
REM
TAL NSH
Total/NA
Analysis
9034
1
473706
11/01/17 15:00
REM
TAL NSH
Total/NA
Analysis
9060A
1
50 mL
50 mL
474798
11/08/17 22:39
RN
TAL NSH
Total/NA
Analysis
SM 2320B
1
35 mL
35 mL
474401
11/08/17 11:46
BMC
TAL NSH
Total/NA
Analysis
SM 2540C
1
100 mL
100 mL
472517
11/01/17 19:09
BMC
TAL NSH
Total/NA
Analysis
SM 4500 P E
1
10 mL
10 mL
471764
10/27/17 17:26
BLM
TAL NSH
Total/NA
Analysis
VFA-IC
5
385877
11/07/17 11:59
DMR
TAL BUF
Client Sample 11): J1155-DUP-1-102617
Lab
Sample ID: 490-139553-7
Date Collected:
10/26/17 16:00
Matrix: Water
Date Received: 10/27/17 09:45
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260B
1
10 mL
10 mL
471321
10/27/17 20:45
C1 A
TAL NSH
Laboratory References:
TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 61 of 70 11/10/2017

Method Summary
Client: CIDIVI Smith, Inc.
TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Method Method Description
Protocol
Laboratory
8260B Volatile Organic Compounds (GC/MS)
SW846
TAL NSH
8270D Semivolatile Organic Compounds (GC/MS)
SW846
TAL NSH
RSK-175 Dissolved Gases (GC)
RSK
TAL NSH
300.0 Anions, Ion Chromatography
MCAWW
TAL NSH
200.7 Rev 4.4 Metals (ICP)
EPA
TAL NSH
200.8 Metals (ICP/MS)
EPA
TAL NSH
350.1 Nitrogen, Ammonia
MCAWW
TAL NSH
9034 Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL NSH
9060A Organic Carbon, Total (TOC)
SW846
TAL NSH
SM 2320B Alkalinity
SM
TAL NSH
SM 2540C Solids, Total Dissolved (TDS)
SM
TAL NSH
SM 4500 P E Orthophosphate
SM
TAL NSH
VFA-IC Volatile Fatty Acids, Ion Chromatography
TestAmerica SOP
TAL BUF
Protocol References:
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
RSK = Sample Prep And Calculations For Dissolved Gas Analysis In Water Samples
Using A GC Headspace Equilibration Technique, RSKSOP-1 75,
Rev. 0, 8/11/94, USEPA Research Lab
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods",
Third Edition, November 1986 And Its Updates.
TestAmerica SOP = TestAmerica, Inc., Standard Operating Procedure
Laboratory References:
TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 62 of 70 11/10/2017

Accreditation/Certification Summary
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139553-1
Project/Site: NGC-Murphy NC
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 387 12-31-17
The following analytes are included in this report, but accred itation/certifi cation is not offered by the governing authority:
Analysis Method Prep Method Matrix Analyte
9034 9030B Water Sulfide
RSK-175 Water Ethane
RSK-175 Water Ethylene
RSK-175 Water Methane
Laboratory: TestAmerica Buffalo
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
EPA Region
Identification Number
Expiration Date
Arkansas DEQ
State Program
6
88-0686
07-06-18
California
State Program
9
2931
04-01-18
Connecticut
State Program
1
PH-0568
09-30-18
Florida
NELAP
4
E87672
06-30-18
Georgia
State Program
4
10026 (NY)
03-31-18
Georgia
State Program
4
956
03-31-18
Illinois
NELAP
5
200003
09-30-18
Iowa
State Program
7
374
03-01-19
Kansas
NELAP
7
E-10187
01-31-18
Kentucky (DW)
State Program
4
90029
12-31-17
Kentucky (UST)
State Program
4
30
03-31-18
Kentucky (WW)
State Program
4
90029
12-31-17
Louisiana
NELAP
6
02031
06-30-18
Maryland
State Program
3
294
03-31-18
Massachusetts
State Program
1
M-NY044
06-30-18
Michigan
State Program
5
9937
04-01-09
Minnesota
NELAP
5
036-999-337
12-31-17
New Hampshire
NELAP
1
2973
09-11-18
New Jersey
NELAP
2
NY455
06-30-18
New York
NELAP
2
10026
03-31-18
North Dakota
State Program
8
R-176
03-31-18
Oklahoma
State Program
6
9421
08-31-18
Oregon
NELAP
10
NY200003
06-09-18
Pennsylvania
NELAP
3
68-00281
07-31-18
Rhode Island
State Program
1
LA000328
12-30-17
Tennessee
State Program
4
TN02970
03-31-18
Texas
NELAP
6
T104704412-15-6
07-31-18
USDA
Federal
P330-11-00386
11 -26-17
Virginia
NELAP
3
460185
09-14-18
Washington
State Program
10
C784
02-10-18
Wisconsin
State Program
5
998310390
08-31-18
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
TestAmerica Nashville
Page 63 of 70 11/10/2017

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTjNG 4 -139553 Chain of ��us��dy
Nashville, TN COOLER RECEIPT FORM
Cooler Received/Opened On 10-27-2017_@_09:45
Time Samples Removed From Coolerj�'o Time Samples Placed In Storage (2 Hour Window)
1. Trackingit—Tisy— (last 4 digits, FedEx) Courier: JedEx
-
t t
_ PH Strip LotAvvn
IR Gun ID31470366 51( Chlorine Strip Lotceq-PW
-
-Iq
2. Temperature of rep. sample or temp blank when opened: I Degrees Celsius
3. If Item #2 temperature is OoC or less, was the representative sample or temp ank frozen?
YES NO.&
4. Were custody seals on outside of cooler?
NO ... NA
If yes, how many and where:
5. Were the seals intact, signed, and dated correctly?
E ... NO ... NA
k Z
6. Were custody papers inside cooler?
... NA
I certify that I opened the cooler and answered questions 1-6 (intiall
7. Were custody seals on containers: YES 6P and Intact
YES ... NO.61A,
Were these signed and dated correctly?
YES ... N 0--FA
8. Packing maV1 used? 49-bble nll� Plastic bag Peanuts Vermiculite Foam Insert Paper
Other None
9. Cooling process: -6p Ice -pack Ice (direct contact) Dry ice
Other None
10. Did all containers arrive in good condition (unbroken)?
... NO ... NA
11. Were all container labels complete (#, date, signed, pres., etc)?
N 0 ... NA
12. Did all container labels and tags agree with custody papers?
NO ... NA
13a. Were VOA vials received?
-O�S ... NO...NA
b. Was there any observable headspace, present in any VOA vial?
-P ... NO...NA
0 04 Larger than this.
14. Was there a Trip Blank in this cooler? YES -:-&...NA If multiple coolers, sequence #
I certify that I unloaded the cooler and answered questions 7-14 (intial)
15a. On pres'd bottles, did PH test strips suggest preservation reached the correct pH level?
b. Did the bottle labels indicate that the correct preservatives were used
16. Was residual chlorine present?
I certifv that I checked for chlorine and DH as Per SOP and answered auestions 15-16 (intial)
17. Were custody papers properly filled out (ink, signed, etc)?
18. Did you sign the custody papers in the appropriate place?
19. Were correct containers used for the analysis requested?
20. Was sufficient amount of sample sent in each container?
Q21. Were there Non -Conformance issues at login? C'S71NO Was a NCM generated? IF .. NO ... #.
BIS = Broken in shipment
Cooler Receipt Fonn.doc LF-1
End ofForrn
Page 64 of 70
.-- NO ... NA
... NO ... NA
YE;$.N
... NO...NA
YES ... NO ... NA
K:;/
()9 ... NO ... NA
Q... NO ... NA
Revised 8/23/17
11/10/2017

Ak 2 a In,
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN
COOLER RECEIPT FORM
Cooler Received/Opened On10/271170945
Loc: 490
139553
Time Samples Removed From Cooler Time Samples Placed In Storage (2 Hour Window)
1. Tracking # t 6 56 (last 4 digits, FedEx) Courier: _FedEx_
IR Gun ID31470368 PH Strip Lot /4�0-7?�qhlorine Strip Lot QMW
2. Temperature of rep. sample or temp blank when opened: (0 '-L-Degrees Celsius
3. If Item #2 temperature is O*C or less, was the representative sample or temp blank frozen? YES NO..(NA)
4. Were custody seals on outside of cooler? I&S.- NO ... NA
If yes, how many and where:
5. Were the seals intact, signed, and dated correctly? NO ... NA
6. Were custody papers inside cooler? It/ YES.JON )...NA
I certify that I opened the cooler and answered questions 1-6 (intial
7. Were custody seals on containers: YES and Intact YES ... NOZ��?
Were these signed and dated correctly'7 YES ... N<P
8. Packing mat'l used? elTu�bblewr Plastic bag Peanuts Vermiculite Foam Insert Paper Other None
9. Cooling process: _Qi�N Ice -pack Ice (direct contact) Dry ice Other None
10. Did all containers arrive in good condition (unbroken)? (I�NO ... NA
11. Were all container labels complete (#, date, signed, pres., etc)? ff) .. NO ... NA
12. Did all container labels and tags agree with custody papers? (Y9 ... NO ... NA
13a. Were VIDA vials received? (215DA6 ... NA
b. Was there any observable headspace present in any VOA vial? YES.&) ... NA
0 4' Larger than this.
14. Was there a Trip Blank in this cooler? YES.�q...NA if multiple coolers, sequence #
I certify that I unloaded the cooler and answered questions 7-14 (Intial At (RL
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct PH level? MR ... NO ... NA
b. Did the bottle labels indicate that the correct preservatives were used f-j% ... NO ... NA
16. Was residual chlorine present? YES.4W .. NA
I certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (intial) Am:± -
11, tw t 1
17. Were custody papers properly filled out (ink, signed, etc)? (:59 ... NO ... NA
18. Did you sign the custody papers in the appropriate place? AD ... NO ... NA
C11-1
19. Were correct containers used for the analysis requested? 61 ... NO ... NA
20. Was sufficient amount of sample sent in each container?
... NO ... NA
21. Were there Non -Conformance issues at login? YES_._9 Was a NCM generated? YES..95>#L.-
BIS = Broken in shipment
Cooler Receipt Forni.doc
LF-1
End of Foi in
Revised 8/23/17
Page 65 of 70 11/10/2017

Loc: 490
TH a S.-tAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN COOLER RECEIPT FORM
Cooler Received/Opened On10127/17_0945
Time Samples Removed From Cooler — Time Samples Placed In Storage (2 Hour Window)
1. Tracking # i �� C--') 0 (last 4 digits, FedEx) Courier: _FedEx_
IR Gun ID 31470368_ pH Strip Lot_&0V_"M Chlorine Strip Lot . W
2. Temperature of rep. sample or temp blank when opened: Degrees Celsius
3. If Item #2 temperature is O'C or less, was the representative sample or temp blank frozen? YES NO.A.
4. Were custody seals on outside of cooler?
If yes, how many and where:
5. Were the seals intact, signed, and dated correctly?
6. Were custody papers inside cooler?
rYE) ... N 0 ... NA
OE .. NO ... NA
YES ... ... NA
I certify that I opened the cooler and answered questions 1-6 (intial
7. Were custody seals on containers: YES and Intact YES ... NO�q
Were these signed and dated correctly? YES ... NO(JR
8. Packing mat'l used? 611�elp Plastic bag Peanuts Vermiculite Foam Insert Paper Other None
9. Cooling process: Ice -pack Ice (direct contact) Dry ice Other None
10. Did all containers arrive in good condition (unbroken)? &E­S�). N 0 ... NA
11. Were all container labels complete (#, date, signed, pros., etc)?
12. Did all container labels and tags agree with custody papers?
13a. Were VOA vials received?
b. Was there any observable headspace present in any VOA vial?
0 4" Larger than this.
14. Was there a Trip Blank in this cooler? YES...&..NA
;4'E S_). NO ... NA
15. NO ... NA
AO ... NA
YES�7�.NA
If multiple coolqrs, sequence #,
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level?
b. Did the bottle labels indicate that the correct preservatives were used
16. Was residual chlorine present?
I certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (Intial)
17. Were custody papers properly filled out (ink, signed, etc)?
18. Did you sign the custody papers in the appropriate place?
19. Were correct containers used for the analysis requested?
20. Was sufficient amount of sample sent in each container?
21. Were there Non -Conformance issues at login? YES.0 Was a NCM generated?
6P.- NO.AA
0 .. NO ... NA
YES..(�?. NA
'�MT
V
�9 ... NO ... NA
r�51_ - NO ... NA
19 .. NO ... NA
--Y0 .. NO ... NA
BIS — Broken in sMprnent
Cooler Receipt Forni.doc LF- I
End of Form
Page 66 of 70
Revised 8/23/17
11/10/2017

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Page 68 of 70
11/10/2017

Client: CIDM Smith, Inc.
Login Number: 139553
List Number: 1
Creator: Huskey, Adam
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
True
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
False
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
Job Number: 490-139553-1
List Source: TestAmerica Nashville
Headspace larger than 1/4".
TestAmerica Nashville
Page 69 of 70 11/10/2017

Client: CIDM Smith, Inc.
Login Number: 139553
List Number: 2
Creator: Hulbert, Michael J
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity either was not measured or, if measured, is at or below
True
background
The cooler's custody seal, if present, is intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the sample IlDs on the containers and
True
the COC.
Samples are received within Holding Time (Excluding tests with immediate
True
HTs)..
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
True
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
True
needs
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Sampling Company provided.
True
Samples received within 48 hours of sampling.
True
Samples requiring field filtration have been filtered in the field.
N/A
Chlorine Residual checked.
N/A
4.4 #1
Job Number: 490-139553-1
List Source: TestAmerica Buffalo
List Creation: 10/28/17 01:45 PM
TestAmerica Nashville
Page 70 of 70 11/10/2017

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-139626-1
Client Project/Site: NGC-Murphy NC
For-
CDM Smith, Inc.
9420 Bunsen Parkway
Suite 225
Louisville, Kentucky 40220
Attn: Mr. Phillip Hendershot
R"0_44U� 6"rv:s
Authorized for release by.-
1111312017 3:59:43 PM
Roxanne Cisneros, Senior Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Table of Contents
TestAmerica Job ID: 490-139626-1
Cover Page ..............................................
1
Table of Contents .........................................
2
Sample Summary .........................................
3
Case Narrative ...........................................
4
Definitions ...............................................
6
Client Sample Results ......................................
7
QC Sample Results ........................................
24
QC Association ...........................................
49
Chronicle................................................
56
Method Summary .........................................
60
Certification Summary ......................................
61
Chain of Custody ..........................................
62
Receipt Checklists .........................................
68
TestAmerica Nashville
Page 2 of 69 11/13/2017

Sample Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Lab Sample ID
Client Sample ID
Matrix
Collected
Received
490-139626-1
J 1 155-MW-7-102717
Water
10&/17 -1017
10/28/17 09:55
490-139626-2
J 1 155-MW-8-102717
Water
10/27/17 09:06
10/28/17 09:55
490-139626-3
J 1 155-MW-32-102617
Water
10/26/17 16:05
10/28/17 09:55
490-139626-4
J1 155-PM-4D-102717
Water
10/27/17 13:09
10/28/17 09:55
490-139626-5
J1 155-PM-10-102717
Water
10/27/17 13:07
10/28/17 09:55
490-139626-6
J1 155-DUP-2-102717
Water
10/27/17 14:00
10/28/17 09:55
TestAmerica Nashville
Page 3 of 69 11/13/2017

Case Narrative
Client: CIDM Smith, Inc.
Project/Site: NGC-Murphy NC
Job ID: 490-139626-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-139626-1
Comments
No additional comments.
TestAmerica Job ID: 490-139626-1
Receipt
The samples were received on 10/28/2017 9:55 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 0.10 C, 0.41 C and 1.61 C.
GC/IVIS VOA
Method(s) 8260B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 490-471835 were outside control
limits. Sample matrix interference and/or non -homogeneity are suspected because the associated laboratory control sample (LCS)
recovery was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GUMS Semi VOA
Method(s) 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-471861 and analytical batch 490-472278.
Method(s) 8270D: The continuing calibration verification (CCV) analyzed in batch 490-472278 was outside the method criteria for the
following analyte: 1,4-Dioxane. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to
be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is
considered estimated.
Method(s) 8270D: The continuing calibration verification (CCVIS) analyzed in batch 490-473059 was outside the method criteria for the
following analyte: 1,4-Dioxane. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to
be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
HPLC/IC
Method(s) 300.0: The following samples were diluted due to the nature of the sample matrix: J1 155-PM-4D-102717 (490-139626-4) and
J1155-PM-10-102717(490-139626-5). Elevated reporting limits (RLs) are provided.
Method(s) 300.0: The matrix spike (MS) recoveries for analytical batch 490-471559 were outside control limits. Sample matrix interference
and/or non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.
Method(s) 300.0: The matrix spike (MS) recoveries for analytical batch 490-471673 were outside control limits. Sample matrix interference
and/or non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.
Method(s) 300.0: The following sample(s) was received with less than 2 days remaining on the holding time or less than one shift (8
hours) remaining on a test with a holding time of 48 hours or less. As such, the laboratory had insufficient time remaining to perform the
analysis within holding time: J 1 155-MW-32-102617 (490-139626-3).
Method(s) 300.0: The following sample was analyzed outside of analytical holding time due to sample was original login as 300_28Day
and was loaded based on the test code. Test code 300 — 48Hours was added 10/29/17 at 7:45arn after the samples was loaded and
analysis for 28D. J1 155-MW-32-102617 (490-139626-3).
Method(s) VFA-IC: The following samples was diluted due to odor: J1 155-MW-7-102717 (490-139626-1), J1 155-MW-8-102717
(490-139626-2), J1 155-MW-32-102617 (490-139626-3), J1 155-PM-4D-102717 (490-139626-4) and J1 155-PM-1 0-102717
(490-139626-5). Elevated reporting limits (RL) are provided.
TestAmerica Nashville
Page 4 of 69 11/13/2017

Case Narrative
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Job ID: 490-139626-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA L
Method(s) RSK-1 75: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-474021.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method(s) 200.8: The matrix spike / matrix spike duplicate / sample duplicate (MS/MSD/DUP) precision for preparation batch 490-472038
and 490-472422 and analytical batch 490-472734 was outside control limits. Sample matrix interference and/or non -homogeneity are
suspected because the associated laboratory control sample / laboratory control sample duplicate (LCS/LCSD) and post dilution spike
(PDS) precision was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
Method(s) SM 4500 P E: The initial calibration blank for analytical batch 490-472376 contained Orthophosphate as P above the method
detection limit. This target analyte concentration was less than the reporting limit (RQ; therefore, re -extraction and/or re -analysis of
samples was not performed. F
Method(s) SM 2320B: The following sample had an initial pH below endpoint for total alkalinity analysis: J1 155-PM-10-102717
(490-139626-5).
Method(s) SM 4500 P E: The initial calibration blank and continuing calibration blank for analytical batch 490-473471 contained
Orthophosphate as P above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore,
re -extraction and/or re -analysis of samples was not performed.
Method(s) SM 4500 P E: The following sample was analyzed outside of analytical holding time: J1 155-PM-10-102717 (490-139626-5).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica Nashville
Page 5 of 69 11/13/2017

Definitions/Glossary
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
HPLC/lC
Qualifier Qualifier Description
H Sample was prepped or analyzed beyond the specified holding time
F1 MS and/or MSD Recovery is outside acceptance limits.
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
E Result exceeded calibration range.
Metals
Qualifier Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
i Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
H Sample was prepped or analyzed beyond the specified holding time
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
rl Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 6 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-7-102717 Lab Sample ID: 490-139626-1
Date Collected: 10/27/17 10:17 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/29/17 00:10
1
Benzene
ND
0.500
0.200
ug/L
10/29/17 00:10
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/29/17 00:10
1
Bromoform
ND
0.500
0.290
ug/L
10/29/17 00:10
1
Bromomethane
ND
0.500
0.350
ug/L
10/29/17 00:10
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/29/17 00:10
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/29/17 00:10
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/29/17 00:10
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/29/17 00:10
1
Chloroethane
ND
0.500
0.360
ug/L
10/29/17 00:10
1
Chloroform
ND
0.500
0.230
ug/L
10/29/17 00:10
1
Chloromethane
ND
0.500
0.360
ug/L
10/29/17 00:10
1
cis- 1,2-Dichloroethene
ND
0.500
0.210
ug/L
10/29/17 00:10
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/29/17 00:10
1
Cyclohexane
ND
1.00
0.130
ug/L
10/29/17 00:10
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/29/17 00:10
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/29/17 00:10
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/29/17 00:10
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/29/17 00:10
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/29/17 00:10
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/29/17 00:10
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/29/17 00:10
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/29/17 00:10
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/29/17 00:10
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/29/17 00:10
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/29/17 00:10
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/29/17 00:10
1
2-Hexanone
ND
5.00
1.28
ug/L
10/29/17 00:10
1
I sopropyl benzene
ND
1.00
0.330
ug/L
10/29/17 00:10
1
Methyl acetate
ND
10.0
0.580
ug/L
10/29/17 00:10
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/29/17 00:10
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/29/17 00:10
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/29/17 00:10
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/29/17 00:10
1
Styrene
ND
0.500
0.280
ug/L
10/29/17 00:10
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/29/17 00:10
1
Tetrachloroethene
ND
0.500
0.140
ug/L
10/29/17 00:10
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/29/17 00:10
1
Toluene
ND
0.500
0.170
ug/L
10/29/17 00:10
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/29/17 00:10
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/29/17 00:10
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/29/17 00:10
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/29/17 00:10
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/29/17 00:10
1
Trichloroethene
ND
0.500
0.200
ug/L
10/29/17 00:10
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/29/17 00:10
1
1,1,2-Trichloro-1,2,2-trifluoroetha
0.211 J
1.00
0.150
ug/L
10/29/17 00:10
1
ne
Vinyl chloride
ND
0.500
0.180
ug/L
10/29/17 00:10
1
TestAmerica Nashville
Page 7 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-7-102717 Lab Sample ID: 490-139626-1
Date Collected: 10/27/17 10:17 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared
Xylenes, Total ND 1.50 0.580 ug/L
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene Fsu-rr)
105
70-130
Dibromofluoromethane (Surr)
102
70-130
1,2-Dichloroethane-d4 (Surr)
104
70-130
Toluene-d8 (Surr)
104
70-130
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
1,4-Dioxane
ND
10.0
Surrogate
%Recovery Qualifier
2,4,6-Tribromophenol (Surr)
60
2-Fluorobiphenyl (Surr)
54
2-Fluorophenol (Surr)
49
Nitrobenzene-d5 (Surr)
52
Phenol-d5 (Surr)
39
Terphenyl-d14 (Surr)
80
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
Ethane
ND
Ethylene
ND
Methane
ND
Surrogate
%Recovery Qualifier
Acetylene (Surr)
97
Method: 300.0 - Anions,
Ion Chromatography
Analyte
Result Qualifier
Chloride
4.23
Nitrate as N
2.47
Sulfate
7.41
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
Iron
ND
Method: 200.8 - Metals (ICP/MS) - Dissolved
Prepared
Analyzed Dil Fac
10/29/17 00:10
1
Analyzed
Dil Fac
10129117 00:10
1
10129117 00:10
1
10129117 00:10
10129117 00:10
1
MDL Unit D Prepared Analyzed Dil Fac
6.10 ug/L 10/30/17 09:34 10/31/17 15:41 1
Limits
Prepared
Analyzed
Dil Fac
10-120
10130117 09:34
10131117 15:41
1
29-120
10130117 09:34
10131117 15:41
1
10-120
10130117 09:34
10131117 15:41
1
27-120
10130117 09:34
10131117 15:41
10-120
10130117 09:34
10131117 15:41
1
13-120
10130117 09:34
10131117 15:41
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.00500
0.00270
mg/L
11/07/17 16:47
1
0.00500
0.00220
mg/L
11/07/17 16:47
1
0.00500
0.00170
mg/L
11/07/17 16:47
1
Limits
62-124
Prepared Analyzed Dil Fac
111071171 1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1.00
0.700
mg/L
10/28/17 20:13
1
0.100
0.0500
mg/L
10/28/17 20:13
1
1.00
0.600
mg/L
10/28/17 20:13
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.100
0.0500
mg/L
11/01/1707:32
11/02/1703:42
1
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.00206
J
0.00400
0.00150
mg/L
11/01/17 07:37
11/01/17 16:48
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
ND
0.0500
0.0500
mg/L
11/01/17 11:20
1
Sulfide
ND
5.00
0.700
mg/L
11/03/17 14:00
11/03/17 15:45
1
Total Organic Carbon
ND
1.00
0.500
mg/L
11/08/17 23:08
1
Alkalinity
7.19
J
10.0
5.00
mg/L
11/08/17 23:16
1
Total Dissolved Solids
76.0
10.0
7.00
mg/L
11/01/17 22:04
1
Orthophosphate as P
ND
0.100
0.0500
mg/L
10/28/17 16:11
1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 12:28
5
TestAmerica Nashville
Page 8 of 69 11/13/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
F
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-7-102717 Lab Sample ID: 490-139626-1
Date Collected: 10/27/17 10:17 Matrix: Water
Date Received: 10/28/17 09:55
General Chemistry (Continued)
Analyte
Formic -acid
Lactic acid
n-Butyric Acid
Propionic acid
Pyruvic Acid
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
ND
5.00
1.30
mg/L
11/07/17 12:28
5
ND
5.00
1.55
mg/L
11/07/17 12:28
5
ND
5.00
1.30
mg/L
11/07/17 12:28
5
ND
5.00
1.75
mg/L
11/07/17 12:28
5
ND
7.50
1.85
mg/L
11/07/17 12:28
5
F
F
TestAmerica Nashville
Page 9 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-8-102717 Lab Sample ID: 490-139626-2
Date Collected: 10/27/17 09:06 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/29/17 00:36
1
Benzene
ND
0.500
0.200
ug/L
10/29/17 00:36
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/29/17 00:36
1
Bromoform
ND
0.500
0.290
ug/L
10/29/17 00:36
1
Bromomethane
ND
0.500
0.350
ug/L
10/29/17 00:36
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/29/17 00:36
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/29/17 00:36
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/29/17 00:36
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/29/17 00:36
1
Chloroethane
ND
0.500
0.360
ug/L
10/29/17 00:36
1
Chloroform
ND
0.500
0.230
ug/L
10/29/17 00:36
1
Chloromethane
ND
0.500
0.360
ug/L
10/29/17 00:36
1
cis-1,2-Dichloroethene
0.819
0.500
0.210
ug/L
10/29/17 00:36
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/29/17 00:36
1
Cyclohexane
ND
1.00
0.130
ug/L
10/29/17 00:36
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/29/17 00:36
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/29/17 00:36
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/29/17 00:36
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/29/17 00:36
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/29/17 00:36
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/29/17 00:36
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/29/17 00:36
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/29/17 00:36
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/29/17 00:36
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/29/17 00:36
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/29/17 00:36
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/29/17 00:36
1
2-Hexanone
ND
5.00
1.28
ug/L
10/29/17 00:36
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/29/17 00:36
1
Methyl acetate
ND
10.0
0.580
ug/L
10/29/17 00:36
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/29/17 00:36
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/29/17 00:36
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/29/17 00:36
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/29/17 00:36
1
Styrene
ND
0.500
0.280
ug/L
10/29/17 00:36
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/29/17 00:36
1
Tetrachloroethene
1.48
0.500
0.140
ug/L
10/29/17 00:36
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/29/17 00:36
1
Toluene
ND
0.500
0.170
ug/L
10/29/17 00:36
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/29/17 00:36
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/29/17 00:36
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/29/17 00:36
1
1,1,1-Trichloroethane
0.661
0.500
0.190
ug/L
10/29/17 00:36
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/29/17 00:36
1
Trichloroethene
6.08
0.500
0.200
ug/L
10/29/17 00:36
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/29/17 00:36
1
1,1,2-Trichloro-1,2,2-trifluoroetha
24.8
1.00
0.150
ug/L
10/29/17 00:36
1
ne
Vinyl chloride
ND
0.500
0.180
ug/L
10/29/17 00:36
1
M
TestAmerica Nashville
Page 10 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-8-102717 Lab Sample ID: 490-139626-2
Date Collected: 10/27/17 09:06 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared
Xylenes, Total ND 1.50 0.580 ug/L
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene Fsu-rr)
105
70-130
Dibromofluoromethane (Surr)
103
70-130
1,2-Dichloroethane-d4 (Surr)
104
70-130
Toluene-d8 (Surr)
105
70-130
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
1,4-Dioxane
ND
10.0
Surrogate
%Recovery Qualifier
2,4,6-Tribromophenol (Surr)
72
2-Fluorobiphenyl (Surr)
73
2-Fluorophenol (Surr)
70
Nitrobenzene-d5 (Surr)
72
Phenol-d5 (Surr)
57
Terphenyl-d14 (Surr)
85
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
Ethane
ND
Ethylene
ND
Methane
ND
Surrogate
%Recovery Qualifier
Acetylene (Surr)
96
Method: 300.0 - Anions,
Ion Chromatography
Analyte
Result Qualifier
Chloride
1.31
Nitrate as N
0.981
Sulfate
3.88
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
Iron
ND
Method: 200.8 - Metals (ICP/MS) - Dissolved
Prepared
Analyzed Dil Fac
10/29/17 00:36
1
Analyzed
Dil Fac
10129117 00:36
1
10129117 00:36
1
10129117 00:36
10129117 00:36
1
MDL Unit D Prepared Analyzed Dil Fac
6.10 ug/L 10/30/17 09:34 10/31/17 16:02 1
Limits
Prepared
Analyzed
Dil Fac
10-120
10130117 09:34
10131117 16:02
1
29-120
10130117 09:34
10131117 16:02
1
10-120
10130117 09:34
10131117 16:02
1
27-120
10130117 09:34
10131117 16:02
10-120
10130117 09:34
10131117 16:02
1
13-120
10130117 09:34
10131117 16:02
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.00500
0.00270
mg/L
11/07/17 16:51
1
0.00500
0.00220
mg/L
11/07/17 16:51
1
0.00500
0.00170
mg/L
11/07/17 16:51
1
Limits
62-124
Prepared Analyzed Dil Fac
111071171 1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1.00
0.700
mg/L
10/28/17 20:42
1
0.100
0.0500
mg/L
10/28/17 20:42
1
1.00
0.600
mg/L
10/28/17 20:42
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.100
0.0500
mg/L
11/01/1707:32
11/02/1703:47
1
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.00403
0.00400
0.00150
mg/L
11/01/17 07:37
11/01/17 16:51
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
ND
0.0500
0.0500
mg/L
11/01/17 11:22
1
Sulfide
ND
5.00
0.700
mg/L
11/03/17 14:00
11/03/17 15:45
1
Total Organic Carbon
ND
1.00
0.500
mg/L
11/08/17 23:37
1
Alkalinity
12.2
10.0
5.00
mg/L
11/08/17 23:22
1
Total Dissolved Solids
35.0
10.0
7.00
mg/L
11/01/17 22:04
1
Orthophosphate as P
0.0520 J
0.100
0.0500
mg/L
10/28/17 16:11
1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 12:57
5
TestAmerica Nashville
Page 11 of 69 11/13/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
F
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-8-102717 Lab Sample ID: 490-139626-2
Date Collected: 10/27/17 09:06 Matrix: Water
Date Received: 10/28/17 09:55
General Chemistry (Continued)
Analyte
Formic -acid
Lactic acid
n-Butyric Acid
Propionic acid
Pyruvic Acid
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
ND
5.00
1.30
mg/L
11/07/17 12:57
5
ND
5.00
1.55
mg/L
11/07/17 12:57
5
ND
5.00
1.30
mg/L
11/07/17 12:57
5
ND
5.00
1.75
mg/L
11/07/17 12:57
5
ND
7.50
1.85
mg/L
11/07/17 12:57
5
F
F
TestAmerica Nashville
Page 12 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-32-102617 Lab Sample ID: 490-139626-3
Date Collected: 10/26/17 16:05 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/30/17 01:02
1
Benzene
ND
0.500
0.200
ug/L
10/30/17 01:02
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/30/17 01:02
1
Brornoform
ND
0.500
0.290
ug/L
10/30/17 01:02
1
Brornornethane
ND
0.500
0.350
ug/L
10/30/17 01:02
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/30/17 01:02
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/30/17 01:02
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/30/17 01:02
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/30/17 01:02
1
Chloroethane
ND
0.500
0.360
ug/L
10/30/17 01:02
1
Chloroform
6.16
0.500
0.230
ug/L
10/30/17 01:02
1
Chloromethane
ND
0.500
0.360
ug/L
10/30/17 01:02
1
cis-1,2-Dichloroethene
76.2
0.500
0.210
ug/L
10/30/17 01:02
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/30/17 01:02
1
Cyclohexane
ND
1.00
0.130
ug/L
10/30/17 01:02
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/30/17 01:02
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/30/17 01:02
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/30/17 01:02
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/30/17 01:02
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/30/17 01:02
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/30/17 01:02
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/30/17 01:02
1
11,11-Dichloroethane
26.7
0.500
0.240
ug/L
10/30/17 01:02
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/30/17 01:02
1
1,1-Dichloroethene
90.8
0.500
0.250
ug/L
10/30/17 01:02
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/30/17 01:02
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/30/17 01:02
1
2-Hexanone
ND
5.00
1.28
ug/L
10/30/17 01:02
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/30/17 01:02
1
Methyl acetate
ND
10.0
0.580
ug/L
10/30/17 01:02
1
Methylcyclohexane
0.0941 J
0.500
0.0900
ug/L
10/30/17 01:02
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/30/17 01:02
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/30/17 01:02
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/30/17 01:02
1
Styrene
ND
0.500
0.280
ug/L
10/30/17 01:02
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/30/17 01:02
1
Tetrachloroethene
98.5
0.500
0.140
ug/L
10/30/17 01:02
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/30/17 01:02
1
Toluene
ND
0.500
0.170
ug/L
10/30/17 01:02
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/30/17 01:02
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/30/17 01:02
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/30/17 01:02
1
11,11,11-Trichloroethane
71.6
0.500
0.190
ug/L
10/30/17 01:02
1
1,1,2-Trichloroethane
0.453 J
0.500
0.190
ug/L
10/30/17 01:02
1
Trichloroethene
334
5.00
2.00
ug/L
10/30/17 19:02
10
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/30/17 01:02
1
1,1,2-Trichloro-1,2,2-trifluoroetha
75.5
1.00
0.150
ug/L
10/30/17 01:02
1
ne
Vinyl chloride
0.716
0.500
0.180
ug/L
10/30/17 01:02
1
M
TestAmerica Nashville
Page 13 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Client Sample ID: J1155-MW-32-102617
Lab Sample
ID: 490-139626-3
Date Collected: 10/26/17 16:05
Matrix:
Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Xylenes, Total
ND
1.50
0.580 ug/L
10/30/17 01:02
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene Fsu-rr)
104
70-130
10130117 01:02
1
4-Bromofluorobenzene (Surr)
98
70-130
10130117 19:02
10
Dibromofluoromethane (Surr)
101
70-130
10130117 01:02
Dibromofluoromethane (Surr)
106
70-130
10130117 19:02
10
1,2-Dichloroethane-d4 (Surr)
105
70-130
10130117 01:02
'
1,2-Dichloroethane-d4 (Surr)
104
70-130
10130117 19:02
lo
Toluene-d8 (Surr)
105
70-130
10130117 01:02
1
Toluene-d8 (Surr)
101
70-130
10130117 19:02
10
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
15.9
10.0
6.10 ug/L
10/30/17 09:34
10/31/17 16:44
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
80
10-120
10130117 09:34
10131117 16:44
1
2-Fluorobiphenyl (Surr)
82
29-120
10130117 09:34
10131117 16:44
1
2-Fluorophenol (Surr)
77
10-120
10130117 09:34
10131117 16:44
1
Nitrobenzene-d5 (Surr)
80
27-120
10130117 09:34
10131117 16:44
1
Phenol-d5 (Surr)
63
10-120
10130117 09:34
10131117 16:44
1
Terphenyl-d14 (Surr)
94
13-120
10130117 09:34
10131117 16:44
1
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Ethane
ND
0.00500
0.00270 mg/L
11/07/17 16:54
1
Ethylene
ND
0.00500
0.00220 mg/L
11/07/17 16:54
1
Methane
0.0497
0.00500
0.00170 mg/L
11/07/17 16:54
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Acetylene (Surr)
101
62-124
11107117 16:54
1
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chloride
4.68
1.00
0.700 mg/L
10/28/17 21:11
1
Nitrate as N
0.400 H
0.100
0.0500 mg/L
10/28/17 21:11
1
Sulfate
35.7
1.00
0.600 mg/L
10/28/17 21:11
1
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Iron
ND
0.100
0.0500
mg/L
11/01/1707:32
11/02/1704:03
1
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.0595
0.00400
0.00150
mg/L
11/01/1707:37
11/01/1716:54
1
General Chemistry
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
0.183
0.0500
0.0500
mg/L
11/01/17 11:23
1
Sulfide
ND
5.00
0.700
mg/L
11/01/17 13:00
11/01/17 15:00
1
Total Organic Carbon
0.628
J
1.00
0.500
mg/L
11/09/17 00:05
1
TestAmerica Nashville
Page 14 of 69 11/13/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-MW-32-102617
Lab Sample ID: 490-139626-3
Date Collected: 10/26/17 16:05
Matrix: Water
Date Received: 10/28/17 09:55
General Chemistry (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Alkalinity
191
10.0
5.00
mg/L
11/08/17 23:28 1
Total Dissolved Solids
318
10.0
7.00
mg/L
11/01/17 19:09 1
Orthophosphate as P
0.0880 J H
0.100
0.0500
mg/L
10/28/17 16:11 1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 13:27 5
Formic -acid
ND
5.00
1.30
mg/L
11/07/17 13:27 5
Lactic acid
ND
5.00
1.55
mg/L
11/07/17 13:27 5
n-Butyric Acid
ND
5.00
1.30
mg/L
11/07/17 13:27 5
Propionic acid
ND
5.00
1.75
mg/L
11/07/17 13:27 5
Pyruvic Acid
ND
7.50
1.85
mg/L
11/07/17 13:27 5
TestAmerica Nashville
Page 15 of 69
11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: A 155-PM-4D-1 02717 Lab Sample ID: 490-139626-4
Date Collected: 10/27/17 13:09 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
4.37 J
5.00
2.66
ug/L
10/30/17 01:29
1
Benzene
2.48
0.500
0.200
ug/L
10/30/17 01:29
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/30/17 01:29
1
Bromoform
ND
0.500
0.290
ug/L
10/30/17 01:29
1
Bromomethane
ND
0.500
0.350
ug/L
10/30/17 01:29
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/30/17 01:29
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/30/17 01:29
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/30/17 01:29
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/30/17 01:29
1
Chloroethane
ND
0.500
0.360
ug/L
10/30/17 01:29
1
Chloroform
ND
0.500
0.230
ug/L
10/30/17 01:29
1
Chloromethane
ND
0.500
0.360
ug/L
10/30/17 01:29
1
cis- 1,2-Dichloroethene
ND
0.500
0.210
ug/L
10/30/17 01:29
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/30/17 01:29
1
Cyclohexane
ND
1.00
0.130
ug/L
10/30/17 01:29
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/30/17 01:29
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/30/17 01:29
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/30/17 01:29
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/30/17 01:29
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/30/17 01:29
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/30/17 01:29
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/30/17 01:29
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/30/17 01:29
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/30/17 01:29
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/30/17 01:29
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/30/17 01:29
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/30/17 01:29
1
2-Hexanone
ND
5.00
1.28
ug/L
10/30/17 01:29
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/30/17 01:29
1
Methyl acetate
ND
10.0
0.580
ug/L
10/30/17 01:29
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/30/17 01:29
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/30/17 01:29
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/30/17 01:29
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/30/17 01:29
1
Styrene
ND
0.500
0.280
ug/L
10/30/17 01:29
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/30/17 01:29
1
Tetrachloroethene
ND
0.500
0.140
ug/L
10/30/17 01:29
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/30/17 01:29
1
Toluene
0.285 J
0.500
0.170
ug/L
10/30/17 01:29
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/30/17 01:29
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/30/17 01:29
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/30/17 01:29
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/30/17 01:29
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/30/17 01:29
1
Trichloroethene
1.61
0.500
0.200
ug/L
10/30/17 12:25
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/30/17 01:29
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.150
ug/L
10/30/17 01:29
1
Vinyl chloride
ND
0.500
0.180
ug/L
10/30/17 01:29
1
Xylenes, Total
ND
1.50
0.580
ug/L
10/30/17 01:29
1
M
TestAmerica Nashville
Page 16 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Client Sample ID: A 155-PM-4D-1 02717
Lab Sample
ID: 490-139626-4
Date Collected: 10/27/17 13:09
Matrix:
Water
Date Received: 10/28/17 09:55
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
102
70-130
10130117 01:29
1
4-Bromofluorobenzene (Surr)
101
70-130
10130117 12:25
Dibromofluoromethane (Surr)
103
70-130
10130117 01:29
1
Dibromofluoromethane (Surr)
106
70-130
10130117 12:25
1
1,2-Dichloroethane-d4 (Surr)
107
70-130
10130117 01:29
1
1,2-Dichloroethane-d4 (Surr)
109
70-130
10130117 12:25
Toluene-d8 (Surr)
104
70-130
10130117 01:29
1
Toluene-d8 (Surr)
102
70-130
10130117 12:25
1
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
ND
10.0
6.10 ug/L
10/30/17 09:34
10/31/17 17:04
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
53
10-120
10130117 09:34
10131117 17:04
1
2-Fluorobiphenyl (Surr)
49
29-120
10130117 09:34
10131117 17:04
1
2-Fluorophenol (Surr)
35
10-120
10130117 09:34
10131117 17:04
1
Nitrobenzene-d5 (Surr)
50
27-120
10130117 09:34
10131117 17:04
1
Phenol-d5 (Surr)
32
10-120
10130117 09:34
10131117 17:04
1
Terphenyl-d14 (Surr)
70
13-120
10130117 09:34
10131117 17:04
1
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Ethane
ND
0.00500
0.00270 mg/L
11/07/17 16:57
1
Ethylene
ND
0.00500
0.00220 mg/L
11/07/17 16:57
1
Methane
ND
0.00500
0.00170 mg/L
11/07/17 16:57
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Acetylene (Surr)
102
62-124
11/07/17 16:57
1
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chloride
59.2
10.0
7.00 mg/L
10/28/17 21:56
10
Nitrate as N
4.30
1.00
0.500 mg/L
10/28/17 21:56
10
Sulfate
128
10.0
6.00 mg/L
10/28/17 21:56
10
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Iron
3.71
0.100
0.0500 mg/L
11/01/1707:32
11/02/1704:08
1
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.00411
0.00400
0.00150
mg/L
11/01/17 07:37
11/01/17 16:57
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
0.273
0.0500
0.0500
mg/L
11/01/17 11:24
1
Sulfide
ND
5.00
0.700
mg/L
11/03/17 14:00
11/03/17 15:45
1
Total Organic Carbon
11.8
1.00
0.500
mg/L
11/09/17 00:34
1
Alkalinity
78.0
10.0
5.00
mg/L
11/08/17 23:36
1
Total Dissolved Solids
559
10.0
7.00
mg/L
11/01/17 19:09
1
Orthophosphate as P
0.0640 J
0.100
0.0500
mg/L
10/28/17 16:11
1
TestAmerica Nashville
Page 17 of 69 11/13/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: A 155-PM-4D-1 02717 Lab Sample ID: 490-139626-4
Date Collected: 10/27/17 13:09 Matrix: Water
Date Received: 10/28/17 09:55
General Chemistry (Continued)
Analyte
Acetic acid
Formic -acid
Lactic acid
n-Butyric Acid
Propionic acid
Pyruvic Acid
Result Qualifier
RL
MDL
Unit D
13.1
5.00
1.45
mg/L
ND
5.00
1.30
mg/L
ND
5.00
1.55
mg/L
ND
5.00
1.30
mg/L
ND
5.00
1.75
mg/L
ND
7.50
1.85
mg/L
Prepared
Analyzed
11/07/17 13:56
11/07/17 13:56
11/07/17 13:56
11/07/17 13:56
11/07/17 13:56
11/07/17 13:56
Dil Fac
5
5 E.
5
5
5
5 E
E
TestAmerica Nashville
Page 18 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-PM-10-102717 Lab Sample ID: 490-139626-5
Date Collected: 10/27/17 13:07 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
5.05
5.00
2.66
ug/L
10/30/17 01:55
1
Benzene
2.32
0.500
0.200
ug/L
10/30/17 01:55
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/30/17 01:55
1
Brornoform
ND
0.500
0.290
ug/L
10/30/17 01:55
1
Brornornethane
ND
0.500
0.350
ug/L
10/30/17 01:55
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/30/17 01:55
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/30/17 01:55
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/30/17 01:55
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/30/17 01:55
1
Chloroethane
ND
0.500
0.360
ug/L
10/30/17 01:55
1
Chloroform
0.561
0.500
0.230
ug/L
10/30/17 01:55
1
Chloromethane
ND
0.500
0.360
ug/L
10/30/17 01:55
1
cis-1,2-Dichloroethene
10.2
0.500
0.210
ug/L
10/30/17 01:55
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/30/17 01:55
1
Cyclohexane
ND
1.00
0.130
ug/L
10/30/17 01:55
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/30/17 01:55
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/30/17 01:55
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/30/17 01:55
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/30/17 01:55
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/30/17 01:55
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/30/17 01:55
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/30/17 01:55
1
11,11-Dichloroethane
0.387 J
0.500
0.240
ug/L
10/30/17 01:55
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/30/17 01:55
1
1,1-Dichloroethene
34.2
0.500
0.250
ug/L
10/30/17 01:55
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/30/17 01:55
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/30/17 01:55
1
2-Hexanone
ND
5.00
1.28
ug/L
10/30/17 01:55
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/30/17 01:55
1
Methyl acetate
ND
10.0
0.580
ug/L
10/30/17 01:55
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/30/17 01:55
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/30/17 01:55
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/30/17 01:55
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/30/17 01:55
1
Styrene
ND
0.500
0.280
ug/L
10/30/17 01:55
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/30/17 01:55
1
Tetrachloroethene
7.03
0.500
0.140
ug/L
10/30/17 01:55
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/30/17 01:55
1
Toluene
0.296 J
0.500
0.170
ug/L
10/30/17 01:55
1
trans-1,2-Dichloroethene
0.333 J
0.500
0.230
ug/L
10/30/17 01:55
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/30/17 01:55
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/30/17 01:55
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/30/17 01:55
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/30/17 01:55
1
Trichloroethene
2450
10.0
4.00
ug/L
10/30/17 18:36
20
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/30/17 01:55
1
1,1,2-Trichloro-1,2,2-trifluoroetha
25.4
1.00
0.150
ug/L
10/30/17 01:55
1
ne
Vinyl chloride
ND
0.500
0.180
ug/L
10/30/17 01:55
1
M
TestAmerica Nashville
Page 19 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Client Sample ID: J1155-PM-10-102717
Lab Sample
ID: 490-139626-5
Date Collected: 10/27/17 13:07
Matrix:
Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Xylenes, Total
ND
1.50
0.580 ug/L
10/30/17 01:55
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene Fsu-rr)
106
70-130
10130117 01:55
1
4-Bromofluorobenzene (Surr)
98
70-130
10130117 18:36
20
Dibromofluoromethane (Surr)
102
70-130
10130117 01:55
1
Dibromofluoromethane (Surr)
111
70-130
10130117 18:36
20
1,2-Dichloroethane-d4 (Surr)
104
70-130
10130117 01:55
1
1,2-Dichloroethane-d4 (Surr)
104
70-130
10130117 18:36
20
Toluene-d8 (Surr)
106
70-130
10130117 01:55
1
Toluene-d8 (Surr)
101
70-130
10130117 18:36
20
Method: 8270D - Sernivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
15.9
10.0
6.10 ug/L
11/03/17 09:37
11/03/17 14:16
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
83
10-120
11103117 09:37
11103117 14:16
1
2-Fluorobiphenyl (Surr)
75
29-120
11103117 09:37
11103117 14:16
1
2-Fluorophenol (Surr)
74
10-120
11103117 09:37
11103117 14:16
1
Nitrobenzene-d5 (Surr)
71
27-120
11103117 09:37
11103117 14:16
1
Phenol-d5 (Surr)
65
10-120
11103117 09:37
11103117 14:16
1
Terphenyl-d14 (Surr)
90
13-120
11103117 09:37
11103117 14:16
1
Method: RSK-175 - Dissolved Gases (GC)
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Ethane
ND
0.00500
0.00270 mg/L
11/07/17 17:14
1
Ethylene
ND
0.00500
0.00220 mg/L
11/07/17 17:14
1
Methane
ND
0.00500
0.00170 mg/L
11/07/17 17:14
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Acetylene (Surr)
98
62-124
11107117 17:14
1
Method: 300.0 - Anions, Ion Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chloride
3.91 F1
1.00
0.700 mg/L
10/28/17 22:40
1
Nitrate as N
0.132 F1
0.100
0.0500 mg/L
10/28/17 22:40
1
Sulfate
283
10.0
6.00 mg/L
10/28/17 23:10
10
Method: 200.7 Rev 4.4 - Metals (ICP) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Iron
0.161
0.100
0.0500
mg/L
11/01/1707:32
11/02/1704:13
1
Method: 200.8 - Metals (ICP/MS) - Dissolved
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Manganese
0.0523
0.00400
0.00150
mg/L
11/01/1707:37
11/01/1717:06
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Ammonia (as N)
ND
0.0500
0.0500
mg/L
11/01/17 11:25
1
Sulfide
ND
5.00
0.700
mg/L
11/03/17 14:00
11/03/17 15:45
1
Total Organic Carbon
ND
1.00
0.500
mg/L
11/09/17 02:01
1
TestAmerica Nashville
Page 20 of 69 11/13/2017

Client Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Client Sample ID: J1155-PM-10-102717
Date Collected: 10/27/17 13:07
Date Received: 10/28/17 09:55
TestAmerica Job ID: 490-139626-1
Lab Sample ID: 490-139626-5
Matrix: Water
General Chemistry (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed Dil Fac
Alkalinity
ND
10.0
5.00
mg/L
11/03/17 00:05 1
Total Dissolved Solids
274
10.0
7.00
mg/L
11/01/17 22:04 1
Orthophosphate as P
0.220 H
0.100
0.0500
mg/L
11/03/17 23:04 1
Acetic acid
ND
5.00
1.45
mg/L
11/07/17 14:25 5
Formic -acid
ND
5.00
1.30
mg/L
11/07/17 14:25 5
Lactic acid
ND
5.00
1.55
mg/L
11/07/17 14:25 5
n-Butyric Acid
ND
5.00
1.30
mg/L
11/07/17 14:25 5
Propionic acid
ND
5.00
1.75
mg/L
11/07/17 14:25 5
Pyruvic Acid
ND
7.50
1.85
mg/L
11/07/17 14:25 5
a
TestAmerica Nashville
Page 21 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-DUP-2-102717 Lab Sample ID: 490-139626-6
Date Collected: 10/27/17 14:00 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
5.13
5.00
2.66
ug/L
10/30/17 02:21
1
Benzene
ND
0.500
0.200
ug/L
10/30/17 02:21
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/30/17 02:21
1
Bromoform
ND
0.500
0.290
ug/L
10/30/17 02:21
1
Bromomethane
ND
0.500
0.350
ug/L
10/30/17 02:21
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/30/17 02:21
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/30/17 02:21
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/30/17 02:21
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/30/17 02:21
1
Chloroethane
ND
0.500
0.360
ug/L
10/30/17 02:21
1
Chloroform
ND
0.500
0.230
ug/L
10/30/17 02:21
1
Chloromethane
ND
0.500
0.360
ug/L
10/30/17 02:21
1
cis-1,2-Dichloroethene
0.516
0.500
0.210
ug/L
10/30/17 02:21
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/30/17 02:21
1
Cyclohexane
ND
1.00
0.130
ug/L
10/30/17 02:21
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/30/17 02:21
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/30/17 02:21
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/30/17 02:21
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/30/17 02:21
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/30/17 02:21
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/30/17 02:21
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/30/17 02:21
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/30/17 02:21
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/30/17 02:21
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/30/17 02:21
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/30/17 02:21
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/30/17 02:21
1
2-Hexanone
ND
5.00
1.28
ug/L
10/30/17 02:21
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/30/17 02:21
1
Methyl acetate
ND
10.0
0.580
ug/L
10/30/17 02:21
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/30/17 02:21
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/30/17 02:21
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/30/17 02:21
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/30/17 02:21
1
Styrene
ND
0.500
0.280
ug/L
10/30/17 02:21
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/30/17 02:21
1
Tetrachloroethene
1.37
0.500
0.140
ug/L
10/30/17 02:21
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/30/17 02:21
1
Toluene
ND
0.500
0.170
ug/L
10/30/17 02:21
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/30/17 02:21
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/30/17 02:21
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/30/17 02:21
1
11,11,11-Trichloroethane
0.450 J
0.500
0.190
ug/L
10/30/17 02:21
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/30/17 02:21
1
Trichloroethene
3.64
0.500
0.200
ug/L
10/30/17 12:52
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/30/17 02:21
1
1,1,2-Trichloro-1,2,2-trifluoroetha
17.4
1.00
0.150
ug/L
10/30/17 02:21
1
ne
Vinyl chloride
ND
0.500
0.180
ug/L
10/30/17 02:21
1
M
TestAmerica Nashville
Page 22 of 69 11/13/2017

Client Sample Results
Client: CDM Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: J1155-DUP-2-102717 Lab Sample ID: 490-139626-6
Date Collected: 10/27/17 14:00 Matrix: Water
Date Received: 10/28/17 09:55
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte Result Qualifier RL MDL Unit D Prepared
Xylenes, Total ND 1.50 0.580 ug/L
Surrogate
%Recovery Qualifier
4-Bromofluorobenzene FSu-rr)
104
4-Bromofluorobenzene (Surr)
101
Dibromofluoromethane (Surr)
102
Dibromofluoromethane (Surr)
107
1,2-Dichloroethane-d4 (Surr)
103
1,2-Dichloroethane-d4 (Surr)
108
Toluene-d8 (Surr)
105
Toluene-d8 (Surr)
102
Limits
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
Prepared
Analyzed Dil Fac
10/30/17 02:21
1
Analyzed
Dil Fac
10130117 02:21
1
10130117 12:52
1
10130117 02:21
10130117 12:52
1
10130117 02:21
10130117 12:52
1
10130117 02:21
1
10130117 12:52
1
Page 23 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 8260B - Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 490-471777/7
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471777
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
TO-/29/1721-08
1
Benzene
ND
0.500
0.200
ug/L
10/29/17 21:08
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/29/17 21:08
1
Bromoform
ND
0.500
0.290
ug/L
10/29/17 21:08
Bromomethane
ND
0.500
0.350
ug/L
10/29/17 21:08
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/29/17 21:08
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/29/17 21:08
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/29/17 21:08
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/29/17 21:08
1
Chloroethane
ND
0.500
0.360
ug/L
10/29/17 21:08
1
Chloroform
ND
0.500
0.230
ug/L
10/29/17 21:08
1
Chloromethane
ND
0.500
0.360
ug/L
10/29/17 21:08
1
cis- 1,2-Dichloroethene
ND
0.500
0.210
ug/L
10/29/17 21:08
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/29/17 21:08
1
Cyclohexane
ND
1.00
0.130
ug/L
10/29/17 21:08
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/29/17 21:08
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/29/17 21:08
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/29/17 21:08
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/29/17 21:08
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/29/17 21:08
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/29/17 21:08
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/29/17 21:08
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/29/17 21:08
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/29/17 21:08
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/29/17 21:08
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/29/17 21:08
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/29/17 21:08
1
2-Hexanone
ND
5.00
1.28
ug/L
10/29/17 21:08
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/29/17 21:08
1
Methyl acetate
ND
10.0
0.580
ug/L
10/29/17 21:08
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/29/17 21:08
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/29/17 21:08
1
4-Methyl-2-pentanone (MlBK)
ND
5.00
0.810
ug/L
10/29/17 21:08
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/29/17 21:08
1
Styrene
ND
0.500
0.280
ug/L
10/29/17 21:08
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/29/17 21:08
1
Tetrachloroethene
ND
0.500
0.140
ug/L
10/29/17 21:08
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/29/17 21:08
1
Toluene
ND
0.500
0.170
ug/L
10/29/17 21:08
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/29/17 21:08
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/29/17 21:08
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/29/17 21:08
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/29/17 21:08
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/29/17 21:08
1
Trichloroethene
ND
0.500
0.200
ug/L
10/29/17 21:08
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/29/17 21:08
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.150
ug/L
10/29/17 21:08
1
Vinyl chloride
ND
0.500
0.180
ug/L
10/29/17 21:08
1
TestAmerica Nashville
Page 24 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 490-47177717
Matrix: Water
Analysis Batch: 471777
MB MB
Analyte Result Qualifier RL MDL Unit
Xylenes, Total ND 1.50 0.580 ug/L
MB MB
F
TestAmerica Job ID: 490-139626-1
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
10/29/17 21:08 1
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed
4-Bromofluorobenzene (Surr)
104
70-130
10129117 21:08
Dibromofluoromethane (Surr)
102
70-130
10129117 21:08
1,2-Dichloroethane-d4 (Surr)
104
70-130
10129117 21:08
Toluene-d8 (Surr)
104
70-130
10129117 21:08
Lab Sample ID: LCS 490-471777/3
Matrix: Water
Analysis Batch: 471777
Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
I sopropyl benzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MlBK)
Methyl tert-butyl ether
Styrene
Dil Fac 9
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
250
214.1
ug/L
86
39-150
50.0
47.90
ug/L
96
70-130
50.0
48.03
ug/L
96
70-130
50.0
52.25
ug/L
105
70-137
50.0
56.53
ug/L
113
53-150
250
222.0
ug/L
89
55-143
50.0
45.97
ug/L
92
64-135
50.0
52.94
ug/L
106
70-147
50.0
53.38
ug/L
107
70-130
50.0
42.41
ug/L
85
60-138
50.0
47.44
ug/L
95
70-130
50.0
40.01
ug/L
80
33-150
50.0
49.69
ug/L
99
70-130
50.0
47.13
ug/L
94
70-133
50.0
46.49
ug/L
93
70-134
50.0
50.91
ug/L
102
70-133
50.0
49.93
ug/L
100
45-138
50.0
49.70
ug/L
99
70-130
50.0
53.83
ug/L
108
70-130
50.0
52.81
ug/L
106
70-130
50.0
53.74
ug/L
107
70-130
50.0
47.13
ug/L
94
48-150
50.0
43.37
ug/L
87
70-130
50.0
41.36
ug/L
83
70-130
50.0
47.16
ug/L
94
70-132
50.0
44.36
ug/L
89
70-130
50.0
51.69
ug/L
103
70-130
250
209.9
ug/L
84
54-142
50.0
54.58
ug/L
109
70-131
100
69.34
ug/L
69
56-136
50.0
52.82
ug/L
106
70-132
50.0
46.37
ug/L
93
70-130
250
211.7
ug/L
85
60-137
50.0
36.73
ug/L
73
70-130
50.0
55.63
ug/L
ill
70-130
TestAmerica Nashville
Page 25 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-471777/3
Matrix: Water
Analysis Batch: 471777
TestAmerica Job ID: 490-139626-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
1,1,2,2-Tetrachloroethane
50.0
44.77
ug/L
90
69-131
Tetrachloroethene
50.0
56.56
ug/L
113
70-130
Tetrahydrofuran
100
65.21
ug/L
65
51-136
Toluene
50.0
50.96
ug/L
102
70-130
trans- 1,2-Dich loroethene
50.0
40.91
ug/L
82
70-130
trans- 1, 3-Dich loropropene
50.0
48.38
ug/L
97
63-142
1,2,4-Trichlorobenzene
50.0
51.57
ug/L
103
58-147
1,1,1-Trichloroethane
50.0
50.35
ug/L
101
70-135
1,1,2-Trichloroethane
50.0
49.15
ug/L
98
70-130
Trichloroethene
50.0
52.33
ug/L
105
70-130
Trichlorofluoromethane
50.0
41.61
ug/L
83
59-150
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
48.10
ug/L
96
69-145
ne
Vinyl chloride
50.0
43.20
ug/L
86
57-137
Xylenes, Total
100
111.5
ug/L
111
70-132
LCS LCS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
91
70-130
Dibromofluoromethane (Surr)
92
70-130
1,2-Dichloroethane-d4 (Surr)
103
70-130
Toluene-d8 (Surr)
100
70-130
Lab Sample ID: LCSID 490-471777/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471777
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
Acetone
250
221.7
ug/L
89
39-150
3
23
Benzene
50.0
47.49
ug/L
95
70-130
1
12
Bromodichloromethane
50.0
47.63
ug/L
95
70-130
1
14
Bromoform
50.0
52.10
ug/L
104
70-137
0
14
Bromomethane
50.0
55.84
ug/L
112
53-150
1
19
2-Butanone (MEK)
250
221.5
ug/L
89
55-143
0
19
Carbon disulfide
50.0
43.99
ug/L
88
64-135
4
16
Carbon tetrachloride
50.0
52.11
ug/L
104
70-147
2
16
Chlorobenzene
50.0
52.08
ug/L
104
70-130
2
12
Chloroethane
50.0
41.91
ug/L
84
60-138
1
15
Chloroform
50.0
47.34
ug/L
95
70-130
0
14
Chloromethane
50.0
36.63
ug/L
73
33-150
9
20
cis- 1,2-Dichloroethene
50.0
49.25
ug/L
99
70-130
1
15
cis- 1,3-Dichloropropene
50.0
46.29
ug/L
93
70-133
2
15
Cyclohexane
50.0
46.74
ug/L
93
70-134
1
16
Dibromochloromethane
50.0
50.08
ug/L
100
70-133
2
13
1,2-Dibromo-3-Chloropropane
50.0
49.44
ug/L
99
45-138
1
19
1,2-Dibromoethane (EDB)
50.0
48.68
ug/L
97
70-130
2
13
1,2-Dichlorobenzene
50.0
53.16
ug/L
106
70-130
1
12
1,3-Dichlorobenzene
50.0
52.49
ug/L
105
70-130
1
13
1,4-Dichlorobenzene
50.0
53.38
ug/L
107
70-130
1
12
TestAmerica Nashville
Page 26 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSID 490-471777/4
Matrix: Water
Analysis Batch: 471777
TestAmerica Job ID: 490-139626-1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec.
RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Dichlorodifluoromethane
50.0
46.83
ug/L
94
48-150
1
16
1,1-Dichloroethane
50.0
43.40
ug/L
87
70-130
0
17
1,2-Dichloroethane
50.0
40.29
ug/L
81
70-130
3
13
1,1-Dichloroethene
50.0
47.18
ug/L
94
70-132
0
20
1,2-Dichloropropane
50.0
43.59
ug/L
87
70-130
2
15
Ethylbenzene
50.0
51.04
ug/L
102
70-130
1
12
2-Hexanone
250
209.2
ug/L
84
54-142
0
17
1 sopropyl benzene
50.0
53.67
ug/L
107
70-131
2
13
Methyl acetate
100
71.39
ug/L
71
56-136
3
18
Methylcyclohexane
50.0
52.72
ug/L
105
70-132
0
17
Methylene Chloride
50.0
46.72
ug/L
93
70-130
1
15
4-Methyl-2-pentanone (MIBK)
250
207.0
ug/L
83
60-137
2
21
Methyl tert-butyl ether
50.0
35.76
ug/L
72
70-130
3
16
Styrene
50.0
55.30
ug/L
111
70-130
1
12
1,1,2,2-Tetrachloroethane
50.0
44.17
ug/L
88
69-131
1
15
Tetrachloroethene
50.0
55.99
ug/L
112
70-130
1
17
Tetrahydrofuran
100
70.74
ug/L
71
51-136
8
20
Toluene
50.0
50.52
ug/L
101
70-130
1
13
trans- 1,2-Dich loroethene
50.0
40.50
ug/L
81
70-130
1
15
trans- 1, 3-Dich loropropene
50.0
47.16
ug/L
94
63-142
3
13
1,2,4-Trichlorobenzene
50.0
51.07
ug/L
102
58-147
1
15
1,1,1-Trichloroethane
50.0
49.69
ug/L
99
70-135
1
15
1,1,2-Trichloroethane
50.0
48.44
ug/L
97
70-130
1
13
Trichloroethene
50.0
52.10
ug/L
104
70-130
0
14
Trichlorofluoromethane
50.0
41.50
ug/L
83
59-150
0
22
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
42.62
ug/L
85
69-145
12
16
ne
Vinyl chloride
50.0
43.56
ug/L
87
57-137
1
15
Xylenes, Total
100
110.2
ug/L
110
70-132
1
11
LCSD LCSD
Surrogate
%Recovety Qualifier
Limits
4-Bromofluorobenzene (Surr)
89
70-130
Dibromofluoromethane (Surr)
91
70-130
1,2-Dichloroethane-d4 (Surr)
83
70-130
Toluene-d8 (Surr)
100
70-130
Lab Sample ID: 490-139598-D-3 MS
Matrix: Water
Analysis Batch: 471777
Sample Sample
Spike
MS MS
Analyte
Result Qualifier
Added
Result Qualifier
Acetone
ND
250
202.3
Benzene
ND
50.0
45.38
Bromodichloromethane
ND
50.0
44.67
Brornoform
ND
50.0
51.67
Brornornethane
ND
50.0
43.86
2-Butanone (MEK)
ND
250
219.7
Carbon disulfide
ND
50.0
39.57
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Unit
D %Rec
%Rec.
Limits
dg/L
81
39-150
ug/L
91
55-147
ug/L
89
70-140
ug/L
103
53-150
ug/L
88
30-150
ug/L
88
50-143
ug/L
79
35-150
TestAmerica Nashville
Page 27 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139598-D-3 MS
Matrix: Water
Analysis Batch: 471777
Analyte
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
Isopropylbenzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dich loroethene
trans- 1, 3-Dich loropropene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Sample
Sample
Spike
MS MS
%Rec.
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
ND
50.0
50.35
ug/L
101
56-150
ND
50.0
49.93
ug/L
100
70-130
ND
50.0
35.18
ug/L
70
58-141
ND
50.0
44.11
ug/L
88
66-138
ND
50.0
26.84
ug/L
54
10-150
ND
50.0
47.31
ug/L
95
68-131
ND
50.0
44.23
ug/L
88
70-133
0.257
J
50.0
44.10
ug/L
88
48-150
ND
50.0
48.95
ug/L
98
66-140
ND
50.0
50.09
ug/L
100
38-138
ND
50.0
48.42
ug/L
97
65-137
ND
50.0
46.81
ug/L
94
70-130
ND
50.0
47.43
ug/L
95
68-131
ND
50.0
47.70
ug/L
95
70-130
ND
50.0
25.37
ug/L
51
10-150
ND
50.0
38.46
ug/L
77
61-139
ND
50.0
38.00
ug/L
76
64-136
ND
50.0
41.49
ug/L
83
54-150
ND
50.0
41.82
ug/L
84
67-130
0.548
50.0
48.27
ug/L
95
65-139
ND
250
210.5
ug/L
84
44-150
ND
50.0
49.68
ug/L
99
70-137
ND
100
66.44
ug/L
66
42-136
0.151
J
50.0
50.15
ug/L
100
59-150
ND
50.0
41.64
ug/L
83
64-130
ND
250
211.2
ug/L
84
50-140
ND
50.0
35.03
ug/L
70
55-141
ND
50.0
51.09
ug/L
102
70-130
ND
50.0
42.59
ug/L
85
56-145
ND
50.0
55.18
ug/L
110
57-138
ND
100
64.31
ug/L
64
40-136
ND
50.0
47.71
ug/L
95
64-136
ND
50.0
36.01
ug/L
72
59-143
ND
50.0
44.92
ug/L
90
63-142
ND
50.0
45.78
ug/L
92
47-147
ND
50.0
46.01
ug/L
92
68-144
ND
50.0
48.26
ug/L
97
70-130
ND
50.0
51.50
ug/L
103
63-135
ND
50.0
35.25
ug/L
71
44-150
ND
50.0
43.10
ug/L
86
63-150
ND
50.0
35.34
ug/L
71
57-150
ND
100
103.1
ug/L
103
69-132
MS MS
%Recovery Qualifier
88
92
98
Limits
70-130
70-130
70-130
Page 28 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139598-D-3 MS Client Sample ID: Matrix Spike
Matrix: Water Prep Type: Total/NA
Analysis Batch: 471777
MS MS
Surrogate %Recovery Qualifier Limits
Toluene-d8 (Surr) 100 70-130
Lab Sample ID: 490-139598-D-3 MSD Client Sample ID: Matrix Spike Duplicate
Matrix: Water Prep Type: Total/NA
Analysis Batch: 471777
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Acetone
ND
250
187.4
ug/L
75
39-150
8
28
Benzene
ND
50.0
45.58
ug/L
91
55-147
0
22
Bromodichloromethane
ND
50.0
44.71
ug/L
89
70-140
0
196
Bromoform
ND
50.0
48.41
ug/L
97
53-150
7
20
Bromomethane
ND
50.0
45.72
ug/L
91
30-150
4
44
2-Butanone (MEK)
ND
250
204.7
ug/L
82
50-143
7
28
Carbon disulfide
ND
50.0
39.58
ug/L
79
35-150
0
34
Carbon tetrachloride
ND
50.0
50.68
ug/L
101
56-150
1
18
Chlorobenzene
ND
50.0
49.49
ug/L
99
70-130
1
15
Chloroethane
ND
50.0
36.52
ug/L
73
58-141
4
31
Chloroform
ND
50.0
44.34
ug/L
89
66-138
1
21
Chloromethane
ND
50.0
27.11
ug/L
54
10-150
1
43
cis- 1,2-Dichloroethene
ND
50.0
47.76
ug/L
96
68-131
1
21
cis- 1,3-Dichloropropene
ND
50.0
42.94
ug/L
86
70-133
3
19
Cyclohexane
0.257 J
50.0
44.84
ug/L
89
48-150
2
22
Dibromochloromethane
ND
50.0
47.16
ug/L
94
66-140
4
19
1,2-Dibromo-3-Chloropropane
ND
50.0
46.48
ug/L
93
38-138
7
26
1,2-Dibromoethane (EDB)
ND
50.0
45.77
ug/L
92
65-137
6
21
1,2-Dichlorobenzene
ND
50.0
47.29
ug/L
95
70-130
1
15
1,3-Dichlorobenzene
ND
50.0
48.27
ug/L
97
68-131
2
14
1,4-Dichlorobenzene
ND
50.0
48.40
ug/L
97
70-130
1
14
Dichlorodifluoromethane
ND
50.0
25.76
ug/L
52
10-150
2
50
1,1-Dichloroethane
ND
50.0
40.74
ug/L
81
61-139
6
23
1,2-Dichloroethane
ND
50.0
37.21
ug/L
74
64-136
2
22
1,1-Dichloroethene
ND
50.0
42.98
ug/L
86
54-150
4
24
1,2-Dichloropropane
ND
50.0
41.45
ug/L
83
67-130
1
19
Ethylbenzene
0.548
50.0
48.41
ug/L
96
65-139
0
18
2-Hexanone
ND
250
193.9
ug/L
78
44-150
8
21
1 sopropyl benzene
ND
50.0
50.27
ug/L
101
70-137
1
17
Methyl acetate
ND
100
67.71
ug/L
68
42-136
2
26
M ethyl cyclohexa ne
0.151 J
50.0
50.42
ug/L
101
59-150
1
20
Methylene Chloride
ND
50.0
41.25
ug/L
83
64-130
1
22
4-Methyl-2-pentanone (MIBK)
ND
250
196.8
ug/L
79
50-140
7
24
Methyl tert-butyl ether
ND
50.0
33.12
ug/L
66
55-141
6
24
Styrene
ND
50.0
51.09
ug/L
102
70-130
0
16
1,1,2,2-Tetrachloroethane
ND
50.0
41.82
ug/L
84
56-145
2
19
Tetrachloroethene
ND
50.0
55.11
ug/L
110
57-138
0
17
Tetrahydrofuran
ND
100
50.02
ug/L
50
40-136
25
27
Toluene
ND
50.0
47.85
ug/L
96
64-136
0
18
trans- 1,2-Dich loroethene
ND
50.0
37.36
ug/L
75
59-143
4
25
trans- 1, 3-Dich loropropene
ND
50.0
43.57
ug/L
87
63-142
3
18
TestAmerica Nashville
Page 29 of 69 11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc. TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139598-D-3 MSID
Matrix: Water
Analysis Batch: 471777
Analyte
1, 2,4-Trich lorobe nzene
1, 1, 1 -Trichloroethane
1, 1,2-Trich loroethane
Trichloroethene
Trichlorofluoromethane
1, 1,2-Trich loro-1,2,2-trifluoroetha
ne
Vinyl chloride
Xylenes, Total
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Sample Sample
Result Qualifier
Spike
Added
MSD MSD
Result Qualifier
Unit
D %Rec
%Rec.
Limits
RPD
ND
50.0
44.51
ug/L
89
47-147
3
ND
50.0
46.86
ug/L
94
68-144
2
ND
50.0
45.88
ug/L
92
70-130
5
ND
50.0
51.64
ug/L
103
63-135
0
ND
50.0
36.09
ug/L
72
44-150
2
ND
50.0
43.07
ug/L
86
63-150
0
ND
ND
MSD MSD
Surrogate %Recovery Qualifier
4-Bromofluorobenzene (Surr) 90
Dibromofluoromethane (Surr) 91
1,2-Dichloroethane-d4 (Surr) 78
Toluene-d8 (Surr) 99
Lab Sample ID: MB 490-471835/7
Matrix: Water
Analysis Batch: 471835
50.0 36.54 ug/L
100 103.3 ug/L
Limits
70-130
70-130
70-130
70-130
73 57-150 3
103 69-132 0
RPD
Limit
24
17
18
17
32
22
37
17
Client Sample ID: Method Blank
Prep Type: Total/NA
Analyte
MlB MB
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
5.00
2.66
ug/L
10/30/17 11:06
1
Benzene
ND
0.500
0.200
ug/L
10/30/17 11:06
1
Bromodichloromethane
ND
0.500
0.170
ug/L
10/30/17 11:06
1
Bromoform
ND
0.500
0.290
ug/L
10/30/17 11:06
1
Bromomethane
ND
0.500
0.350
ug/L
10/30/17 11:06
1
2-Butanone (MEK)
ND
50.0
2.64
ug/L
10/30/17 11:06
1
Carbon disulfide
ND
0.500
0.220
ug/L
10/30/17 11:06
1
Carbon tetrachloride
ND
0.500
0.180
ug/L
10/30/17 11:06
1
Chlorobenzene
ND
0.500
0.180
ug/L
10/30/17 11:06
1
Chloroethane
ND
0.500
0.360
ug/L
10/30/17 11:06
1
Chloroform
ND
0.500
0.230
ug/L
10/30/17 11:06
1
Chloromethane
ND
0.500
0.360
ug/L
10/30/17 11:06
1
cis- 1,2-Dichloroethene
ND
0.500
0.210
ug/L
10/30/17 11:06
1
cis- 1,3-Dichloropropene
ND
0.500
0.170
ug/L
10/30/17 11:06
1
Cyclohexane
ND
1.00
0.130
ug/L
10/30/17 11:06
1
Dibromochloromethane
ND
0.500
0.250
ug/L
10/30/17 11:06
1
1,2-Dibromo-3-Chloropropane
ND
5.00
0.940
ug/L
10/30/17 11:06
1
1,2-Dibromoethane (EDB)
ND
0.500
0.210
ug/L
10/30/17 11:06
1
1,2-Dichlorobenzene
ND
0.500
0.190
ug/L
10/30/17 11:06
1
1,3-Dichlorobenzene
ND
0.500
0.180
ug/L
10/30/17 11:06
1
1,4-Dichlorobenzene
ND
0.500
0.170
ug/L
10/30/17 11:06
1
Dichlorodifluoromethane
ND
0.500
0.170
ug/L
10/30/17 11:06
1
1,1-Dichloroethane
ND
0.500
0.240
ug/L
10/30/17 11:06
1
1,2-Dichloroethane
ND
0.500
0.200
ug/L
10/30/17 11:06
1
1,1-Dichloroethene
ND
0.500
0.250
ug/L
10/30/17 11:06
1
1,2-Dichloropropane
ND
0.500
0.250
ug/L
10/30/17 11:06
1
Ethylbenzene
ND
0.500
0.190
ug/L
10/30/17 11:06
1
Page 30 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 490-47183517
Matrix: Water
Analysis Batch: 471835
MB MB
Analyte Result Qualifier RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
2-Hexanone
ND
5.00
1.28
ug/L
10/30/17 11:06
1
1 sopropyl benzene
ND
1.00
0.330
ug/L
10/30/17 11:06
1
Methyl acetate
ND
10.0
0.580
ug/L
10/30/17 11:06
1
Methylcyclohexane
ND
0.500
0.0900
ug/L
10/30/17 11:06
1
Methylene Chloride
ND
5.00
1.00
ug/L
10/30/17 11:06
1
4-Methyl-2-pentanone (MIBK)
ND
5.00
0.810
ug/L
10/30/17 11:06
1
Methyl tert-butyl ether
ND
0.500
0.170
ug/L
10/30/17 11:06
1
Styrene
ND
0.500
0.280
ug/L
10/30/17 11:06
1
1,1,2,2-Tetrachloroethane
ND
0.500
0.190
ug/L
10/30/17 11:06
1
Tetrachloroethene
ND
0.500
0.140
ug/L
10/30/17 11:06
1
Tetrahydrofuran
ND
5.00
0.820
ug/L
10/30/17 11:06
1
Toluene
ND
0.500
0.170
ug/L
10/30/17 11:06
1
trans- 1,2-Dich loroethene
ND
0.500
0.230
ug/L
10/30/17 11:06
1
trans- 1, 3-Dich loropropene
ND
0.500
0.170
ug/L
10/30/17 11:06
1
1,2,4-Trichlorobenzene
ND
0.500
0.200
ug/L
10/30/17 11:06
1
1,1,1-Trichloroethane
ND
0.500
0.190
ug/L
10/30/17 11:06
1
1,1,2-Trichloroethane
ND
0.500
0.190
ug/L
10/30/17 11:06
1
Trichloroethene
ND
0.500
0.200
ug/L
10/30/17 11:06
1
Trichlorofluoromethane
ND
0.500
0.210
ug/L
10/30/17 11:06
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.150
ug/L
10/30/17 11:06
1
Vinyl chloride
ND
0.500
0.180
ug/L
10/30/17 11:06
1
Xylenes, Total
ND
1.50
0.580
ug/L
10/30/17 11:06
1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene (Surr)
102
70-130
10130117 11:06
1
Dibromofluoromethane (Surr)
109
70-130
10130117 11:06
1
1,2-Dichloroethane-d4 (Surr)
103
70-130
10130117 11:06
1
Toluene-d8 (Surr)
103
70-130
10130117 11:06
1
Lab Sample ID: LCS 490-471835/3
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471835
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
250
220.7
ug A
-88
-3-9-- 15-0
Benzene
50.0
47.82
ug/L
96
70-130
Bromodichloromethane
50.0
48.43
ug/L
97
70-130
Bromoform
50.0
54.26
ug/L
109
70-137
Bromomethane
50.0
56.47
ug/L
113
53-150
2-Butanone (MEK)
250
227.9
ug/L
91
55-143
Carbon disulfide
50.0
45.62
ug/L
91
64-135
Carbon tetrachloride
50.0
53.42
ug/L
107
70-147
Chlorobenzene
50.0
52.76
ug/L
106
70-130
Chloroethane
50.0
42.36
ug/L
85
60-138
Chloroform
50.0
47.71
ug/L
95
70-130
Chloromethane
50.0
37.22
ug/L
74
33-150
cis- 1,2-Dichloroethene
50.0
49.49
ug/L
99
70-130
cis- 1,3-Dichloropropene
50.0
48.13
ug/L
96
70-133
TestAmerica Nashville
Page 31 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-471835/3
Matrix: Water
Analysis Batch: 471835
TestAmerica Job ID: 490-139626-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Cyclohexane
50.0
47.94
ug/L
96
70-134
Dibromochloromethane
50.0
51.53
ug/L
103
70-133
1,2-Dibromo-3-Chloropropane
50.0
52.24
ug/L
104
45-138
1,2-Dibromoethane (EDB)
50.0
50.72
ug/L
101
70-130
1,2-Dichlorobenzene
50.0
52.84
ug/L
106
70-130
1,3-Dichlorobenzene
50.0
52.64
ug/L
105
70-130
1,4-Dichlorobenzene
50.0
53.60
ug/L
107
70-130
Dichlorodifluoromethane
50.0
48.32
ug/L
97
48-150
1,1-Dichloroethane
50.0
42.61
ug/L
85
70-130
1,2-Dichloroethane
50.0
41.31
ug/L
83
70-130
1,1-Dichloroethene
50.0
47.32
ug/L
95
70-132
1,2-Dichloropropane
50.0
44.15
ug/L
88
70-130
Ethylbenzene
50.0
51.40
ug/L
103
70-130
2-Hexanone
250
219.2
ug/L
88
54-142
1 sopropyl benzene
50.0
54.03
ug/L
108
70-131
Methyl acetate
100
71.86
ug/L
72
56-136
Methylcyclohexane
50.0
56.12
ug/L
112
70-132
Methylene Chloride
50.0
47.05
ug/L
94
70-130
4-Methyl-2-pentanone (MIBK)
250
219.3
ug/L
88
60-137
Methyl tert-butyl ether
50.0
37.69
ug/L
75
70-130
Styrene
50.0
55.66
ug/L
ill
70-130
1,1,2,2-Tetrachloroethane
50.0
44.88
ug/L
90
69-131
Tetrachloroethene
50.0
57.39
ug/L
115
70-130
Tetrahydrofuran
100
67.04
ug/L
67
51-136
Toluene
50.0
50.68
ug/L
101
70-130
trans- 1,2-Dich loroethene
50.0
40.40
ug/L
81
70-130
trans- 1, 3-Dich loropropene
50.0
49.09
ug/L
98
63-142
1,2,4-Trichlorobenzene
50.0
52.48
ug/L
105
58-147
1,1,1-Trichloroethane
50.0
50.08
ug/L
100
70-135
1,1,2-Trichloroethane
50.0
50.23
ug/L
100
70-130
Trichloroethene
50.0
52.83
ug/L
106
70-130
Trichlorofluoromethane
50.0
40.01
ug/L
80
59-150
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
46.85
ug/L
94
69-145
ne
Vinyl chloride
50.0
43.63
ug/L
87
57-137
Xylenes, Total
100
111.0
ug/L
111
70-132
LCS LCS
Surrogate
%Recovery Qualifier
Limits
4-Bromofluorobenzene (Surr)
88
70-130
Dibromofluoromethane (Surr)
92
70-130
1,2-Dichloroethane-d4 (Surr)
102
70-130
Toluene-d8 (Surr)
101
70-130
TestAmerica Nashville
Page 32 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-47183514 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 471835
Analyte
Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis- 1,2-Dichloroethene
cis- 1,3-Dichloropropene
Cyclohexane
Dibromochloromethane
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
Ethylbenzene
2-Hexanone
I sopropyl benzene
Methyl acetate
Methylcyclohexane
Methylene Chloride
4-Methyl-2-pentanone (MlBK)
Methyl tert-butyl ether
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
trans- 1,2-Dich loroethene
trans- 1, 3-Dich loropropene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
Spike
LCSD LCSD
Added
Result Qualifier
250
222 5
50.0
47.19
50.0
48.27
50.0
54.31
50.0
55.53
250
228.0
50.0
43.30
50.0
53.13
50.0
52.73
50.0
42.10
50.0
47.52
50.0
36.12
50.0
50.15
50.0
46.49
50.0
47.38
50.0
51.90
50.0
51.90
50.0
50.63
50.0
52.66
50.0
52.43
50.0
52.51
50.0
48.08
50.0
42.17
50.0
41.44
50.0
46.44
50.0
44.16
50.0
50.68
250
221.4
50.0
53.26
100
70.67
50.0
55.33
50.0
47.01
250
219.3
50.0
38.26
50.0
54.54
50.0
45.92
50.0
56.43
100
72.89
50.0
49.69
50.0
39.65
50.0
48.43
50.0
53.43
50.0
48.71
50.0
50.06
50.0
52.10
50.0
41.40
50.0
47.04
%Rec.
RPD
Unit
D %Rec
Limits
RPD
Limit
dg-/ -L
-89
39-150
1
23
ug/L
94
70-130
1
12
ug/L
97
70-130
0
14
ug/L
109
70-137
0
14
ug/L
111
53-150
2
19
ug/L
91
55-143
0
19
ug/L
87
64-135
5
16
ug/L
106
70-147
1
16
ug/L
105
70-130
0
12
ug/L
84
60-138
1
15
ug/L
95
70-130
0
14
ug/L
72
33-150
3
20
ug/L
100
70-130
1
15
ug/L
93
70-133
3
15
ug/L
95
70-134
1
16
ug/L
104
70-133
1
13
ug/L
104
45-138
1
19
ug/L
101
70-130
0
13
ug/L
105
70-130
0
12
ug/L
105
70-130
0
13
ug/L
105
70-130
2
12
ug/L
96
48-150
1
16
ug/L
84
70-130
1
17
ug/L
83
70-130
0
13
ug/L
93
70-132
2
20
ug/L
88
70-130
0
15
ug/L
101
70-130
1
12
ug/L
89
54-142
1
17
ug/L
107
70-131
1
13
ug/L
71
56-136
2
18
ug/L
ill
70-132
1
17
ug/L
94
70-130
0
15
ug/L
88
60-137
0
21
ug/L
77
70-130
1
16
ug/L
109
70-130
2
12
ug/L
92
69-131
2
15
ug/L
113
70-130
2
17
ug/L
73
51-136
8
20
ug/L
99
70-130
2
13
ug/L
79
70-130
2
15
ug/L
97
63-142
1
13
ug/L
107
58-147
2
15
ug/L
97
70-135
3
15
ug/L
100
70-130
0
13
ug/L
104
70-130
1
14
ug/L
83
59-150
3
22
ug/L
94
69-145
0
16
TestAmerica Nashville
Page 33 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-471835/4
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471835
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D %Rec Limits RPD Limit
Vinyl chloride
50.0
43.58
ug/L
87 57-137 0 15
Xylenes, Total
100
109.2
ug/L
109 70-132 2 11
LCSD LCSD
Surrogate %Recovery Qualifier Limits
4-Bromofluorobenzene (Surr) 89 70-130
Dibromofluoromethane (Surr) 92 70-130
1,2-Dichloroethane-d4 (Surr) 102 70-130
Toluene-d8 (Surr) 100 70-130
Lab Sample ID: 490-139688-B-12 MS
Matrix: Water
Analysis Batch: 471835
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Analyte
Sample Sample
Result Qualifier
Spike
Added
MS MS
Result Qualifier
Unit
D %Rec
%Rec.
Limits
Acetone
ND
250
256.3
ug/L
103
39-150
Benzene
ND
50.0
50.40
ug/L
101
55-147
Bromodichloromethane
ND
50.0
52.01
ug/L
104
70-140
Bromoform
ND
50.0
60.17
ug/L
120
53-150
Bromomethane
ND
50.0
58.41
ug/L
117
30-150
2-Butanone (MEK)
ND
250
290.1
ug/L
116
50-143
Carbon disulfide
ND
50.0
49.97
ug/L
100
35-150
Carbon tetrachloride
ND
50.0
58.06
ug/L
116
56-150
Chlorobenzene
ND
50.0
54.51
ug/L
109
70-130
Chloroethane
ND
50.0
44.89
ug/L
90
58-141
Chloroform
0.352 J
50.0
49.53
ug/L
98
66-138
Chloromethane
ND
50.0
38.86
ug/L
78
10-150
cis- 1,2-Dichloroethene
37.7
50.0
91.36
ug/L
107
68-131
cis- 1,3-Dichloropropene
ND
50.0
48.94
ug/L
98
70-133
Cyclohexane
ND
50.0
51.38
ug/L
103
48-150
Dibromochloromethane
ND
50.0
55.78
ug/L
112
66-140
1,2-Dibromo-3-Chloropropane
ND
50.0
59.16
ug/L
118
38-138
1,2-Dibromoethane (EDB)
ND
50.0
55.26
ug/L
111
65-137
1,2-Dichlorobenzene
ND
50.0
56.43
ug/L
113
70-130
1,3-Dichlorobenzene
ND
50.0
54.57
ug/L
109
68-131
1,4-Dichlorobenzene
ND
50.0
54.60
ug/L
109
70-130
Dichlorodifluoromethane
ND
50.0
50.56
ug/L
101
10-150
1,1-Dichloroethane
ND
50.0
44.49
ug/L
89
61-139
1,2-Dichloroethane
ND
50.0
44.49
ug/L
89
64-136
1,1-Dichloroethene
ND
50.0
51.57
ug/L
103
54-150
1,2-Dichloropropane
ND
50.0
47.40
ug/L
95
67-130
Ethylbenzene
ND
50.0
52.29
ug/L
105
65-139
2-Hexanone
ND
250
253.2
ug/L
101
44-150
1 sopropyl benzene
ND
50.0
56.15
ug/L
112
70-137
Methyl acetate
ND
100
80.44
ug/L
80
42-136
Methylcyclohexane
ND
50.0
60.88
ug/L
122
59-150
Methylene Chloride
ND
50.0
50.98
ug/L
102
64-130
4-Methyl-2-pentanone (MlBK)
ND
250
251.9
ug/L
101
50-140
Methyl tert-butyl ether
1.07
50.0
44.62
ug/L
87
55-141
TestAmerica Nashville
Page 34 of 69 11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139688-B-12 MS
Matrix: Water
Analysis Batch: 471835
Sample Sample Spike MS MS
Analyte Result Qualifier Added Result Qualifier Unit
Client Sample ID: Matrix Spike
Prep Type: Total/NA
%Rec.
D %Rec Limits
Styrene
ND
50.0
57.17
ug/L
114
70-130
1,1,2,2-Tetrachloroethane
ND
50.0
49.91
ug/L
100
56-145
Tetrachloroethene
3.39
50.0
62.61
ug/L
118
57-138
Tetrahydrofuran
ND
100
75.34
ug/L
75
40-136
Toluene
ND
50.0
51.01
ug/L
102
64-136
trans- 1,2-Dich loroethene
ND
50.0
41.60
ug/L
83
59-143
trans- 1, 3-Dich loropropene
ND
50.0
50.78
ug/L
102
63-142
1,2,4-Trichlorobenzene
ND
50.0
59.19
ug/L
118
47-147
1,1,1-Trichloroethane
ND
50.0
52.80
ug/L
106
68-144
1,1,2-Trichloroethane
ND
50.0
54.56
ug/L
109
70-130
Trichloroethene
0.724
50.0
56.71
ug/L
112
63-135
Trichlorofluoromethane
ND
50.0
42.00
ug/L
84
44-150
1,1,2-Trichloro-1,2,2-trifluoroetha
ND
50.0
51.82
ug/L
104
63-150
ne
Vinyl chloride
ND
50.0
46.27
ug/L
93
57-150
Xylenes, Total
ND
100
111.1
ug/L
111
69-132
MS
MS
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr)
87
70-130
Dibromofluoromethane (Surr)
98
70-130
1,2-Dichloroethane-d4 (Surr)
87
70-130
Toluene-d8 (Surr)
97
70-130
Lab Sample ID: 490-139688-C-12 MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471835
Sample
Sample
Spike
MSD
MSD
%Rec.
RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
RPD
Limit
Acetone
ND
250
236.3
ug/L
95
39-150
8
28
Benzene
ND
50.0
47.05
ug/L
94
55-147
7
22
Bromodichloromethane
ND
50.0
47.24
ug/L
94
70-140
10
196
Bromoform
ND
50.0
54.90
ug/L
110
53-150
9
20
Bromomethane
ND
50.0
53.25
ug/L
106
30-150
9
44
2-Butanone (MEK)
ND
250
270.3
ug/L
108
50-143
7
28
Carbon disulfide
ND
50.0
44.76
ug/L
90
35-150
11
34
Carbon tetrachloride
ND
50.0
53.03
ug/L
106
56-150
9
18
Chlorobenzene
ND
50.0
51.39
ug/L
103
70-130
6
15
Chloroethane
ND
50.0
40.73
ug/L
81
58-141
10
31
Chloroform
0.352
J
50.0
46.46
ug/L
92
66-138
6
21
Chloromethane
ND
50.0
35.94
ug/L
72
10-150
8
43
cis- 1,2-Dichloroethene
37.7
50.0
84.99
ug/L
95
68-131
7
21
cis- 1,3-Dichloropropene
ND
50.0
45.75
ug/L
92
70-133
7
19
Cyclohexane
ND
50.0
47.14
ug/L
94
48-150
9
22
Dibromochloromethane
ND
50.0
51.84
ug/L
104
66-140
7
19
1,2-Dibromo-3-Chloropropane
ND
50.0
55.81
ug/L
112
38-138
6
26
1,2-Dibromoethane (EDB)
ND
50.0
51.55
ug/L
103
65-137
7
21
1,2-Dichlorobenzene
ND
50.0
52.21
ug/L
104
70-130
8
15
1,3-Dichlorobenzene
ND
50.0
51.14
ug/L
102
68-131
6
14
TestAmerica Nashville
Page 35 of 69 11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-139688-C-12 MSD
Matrix: Water
Analysis Batch: 471835
TestAmerica Job ID: 490-139626-1
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Sample
Sample
Spike
MSD MSD
%Rec.
RPD
Analyte
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD
Limit
1,4-Dichlorobenzene
ND
50.0
50.37
ug/L
101
70-130
8
14
Dichlorodifluoromethane
ND
50.0
46.75
ug/L
93
10-150
8
50
1,1-Dichloroethane
ND
50.0
40.42
ug/L
81
61-139
10
23
1,2-Dichloroethane
ND
50.0
40.89
ug/L
82
64-136
8
22
1,1-Dichloroethene
ND
50.0
48.00
ug/L
96
54-150
7
24
1,2-Dichloropropane
ND
50.0
43.55
ug/L
87
67-130
8
19
Ethylbenzene
ND
50.0
48.99
ug/L
98
65-139
7
18
2-Hexanone
ND
250
237.8
ug/L
95
44-150
6
21
1 sopropyl benzene
ND
50.0
51.87
ug/L
104
70-137
8
17
Methyl acetate
ND
100
71.50
ug/L
71
42-136
12
26
Methylcyclohexane
ND
50.0
55.89
ug/L
112
59-150
9
20
Methylene Chloride
ND
50.0
47.23
ug/L
94
64-130
8
22
4-Methyl-2-pentanone (MIBK)
ND
250
232.8
ug/L
93
50-140
8
24
Methyl tert-butyl ether
1.07
50.0
40.52
ug/L
79
55-141
10
24
Styrene
ND
50.0
53.31
ug/L
107
70-130
7
16
1,1,2,2-Tetrachloroethane
ND
50.0
46.20
ug/L
92
56-145
8
19
Tetrachloroethene
3.39
50.0
59.98
ug/L
113
57-138
4
17
Tetrahydrofuran
ND
100
66.77
ug/L
67
40-136
12
27
Toluene
ND
50.0
47.88
ug/L
96
64-136
6
18
trans- 1,2-Dich loroethene
ND
50.0
37.68
ug/L
75
59-143
10
25
trans- 1, 3-Dich loropropene
ND
50.0
47.48
ug/L
95
63-142
7
18
1,2,4-Trichlorobenzene
ND
50.0
54.65
ug/L
109
47-147
8
24
1,1,1-Trichloroethane
ND
50.0
48.72
ug/L
97
68-144
8
17
1,1,2-Trichloroethane
ND
50.0
50.97
ug/L
102
70-130
7
18
Trichloroethene
0.724
50.0
52.79
ug/L
104
63-135
7
17
Trichlorofluoromethane
ND
50.0
39.45
ug/L
79
44-150
6
32
1,1,2-Trichloro-1,2,2-trifluoroetha
ND
50.0
48.65
ug/L
97
63-150
6
22
ne
Vinyl chloride
ND
50.0
43.85
ug/L
88
57-150
5
37
Xylenes, Total
ND
100
104.6
ug/L
105
69-132
6
17
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene (Surr)
87
70-130
Dibromofluoromethane (Surr)
95
70-130
1,2-Dichloroethane-d4 (Surr)
84
70-130
Toluene-d8 (Surr)
97
70-130
Method: 8270D - Semivolatile Organic Compounds
(GC/MS)
Lab Sample ID: MB 490-471861/1-A
Client Sample ID: Method
Blank
Matrix: Water
Prep Type:
Total/NA
Analysis Batch: 472278
Prep Batch: 471861
MB MB
Analyte
Result Qualifier
RL MDL Unit
D Prepared
Analyzed
Dil Fac
1,4-Dioxane
ND
10.0 6.10 ug/L
10/30/17 09:34
10/31/17 13:58
1
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Page 36 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 8270D - Sernivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 490-471861/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472278
Prep Batch: 471861
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
2,4,6-Tribromophenol (Surr) 71
10-120
10130117 09:34 101311171 1
2-Fluorobiphenyl (Surr) 77
29-120
10130117 09:34 10131117 13:58 1
2-Fluorophenol (Surr) 71
10-120
10130117 09:34 10131117 13:58 1
Nitrobenzene-c/5 (Surr) 73
27-120
10130117 09:34 10131117 13:58
Phenol-d5 (Surr) 55
10-120
10130117 09:34 10131117 13:58 1
Terphenyl-c/14 (Surr) 86
13-120
10130117 09:34 10131117 13:58 '
Lab Sample ID: LCS 490-471861/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472278
Prep Batch: 471861
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
1,4-Dioxane ----40b
16.22
41 16-�
LCS LCS
Surrogate %Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr) 96
10-120
2-Fluorobiphenyl (Surr) 92
29-120
2-Fluorophenol (Surr) 79
10-120
Nitrobenzene-d5 (Surr) 90
27-120
Phenol-d5 (Surr) 71
10-120
Terphenyl-d14 (Surr) 100
13-120
Lab Sample ID: LCSID 490-471861/3-A
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 472278
Prep Batch: 471861
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
1,4-Dioxane
40.0
16.72
ug/L 42 10-110 3 33
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr) 71
10-120
2-Fluorobiphenyl (Surr) 68
29-120
2-Fluorophenol (Surr) 59
10-120
Nitrobenzene-d5 (Surr) 68
27-120
Phenol-d5 (Surr) 50
10-120
L Terphenyl-d14 (Surr) 73
13-120
Method: RSK-175 - Dissolved Gases (GC)
F
Lab Sample ID: MB 490-474021/32
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474021
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Ethane ND
0.00500
0.00270 mg/L
11/07/17 15:58 1
Ethylene ND
0.00500
0.00220 mg/L
11/07/17 15:58 1
Methane ND
0.00500
0.00170 mg/L
11/07/17 15:58 1
TestAmerica Nashville
Page 37 of 69 11/13/2017

QC Sample Results
Client: CIDM Smith, Inc.
ProjecVSite: NGC-Murphy NC
Method: RSK-175 - Dissolved Gases (GC) (Continued)
Lab Sample ID: MB 490-474021/32
Matrix: Water
Analysis Batch: 474021
MB MB
Surrogate %Recovery Qualifier Limits
Acetylene (Surr) 91 62-124
Lab Sample ID: LCS 490-474021/33
Matrix: Water
Analysis Batch: 474021
TestAmerica Job ID: 490-139626-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed DR Fac
111071171 1
Client Sample ID: Lab Control Sample 9
Prep Type: Total/NA F
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Ethane
-
0.527
- -
0.5497
rrig/L
104
60-120
Ethylene
0.493
0.5241
mg/L
106
80-120
Methane
0.287
0.3005
mg/L
105
80-120
LCS LCS
Surrogate %Recovery Qualifier Limits
Acetylene (Surr) 99 62-124
Lab Sample ID: LCSID 490-474021134
Matrix: Water
Analysis Batch: 474021
Analyte
Ethane
Ethylene
Methane
LCSD LCSD
Surrogate %Recovery Qualifier
Acetylene (Surr) 93
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD LCSD
%Rec.
RPD
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
0.527
0.5193
mg/L
99
80-120
6
30
0.493
0.4833
mg/L
98
80-120
8
29
0.287
0.2841
mg/L
99
80-120
6
33
Limits
62-124
Method: 300.0 - Anions, Ion Chromatography
Lab Sample ID: MB 490-471559/3
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471559
MB MB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Chloride ND
1.00 0.700 mg/L
10/28/17 18:44 1
Sulfate ND
1.00 0.600 mg/L
10/28/17 18:44 1
Lab Sample ID: LCS 490-471559/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471559
Spike
LCS LCS
%Rec.
Analyte Added
Result Qualifier
Unit D %Rec Limits
Chloride 10.0
- -
9.650
m-g/L -96 --90 - 1-10
Sulfate 10.0
9.277
mg/L 93 90-110
Page 38 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Method: 300.0 - Anions, Ion Chromatography (Continued)
Lab Sample ID: LCSD 490-471559/5
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471559
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
Chloride
10.0
9.529
mg/L 95 90-110 1 20
—Sulfate
10.0
9.245
mg/L 92 90-110 0 20
Lab Sample ID: 490-139626-5 MS
Client Sample ID: J1 155-PM-10-102717
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471559
Sample Sample
Spike
IVIS
IVIS
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit D %Rec Limits
Chloride 3.91 F-1—
—2.00
—5.195
F-1—
-m-g—/L —64 80- 12-0
Sulfate 261 E
2.00
213.5
E 4
mg/L -2361 80-120
Lab Sample ID: MB 490-471673/3
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471673
IVIB IVIB
Analyte Result Qualifier
RL
IVIDL Unit
D Prepared Analyzed Dil Fac
L Nitrate as N ND
0.100
0.0500 mg/L
10/28/17 18:44 1
FLab Sample ID: LCS 490-471673/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471673
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Nitrate as N
1.00
0.9134
mg/L 91 90-110
Lab Sample ID: LCSD 490-471673/5
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471673
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
Nitrate as N
1.00
0.8995
mg/L 90 90-110 2 20
Lab Sample ID: 490-139626-5 MS
Client Sample ID: J1 155-PM-10-102717
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471673
Sample Sample
Spike
IVIS
IVIS
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit D %Rec Limits
Nitrate as N 0.132 F1
0.200
0.2654
F1
mg/L 67 80-120
Method: 200.7 Rev 4.4 - Metals (ICP)
F Lab Sample ID: MB 490-472037/1-B
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472726
Prep Batch: 472418
IVIB IVIB
Analyte Result Qualifier
RL
IVIDL Unit
D Prepared Analyzed Dil Fac
Iron ND
0.100
0.0500 mg/L
11/01/1707:32 11/02/1702:30 1
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Page 39 of 69 11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 200.7 Rev 4.4 - Metals (ICP) (Continued)
Lab Sample ID: LCS 490-472037/2-B
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472920
Prep Batch: 472418
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier Unit
D %Rec Limits
Iron
1.00
1.023 rwg-/L
-102 85--115
Lab Sample ID: 490-139553-M-1-H MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472726
Prep Batch: 472418
Sample Sample
Spike
IVIS IVIS
%Rec.
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
Iron ND
-
1.00
0.8653 -Fn-g-lL
-87 70-- 1-30
Lab Sample ID: 490-139553-M-1-1 MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472726
Prep Batch: 472418
Sample Sample
Spike
IVISD IVISD
%Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits RPD Limit
Iron ND
-
1.00
0.8859 -Fn-g-lL
-89 70---130 -2 -20
Method: 200.8 - Metals (ICP/MS)
Lab Sample ID: MB 490-472038/1-B
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472734
Prep Batch: 472422
IVIB IVIB
Analyte Result Qualifier
RL
IVIDL Unit
D Prepared Analyzed Dil Fac
Manganese ND
0.00400
0.00150 mg/L
11/01/1707:37 11/01/1716:06 1
Lab Sample ID: LCS 490-472038/2-B
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472734
Prep Batch: 472422
Spike
LCS LCS
%Rec.
Analyte
L'M'a-nganese
Added
0.100
Result Qualifier Unit
0.09639 mg/L
D %Rec Limits
96 85-115
Lab Sample ID: 490-139553-M-1-K MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472734
Prep Batch: 472422
Sample Sample
Spike
IVIS IVIS
%Rec.
Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits
L�Analyte
Manganese 0.261 F1
0.100
0.3490 mg/L
88 70-130
Lab Sample ID: 490-139553-M-1-L MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Water
Prep Type: Dissolved
Analysis Batch: 472734
Prep Batch: 472422
Sample Sample
Spike
IVISD IVISD
%Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier Unit
D %Rec Limits RPD Limit
L Manganese 0.261 F1
0.100
0.2912 F1 mg/L
30 70-130 18 20
TestAmerica Nashville
Page 40 of 69 11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 350.1 - Nitrogen, Ammonia
Lab Sample ID: MB 490-472555/5
Matrix: Water
Analysis Batch: 472555
MB MB
Analyte Result Qualifier
Ammonia (as N) ND
Lab Sample ID: LCS 490-472555/6
Matrix: Water
Analysis Batch: 472555
Analyte
LAmmonia (as N)
Lab Sample ID: LCSD 490-472555/7
Matrix: Water
Analysis Batch: 472555
Analyte
Ammonia (as N)
Lab Sample ID: 490-139626-1 MS
Matrix: Water
Analysis Batch: 472555
Sample
Sample
Analyte
Result
Qualifier
LAmmonia (as N)
ND
Lab Sample ID: 490-139745-0-4
MS
Matrix: Water
Analysis Batch: 472555
Sample
Sample
Analyte
Result
Qualifier
Ammonia (as N)
ND
TestAmerica Job ID: 490-139626-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
0.0500 0.0500 mg/L 11/01/17 1 1:ff 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
500 5420 m-g-AL — —108 90-110
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
5.00 5.410 mgl — 109 —W:110 -0 -20
Client Sample ID: J1155-MW-7-102717
Prep Type: Total/NA
Spike IVIS ms %Rec.
Added Result Qualifier Unit D %Rec Limits
5.00 5.240 mg/L 105 90-110
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Spike ms ms %Rec.
Added Result Qualifier Unit D %Rec Limits
5.00 5.250 mg/L 105 90-110
Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 490-473647/1-A
Matrix: Water
Analysis Batch: 473706
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 473647
MB MB
LAnlalyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Su fide ND 5.00 0.700 ing/L 11/01/17 13:00 11/01/17 15:00 1
Lab Sample ID: LCS 490-473647/2-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 473706 Prep Batch: 473647
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
- -Fn-g-1 -98 fO - 130
Lsulfide 20.0 19.63 L
Page 41 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 490-139537-D-2-B MS
Client Sample ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 473706
Prep Batch: 473647
Sample Sample
Spike
ms
MS
%Rec.
Analyte Result Qualifier
Added
Result
Qualifier
Unit D %Rec Limits
Sulfide ND
20.0
19.16
mg/L 96 70-130
Lab Sample ID: 490-139537-D-2-C MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 473706
Prep Batch: 473647
Sample Sample
Spike
MSD
MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result
Qualifier
Unit D %Rec Limits RPE) Limit
Sulfide ND
—
20.0
19.32
-Fn-g—lL —96 --TO-- 1-30 —1 —10
Lab Sample ID: 490-139626-3 DU
Client Sample ID: J1155-MW-32-102617
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 473706
Prep Batch: 473647
Sample Sample
DU
DU
RPD
Analyte Result Qualifier
Result
Qualifier
Unit D RPD Limit
Sulfide ND
ND
mg/L NC 20
Lab Sample ID: MB 490-474687/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474698
Prep Batch: 474687
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Lsulfide ND
5.00 0.700 mg/L
11/03/17 14:00 11/03/17 15:45 1
Lab Sample ID: LCS 490-474687/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 474698
Prep Batch: 474687
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit D %Rec Limits
Sulfide
20.0
2003
rug -AL — 106 70---130
Lab Sample ID: 490-139626-1 MS
Matrix: Water
Analysis Batch: 474698
Sample
Sample
Analyte
Result
Qualifier
Lsulfide
ND
Lab Sample ID: 490-139626-1
MSD
Matrix: Water
Analysis Batch: 474698
Sample
Sample
Analyte
Result
Qualifier
Sulfide
ND
Lab Sample ID: 490-139745-N-1
1 -B DU
Matrix: Water
Analysis Batch: 474698
Sample
Sample
Analyte
Result
Qualifier
Sulfide
ND
Client Sample ID: J1 155-MW-7-102717
Prep Type: Total/NA
Prep Batch: 474687
Spike ms IVIS %Rec.
Added Result Qualifier Unit D %Rec Limits
20.0 17.88 mg/L 89 70-130
Client Sample ID: J1155-MW-7-102717
Prep Type: Total/NA
Prep Batch: 474687
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 18.04 mg/L 90 70-130 1 10
DU DU
Result Qualifier Unit D
-Fn-g—lL
ND
Client Sample ID: Duplicate
Prep Type: Total/NA
Prep Batch: 474687
RPD
RPD Limit
NC 20
TestAmerica Nashville
Page 42 of 69 11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: 9060A - Organic Carbon, Total (TOC)
Lab Sample ID: MB 490-474798/2
Matrix: Water
Analysis Batch: 474798
MB MB
Analyte Result Qualifier
LTotal Organic Carbon ND
Lab Sample ID: LCS 490-474798/6
Matrix: Water
Analysis Batch: 474798
Analyte
LTotal Organic Carbon
Lab Sample ID: 490-139553-0-1 MS
Matrix: Water
Analysis Batch: 474798
Sample
Sample
Analyte Result
Qualifier
Total Organic Carbon 0.563
J
Lab Sample ID: 490-139553-0-1 MSD
Matrix: Water
Analysis Batch: 474798
Sample
Sample
Analyte Result
Qualifier
Total Organic Carbon 0.563
J
Lab Sample ID: 490-139626-5 MS
Matrix: Water
Analysis Batch: 474798
Sample
Sample
Analyte Result
Qualifier
Total Organic Carbon ND
Lab Sample ID: 490-139626-5 MSD
Matrix: Water
Analysis Batch: 474798
Sample
Sample
Analyte Result
Qualifier
LTotal Organic Carbon ND
Method: SM 2320B - Alkalinity
RL MDL Unit D
1.00 0.500 mg/L
Spike LCS LCS
Added Result Qualifier
10.0 10.15
Spike IVIS IVIS
Added Result Qualifier
20.0 20.92
Spike MSD MSD
Added Result Qualifier
20.0 21.08
Spike ms ms
Added Result Qualifier
20.0 20.60
TestAmerica Job ID: 490-139626-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed Dil Fac
11/08/17 16:53 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec.
Unit D %Rec Limits
Wg--/L — —102 90-110
Client Sample ID: Matrix Spike
Prep Type: Total/NA
%Rec.
Unit D %Rec Limits
mg/L 102 75-122
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
%Rec. RPD
Unit D %Rec Limits RPD Limit
m-g—/L — 10 75 12-2 1 20
Client Sample ID: J 1 155-PM-1 0-102717
Prep Type: Total/NA
%Rec.
Unit D %Rec Limits
- -- — 103 75-122
mg/L
Client Sample ID: J1 155-PM-10-102717
Prep Type: Total/NA
Spike MSD MSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 20.76 mg/L 104 75-122 1 20
Lab Sample ID: MB 490-473223/5
Matrix: Water
Analysis Batch: 473223
MB MB
Analyte Result Qualifier RL MDL Unit D
Alkalinity ND 10.0 5.00 mg/L
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed Dil Fac
11/02/17 23:19 1
Page 43 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: SM 2320B - Alkalinity (Continued)
Lab Sample ID: LCS 490-473223/6
Matrix: Water
Analysis Batch: 473223
TestAmerica Job ID: 490-139626-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Alkalinity 100 100.9 rwg/L 101 --§-0---110
Lab Sample ID: LCSD 490-473223/26 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 473223
Spike LCSD LCSD
Analyte Added Result Qualifier
Alkalinity —100 98.71 —
Lab Sample ID: 160-25167-H-1 DU
Matrix: Water
Analysis Batch: 473223
Sample Sample
Analyte Result Qualifier
Alkalinity 148
F
Lab Sample ID: MB 490-474685/16
Matrix: Water
Analysis Batch: 474685
MB MB
Analyte Result Qualifier
LAlkalinity ND
Lab Sample ID: LCS 490-474685/17
Matrix: Water
Analysis Batch: 474685
Analyte
Alkalinity
Lab Sample ID: LCSD 490-474685/37
Matrix: Water
Analysis Batch: 474685
Analyte
LAlkalinity
Lab Sample ID: 490-139745-Q-5 DU
Matrix: Water
Analysis Batch: 474685
Sample Sample
Analyte Result Qualifier
Alkalinity ND
%Rec. RPD
Unit D %Rec Limits RPD Limit
rwg—/L —99 90- 11-0 —2 —20
DU DU
Result Qualifier Unit D
149.2 mg/L
RL MDL Unit D
10.0 5.00 mg/L
Client Sample ID: Duplicate
Prep Type: Total/NA
RPD
RPD Limit
1 20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed Dil Fac
11/08/17 23:02 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
100 96.87 mg--/L 97 90-110
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
— — — -Eg—/L— — —98 9-0-- 11-0 —1 20
100 98.19
DU DU
Result Qualifier Unit D
ND rwg—/L
Client Sample ID: Duplicate
Prep Type: Total/NA
RPD
RPD Limit
NC 20
Page 44 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: SM 2540C - Solids, Total Dissolved (TDS)
Lab Sample ID: MB 490-472515/1
Matrix: Water
Analysis Batch: 472515
Analyte
Total Dissolved Solids
Lab Sample ID: LCS 490-472515/2
Matrix: Water
Analysis Batch: 472515
Analyte
Total Dissolved Solids
Lab Sample ID: 490-139745-P-5 DU
Matrix: Water
Analysis Batch: 472515
MB MB
Result Qualifier
ND
Sample
Sample
Analyte Result
Qualifier
LTotal Dissolved Solids 71.0
Lab Sample ID: 490-139849-M-1 DU
Matrix: Water
Analysis Batch: 472515
Sample
Sample
Analyte Result
Qualifier
Total Dissolved Solids 1420
Lab Sample ID: MB 490-472517/1
Matrix: Water
Analysis Batch: 472517
Analyte
Total Dissolved Solids
Lab Sample ID: LCS 490-472517/2
Matrix: Water
Analysis Batch: 472517
Analyte
Total Dissolved Solids
Lab Sample ID: LCSD 490-47251713
Matrix: Water
Analysis Batch: 472517
Analyte
Total Dissolved Solids
Lab Sample ID: 490-139538-B-1 DU
Matrix: Water
Analysis Batch: 472517
F
TestAmerica Job ID: 490-139626-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
10.0 7.06 Tl—/01/1722-04 1
Client Sample ID: Lab Control Sample 9
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
— — — rrig—/L — —104 9-0--1-10
100 104.0
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
75.00 mg/L 5 20
Client Sample ID: Duplicate
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
1433 mg/L 1 20
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
ND 10.0 7.00 mg/L 11/01/17 19:09 1
Sample Sample
Analyte Result Qualifier
Total Dissolved Solids 310
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
100 106.0 mg/L 106 90-110
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD
LCSD
%Rec. RPD
Added Result
Qualifier
Unit
D %Rec Limits RPD Limit
100 104.0
mg/L
104 90-110 2 20
Client Sample ID: Duplicate
Prep Type: Total/NA
DU
DU
RPD
Result
Qualifier
Unit
D RPD Limit
316.0
mg/L
2 20
TestAmerica Nashville
Page 45 of 69 11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Lab Sample ID: 490-139740-E-1 DU
Matrix: Water
Analysis Batch: 472517
Sample Sample
Analyte Result Qualifier
Total Dissolved Solids -21 M
Method: SM 4500 P E - Orthophosphate
Lab Sample ID: MB 490-471767/3
Matrix: Water
Analysis Batch: 471767
MB MB
Analyte Result Qualifier
Orthophosphate as P ND
Lab Sample ID: LCS 490-471767/4
Matrix: Water
Analysis Batch: 471767
Analyte
Orthophosphate as P
Lab Sample ID: LCSD 490-471767/5
Matrix: Water
Analysis Batch: 471767
Analyte
Orthophosphate as P
Lab Sample ID: 490-139626-1 MS
Matrix: Water
Analysis Batch: 471767
F
TestAmerica Job ID: 490-139626-1
DU DU
Result Qualifier Unit D
—�i� — mg� —
RL MDL Unit D
0.100 0.0500 mg/L
Client Sample ID: Duplicate
Prep Type: Total/NA
RPD
RPD Limit
20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prepared Analyzed Dil Fac
10/28/17 16:11 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
LCS
LCS
%Rec.
Added
Result
Qualifier Unit
D %Rec
Limits
0.500
0.4880
mg/L
98
90-110
Client Sample
ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
LCSD
LCSD
%Rec. RPD
Added
Result
Qualifier Unit
D %Rec
Limits RPD Limit
0.500
0.4880
mg/L
98
90-110 0 20
Client Sample ID: J1 155-MW-7-102717
Prep Type: Total/NA
Sample
Analyte Result
Sample
Qualifier
Spike
Added
ms
Result
ms
Qualifier
%Rec.
Unit D %Rec Limits
Orthophosphate as P ND
0.500
0.5060
mg/L 101 72-129
Lab Sample ID: 490-139626-1 MSD
Client Sample ID: J1 155-MW-7-102717
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471767
Sample
Sample
Spike
MSD
MSD
%Rec. RPD
Analyte Result
Qualifier
Added
Result
Qualifier
Unit D %Rec Limits RPD Limit
Orthophosphate as P ND
0.500
0.5110
mg/L — —102 —72-129 1 20
Lab Sample ID: 490-139626-2 DU
Client Sample ID: J1 155-MW-8-102717
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 471767
Sample
Sample
DU
DU
RPD
Analyte Result
Qualifier
Result
Qualifier
Unit D RPD Limit
Orthophosphate as P 0.0520
J
0.05000
J
mg/L 4 20
Page 46 of 69
TestAmerica Nashville
11/13/2017

QC Sample Results
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Method: SM 4500 P E - Orthophosphate (Continued)
Lab Sample ID: MB 490-473471/3
Matrix: Water
Analysis Batch: 473471
Analyte
Orthophosphate as P
Lab Sample ID: LCS 490-473471/4
Matrix: Water
Analysis Batch: 473471
Analyte
Orthophosphate as P
Lab Sample ID: LCSD 490-473471/5
Matrix: Water
Analysis Batch: 473471
Analyte
Orthophosphate as P
Lab Sample ID: 590-7438-A-1 MS
Matrix: Water
Analysis Batch: 473471
MB MB
Result Qualifier
ND
Sample Sample
Analyte Result Qualifier
Orthophosphate as P ND
Lab Sample ID: 590-7438-A-1 MSD
Matrix: Water
Analysis Batch: 473471
TestAmerica Job ID: 490-139626-1
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
0.100 0.0506 Tl—/03/1723-04 1
Client Sample ID: Lab Control Sample 9
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
— — — 90-
0500 0.5080 mg/L 102 -110
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
0.500 0.5080 mg/L 102 90-110 0 20
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Spike MS MS %Rec.
Added Result Qualifier Unit D %Rec Limits
0.500 0.4900 mg/L 98 72-129
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Sample
Analyte Result
Sample Spike
Qualifier Added
MSD MSD
Result Qualifier Unit
%Rec.
D %Rec Limits RPD
RPD
Limit
Orthophosphate as P ND
0.500
04930
mg/L
99 72-129 1
20
Method: VFA-lC - Volatile Fatty Acids, Ion Chromatography
Lab Sample ID: MB 480-385877/28
Client Sample ID: Method
Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 385877
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetic acid
ND
1.0o
-6-2-90
m—g/L_
M/0-7/1706:09
1
Formic -acid
ND
1.00
0.260
mg/L
11/07/17 06:09
1
Lactic acid
ND
1.00
0.310
mg/L
11/07/17 06:09
1
n-Butyric Acid
ND
1.00
0.260
mg/L
11/07/17 06:09
1
Propionic acid
ND
1.00
0.350
mg/L
11/07/17 06:09
1
Pyruvic Acid
ND
1.50
0.370
mg/L
11/07/17 06:09
1
TestAmerica Nashville
Page 47 of 69 11/13/2017

QC Sample Results
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Method: VFA-IC - Volatile Fatty Acids, Ion Chromatography (Continued)
Lab Sample ID: LCS 480-385877/27 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 385877 Spike LCS LCS %Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetic acid
10.0
10.11
m-g-1
-101
80- 12-0
Formic -acid
10.0
8.531
mg/L
85
80-120
Lactic acid
10.0
10.14
mg/L
101
80-120
n-Butyric Acid
10.0
10.26
mg/L
103
80-120
Propionic acid
10.0
9.815
mg/L
98
80-120
Pyruvic Acid
10.0
9.414
mg/L
94
80-120
Lab Sample ID: 490-139745-H-2
MS
Client Sample
ID: Matrix Spike
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 385877
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Acetic acid
ND
50.0
49.51
mg/L
99
80-120
Formic -acid
ND
50.0
40.95
mg/L
82
80-120
Lactic acid
ND
50.0
48.76
mg/L
98
80-120
n-Butyric Acid
ND
50.0
49.91
mg/L
100
80-120
Propionic acid
ND
50.0
48.76
mg/L
98
80-120
Pyruvic Acid
ND
50.0
43.91
mg/L
88
80-120
TestAmerica Nashville
Page 48 of 69 11/13/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
GC/MS VOA
Analysis Batch: 471777
TestAmerica Job ID: 490-139626-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
A 155-MW-7-102717
Total/NA
Water
8260B
490-139626-2
A 155-MW-8-102717
Total/NA
Water
8260B
490-139626-3
A 155-MW-32-102617
Total/NA
Water
8260B
490-139626-4
J I 155-PM-4D-1 02717
Total/NA
Water
8260B
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
8260B
490-139626-6
A 155-DUP-2-102717
Total/NA
Water
8260B
MB 490-471777/7
Method Blank
Total/NA
Water
8260B
LCS 490-471777/3
Lab Control Sample
Total/NA
Water
8260B
LCSD 490-471777/4
Lab Control Sample Dup
Total/NA
Water
8260B
490-139598-D-3 MS
Matrix Spike
Total/NA
Water
8260B
490-139598-D-3 MSD
Matrix Spike Duplicate
Total/NA
Water
8260B
Analysis Batch: 471835
Prep Batch
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-139626-3
J1 155-MW-32-102617
Total/NA
Water
8260B
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
8260B
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
8260B
490-139626-6
A 155-DUP-2-102717
Total/NA
Water
8260B
MB 490-471835/7
Method Blank
Total/NA
Water
8260B
LCS 490-471835/3
Lab Control Sample
Total/NA
Water
8260B
LCSD 490-471835/4
Lab Control Sample Dup
Total/NA
Water
8260B
490-139688-B-12 MS
Matrix Spike
Total/NA
Water
8260B
490-139688-C-12 MSD
Matrix Spike Duplicate
Total/NA
Water
8260B
GUMS Semi VOA
Prep Batch: 471861
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-139626-1
A 155-MW-7-102717
Total/NA
Water
3510C
490-139626-2
J I 155-MW-8-102717
Total/NA
Water
3510C
490-139626-3
J I 155-MW-32-102617
Total/NA
Water
3510C
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
351 OC
M B 490-471861 /1 -A
Method Blank
Total/NA
Water
351 OC
LCS 490-471861/2-A
Lab Control Sample
Total/NA
Water
351 OC
LCSD 490-471861/3-A
Lab Control Sample Dup
Total/NA
Water
3510C
Analysis Batch: 472278
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
J I 155-MW-7-102717
Total/NA
Water
8270D
471861
490-139626-2
J I 155-MW-8-102717
Total/NA
Water
8270D
471861
490-139626-3
J I 155-MW-32-102617
Total/NA
Water
8270D
471861
490-139626-4
J I 155-PM-4D-1 02717
Total/NA
Water
8270D
471861
M B 490-471861 /1 -A
Method Blank
Total/NA
Water
8270D
471861
LCS 490-471861/2-A
Lab Control Sample
Total/NA
Water
8270D
471861
LCSD 490-471861/3-A
Lab Control Sample Dup
Total/NA
Water
8270D
471861
Prep Batch: 472575
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
3510C
a
F
TestAmerica Nashville
Page 49 of 69 11/13/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
GC/MS Semi VOA (Continued)
TestAmerica Job ID: 490-139626-1
Analysis Batch: 473059
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
490-139626-5 J1 155-PM-10-102717 Total/NA Water 8270D 472575
GC VOA
Analysis Batch: 474021
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
J1 155-MW-7-102717
Total/NA
Water
RSK-175
490-139626-2
J1 155-MW-8-102717
Total/NA
Water
RSK-175
490-139626-3
A 155-MW-32-102617
Total/NA
Water
RSK-175
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
RSK-175
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
RSK-175
MB 490-474021/32
Method Blank
Total/NA
Water
RSK-175
LCS 490-474021/33
Lab Control Sample
Total/NA
Water
RSK-175
LCSD 490-474021/34
Lab Control Sample Dup
Total/NA
Water
RSK-175
HPLCAC
Analysis Batch: 471559
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
J I 155-MW-7-102717
Total/NA
Water
300.0
490-139626-2
J I 155-MW-8-102717
Total/NA
Water
300.0
490-139626-3
J I 155-MW-32-102617
Total/NA
Water
300.0
490-139626-4
J I 155-PM-4D-1 02717
Total/NA
Water
300.0
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
300.0
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
300.0
MB 490-471559/3
Method Blank
Total/NA
Water
300.0
LCS 490-471559/4
Lab Control Sample
Total/NA
Water
300.0
LCSD 490-471559/5
Lab Control Sample Dup
Total/NA
Water
300.0
490-139626-5 MS
A 155-PM-1 0-102717
Total/NA
Water
300.0
Analysis Batch: 471673
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
J I 155-MW-7-102717
Total/NA
Water
300.0
490-139626-2
J I 155-MW-8-102717
Total/NA
Water
300.0
490-139626-3
J I 155-MW-32-102617
Total/NA
Water
300.0
490-139626-4
J I 155-PM-4D-1 02717
Total/NA
Water
300.0
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
300.0
MB 490-471673/3
Method Blank
Total/NA
Water
300.0
LCS 490-471673/4
Lab Control Sample
Total/NA
Water
300.0
LCSD 490-471673/5
Lab Control Sample Dup
Total/NA
Water
300.0
490-139626-5 MS
J1 155-PM-1 0-102717
Total/NA
Water
300.0
Metals
Filtration Batch: 472037
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
A 155-MW-7-102717
Dissolved
Water
Filtration
490-139626-2
A 155-MW-8-102717
Dissolved
Water
Filtration
490-139626-3
A 155-MW-32-102617
Dissolved
Water
Filtration
490-139626-4
J 1 155-PM-4D-1 02717
Dissolved
Water
Filtration
Prep Batch a
E:
Prep Batch
Prep Batch
Prep Batch
TestAmerica Nashville
Page 50 of 69 11/13/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Metals (Continued)
Filtration Batch: 472037 (Continued)
TestAmerica Job ID: 490-139626-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-139626-5
A 155-PM-1 0-102717
Dissolved
Water
Filtration
M B 490-472037/1 -B
Method Blank
Dissolved
Water
Filtration
LCS 490-472037/2-B
Lab Control Sample
Dissolved
Water
Filtration
490-139553-M-1-H MS
Matrix Spike
Dissolved
Water
Filtration
490-139553-M-1-1 MSD
Matrix Spike Duplicate
Dissolved
Water
Filtration
Filtration Batch: 472038
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
A 155-MW-7-102717
Dissolved
Water
Filtration
490-139626-2
A 155-MW-8-102717
Dissolved
Water
Filtration
490-139626-3
A 155-MW-32-102617
Dissolved
Water
Filtration
490-139626-4
J 1 155-PM-4D-1 02717
Dissolved
Water
Filtration
490-139626-5
A 155-PM-1 0-102717
Dissolved
Water
Filtration
M B 490-472038/1 -B
Method Blank
Dissolved
Water
Filtration
LCS 490-472038/2-B
Lab Control Sample
Dissolved
Water
Filtration
490-139553-M-1-K MS
Matrix Spike
Dissolved
Water
Filtration
490-139553-M-1-L MSD
Matrix Spike Duplicate
Dissolved
Water
Filtration
Prep Batch: 472418
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
J I 155-MW-7-102717
Dissolved
Water
200.7
490-139626-2
J I 155-MW-8-102717
Dissolved
Water
200.7
490-139626-3
J I 155-MW-32-102617
Dissolved
Water
200.7
490-139626-4
J 1 155-PM-4D-1 02717
Dissolved
Water
200.7
490-139626-5
A 155-PM-1 0-102717
Dissolved
Water
200.7
M B 490-472037/1 -B
Method Blank
Dissolved
Water
200.7
LCS 490-472037/2-B
Lab Control Sample
Dissolved
Water
200.7
490-139553-M-1-H MS
Matrix Spike
Dissolved
Water
200.7
490-139553-M-1-1 MSD
Matrix Spike Duplicate
Dissolved
Water
200.7
Prep Batch: 472422
Prep Batch a
Prep Batch
472037
472037
472037
472037
472037
472037
472037
472037
472037
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
A 155-MW-7-102717
Dissolved
Water
200.8
472038
490-139626-2
A 155-MW-8-102717
Dissolved
Water
200.8
472038
490-139626-3
A 155-MW-32-102617
Dissolved
Water
200.8
472038
490-139626-4
J I 155-PM-4D-1 02717
Dissolved
Water
200.8
472038
490-139626-5
A 155-PM-1 0-102717
Dissolved
Water
200.8
472038
M B 490-472038/1 -B
Method Blank
Dissolved
Water
200.8
472038
LCS 490-472038/2-B
Lab Control Sample
Dissolved
Water
200.8
472038
490-139553-M-1-K MS
Matrix Spike
Dissolved
Water
200.8
472038
490-139553-M-1-L MSD
Matrix Spike Duplicate
Dissolved
Water
200.8
472038
Analysis Batch: 472726
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
A 155-MW-7-102717
Dissolved
Water
200.7 Rev 4.4
472418
490-139626-2
A 155-MW-8-102717
Dissolved
Water
200.7 Rev 4.4
472418
490-139626-3
A 155-MW-32-102617
Dissolved
Water
200.7 Rev 4.4
472418
490-139626-4
J 1 155-PM-4D-1 02717
Dissolved
Water
200.7 Rev 4.4
472418
490-139626-5
A 155-PM-1 0-102717
Dissolved
Water
200.7 Rev 4.4
472418
M B 490-472037/1 -B
Method Blank
Dissolved
Water
200.7 Rev 4.4
472418
490-139553-M-1-H MS
Matrix Spike
Dissolved
Water
200.7 Rev 4.4
472418
TestAmerica Nashville
Page 51 of 69 11/13/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Metals (Continued)
Analysis Batch: 472726
(Continued)
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139553-M-1-1 MSD
Matrix Spike Duplicate
Dissolved
Water
200.7 Rev 4.4
472418
Analysis Batch: 472734
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
J I 155-MW-7-102717
Dissolved
Water
200.8
472422
490-139626-2
J I 155-MW-8-102717
Dissolved
Water
200.8
472422
490-139626-3
J I 155-MW-32-102617
Dissolved
Water
200.8
472422
490-139626-4
J 1 155-PM-4D-1 02717
Dissolved
Water
200.8
472422
490-139626-5
A 155-PM-10-102717
Dissolved
Water
200.8
472422
M B 490-472038/1 -B
Method Blank
Dissolved
Water
200.8
472422
LCS 490-472038/2-B
Lab Control Sample
Dissolved
Water
200.8
472422
490-139553-M-1-K MS
Matrix Spike
Dissolved
Water
200.8
472422
490-139553-M-1-L MSD
Matrix Spike Duplicate
Dissolved
Water
200.8
472422
Analysis Batch: 472920
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCS 490-472037/2-B
Lab Control Sample
Dissolved
Water
200.7 Rev 4.4
472418
General Chemistry
Analysis Batch: 385877
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-139626-1
A 155-MW-7-102717
Total/NA
Water
VFA-lC
490-139626-2
A 155-MW-8-102717
Total/NA
Water
VFA-lC
490-139626-3
A 155-MW-32-102617
Total/NA
Water
VFA-lC
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
VFA-lC
490-139626-5
A 155-PM-10-102717
Total/NA
Water
VFA-lC
MB 480-385877/28
Method Blank
Total/NA
Water
VFA-lC
LCS 480-385877/27
Lab Control Sample
Total/NA
Water
VFA-lC
490-139745-H-2 MS
Matrix Spike
Total/NA
Water
VFA-lC
Analysis Batch: 471767
Lab Sample ID
Client Sample ID
490-139626-1
A 155-MW-7-102717
490-139626-2
A 155-MW-8-102717
490-139626-3
A 155-MW-32-102617
490-139626-4
J 1 155-PM-4D-1 02717
MB 490-471767/3
Method Blank
LCS 490-471767/4
Lab Control Sample
LCSD 490-471767/5
Lab Control Sample Dup
490-139626-1 MS
J I 155-MW-7-102717
490-139626-1 MSD
J I 155-MW-7-102717
490-139626-2 DU
J I 155-MW-8-102717
Analysis Batch: 472515
Lab Sample ID
490-139626-1
490-139626-2
490-139626-5
MB 490-472515/1
Prep Type
Matrix
Method Prep Batch
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Total/NA
Water
SM 4500 P E
Client Sample ID
Prep Type
Matrix
Method
A 155-MW-7-102717
Total/NA
Water
SM 2540C
A 155-MW-8-102717
Total/NA
Water
SM 2540C
A 155-PM-1 0-102717
Total/NA
Water
SM 2540C
Method Blank
Total/NA
Water
SM 2540C
Prep Batch
Page 52 of 69
TestAmerica Nashville
11/13/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
General Chemistry (Continued)
Analysis Batch: 472515 (Continued)
Lab Sample ID Client Sample ID
LCS 490-472515/2 Lab Control Sample
490-139745-P-5 DU Duplicate
490-139849-M-1 DU Duplicate
Analysis Batch: 472517
TestAmerica Job ID: 490-139626-1
Prep Type
Matrix
Method Prep Batch
Total/NA
Water
SM 2540C
L
Total/NA
Water
SM 2540C
Total/NA
Water
SM 2540C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-3
A 155-MW-32-102617
Total/NA
Water
SM 2540C
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
SM 2540C
MB 490-472517/1
Method Blank
Total/NA
Water
SM 2540C
LCS 490-472517/2
Lab Control Sample
Total/NA
Water
SM 2540C
LCSD 490-472517/3
Lab Control Sample Dup
Total/NA
Water
SM 2540C
490-139538-B-1 DU
Duplicate
Total/NA
Water
SM 2540C
490-139740-E-1 DU
Duplicate
Total/NA
Water
SM 2540C
Analysis Batch: 472555
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-1
J I 155-MW-7-102717
Total/NA
Water
350.1
490-139626-2
J I 155-MW-8-102717
Total/NA
Water
350.1
490-139626-3
J I 155-MW-32-102617
Total/NA
Water
350.1
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
350.1
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
350.1
MB 490-472555/5
Method Blank
Total/NA
Water
350.1
LCS 490-472555/6
Lab Control Sample
Total/NA
Water
350.1
LCSD 490-472555/7
Lab Control Sample Dup
Total/NA
Water
350.1
490-139626-1 MS
A 155-MW-7-102717
Total/NA
Water
350.1
490-139745-0-4 MS
Matrix Spike
Total/NA
Water
350.1
Analysis Batch: 473223
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
SM 2320B
MB 490-473223/5
Method Blank
Total/NA
Water
SM 2320B
LCS 490-473223/6
Lab Control Sample
Total/NA
Water
SM 2320B
LCSD 490-473223/26
Lab Control Sample Dup
Total/NA
Water
SM 2320B
160-25167-H-1 DU
Duplicate
Total/NA
Water
SM 2320B
Analysis Batch: 473471
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
SM 4500 P E
MB 490-473471/3
Method Blank
Total/NA
Water
SM 4500 P E
LCS 490-473471/4
Lab Control Sample
Total/NA
Water
SM 4500 P E
LCSD 490-473471/5
Lab Control Sample Dup
Total/NA
Water
SM 4500 P E
590-7438-A-1 MS
Matrix Spike
Total/NA
Water
SM 4500 P E
590-7438-A-1 MSD
Matrix Spike Duplicate
Total/NA
Water
SM 4500 P E
Prep Batch: 473647
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-139626-3
A 155-MW-32-102617
Total/NA
Water
9030B
M B 490-473647/1 -A
Method Blank
Total/NA
Water
9030B
LCS 490-473647/2-A
Lab Control Sample
Total/NA
Water
9030B
490-139537-D-2-B MS
Matrix Spike
Total/NA
Water
9030B
490-139537-D-2-C MSD
Matrix Spike Duplicate
Total/NA
Water
9030B
Prep Batch
Prep Batch
Prep Batch
Prep Batch
Prep Batch
a
F
Page 53 of 69
TestAmerica Nashville
11/13/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
General Chemistry (Continued)
Prep Batch: 473647 (Continued)
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-3 DU A 155-MW-32-102617
Total/NA
Water
9030B
Analysis Batch: 473706
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-3 J I 155-MW-32-102617
Total/NA
Water
9034
473647
M B 490-473647/1 -A Method Blank
Total/NA
Water
9034
473647
LCS 490-473647/2-A Lab Control Sample
Total/NA
Water
9034
473647
490-139537-D-2-B MS Matrix Spike
Total/NA
Water
9034
473647
490-139537-D-2-C MSD Matrix Spike Duplicate
Total/NA
Water
9034
473647
490-139626-3 DU A 155-MW-32-102617
Total/NA
Water
9034
473647
Analysis Batch: 474685
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
A 155-MW-7-102717
Total/NA
Water
SM 2320B
490-139626-2
A 155-MW-8-102717
Total/NA
Water
SM 2320B
490-139626-3
A 155-MW-32-102617
Total/NA
Water
SM 2320B
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
SM 2320B
MB 490-474685/16
Method Blank
Total/NA
Water
SM 2320B
LCS 490-474685/17
Lab Control Sample
Total/NA
Water
SM 2320B
LCSD 490-474685/37
Lab Control Sample Dup
Total/NA
Water
SM 2320B
490-139745-Q-5 DU
Duplicate
Total/NA
Water
SM 2320B
Prep Batch: 474687
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
A 155-MW-7-102717
Total/NA
Water
9030B
490-139626-2
A 155-MW-8-102717
Total/NA
Water
9030B
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
9030B
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
9030B
M B 490-474687/1 -A
Method Blank
Total/NA
Water
9030B
LCS 490-474687/2-A
Lab Control Sample
Total/NA
Water
9030B
490-139626-1 MS
A 155-MW-7-102717
Total/NA
Water
9030B
490-139626-1 MSD
A 155-MW-7-102717
Total/NA
Water
9030B
490-139745-N-1 1 -B DU
Duplicate
Total/NA
Water
9030B
Analysis Batch: 474698
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
A 155-MW-7-102717
Total/NA
Water
9034
474687
490-139626-2
A 155-MW-8-102717
Total/NA
Water
9034
474687
490-139626-4
J 1 155-PM-4D-1 02717
Total/NA
Water
9034
474687
490-139626-5
A 155-PM-1 0-102717
Total/NA
Water
9034
474687
M B 490-474687/1 -A
Method Blank
Total/NA
Water
9034
474687
LCS 490-474687/2-A
Lab Control Sample
Total/NA
Water
9034
474687
490-139626-1 MS
A 155-MW-7-102717
Total/NA
Water
9034
474687
490-139626-1 MSD
A 155-MW-7-102717
Total/NA
Water
9034
474687
490-139745-N-1 1 -B DU
Duplicate
Total/NA
Water
9034
474687
Analysis Batch: 474798
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-139626-1
J I 155-MW-7-102717
Total/NA
Water
9060A
490-139626-2
J I 155-MW-8-102717
Total/NA
Water
9060A
490-139626-3
J I 155-MW-32-102617
Total/NA
Water
9060A
TestAmerica Nashville
Page 54 of 69 11/13/2017

QC Association Summary
Client: CIDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
General Chemistry (Continued)
Analysis Batch: 474798 (Continued)
Lab Sample ID
Client Sample ID
490-139626-4
J 1 155-PM-4D-1 02717
490-139626-5
A 155-PM-1 0-102717
MB 490-474798/2
Method Blank
LCS 490-474798/6
Lab Control Sample
490-139553-0-1 MS
Matrix Spike
490-139553-0-1 MSD
Matrix Spike Duplicate
490-139626-5 MS
A 155-PM-1 0-102717
490-139626-5 MSD
A 155-PM-1 0-102717
TestAmerica Job ID: 490-139626-1
Prep Type
Matrix
Method
Total/NA
Water
9060A
Total/NA
Water
9060A
Total/NA
Water
9060A
Total/NA
Water
9060A
Total/NA
Water
9060A
Total/NA
Water
9060A
Total/NA
Water
9060A
Total/NA
Water
9060A
Prep Batch
a
F
Page 55 of 69
TestAmerica Nashville
11/13/2017

Lab Chronicle
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Client Sample ID: A 155-MW-7-102717
Date Collected: 10/27117 10:17
Date Received: 10/28/17 09:55
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analysis
8266B
Total/NA
Prep
351 OC
Total/NA
Analysis
8270D
Total/NA
Analysis
RSK-175
Total/NA
Analysis
300.0
Total/NA
Analysis
300.0
Dissolved
Filtration
Filtration
Dissolved
Prep
200.7
Dissolved
Analysis
200.7 Rev 4.4
Dissolved
Filtration
Filtration
Dissolved
Prep
200.8
Dissolved
Analysis
200.8
Total/NA
Analysis
350.1
Total/NA
Prep
9030B
Total/NA
Analysis
9034
Total/NA
Analysis
9060A
Total/NA
Analysis
SM 2320B
Total/NA
Analysis
SM 2540C
Total/NA
Analysis
SM 4500 P E
Total/NA
Analysis
VFA-IC
Client Sample ID: J1155-MW-8-102717
Date Collected:
10/27/17 09:06
Date Received: 10/28/17 09:55
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analysis
8260B
Total/NA
Prep
351 OC
Total/NA
Analysis
8270D
Total/NA
Analysis
RSK-175
Total/NA
Analysis
300.0
Total/NA
Analysis
300.0
Dissolved
Filtration
Filtration
Dissolved
Prep
200.7
Dissolved
Analysis
200.7 Rev 4.4
Dissolved
Filtration
Filtration
Dissolved
Prep
200.8
Dissolved
Analysis
200.8
Total/NA
Analysis
350.1
Total/NA
Prep
9030B
Total/NA
Analysis
9034
Total/NA
Analysis
9060A
TestAmerica Job ID: 490-139626-1
Lab Sample ID: 490-139626-1
Matrix: Water
Dil
Factor
Initial
Amount
Final
Amount
Batch
Number
Prepared
or Analyzed
Analyst
Lab
—
1
--T--
0 mL
1-0 —mL
47-1-777
MO/2-9/17 00:10
CIA
TAL NSH
250 mL
1 mL
471861
10/30/17 09:34
CC
TAL NSH
1
472278
10/31/17 15:41
KME
TAL NSH
1
21 mL
21 rnL
474021
11/07/17 16:47
AAB
TAL NSH
1
471559
10/28/17 20:13
TIC
TAL NSH
1
471673
10/28/17 20:13
TIC
TAL NSH
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NSH
1
472726
11/02/17 03:42
LCS
TAL NSH
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
1
472734
11/01/17 16:48
BLG
TAL NSH
1
50 mL
50 mL
472555
11/01/17 11:20
GRM
TAL NSH
50 mL
50 mL
474687
11/03/17 14:00
REM
TAL NSH
1
474698
11/03/17 15:45
REM
TAL NSH
1
50 mL
50 mL
474798
11/08/17 23:08
RN
TAL NSH
1
35 mL
35 mL
474685
11/08/17 23:16
AEC
TAL NSH
1
100 mL
100 mL
472515
11/01/17 22:04
AEC
TAL NSH
1
10 mL
10 mL
471767
10/28/17 16:11
AEC
TAL NSH
5
385877
11/07/17 12:28
DMIR
TAL BUF
Lab Sample ID: 490-139626-2
Matrix: Water
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
—
1
—1---
OmL
--TO —mL
47-1777
TO—/29/1700.36
CA —A
TAL NSH
250 mL
1 mL
471861
10/30/17 09:34
CC
TAL NSH
1
472278
10/31/17 16:02
KME
TAL NSH
1
21 mL
21 mL
474021
11/07/17 16:51
AAB
TAL NSH
1
471559
10/28/17 20:42
TIC
TAL NSH
1
471673
10/28/17 20:42
TIC
TAL NSH
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NSH
1
472726
11/02/17 03:47
LCS
TAL NSH
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
1
472734
11/01/17 16:51
BLG
TAL NSH
1
50 mL
50 mL
472555
11/01/17 11:22
GRM
TAL NSH
50 mL
50 mL
474687
11/03/17 14:00
REM
TAL NSH
1
474698
11/03/17 15:45
REM
TAL NSH
1
50 mL
50 mL
474798
11/08/17 23:37
RN
TAL NSH
Page 56 of 69
TestAmerica Nashville
11/13/2017

Lab Chronicle
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
TestAmerica Job ID: 490-139626-1
Client Sample ID: A 155-MW-8-102717
Lab Sample ID: 490-139626-2
Date Collected: 10/27/17 09:06
Matrix: Water
Date Received: 10/28/17 09:55
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis SM 23��
—35 rnL
—35 rnL
474� 11�23:22 AEC TAL NSH
Total/NA Analysis SM 2540C
1
100 mL
100 mL
472515 11/01/17 22:04 AEC TAL NSH
Total/NA Analysis SM 4500 P E
1
10 mL
10 mL
471767 10/28/17 16:11 AEC TAL NSH
Total/NA Analysis VFA-IC
5
385877 11/07/17 12:57 DMR TAL BUF
Client Sample ID: A 155-MW-32-102617
Lab Sample ID: 490-139626-3
Date Collected: 10/26/17 16:05
Matrix: Water
Date Received: 10/28/17 09:55
Batch
Batch
Prep Type
Type
Method Run
Total/NA
Analysis
8266B
Total/NA
Analysis
8260B
Total/NA
Prep
351 OC
Total/NA
Analysis
8270D
Total/NA
Analysis
RSK-175
Total/NA
Analysis
300.0
Total/NA
Analysis
300.0
Dissolved
Filtration
Filtration
Dissolved
Prep
200.7
Dissolved
Analysis
200.7 Rev 4.4
Dissolved
Filtration
Filtration
Dissolved
Prep
200.8
Dissolved
Analysis
200.8
Total/NA
Analysis
350.1
Total/NA
Prep
9030B
Total/NA
Analysis
9034
Total/NA
Analysis
9060A
Total/NA
Analysis
SM 2320B
Total/NA
Analysis
SM 2540C
Total/NA
Analysis
SM 4500 P E
Total/NA
Analysis
VFA-IC
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
—
1
--T--
0 mL
10 mL
471777
M30/17 01:02
ClA
TAL NSH
10
10 mL
10 mL
471835
10/30/17 19:02
ClA
TAL NSH
250 mL
1 mL
471861
10/30/17 09:34
CC
TAL NSH
1
472278
10/31/17 16:44
KME
TAL NSH
1
21 mL
21 mL
474021
11/07/17 16:54
AAB
TAL NSH
1
471559
10/28/17 21:11
T1C
TAL NSH
1
471673
10/28/17 21:11
T1C
TAL NSH
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NSH
1
472726
11/02/17 04:03
LCS
TAL NSH
50 mL
50 mL
472038
10/30/17 15:34
JU
TAL NSH
50 mL
50 mL
472422
11/01/17 07:37
JU
TAL NSH
1
472734
11/01/17 16:54
BLG
TAL NSH
1
50 mL
50 mL
472555
11/01/17 11:23
GRM
TAL NSH
50 mL
50 mL
473647
11/01/17 13:00
REM
TAL NSH
1
473706
11/01/17 15:00
REM
TAL NSH
1
50 mL
50 mL
474798
11/09/17 00:05
RN
TAL NSH
1
35 mL
35 mL
474685
11/08/17 23:28
AEC
TAL NSH
1
100 mL
100 mL
472517
11/01/17 19:09
BMC
TAL NSH
1
10 mL
10 mL
471767
10/28/17 16:11
AEC
TAL NSH
5
385877
11/07/17 13:27
DMR
TAL BUF
Client Sample 11): A 155-PM-4D-1 02717
Date Collected: 10/27117 13:09
Date Received: 10/28/17 09:55
Lab Sample ID: 490-139626-4
Matrix: Water
Batch Batch
DII
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA An-a-lysis 8260B
1
10 mL
10 mL
471777
10/30/17 01:29
ClA TAL NSH
Total/NA Analysis 8260B
1
10 mL
10 mL
471835
10/30/17 12:25
ClA TAL NSH
Total/NA Prep 3510C
250 mL
1 mL
471861
10/30/17 09:34
CC TAL NSH
Total/NA Analysis 8270D
1
472278
10/31/17 17:04
KME TAL NSH
Total/NA Analysis RSK-175
1
21 mL
21 mL
474021
11/07/17 16:57
AAB TAL NSH
Page 57 of 69
TestAmerica Nashville
11/13/2017

Lab Chronicle
Client: CDIVI Smith, Inc.
TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy
NC
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Analysis
300.0
10
471559
10/28/17 21:56
TIC
TAL NSH
Total/NA
Analysis
300.0
10
471673
10/28/17 21:56
TIC
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472037
10/30/17 15:32
JLJ
TAL NSH
Dissolved
Prep
200.7
50 mL
50 mL
472418
11/01/17 07:32
JLJ
TAL NSH
Dissolved
Analysis
200.7 Rev 4.4
1
472726
11/02/17 04:08
LCS
TAL NSH
Dissolved
Filtration
Filtration
50 mL
50 mL
472038
10/30/17 15:34
JU
TAL NSH
Dissolved
Prep
200.8
50 mL
50 mL
472422
11/01/17 07:37
JU
TAL NSH
Dissolved
Analysis
200.8
1
472734
11/01/17 16:57
BLG
TAL NSH
Total/NA
Analysis
350.1
1
50 mL
50 mL
472555
11/01/17 11:24
GRM
TAL NSH
Total/NA
Prep
9030B
50 mL
50 mL
474687
11/03/17 14:00
REM
TAL NSH
Total/NA
Analysis
9034
1
474698
11/03/17 15:45
REM
TAL NSH
Total/NA
Analysis
9060A
1
50 mL
50 mL
474798
11/09/17 00:34
RN
TAL NSH
Total/NA
Analysis
SM 2320B
1
35 mL
35 mL
474685
11/08/17 23:36
AEC
TAL NSH
Total/NA
Analysis
SM 2540C
1
100 mL
100 mL
472517
11/01/17 19:09
BMC
TAL NSH
Total/NA
Analysis
SM 4500 P E
1
10 mL
10 mL
471767
10/28/17 16:11
AEC
TAL NSH
Total/NA
Analysis
VFA-IC
5
385877
11/07/17 13:56
DMR
TAL BUF
Client Sample ID: J1155-PM-10-102717
Date Collected:
10/27/17 13:07
Date Received: 10/28117 09:55
Batch
Batch
Prep Type
Type
Method Run
Total/NA
An—a—lysis
8260B
Total/NA
Analysis
8260B
Total/NA
Prep
351 OC
Total/NA
Analysis
8270D
Total/NA
Analysis
RSK-175
Total/NA
Analysis
300.0
Total/NA
Analysis
300.0
Total/NA
Analysis
300.0
Dissolved
Filtration
Filtration
Dissolved
Prep
200.7
Dissolved
Analysis
200.7 Rev 4.4
Dissolved
Filtration
Filtration
Dissolved
Prep
200.8
Dissolved
Analysis
200.8
Total/NA
Analysis
350.1
Total/NA
Prep
9030B
Total/NA
Analysis
9034
Total/NA
Analysis
9060A
Total/NA
Analysis
SM 2320B
Total/NA
Analysis
SM 2540C
Total/NA
Analysis
SM 4500 P E
Total/NA
Analysis
VFA-IC
Lab Sample ID: 490-139626-5
Matrix: Water
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
1
10 mL
10 mL
471777
10/30/17 01:55
CIA
TAL NSH
20
10 mL
10 mL
471835
10/30/17 18:36
CIA
TAL NSH
250 mL
I mL
472575
11/03/17 09:37
CC
TAL NSH
1
473059
11/03/17 14:16
ZLN
TAL NSH
1
21 mL
21 mL
474021
11/07/17 17:14
AAB
TAL NSH
1
471559
10/28/17 22:40
TIC
TAL NSH
1
471673
10/28/17 22:40
TIC
TAL NSH
10
471559
10/28/17 23:10
TIC
TAL NSH
50 mL
50 mL
472037
10/30/17 15:32
JU
TAL NSH
50 mL
50 mL
472418
11/01/17 07:32
JU
TAL NSH
1
472726
11/02/17 04:13
LCS
TAL NSH
50 mL
50 mL
472038
10/30/17 15:34
JLJ
TAL NSH
50 mL
50 mL
472422
11/01/17 07:37
JLJ
TAL NSH
1
472734
11/01/17 17:06
BLG
TAL NSH
1
50 mL
50 mL
472555
11/01/17 11:25
GRM
TAL NSH
50 mL
50 mL
474687
11/03/17 14:00
REM
TAL NSH
1
474698
11/03/17 15:45
REM
TAL NSH
1
50 mL
50 mL
474798
11/09/17 02:01
RN
TAL NSH
1
35 mL
35 mL
473223
11/03/17 00:05
AEC
TAL NSH
1
100 mL
100 mL
472515
11/01/17 22:04
AEC
TAL NSH
1
10 mL
10 mL
473471
11/03/17 23:04
AEC
TAL NSH
5
385877
11/07/17 14:25
DMR
TAL BUF
Page 58 of 69
TestAmerica Nashville
11/13/2017

Lab Chronicle
Client: CDIVI Smith, Inc.
Project/Site: NGC-Murphy NC
Client Sample ID: A 155-DUP-2-102717
Date Collected: 10/27/17 14:00
Date Received: 10/28/17 09:55
F
TestAmerica Job ID: 490-139626-1
Lab Sample ID: 490-139626-6
Matrix: Water
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA An-alysis
8260B
1
10 mL
10 mL
471777
10/30/17 02:21 ClA TAL NSH
Total/NA Analysis
8260B
1
10 mL
10 mL
471835
10/30/17 12:52 ClA TAL NSH
Laboratory References:
TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TIN 37204, TEL [phone]
Page 59 of 69
TestAmerica Nashville
11/13/2017

Method Summary
Client: CIDIVI Smith, Inc.
TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Method Method Description
Protocol
Laboratory
8260B Volatile Organic Compounds (GC/MS)
SW846
TAL NSH
8270D Semivolatile Organic Compounds (GC/MS)
SW846
TAL NSH
RSK-175 Dissolved Gases (GC)
RSK
TAL NSH
300.0 Anions, Ion Chromatography
MCAWW
TAL NSH
200.7 Rev 4.4 Metals (ICP)
EPA
TAL NSH
200.8 Metals (ICP/MS)
EPA
TAL NSH
350.1 Nitrogen, Ammonia
MCAWW
TAL NSH
9034 Sulfide, Acid soluble and Insoluble (Titrimetric)
SW846
TAL NSH
9060A Organic Carbon, Total (TOC)
SW846
TAL NSH
SM 2320B Alkalinity
SM
TAL NSH
SM 2540C Solids, Total Dissolved (TDS)
SM
TAL NSH
SM 4500 P E Orthophosphate
SM
TAL NSH
VFA-IC Volatile Fatty Acids, Ion Chromatography
TestAmerica SOP
TAL BUF
Protocol References:
EPA = US Environmental Protection Agency
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
RSK = Sample Prep And Calculations For Dissolved Gas Analysis In Water Samples
Using A GC Headspace Equilibration Technique, RSKSOP-1 75,
Rev. 0, 8/11/94, USEPA Research Lab
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods",
Third Edition, November 1986 And Its Updates.
TestAmerica SOP = TestAmerica, Inc., Standard Operating Procedure
Laboratory References:
TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
Page 60 of 69 11/13/2017

Accreditation/Certification Summary
Client: CIDIVI Smith, Inc. TestAmerica Job ID: 490-139626-1
Project/Site: NGC-Murphy NC
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW) State Program 4 387 12-31-17
The following analytes are included in this report, but accred itation/certifi cation is not offered by the governing authority:
Analysis Method Prep Method Matrix Analyte
9034 9030B Water Sulfide
RSK-175 Water Ethane
RSK-175 Water Ethylene
RSK-175 Water Methane
Laboratory: TestAmerica Buffalo
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority
Program
EPA Region
Identification Number
Expiration Date
Arkansas DEQ
State Program
6
88-0686
07-06-18
California
State Program
9
2931
04-01-18
Connecticut
State Program
1
PH-0568
09-30-18
Florida
NELAP
4
E87672
06-30-18
Georgia
State Program
4
10026 (NY)
03-31-18
Georgia
State Program
4
956
03-31-18
Illinois
NELAP
5
200003
09-30-18
Iowa
State Program
7
374
03-01-19
Kansas
NELAP
7
E-10187
01-31-18
Kentucky (DW)
State Program
4
90029
12-31-17
Kentucky (UST)
State Program
4
30
03-31-18
Kentucky (WW)
State Program
4
90029
12-31-17
Louisiana
NELAP
6
02031
06-30-18
Maryland
State Program
3
294
03-31-18
Massachusetts
State Program
1
M-NY044
06-30-18
Michigan
State Program
5
9937
04-01-09
Minnesota
NELAP
5
036-999-337
12-31-17
New Hampshire
NELAP
1
2973
09-11-18
New Jersey
NELAP
2
NY455
06-30-18
New York
NELAP
2
10026
03-31-18
North Dakota
State Program
8
R-176
03-31-18
Oklahoma
State Program
6
9421
08-31-18
Oregon
NELAP
10
NY200003
06-09-18
Pennsylvania
NELAP
3
68-00281
07-31-18
Rhode Island
State Program
1
LA000328
12-30-17
Tennessee
State Program
4
TN02970
03-31-18
Texas
NELAP
6
T104704412-15-6
07-31-18
USDA
Federal
P330-11-00386
11 -26-17
Virginia
NELAP
3
460185
09-14-18
Washington
State Program
10
C784
02-10-18
Wisconsin
State Program
5
998310390
08-31-18
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
TestAmerica Nashville
Page 61 of 69 11/13/2017

_TestAmedca
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN
COOLER RECEIPT FORM
490-139626 Chain of Custody
Cooler Received/Opened On10128/17 0955
Time Samples Removed From Cooler 'L'oy( Time Samples Placed In Storage k (_7>5 (2 Hour Window)
1. Tracking # �L C4 5 IG (last 4 digits, FedEx) Courier: FedEx
IR Gun ID31470366 pHStripLot Chlorine Strip Lot Jk0011(a
2. Temperature of rep. sample or temp blank when opened: 0- C( DegreesCelsius
3. If Item #2 temperature is O'C or less, was the representative sample or temp blank frozen? YES N% �n
4. Were custody seals on outside of cooler? (n.-NO ... NA
If yes, how many and where:
5. Were the seals intact, signed, and dated correctly? Q ...NO ... NA
6. Were custody papers inside cooler? Q�) ... NO ... NA
I certify that I opened the cooler and answered questions 1-6 (intial) ka G�'
7. Were custody seals on containers: YES and Intact YES...NO..&
Were these signed and dated correctly? Y ES ... NO ... CA)
8. Packing maVI used? <!Cub�ra:p)Plastic bag Peanuts Vermiculite Foam Insert Paper Other None
9. Cooling process: (!!!) Ice -pack Ice (direct contact) Dry ice Other None
10. Did all containers arrive in good condition (unbroken)?
I@E ... NO.AA
11. Were all container labels complete (#, date, signed, pres., etc)?
e ... NO ... NA
12. Did all container labels and tags agree with custody papers?
... NO ... NA
13a. Were VIDA vials received?
... NO ... NA
b. Was there any observable headspace present in any VOA vial?
YES..UO..NA
0 4" Larger than this.
14. Was there a Trip Blank in this cooler? YES..@...NA If multiple coolers, sequence #
I certify that I unloaded the cooler and answered questions 7-14 (intial 6A
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level? 1@ .. NO ... NA
b. Did the bottle labels indicate that the correct preservatives were used 0 ... NO ... NA
16. Was residual chlorine present? YESA& ... NA
I certify that I checked for chlorine and PH as Der SOP and answered questions 15-16 (intial)
17. Were custody papers properly filled out (ink, signed, etc)? &_E� ... NO...NA
18. Did you sign the custody papers in the appropriate place? NO ... NA
19. Were correct containers used for the analysis requested? ... NO ... NA
20. Was sufficient amount of sample sent in each container? q�E ... NO ... NA
21. Were there Non -Conformance issues at login? YES. N Was a NCM generated? YES. &.-_NO- ..#
.�n
BIS = Broken in shipment
Cooler Receipt Forni.doc LF-1
End of Fonn
Page 62 of 69
Revised 8/23/17
11/13/2017

Te
Loc: 490
smmedca
139626
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN COOLER RECEIPT FORM
Cooler Received/Opened On10128/170955
Time Samples Removed From Cooler-1 Time Samples Placed In Storage
(2 Hour Window)
1 g # -FedEx
Trackin Z (last 4 digits, FedEx) Courier:
IR Gun ID 31470366 pH Strip Lot_kkallq Chlorine Strip Lot 'D
2. Temperature of rep. sample or temp blank when opened: Degrees Celsius
3. If Item #2 temperature is O'C or less, was the representative sample or temp blank frozen?
YES NO.(NDA
4. Were custody seals on outside of cooler?
X-r-0
NO ... NA
If yes, how many and where:
5. Were the seals intact, signed, and dated correctly?
Q� �S. NO...NA
6. Were custody papers inside cooler?
�E .. NO.AA
I certify that I opened the cooler and answered questions 1-6 Ontial)
7. Were custody seals on containers: YES and Intact
YES ... NO..R
Were these signed and dated correctly?
YES ... N 0. O.N-1
8. Packing mat'l used? (216*1_e�wra) Plastic bag Peanuts Vermiculite Foam Insert
Paper Other None
9. Cooling process: Ice -pack Ice (direct contact) Dry
ice Other None
10. Did all containers arrive in good condition (unbroken)?
... NO ... NA
11. Were all container labels complete (#, date, signed, pres., etc)?
qR�3 ... NO ... NA
12. Did all container labels and tags agree with custody papers?
YOE ... NO ... NA
13a. Were VIDA vials received?
... NO ... NA
b. Was there any observable headspace present in any VOA vial?
YESJ(��q ... NA
0 40 Larger than this.
14. Was there a Trip Blank in this cooler? YES ... f@..NA If multiple coolers, sequence k__
I certify that I unloaded the cooler and answered questions 7-14 (intial W-L" —
15a. On pres'd bottles, did pHI test strips suggest preservation reached the correct pH level? NO ... NA
b. Did the bottle labels indicate that the correct preservatives were used - NO...NA
16. Was residual chlorine present? YES,1C0...NA
I certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (intial)
_�.,.NO ... NA
17. Were custody papers properly filled out (ink, signed, etc)? &_E
18. Did you sign the custody papers in the appropriate place? &-E-$...NO ... NA
19. Were correct containers used for the analysis requested?
20. Was sufficient amount of sample sent in each container?
I certify that I attached a label with the unique LIMS number to each container (intial)
21. Were there Non -Conformance issues at login? YES.. @) Was a NCM generated? YES.-(N_b)..#
... NO ... NA
.NO ... NA
BIS = Broken in shipment
Cooler Receipt Form. doe LF-1
End of Forin
Page 63 of 69
Revised 8/23/17
11/13/2017

Loc: 490
139626
THE LEADER IN ENVIRONMENTAL TESTING
Nashville, TN
COOLER RECEIPT FORM
Cooler Received/Opened On_10-28-2017@_09.55
Time Samples Removed From Cooler DO i� Time Samples Placed In Storage (2 Hour Window)
1. Tracking# _ 2M (last 4 digits, FedEx) Courier: _FedEx_
IR Gun ID31470368 pH Strip Lot 4CMI U( Chlorine Strip Lotj IC101 16
. I
2. Temperature of rep. sample or temp blank when opened: Degrees Celsius
3. If Item #2 temperature is O'C or less, was the representative sample or temp blank frozen? YES NO..&
4. Were custody seals on outside of cooler? (9s-- NO...NA
If yes, how many and where:
5. Were the seals intact, signed, and dated correctly?
OES -.NO...NA
6. Were custody papers inside cooler?
YES.. (9. NA
I certify that I opened the cooler and answered questions 1-6 (Intial
7. Were custody seals on containers: YES and Intact
YES ... NO..�W
Were these signed and dated correctly?
YES ... NO..(�)
8. Packing mat'l used? kBub�blewr�W Plastic bag Peanuts Vermiculite Foaminsert Paper Other None
9. Cooling process: Ice -pack Ice (direct contact)
Dry ice Other None
10. Did all containers arrive in good condition (unbroken)?
.. NO ... NA
11. Were all container labels complete (#, date, signed, pres., etG)?
(� JE ... NO.AA
12. Did all container labels and tags agree with custody papers?
"E .. NO ... NA
13a. Were VOA vials received?
Q�� ... NO...NA
b. Was there any observable headspace present in any VIDA vial?
YES. 0.0.- NA
*ON Larger than this.
14. Was there a Trip Blank in this cooler? YES.J(R0..NA If multiple coolers, sequence #
I certify that I unloaded the cooler and answered questions 7-14 (intial kA
—
15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level?
0.- NO ... NA
b. Did the bottle labels indicate that the correct preservatives were used
(0 .. NO...NA
16. Was residual chlorine present?
YESJf�AAA
I certify that I checked for chlorine and pH as per SOP and answered questions 15-16 (intial)
�% —
'17. Were custody papers properly filled out (ink, signed, etc)?
(!Ygi 4 ... NO ... NA
18. Did you sign the custody papers in the appropriate place?
0... NO ... NA
19. Were correct containers used for the analysis requested?
(0 ... NO...NA
9n Wncciiffirionfnmniintnfcnmninconfinonrhrnnfninar'?
�r�- Mn NA
21. Were there Non -Conformance issues at login? YES. MAO Was a NCM generated? YES..CNO.)#
BIS = Broken in shipment
Cooler Receipt Fonn.doc
U-1
End of Form
Revised 8/23/17
Page 64 of 69 11/13/2017

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Page 67 of 69 11/13/2017

Login Sample Receipt Checklist
Client: CIDM Smith, Inc.
Job Number: 490-139626-1
Login Number: 139626
List Number: 1
Creator: Gundi, Hozar K
Question
List Source: TestAmerica Nashville
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
TestAmerica Nashville
Page 68 of 69 11/13/2017

Client: CIDM Smith, Inc.
Login Number: 139626
List Number: 2
Creator: Hulbert, Michael J
Question
Login Sample Receipt Checklist
Answer Comment
Radioactivity either was not measured or, if measured, is at or below
True
background
The cooler's custody seal, if present, is intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the sample IlDs on the containers and
True
the COC.
Samples are received within Holding Time (Excluding tests with immediate
True
HTs)..
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
True
diameter.
If necessary, staff have been informed of any short hold time or quick TAT
True
needs
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Sampling Company provided.
True
Samples received within 48 hours of sampling.
False
Samples requiring field filtration have been filtered in the field.
N/A
Chlorine Residual checked.
N/A
2.9 #1
Job Number: 490-139626-1
List Source: TestAmerica Buffalo
List Creation: 10/31/17 04:29 PM
TestAmerica Nashville
Page 69 of 69 11/13/2017

Corrective Action Monitoring Report
October 2017 Semiannual Event
Appendix B

EMServices
Environmental Monitoring Services, LLC
Phone [phone] Fax [phone]
November 1, 2017
Mr. Kurt Batsel
The Dextra Group
4665 Lower Roswell Rd # 154
Marietta, GA 30068
RE: Groundwater Sampling at the Murphy, NC (former Clifton Precision) site
Kurt,
On October 24' - 27" we completed the semi-annual groundwater -sampling event at the Murphy, NC site.
The following points were sampled for:
MW-10, 11, 13, 17, 20, 28, 33, 34, 35, 36, 40, 41, 42, Permit specific VOC's by EPA 8260B
43, 45, 47, 60, 61, 62, 63, DUP- I (MW-20), DUP-2
(MW-35), DUP-3 (MW-33), DUP-4 (MW-61), CMP-1,
3, 4, SW-3, 6, 10, SP-26, PW- 16, RW-2, 3, 5
The sampling activities were performed according to EPA Region IV Science and Ecosystem Support
Division's Field Branches Quality System and Technical Procedures.
Upon arrival at the site, the process of collecting water levels began. The depth to water was measured
from a surveyed mark on the top of casing, if present. The process of collecting water levels was completed
within a 24-hour period to ensure a representative potentiometric map. The water level indicator was
cleaned in between each well using a Liquinox soap solution followed by a water rinse, then a DI water
rinse.
Upon arrival at each well, notes were taken as to the condition of the area around the well and the condition
of the well itself. The samplers then donned new Nitrile gloves. These gloves were changed as often as
deemed necessary to prevent contamination of the samples. A new piece of plastic was laid down next to
the well to serve as a work area.
We calculated the purge volume to three well -volumes using a standard formula. Purging continued until at
least three well -volumes were removed and the field parameters were stable or until the well was purged
dry. The purge water was captured in 5-gallon buckets to quantify the purge volumes.
We used an electric submersible pump for the purging of all wells. The pump used was a Grundfos Redi-
Flo 2 model that was attached to dedicated Teflon tubing at each well. After purging was complete, the
pump was washed using a Liquinox soap solution followed by a water rinse and a DI water rinse.
Each well was sampled using a dedicated Teflon bailer. The VOC samples were collected immediately
following the purging process or upon sufficient recovery for the wells that purged dry. Well RW-2 was
sampled with a new disposable Teflon bailer as this well no longer has in -place plumbing.
"For all your environmental monitoring needs
106A Hartwood Drive
Woodstock, GA 30189
[e-mail] Page I of2

During the purging process, pH, conductivity, temperature, and turbidity readings were collected at each
well -volume and recorded in the logbook. These readings were recorded from a YSI Professional Plus that
was calibrated each morning. Turbidity readings were collected using a Hach 2 1 OOQ. The Hach 21 OOQ
contains a factory calibration that is checked in-house using formazine standards.
The samples were collected in containers provided by the laboratory. These containers were of types, sizes
and preserved in a manner consistent with EPA Region IV SESD guidance. Upon filling, the containers
were placed on ice. The samples were delivered via Federal Express under chain of custody to Test
America located in Savannah, GA.
We appreciate the opportunity to work with you on this project, and look forward to any feedback you
have.
Respectfully,
%-I--
Jeff Johnson
Attachments: Field Notes
NGC-FSK
Page 2 of2

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-10
Date
DTW'
DTB'
35.91
I Well Volume
(DTB - DTW).* 0. 163
3 Well Volumes
IWV * 3
Purge Method
SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: JI 15510171
Time Started:
Purge Rate
(gallons,per
Actual
Volume
(gallons)
pH
SC (tt&cm)
T ('C)
Turbidity
(NTU)
Time
a j
1)
'5
el
t
5
0. 6?-
3") '5-
06
125
(50
34L�
t 5�- 0
q-"c�
501
L
LI
0 11 5;
SD
OY
0.0
6, G'G
35D
Comments
Fump control settingi 0.3 !1 �z
Sample time:
414
Depth to water as measured in f&t from top of casing
Total well depth measured in feet from top of casing
Field Technician: fNA

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Fon-ner Clifton Precision
Site
Murphy, NC
Well ID
W-
Date
DTW
DTB 2
2q.73
I Well Volume
(DTB - DTW) * 0,653
3 Well Volumes
lWV * 3 = 130, 6 1
Purge Method
SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: J 115 5 (0 (-7 j
ITime Started:
Purge Rate
(gallons per
minute
Actual
Volume
(gallons)
pH
SC ([L$/cm)
T (-C)
Turbidity
__LTUL_
I Time
Q'Q' to
1
5,21
-1&
t
QQ0
q'3.15
'30
56
1-7, -3
1 Q
Comments
Pump control setting: 253 hz (' o 6 ab
e'A� 64� OJ LAI V
time:
I Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician:

GROUNDWATER SAMPLING LOG
SITE
Murphy
SITE
LOCATION: Murphy, NC
-NAME:
WELL NO: MW-Q
SAMPLE ID: J 1 155-MWA;a - gpza4fteo it" Ii
DATE:
PURGING DATA
WELL
DIAMETER (inches) -fad I
TUBING
DIAMETER (inches).0.370
WELL SCREEN INTERVAL
I DEPTH: 11 feet to n. feet
STATIC DEPTH
TO WATER (feet):
PURGE PUMP
TYPE: ESP
WELL VOLUME PURGE: I WELL VOLUME (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
(only fill out if applicable) ( 31 �,%-7 feet - P?L�,5c) feet) X 3mm 0�� 114'7139allons/foot = i�S3 gallons
EQUIPMENTVOLUME PURGE: 1 EQUIPMENTVOL. PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(only fill out if applicable)
gallons + gallons/foot X feet) + gallons gallons
INITIAL PUMP OR TUBING -
DEPTH IN WELL (feet): 0
FINAL PUMP OR TUBING
DEPTH IN WELL (feet): 30,00
PURGING
IINITIATED ATA'Siq<K
PURGING
I ENDED AT: O�60
TOTALVOLUME
1 PURGED (gallons): IL 1.1-75.
TIME
VOLUME
PURGED
(gallons)
CUMUL.
VOLUME
PURGED
(gallons)
P URGE
RATE
(gpm)
DEPTH
TO
WATER
(feet)
H
pH
(standard
u it.;
units)
SPECIFIC
COND.
gs/cm
TEMP.
(0c)
U R
TURBIDITY
(;B I ;DI)T Y
TUs
(NTUs)
DISSOLVED
OXYGEN
mg/L
ORP
mv
ODOR
(describe)
-9 52
C­15
6-7L�
ASD
20, 6 1
294
115A
.1)9
1, .2
n r>
ASH
VW0.1
so
0,S5
;?D,1;)
616:9
1
15!��4�
%&5A5
liQ5
6 d 50
QS, 17
6:73
31L[�'
M I
Ila&->
AZ>
440&,-15
41, bC)
6.5(>
ea 3, b 4
6,?5'
-oi-i 5
i 13
OrIW
k-)�—
LA,`15
0,50
23A
L26
'RLeS
11, 1
J0,7
WELL CAPACITY (Gallons Per Foot): 0.76"=0.02; 1" = 0.04; 1.2611 = 0,06; 2" = 0.16; 3" = 0.37; 411 0.65; 511 1.02; 6" 1.47; 1211 = 5.88
TUBING INSIDE DIA. CAPACITY (Gal./Ft.): 1/8"=0.0006; 3116" = 0.0014; 111/4" = 0.0026; 6/16" = 0. 004; 3/8" 0.006; 1/2" = 0.010; 6/8" = 0.016
PURGING EQUIPMENT CODES: B = Bailer, BIP = Bladder Pump; ESP = Electric Submersible Pump; PP.= Peristaltic Pump; 0 = Other (Specify)
SAMPLING DATA
SAMPLED BY (PRINT) / AFFILIATION:
/EMServices
SAMPLER(S) SIGNATURE(S):
SAMPLING
INITIATED AT:
SAMPLING
ENDEDAT: com
PUMP OR TUBING
DEPTH IN WELL (feet): -joic.0 cf
4�'U BI N G
MATERIAL CODE: Teflon
FIELD -FILTERED: (Z) N FILTER SIZE: 0.45 I.Lm
Filtration Equipment Type:
FIELD DECONTAMINATION: PUMP Y Q TUBING Y <J��
DUPLICATE: Y
SAMPLE CONTAINER SPECIFICATION
SAMPLE PRESERVATION (including wet ice)
INTENDED
ANALYSIS AND/OR
METHOD
SAMPLING
EQUIPMENT
CODE
SAMPLE PUMP
FLOW RATE
(mL per minute)
SAMPLE
ID CODE
#
CONTAINERS
MATERIAL
CODE
VOLUME
PRESERVATIVE
USED_
TOTALVOL
ADDED IN FIELD (mL)
FINAL
pH
.11�55
6
CG
40rnL
Ice / HCI
<2
ILL VOC 8260, RSK 175
B
N/A
T11;5
3
CG
40rnL
Ice
6'j 6
VFA
B
N/A
S6
2
AG
250ml-
Ice
G/76
1,4-Dioxane
B
N/A
NS$
2
HDPE
5OOmL
Ice
TDS, Alk, 1. NO3, SO4, O-Ph.�
B
N/A
ft It 5 5
1
HDPE
5OOmL
Ice / H2SO4
<2
Ammonia
B
N/A
juss,
1
AG
500rnL
Ice / 1-12SO4
<2
TOC
B
N/A
REMARKS: Additional Bottlesrrests: 1, HDPE, 25OmL, Ice NaOH+ZnAc, >9, Sulfide, B; 1, HDPE, 250 MIL, Ice HNO3 Field Filtered, <2, Dissolved Fe, Mn, B
(6 t0AW I Slthtj = hl­� �7- 603& ho 0,40v—
M�TERIAL CODE9. AG = Amber Glass; CG = Clear Glas;; HDPE = High Density Polyethylene; LDPE = Low Density Polyethylene; PP Polypropylene;
S = Silicone; T = Teflon; 0 = Other (Specify)
SAMPLING EQUIPMENT CODES: APP = After (Through) Peristaltic Pump; B = Bailer; BP = Bladder Pump; ESP'= Electric Submersible Pump;
RFPP = Reverse Flow Peristaltic Pump; SM = Straw Method (Tubing Gravity Drain); 0 = Other (Specify)
NQ FES: 1. Low Flow also referred to as "Tubing -in -Screened Interval" (tubing placed in the center of the well screen)
2. STA131LIZATION CRITERIA FOR RANGE OF VARIATION OF AT LEAST THREE CONSECUTIVE READINGS (regired parameters in bold)
pH: + 0.1 units; Specific Conductance: + 3%; Dissolved Oxygen: + 0.2 mg/L or 10% saturation (whichever is greater);Turbidity: < 10 NTU or
+10%

EM Services
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-13
Date
/0— ) L02
DTW
DTB 2
31.12
I Well Volume
(DTB - DTW) * 0. 163
3 Well Volumes
IWV*3—
Purge Method
SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Baer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: JI 15510171
ITime Started:
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (gS/cm)
T ('C)
Turbidity
_LNTU)
Time
1693
X10
C'70
132
qJ
100
Q� 67
� 06
1 too
-9
163Q
0 4-1
1 7-25
6� 51
13 1
ALI
Z 160
e),
519
14) L--)
I'm 0
0) C- -7
1 1�-75
I S.-�S
1q, S.
q97
-190
Comments
Pump control setting: 1 J-7 hZ
b v
� . I P-- "U, r) 0 odo
iSampletime:
I Depth to water as measured in feet fTom top of casing
2 Total well depth measured in feet from top of casing
Field Technician: OkA t�Z-K V'

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-17
Date
DTWI
q,
DTB 2
37.20
I Well Volume
(DTB-DTW)*0.163=
3 Well Volumes
IWV * 3 = 0"10
Purge Method
SS Submersible Pump / Dedicate Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: J1 15510171
ITime Started:L3 3�lt
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (�LS/cm)
T ('C)
Turbidity
__�NTU�_
I Time —71
Ot 253
q.,-75
G,'70
QG7
I (i,'g
1-5
3
0,13
134 G
Q,'3 3
q,;6
Co,10
Q�
11-50
6AH
I C-6
5-
is sz
O�93
13,-7s,
6, qG
q
(6,
.3
Comments
Pump control setting: IV -7
�O odi)r
time:
Depth to water as measured in feet from top of casing
Total well depth measured in feet from top of casing
Field Technician:

EM Services
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-20
Date
/1) — D
DTW'
7A
DTB2
13.93
I Well Volume
(DTB - DTW) 0. 163 0
3 Well Volumes
I WV - 3
Purge Method
SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: JI 15510171
ITime Startedm
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (gS/cm)
T ('C)
Turbidity
(NTU)
Time
055C
Q-2q
0 -23
TO
DOG
2 U 1
3 C6
OIT513
O)D�q
1,,.)s
6.53
2o3
?o, L(
5�4_
1 C)-FDO
&�3q
(J 5
6131,
i
31
looq
5
6 p5'
)q7
11906
0,-).q
-3,50
6', 2'1
117
'20,'q
15
Comments
Pump control setting:63 hr-
'1911-f I CO I (le C
Sample time: 100-7 -
Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician: P,

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client Former Clifton Precision
Site Murphy, NC
Well ID MW-28
Date /t— a
DTW' 1c)
2
DTB 51.04
1 Well Volume (DTB - DTW) 0.653
3 Well Volumes IWV * 3 = ci t 9-,Co
Purge Method SS Submersible Pump / Dedicated Teflon Tubing
Sample Method Dedicated Teflon Bailer
Parameters Site Specific VOC's (EPA 8260B)
Laboratory/CoC No. Test America - Savannah CoC No: JI 15510171
ITime Started: f
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (pS/cm)
T ('C)
Turbidity
(NTU)
I Time
I 11-i 5S
1, CI
15,51)
7, SS
POG
IS �9
P53
Comments
Pump control setting: kz�
d
Sample time: 1501 PI-F df7 a -
I Depth to water as measured in feet from top of casing
7. Total well depth measured in feet from top of casing
Field Tpchnician:

GROUNDWATER SAMPLING LOG
SITE __J_�ITE
AME: Murphy LOCATION: Murphy, NC
DATE: 1
WELL NO: MW-32 ___TSAMPLE ID:J1 155-MW-��?- (&�6[1
PURGING DATA
WELL __T
DIAMETER (inches): 2
—TUBING _FWELL
1 DIAMETER (inches)0.375
SCREEN INTERVAL
I DEPTH:21 feetto 31 feet
STATIC DEPTH
I TO WATER (feet):
PURGE PUMP
TYPE: ESP
WELL VOLUME PURGE: I WELL VOLUME (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
(only fill out if applicable) 31.60 0.163
60 S
feet - feet) X gallons/foot gallons
EQUIPMENT VOLUME PURGE: I EQUIPMENT VOL. PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(only fill out if applicable)
gallons + gallons/foot X feet) + gallons gallons
INITIAL PUMP OR TUBING
26
1
FINAL PUMP OR TUBING PURGII G
26
PURGING
60q
T TAL VOLUME
PURGED 5
DEPTH IN WELL (feet):
DEPTH IN WELL (feet): INITIAT D AT:
ENDED AT:
(gallons): 1_7
TIME
VOLUME
PURGED
CUMUL.
VOLUME
PURGED
PURGE
RATE
DEPTH
TO
WATER
pH
dard
(stant;
SPECIFIC
COND.
TEMP.
TURBIDITY
DISSOLVED
OXYGEN
ORP
ODOR
describe)
(gallons)
(gallons)
(gpm)
(feet)
units)
4S/crn
(,)C)
(NTUs)
mg/L
mv
('5'25
-r?
�0
01 SO
-7 eq 1
g�cl
iLn
153 -A
["75
3,15
0"So
_q7;_?977L4_q_
�2' ? -S
jqq
��-?`
I
Is 34�
1 :2, o o
5,75
0, 50
A3Q
-2Vq
q
L-1-7
3 -7
;2-3
In&
I '�'Hb
1,-75
7� 5,'o
Q, So
q, 35
0
01*
1 '7
Ao
t 5H L/
Qt0c,
4, So
O'so
CF,36
Iq 5,
k:?6&17
f-6 q
Opli
52-
luas
0,50
q, n
-7, q 5'
T
1-7 Li
tol
h6
155,2
_D,00
13.D S
ASO
-1, 3
-- �7, q�
-3
S.
-76
/A3
I I
A&
�556
1,15
t 5, 60
060
T,31
7A5
3,� C,
lf,4
159
Y-3
�q
1,�.-q
-3
-Lb
10
-7-5
P9,75
S' q
10
L
L
WELL CAPACITY (Gallons Per Foot): 0.75" = 0.02; 1" = 0.04; 1.2611 = 0.06; 211 = 0.16; 3" = 0.3T W1 = 0.65; 5" = 1.02; 6" = 1.47; 1211 = 5.88
TUBING INSIDE DIA. CAPACITY (Gal./Ft.): 1/8" = 0.0006; 3116" = 0.0014; 1/4" 0.0026; 6116" = 0.004; 3/8" = 0.006; 1/2" = 0.010; 5/8" = 0.016
PURGING EQUIPMENT CODES: B = Bailer; EIP = Bladder Pump; ESP = Electric Submersible Pump; PIP = Peristaltic Pump; 0 =Other (Specify)
I�VA i'll 1:2 11 k, Nil I'M f±1
SAMMLED BY (PRIN AFFILIATION:
J—P lwk I /EMServices
SAM R(S),59NIATURE(S):
7 :1 ��
SAMPLING
I INITIATED AT: 4.4
SAMPLING
ENDED AT: t(o Is
PUMP OR TUBING 4-TUBING
DE . 26
PTH IN WELL (feet).
MA TERIAL CODE: Teflon
FIELD -FILTERED: (7) N FILTER SIZE: 0.45
Filtration Equipment-T-ype: I'M
FIELD DECONTAMINATION: PUMP Y (S) TUBING Y
DUPLICATE: Y
SAMPLE CONTAINER SPECIFICATION
SAMPLE PRESERVATION (including wet ice)
INTENDED
ANALYSIS AND/OR
METHOD
SAMPLING
EQUIPMENT
CODE
SAMPLE PUMP
FLOW RATE
(mL per minute)
SAMPLE
ID CODE
#
CONTAINERS
MATERIAL
CODE
VOLUME
PRESERVATIVE
USED
TOTALVOL
ADDED IN FIELD (mL)
FINAL
pH
6
CG
40mL
_
Ice / HCI
<2
LL VOC 8260, RSK 175
B
N/A
3
CGI
40mL
Ice
,-is
VFA
B
N/A
2
AG
25OmL
Ice
1,4-Dioxane
B
N/A
2
HDPE
5OOmL
ice
TDS, Alk. Cl. NO3, SO4, O-Phos
B
N/A
I
HDPE
50 mL
Ice / H2SO4
<2
Ammonia
B
I
AG
500ML
Ice/ H2SO4
<2
TOC
B
N/A
REMARKS: Additional Botties7ests: 1, HDPE, 250ml., Ice I NaQH+ZnAe, �9, Sulfide, B; 1, HDPE, 250 Ice I HNO3 Field Filtered, <, Dissolved Fe, Mn, B; 1, HDPE, I L, Ice, qPOR, B
'S
/15 C �4 UA I I\ 0 (5 or
MATERIAL CODES: AG = Amber Glass; CG = Clear Glass; HbPE = High Density Polyethylene; LDPE = Low Density Polyethylene; PP = Polypropylene-,
S = Silicone; T = Teflon; 0 = Other (Specify)
SAMPLING EQUIPMENT CODES: APP = After (Through) Peristaltic Pump; B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump;
RFPP = Reverse Flow Peristaltic Pump; SM = Straw Method (Tubing Gravity Drain); 0 = Other (Specify)
NU I =�: 1. LOW riow also reTerrea io as - I uwng-in­-�creenea interval-, (tuning piacea in tne center oT tne well screen)
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF AT LEAST THREE CONSECUTIVE READINGS (regired parameters in bold)
pH: + 0.1 units; Specific Conductance: + 3%; Dissolved Oxygen: + 0.2 mg/L or 10% saturation (whichever is greater); Turbidity: < 10 NTU or
+107%

EMServices.
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-31
Date
DTWI
0 L-)
DTB'
74.56
I Well Volume
(DTB - DTW) 0. 163
3 Well Volumes
IWV*3=
Purge Method
�SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 8260B)
Laboratory/CoC No.
Test America - Sa,�annah CoC No: JI 15510171
ITime Started.0a '
Purge Rate
(gallons per
minute),
Actual
Volume
(gallons)
pH
SC (�Ocm)
T ('C)
1,
Turbidity
(NTU)
Time
6�25
-7 3q
jqq
IS,6
S Ce
I'D .',-4 5
7,95
IqS
(5,(o
6I)o
L$6
Q 4t,
"715 S
I qLt
scol
9A
k,SG
30�, SO
7, S 1
5-,.!5
Q q
Comments
Pump control setting:
te
V Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician:.
16 60 .

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Fortner Clifton Precision
Site
Murphy, NC
Well ID
MW-34
Date
11-7
DTW
DTB 2
40.86
1 Well Volume
(DTB - DTW) 0. 163
3 Well Volumes
IWV * 3 = �-i 3 LA
Purge Method
SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: JI 15510171
ITime Started:
Purge Rate
(gallons p er
Actual
Volume
(gallons)
pH
SC (gS/cm)
T ('C)
Turbidity
__2LTU
I Time —]=
0Q
'3,00
-7, '55
DO 5
Ot. 6
1
I�Ias
1, 00
6100IL?'53
2VA
11, �
0
i 113
f- 00
91"IS
92H
1-7.1
0
1,-(,34
nO
11,.-75
-?, LI L�
L(,:.'
JH3-7
J,t)o
jL(',5C)
q,4j,�'
20LI
1-7, -D
q 0
(.00
I "F
I
I
0
Comments
Pump control setting: W141-, A 69
Sample time:
Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician:

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
site
Murphy, NC
Well ID
MW-35
Date
DTW
DTB 2
90.04
I Well Volume
(DTB - DTW) 0. 163 -3.
3 Well Volumes
IWV * 3 = "to, 5'3
Purge Method
SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC NO: J 115 510171
ITime Started: to
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (ftS/cm)
T ('C)
Turbidity
__jl�jT�U
163
LOD
-IZO
'-7,9%
-)15
)GM
i I 10
L60
MIS
-7, 5r
(o
!S,9
1-7
koo
2o,90
1, 3 -7
1-1
�3
rO I ID
D-7.;IS
-T. i4o
1 L3'1
J>C,
qa
�D jtg
[,�',-7
L)
C3$
1,00
3
59
Comments
Pump control setting: (-75 ke
t 10%A�j t\t) odor
Sample time: 113'9 Okq 2 (Ofllec�-j Le-�A
I Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician: V",
161()

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-36
Date
DTW
DTB 2
69.64
I Well Volume
(DTB - DTW) 0. 163 3
3 Well Volumes
IWV * 3 = j ��' 41n
Purge Method
SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: J 115510171
ITime Started: C)
Purge Rate
(gallons p er
minute
Actual
Volume
(gallons)
pH
SC (gS/cm)
T (OC)
Turbidity
Turbidity
NI
E TU
I Time —]=
Q?p 3
1,09
3,'�L5
-7.61
'3 11'
1-7.5
1101
61
13
Comments
Pump control setting: !g' A z-
0-f Oko
AY 'qL'I [WV I
I Depth to water as measured in feet from top of casing
7. Total well depth measured in feet from top of casing
Field Technician: 2 "q tk If-

GROUNDWATER SAMPLING LOG
SITE SITE
-NAME: Murphy 77T!LOCATION: Murphy, NC
WELL NO: MW-37 __JSAMPLEID:J1155-MW-37- 102_(pj-7 DATE: 10
Pt]Pr.lNr. DATA
WELL
DIAMETER (inches): 2
TUBING
DIAMETER (inches)0.375
WELL SCREEN INTERVAL
DEPTH: 101 feet to 106 feet
STATIC DEPTH
I TO WATER (feet): 21.-8 7
I PURGE PUM IP
TYPE: ESP
WELL VOLUME PURGE: 1 WELL VOLUME (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
(only fill out if applicable) ( 108.22 feet- ­z 1. e­7 feet) X 0.163 gallons/foot = 14, D8 gallons
EQUIPMENTVOLUME PURGE: I EQUIPMENTVOL. PUMP VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
(only fill out if applicable) gallons + gallons/foot X feet) + gallons = / ' gallons
INITIAL PUMP OR TUBING
DEPTH IN WELL (feet): C) ��>l
FINAL PUMP OR TUBING
DEPTH IN WELL (feet): >9�7
PURGING
� INITIATED AT: 01-
PURGING
ENDED AT:
T TALVOLUME
PURGED (gallons): 14;2_5
TIME
VOLUME
PURGED
(gallons)
CUMUL.
VOLUME
PURGED
(gallons)
PURGE
RATE
(gpm)
DEPTH
To
WATER
(feet)
pH
(standard
units)
SPECIFIC
COND.
AS/cm
TEMP.
(OC)
TURBIDITY
(NTUs)
DISSOLVED
OXYGEN
mg/L
ORP
mv
ODOR
(describe)
0q,3,L
-2,LS
7-5
0- -e(
-2) J�D
q,0
��4
1-7,(,
'3 '-
P Z-/
vrfsy�
I DO 1
-7 00
1
$'
-1
1 1-7, f)
�3 D
1),
WELL CAPACITY (Gallons Per Foot): 0.75" 0.02; 1" 0.04; 1.2511 0.06; 2" 0.16; 3" 0.37; 411 0.65; 511 1.02; 611 1.47; 12" = 5,88
TUBING INSIDE DIA. CAPACITY (Gal./Ft.): 1/8" = 0.0006; 3116" = 0.0014; 1/4" = 0.0026; 5116" = 0. 004; 3/8" 0.006; 112" = 0.0 10; 518" = 0.016
PURGING EQUIPMENT CODES: B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP Peristaltic Pump; 0 = Other (Specify)
SAMPLING DATA
SAMPLED BY (PRINT) / AFFILIATION:
/EMServices
A -R(S) SIG S):
SAMPLING
INITIATED AT: lvo7-
SAMPLING
ENDED AT:
PUMP OR TUBING
DEPTH IN WELL (feet): D-7
Tt 19ING
MATERIAL CODE: Teflon
FIELD -FILTERED: (7) N FILTER SIZE: 0.45
Filtration Equipment -Type:
FIELD DECONTAMINATION: PUMP Y TUBING Y
DUPLICATE: Y N
SAMPLE CONTAINER SPECIFICATION
SAMPLE PRESERVATION (including wet ice)
INTENDED
ANALYSIS AND/OR
METHOD
SAMPLING
EQUIPMENT
CODE
SAMPLE PUMP
FLOW RATE
(mL per minute)
SAMPLE
ID CODE
ft
CONTAINERS
MATERIAL
CODE
VOLUME
PRESERVATIVE
USED
TOTAL VOL )
ADDED IN FIELD (mL
FINAL
pH
6
CG
40rnL
Ice / HCI
-
<2
LL VOC 8260, RSK 175
B
N/A
3
CG
40mL
Ice
-
L -3
VFA
B
N/A
2
AG
25OmL
Ice
-
e�r, 03 1
1,4-Dioxane
B
N/A
2
HDPE
500mL
Ice
-
6�, tD "-->
TDS, Alk, C1, NO3, $04, O-Ph..
B
N/A
I
HDPE
500nnL
Ice/ H2SO4
-
<2
Ammonia
B
N/A
1
AG
5OOmL
Ice / H2SO4
-
<2
TOC
B
N/A
REMARKS: Additional Bottlesrrests: 1, HDPE, 250mL, Ice I NaOH+ZnAc, �9, Sulfide, B; 1, HDPE, 250 mL, Ice I HN 3 Field Filtered, <2, Dissolved Fe, Mn, 13; 1, HDPE, IL, Ice, qPCR, 13
,PC,5 ; ZD I N I z 0— 1 o� A.9 ,-j ') r i P 5)-r4 a / LAD I/
MATERIAL CODES: AG = Amber Glass; 0 WClear Glass; HDPE = High Density Polyethylene; LDPE = Low Density Polyethylene; PP = Polypropylene;
S = Silicone; T = Teflon; 0 = Other (Specify)
SAMPLING EQUIPMENT CODES: APP = After (Through) Peristaltic Pump; B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump;
RFPP = Reverse Flow Peristaltic Pump; SM = Straw Method (Tubing Gravity Drain); 0 = Other (Specify)
NOTES: 1. Low Flow also referred to as "Tubing -in -Screened Interval" (tubing placed in the center ofthe well screen)
2. STABILIZATION CRITERIA FOR RANGE OF VARIATION OF AT LEAST THREE CONSECUTIVE READINGS fregired parameters in bold)
pH: + 0.1 units; Specific Conductance: ± 3%; Dissolved Oxygen: + 0.2 mg/L or 10% saturation (whichever is greater);Turbidity: < 10 NTU or
+10%

01
EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-40
Date
DTW'
DTB 2
156.29
I Well Volume
(DTB - DTW) 0. 163
3 Well Volumes
IWV * 3
Purge Method
SS Submersible Pump Dedicated Teflon Tubing,
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah COGNO',�--11,15510172
ITime Started: Oc7t36
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH,
SC ([tS/cm)
T ('C)
Turbidity
__ILTU
I Time —1
bqq5ow
13
C)q,5�
I, q-'C--:�
so
Gt7l
QOP-
z-t -a
1003
1 nD-
S 0
L
Comments
P p control setting:
time:
I Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician: J— A4a'� (b,4- R, ke'r V-

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-41
Date
110—a S— —1
DTW'
.5,
DTB 2
157.90
I Well Volume
(DTB - DTW) 0. 163
3 Well Volumes
IWV*3= '-75,-7D
Purge Method
SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: J1 155 10 1\72
ITime Started:
Purge Rate
(gallons per
minute
Actual
Volume
(gallons)
pH
SC (16/cm)
T (OC)
Turbidity
__jNTU)
I Time
13 5-L-(
[DISC
1403
7 CDC
1 6 (T
11%
E7
Comments
Pump control setting: ;t L-7 KZ
C I vv-c� ) Y Y'
j
Lq
Sample time:( 14 05
Depth to water as measured in feet from top of casing,,,
2 Total well depth measured in feet from top of casing
Field Technician: J- 44 1'

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
site
Murphy, NC
Well ID
MW-42
Date
DTW'
qg
DTB2
27.34
I Well Volume
(DTB - DTW) 0. 163 3,
3 Well Volumes
IWV�3= lt-i�a
Purge Method
SS Submersible Pump / Dedicate_ Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 8260B)
Laboratory/CoC No.
Test America - Savannah CoC No: J 115 510172
Time Started:
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (ASICM)
T ('C)
Turbidity
(NTU)
Time
PAPG
75
1 ai s
i-kpo
i-I 3
16,Co
3-7
0,50
51
6, 6�
9-7
S-O�
4"�
L
16.(
1 1Z
t 3po
0-5c>
1.,'75
'5'10'7
LA 3
16.6
1
f3M
0' So
I t'50
Ll .3
-7
Comments
control setting: I'd.".-> odop-
time;
I Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician:

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Fortner Clifton Precision
Site
Murphy, NC
Well ID
MW-43
Date
1-7
DTW'
DTB 2
82.40
I Well Volume
(DTB - DTW) 0. 163
3 Well Volumes
I WV * 3 = 11 1$1 q'I
Purge Method
SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: J 115510172
ITime Started:
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
PH
SC (pS/cm)
T ('C)
Turbidity
(NTU)
I Time
119E
6�
ITI
3
0,0C 1
'10
to C
'2
C -'G�
--nA-
Q
Q I �f
1, ID
1 6, r) C)
"Go
n
ts, I
i �)') q
1110
oi,-j5
C(5�
-3
h3
N 3
ID
97.
Cc 53
1-7?
ISIII
I Q �2q
it 10
-5,;? Ob-
65
1-7-3
VT'
F— Comments
Pump control setting: DOS A z
C [0�' X'6
time: I —� -3. 0
Depth to water as measured in feet from top of casing
Total well depth measured in feet from top of casin�
Field Technician: )r

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-45
Date
DTW'
DTB'
76.65
1 Well Volume
(DTB - DTW) 0. 163
3 Well Volumes
IWV * 3
Purge Method
SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 8260B)
Laboratory/CoC No.
Test America - Savannah CoC No: JI 15510172
ITime Started:
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (pS/cm)
T (IC)
Turbidity
__LNTU)
Time I
�3
-2 5:5
1 -7,
I'll 5
L-39
11 1 06
'79 5
Q!99
16,5
G14
1 1-11 R
1 Ci 5C)
7 51
ICI?
3 5C
a[ 75
7S'Ce
Lre --7
-S-7
1,35
D-7, a5
?, S?�
16,5
5�;)
.11-1,31
7, 5c[
D s8
16,5
t D I
-3.�j�
Comments
Pump control, -setting: k'51 k-Z
lov &Y Ao Odo V
Sample time: I 43D
1 Depth to water as measured in feet ' ftorn top of casing
2 Total well depth measured in feet from t9p of casing
Field Technician:

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-47
Date
DTWI
DTB 2
92.62
I Well Volume
(DTB - DTW) 0. 163 e3 -7
3 Well Volumes
IWV * 3
Purge Method
SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 8260B)
Laboratory/CoC No.
Test America - Savannah CoC No: JI 15510172
ITime Started:
Purge Rat I e
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (VS/cm)
T ('C)
Turbidity
(NTU)
I Time
),()$
0 111;0
--� ,-15
1139,
1 Is, G
� 3
N
1-3 � t)V
7. ? q/
IL7
is, 6
6'
130
1, CA
I 1q,50
7, 7 0/
1 Z'�
z e-
1 0'5
'p 5115
13 1 S'
1,05
3
-z I q
2- 3
f5,G
Q
nq-)
-3'9 �I 5
-ISO
LI-S
[S.G
Comments
Pump control setting:,26-7
Y149 0 dol
Sample time:
I Depth to water as measured in feet from top, of casing
2 Total we] I depth measured in feet from top. of casing
Field Technician:

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-60
Date
16-a 51, ) __7
DTW'
0, 00
DTB 2
49.18
1 Well Volume
(DTB - DTW) 0.163=
3 Well Volumes
lWV * 3 =PIJ,6 S
Purge Method
SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
-Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 8260B)
Laboratory/CoC 346.
Test America - Savannah CoC No: J 115 510172
ITime Started:
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
pH
SC (pS/cm)
T ('C)
Turbidity
__(I�TU)
Time
M3
6,3,5
IkIF
(-7 L(
o�5
-71-)b
P05
J-7p
1120
0.55
1 Co.-.) 'S
7.,� q
U
t'33
0,155
-�z 6, AS
7 a?
Do S
6
'31
k
L9 1
Qq
G,6
1-f
PIS
I Comments
Pump control setting: 0 Ott h2- C JNA6�, JAD&Ar>r
ISampletime:
Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician: Kaf

EMServices
Environmental Monitoring Services, LLC
,r-,,Tield Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-61
Date
C) o
DTWI
DTB'
84.15
I Well Volume
(DTB - DTW) 0. 163
3..Well Volumes
IWV*3=
Purge Method
SS Submersible Pump Dedicated Teflon Tubing
Sample Method
Dedicated Tefldh Bailer
Site Specific VOC's (EPA 8260B)
,garameters
14, CoC No.
Test America - Savannah CoC No: JI 15510172
ITime Started:
Purge Rate
(gallons per
minute)
Actual
Volume
(gallons)
PH
SC (4slcm)
T ('C)
Turbidity
(NTU)
I Time
1030
6 c6
'P65
1-1-7
3D
�6,'25
'266
;?Q q
15'. q
3:
-SO
'7, Co Li
1-7
t,�O
9
I,Z
-2, 63
10
A:
Comments
Pump control setting:D3R K-z
Sample time: 5G
I Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing
Field Technician:.

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-62
Date
DTW
DTB 2
44.55
I Well Volume
(DTB-DTW)*0.163=
3 Well Volumes
IWV * 3 = ;� I 'a I
Purge Method
SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
Site Specific VOC's (EPA 826013)
Laboratory/CoC No.
Test America - Savannah CoC No: J 115510172
ITime Started:
Purge Rate
(gallons per
minute)
Act I ual
Volume
(gallons)
pH
SC (gS/cm)
T ('C)
Turbidity
__j]�LT�U
I Time —1
I IDO 5
1,25
'3,�-75
-�2 6 -7
15, G
10 '15
-7,15
-D q 6
1 5,'�
1-0)[9
tp�
1 144 "�5
'—Z
a Cjq
I'D t-7
I
F- Comments I
IPump control setting: 1 Y'7 h-z ckc� Y- I
IlSample time: J�dc) I
I Depth to water as measured in feet from top of casing
2 Total we] I depth measured in feet from top of casing
Field Technician: j— L'u, Ly-

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client
Former Clifton Precision
Site
Murphy, NC
Well ID
MW-63 -7
Date
t
DTW'
DTB 2
84.00
I well Volume
(DTB - DTW) * 0.163
3 Well Volumes
I WV * 3 = -4+To*
Purge Method
_SS Submersible Pump / Dedicated Teflon Tubing
Sample Method
Dedicated Teflon Bailer
Parameters
-Site Specific VOC's (EPA 8260B)
Laboratory/CoC No.
Test America - Savannah CoC No: J 115510172
Time Started-'-t47f�l
Purge Rate
(gallons per
minute)
Actual
Volume
(gall ns)
pH
SC (�ts/cm)
T ('C)
Turbidity
(NTU)
PC`
F. Time DTW
1,27
7, CI
0.37
OSS7 7. 11
C) q c) 1 t142
0, 0 0 z,
0,
t_--2-�" -C--'
r 4'_'�k_Zu
1, 7�
-
4
-6 0 IL
S02.,
14.
11�- 7
J0,1
0�0:s 19,16'
T6S.
3 02.
1 L4, 7
oqol 1"
0 .0 6 3
7­27
? S 1�
Z-
I 't-7
10 3� I
-
Comments
Sample time:
I Depth to water as measured in feet from top of casing
2 Total well depth measured in feet from top of casing

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
client Former Clifton Precision
Site Murphy, NC
Sample Method Direct grab
Parameters Site Specific VOC's (EPA 8260B)
Laboratory/CoC No. Test America - Savannah CoC No: JI 15510172
Sample ID
PW -16
Date
(U-0-7-17
Time
I&ZO
pH
7, 6-3
SC (�ts/cm)
67
Turbidity
T ('C) (NTU)
S�-)"-
[04-3
1()ZC
-R-i--+6-?i
15-5 r
I(V
C 7)
Or
-3
vs,7 ac�
6. 6 q
--L7
Field Technician:

EMServices
Environmental Monitoring Services, LLC
Field Data Sheet
Client Former Clifton Precision
site Murphy, NC,
Sample Method RW-2: bailer, Other RW's: sample ports, SW's: direct grab
Parameters Site Specific VOC's (EPA 826013)
Laboratory/CoC No. Test America - Savannah CoC No: J 115 510173
Sample ID
Date
Time
pH
SC I ([tS/cm)
T ('C)
Turbidity
___�NTU)
RW-2
77�5-
Z'47
RW-3
RW-5
IO-Z6-17
IM
7. 7
'Zil
CMP-1
'7
CMP-3
10--2,7-/-r
7, Z
74,
3
CMP-4
-2-7-)7-
Ocl-Z-I
LDIG
UV
SW-3
10-'�-7-n
OA4-3
7,60
7/
1�
SW-6
6 Z-
-10
10
7-7
1
SP-26
Field Technician:

EM, Services
Environmental Monitoring Services, LLC
Field Data Sheet
Client Former Clifton Precision
Site Murphy, NC
Sample Method Direct grab
Parameters Site Specific VOC's (EPA 8260B)
Laboratory/CoC No. Test America - Savannah CoC No: JI 1 5510174
.e, ,
Sample ID
Date
Time
EB-1
EB-2
VS F3
B
EB-4
12d:
Comments
DI Water from Test America Atlanta Service Center stored at EM
Services' office. Equipment Blanks poured* at equipment trailer near
storage area.
Field Technician: NA��w

M Se
� jmces
Envirionmenta. 6�4 rini Services, LLC
-M
AG Water L '.el
c* S.
':Date: 3Aa
Well ID
Tim�
DTW.�
4
:
':Time.-,,.,;.
.. W. .-:
DT,
v
mw- -
.1
.. 7
1. , *5
m
f61 3 51
ell
MW-7
(34 5);�
M.WT, Ing 40
15&29�
j
mw8j;
...BT90:
MW-9
9 59�
lw-7.
-2
27.34
mw�10.
.40.
mw-I t
4
'7 1.7�
.7,
'j-.43
MW-12
76.�65,
MW-43
M��446
K4
52,90 -
MW-14Ri
8,001..
MW-�417
2.62,
1%26.�
MW-17
372W�
-MW�5 0
81,41.,
MW-18
�ffl.04:-
MW,-5,1
MW49R
6930-
W .52
-D
40
MW-20.
A3 91
MW...5,3
.2
MW-22'
JWc)
7
-W,-�4
3T8
MW-23,
-_.55.
09..51
.'MW-25
(0
2 4
MW-66
.2�1
mw
MW-27
VA.
M-W-.57:
mw-
MW-2gr'
Ell
0'
5
&6
M.W 0
m
29,63.,.,'.
�,- 1
, M-W 61
8 4.15
mw-
N
w I
low. ..6,2
Is:
�W-
MW_
A 6:
84.0
W�31-
31 60,;'�
mw�.,84
15A3,
I -A
W�3 3:
ID
W
10
T9 -
MW-34�� -
40.86.
IKW-3
3:
MW-�3:5i
90. 4
R - 4.
W
-377,
r
IMW -16 - : . F
16i:
r 69.6
77777777-
RW_5:�
MW-37
6
PW4;-,
f
MW
446
Page 1 of 2

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