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NCG120064_DMR_20201013
•r. fli September 25, 2020 Chambers Development of NC, Inc. and Waste Connections of the Carolinas, Inc. Anson Waste Management Facility 375 Dozer Road Polkton, NC 28135 Attention: Mr. Tyler Fitzgerald Reference: Second Semi -Annual Stormwater Monitoring Anson Waste Management Facility NCG120064 Polkton, North Carolina S&ME Project No. 4140-15-007 Dear Mr. Fitzgerald: � y17 w I. G A ; A t11-f nEQ-FAYETTEVILLE REGIONALO!=FICE S&ME, Inc. (S&ME) is pleased to submit this report detailing the results of the September 2020 stormwater monitoring activities conducted at the Anson Waste Management Facility (AWMF) in Polkton, North Carolina. This work was completed in accordance with our Master Services Agreement dated January 2, 2017, and in accordance with Task 2 in S&ME Proposal No. 41-1600394 (Rev. 1) dated August 8, 2016. This letter summarizes results of sampling efforts conducted by facility personnel. * Background Stormwater sampling is required on a semi-annual basis, as defined by the National Pollutant Discharge Elimination System (NPDES) General Permit for Landfills (Permit No. NCG120000) for the facility outfalls. The following outfalls are identified at the facility: Outfall 1, Outfall 2, Outfall 3, Outfall 4, Borrow Area North Outfall, and Borrow Area West Outfall. Outfall 2 was eliminated in August 2018 by the expansion of Sediment Basin 3 and, therefore, is no longer sampled. Monthly sampling was initiated following December 2019 results at Outfall 3 and Outfall 4, in response to Tier 2 and Tier 3 response actions at the facility. Parameters for quantitative analysis include chemical oxygen demand (COD) per Standard Method (SM) 2540D, fecal coliform per SM 9222D, and total suspended solids (TSS) utilizing SM 2540D. In addition to the previously listed parameters, Outfall 1 and Outfall 3 are also sampled for chemical parameters associated with vehicle maintenance which include total petroleum hydrocarbons (TPH) per Environmental Protection Agency (EPA) Method 1664B and pH utilizing SM 4500. Stormwater Sampling and Quantitative Analyses AWMF personnel collected the second semi-annual stormwater samples at five (5) designated outfall locations on September 15, 2020. The total rainfall for the September 15, 2020 storm event was reported as approximately 1.64 inches in 24 hours. Sampling was performed during that storm event. S&ME, Inc. 1 644 Eastern Star Road I Kingsport, TN 37663 1 p 423.349.2800 1 www.smeinc.com ANEW Second Semi -Annual Stormwater Monitoring c. Anson Waste Management Facility S&ME Project No. 4140-15-007 Quantitative chemical laboratory results for the monitoring event are compared to benchmark values established by the facility NPDES permit on the attached Discharge Monitoring Report (DMR). Parameter exceedances of benchmark values, if any were documented through field and laboratory analyses, are summarized in bold type below. Total i Fecal • OxygenChemical Outfall Denialid Solids 00 Benchmark 120 100 1000 15 6 — 9 Outfall 1 Sed Basin 1 29.7 13.0 12.0 ANR 6.44 Outfall 3 Sed Basin 3 <25.0 6.6 38.0 <8.9 6.40 Outfall 4 Sed Basin 4 25.0 8.2 88.0 <8.2 6.84 Borrow North 41.5 17.3 570 ANR 7.12 Borrow West <25.0 <5.7 260 ANR 7.03 ANR = Analyte not requested and not required by the NPDES Permit mg/l= milligrams per liter CFU/ml= colony -forming units per milliliter The DMR is included with this letter as Attachment I for signature and submittal to the North Carolina Department of Environmental Quality (NCDEQ), Division of Water Quality. The Laboratory Data Report for this sampling event is included as Attachment II. ® Closure S&ME appreciates this opportunity to be of service to Waste Connections and trust this information is responsive to your current needs. If you have any questions, please contact us at your convenience. Sincerely, S&ME, Inc. Lindse O: y Marris James R. Bruce Project Manager Senior Reviewer Attachments: Discharge Monitoring Report Laboratory Data Report Site SWPPP Map cc: Mike Lawyer, Fayetteville Regional Office Lana Brown, Waste Connections Nelson Breeden, Waste Connections of the Carolinas, Inc. Page 2 Attachments Attachment I Discharge Monitoring Report m .0 V C L m E L. C C •E aJ V'f 0 L U s O Z L. 42 Q El 3 L --- 1 3 N L 0U) 3 OL O (V ar �, O N O ❑EIFJ OC W 7 C �o ate+ 0 N G O QQ U LLI 0 �- � O O 2 a z a a Q � N Ln Ph _N ti h ,tI U Z � ta t! �L DI 0 y N � m F- J •>. m V Z —j N m L IA -F+ (A _ O C M fp z 7 W O V t C , G O = o ca > N C Q °' m oQ z O G. E 07 3 U. 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C. m O LA �o a m a N O c 0 O LL UJ � W a J J c W d W O W V1 Z O Z T U, Z 2 a WLU Q LU L w m N Q Q W d ~ ~ LI U L w W N � N W ¢ J ~ aCC F- Q O LL H LL Z)w a O U LU Z LU W C 0 . N W H W X Z H w W Y W 0Lu a Cf U Lu w U Z 0wLLJ ei W � � LL,O w N w O C9 w O � o ~ } uw O LLI- U Z J O LULU a LL X Z w V, O w U } a a = o = U W Z W M m W W ¢ N H El O Z 13 W } w U LL LL a Z _O (7 LU K LU w 0 w w b w z a O Z U �a 0 Z Qu _ W } O LL J Q Z O w w Ql Q1 cu fa N c C_ C LL U O m M O1 Y U U u a) t O O •m Z O O to o a1 o a v4'i u T •N N � F' ai O v v o +� +ru ro j c u O N mU > f0 E M LD s o 3 3 o U C Y C O •— .fl �+ O a a N O f0 E U) v o o v v a a a1 o E a1 +c+ Y O 7 O T M N C N O C C cr f+= O C a1 O E t O O +� N CQ Co v v C t O N C t0 E N O N -0 C U o a N yr N C (a C p E O N 41 +N, E c E U al C N M 4� O m `m E c — a ro MO c c E 4� a1 C C N a1 E a5 c u v U) O m t ••I—+ W N N T � CL .r- ° a)c 41 a 9 m CC o a .N4 0 v 4T+ a1 L a T to C t v a)CL ?E v t N i =p a1 > N + O 4 . o y VI W L ` � a1 v 3 U o E iA M +j M 1 m 00 0 N O N e\-I c Ln 00 c-I O N 41 c-I a1 fO 0 E (U d Attachment II — Laboratory Data Report aceAnalj6cal www.pacelabs.com September 22, 2020 Lindsey Harris SWE, Inc. 644 Eastern Star Road Kingsport, TN 37663 RE: Project: Anson LF Stormwater Pace Project No.: 92495552 Dear Lindsey Harris: Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on September 15, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, I "�` o, 14y, Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 16 aceAnai(Xical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville; NC 28078 (704)875-9092 CERTIFICATIONS Project: Anson LF Stormwater Pace Project No.: 92495552 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 aceAnaljftal www.pacoiabs.com SAMPLE ANALYTE COUNT Project: Anson LF Stormwater Pace Project No.: 92495552 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92495552001 OUTFALL 1 SM 922213-2006 KDF 1 PASI-C SM 2540D-2011 ALP 1 PASI-A SM 5220D-2011 BAS 1 PASI-A 92495662002 OUTFALL 3 SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 ALP 1 PASI-A SM 5220D-2011 BAS 1 PASI-A 92495662003 OUTFALL 4 SM 9222D-2006 KDF 1 PASI-C SM 2540D-2011 ALP 1 PASI-A SM 5220D-2011 BAS 1 PASI-A 92495562004 BORROW NORTH SM 9222D-2006 KDF 1 PASI-C SM 2540D-2011 ALP 1 PASI-A SM 5220D-2011 BAS 1 PASI-A 92495562005 BORROW WEST SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 ALP 1 PASI-A SM 5220D-2011 BAS 1 PASI-A 92495552006 Outfall 4 (Sed 4) EPA 1664B HH 1 PASI-C 92496552007 Outfall 3 (Sed 3) EPA 1664B HH 1 PASI-C PASI-A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 aceAnalytical (*2 www.pacelabs.com SUMMARY OF DETECTION Project: Anson LF Stormwater Pace Project No.: 92495552 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92495552001 OUTFALL 1 SM 9222D-2006 Fecal Coliforms 12.0 CFU/100 mL 1.0 09/16/20 14:36 SM 2540D-2011 Total Suspended Solids 13.0 mg/L 2.9 09/21/20 11:25 SM 5220D-2011 Chemical Oxygen Demand 29.7 mg/L 25.0 09/16/20 22:05 92495552002 OUTFALL 3 SM 9222D-2006 Fecal Coliforms 38.0 CFU/100 mL 1.0 09/16/20 14:53 SM 2540D-2011 Total Suspended Solids 6.6 mg/L 2.7 09/21/20 11:26 92495552003 OUTFALL 4 SM 9222D-2006 Fecal Coliforms 88.0 CFU/100 mL 1.0 09/16/20 14:36 SM 254OD-2011 Total Suspended Solids 8.2 mg/L 3.8 09/21/20 11:26 SM 5220D-2011 Chemical Oxygen Demand 25.0 mg/L 25.0 09/16/20 22:06 92495562004 BORROW NORTH SM 9222D-2006 Fecal Coliforms 570 CFU/100 mL 1.0 09/16/20 14:36 SM 2540D-2011 Total Suspended Solids 17.3 mg/L 4.8 09/21/20 11:26 SM 5220D-2011 Chemical Oxygen Demand 41.5 mg/L 25.0 09/16/20 22:06 92495652005 BORROW WEST SM 9222D-2006 Fecal Coliforms 260 CFU/100 mL 1.0 09/16/20 14:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 4 of 16 Pace Analytical Services, LLC aceAnalytical ® 9800 ney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Anson LF Stormwater Pace Project No.: 92495552 Sample: OUTFALL 1 Lab ID: 92495552001 Collected: 09/15/20 08:25 Received: 09/15/20 12:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 12.0 CFU/100 mL 1.0 1 09/15/20 15:15 09/16/20 14:36 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 13.0 mg/L 2.9 1 09/21/20 11:25 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 29.7 mg/L 25.0 1 09/16/20 16:56 09/16/20 22:05 Sample: OUTFALL 3 Lab ID: 92495552002 Collected: 09/15/20 08:34 Received: 09/15/20 12:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 38.0 CFU/100 mL 1.0 1 09/15/20 15:43 09/16/20 14:53 2640D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services - Asheville Total Suspended Solids 6.6 mg/L 2.7 1 09/21/20 11:26 6220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand ND mg/L 25.0 1 09/16/20 16:56 09/16/20 22:06 Sample: OUTFALL 4 Lab ID: 92495552003 Collected: 09/15/20 07:48 Received: 09/15/20 12:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 88.0 CFU/100 mL 1.0 1 09/15/20 15:15 09/16/20 14:36 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 8.2 mg/L 3.8 1 09/21/20 11:26 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand 25.0 mg/L 25.0 1 09/16/20 16:56 09/16/20 22:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 16 Pace Analytical Services, LLC Kincey Ave.leac, Anaiytical® 9800Huntesvlle, NC128078 100 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Anson LF Stormwater Pace Project No.: 92495552 Sample: BORROW NORTH Lab ID: 92495552004 Collected: 09/15/20 08:16 Received: 09/15/20 12:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 570 CFU/100 mL 1.0 1 09/15/20 15:15 09/16/20 14:36 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Pace Analytical Services -Asheville Total Suspended Solids 17.3 mg/L 4.8 1 09/21/20 11:26 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services - Asheville Chemical Oxygen Demand 41.5 mg/L 25.0 1 09/16/20 16:56 09/16/20 22:06 Sample: BORROW WEST Lab ID: 92495562005 Collected: 09/15/20 08:01 Received: 09/15/20 12:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 260 CFU/100 mL 1.0 1 09/15/20 15:15 09/16/20 14:36 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids ND mg/L 5.7 1 09/21/20 11:27 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand ND mg/L 25.0 1 09/16/20 16:56 09/16/20 22:06 Sample: Outfall 4 (Sed 4) Lab ID: 92495552006 Collected: 09/15/20 00:00 Received: 09/15/20 12:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 8.2 1 09/21/20 08:45 Sample: Outfall 3 (Sed 3) Lab ID: 92495552007 Collected: 09/15/20 00:00 Received: 09/15/20 12:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 8.9 1 09/21/20 08:46 M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 aceAnalytical www.pecolobs.com QUALITY CONTROL DATA Project: Anson LF Stormwater Pace Project No.: 92495552 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 567698 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92495552006, 92495552007 METHOD BLANK: 3008329 Matrix: Water Associated Lab Samples: 92495552006, 92495552007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 09/21/20 08:20 LABORATORY CONTROL SAMPLE: 3008330 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 18.7 94 64-132 MATRIX SPIKE SAMPLE: 3008331 92495552007 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 37 18.9 51 64-132 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 aceAnalytical www.pecolobs.com QUALITY CONTROL DATA Project: Anson LF Stormwater Pace Project No.: 92495552 QC Batch: 566935 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92495552001, 92495552003, 92495552004, 92495552005 METHOD BLANK: 3004314 Matrix: Water Associated Lab Samples: 92495552001, 92495552003, 92495552004, 92495552005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 09/16/20 14:36 SAMPLE DUPLICATE: 3004315 92495552001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 12.0 10.0 18 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 16 laneAnaljftalo www.pacelabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater Pace Project No.: 92495552 QC Batch: 566938 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92495552002 METHOD BLANK: 3004340 Matrix: Water Associated Lab Samples: 92495552002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 09/16/20 14:53 SAMPLE DUPLICATE: 3004341 Parameter Units Fecal Coliforms CFU/100 mL 92495548003 Dup Result Result RPD Qualifiers 1.0 ND Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 16 aceAnalytical www.pecolabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater Pace Project No.: 92495552 QC Batch: 567660 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92495552001, 92495552002, 92495552003, 92495552004, 92495552005 METHOD BLANK: 3008214 Matrix: Water Associated Lab Samples: 92495552001, 92495552002, 92495552003, 92495552004, 92495552005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 09/21/20 11:20 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE & LCSD: 3008215 3008571 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Cone. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Suspended Solids mg/L 250 240 238 96 95 90-110 1 25 SAMPLE DUPLICATE: 3008572 Parameter Total Suspended Solids 92495634001 Dup Units Result Result mg/L 2820 3660 RPD Qualifiers 26 D6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater Pace Project No.: 92495552 QC Batch: 566889 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92495552001, 92495552002, 92495552003, 92495552004, 92495552005 METHOD BLANK: 3004024 Matrix: Water Associated Lab Samples: 92495552001, 92495552002, 92495552003, 92495552004, 92495552005 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 09/16/20 22:03 LABORATORY CONTROL SAMPLE: 3004025 Spike LCS Parameter Units Cone. Result Chemical Oxygen Demand mg/L 750 783 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3004026 3004027 MS MSD 92495454001 Spike Spike MS Parameter Units Result Cone. Cone. Result Chemical Oxygen Demand mg/L 590 100 100 694 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 104 90-110 MSD MS MSD % Rec Result % Rec % Rec Limits RPD Qual 694 104 104 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3004028 3004029 MS MSD 92495454003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua] Chemical Oxygen Demand mg/L 181 100 100 285 290 104 109 90-110 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 16 Pace Analytical Services, LLC aceAnaljdical ® 9800HunteyAve. Suite 100 www.pacela6s.eom 078 (704)875-9092 QUALIFIERS Project: Anson LF Stormwater Pace Project No.: 92495552 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Anson LF Stormwater Pace Project No.: 92495552 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92495552006 Outfall 4 (Sed 4) EPA 1664B 567698 92496652007 Outfall 3 (Sod 3) EPA 1664E 567698 92495552001 OUTFALL 1 SM 9222D-2006 566935 SM 9222D-2006 566936 92495552002 OUTFALL 3 SM 9222D-2006 566938 SM 9222D-2006 566939 92495552003 OUTFALL 4 SM 9222D-2006 566935 SM 9222D-2006 566936 92495552004 BORROW NORTH SM 9222D-2006 566935 SM 9222D-2006 566936 92495652005 BORROW WEST SM 9222D-2006 566935 SM 9222D-2006 566936 92495552001 OUTFALL 1 SM 2540D-2011 567660 92495652002 OUTFALL 3 SM 254OD-2011 567660 92495652003 OUTFALL 4 SM 254OD-2011 567660 92495552004 BORROW NORTH SM 2540D-2011 567660 92495552005 BORROW WEST SM 254OD-2011 567660 92495552001 OUTFALL 1 SM 5220D-2011 566889 SM 5220D-2011 566990 92495552002 OUTFALL 3 SM 5220D-2011 566889 SM 5220D-2011 566990 92495562003 OUTFALL 4 SM 5220D-2011 566889 SM 5220D-2011 566990 92495552004 BORROW NORTH SM 5220D-2011 566889 SM 5220D-2011 566990 92495552005 BORROW WEST SM 5220D-2011 566889 SM 5220D-2011 566990 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/22/2020 05:00 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 16 Document Name: Document Revised: February 7, 2018 Sample Condition Upon RecelptiSCUR) Page 1 of 2 8C2Analytical' Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville [' Raleigh❑ Mechanicsville[] Client Narne: Project #: WO# : 92495552 > S r i,te Ill'IIIllIIIIIIIIIII Courier: ❑Fe Ex ❑UPS ❑LISPS Client ill ❑ Commercial Q ace ❑Other: 82495552 Paciting Material: ®ubbie Wrap [BA6 ble Bags ❑None ❑ Other Thermome,,ter%� 92T061 Type of Ice: (�w� ❑Blue i_yIa Gun10: Cooler Temp (°C): Correction Factor: Add/Subtract (°C) 0,0 Cooler Temp Corrected ("C): USDA Regulated Soil Q!rN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Datef Initials Person Examining Biological Tissue Frozen? Des • ❑No QN [:]None Temp should be above freezing to 6'C ❑Samples out of temp criteria. samples on ice, cooling process has begun Did samples originate from a foreign source ilnternationally, „A e..e _ 01..d7 i-lvo r 1ti. LJYes I_iNo ---� — Comments/Dlstrepancy: Chain of Custody Present? 0Yes ON. ❑N/A 1. Samples Arrived within Hold Time? es DNo ❑N/A 2. Short Hold Time Analysis (02 hr.)? O es ONO —❑N/A 3. Rush Turn Around Time Requested? Yye-s ©No ❑N/A 4. Sufficient Volurne? ❑No ❑N/A 5. Correct Contain ers Used? O ess [:]No ❑N/A 6. -Pace Containers Used? 0 eY�s (:]No ❑N/A Containers Intact? ©Yes ❑Na ❑N/A 7. Dissolved analysis: Samples Field Filtered? []Yes No N/A 8. �6✓ct �1 Sample Labels Match CDC? r j/ ©o ❑N/A 9. -includes Date/Time/ID/Analysis Matrix: vvr Headspace in VOA Vials (>S-6mm)? ❑Yes No ®N/ 10, Trip Blank Present? ❑Yes []NO/A 11. Trip Blank Custody Seals Present? ❑Yes ❑No /N A COMMENTS/SAMPLE DISCREPANCY Field Date Required? ❑Yes ❑No ll itD[f C%u{TF.Ii'1 Cl (/)rtf�s(1 / !,c �� •}+�iif o,/ renal uPrc.s•r 1.1- ti r- 1v6ils FuY G1ll 17p1alYi.(!i Al'P N" lUl C /r 1t h.. fV-^ b�:� - Iv t 1( tV i, l h 1, Lot 10 of soft containers: CLIENT NOTIFICATION/RESOLUTION d D � Q� 1 - rw w s ��� S061 or 4 Ta n�i�nn rTvto . t S �1 � r act � �� � (� tsLrtJ- M Ar- m-ed 1ri aYl Gu P L II v ip- W e Person contacted: 1� _S `lam Date/Time: �( , Date: " I — � Project Manager SCURF Review: �nJ Project Manager SRF Review: t ' { Date: ✓ I'D70 Page 14 of 16 Document Name: Document Revised: February 7, 2019 a C2Afir3i}/lfCc?� Sample Condition Upon Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F•CAR-CS•033•Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/5015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project tt WO# : 92495552 PM: AMB Due Date: 09/22/20 CLIENT: 92—S&ME TN N Z m N a. J {/ryE 'i W Ul > H a J o N L !: ?3 bi C a J o V0I ? W is a d r{ V S ^� S c J {/E� N N v _ a J E tY i m M. 2 N a J ;E N = a O Z = a J yis� N o. m, VI o E —01° �i L 2 GI e ' A E a ' N v u = a 2 L. Z m �i E ¢ J c N N V xa p i a E Q ;; y S ° 9 ys� N E a J o ? tJ 2 z d J C N {�. L1 Z a O > E v _ Q x N Ova a O > E ? Z. ¢ O > E a Z ¢ O > E �. Ln u y ? Y ° j ii T a Z tL N J ryE 'o \ _N a d vi J yE� N V Z a J uE� N '� 2 j E a J Q�E '" ? A c T+ y -J E N m d Z d e E a E y C iii4111 7 a m 7 6 m it m m tit op. m 2- 6 m N 6 m a m 3 l7 a a a a a a e >> o>> to a ��I G 1 2I \N 2 t 2 3 i� Q 5 I 6 7 8 9 10 11 12 \\NN pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 11 Note: whenevertnere is a discrepancy affecting North Carolina compliance samples, a copy of this rdrm wui ee stntto the North Carolina OEHNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 15 of 16 sD OD V 1-, Ih A W N + ITEM # n ° Y n A $ 3 a iK o O O O a o z N � l5 6 ,. O y p A w d O fNil dEr N A 7 n p _ o e fv�' � 0 8 3 � 0 A ��� rn A a o U oo „ 1' `; -'s�fo�affQg y` , e) O .. 5 •e- o O v AAfn m a Q ° iii rva w 1 » a MATRI%CODE (see valid codes to left) # I � g. SAMPLETYPE (G=GRAB C--COMP) m v r. 3'n j 6 c 00m `l 17,X—, m m _ m n D In v�O � ° Z A ..� �, 71 SAMPLE TEMP AT COLLECTION CL p OF CONTAINERS - D gD 3 UnpreServed m: C N 'C^ H2SO4 m ?° Z e O m o HNO3 m 3 c D C HCI m N N g O D �Y NaOH m n Na2S203 y 9 !S1 Methanol m — z c Other m Analyses Test YIN (� 1 g x X X X X COD \ x x x x m z x Fecal Coll (8 Hr Hold) A 3ID N ey-h x x TPH Oil and Grease by 166 K X x X X TSS c c 0 O o• 0 fD C C�. fD P+ V � J \ all m y A '17 m m � TEMP in C Residual Chlorine (YIN) rJ o Received on (YIN) (Y o ) �� usto y Sealed Cooler o YIN � l Samples p nlacl (Y/N) Page 16 of 16 Attachment III — Site SWPPP Map w z Q sty v Z Z V a w¢ '". of L Q¢ z A W Z :ELL,W QW UWC� U �O .lz Z f-lil IJ Z� =�Z dVi aL�i W u VJ � W cJi (ov) (,Wa- (I)o I'M �Y `r X. a ' } 'eV I + 1 1 4,AL lod IL N �., 1 f j r i rtr at n r vi - r• - I, sox-& aoa rep rw a