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HomeMy WebLinkAboutWQ0035748_Complete File - Historical_20150605INTERIM REPORT (DECEMBER 2013 — FEBRUARY 2015) SURFACTANT RECIRCULATION PROJECT BUILDING 1083 MARINE CORPS AIR STATION CHERRY POINT, NORTH CAROLINA NCDENR INCIDENT NO.: 9839 NCDENR GROUNDWATER REMEDIATION PERMIT NO.: WQ0035748 CATLIN PROJECT NO. 210022.08 June 5, 2015 HLRIFA iC Prepared By: CATLIN Engineers and ScierrtisU 220 Old Dairy Road Wilmington, NC 28405 (910) 452-5861 CORPORATE LICENSURE NO. FOR ENGINEERING SERVICES C-0585 CORPORATE GEOLOGY LICENSE NO. C-118 INTERIM REPORT (DECEMBER 2013 - FEBRUARY 2015) SURFACTANT RECIRCULATION PROJECT BUILDING 1083 MARINE CORPS AIR STATION CHERRY POINT, NORTH CAROLINA NCDENR INCIDENT NO.: 9839 NCDENR GROUNDWATER REMEDIATION PERMIT NO.: W00035748 CATLIN PROJECT NO. 210022.08 June 5, 2015 SEAL_ :N'y •. OLOGN�'•' Pre(laracAol SDC Group, Inc. 1 Cherry Point Trailer Building 4376T MCAS Cherry Point, North Carolina 28533 Prepared by: CATLIN Engineers and Scientists P.O. Box 10279 Wilmington, North Carolina 28404-0279 (910) 452-5861 Corporate Licensure Number for Engineering Services — C-0585 TABLE OF CONTENTS PAGE 1.0 INTRODUCTION AND PURPOSE 1 1.1 PROJECT OBJECTIVES 1 1.2 SITE BACKGROUND 1 2.0 SUMMARY OF PREVIOUS SURFACTANT RECIRCULATION EVENTS 2 2.1 AREA A EVENT SUMMARY 3 2.2 AREA B EVENT SUMMARY 4 2.3 AREA C EVENT SUMMARY 5 3.0 SUMMARY OF PREVIOUS GROUNDWATER MONITORING ACTIVITIES 5 4.0 CURRENT GROUNDWATER MONITORING ACTIVITIES 6 5.0 CONCLUSIONS AND RECOMMENDATIONS 7 6.0 LIMITATIONS 8 7.0 REFERENCES 8 TABLES TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA TABLE 2 SITE 1083 GROUNDWATER LABORATORY ANALYTICAL RESULTS - EPA METHOD 602 BY SM 6200B TABLE 3 SITE 1083 GROUNDWATER LABORATORY ANALYTICAL RESULTS - EPA METHOD 610 BY EPA METHOD 625 FIGURES FIGURE 1 GENERAL VICINITY MAP FIGURE 2 SITE MAP WITH INJECTION/EXTRACTION AREAS FIGURE 3A FREE PRODUCT PLUME MAP AS OF AUGUST 2014 FIGURE 313 FREE PRODUCT PLUME MAP AS OF FEBRUARY 2015 FIGURE 4 EPA METHOD 602 BY SM 6200B COLORIMETRY AND PLUME IN EXCESS OF 2L AS OF AUGUST 2014 FIGURE 5 EPA METHOD 610 BY EPA METHOD 625 COLORIMETRY AND PLUME IN EXCESS OF 2L AS OF AUGUST 2014 APPENDICES APPENDIX A LABORATORY ANALYTICAL REPORTS APPENDIX B WELL ABANDONMENT RECORDS, WELL LOGS AND WELL CONSTRUCTION RECORDS DOD; 210022.08_1083_lnterim_Report Dec2013-Feb2015_FlNAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 June 2015 INTERIM REPORT (DECEMBER 2013 — FEBRUARY 2015) SURFACTANT RECIRCULATION PROJECT Building 1083 Marine Corps Air Station Cherry Point, North Carolina June 5, 2015 1.0 INTRODUCTION AND PURPOSE The purpose of this annual report is to summarize the year (December 2013 — February 2015) of events and activities associated with the Building 1083 Surfactant Recirculation Project as outlined in the Workplan; Building 1083 Remedial Implementation, Mobile Surfactant Recirculation submitted by CATLIN Engineers and Scientists (CATLIN) on July 30, 2012, and under the guidance on the Groundwater Remediation Permit Number WQ0035748 awarded by the North Carolina Department of Environment and Natural Resources, Division of Water Quality (NCDENR, DWQ). Please note, no surfactant recirculation activities were conducted during the time period of December 2013 through February 2015. However, site monitoring/sampling was conducted under another project during this time frame; therefore, this data is reported within. 1.1 PROJECT OBJECTIVES Project objectives are to address the continual presence of free -phase product (Jet Propulsion [JP]-5 aviation fuel) and dissolved petroleum groundwater contamination identified in several groundwater monitoring wells across the site, located at the Marine Corps Air Station (MCAS), Cherry Point, North Carolina. The objective of the Surfactant Recirculation Project is to eliminate free -phase product and reduce groundwater contamination, in order to reduce the site risk classification to Low. 1.2 SITE BACKGROUND The site is located at the MCAS, Cherry Point, North Carolina (see Figure 1). The project site is located within the Officer's housing area (see Figure 2). An inactive pipeline (Marine Transfer Pipeline (MTP), formerly used to transfer aviation gasoline and various grades of JP Fuel, transects the project site and is believed to be the primary source of contamination. The pipeline was taken out of service in January 1993. A site assessment conducted in June 1993 revealed the presence of free - phase product at the project site and for that reason; an active recovery system was installed in February 1994. The completed free -phase DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 1 June 2015 product/groundwater recovery system consisted of approximately 36 product recovery wells containing controllerless, pneumatic, total fluid recovery pumps. A horizontal Soil Vapor Extraction (SVE) system was installed as part of the overall active recovery system, in order to address the vadose zone soil contamination. The remediation system operated from startup in 1994 through 2012; however, over the years diminishing amounts of free -phase product were recovered. Modifications were made to the remediation system in 2008 and 2009 to address iron fouling and to optimize remedial activities. Since that time, CATLIN provided continual optimization through the Operation and Maintenance (O&M) Program. However, ultimately the on -site remediation system was shutdown permanently on August 13, 2012. In September 2010, an in -situ free -phase product investigation was conducted. This investigation revealed free -phase product remained present in three small areas across the site that were not being influenced by the current remedial system. Therefore, a Corrective Action Plan Addendum (CAPA) was submitted in August 2011 and was subsequently approved by the NCDENR, which recommended surfactant injection/re-circulation as an alternative approach to enhance free -phase product recovery efforts at this site. In order to implement this approach, a Non -Discharge Permit was required. Therefore, a Non -Discharge Permit Application was submitted to the NCDENR in January 2012 and approved on April 6, 2012. CATLIN completed a Workplan in July 2012 to implement the approved remediation technology that contains the following: • Eighteen 4-inch diameter, Type 51 injection/extraction wells 25 feet deep (41 PR200 - 41 PR204, 41 PR210 - 41 PR221, and 41 PR230) installed in Areas A, B, and C as depicted on Figure 2. • A trailer mounted mobile recirculation system that includes five well pumps, a holding tank, six carbon filters, four particulate filters, two mixing tanks, a transfer and injection pump for recirculation activities. 2.0 SUMMARY OF PREVIOUS SURFACTANT RECIRCULATION EVENTS The goal of the surfactant recirculation events was to remove residual free -phase product from the subsurface to a thickness of less than 0.01 feet. These surfactant recirculation events focused on Areas A, B and C at the Building 1083 site. This technology generally consisted of the extraction and treatment of site groundwater, mixing the treated groundwater with a surfactant solution (PetroSolVTM) and re- injecting the mixture into wells targeted for treatment. Extraction and injection activities occurred simultaneously in select wells in order to circulate PetroSOIVTM solution within the subsurface. Manual surging was performed at the injection wells intermittently, throughout the recirculation process to enhance the in -situ mixing of the surfactant solution and to increase the radial influence. Chase water was also injected following each surfactant injection phase to facilitate radial influence into the formation. The surfactant solution, once flushed into the aquifer, facilitates contaminant removal by increasing the solubility of free -phase product through the DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 2 June 2015 formation of micro -emulsions and reduces the interfacial tension and adsorption forces between the free -phase product and the soil grains, thus mobilizing the residual free -phase product for easy removal. Recirculation events were followed by a multiple day total fluid recovery and disposal event. These events were designed to remove dissolved and mobilized free -phase product from the target area. Following the recovery and disposal event, a nutrient/bacteria injection event was conducted in order to promote aggressive biological degradation of residual dissolved -phase constituents remaining in the surrounding soil/groundwater formation following the surfactant recirculation activities. A solution of EZT-A2TM bacteria and CBNTm nutrients was mixed with potable water and injected into the targeted wells. Area specific surfactant recirculation events were developed within the aforementioned Workplan based on the most recent free -phase product gauging data available. Each event presented implementation activities in a series of phases, specifying which wells were to be used as extraction wells and which wells were to be used as injection wells in each phase. Specified volumes of surfactant solution were injected into targeted wells during each phase. Intermittent surging and chase water injection activities were also defined. The phases were designed to adequately introduce calculated volumes of surfactant solution into targeted wells while extracting from strategic adjacent wells; in order to maintain hydraulic control of the system and to enhance the radial influence of the targeted area. During each new phase, the configuration of injection wells, extraction wells and required volumes of surfactant solution to be injected were defined. Each phase modification was designed to optimize the surfactant recirculation activities, while conforming to all permit requirements. Due to the specific nature of each designed recirculation event, the Workplan specified that recirculation strategies could be adjusted accordingly based on changing site conditions. The new event strategies were developed to more effectively focus remedial efforts on specific wells with remaining free -phase product. Initially, there were three recirculation events planned for Area A and two recirculation events planned for Areas B and C. Following Event 1 at Areas A, B, and C, Event 2 plans were adjusted for Areas A, B and C reducing the number of targeted wells and/or increasing surfactant and nutrient solution volumes per well. Following Event 2, it was determined that resources for Event 3 would be spilt between Area A and B to target remaining wells containing free -phase product. A summary of each Area's events has been provided below. Details of these surfactant activities were provided in the previous Annual Report (August 2012 — November 2013) Surfactant Recirculation Project Building 1083, dated December 17, 2013 by CATLIN. 2.1 AREA A EVENT SUMMARY Three Surfactant Recirculation Events, averaging six phases per event, were conducted in Area A. The three events were conducted as follows: DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 3 June 2015 • Event 1 - August 20 to August 29, 2012 • Event 2 - January 3 to January 24, 2013 • Event 3 - July 16 to August 16, 2013. All three events focused remedial efforts on wells 41 GW 106, 41 PR200, 41 PR201, 41 PR202, 41 PR203, 41 PR204 and 41 PR77. During the second event at Area A, wells 41 GW 106, 41 PR201, 41 PR202, and 41 PR77 were specifically targeted for surfactant injection and during the third event at Area A, wells 41 GW 106 and 41 PR202 were specifically targeted for injection. Over the course of these three events a combined total of 11,042 gallons of groundwater was extracted, treated and mixed with 3% surfactant solution and re -injected into the targeted wells. A combined total of 13,899 gallons of surfactant solution and chase water was injected into targeted wells at a pressure ranging from 0-5 pounds per square inch (psi) during the first event, 0-2 psi during the second and 0-3 psi during the third event. The additional injected volume consisted of clean potable water. Manual surging was performed between each phase during every event. Over the course of these three events a combined total of 16,850 gallons of contaminated water was removed from Area A during the final extraction and disposed of at the Air Station's Waste Water Treatment Plant (WWTP). Additionally, during the course of these three events, a combined total of 3,712 gallons of nutrients and bacteria solution was injected into targeted Area A wells at a pressure ranging from 0-2 psi. 2.2 AREA B EVENT SUMMARY Three Surfactant Recirculation Events, averaging seven phases per event, were conducted in Area B. The three events were conducted as follows: • Event 1 - September 10 to October 1, 2012 • Event 2 - January 30 to February 23, 2013 • Event 3 - August 23 to October 16, 2013. All three events focused remedial efforts on wells 41 GW02, 41 GW03, 41 GW06, 41 PR82, 41 PR210, 41 PR211, 41 PR212, 41 PR213, 41 PR214, 41 PR215, 41 PR216, 41 PR217, 41 PR218, 41 PR219, 41 PR220, and 41 PR221. During the second event at Area B, wells 41 GW02, 41 GW03, 41 GW06, 41 PR214, 41 PR216, 41 PR218 and 41 PR219 were specifically targeted for surfactant injection and during the third event, wells 41 GW03, 41 PR213, 41 PR216, 41 PR217, 41 PR218, 41 PR220 and 41 PR221 were specifically targeted for injection. Over the course of these three events, a combined total of 34,034 gallons of groundwater was extracted, treated and mixed with 3% surfactant solution and re -injected into the targeted wells. A combined total of 37,850 gallons of surfactant solution and chase water was injected into targeted wells at a pressure ranging from 0-8 psi during the first event and 0-2 psi during the second and third events. The additional injected volume consisted of clean potable water. Manual surging was performed between each phase during every event. Over the course of these three DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 4 June 2015 events a combined total of 27,642 gallons of contaminated water was removed from Area B during the final extraction and disposed of at the Air Station's WWTP. Additionally, during the course of these three events, a combined total of 11,220 gallons of nutrients and bacteria solution was injected into targeted Area B wells at a pressure ranging from 0-2 psi. 2.3 AREA C EVENT SUMMARY Two Surfactant Recirculation Events, the first spanning two phases and the second five phases, were conducted in Area C. The two events were conducted as follows: • Event 1 - October 23 to October 26, 2012 • Event 2 - February 27 to March 6, 2013. Both events focused remedial efforts on wells 41 GW25, 41 PR101 and 41 PR230. Over the course of these two events, a combined total of 4,853 gallons of groundwater was extracted, treated and mixed with 3% surfactant solution and re -injected into the targeted wells. A combined total of 4,205 gallons of surfactant solution and chase water was injected into targeted wells at a pressure ranging from 0-3 psi during the first event and 1-3 psi during the second event. The additional injected volume consisted of clean potable water. Manual surging was performed between each phase during every event. Over the course of these two events a combined total of 8,803 gallons of contaminated water was removed from Area C during the final extraction and disposed of at the Air Station's WWTP. Additionally, during the course of these two events, a combined total of 2,107 gallons of nutrients and bacteria solution was injected into targeted Area C wells at a pressure ranging from 0-2 psi. 3.0 SUMMARY OF PREVIOUS GROUNDWATER MONITORING ACTIVITIES Groundwater and free -phase product gauging activities have historically been performed on a monthly basis and have continued on a monthly basis as part of the MCAS Cherry Point Closure and Monitoring Program (CAMP). In addition, select groundwater monitoring wells on site have historically been sampled on a semi- annual basis (typically February and August) as part of the MCAS Cherry Point CAMP. The August 2012 CAMP sampling event was utilized as the baseline groundwater sampling event for the selected monitoring wells, prior to commencement of the surfactant recirculation activities on August 20, 2012. The November 2013 sampling event was performed at the conclusion of previously described surfactant recirculation events. Please note, the previously submitted Annual Report provides details on the results of the August 2012 and November 2013 sampling events, below is a brief summary: Groundwater Gauging In August 2012, prior to surfactant recirculation activities, wells within Areas A, B, and C contained measurable thicknesses of free -phase product up to 0.38 feet. DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 5 June 2015 Gauging data from November 2013 indicated a significant reduction in the extent and thicknesses of free -phase product within Areas A, B and C as 0.06 feet of free - phase product was the largest thickness measured. Groundwater flow was generally toward the northeast during both events. Groundwater Sampling The groundwater sample analytical data indicated that EPA Method 602, 625, MADEP VPH/EPH compounds were detected above the North Carolina 2L Groundwater Quality Standards (2L GWQS) during the August 2012 and November 2013 groundwater monitoring events. These contaminant concentrations appeared to have remained consistent during recirculation activities. 1,2-Dibromoethane (EDB) by EPA Method 504.1 was not detected in the August 2012 or November 2013 sampling events. Concentrations of TKN, Ammonia Nitrogen, Nitrate Nitrogen and Nitrite Nitrogen increased from August 2012 to November 2013, due to injection of the solution of EZT-A2Tm bacteria and CBNTm nutrients into targeted monitoring wells, which contain nitrogen compounds. This solution is designed to promote aggressive biological degradation of residual dissolved -phase constituents remaining in the surrounding soil/groundwater formation following surfactant recirculation activities and these compounds are expected to be biologically degraded over time. CTAS was detected during the October 2012 and January 2013 sampling events at relatively low concentrations. The CTAS results are used to determine the presence of the surfactant solution remaining in the subsurface as a quantifier of final extraction phase completions. 4.0 CURRENT GROUNDWATER MONITORING ACTIVITIES As previously stated, no surfactant related activities were conducted during the time period of December 2013 through February 2015. However, groundwater and free - phase product gauging activities were performed on a monthly basis as part of the MCAS Cherry Point CAMP. Also, select groundwater monitoring wells on site were also sampled in August 2014 as part of the MCAS Cherry Point CAMP. Groundwater Gauging Groundwater gauging data from August 2014 and February 2015 was used to calculate groundwater elevations and produce groundwater contours. Groundwater flow direction is towards the northeast, as indicated on Figures 3A and 3B, respectively. In August 2014, wells within Areas A and B contained measureable thicknesses of free -phase product up to 0.5 feet, while Area C revealed no measureable product thicknesses. Gauging data from February 2015 indicates a slight increase in the extent and/or thicknesses of free -phase product measured in Areas A and B, while Area C remained product free. Monthly gauging data from December 2013 through February 2015 is referenced in Table 1. DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 6 June 2015 Groundwater Sampling The Building 1083 semi-annual groundwater sampling event was conducted on August 13, 2014, and samples were analyzed for EPA Method 602 by SM6200B and EPA Method 610 by EPA Method 625 compounds. One EPA Method 602 compound (Benzene) was detected at concentrations exceeding the 2L GWQS in five monitoring wells (See Figure 4). The EPA Method 625 compound Naphthalene was revealed in twelve monitoring wells at concentrations exceeding the 2L GWQS, in addition to 2-Methyl naphthalene, which was present in four monitoring wells at concentrations exceeding the 2L GWQS (See Figure 5). See Table 2 and Table 3 for a summary of analytical results by method. The laboratory analytical report and chain of custody documentation is provided in Appendix A. Monitoring Well Replacement On December 9 and 10, 2014, CATLIN personnel were on -site to abandon two existing monitoring wells (41 GW02 and 41 GW03) within Area B that had been used for surfactant recirculation and were in need of replacement. These two wells were 2-inch diameter monitoring wells that were replaced with 4-inch diameter wells. Wells 41 GW02 and 41 GW03 were properly abandoned by a North Carolina Licensed Driller. Also, the two replacement wells (41 GW02R and 41 GW03R) were installed by a North Carolina Licensed Driller. These replacement wells will be utilized during an additional round of surfactant recirculation in the nearfuture. Well abandonment records, well logs and well construction records are located in Appendix B. 5.0 CONCLUSIONS AND RECOMMENDATIONS A review of the monthly gauging data from December 2013 through February 2015 indicates an increase in the thickness and extent of free -phase product in Areas A and B. It is suspected that the previously conducted surfactant recirculation activities in these areas liberated free -phase product that was trapped in the subsurface and now has been mobilized and is accumulating in the recovery wells in these areas. Free -phase product has not returned to the wells in Area C since the last surfactant recirculation event (March 2013). Dissolved -phase contaminant concentrations from the August 2014 sampling event remained similar to the historical dissolved -phase contamination levels. Based on the recurrence of free -phase product at Areas A and B, CATLIN has recommended additional surfactant recirculation activities. An additional surfactant recirculation event is planned to begin at Area A in early May 2015 followed by an additional event at Area B. The information/data collected during these recirculation events and the subsequent gauging/sampling data will be documented in the next Annual Report per the requirements of Groundwater Remediation Permit Number WQ0035748. DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 7 June 2015 6.0 LIMITATIONS The groundwater samples analyzed as part of this investigation only provide isolated data points and may not represent conditions at every location in the project area. Analyses and conclusions of this report, being based on interpolation between data points at the project area, may not be completely representative of all site conditions. Conclusions and recommendations of this investigation and report are based on the best available data in an effort to comply with current regulatory requirements. 7.0 REFERENCES CATLIN Engineers and Scientists, Corrective Action Plan Addendum, Building 1083, Marine Corps Air Station, Cherry Point, NC, dated August 3, 2011. CATLIN Engineers and Scientists, In -Situ Free -Phase Product Assessment at Building 1083, Marine Corps Air Station, Cherry Point, North Carolina, September 22, 2011. CATLIN Engineers and Scientists, Base Wide and Site Specific (Building 1083) Non -Discharge Permit Application for MCAS, Cherry Point, North Carolina, January 2, 2012 CATLIN Engineers and Scientists, Workplan Building 1083 Remedial Implementation, Marine Corps Air Station, Cherry Point, NC, dated July 30, 2012. CATLIN Engineers and Scientists, Annual Report (August 2012 — November 2013) Surfactant Recirculation Project Building 1083, Marine Corps Air Station, Cherry Point, NC, dated December 17, 2013. North Carolina Department of Environment and Natural Resources, Division of Water Quality, Groundwater Remediation Permit Number WQ0035748. Building 1083 Area Remediation Sites, Craven County. Originally Issued April 6, 2012. Renewed on November 8, 2013. DOD; 210022.08_1083_Interim_Report Dec2013-Feb2015_F1NAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 8 June 2015 TABLES DOD; 210022.08_1083_Interim Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 June 2015 TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41GW02 12/3/2013 16.09 -0.6 11.63 NMT 12.23 4.46 41GW02 1/7/2014 16.09 -0.6 11.35 NMT 11.95 4.74 41GW02 2/4/2014 16.09 -0.6 10.26 0.03 10.86 5.80 41GW02 3/3/2014 16.09 -0.6 10.32 0.03 10.92 5.74 41GW02 4/7/2014 16.09 -0.6 10.07 0.04 10.67 5.98 41GW02 5/1/2014 16.09 -0.6 9.93 0.03 10.53 6.13 41GW02 6/2/2014 16.09 -0.6 11.48 NMT 12.08 4.61 41GW02 7/1/2014 16.09 -0.6 10.3 0.02 10.9 5.77 41GW02 8/13/2014 16.09 -0.6 9.09 0.04 9.69 6.96 41GW02 9/15/2014 16.09 -0.6 9.59 0.05 10.19 6.45 41GW02 10/1/2014 16.09 -0.6 9.53 0.07 10.13 6.49 41GW02 11/5/2014 16.09 -0.6 11.35 0.02 11.95 4.72 41GW02 12/1/2014 16.09 -0.6 10.38 0.03 10.98 5.68 41GW02R 1/2/2015 14.87 -0.03 11.72 NMT 11.75 3.15 41GW02R 2/2/2015 14.87 -0.03 11.58 NMT 11.61 3.29 41GW03 12/3/2013 16.18 -0.33 12.12 0.02 12.45 4.04 41GW03 1/7/2014 16.18 -0.33 11.79 0.03 12.12 4.36 41GW03 2/4/2014 16.18 -0.33 10.79 NMT 11.12 5.39 41GW03 3/3/2014 16.18 -0.33 10.9 0.05 11.23 5.23 41GW03 4/7/2014 16.18 -0.33 10.64 0.01 10.97 5.53 41GW03 5/1/2014 16.18 -0.33 9.42 0.04 9.75 6.72 41GW03 6/2/2014 16.18 -0.33 12.05 0.03 12.38 4.10 41GW03 7/1/2014 16.18 -0.33 10.83 NMT 11.16 5.35 41GW03 8/13/2014 16.18 -0.33 9.69 0.05 10.02 6.44 41GW03 9/15/2014 16.18 -0.33 9.01 0.12 9.34 7.05 41GW03 10/1/2014 16.18 -0.33 11.37 0.12 11.7 4.69 41GW03 11/5/2014 16.18 -0.33 11.92 0.13 12.25 4.13 41GW03 12/1/2014 16.18 -0.33 10.9 0.10 11.23 5.18 41GW03R 1/2/2015 14.93 0.03 12.4 NMT 12.37 2.53 41GW03R 2/2/2015 14.93 0.03 10.86 NMT 10.83 4.07 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 1 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41GW05 12/3/2013 16.68 -0.2 13 0.11 13.2 3.57 41GW05 1/7/2014 16.68 -0.2 12.72 0.10 12.92 3.86 41GW05 2/4/2014 16.68 -0.2 11.7 0.10 11.9 4.88 41GW05 3/3/2014 16.68 -0.2 11.61 0.09 11.81 4.98 41GW05 4/7/2014 16.68 -0.2 10.68 0.09 10.88 5.91 41GW05 5/1/2014 16.68 -0.2 11.44 0.10 11.64 5.14 41GW05 6/2/2014 16.68 -0.2 12.75 NMT 12.95 3.93 41GW05 7/1/2014 16.68 -0.2 11.76 NMT 11.96 4.92 41GW05 8/13/2014 16.68 -0.2 10.81 NMT 11.01 5.87 41GW05 9/15/2014 16.68 -0.2 11.68 0.02 11.88 4.98 41GW05 10/1/2014 16.68 -0.2 11.31 0.01 11.51 5.36 41GW05 11/5/2014 16.68 -0.2 12.54 0.01 12.74 4.13 41GW05 12/1/2014 16.68 -0.2 12.06 0.03 12.26 4.59 41GW05 1/2/2015 16.68 -0.2 11.87 0.04 12.07 4.77 41GW05 2/2/2015 16.68 -0.2 10.72 0.05 10.92 5.91 41GW06 12/3/2013 16.68 -0.48 13.08 NMT 13.56 3.60 41GW06 1/7/2014 16.68 -0.48 12.6 NMT 13.08 4.08 41GW06 2/4/2014 16.68 -0.48 11.51 NMT 11.99 5.17 41GW06 3/3/2014 16.68 -0.48 11.66 NMT 12.14 5.02 41GW06 4/7/2014 16.68 -0.48 11.69 NMT 12.17 4.99 41GW06 5/1/2014 16.68 -0.48 11.21 NMT 11.69 5.47 41GW06 6/2/2014 16.68 -0.48 13.08 NMT 13.56 3.60 41GW06 7/1/2014 16.68 -0.48 11.98 NMT 12.46 4.70 41GW06 8/13/2014 16.68 -0.48 10.31 NMT 10.79 6.37 41GW06 9/15/2014 16.68 -0.48 10.25 NMT 10.73 6.43 41GW06 10/1/2014 16.68 -0.48 11.57 NMT 12.05 5.11 41GW06 11/5/2014 16.68 -0.48 13.09 NMT 13.57 3.59 41GW06 12/1/2014 16.68 -0.48 11.95 NMT 12.43 4.73 41GW06 1/2/2015 16.68 -0.48 11.75 NMT 12.23 4.93 41GW06 2/2/2015 16.68 -0.48 10.68 NMT 11.16 6.00 41GW21 8/13/2014 17.03 -0.28 10.79 NMT 11.07 6.24 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 2 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41GW22 8/13/2014 15.48 -0.34 10.5 NMT 10.84 4.98 41GW23 8/13/2014 14.82 -0.35 8.3 NMT 8.65 6.52 41GW25 12/3/2013 17.12 -0.3 12.83 NMT 13.13 4.29 41GW25 1/7/2014 17.12 -0.3 12.53 NMT 12.83 4.59 41GW25 2/4/2014 17.12 -0.3 11.95 NMT 12.25 5.17 41GW25 3/3/2014 17.12 -0.3 11.28 NMT 11.58 5.84 41GW25 4/7/2014 17.12 -0.3 10.85 NMT 11.15 6.27 41GW25 5/1/2014 17.12 -0.3 9.49 NMT 9.79 7.63 41GW25 6/2/2014 17.12 -0.3 11.55 NMT 11.85 5.57 41GW25 7/1/2014 17.12 -0.3 11.63 NMT 11.93 5.49 41GW25 8/13/2014 17.12 -0.3 10.5 NMT 10.8 6.62 41GW25 9/15/2014 17.12 -0.3 10.43 NMT 10.73 6.69 41GW25 10/1/2014 17.12 -0.3 10.53 NMT 10.83 6.59 41GW25 11/5/2014 17.12 -0.3 11.42 NMT 11.72 5.70 41GW25 12/1/2014 17.12 -0.3 11.61 NMT 11.91 5.51 41GW25 1/2/2015 17.12 -0.3 11.34 NMT 11.64 5.78 41GW25 2/2/2015 17.12 -0.3 10.21 NMT 10.51 6.91 41GW26 8/13/2014 14.98 3.33 6.07 NMT 2.74 8.91 41GW27 8/13/2014 15.02 0.52 6.95 NMT 6.43 8.07 41GW28 8/13/2014 12.9 2.45 8.79 NMT 6.34 4.11 41GW29 8/13/2014 11.21 2.23 6.46 NMT 4.23 4.75 41GW30 8/13/2014 15.73 -0.35 10.26 NMT 10.61 5.47 41GW31 8/13/2014 13.61 -0.3 9.51 NMT 9.81 4.10 41GW32 8/13/2014 15.46 -0.55 9.22 NMT 9.77 6.24 41GW33 8/13/2014 13.7 -0.29 9.75 NMT 10.04 3.95 41GW34 8/13/2014 15.88 -0.29 9.16 NMT 9.45 6.72 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 3 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41GW36 12/3/2013 17.13 -0.75 11.97 NMT 12.72 5.16 41GW36 1/7/2014 17.13 -0.75 11.57 NMT 12.32 5.56 41GW36 2/4/2014 17.13 -0.75 10.74 NMT 11.49 6.39 41GW36 3/3/2014 17.13 -0.75 10.6 NMT 11.35 6.53 41GW36 4/7/2014 17.13 -0.75 10.32 NMT 11.07 6.81 41GW36 5/1/2014 17.13 -0.75 9.93 NMT 10.68 7.20 41GW36 6/2/2014 17.13 -0.75 11.46 NMT 12.21 5.67 41GW36 7/1/2014 17.13 -0.75 10.7 NMT 11.45 6.43 41GW36 8/13/2014 17.13 -0.75 8.95 NMT 9.7 8.18 41GW36 9/15/2014 17.13 -0.75 9.31 NMT 10.06 7.82 41GW36 10/1/2014 17.13 -0.75 9.99 NMT 10.74 7.14 41GW36 11/5/2014 17.13 -0.75 11.46 NMT 12.21 5.67 41GW36 12/1/2014 17.13 -0.75 10.78 NMT 11.53 6.35 41GW36 1/2/2015 17.13 -0.75 9.59 NMT 10.34 7.54 41GW36 2/2/2015 17.13 -0.75 9.38 NMT 10.13 7.75 41GW37 8/13/2014 9.79 -1.59 4.27 NMT 5.86 5.52 41GW40 8/13/2014 13.46 -0.32 9.82 NMT 10.14 3.64 41GW41 8/13/2014 15.63 -0.34 11.86 NMT 12.2 3.77 41GW42 8/13/2014 15.59 -0.38 9.04 NMT 9.42 6.55 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 4 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41 GW43 12/3/2013 16.76 -0.71 11.48 0.06 12.19 5.22 41 GW43 1/7/2014 16.76 -0.71 11.18 0.05 11.89 5.53 41 GW43 2/4/2014 16.76 -0.71 10.55 0.07 11.26 6.14 41 GW43 3/3/2014 16.76 -0.71 9.81 NMT 10.52 6.95 41 GW43 4/7/2014 16.76 -0.71 9.3 NMT 10.01 7.46 41 GW43 5/1/2014 16.76 -0.71 8.94 0.01 9.65 7.81 41 GW43 6/2/2014 16.76 -0.71 10.26 NMT 10.97 6.50 41 GW43 7/1/2014 16.76 -0.71 10.28 NMT 10.99 6.48 41 GW43 8/13/2014 16.76 -0.71 9.52 NMT 10.23 7.24 41 GW43 9/15/2014 16.76 -0.71 7.99 NMT 8.7 8.77 41 GW43 10/1/2014 16.76 -0.71 9.13 NMT 9.84 7.63 41 GW43 11/5/2014 16.76 -0.71 10.01 NMT 10.72 6.75 41 GW43 12/1/2014 16.76 -0.71 10.26 NMT 10.97 6.50 41 GW43 1/2/2015 16.76 -0.71 10 NMT 10.71 6.76 41 GW43 2/2/2015 16.76 -0.71 8.64 NMT 9.35 8.12 41GW44 8/13/2014 16.72 -0.52 9.82 NMT 10.34 6.90 41GW45 8/13/2014 15.8 3.05 10.88 NMT 7.83 4.92 41GW46 8/13/2014 15.7 3.34 7.33 NMT 3.99 8.37 41GW62 8/13/2014 16.83 -0.39 10.62 NMT 11.01 6.21 41GW63 8/13/2014 16.55 -0.48 9.71 NMT 10.19 6.84 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 5 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41GW64 12/3/2013 15.41 -0.26 11.05 NMT 11.31 4.36 41GW64 1/7/2014 15.41 -0.26 10.75 NMT 11.01 4.66 41GW64 2/4/2014 15.41 -0.26 10.36 NMT 10.62 5.05 41GW64 3/3/2014 15.41 -0.26 9.55 NMT 9.81 5.86 41GW64 4/7/2014 15.41 -0.26 9.05 NMT 9.31 6.36 41GW64 5/1/2014 15.41 -0.26 9.03 NMT 9.29 6.38 41GW64 6/2/2014 15.41 -0.26 9.76 NMT 10.02 5.65 41GW64 7/1/2014 15.41 -0.26 9.87 NMT 10.13 5.54 41GW64 8/13/2014 15.41 -0.26 9.41 NMT 9.67 6.00 41GW64 9/15/2014 15.41 -0.26 8.86 NMT 9.12 6.55 41GW64 10/1/2014 15.41 -0.26 8.87 NMT 9.13 6.54 41GW64 11/5/2014 15.41 -0.26 9.64 NMT 9.9 5.77 41GW64 12/1/2014 15.41 -0.26 9.8 NMT 10.06 5.61 41GW64 1/2/2015 15.41 -0.26 9.42 NMT 9.68 5.99 41GW64 2/2/2015 15.41 -0.26 8.7 NMT 8.96 6.71 41GW65 8/13/2014 14.11 -0.3 5.67 NMT 5.97 8.44 41GW66 8/13/2014 13.54 -0.3 7.19 NMT 7.49 6.35 41GW102 8/13/2014 16.94 -0.27 10.93 NMT 11.2 6.01 41GW103 8/13/2014 16.98 -0.23 10.38 NMT 10.61 6.60 41GW104 8/13/2014 16.26 -0.73 9.58 NMT 10.31 6.68 41GW105 8/13/2014 16.75 -0.68 9.94 NMT 10.62 6.81 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 6 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41GW106 12/3/2013 17.09 -0.37 12.22 NMT 12.59 4.87 41GW106 1/7/2014 17.09 -0.37 11.96 NMT 12.33 5.13 41GW106 2/4/2014 17.09 -0.37 11.08 NMT 11.45 6.01 41GW106 3/3/2014 17.09 -0.37 10.98 NMT 11.35 6.11 41GW106 4/7/2014 17.09 -0.37 10.32 NMT 10.69 6.77 41GW106 5/1/2014 17.09 -0.37 9.98 NMT 10.35 7.11 41GW106 6/2/2014 17.09 -0.37 11.06 NMT 11.43 6.03 41GW106 7/1/2014 17.09 -0.37 11.38 NMT 11.75 5.71 41GW106 8/13/2014 17.09 -0.37 10.2 NMT 10.57 6.89 41GW106 9/15/2014 17.09 -0.37 10.19 NMT 10.56 6.90 41GW106 10/1/2014 17.09 -0.37 10.55 NMT 10.92 6.54 41GW106 11/5/2014 17.09 -0.37 11.33 NMT 11.7 5.76 41GW106 12/1 /2014 17.09 -0.37 11.44 0.02 11.81 5.63 41GW106 1 /2/2015 17.09 -0.37 11.22 0.02 11.59 5.85 41GW106 2/2/2015 17.09 -0.37 10.05 NMT 10.42 7.04 41GW107 12/3/2013 17.06 -0.54 13.83 NMT 14.37 3.23 41GW107 8/13/2014 17.06 -0.54 12 NMT 12.54 5.06 41GW108 8/13/2014 16.7 -0.2 13.39 NMT 13.59 3.31 41GW111 12/3/2013 16.85 -0.59 11.29 NMT 11.88 5.56 41GW111 8/13/2014 16.85 -0.59 9.18 NMT 9.77 7.67 41GW112 12/3/2013 17.21 -0.16 12.83 NMT 12.99 4.38 41GW112 8/13/2014 17.21 -0.16 10.3 NMT 10.46 6.91 41GW113 8/13/2014 15.17 -0.24 8.22 NMT 8.46 6.95 41GW114 8/13/2014 15.45 -0.14 9.85 NMT 9.99 5.60 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 7 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR67 12/3/2013 14.94 -1.62 10.98 NMT 12.6 3.96 41PR67 1/8/2014 14.94 -1.62 10.95 NMT 12.57 3.99 41PR67 2/4/2014 14.94 -1.62 10 NMT 11.62 4.94 41PR67 3/3/2014 14.94 -1.62 9.38 NMT 11 5.56 41PR67 4/7/2014 14.94 -1.62 8.89 NMT 10.51 6.05 41PR67 5/1/2014 14.94 -1.62 8.19 NMT 9.81 6.75 41PR67 6/2/2014 14.94 -1.62 9.68 NMT 11.3 5.26 41PR67 7/1/2014 14.94 -1.62 9.73 NMT 11.35 5.21 41PR67 8/13/2014 14.94 -1.62 8.03 NMT 9.65 6.91 41PR67 9/15/2014 14.94 -1.62 8.05 NMT 9.67 6.89 41PR67 10/1/2014 14.94 -1.62 8.59 NMT 10.21 6.35 41PR67 11/5/2014 14.94 -1.62 9.54 NMT 11.16 5.40 41PR67 12/1/2014 14.94 -1.62 9.68 NMT 11.3 5.26 41PR67 1/2/2015 14.94 -1.62 9.31 NMT 10.93 5.63 41PR67 2/2/2015 14.94 -1.62 7.86 NMT 9.48 7.08 41 PR68 12/3/2013 15.86 -1.32 11.39 0.04 12.71 4.43 41PR68 1/8/2014 15.86 -1.32 11.1 NMT 12.42 4.76 41PR68 2/4/2014 15.86 -1.32 10.55 NMT 11.87 5.31 41PR68 3/3/2014 15.86 -1.32 9.88 NMT 11.2 5.98 41PR68 4/7/2014 15.86 -1.32 9.4 NMT 10.72 6.46 41PR68 5/1/2014 15.86 -1.32 10.09 NMT 11.41 5.77 41PR68 6/2/2014 15.86 -1.32 10.1 NMT 11.42 5.76 41PR68 7/1/2014 15.86 -1.32 10.17 NMT 11.49 5.69 41PR68 8/13/2014 15.86 -1.32 8.9 NMT 10.22 6.96 41PR68 9/15/2014 15.86 -1.32 8.97 NMT 10.29 6.89 41PR68 10/1/2014 15.86 -1.32 9.1 NMT 10.42 6.76 41PR68 11/5/2014 15.86 -1.32 9.92 NMT 11.24 5.94 41PR68 12/1/2014 15.86 -1.32 10.17 NMT 11.49 5.69 41PR68 1/2/2015 15.86 -1.32 9.87 NMT 11.19 5.99 41PR68 2/2/2015 15.86 -1.32 8.72 NMT 10.04 7.14 41PR69 8/13/2014 16.65 -0.78 10.01 NMT 10.79 6.64 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 8 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR70 8/13/2014 16.55 -0.52 9.32 NMT 9.84 7.23 41PR71 8/13/2014 15.68 -0.71 8.77 NMT 9.48 6.91 41PR72 12/3/2013 15.78 -0.89 11.35 NMT 12.24 4.43 41PR72 1/8/2014 15.78 -0.89 11.16 NMT 12.05 4.62 41PR72 8/13/2014 15.78 -0.89 8.99 NMT 9.88 6.79 41PR73 8/13/2014 16.74 -0.55 9.71 NMT 10.26 7.03 41PR74 12/3/2013 16.12 -1.58 12.25 NMT 13.83 3.87 41PR74 1/8/2014 16.12 -1.58 11.92 NMT 13.5 4.20 41PR74 2/4/2014 16.12 -1.58 11.52 NMT 13.1 4.60 41PR74 3/3/2014 16.12 -1.58 10.85 NMT 12.43 5.27 41PR74 4/7/2014 16.12 -1.58 10.39 NMT 11.97 5.73 41PR74 5/1/2014 16.12 -1.58 9.98 NMT 11.56 6.14 41PR74 6/2/2014 16.12 -1.58 11.14 NMT 12.72 4.98 41PR74 7/1/2014 16.12 -1.58 11.31 NMT 12.89 4.81 41PR74 8/13/2014 16.12 -1.58 10.99 NMT 12.57 5.13 41PR74 9/15/2014 16.12 -1.58 9.94 NMT 11.52 6.18 41PR74 10/1/2014 16.12 -1.58 10.11 NMT 11.69 6.01 41PR74 11/5/2014 16.12 -1.58 9.93 NMT 11.51 6.19 41PR74 12/1/2014 16.12 -1.58 11.04 NMT 12.62 5.08 41PR74 1/2/2015 16.12 -1.58 10.85 NMT 12.43 5.27 41PR74 2/2/2015 16.12 -1.58 10.64 NMT 12.22 5.48 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 9 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR75 12/3/2013 16.02 -0.89 11.6 NMT 12.49 4.42 41PR75 1/8/2014 16.02 -0.89 11.28 NMT 12.17 4.74 41PR75 2/4/2014 16.02 -0.89 10.65 NMT 11.54 5.37 41PR75 3/3/2014 16.02 -0.89 10.05 NMT 10.94 5.97 41PR75 4/7/2014 16.02 -0.89 9.59 NMT 10.48 6.43 41PR75 5/1/2014 16.02 -0.89 9.32 NMT 10.21 6.70 41PR75 6/2/2014 16.02 -0.89 10.34 NMT 11.23 5.68 41PR75 7/1/2014 16.02 -0.89 9.4 NMT 10.29 6.62 41PR75 8/13/2014 16.02 -0.89 10.15 NMT 11.04 5.87 41PR75 9/15/2014 16.02 -0.89 9.17 NMT 10.06 6.85 41PR75 10/1/2014 16.02 -0.89 9.32 NMT 10.21 6.70 41PR75 11/5/2014 16.02 -0.89 10.18 NMT 11.07 5.84 41PR75 12/1/2014 16.02 -0.89 10.37 NMT 11.26 5.65 41PR75 1/2/2015 16.02 -0.89 10.1 NMT 10.99 5.92 41PR75 2/2/2015 16.02 -0.89 8.9 NMT 9.79 7.12 41PR76 8/13/2014 15.98 -0.76 8.44 NMT 9.2 7.54 41 PR77 12/3/2013 16.93 -0.66 9.98 0.02 10.64 6.93 41PR77 1/8/2014 16.93 -0.66 9.82 NMT 10.48 7.11 41PR77 2/4/2014 16.93 -0.66 9.5 NMT 10.16 7.43 41PR77 3/3/2014 16.93 -0.66 9.62 NMT 10.28 7.31 41PR77 4/7/2014 16.93 -0.66 9.28 NMT 9.94 7.65 41PR77 5/1/2014 16.93 -0.66 9.04 NMT 9.7 7.89 41PR77 6/2/2014 16.93 -0.66 10.44 NMT 11.1 6.49 41PR77 7/1/2014 16.93 -0.66 9.87 NMT 10.53 7.06 41PR77 8/13/2014 16.93 -0.66 8.61 NMT 9.27 8.32 41PR77 9/15/2014 16.93 -0.66 7.44 NMT 8.1 9.49 41PR77 10/1/2014 16.93 -0.66 9.19 NMT 9.85 7.74 41PR77 11/5/2014 16.93 -0.66 10.28 NMT 10.94 6.65 41PR77 12/1/2014 16.93 -0.66 9.64 NMT 10.3 7.29 41PR77 1/2/2015 16.93 -0.66 9.48 NMT 10.14 7.45 41PR77 2/2/2015 16.93 -0.66 8.37 NMT 9.03 8.56 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 10 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR78 8/13/2014 15.72 -1.18 9.38 NMT 10.56 6.34 41PR79 12/3/2013 15.27 -0.81 9.59 NMT 10.4 5.68 41PR79 1/8/2014 15.27 -0.81 9.03 NMT 9.84 6.24 41PR79 2/4/2014 15.27 -0.81 7.4 NMT 8.21 7.87 41PR79 3/3/2014 15.27 -0.81 7.89 NMT 8.7 7.38 41PR79 4/7/2014 15.27 -0.81 7.24 NMT 8.05 8.03 41PR79 5/1/2014 15.27 -0.81 6.62 NMT 7.43 8.65 41PR79 6/2/2014 15.27 -0.81 9 NMT 9.81 6.27 41PR79 7/1/2014 15.27 -0.81 7.91 NMT 8.72 7.36 41PR79 8/13/2014 15.27 -0.81 7.5 NMT 8.31 7.77 41PR79 9/15/2014 15.27 -0.81 6.64 NMT 7.45 8.63 41PR79 10/1/2014 15.27 -0.81 7.21 NMT 8.02 8.06 41PR79 11/5/2014 15.27 -0.81 8.83 NMT 9.64 6.44 41PR79 12/1/2014 15.27 -0.81 7.89 NMT 8.7 7.38 41PR79 1/2/2015 15.27 -0.81 7.7 NMT 8.51 7.57 41PR79 2/2/2015 15.27 -0.81 5.89 NMT 6.7 9.38 41PR80 2/4/2014 16.1 -0.84 9.8 NMT 10.64 6.30 41PR80 3/3/2014 16.1 -0.84 8.77 NMT 9.61 7.33 41PR80 4/7/2014 16.1 -0.84 8.48 NMT 9.32 7.62 41PR80 5/1/2014 16.1 -0.84 8.07 NMT 8.91 8.03 41PR80 6/2/2014 16.1 -0.84 9.82 NMT 10.66 6.28 41PR80 7/1/2014 16.1 -0.84 9.23 NMT 10.07 6.87 41PR80 8/13/2014 16.1 -0.84 7.97 NMT 8.81 8.13 41PR80 9/15/2014 16.1 -0.84 7.51 NMT 8.35 8.59 41PR80 10/1/2014 16.1 -0.84 8.48 NMT 9.32 7.62 41PR80 11/5/2014 16.1 -0.84 9.77 NMT 10.61 6.33 41PR80 12/1/2014 16.1 -0.84 9.14 NMT 9.98 6.96 41PR80 1/2/2015 16.1 -0.84 8.95 NMT 9.79 7.15 41PR80 2/2/2015 16.1 -0.84 7.04 NMT 7.88 9.06 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 11 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR81 12/3/2013 15.28 -1.17 11.28 NMT 12.45 4.00 41PR81 1/8/2014 15.28 -1.17 10.77 NMT 11.94 4.51 41 PR81 2/4/2014 15.28 -1.17 8.04 0.01 9.21 7.23 41PR81 4/7/2014 15.28 -1.17 9.68 NMT 10.85 5.60 41PR81 5/1/2014 15.28 -1.17 8.21 NMT 9.38 7.07 41PR81 7/1/2014 15.28 -1.17 8.62 NMT 9.79 6.66 41PR81 8/13/2014 15.28 -1.17 8.32 NMT 9.49 6.96 41PR81 9/15/2014 15.28 -1.17 8.02 NMT 9.19 7.26 41PR81 10/1/2014 15.28 -1.17 9.41 NMT 10.58 5.87 41PR81 11/5/2014 15.28 -1.17 11.08 NMT 12.25 4.20 41PR81 12/1/2014 15.28 -1.17 7.48 NMT 8.65 7.80 41PR81 1/2/2015 15.28 -1.17 10.06 NMT 11.23 5.22 41PR81 2/2/2015 15.28 -1.17 8.71 NMT 9.88 6.57 41PR82 12/3/2013 16.21 -0.71 10.77 NMT 11.48 5.44 41PR82 1/8/2014 16.21 -0.71 11.1 NMT 11.81 5.11 41PR82 2/4/2014 16.21 -0.71 9.52 NMT 10.23 6.69 41 PR82 3/3/2014 16.21 -0.71 9.59 0.01 10.3 6.61 41PR82 4/7/2014 16.21 -0.71 9.45 NMT 10.16 6.76 41PR82 5/1/2014 16.21 -0.71 8.72 NMT 9.43 7.49 41PR82 6/2/2014 16.21 -0.71 10.75 NMT 11.46 5.46 41PR82 7/1/2014 16.21 -0.71 9.55 NMT 10.26 6.66 41PR82 8/13/2014 16.21 -0.71 8.17 NMT 8.88 8.04 41PR82 9/15/2014 16.21 -0.71 7.84 NMT 8.55 8.37 41PR82 10/1/2014 16.21 -0.71 9.08 NMT 9.79 7.13 41PR82 11/5/2014 16.21 -0.71 10.61 NMT 11.32 5.60 41PR82 12/1/2014 16.21 -0.71 9.49 NMT 10.2 6.72 41PR82 1/2/2015 16.21 -0.71 9.32 NMT 10.03 6.89 41PR82 2/2/2015 16.21 -0.71 8.02 NMT 8.73 8.19 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 12 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41 PR83 12/3/2013 16.39 -0.58 11.15 0.04 11.73 5.20 41 PR83 1 /8/2014 16.39 -0.58 10.75 0.03 11.33 5.61 41 PR83 2/4/2014 16.39 -0.58 9.93 0.05 10.51 6.41 41 PR83 3/3/2014 16.39 -0.58 9.98 NMT 10.56 6.41 41 PR83 4/7/2014 16.39 -0.58 9.6 0.01 10.18 6.78 41 PR83 5/1/2014 16.39 -0.58 8.83 0.05 9.41 7.51 41 PR83 6/2/2014 16.39 -0.58 10.88 NMT 11.46 5.51 41 PR83 7/1/2014 16.39 -0.58 9.8 0.01 10.38 6.58 41 PR83 8/13/2014 16.39 -0.58 8.02 0.08 8.6 8.29 41 PR83 9/15/2014 16.39 -0.58 7.64 NMT 8.22 8.75 41 PR83 10/1/2014 16.39 -0.58 9.15 0.08 9.73 7.16 41 PR83 11/5/2014 16.39 -0.58 10.76 NMT 11.34 5.63 41 PR83 12/1/2014 16.39 -0.58 9.92 NMT 10.5 6.47 41 PR83 1/2/2015 16.39 -0.58 9.76 NMT 10.34 6.63 41 PR83 2/2/2015 16.39 -0.58 8.03 0.02 8.61 8.34 41PR84 8/13/2014 14.57 -1.21 8.56 NMT 9.77 6.01 41PR85 12/3/2013 14.61 -0.83 10.99 NMT 11.82 3.62 41PR85 1/8/2014 14.61 -0.83 10.68 NMT 11.51 3.93 41PR85 2/4/2014 14.61 -0.83 9.78 NMT 10.61 4.83 41PR85 3/3/2014 14.61 -0.83 9.88 NMT 10.71 4.73 41PR85 4/7/2014 14.61 -0.83 9.74 NMT 10.57 4.87 41PR85 5/1/2014 14.61 -0.83 9.31 NMT 10.14 5.30 41PR85 6/2/2014 14.61 -0.83 10.82 NMT 11.65 3.79 41PR85 7/1/2014 14.61 -0.83 10.21 NMT 11.04 4.40 41PR85 8/13/2014 14.61 -0.83 9.04 NMT 9.87 5.57 41PR85 9/15/2014 14.61 -0.83 9.13 NMT 9.96 5.48 41PR85 10/1/2014 14.61 -0.83 9.61 NMT 10.44 5.00 41PR85 11/5/2014 14.61 -0.83 10.81 NMT 11.64 3.80 41PR85 12/1/2014 14.61 -0.83 10.23 NMT 11.06 4.38 41PR85 1/2/2015 14.61 -0.83 10.02 NMT 10.85 4.59 41PR85 2/2/2015 14.61 -0.83 8.9 NMT 9.73 5.71 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 13 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR86 12/3/2013 14.93 -0.78 11.72 NMT 12.5 3.21 41PR86 1/8/2014 14.93 -0.78 11.35 NMT 12.13 3.58 41PR86 2/4/2014 14.93 -0.78 10.7 NMT 11.48 4.23 41PR86 3/3/2014 14.93 -0.78 10.61 NMT 11.39 4.32 41PR86 4/7/2014 14.93 -0.78 10.42 NMT 11.2 4.51 41PR86 5/1/2014 14.93 -0.78 9.96 NMT 10.74 4.97 41PR86 6/2/2014 14.93 -0.78 11.41 NMT 12.19 3.52 41PR86 7/1/2014 14.93 -0.78 10.82 NMT 11.6 4.11 41PR86 8/13/2014 14.93 -0.78 9.75 NMT 10.53 5.18 41PR86 9/15/2014 14.93 -0.78 9.46 NMT 10.24 5.47 41PR86 10/1/2014 14.93 -0.78 10.12 NMT 10.9 4.81 41PR86 11/5/2014 14.93 -0.78 11.29 NMT 12.07 3.64 41PR86 12/1/2014 14.93 -0.78 10.77 NMT 11.55 4.16 41PR86 1/2/2015 14.93 -0.78 9.51 NMT 10.29 5.42 41PR86 2/2/2015 14.93 -0.78 9.45 NMT 10.23 5.48 41PR87 8/13/2014 14.86 -0.76 9.69 NMT 10.45 5.17 41PR88 8/13/2014 13.95 -0.7 9 NMT 9.7 4.95 41PR89 8/13/2014 13.4 -0.74 8.33 NMT 9.07 5.07 41PR90 8/13/2014 13.56 -0.71 8.21 NMT 8.92 5.35 41PR91 8/13/2014 12.7 -0.6 7.16 NMT 7.76 5.54 41PR93 8/13/2014 11.05 -0.98 5.93 NMT 6.91 5.12 41PR94 8/13/2014 10.07 -1.54 5.19 NMT 6.73 4.88 41PR95 8/13/2014 10.52 -0.74 5.58 NMT 6.32 4.94 41PR96 8/13/2014 8.31 -0.74 3.13 NMT 3.87 5.18 41PR97 8/13/2014 12.3 -0.67 6.93 NMT 7.6 5.37 41PR98 8/13/2014 9.32 -1.1 4.66 NMT 5.76 4.66 41PR99 8/13/2014 7.73 -1.27 3.81 NMT 5.08 3.92 41PR100 8/13/2014 15.33 -0.68 8.81 NMT 9.49 6.52 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 14 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR101 12/3/2013 16.32 -1.27 12 NMT 13.27 4.32 41PR101 1/8/2014 16.32 -1.27 11.63 NMT 12.9 4.69 41PR101 2/4/2014 16.32 -1.27 11 NMT 12.27 5.32 41PR101 3/3/2014 16.32 -1.27 10.43 NMT 11.7 5.89 41PR101 4/7/2014 16.32 -1.27 9.96 NMT 11.23 6.36 41PR101 5/1/2014 16.32 -1.27 9.65 NMT 10.92 6.67 41PR101 6/2/2014 16.32 -1.27 10.8 NMT 12.07 5.52 41PR101 7/1/2014 16.32 -1.27 11.77 NMT 13.04 4.55 41PR101 8/13/2014 16.32 -1.27 9.6 NMT 10.87 6.72 41PR101 9/15/2014 16.32 -1.27 9.51 NMT 10.78 6.81 41PR101 10/1/2014 16.32 -1.27 9.65 NMT 10.92 6.67 41PR101 11/5/2014 16.32 -1.27 10.6 NMT 11.87 5.72 41PR101 12/1/2014 16.32 -1.27 10.66 NMT 11.93 5.66 41PR101 1/2/2015 16.32 -1.27 10.45 NMT 11.72 5.87 41PR101 2/2/2015 16.32 -1.27 9.23 NMT 10.5 7.09 41PR200 12/3/2013 15.67 -0.52 12.34 NMT 12.86 3.33 41PR200 1/8/2014 15.67 -0.52 11.94 NMT 12.46 3.73 41PR200 2/4/2014 15.67 -0.52 11.16 NMT 11.68 4.51 41PR200 3/3/2014 15.67 -0.52 10.94 NMT 11.46 4.73 41PR200 4/7/2014 15.67 -0.52 10.56 NMT 11.08 5.11 41PR200 5/1/2014 15.67 -0.52 10.29 NMT 10.81 5.38 41PR200 6/2/2014 15.67 -0.52 11.52 NMT 12.04 4.15 41PR200 7/1/2014 15.67 -0.52 11.21 NMT 11.73 4.46 41PR200 8/13/2014 15.67 -0.52 10.36 NMT 10.88 5.31 41PR200 9/15/2014 15.67 -0.52 9.94 NMT 10.46 5.73 41PR200 10/1/2014 15.67 -0.52 10.35 NMT 10.87 5.32 41PR200 11/5/2014 15.67 -0.52 11.41 NMT 11.93 4.26 41PR200 12/1/2014 15.67 -0.52 11.14 NMT 11.66 4.53 41PR200 1/2/2015 15.67 -0.52 10.95 NMT 11.47 4.72 41PR200 2/2/2015 15.67 -0.52 9.82 NMT 10.34 5.85 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 15 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR201 12/3/2013 16.31 -0.28 12.9 NMT 13.18 3.41 41PR201 1/8/2014 16.31 -0.28 12.42 NMT 12.7 3.89 41PR201 2/4/2014 16.31 -0.28 11.27 NMT 11.55 5.04 41PR201 3/3/2014 16.31 -0.28 11.39 NMT 11.67 4.92 41PR201 4/7/2014 16.31 -0.28 10.94 NMT 11.22 5.37 41PR201 5/1/2014 16.31 -0.28 10.33 NMT 10.61 5.98 41PR201 6/2/2014 16.31 -0.28 12.05 NMT 12.33 4.26 41PR201 7/1/2014 16.31 -0.28 11.33 NMT 11.61 4.98 41PR201 8/13/2014 16.31 -0.28 9.91 NMT 10.19 6.40 41PR201 9/15/2014 16.31 -0.28 9.28 NMT 9.56 7.03 41PR201 10/1/2014 16.31 -0.28 10.67 NMT 10.95 5.64 41PR201 11/5/2014 16.31 -0.28 12.06 NMT 12.34 4.25 41PR201 12/1/2014 16.31 -0.28 11.46 NMT 11.74 4.85 41PR201 1/2/2015 16.31 -0.28 11.31 NMT 11.59 5.00 41PR201 2/2/2015 16.31 -0.28 9.97 NMT 10.25 6.34 41 PR202 12/3/2013 16.17 -0.35 11.91 0.07 12.26 4.19 41 PR202 1 /8/2014 16.17 -0.35 11.78 0.02 12.13 4.37 41 PR202 2/4/2014 16.17 -0.35 10.8 0.07 11.15 5.30 41 PR202 3/3/2014 16.17 -0.35 10.71 NMT 11.06 5.46 41 PR202 4/7/2014 16.17 -0.35 10.28 NMT 10.63 5.89 41 PR202 5/1/2014 16.17 -0.35 9.95 NMT 10.3 6.22 41 PR202 6/2/2014 16.17 -0.35 11.32 0.13 11.67 4.72 41 PR202 7/1/2014 16.17 -0.35 10.97 0.14 11.32 5.06 41 PR202 8/13/2014 16.17 -0.35 10 0.18 10.35 5.99 41 PR202 9/15/2014 16.17 -0.35 9.86 0.21 10.21 6.10 41 PR202 10/1/2014 16.17 -0.35 10.19 0.23 10.54 5.75 41 PR202 11 /5/2014 16.17 -0.35 11.35 0.26 11.7 4.56 41 PR202 12/1/2014 16.17 -0.35 11.01 0.27 11.36 4.89 41 PR202 1 /2/2015 16.17 -0.35 10.8 0.31 11.15 5.06 41 PR202 2/2/2015 16.17 -0.35 9.61 0.27 9.96 6.29 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 16 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR203 12/3/2013 16.16 -0.32 12.81 NMT 13.13 3.35 41PR203 1/8/2014 16.16 -0.32 12.35 NMT 12.67 3.81 41PR203 2/4/2014 16.16 -0.32 11.76 NMT 12.08 4.40 41PR203 3/3/2014 16.16 -0.32 11.1 NMT 11.42 5.06 41PR203 4/7/2014 16.16 -0.32 10.63 NMT 10.95 5.53 41PR203 5/1/2014 16.16 -0.32 10.55 NMT 10.87 5.61 41PR203 6/2/2014 16.16 -0.32 11.65 NMT 11.97 4.51 41PR203 7/1/2014 16.16 -0.32 11.56 NMT 11.88 4.60 41PR203 8/13/2014 16.16 -0.32 10.33 NMT 10.65 5.83 41PR203 9/15/2014 16.16 -0.32 10.36 NMT 10.68 5.80 41PR203 10/1/2014 16.16 -0.32 10.58 NMT 10.9 5.58 41PR203 11/5/2014 16.16 -0.32 11.54 NMT 11.86 4.62 41PR203 12/1/2014 16.16 -0.32 11.5 NMT 11.82 4.66 41PR203 1/2/2015 16.16 -0.32 11.23 NMT 11.55 4.93 41PR203 2/2/2015 16.16 -0.32 10.02 NMT 10.34 6.14 41PR204 12/3/2013 15.81 -0.21 12.48 NMT 12.69 3.33 41PR204 1/8/2014 15.81 -0.21 11.97 NMT 12.18 3.84 41PR204 2/4/2014 15.81 -0.21 11.28 NMT 11.49 4.53 41PR204 3/3/2014 15.81 -0.21 10.86 NMT 11.07 4.95 41PR204 4/7/2014 15.81 -0.21 10.34 NMT 10.55 5.47 41PR204 5/1/2014 15.81 -0.21 9.9 NMT 10.11 5.91 41PR204 6/2/2014 15.81 -0.21 11.33 NMT 11.54 4.48 41PR204 7/1/2014 15.81 -0.21 11.14 NMT 11.35 4.67 41PR204 8/13/2014 15.81 -0.21 9.91 NMT 10.12 5.90 41PR204 9/15/2014 15.81 -0.21 9.68 NMT 9.89 6.13 41PR204 10/1/2014 15.81 -0.21 10.06 NMT 10.27 5.75 41PR204 11/5/2014 15.81 -0.21 11.21 NMT 11.42 4.60 41PR204 12/1/2014 15.81 -0.21 11.13 NMT 11.34 4.68 41PR204 1/2/2015 15.81 -0.21 10.8 NMT 11.01 5.01 41PR204 2/2/2015 15.81 -0.21 9.54 NMT 9.75 6.27 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 17 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR210 12/3/2013 15.5 0 12.43 NMT 12.43 3.07 41PR210 1/8/2014 15.5 0 12 NMT 12 3.50 41PR210 2/4/2014 15.5 0 11.11 NMT 11.11 4.39 41PR210 3/3/2014 15.5 0 11.13 NMT 11.13 4.37 41PR210 4/7/2014 15.5 0 10.91 NMT 10.91 4.59 41PR210 5/1/2014 15.5 0 10.43 NMT 10.43 5.07 41 PR210 6/2/2014 15.5 0 12.18 0.03 12.18 3.29 41PR210 7/1/2014 15.5 0 11.1 0.04 11.1 4.36 41 PR210 8/13/2014 15.5 0 10.02 0.04 10.02 5.44 41 PR210 9/15/2014 15.5 0 9.4 0.04 9.4 6.06 41PR210 10/1/2014 15.5 0 10.57 0.06 10.57 4.87 41 PR210 11 /5/2014 15.5 0 12.05 0.11 12.05 3.34 41PR210 12/1/2014 15.5 0 11.2 0.12 11.2 4.18 41 PR210 1 /2/2015 15.5 0 11.11 0.10 11.11 4.29 41 PR210 2/2/2015 15.5 0 9.89 0.09 9.89 5.52 41PR211 12/3/2013 15.43 0 12.47 NMT 12.47 2.96 41PR211 1/8/2014 15.43 0 12.13 NMT 12.13 3.30 41PR211 2/4/2014 15.43 0 11.27 NMT 11.27 4.16 41PR211 3/3/2014 15.43 0 11.18 NMT 11.18 4.25 41PR211 4/7/2014 15.43 0 11.01 NMT 11.01 4.42 41PR211 5/1/2014 15.43 0 10.64 NMT 10.64 4.79 41PR211 6/2/2014 15.43 0 12.26 NMT 12.26 3.17 41PR211 7/1/2014 15.43 0 11.27 NMT 11.27 4.16 41PR211 8/13/2014 15.43 0 10.14 NMT 10.14 5.29 41PR211 9/15/2014 15.43 0 9.75 NMT 9.75 5.68 41PR211 10/1/2014 15.43 0 10.73 NMT 10.73 4.70 41PR211 11/5/2014 15.43 0 12.21 NMT 12.21 3.22 41PR211 12/1/2014 15.43 0 11.32 NMT 11.32 4.11 41PR211 1/2/2015 15.43 0 11.21 NMT 11.21 4.22 41PR211 2/2/2015 15.43 0 10.18 NMT 10.18 5.25 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 18 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR212 12/3/2013 15.38 0 12.84 NMT 12.84 2.54 41PR212 1/8/2014 15.38 0 12 NMT 12 3.38 41PR212 2/4/2014 15.38 0 11.25 NMT 11.25 4.13 41PR212 3/3/2014 15.38 0 11.42 NMT 11.42 3.96 41PR212 4/7/2014 15.38 0 11.56 NMT 11.56 3.82 41PR212 5/1/2014 15.38 0 10.89 NMT 10.89 4.49 41PR212 6/2/2014 15.38 0 13 NMT 13 2.38 41PR212 7/1/2014 15.38 0 11.9 NMT 11.9 3.48 41PR212 8/13/2014 15.38 0 12.01 NMT 12.01 3.37 41PR212 9/15/2014 15.38 0 10.21 NMT 10.21 5.17 41PR212 10/1/2014 15.38 0 11.57 NMT 11.57 3.81 41PR212 11/5/2014 15.38 0 13.03 NMT 13.03 2.35 41PR212 12/1/2014 15.38 0 12.08 NMT 12.08 3.30 41PR212 1/2/2015 15.38 0 11.92 NMT 11.92 3.46 41PR212 2/2/2015 15.38 0 10.66 NMT 10.66 4.72 41PR213 12/3/2013 15.35 0 13 NMT 13 2.35 41PR213 1/8/2014 15.35 0 12.61 NMT 12.61 2.74 41PR213 2/4/2014 15.35 0 11.8 NMT 11.8 3.55 41PR213 3/3/2014 15.35 0 11.9 NMT 11.9 3.45 41PR213 4/7/2014 15.35 0 11.76 NMT 11.76 3.59 41PR213 5/1/2014 15.35 0 11.48 NMT 11.48 3.87 41PR213 6/2/2014 15.35 0 13.01 NMT 13.01 2.34 41PR213 7/1/2014 15.35 0 12.03 NMT 12.03 3.32 41PR213 8/13/2014 15.35 0 11.21 NMT 11.21 4.14 41PR213 9/15/2014 15.35 0 10.64 NMT 10.64 4.71 41PR213 10/1/2014 15.35 0 11.58 NMT 11.58 3.77 41 PR213 11 /5/2014 15.35 0 12.94 0.01 12.94 2.40 41PR213 12/1/2014 15.35 0 12.25 NMT 12.25 3.10 41PR213 1/2/2015 15.35 0 11.88 NMT 11.88 3.47 41PR213 2/2/2015 15.35 0 10.67 NMT 10.67 4.68 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 19 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41 PR214 12/3/2013 15.3 0 12.28 0.02 12.28 3.00 41 PR214 1 /8/2014 15.3 0 11.93 0.03 11.93 3.34 41 PR214 2/4/2014 15.3 0 10.99 NMT 10.99 4.31 41 PR214 3/3/2014 15.3 0 11.31 0.01 11.31 3.98 41 PR214 4/7/2014 15.3 0 11.28 NMT 11.28 4.02 41 PR214 5/1/2014 15.3 0 10.55 NMT 10.55 4.75 41 PR214 6/2/2014 15.3 0 12.6 0.11 12.6 2.59 41 PR214 7/1/2014 15.3 0 11.3 0.08 11.3 3.92 41 PR214 8/13/2014 15.3 0 10.24 NMT 10.24 5.06 41 PR214 9/15/2014 15.3 0 9.46 0.09 9.46 5.75 41 PR214 10/1/2014 15.3 0 11.07 0.10 11.07 4.13 41 PR214 11 /5/2014 15.3 0 12.51 0.28 12.51 2.51 41 PR214 12/1/2014 15.3 0 11.72 0.24 11.72 3.34 41 PR214 1 /2/2015 15.3 0 11.51 0.25 11.51 3.54 41 PR214 2/2/2015 15.3 0 10.69 0.14 10.69 4.47 41PR215 12/3/2013 15.79 0 12.5 NMT 12.5 3.29 41PR215 1/8/2014 15.79 0 12.13 NMT 12.13 3.66 41PR215 2/4/2014 15.79 0 11.22 NMT 11.22 4.57 41PR215 3/3/2014 15.79 0 11.22 NMT 11.22 4.57 41PR215 4/7/2014 15.79 0 11.06 NMT 11.06 4.73 41PR215 5/1/2014 15.79 0 10.58 NMT 10.58 5.21 41PR215 6/2/2014 15.79 0 12.38 NMT 12.38 3.41 41PR215 7/1/2014 15.79 0 11.25 NMT 11.25 4.54 41PR215 8/13/2014 15.79 0 10.26 NMT 10.26 5.53 41PR215 9/15/2014 15.79 0 9.66 NMT 9.66 6.13 41PR215 10/1/2014 15.79 0 10.81 NMT 10.81 4.98 41PR215 11/5/2014 15.79 0 12.19 NMT 12.19 3.60 41PR215 12/1/2014 15.79 0 11.38 NMT 11.38 4.41 41PR215 1/2/2015 15.79 0 11.27 NMT 11.27 4.52 41PR215 2/2/2015 15.79 0 10.03 NMT 10.03 5.76 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 20 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41 PR216 12/3/2013 15.81 0 12.37 NMT 12.37 3.44 41 PR216 1 /8/2014 15.81 0 12.07 0.02 12.07 3.72 41 PR216 2/4/2014 15.81 0 11.06 0.06 11.06 4.69 41 PR216 3/3/2014 15.81 0 11.08 0.17 11.08 4.56 41 PR216 4/7/2014 15.81 0 11.21 0.26 11.21 4.34 41 PR216 5/1/2014 15.81 0 10.77 0.33 10.77 4.71 41 PR216 6/2/2014 15.81 0 11.95 0.38 11.95 3.48 41 PR216 7/1/2014 15.81 0 10.91 0.43 10.91 4.47 41 PR216 8/13/2014 15.81 0 9.97 0.50 9.97 5.34 41 PR216 9/15/2014 15.81 0 9.36 0.62 9.36 5.83 41 PR216 10/1/2014 15.81 0 10.38 0.65 10.38 4.78 41 PR216 11 /5/2014 15.81 0 11.83 0.59 11.83 3.39 41 PR216 12/1/2014 15.81 0 11.35 0.61 11.35 3.85 41 PR216 1 /2/2015 15.81 0 11.02 0.74 11.02 4.05 41 PR216 2/2/2015 15.81 0 9.74 0.82 9.74 5.25 41 PR217 12/3/2013 15.81 0 12.36 NMT 12.36 3.45 41 PR217 1/8/2014 15.81 0 11.94 NMT 11.94 3.87 41 PR217 2/4/2014 15.81 0 10.9 0.01 10.9 4.90 41 PR217 3/3/2014 15.81 0 10.8 0.22 10.8 4.79 41 PR217 4/7/2014 15.81 0 10.52 0.39 10.52 4.90 41 PR217 5/1/2014 15.81 0 10.01 0.52 10.01 5.28 41 PR217 6/2/2014 15.81 0 11.72 0.43 11.72 3.66 41 PR217 7/1/2014 15.81 0 10.82 0.43 10.82 4.56 41 PR217 8/13/2014 15.81 0 9.81 NMT 9.81 6.00 41 PR217 9/15/2014 15.81 0 9.16 0.50 9.16 6.15 41 PR217 10/1/2014 15.81 0 10.23 0.52 10.23 5.06 41 PR217 11 /5/2014 15.81 0 11.62 0.46 11.62 3.73 41 PR217 12/1 /2014 15.81 0 11.01 0.49 11.01 4.31 41 PR217 1 /2/2015 15.81 0 10.95 0.50 10.95 4.36 41 PR217 2/2/2015 15.81 0 9.59 0.51 9.59 5.71 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 21 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41 PR218 12/3/2013 15.29 0 12.43 NMT 12.43 2.86 41 PR218 1/8/2014 15.29 0 11.3 NMT 11.3 3.99 41 PR218 2/4/2014 15.29 0 10.16 0.03 10.16 5.10 41 PR218 3/3/2014 15.29 0 11.39 0.02 11.39 3.88 41 PR218 4/7/2014 15.29 0 10.23 0.02 10.23 5.04 41 PR218 5/1/2014 15.29 0 9.72 0.02 9.72 5.55 41 PR218 6/2/2014 15.29 0 11.75 0.02 11.75 3.52 41 PR218 7/1/2014 15.29 0 10.28 0.02 10.28 4.99 41 PR218 8/13/2014 15.29 0 9.51 NMT 9.51 5.78 41 PR218 9/15/2014 15.29 0 9.72 0.04 9.72 5.53 41 PR218 10/1/2014 15.29 0 10.14 0.04 10.14 5.11 41 PR218 11 /5/2014 15.29 0 11.7 0.04 11.7 3.55 41 PR218 12/1/2014 15.29 0 10.52 0.04 10.52 4.73 41 PR218 1 /2/2015 15.29 0 11.53 0.03 11.53 3.73 41 PR218 2/2/2015 15.29 0 9.2 0.03 9.2 6.06 41 PR219 12/3/2013 15.48 0 11.92 NMT 11.92 3.56 41 PR219 1/8/2014 15.48 0 11.61 NMT 11.61 3.87 41 PR219 2/4/2014 15.48 0 10.5 0.04 10.5 4.94 41 PR219 3/3/2014 15.48 0 10.45 0.23 10.45 4.80 41 PR219 4/7/2014 15.48 0 10.11 0.21 10.11 5.16 41 PR219 5/1/2014 15.48 0 9.82 0.33 9.82 5.33 41 PR219 6/2/2014 15.48 0 11.45 0.46 11.45 3.57 41 PR219 7/1/2014 15.48 0 10.47 0.46 10.47 4.55 41 PR219 8/13/2014 15.48 0 9.35 0.46 9.35 5.67 41 PR219 9/15/2014 15.48 0 8.89 0.51 8.89 6.08 41 PR219 10/1/2014 15.48 0 9.98 0.44 9.98 5.06 41 PR219 11 /5/2014 15.48 0 11.37 0.58 11.37 3.53 41 PR219 12/1/2014 15.48 0 10.7 0.56 10.7 4.22 41 PR219 1 /2/2015 15.48 0 10.5 0.54 10.5 4.44 41 PR219 2/2/2015 15.48 0 9.11 0.68 9.11 5.69 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 22 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41 PR220 12/3/2013 15.88 0 12.05 NMT 12.05 3.83 41 PR220 1/8/2014 15.88 0 12.01 NMT 12.01 3.87 41 PR220 2/4/2014 15.88 0 11.1 NMT 11.1 4.78 41 PR220 3/3/2014 15.88 0 10.88 NMT 10.88 5.00 41 PR220 4/7/2014 15.88 0 10.63 NMT 10.63 5.25 41 PR220 5/1/2014 15.88 0 10.24 NMT 10.24 5.64 41 PR220 6/2/2014 15.88 0 11.89 NMT 11.89 3.99 41 PR220 7/1/2014 15.88 0 11.01 NMT 11.01 4.87 41 PR220 8/13/2014 15.88 0 10 NMT 10 5.88 41 PR220 9/15/2014 15.88 0 9.44 NMT 9.44 6.44 41 PR220 10/1/2014 15.88 0 10.45 NMT 10.45 5.43 41 PR220 11 /5/2014 15.88 0 11.75 0.09 11.75 4.04 41 PR220 12/1/2014 15.88 0 11.13 0.02 11.13 4.73 41 PR220 1 /2/2015 15.88 0 11.02 0.04 11.02 4.82 41 PR220 2/2/2015 15.88 0 9.51 0.02 9.51 6.35 41 PR221 12/3/2013 15.82 0 11.95 NMT 11.95 3.87 41 PR221 1/8/2014 15.82 0 11.84 NMT 11.84 3.98 41 PR221 2/4/2014 15.82 0 10.98 NMT 10.98 4.84 41 PR221 3/3/2014 15.82 0 10.74 NMT 10.74 5.08 41 PR221 4/7/2014 15.82 0 10.63 NMT 10.63 5.19 41 PR221 5/1/2014 15.82 0 10.01 NMT 10.01 5.81 41 PR221 6/2/2014 15.82 0 11.74 NMT 11.74 4.08 41 PR221 7/1/2014 15.82 0 10.88 NMT 10.88 4.94 41 PR221 8/13/2014 15.82 0 9.66 NMT 9.66 6.16 41 PR221 9/15/2014 15.82 0 9.4 0.01 9.4 6.41 41 PR221 10/1/2014 15.82 0 10.29 0.02 10.29 5.51 41 PR221 11 /5/2014 15.82 0 11.654 0.02 11.654 4.15 41 PR221 12/1/2014 15.82 0 11.08 0.02 11.08 4.72 41 PR221 1 /2/2015 15.82 0 10.83 0.01 10.83 4.98 41 PR221 2/2/2015 15.82 0 9.5 0.02 9.5 6.30 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 23 4. TBM = To Be Measured TABLE 1 SITE 1083 HISTORICAL FIELD MEASUREMENT DATA Well ID Date TOC Stickup DTW/DTP Product Thickness DTW/DTP BGS GWT Elevation 41PR230 12/3/2013 16.11 0 12.82 NMT 12.82 3.29 41PR230 1/8/2014 16.11 0 12.18 NMT 12.18 3.93 41PR230 2/4/2014 16.11 0 11.64 NMT 11.64 4.47 41PR230 3/3/2014 16.11 0 11 NMT 11 5.11 41PR230 4/7/2014 16.11 0 10.52 NMT 10.52 5.59 41PR230 5/1/2014 16.11 0 10.25 NMT 10.25 5.86 41PR230 6/2/2014 16.11 0 11.25 NMT 11.25 4.86 41PR230 7/1/2014 16.11 0 11.32 NMT 11.32 4.79 41PR230 8/13/2014 16.11 0 10.2 NMT 10.2 5.91 41PR230 9/15/2014 16.11 0 10.14 NMT 10.14 5.97 41PR230 10/1/2014 16.11 0 10.12 NMT 10.12 5.99 41PR230 11/5/2014 16.11 0 11.07 NMT 11.07 5.04 41PR230 12/1/2014 16.11 0 11.31 NMT 11.31 4.80 41PR230 1/2/2015 16.11 0 11.04 NMT 11.04 5.07 41PR230 2/2/2015 16.11 0 9.93 NMT 9.93 6.18 Notes: 1. NMT = No Measurable Thickness 2. NM = Not Measured 3. Data in BOLD ITALICS indicates measurable thicknesses of product detected Page 24 4. TBM = To Be Measured Date Sampled: 8/13/2014 PARAMETER 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzene Ethylbenzene Toluene Total Xylenes Totals: 2L GWQS GCL 20.0000 20,000.0000 200.0000 61,500.0000 6.0000 6,000.0000 1.0000 5,000.0000 600.0000 84,500.0000 600.0000 260,000.0000 500.0000 85,500.0000 TABLE 2 SITE 1083 GROUNDWATER LABORATORY ANALYTICAL RESULTS EPA METHOD 602 BY SM 6200B m r N N N N N r N r N A A 4 A 4 A 4 4 I� $N sN $r $r C 47 aS O O I -A V V V V V OAO 0) � r I-A47 N w w U1 w O 0 r w N -4 00 4 u1 14 00 %o O e M UNITS ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 1.39 0.66 0.00 0.00 0.00 0.00 0.00 5.41 0.00 0.00 0.00 0.33 1.73 1.14 1.37 0.00 0.69 0.00 0.44 0.00 0.00 0.00 0.00 0.00 ug/L 2.64 11.8 0.00 0.00 0.00 0.00 0.00 8.41 0.00 0.00 0.7 0.31 5.32 3.17 2.03 0.00 1.79 0.00 0.00 1.49 2.35 3.25 0.35 0.00 ug/L 0.00 0.38 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 1.54 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 1.49 18.4 0.00 0.00 0.00 0.00 0.00 4.61 0.00 0.00 0.00 0.00 3.15 6.21 1.28 0.00 0.57 0.00 0.00 0.00 4.96 2.44 0.00 0.00 5.52 31.24 0.00 0.00 0.00 0.00 0.00 18.43 0.00 0.00 2.24 0.64 10.2 10.52 4.68 0.00 3.05 0.00 0.44 1.49 7.31 5.69 0.35 0.00 Notes: 1. 2L GWQS = North Carolina Groundwater Quality Standard 15A NCAC 2L .0202 2. GCL = Gross Contamination Levels for groundwater as defined in "Guidelines for Assessment and Corrective Action for UST Releases" July 15, 2008 Version, Change 3 effective December 1, 2013 3. ug/L = Micrograms per Liter 4. A zero ("0.00") in the results column indicates concentration is either below detection limit or below quantitation limit 5. A zero ("0.0000") in the 2L GWQS column indicates the 2L standard is equal to the laboratory detection limit 6. A zero ("0.0000") in the GCL column indicates a GCL has not been established Page 1 Date Sampled: 8/13/2014 PARAMETER 2-Methyl naphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Di benzo(a, h)anthracene Fluoranthene Fluorene Indeno(1,2,3-c,d)pyrene Naphthalene Phenanthrene Pyrene Totals: 2L GWQS GCL 30.0000 12,500.0000 80.0000 2,120.0000 200.0000 1,965.0000 2,000.0000 2,000.0000 0.0500 4.7000 0.0050 0.8100 0.0500 0.7500 200.0000 200.0000 0.5000 0.5000 5.0000 5.0000 0.0050 1.2000 300.0000 300.0000 300.0000 990.0000 0.0500 0.0500 6.0000 6,000.0000 200.0000 410.0000 200.0000 200.0000 TABLE 3 SITE 1083 GROUNDWATER LABORATORY ANALYTICAL RESULTS EPA METHOD 610 BY EPA METHOD 625 m r N N N PA PA$r r r r r r I� $r sr C 47 g O O N G�1 9 V V V V V 9 R 0) � r N w w U1 w O M r w Ili-4 00 4 0 � 00 %o O ro UNITS ug/L 8.89 84.5 0.00 0.00 0.00 16.9 0.00 43.2 0.00 0.00 26.9 41.1 60.1 7.39 8.39 0.00 18 0.00 6.74 1.13 12 12.3 0.962 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.42 0.49 0.3 0.00 0.00 0.00 0.00 0.00 0.648 0.00 0.00 0.00 0.00 0.00 0.308 0.34 0.00 0.457 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.477 0.00 0.00 0.00 0.59 0.373 0.52 0.00 0.00 0.618 0.743 0.434 0.505 0.41 0.00 0.00 0.00 0.00 0.00 0.396 0.377 0.314 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 21.2 92.8 0.83 0.00 0.00 1.19 0.755 65.7 0.00 0.00 12.2 67.8 52.5 12.9 10.4 0.00 30.3 0.00 17.8 3.49 10.9 27 1.5 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 ug/L 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 30.09 177.777 0.83 0.00 0.00 19.1 1.618 109.72 0.00 0.00 39.718 109.643 113.034 21.443 19.2 0.00 48.3 0.00 24.54 4.928 23.636 39.677 3.233 0.00 Notes: 1. 2L GWQS = North Carolina Groundwater Quality Standard 15A NCAC 2L .0202 2. GCL = Gross Contamination Levels for groundwater as defined in "Guidelines for Assessment and Corrective Action for UST Releases" July 15, 2008 Version, Change 3 effective December 1, 2013 3. ug/L = Micrograms per Liter 4. A zero ("0.00") in the results column indicates concentration is either below detection limit or below quantitation limit 5. A zero ("0.0000") in the 2L GWQS column indicates the 2L standard is equal to the laboratory detection limit 6. A zero ("0.0000") in the GCL column indicates a GCL has not been established Page 1 FIGURES DOD; 210022.08_1083_Interim Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 June 2015 64 3 E Legend - Athletic Field Golf Course Misc Recreation Area - Buildings and Structures Roads Parking Areas Driveways F— Airfield Surface Neuse River Surface Water L�� NEUSE RIVER SITE LOCATION c Data Sources: GIs data layers provided by the MCAS Cherry Point GIS Department. �t J WARNING: This document is "FOR OFFICIAL USE ONLY" and it contains info that may be exempt from public release under the FOI Act (5 U.S.C. 552). It is to be handled IAW DoD policy and is not to be released to the public or personnel who do not have a valid "need -to -know" without prior approval of an authorized DoD official. 4,000 2,000 0 4,000 Feet SCALE ---'-En9nyea's ��� CATLIN PROJECT ANNUAL REPORT (DEC 2013 - FEB 2015) SURFACTANTULATIONPROJECT BUILDING 1083 TITLE GENERAL VICINITY MAP FIGURE Scienusts 220 Old Dairy Road MARINE CORPS AIR STATION CHERRY POINT, NORTH CAROLINA Wilmington, NC 78405 Corporate Llcensum No. for Enginecring Services C-0S85 OB N0, 210022.08DATE MAY 2015 SCALE AS SHOWN DRAWN BY THW CHECKED BY SAC 9 \>� r 41 Gwsz LI 41GW32 ® 41GW22 00,�\ 3�13,1 41GW42 41PR71 L'J � 41 PR100 41GW104 ® 41 PR70 tej ❑■ N � Wj A �4? 41 PR69 d� rpm c Eil �10 Area C w �7 V 41PR74 0 3788-2 41PR7❑8 .100 000> 41PR79 000, ■ OIIGW43 lwJ 41GW41 41 PR200 41 PR201 41 P R204 41GW106 41 PR203 41 PR202 41 P R77 �3788-3 41GW05 41GW36 41PR81 41GW23 Area A ❑�. ■ 41 PR92 ��. 41 PR85 r� LJ ■ / � 41 L L� U L■J LF r I 41 PR221 41 P R220 A 41PR93 41PR90 �■ ,��, ����41GW31 1 41OW33 `= 41PR87 41GW37 4;PR91 d■ 41GW35 41 PR216 41 G W46 ANNUAL REPORT 41GW112 ® (DEC. 2013 - FEB. 2015) SURFACTANT RECIRCULATION PROJECT BUILDING 1083 MCAS CHERRY POINT "Wmp All ANTR; n11/1.... 745 41GW24 41PR95 ❑■ 41GW29 41PR98 Area 6 ❑ 41PR96 ® ❑ a 747 41GW26 41 PR211 41 PR212 41GW06 41 P R213 Eil41 PR214 0 41 G W 03 41 PR86 LEGEND Well by Type 40 Well 0 RW Surface Water T-1 ® T-11 DO T-111 z Unknown NOTES Small Tributaries Rivers and Creeks Building Groundwater Flow Direction Former JP-5 Pipeline 41PR218 CATLIN Engineers and Scientists FIGURE SITE MAP WITH INJECTION/EXTRACTION AREAS 2 100 50 0 100 Feet Job No.: Date Drawn: Scale: Drawn By: Checked By: SCALE 210022.08 MAY 2015 AS SHOWN I THW SAC 41GW62 41GW32 RJ �0� WARNING: N This document is "FOR OFFICIAL USE ONLY" and �1A it contains info that may be exempt from public release under the FOI Act (5 U.S.C. 552). It is to be handled IAW DoD policy and 11tk is not to be released to the public or personnel who do not have a valid "need -to -know" without prior approval of an authorized DoD official. GW102 UROR�JE 41GW104 PR�N w3 01 b 41GW105 __' W 41GW63 41GW44 Well Number Well Type Date Product Thickness 41GW02 T-11 8/13/2014 0.04 41GW03 T-11 8/13/2014 0.05 41 P R83 RW 8/13/2014 0.08 41 P R202 RW 8/13/2014 0.18 41 P R210 RW 8/13/2014 0.04 41 P R216 RW 8/13/2014 0.50 41 P R219 RW 8/ 13/2014 0.46 PR100I 'll 11---' 41 PR77 PR73 41PR78 / 41PR80 _____g �4D (� 41PR76 GOER\ L777 � PF� w 's w� s 41GW111 wd6+ 41GW112 P11200 W w, 41 GW21 41 PR201 dp s )41GW107�nP1V� 41 GW119 Monitoring Well 41GW45 (D located approximately 180 feet south of 41GW119 GW41 41GW66 ED A 41 PR92 ❑ ®41GW24 Monitoring Wells 41GW39 & 41GW40 located approximately 250 feet northeast and 300 feet southeast of 41GW24 41 PR9i� 3 41 PR95 41GW26 41 PR98 41 P R 9 91 41 PR97 41GW38 ANNUAL REPORT (DEC. 2013 - FEB. 2015) SURFACTANT RECIRCULATION PROJECT BUILDING 1083 MCAS CHERRY POINT = s � LEGEND Well by Type Free Product Well 40 No Measurable Thickness RW Product Detected ® Free Product Plume Surface Water Small Tributaries T-I Rivers and Creeks (D T-II Building QO T-III Historical Groundwater ® Unknown Flow Direction Former JP-5 Pipeline NOTES J"�-�.`-" CATLIN Engineers and Scientists FIGURE FREE PRODUCT PLUME MAP AS OF AUGUST 2014 3A 100 50 0 100 GW46 Feet Job No.: Date Drawn: Scale: Drawn By: Checked By: SCALE 210022.08 1 MAY 2015 AS SHOWN THW I SAC GW102 R�N�ROR\J � P 41GW105 __' W 41GW63 G00R 3777-3 41GW41 r 41GW32 41GW62 �PF� ?g4.4 L 41GW44 ;CZ WARNING: This document is "FOR OFFICIAL USE ONLY" and it contains info that may be exempt from public release under the FOI Act (5 U.S.C. 552). It is to be handled IAW DoD policy and is not to be released to the public or personnel who do not have a valid "need -to -know" without prior approval of an authorized DoD official. Well Number Well Type Date Product Thickness 41GW05 T-11 2/2/2015 0.05 41 P R83 RW 2/2/2015 0.02 41 P R202 RW 2/2/2015 0.27 41 P R210 RW 2/2/2015 0.09 41 P R214 RW 2/2/2015 0.14 41 P R216 RW 2/2/2015 0.82 41 P R217 RW 2/2/2015 0.51 41 PR218 RW 2/2/2015 0.03 41 P R219 RW 2/2/2015 0.68 41 P R220 RW 2/2/2015 0.02 41 P R221 RW 2/2/2015 0.02 uj 6� 41GW111 �d� / 41PR80--____� �40 (� 41PR76 41 GW119 Monitoring Well 41GW45 (D located approximately 180 feet south of 41GW119 41GW21 J41GW1o7c)PV� � 41 PR92 ❑ ®41GW24 Monitoring Wells 41GW39 & 41GW40 located approximately 250 feet northeast and 300 feet southeast of 41GW24 41 PR9i� 3 41 PR95 41GW26 41 PR99 41 PR97 41GW38 ANNUAL REPORT (DEC. 2013 - FEB. 2015) SURFACTANT RECIRCULATION PROJECT BUILDING 1083 MCAS CHERRY POINT Engineering Cbrnrriand'S „xs K.- LEGEND Well by Type Free Product Well No Measurable Thickness RW Product Detected ® Free Product Plume Surface Water Small Tributaries T-I Rivers and Creeks ® T-II Building QO T-III Historical Groundwater ® Unknown Flow Direction Former JP-5 Pipeline NOTES J"�-�.`-" CATLIN Engineers and Scientists FIGURE FREE PRODUCT PLUME MAP AS OF FEBRUARY 2015 3B 100 50 0 100 GW46 I Feet Job No.: Date Drawn: Scale: Drawn By: Checked By: SCALE 210022.08 1 MAY 2015 AS SHOWN THW I SAC I� n 764 6s -4 41GI 0) �s WARNING: This document is "FOR OFFICIAL USE ONLY" and it contains info that may be exempt from public release under the FOI Act (5 U.S.C. 552). It is to be handled IAW Doll) policy and is not to be released to the public or personnel who do not have a valid "need -to -know" without prior approval of an authorized DoD official. 41GW42 L'J41PR71 3113:L � 41PR100 W10 �NURO�\� ®1GW104 Gw 41PR70 ® P,R >> �■ 41PR73 41GW103 ❑' 41PR69 d 41GW30 j w> A tv 1 Eil 41GW34 wj j ZP 41GW63 41GW44 41 PR74 AG ❑� 41 GW43 ov 41PR80 41PR76 0 41GW119 Sample ID Well Type Well Depth Date Parameter Results 2L Standard GCL 41GW06 T-11 20.00 8/13/2014 Benzene 1.39000 1.00000 5000.00000 41GW25 T-II 18.50 8/13/2014 Benzene 5.41000 EUnits 1.00000 5000.00000 41PR101 RW 25.00 8/13/2014 Benzene 1.73000 1.00000 5000.00000 41 PR203 RW 25.00 8/13/2014 Benzene 1.14000 1.00000 5000.00000 41 PR212 I RWI 25.0018/13/20141 Benzene I 1.37000 u / 1 1.00000 5000.00000 41GW22 � Go0 � PF1 0 w 's >> �r C+ 41GW111 r- 3777 41GW46 318y 10 1 319.15 1 P- 41PR84 41PR88 ❑■ ❑■ 41GW23 PR85 Ic TV \ w 0 41PR89 41 G W41 L 41GW66 -4 A V• 41PR92 ®41GW24 41PR93 41PR90 ■❑ 0 41GW31 41 PR91 ❑■ 41PR95 ❑ 41GW37 of 41 GW35 n N v 41 PR96 ® ❑41 PR98 ■ 41PR94 El41GW29 41PR99 ❑■ 41 PR97 0 41GW28 41 G W26 41GW38 ANNUAL REPORT (DEC.2013 FEB.2015) SURFACTANT RECIRCULATION PROJECT BUILDING 1083 MCAS CHERRY POINT r� Naval Faciirties Engineering Command LEGEND Well by Type EPA 602 by SM 6200B Well 2L Compliant EPA 602 by SM 6200B • �. RW 2L Non -Compliant Free Product Detected Surface Water EPA 602 by SM 6200B (D T-1 Plume in Excess of 2L Small Tributaries ® T-11 Rivers and Creeks 0° T-111 Building ® Unknown Groundwater Flow Direction Former JP-5 Pipeline NOTES 1. 2L Standard refers to North Carolina Groundwater Quality Standard 15A NCAC 2L.0202. 2. GCL refers to Gross Contaminant Level as defined in "Guildelines for Assessment and Corrective Action for UST Releases" July 15, 2008 Version, change 3 Effective December 1, 2013. 3. A 2L Standard of "0.00" implies a standard has not yet been established. According to NCAC T15:02L, any compound found above laboratory detection limits is considered non -compliant unless otherwise specified by the NCDENR. CATLIN Engineers and Scientists FIGURE EPA METHOD 602 BY SM 6200B COLORIMETRY AND PLUME IN EXCESS A OF 2L AS OF AUGUST 2014 4 100 50 0 100 Feet Job No.: Date Drawn: Scale: Drawn By: Checked By: SCALE 210022.08 MAY 2015 AS SHOWN THW SAC 41GW32 v'A 769 I,.- 7- 41GW62 "A Q04, SOO WARNING: This document is "FOR OFFICIAL USE ONLY" and it contains info that may be exempt from public release under the FOI Act (5 U.S.C. 552). It is to be handled IAW DoD policy and is not to be released to the public or personnel who do not have a valid "need -to -know" without prior approval of an authorized 13'� 41GW42 DoD official. 'y� 41PR71 3� 41 PR100 41GW102 N�RQR\J� 41GW104 PRT ®04.1PR69 ❑41PR70 41 GW103 41GW30 j ® 's 041GW34��41G 41GW105 41GW63 41GW44 5 Q� �O O 11�0 9 41PR72❑41PR204 41 P R203 41 PR73 0 41GW22>> (D >� �, tr �r >s e 41GW111 41GW112 41 PR200 41 PR201 41GW106 e 41 PR 41GW107 7>PR� 41 PR84 41 PR88 41 PR77 I] 041GW05 41GW23 41GW36 �41PR7 --, "X41PR21s 41PR85 ���f R21 a1P 11 41PR212 sr� 41PR82 41GW06 41PR216 41PR213 ? ❑� ..... PR217 ❑� 41 PR86 W 41 PR89 .� ® 1PR214 41 GW03 41GW66 .p v, 41 PR92 ❑(D 41GW24 41PR221 ❑� 41PR86 41 PR220 El 41PR219 R218 41 PR90 �. 41PR93 41 PR68 41 PR75 ' / ^�� 41GW02 0 41PR80 000 41 PR76 > 00 ^I ,UI. `n, 0o 12 13 41GW64 �3l 130 �3S 41GW113 0 -a 41 G W 114 41 PR67 41 PR230 Sample ID Well Type Well Depth Date Parameter Results Units 2L Standard GCL 41GW06 T-11 20.00 8/13/2014 Naphthalene 21.20000 ug/L 6.00000 6000.00000 41GW25 T-II 18.50 8/13/2014 2-Methylnaphthalene 43.20000 ug/L 30.00000 12500.00000 41GW25 T-11 18.50 8/13/2014 Naphthalene 65.70000 ug/L 6.00000 6000.00000 41GW36 RW 20.00 8/13/2014 Naphthalene 12.20000 ug/L 6.00000 6000.00000 41GW64 T-11 18.00 8/13/2014 2-Methylnaphthalene 41.10000 ug/L 30.00000 12500.00000 41GW64 T-11 18.00 8/13/2014 Naphthalene 67.80000 ug/L 6.00000 6000.00000 41GW106 T-11 25.00 8/13/2014 2-Methyl naphthalene 84.50000 ug/L 30.00000 12500.00000 41GW106 T-11 25.00 8/13/2014 Naphthalene 92.80000 ug/L 6.00000 6000.00000 41PR68 RW 30.00 8/13/2014 Naphthalene 50.30000 ug/L 6.00000 6000.00000 41PR75 RW 29.00 8/13/2014 Naphthalene 17.80000 ug/L 6.00000 6000.00000 41PR78 RW 30.50 8/13/2014 Naphthalene 10.90000 ug/L 6.00000 6000.00000 41PR79 RW 30.50 8/13/2014 Naphthalene 27.00000 ug/L 6.00000 6000.00000 41PR101 RW 25.00 8/13/2014 2-Methylnaphthalene 60.10000 ug/L 30.00000 12500.00000 41PR101 RW 25.00 8/13/2014 Naphthalene 52.50000 ug/L 6.00000 6000.00000 41PR203 RW 25.00 8/13/2014 Naphthalene 12.90000 ug/L 6.00000 6000.00000 41PR212 RW 25.00 8/13/2014 Naphthalene 10.40000 ug/L 6.00000 6000.00000 jV141 PR7G0 41GW43 41PR101 _ I ®"',9 641GW33 41GW31 41PR83 ^b 41PR95 41 PR87 41GW37 41PR91 O 41GW108 :�� � 41("""` M9) 41GW65 41GW46 41 PR94 0 El 41PR96 41PR98 101 41GW29 ANNUAL REPORT (DEC. 2013 - FEB. 2015) SURFACTANT RECIRCULATION PROJECT BUILDING 1083 MCAS CHERRY POINT �� f�: �s�l: �.,r:•!i[ • :�. r:�•:3 r-., .. .. r.�'''�=ate-rr.a� .;� LEGEND Well by Type EPA 610 by EPA 625 Well 2L Compliant • EPA 610 by EPA 625 �. RW 2L Non -Compliant Free Product Detected Surface Water EPA 610 by EPA 625 T-1 Plume in Excess of 2L Small Tributaries ® T-I I Rivers and Creeks 0° T-111 Building ® Unknown Groundwater Flow Direction Former JP-5 Pipeline NOTES 1. 2L Standard refers to North Carolina Groundwater Quality Standard 15A NCAC 2L.0202. 2. GCL refers to Gross Contaminant Level as defined in 41 PR99 "Guildelines for Assessment and Corrective Action for 0 UST Releases" July 15, 2008 Version, change 3 41PR97 Effective December 1, 2013. 3. A 2L Standard of "0.00" implies a standard has not yet 41GW28 been established. According to NCAC T15:02L, any ® compound found above laboratory detection limits is considered non -compliant unless otherwise specified by the NCDENR. CATLIN Engineers and Scientists EPA METHOD 610 BY FIGURE EPA METHOD 625 COLORIMETRY AND PLUME IN EXCESS OF 2L 5 100 50 0 100 AS OF AUGUST 2014 Feet Job No.: Date Drawn: Scale: Drawn By: Checked By: SCALE 210022.08 1 MAY 2015 1 AS SHOWN THW 0 SAC APPENDICES DOD; 210022.08_1083_Interim Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 June 2015 APPENDIX A LABORATORY ANALYTICAL REPORTS DOD; 210022.08_1083_Interim Report Dec2013-Feb2015_FINAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 June 2015 ® I Laboratories LLC a member of The GEL Group INC August 28, 2014 Mr. Tom Landis SDC Group, Inc. 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Re: Analytical for Site 1083 Work Order: 354692 Dear Mr. Landis: PO Box 30712 Charleston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766,1178 GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the following analytical results for the sample(s) we received on August 14, 2014, and analyzed for GC/MS Semivolatile and GUMS Volatile. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4485. Sincerely, Hope Taylor for Valerie Davis Project Manager Purchase Order: 6120 Enclosures www.gel.com problem solved SDC Group, Inc. Analytical for Work Order #: 354692 SDG: 354692 Case Narrative Case Narrative for SDC Group, Inc. Analytical for Workorder #: 354692 SDG # : 354692 August 28, 2014 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843)556-8171 Summary Sample receipt The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on August 14, 2014 for analysis. Sample Identification The laboratory received the following samples: Laboratory ID Client ID 354692001 41 GW 113 354692002 41PR67 354692003 41PR80 354692004 41GW06 354692005 41GW33 354692006 41GW999 354692007 41GW23 354692008 41 GW 107 354692009 41PR75 354692010 41PR74 354692011 41PR203 354692012 41 GW 111 354692013 41 GW 112 354692014 41PR78 354692015 41GW64 354692016 41PR212 354692017 41GW36 354692018 41PR79 354692019 41PR101 354692020 41GW25 354692021 41PR68 354692022 41PR77 354692023 41GW106 354692024 Equipment Rinsate Case Narrative GEL Laboratories LLc PO Box 30712 Chadestan, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gal.com Sample analyses were conducted using methodology as outlined in GEL Laboratories, LLC (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Data Package The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: GUMS Semivolatile and GUMS Volatile. I certify that this data report is in compliance with the terms and conditions of the subcontract and task order, both technically and for completeness, for other than the conditions detailed in the attached case narrative. W Hope Taylor for Valerie Davis Project Manager GEL Laboratories LLc PO Box 30712 Chareston, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gal.com List of current GEL Certifications as of 28 August 2014 State Certification Alaska UST-110 Arkansas 88-0651 CLIA 42D0904046 California NELAP 01151 CA Colorado SC00012 Connecticut PH-0169 Delaware SC000122013-10 DoD ELAP/ ISO17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-12-00283, P330-12-00284 Georgia SC00012 Georgia SDWA 967 Hawaii SC000122013-10 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana C—SC-01 Kansas NELAP E-10332 Kentucky 90129 Louisiana NELAP 03046 (AI33904) Louisiana SDWA LA130005 Maryland 270 Massachusetts M—SC012 Michigan 9976 Mississippi SC000122013-10 Nebraska NE—OS-26-13 Nevada SC000122014-1 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 Oklahoma 9904 Pennsylvania NELAP 68-00485 Plant Material Permit PDEP-12-00260 South Carolina Chemistry 10120001 South Carolina GVL 23611001 South Carolina Radiochemi 10120002 Tennessee TN 02934 Texas NELAP T104704235-14-9 Utah NELAP SC000122014-14 Vermont VT87156 Virginia NELAP 460202 Washington C780-12 Wisconsin 999887790 Chain of Custody and Supporting Documentation Page: Iof GEL Laboratories, LLC Project#: o GEL Chain of Custody and Analytical Request 2040SavageRoad GEL Quote #: .,�❑ Charleston, 5C 29407 Number [ �: PO Number: �6 0 GEL Work Order Number:COC Phone: (843) 556-8171 Fax: {843} 765-1.178 Client Name: f, `-t ts' � Ph is; vQ 17- Sample Analysis Requested tsl 7 (Fill in the number of containers for each test) ProjectJSite Name: 16?Z Fax 11: Should this L. HA - r_- Preservative Type (d) Address: I%lip ��j) IyJac,�7 Ch L^[�?.! D TC� IYI Sample be considered: ` Comments Collected by; Send Results To: 9 Note: is r— r fi ► 6 /Y1 p extra sample 'l me 'DateCnuected = 8 - e Q required for sample 4 P Sample ID Collected DC Cock Field (l(htlm ry) t Pilfered "' Sample a Matrix "'! s U y specific QC For composites - indicatestartand step dratelUme [ mm�d- yy) F a F q j(ghmm) I Y3tQ L1� -5 3 -. 1!7Q �t/ 7 r 0: 13 C� 3 ec +Lar,- ` IG ltzb U) 5 3 13 Ic1 07 -Zo Al Csu3 5 3 2- Y r� /"l c7 25 /V � ?, a I L 10 3 o; N 611.E 5 3 41 1 -7S 3,11el 011:5, N W 5 3 � �Vr Pr' 7 /2 c q.. 35 N U) -S 13 A TAT Requested: Normal; flush: Specify: (subject to Surcharge), I Fax Results: Yes 1 Na j Circle Deliverable. C ofA 1 C Summary 1 Level 1 1 Level 2 I Level 3 1 Level 4 Remarks.- Are there any known hazards applicable to these samples? If, so, please list the hazards Sam le Collection Time Zone astern Pacific Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details Relinquished By (Signed) fate Time Re ed h} (signed) !:)a F,;e GEL PM: Method ofShiymcnt: Date Shipped: 2 , Airbili rt• 3 3 Airbill #_ l,l Chain orCuslody NLimber = Client Determined For Lab Receiving Use Only 1) ¢C Codes: N = Normal Sample. TB = Trip Stank, FD = meld Duplicate, EB = Equipment BFank. %IS i .Matrix Spike 5ample, MSD • Matrix Spike Duplicate Sample, G = Grab, C = Composite 3,) Field FiAered: For liquid matrices, indicate with a - V - for yes the Sample was field filtered or - N- torple was not field filtered. Cuslody' Seat Intact? 4.) Matriv. Codes: ➢W=Drinking Water. GW=Groundwater, S Y-Surface Water, WW=Waste Wafer, ater. SO-Soil.SD=Sediment. SL=Sludge.5S=Solid Wash. O�Cil. F40ter. P-Wipe, V-Uhine, F-Fecal, N=Nasal YES NO S.) Sample Analysis Requesled: Analytical method requested [i,e. 92608.56rOW7470A I and ntanher of c"iners prodded for each (i& 82608 - 3, 601OB17470A -1)• Cooler Temp: 6.) Preservative Typc nA = hydrochloric Acid, NI = Nitric Acid, Sii - Sodium Hydroxide. SA - Sulfuric �4td. AA - Ascorbiv. Acid, 1[x = Hexane, ST = Sodium Thiosulrate. II`no preservative is added - leave Field blank C WHITE = LABORATORV I vr.i.i nw = Fri F PrNrc = rr re; NT Page: of GEL Laboratories, LLC Project;!!: b 3 GEL Chain of Custody and Analytical Request 2D40 Savage Road GEL Quote #: D:5D Charleston, SC 29407 CGCNumberil): Phone: (843) 556-8171 GEL Work Order Numbers NumberPa Numhe Fax- (843) 766-1178 Client Name: Phone t€:- is) �� ��� r ��'� � �� Sample Analysis Requested (Fill in the number of containers for each test) Project/Site Name: /�1 Fax #: Should this Sample be considered: 16 w a Preservative Type (6) Address: r7 r1� �1?fir j� ° Comments Nate: extra sample is required for sample Collected by: "� F. A ,� Send Results Ta: N' C , nq Lan & �,° • Date Col Iceted ,*Time dollected Field Sample ID QC de Co ,, Sample o � specific QC a For composites - Indicate start and crap dore/rime mm-dd- i YY) I07lhtary) to Filtered Matrix „ a Q y 5, 31 A Do7 ew) r i Y� /Q ��, L� s 3 g1C2�� �. -s GW s 3 r' ss 0 e � �w 5 3 a r TW/0 o3�'; N Ki i.r`7 TAT Requested: Normal: X Rush: 5 eci : isubjvcttosurehargc) Fax Results: Yes i No Circle Deliverable: C of 2C Summary i Level I 1 Level 1 Level 3 / Level 4 Remarks. Are there any known hazards applicable to these samples? ff ski, please fist the hazards Sa=le oll c ion Time Zone Eastern Pacific Central Other Mountain Chain of Custody Signatures Sample Stripping and Delivery Details Relinquished By (Signe Date Time Receiv d b} {signed) Date Time GEL PM: l % �T �r g 11' ! J rVD Method of Shi went: Date Shipped: 2 2 Airbill 3 13 Airhill a: I.) Chain of Custody Number = Client Determined 2.) QC Codes: N = Nrnmal Sample. TS = Trip Blank, Fri =Field Duplicatc, EB = Equipment Blank, ht5 Mauix Spike Sample, MSD - Matrix Spike Duplicate Sam plc. G - Grab, C = Composite For Lab Receiving Use Only 3.) Field Flltered: For liquid matrices, indicate with a - Y - for yes the sample was field filtered or - N - for sample was not field filtered. Custody Seat Intact? 4.) Matrix Codes: DW=Drinking Water. G—Groundwater. Sw-surface Waur. ww=Waste Water. W= rater, SO -Soil. St)=Sedimem, St.-Sludsc, SS-Solld Wasw.0-011. F=Filter. P=Wipe. U=Urine, F=Fccal. N=Nasal YES NO S.) Sample Analysis Requested: Analytical method requested (i.e. 92608. 60i1013r14'70A) and number ore lainers provided for each 0,c_ 8260B - 3, 401 RB11470A - 1). Cooler Temp' 6.) Preservative Type; HA - Hydrochloric Acid, Ni = Nitric Acid. SH = Sodium Hydroxide, SA - Sulfuric �cid, AA = Ascorbic Acid. HX = Hexane, ST - Sodium Thiosulfatc, Ifno preservative is added = icave rield blank C WHITE = LABORATCIRY l wi-i-f1W = FtF PiNW -f i.fiF.NT Page. 3 of a GEL Laboratories, LLC Project#: 1025 GEL Chain of Custody and Analytical Request 204OSavage Road GEL Quote #: P Charleston, SC 29407 CGC Number t": GEL Work Order Number: Phone- (843) 556-8171 PO Number: [] I Fax: (843) 766-1 l78 Client Name: FS Phone #�� _ /��� �� ! Sample Analysis Requested [s) (Fill in the number of containers for each test) Fax #: Project/Site ]'Jame: ! V Should this Preservative Type (6) fJ� sample be a' Address: MC1Ac /J �, 1 + A r considered: ,° a c �.9 Comments Note: extra sample is req uired for sample Collected b : �`M'�^f Send Results To: y r, Df y� 5 T m •Date Collected •Time Sample ID Culld ccte Qctaae Field Sample C1 specific QC • For composites - lndicare snarl and stop darelrime tmmald _vy> X.Mlitary) (Ithmm)" i), Filtered "' Matrix cs r a h 1 rr ]5 I tl EI 1 S 3 2- -VoA> tab to &1130 S 3 15 3 U) -2_ e TAT Regnested: Normal: Rush: S eciJ abject to Surcharge) Fax Results: Yes No Circle Deliverable: C of QC Summary / Level l ! Level 1 Level 3 i Level 4 Remarks.- Are there any known hazards applicable to these samples? If so, please list the hazards SampleLpflection Time Zone Easter Paciric Central Other Mountain Chain of Custody Signatures Sample Shipping and Delivery Details _Relinquished By (Signed) Bate Time Rec ' d by (signed) Bate Time GEL PM- 1 l j/ M I I /I I s ►/ Method of Shipment: date Shipped; 2 2 Airbill b: 3 13 Airbili k: I.) Chain of Custody Number = Client Determincd For Lob Receiving Use Only 2.) QC Codes: N - Normal Sample, TS - Trip Blank. FD = Field Duplicate, ES - Cquipment Stank. Mao = Matrix Spike Samplc. MSO = Matrix Spike Duplicate sample, G - Grab, C = Composite 3.) Field Filtered_ For liquid matrices. indicate with a - Y - for yes lice sample was Geld filtered or- N - Corsampie was not field filtered. Custody Seal intact? 4.) Matrix Codes: DW=Drinking Water, GW-Groundwater, Sw-Surrace Water, WW=Waste Water, lll-Water. SO -Soil. SD=Scdiment, SL-Sludge, 55=Solid Waste, p-Oil. F=Filter. P=Wipe, U-Urine, F=Fecal. N=Nasal YES NO 5.) Sample Analysis Requested: Analytical method requested (i.e- 82600, 60100n470A) and number of comaimrs provided for each (1-e. 8260E - 3,6010817470A . 1)- Cooler Ternp. C-A;­ Tl,inru,(avr rr,... ....:r+7.7vf..r :. ,.,tArd e< Irnvr fr.elr! hlan4c C 0.) r"WrVauve lypc: nn - nyuruun,unc nww. i,. - .,,., �. „�,... .... - .�w,,,v„ ,.wv..r,r.�. .•,-• .,....,......_........ ..---. -.- ..-._, WHITF = I.ARf1RATORY YELLOW = FILL PINK=CLIENT L..abn[aiieS LI_E- SAMPLE RECEIPT & REVIEW FORM Client; SDClARICDCAVork der: 0 CIO Received I3 : l Date Received: Suspected lea cord Informationd o *IrNet Counts > I00cpm on sa nflilcs not mih ark "radioactve", contact te Radiation Safety Group for III rtlrcr investigation. COC/Sainplc�s marked ws raditlactive? M$,Yinitnn Net Counts Observcd* (Observed Counts - Area Background Counts): Classified R,udivactivc 11 or Ill by RSO? Kilf yes, Wure swipes Laken ol"sample cunlaliners a action levels? COClsarn les marked ewituining PCBs? xi Package, COC, andlor Samples marked as beryllium or asbestos conwining'! If yes, samples a c to be segn;gcntcd as Sarety Controlled Samples, and opened by the GI?I, Safety Oroup. Sh ipped as a DOT Hazardous? I Ia7Ard Class Shipped: tJNN: Sam les identified as rorei n Soil? Sample IZcreipl Crilerin �°', Cnlnawnts/QuHliflers (Required for Non -Conforming lions) 1 Shipping coniainers TccOived intas l circle AppiiwWc. Seals broken Damaged container leaking container other (describe ) and sealed? I Samples requiring cold preservation Pmcrvulior1 hlatho 4 lec Blue ice Ivry iris Nonc Othcr(d=ribc) within (0 _< G deg. C)?* x [I' all temperatures are recorded in Celsius +. 22 Daily check performed Lind passed on Tcmperaturc Dwce Surial #- Securidary TcmVeraturc Devices Scriat II (If Applicable): 9 IR temperature~ guiV 3 Chain ol'costody rinctimants included with shipment? - Circle Appliclrble: A Sample containers intact and scaled? Seals broken Damaged container Leaking container Other (describe) Samples requiring chemical Sample IM, carl imors alIectad and oh9erved pH: i presorvalion at proper pI l? G VOA vials free of headspace (defined Sam Ic 's and wriloinors aNctud as < 6mrn bubble)? r i (If yes, immediately deliver to Vulaliles laboratory) 7 Are Encore containers present? Samples received within holding ID's and tests drreeWd 8 time:? Sample ID's on COC: match ID's till St in;plc Iffs and containers 41111xled: bottles? Date & time on COC ninwh date Sample It's aflecled: 10 time on boilles? - Number of c:cmiainers rercivcd match Sample Ilys anected: 11 nurnber indicated on 1_:OL'7 12 Are saniple containers identifiable as GEL provided? 13 COC form is properly signed in rc.Iirtquishedlrcceivcd sections? Circle Applicable: L,lr-. Ai, redEx Ground UPS Field Services C'tnlrier 0111ur 5 7' 0/1 *q T Y 14 Carrier and tracking number. t , p 0'];� (*- 5?� Comments (Usc Continuation Form il'needcd); � i � � � `i +J� f JJ PM (or PMA) tQViL'w' lnitial5 Date s { ]'age Of 1 Data Review Qualifier Flag Definition Sheet Data Review Qualifier Definitions Qualifier Explanation * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound < Result is less than value reported > Result is greater than value reported RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank B Metals -Either presence of analyte detected in the associated blank, or MDL/IDL < sample value < PQL BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample d 5-day BOD-The 2:1 depletion requirement was not met for this sample E Organics -Concentration of the target analyte exceeds the instrument calibration range E Metals -%difference of sample and SD is >10%. Sample concentration must meet flagging criteria H Analytical holding time was exceeded h Preparation or preservation holding time was exceeded J Value is estimated N Metals -The Matrix spike sample recovery is not within specified control limits N Organics -Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest internal standard response factor N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more ND Analyte concentration is not detected above the reporting limit UI Gamma Spectroscopy -Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound Z Paint Filter Test -Particulates passed through the filter, however no free liquids were observed. GEL Laboratories LLc PO Box 30712 Charestan, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gal.com P Organics -The concentrations between the primary and confirmation columns/detectors is >40% difference. For HPLC, the difference is >70%. U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD. GEL Laboratories LLc PO Box 30712 Charestan, SC 29417 2040 Savage Road Charleston, SC 29407 P 843.556.8171 F 843.766.1178 www.gal.com GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for SDCGO01 SDC Group, Inc. Client SDG: 354692 GEL Work Order: 354692 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a Tracer compound ** Analyte is a surrogate compound E Concentration of the target analyte exceeds the instrument calibration range J Value is estimated U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis. The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above. This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Valerie Davis. Reviewed by GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW113 354692001 GW 13-AUG-14 13:30 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 16.9 0.300 1.00 ug/L 1 JMB3 08/20/14 2135 1412623 1 Acenaphthene J 0.420 0.300 1.00 ug/L 1 Acenaphthylene U ND 0.300 1.00 ug/L 1 Anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)pyrene U ND 0.300 1.00 ug/L 1 Benzo(b)fluoranthene U ND 0.300 1.00 ug/L 1 Benzo(ghi)perylene U ND 0.300 1.00 ug/L 1 Benzo(k)fluoranthene U ND 0.300 1.00 ug/L 1 Chrysene U ND 0.300 1.00 ug/L 1 Dibenzo(a,h)anthracene U ND 0.300 1.00 ug/L 1 Fluoranthene U ND 0.300 1.00 ug/L 1 Fluorene J 0.590 0.300 1.00 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.300 1.00 ug/L 1 Naphthalene 1.19 0.300 1.00 ug/L 1 Phenanthrene U ND 0.300 1.00 ug/L 1 Pyrene U ND 0.300 1.00 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 1404 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW113 Project: SDCGO0213 Sample ID: 354692001 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 38.1 ug/L 50.0 76.2 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 39.3 ug/L 50.0 78.5 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 29.9 ug/L 50.0 59.7 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 50.4 ug/L 50.0 101 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 51.1 ug/L 50.0 102 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 53.8 ug/L 50.0 108 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR67 354692002 GW 13-AUG-14 07:45 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.300 1.00 ug/L 1 JMB3 08/20/14 2308 1412623 1 Acenaphthene U ND 0.300 1.00 ug/L 1 Acenaphthylene U ND 0.300 1.00 ug/L 1 Anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)pyrene U ND 0.300 1.00 ug/L 1 Benzo(b)fluoranthene U ND 0.300 1.00 ug/L 1 Benzo(ghi)perylene U ND 0.300 1.00 ug/L 1 Benzo(k)fluoranthene U ND 0.300 1.00 ug/L 1 Chrysene U ND 0.300 1.00 ug/L 1 Dibenzo(a,h)anthracene U ND 0.300 1.00 ug/L 1 Fluoranthene U ND 0.300 1.00 ug/L 1 Fluorene U ND 0.300 1.00 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.300 1.00 ug/L 1 Naphthalene U ND 0.300 1.00 ug/L 1 Phenanthrene U ND 0.300 1.00 ug/L 1 Pyrene U ND 0.300 1.00 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 1433 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR67 Project: SDCGO0213 Sample ID: 354692002 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 38.9 ug/L 50.0 77.9 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 41.1 ug/L 50.0 82.2 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 40.1 ug/L 50.0 80.2 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 49.1 ug/L 50.0 98.2 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 49.1 ug/L 50.0 98.2 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.5 ug/L 50.0 103 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR80 354692003 GW 13-AUG-14 08:30 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 0.962 0.286 0.952 ug/L 1 JMB3 08/20/14 2339 1412623 1 Acenaphthene J 0.457 0.286 0.952 ug/L 1 Acenaphthylene U ND 0.286 0.952 ug/L 1 Anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)pyrene U ND 0.286 0.952 ug/L 1 Benzo(b)fluoranthene U ND 0.286 0.952 ug/L 1 Benzo(ghi)perylene U ND 0.286 0.952 ug/L 1 Benzo(k)fluoranthene U ND 0.286 0.952 ug/L 1 Chrysene U ND 0.286 0.952 ug/L 1 Dibenzo(a,h)anthracene U ND 0.286 0.952 ug/L 1 Fluoranthene U ND 0.286 0.952 ug/L 1 Fluorene J 0.314 0.286 0.952 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.286 0.952 ug/L 1 Naphthalene 1.50 0.286 0.952 ug/L 1 Phenanthrene U ND 0.286 0.952 ug/L 1 Pyrene U ND 0.286 0.952 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 1502 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene J 0.350 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR80 Project: SDCGO0213 Sample ID: 354692003 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 33.8 ug/L 47.6 71.0 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 33.8 ug/L 47.6 71.0 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 34.6 ug/L 47.6 72.7 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 53.9 ug/L 50.0 108 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 50.0 ug/L 50.0 100 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.4 ug/L 50.0 103 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW06 354692004 GW 13-AUG-14 07:15 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 8.89 0.288 0.962 ug/L 1 JMB3 08/21/14 0010 1412623 1 Acenaphthene U ND 0.288 0.962 ug/L 1 Acenaphthylene U ND 0.288 0.962 ug/L 1 Anthracene U ND 0.288 0.962 ug/L 1 Benzo(a)anthracene U ND 0.288 0.962 ug/L 1 Benzo(a)pyrene U ND 0.288 0.962 ug/L 1 Benzo(b)fluoranthene U ND 0.288 0.962 ug/L 1 Benzo(ghi)perylene U ND 0.288 0.962 ug/L 1 Benzo(k)fluoranthene U ND 0.288 0.962 ug/L 1 Chrysene U ND 0.288 0.962 ug/L 1 Dibenzo(a,h)anthracene U ND 0.288 0.962 ug/L 1 Fluoranthene U ND 0.288 0.962 ug/L 1 Fluorene U ND 0.288 0.962 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.288 0.962 ug/L 1 Naphthalene 21.2 0.288 0.962 ug/L 1 Phenanthrene U ND 0.288 0.962 ug/L 1 Pyrene U ND 0.288 0.962 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 1530 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene 1.39 0.300 1.00 ug/L 1 Ethylbenzene 2.64 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) J 1.49 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW06 Project: SDCGO0213 Sample ID: 354692004 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 29.5 ug/L 48.1 61.3 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 38.8 ug/L 48.1 80.8 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 36.4 ug/L 48.1 75.6 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 54.1 ug/L 50.0 108 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 51.3 ug/L 50.0 103 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.7 ug/L 50.0 103 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW33 354692005 GW 13-AUG-14 07:20 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.294 0.980 ug/L 1 JMB3 08/21/14 0041 1412623 1 Acenaphthene U ND 0.294 0.980 ug/L 1 Acenaphthylene U ND 0.294 0.980 ug/L 1 Anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)pyrene U ND 0.294 0.980 ug/L 1 Benzo(b)fluoranthene U ND 0.294 0.980 ug/L 1 Benzo(ghi)perylene U ND 0.294 0.980 ug/L 1 Benzo(k)fluoranthene U ND 0.294 0.980 ug/L 1 Chrysene U ND 0.294 0.980 ug/L 1 Dibenzo(a,h)anthracene U ND 0.294 0.980 ug/L 1 Fluoranthene U ND 0.294 0.980 ug/L 1 Fluorene U ND 0.294 0.980 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.294 0.980 ug/L 1 Naphthalene U ND 0.294 0.980 ug/L 1 Phenanthrene U ND 0.294 0.980 ug/L 1 Pyrene U ND 0.294 0.980 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 2159 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW33 Project: SDCGO0213 Sample ID: 354692005 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 39.6 ug/L 49.0 80.7 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 38.6 ug/L 49.0 78.7 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 43.4 ug/L 49.0 88.5 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 55.5 ug/L 50.0 ill (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 49.7 ug/L 50.0 99.3 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.9 ug/L 50.0 104 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW999 354692006 GW 13-AUG-14 07:25 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.283 0.943 ug/L 1 JMB3 08/21/14 0112 1412623 1 Acenaphthene U ND 0.283 0.943 ug/L 1 Acenaphthylene U ND 0.283 0.943 ug/L 1 Anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)pyrene U ND 0.283 0.943 ug/L 1 Benzo(b)fluoranthene U ND 0.283 0.943 ug/L 1 Benzo(ghi)perylene U ND 0.283 0.943 ug/L 1 Benzo(k)fluoranthene U ND 0.283 0.943 ug/L 1 Chrysene U ND 0.283 0.943 ug/L 1 Dibenzo(a,h)anthracene U ND 0.283 0.943 ug/L 1 Fluoranthene U ND 0.283 0.943 ug/L 1 Fluorene U ND 0.283 0.943 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.283 0.943 ug/L 1 Naphthalene U ND 0.283 0.943 ug/L 1 Phenanthrene U ND 0.283 0.943 ug/L 1 Pyrene U ND 0.283 0.943 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 2227 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW999 Project: SDCGO0213 Sample ID: 354692006 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 38.2 ug/L 47.2 81.0 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 37.6 ug/L 47.2 79.7 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 41.8 ug/L 47.2 88.6 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 54.0 ug/L 50.0 108 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 50.4 ug/L 50.0 101 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 52.3 ug/L 50.0 105 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW23 354692007 GW 13-AUG-14 08:00 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.294 0.980 ug/L 1 JMB3 08/21/14 0143 1412623 1 Acenaphthene J 0.490 0.294 0.980 ug/L 1 Acenaphthylene U ND 0.294 0.980 ug/L 1 Anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)pyrene U ND 0.294 0.980 ug/L 1 Benzo(b)fluoranthene U ND 0.294 0.980 ug/L 1 Benzo(ghi)perylene U ND 0.294 0.980 ug/L 1 Benzo(k)fluoranthene U ND 0.294 0.980 ug/L 1 Chrysene U ND 0.294 0.980 ug/L 1 Dibenzo(a,h)anthracene U ND 0.294 0.980 ug/L 1 Fluoranthene U ND 0.294 0.980 ug/L 1 Fluorene J 0.373 0.294 0.980 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.294 0.980 ug/L 1 Naphthalene J 0.755 0.294 0.980 ug/L 1 Phenanthrene U ND 0.294 0.980 ug/L 1 Pyrene U ND 0.294 0.980 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 1124 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW23 Project: SDCGO0213 Sample ID: 354692007 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 35.0 ug/L 49.0 71.3 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 36.2 ug/L 49.0 73.9 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 44.4 ug/L 49.0 90.6 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 57.0 ug/L 50.0 114 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 51.7 ug/L 50.0 103 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.7 ug/L 50.0 103 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW107 354692008 GW 13-AUG-14 08:00 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.300 1.00 ug/L 1 JMB3 08/21/14 0214 1412623 1 Acenaphthene U ND 0.300 1.00 ug/L 1 Acenaphthylene U ND 0.300 1.00 ug/L 1 Anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)pyrene U ND 0.300 1.00 ug/L 1 Benzo(b)fluoranthene U ND 0.300 1.00 ug/L 1 Benzo(ghi)perylene U ND 0.300 1.00 ug/L 1 Benzo(k)fluoranthene U ND 0.300 1.00 ug/L 1 Chrysene U ND 0.300 1.00 ug/L 1 Dibenzo(a,h)anthracene U ND 0.300 1.00 ug/L 1 Fluoranthene U ND 0.300 1.00 ug/L 1 Fluorene U ND 0.300 1.00 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.300 1.00 ug/L 1 Naphthalene J 0.830 0.300 1.00 ug/L 1 Phenanthrene U ND 0.300 1.00 ug/L 1 Pyrene U ND 0.300 1.00 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 2255 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW107 Project: SDCGO0213 Sample ID: 354692008 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 37.6 ug/L 50.0 75.3 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 38.2 ug/L 50.0 76.3 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 39.1 ug/L 50.0 78.2 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 53.6 ug/L 50.0 107 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 49.2 ug/L 50.0 98.4 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.3 ug/L 50.0 103 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR75 354692009 GW 13-AUG-14 09:50 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 6.74 0.283 0.943 ug/L 1 JMB3 08/21/14 0245 1412623 1 Acenaphthene U ND 0.283 0.943 ug/L 1 Acenaphthylene U ND 0.283 0.943 ug/L 1 Anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)pyrene U ND 0.283 0.943 ug/L 1 Benzo(b)fluoranthene U ND 0.283 0.943 ug/L 1 Benzo(ghi)perylene U ND 0.283 0.943 ug/L 1 Benzo(k)fluoranthene U ND 0.283 0.943 ug/L 1 Chrysene U ND 0.283 0.943 ug/L 1 Dibenzo(a,h)anthracene U ND 0.283 0.943 ug/L 1 Fluoranthene U ND 0.283 0.943 ug/L 1 Fluorene U ND 0.283 0.943 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.283 0.943 ug/L 1 Naphthalene 17.8 0.283 0.943 ug/L 1 Phenanthrene U ND 0.283 0.943 ug/L 1 Pyrene U ND 0.283 0.943 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 2323 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene J 0.440 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR75 Project: SDCGO0213 Sample ID: 354692009 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 30.3 ug/L 47.2 64.3 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 30.2 ug/L 47.2 64.1 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 43.6 ug/L 47.2 92.5 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 52.5 ug/L 50.0 105 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 50.4 ug/L 50.0 101 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 50.9 ug/L 50.0 102 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR74 354692010 GW 13-AUG-14 09:35 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.294 0.980 ug/L 1 JMB3 08/21/14 0316 1412623 1 Acenaphthene U ND 0.294 0.980 ug/L 1 Acenaphthylene U ND 0.294 0.980 ug/L 1 Anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)pyrene U ND 0.294 0.980 ug/L 1 Benzo(b)fluoranthene U ND 0.294 0.980 ug/L 1 Benzo(ghi)perylene U ND 0.294 0.980 ug/L 1 Benzo(k)fluoranthene U ND 0.294 0.980 ug/L 1 Chrysene U ND 0.294 0.980 ug/L 1 Dibenzo(a,h)anthracene U ND 0.294 0.980 ug/L 1 Fluoranthene U ND 0.294 0.980 ug/L 1 Fluorene U ND 0.294 0.980 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.294 0.980 ug/L 1 Naphthalene U ND 0.294 0.980 ug/L 1 Phenanthrene U ND 0.294 0.980 ug/L 1 Pyrene U ND 0.294 0.980 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/26/14 2351 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR74 Project: SDCGO0213 Sample ID: 354692010 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 31.5 ug/L 49.0 64.3 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 30.3 ug/L 49.0 61.9 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 45.8 ug/L 49.0 93.5 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 54.6 ug/L 50.0 109 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 50.5 ug/L 50.0 101 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 50.9 ug/L 50.0 102 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR203 354692011 GW 13-AUG-14 08:40 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 7.39 0.286 0.952 ug/L 1 JMB3 08/21/14 0346 1412623 1 Acenaphthene J 0.648 0.286 0.952 ug/L 1 Acenaphthylene U ND 0.286 0.952 ug/L 1 Anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)pyrene U ND 0.286 0.952 ug/L 1 Benzo(b)fluoranthene U ND 0.286 0.952 ug/L 1 Benzo(ghi)perylene U ND 0.286 0.952 ug/L 1 Benzo(k)fluoranthene U ND 0.286 0.952 ug/L 1 Chrysene U ND 0.286 0.952 ug/L 1 Dibenzo(a,h)anthracene U ND 0.286 0.952 ug/L 1 Fluoranthene U ND 0.286 0.952 ug/L 1 Fluorene J 0.505 0.286 0.952 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.286 0.952 ug/L 1 Naphthalene 12.9 0.286 0.952 ug/L 1 Phenanthrene U ND 0.286 0.952 ug/L 1 Pyrene U ND 0.286 0.952 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 0019 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene 1.14 0.300 1.00 ug/L 1 Ethylbenzene 3.17 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) 6.21 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR203 Project: SDCGO0213 Sample ID: 354692011 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 36.2 ug/L 47.6 76.1 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 33.0 ug/L 47.6 69.3 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 46.8 ug/L 47.6 98.2 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 52.9 ug/L 50.0 106 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 51.5 ug/L 50.0 103 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 49.8 ug/L 50.0 99.6 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GWI I I 354692012 GW 13-AUG-14 09:00 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.283 0.943 ug/L 1 JMB3 08/21/14 0417 1412623 1 Acenaphthene U ND 0.283 0.943 ug/L 1 Acenaphthylene U ND 0.283 0.943 ug/L 1 Anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)pyrene U ND 0.283 0.943 ug/L 1 Benzo(b)fluoranthene U ND 0.283 0.943 ug/L 1 Benzo(ghi)perylene U ND 0.283 0.943 ug/L 1 Benzo(k)fluoranthene U ND 0.283 0.943 ug/L 1 Chrysene U ND 0.283 0.943 ug/L 1 Dibenzo(a,h)anthracene U ND 0.283 0.943 ug/L 1 Fluoranthene U ND 0.283 0.943 ug/L 1 Fluorene U ND 0.283 0.943 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.283 0.943 ug/L 1 Naphthalene U ND 0.283 0.943 ug/L 1 Phenanthrene U ND 0.283 0.943 ug/L 1 Pyrene U ND 0.283 0.943 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 0047 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GWI I I Project: SDCGO0213 Sample ID: 354692012 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 30.1 ug/L 47.2 63.8 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 29.4 ug/L 47.2 62.4 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 40.3 ug/L 47.2 85.5 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 54.9 ug/L 50.0 110 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 49.3 ug/L 50.0 98.6 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 50.8 ug/L 50.0 102 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW112 354692013 GW 13-AUG-14 09:15 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.283 0.943 ug/L 1 JMB3 08/21/14 0448 1412623 1 Acenaphthene U ND 0.283 0.943 ug/L 1 Acenaphthylene U ND 0.283 0.943 ug/L 1 Anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)pyrene U ND 0.283 0.943 ug/L 1 Benzo(b)fluoranthene U ND 0.283 0.943 ug/L 1 Benzo(ghi)perylene U ND 0.283 0.943 ug/L 1 Benzo(k)fluoranthene U ND 0.283 0.943 ug/L 1 Chrysene U ND 0.283 0.943 ug/L 1 Dibenzo(a,h)anthracene U ND 0.283 0.943 ug/L 1 Fluoranthene U ND 0.283 0.943 ug/L 1 Fluorene U ND 0.283 0.943 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.283 0.943 ug/L 1 Naphthalene U ND 0.283 0.943 ug/L 1 Phenanthrene U ND 0.283 0.943 ug/L 1 Pyrene U ND 0.283 0.943 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 1055 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW112 Project: SDCGO0213 Sample ID: 354692013 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 30.3 ug/L 47.2 64.3 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 30.4 ug/L 47.2 64.5 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 41.4 ug/L 47.2 87.8 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 57.2 ug/L 50.0 114 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 51.8 ug/L 50.0 104 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 53.2 ug/L 50.0 106 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR78 354692014 GW 13-AUG-14 10:00 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 12.0 0.283 0.943 ug/L 1 JMB3 08/21/14 0519 1412623 1 Acenaphthene J 0.340 0.283 0.943 ug/L 1 Acenaphthylene U ND 0.283 0.943 ug/L 1 Anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)pyrene U ND 0.283 0.943 ug/L 1 Benzo(b)fluoranthene U ND 0.283 0.943 ug/L 1 Benzo(ghi)perylene U ND 0.283 0.943 ug/L 1 Benzo(k)fluoranthene U ND 0.283 0.943 ug/L 1 Chrysene U ND 0.283 0.943 ug/L 1 Dibenzo(a,h)anthracene U ND 0.283 0.943 ug/L 1 Fluoranthene U ND 0.283 0.943 ug/L 1 Fluorene J 0.396 0.283 0.943 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.283 0.943 ug/L 1 Naphthalene 10.9 0.283 0.943 ug/L 1 Phenanthrene U ND 0.283 0.943 ug/L 1 Pyrene U ND 0.283 0.943 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 0116 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene 2.35 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) 4.96 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR78 Project: SDCGO0213 Sample ID: 354692014 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 33.4 ug/L 47.2 70.9 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 33.8 ug/L 47.2 71.6 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 47.0 ug/L 47.2 99.6 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 54.7 ug/L 50.0 109 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 49.7 ug/L 50.0 99.4 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.0 ug/L 50.0 102 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW64 354692015 GW 13-AUG-14 10:45 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 41.1 0.286 0.952 ug/L 1 JMB3 08/21/14 0550 1412623 1 Acenaphthene U ND 0.286 0.952 ug/L 1 Acenaphthylene U ND 0.286 0.952 ug/L 1 Anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)pyrene U ND 0.286 0.952 ug/L 1 Benzo(b)fluoranthene U ND 0.286 0.952 ug/L 1 Benzo(ghi)perylene U ND 0.286 0.952 ug/L 1 Benzo(k)fluoranthene U ND 0.286 0.952 ug/L 1 Chrysene U ND 0.286 0.952 ug/L 1 Dibenzo(a,h)anthracene U ND 0.286 0.952 ug/L 1 Fluoranthene U ND 0.286 0.952 ug/L 1 Fluorene J 0.743 0.286 0.952 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.286 0.952 ug/L 1 Naphthalene 67.8 0.286 0.952 ug/L 1 Phenanthrene U ND 0.286 0.952 ug/L 1 Pyrene U ND 0.286 0.952 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 0144 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene J 0.330 0.300 1.00 ug/L 1 Ethylbenzene J 0.310 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW64 Project: SDCGO0213 Sample ID: 354692015 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 36.9 ug/L 47.6 77.5 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 38.1 ug/L 47.6 80.0 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 45.2 ug/L 47.6 94.9 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 56.0 ug/L 50.0 112 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 52.1 ug/L 50.0 104 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.9 ug/L 50.0 104 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41PR212 354692016 GW 13-AUG-14 11:55 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 8.39 0.286 0.952 ug/L 1 JMB3 08/21/14 0621 1412623 1 Acenaphthene U ND 0.286 0.952 ug/L 1 Acenaphthylene U ND 0.286 0.952 ug/L 1 Anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)anthracene U ND 0.286 0.952 ug/L 1 Benzo(a)pyrene U ND 0.286 0.952 ug/L 1 Benzo(b)fluoranthene U ND 0.286 0.952 ug/L 1 Benzo(ghi)perylene U ND 0.286 0.952 ug/L 1 Benzo(k)fluoranthene U ND 0.286 0.952 ug/L 1 Chrysene U ND 0.286 0.952 ug/L 1 Dibenzo(a,h)anthracene U ND 0.286 0.952 ug/L 1 Fluoranthene U ND 0.286 0.952 ug/L 1 Fluorene J 0.410 0.286 0.952 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.286 0.952 ug/L 1 Naphthalene 10.4 0.286 0.952 ug/L 1 Phenanthrene U ND 0.286 0.952 ug/L 1 Pyrene U ND 0.286 0.952 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 1152 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene 1.37 0.300 1.00 ug/L 1 Ethylbenzene 2.03 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) J 1.28 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR212 Project: SDCGO0213 Sample ID: 354692016 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 29.4 ug/L 47.6 61.8 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 32.4 ug/L 47.6 68.0 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 40.6 ug/L 47.6 85.2 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 55.8 ug/L 50.0 112 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 48.6 ug/L 50.0 97.3 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 51.8 ug/L 50.0 104 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW36 354692017 GW 13-AUG-14 13:00 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 26.9 0.294 0.980 ug/L 1 JMB3 08/21/14 0652 1412623 1 Acenaphthene U ND 0.294 0.980 ug/L 1 Acenaphthylene U ND 0.294 0.980 ug/L 1 Anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)pyrene U ND 0.294 0.980 ug/L 1 Benzo(b)fluoranthene U ND 0.294 0.980 ug/L 1 Benzo(ghi)perylene U ND 0.294 0.980 ug/L 1 Benzo(k)fluoranthene U ND 0.294 0.980 ug/L 1 Chrysene U ND 0.294 0.980 ug/L 1 Dibenzo(a,h)anthracene U ND 0.294 0.980 ug/L 1 Fluoranthene U ND 0.294 0.980 ug/L 1 Fluorene J 0.618 0.294 0.980 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.294 0.980 ug/L 1 Naphthalene 12.2 0.294 0.980 ug/L 1 Phenanthrene U ND 0.294 0.980 ug/L 1 Pyrene U ND 0.294 0.980 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 0212 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene J 0.700 0.300 1.00 ug/L 1 Toluene 1.54 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW36 Project: SDCGO0213 Sample ID: 354692017 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 28.4 ug/L 49.0 58.0 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 28.4 ug/L 49.0 57.8 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 37.4 ug/L 49.0 76.2 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 54.8 ug/L 50.0 110 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 51.7 ug/L 50.0 103 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 50.6 ug/L 50.0 101 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR79 354692018 GW 13-AUG-14 12:20 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 12.3 0.283 0.943 ug/L 1 JMB3 08/21/14 0723 1412623 1 Acenaphthene U ND 0.283 0.943 ug/L 1 Acenaphthylene U ND 0.283 0.943 ug/L 1 Anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)pyrene U ND 0.283 0.943 ug/L 1 Benzo(b)fluoranthene U ND 0.283 0.943 ug/L 1 Benzo(ghi)perylene U ND 0.283 0.943 ug/L 1 Benzo(k)fluoranthene U ND 0.283 0.943 ug/L 1 Chrysene U ND 0.283 0.943 ug/L 1 Dibenzo(a,h)anthracene U ND 0.283 0.943 ug/L 1 Fluoranthene U ND 0.283 0.943 ug/L 1 Fluorene J 0.377 0.283 0.943 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.283 0.943 ug/L 1 Naphthalene 27.0 0.283 0.943 ug/L 1 Phenanthrene U ND 0.283 0.943 ug/L 1 Pyrene U ND 0.283 0.943 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 0240 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene 3.25 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) J 2.44 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR79 Project: SDCGO0213 Sample ID: 354692018 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 33.4 ug/L 47.2 70.8 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 34.2 ug/L 47.2 72.5 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 44.4 ug/L 47.2 94.1 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 53.8 ug/L 50.0 108 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 51.5 ug/L 50.0 103 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 50.2 ug/L 50.0 100 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41PR101 354692019 GW 13-AUG-14 10:30 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 60.1 0.283 0.943 ug/L 1 JMB3 08/21/14 0753 1412623 1 Acenaphthene U ND 0.283 0.943 ug/L 1 Acenaphthylene U ND 0.283 0.943 ug/L 1 Anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)anthracene U ND 0.283 0.943 ug/L 1 Benzo(a)pyrene U ND 0.283 0.943 ug/L 1 Benzo(b)fluoranthene U ND 0.283 0.943 ug/L 1 Benzo(ghi)perylene U ND 0.283 0.943 ug/L 1 Benzo(k)fluoranthene U ND 0.283 0.943 ug/L 1 Chrysene U ND 0.283 0.943 ug/L 1 Dibenzo(a,h)anthracene U ND 0.283 0.943 ug/L 1 Fluoranthene U ND 0.283 0.943 ug/L 1 Fluorene J 0.434 0.283 0.943 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.283 0.943 ug/L 1 Naphthalene 52.5 0.283 0.943 ug/L 1 Phenanthrene U ND 0.283 0.943 ug/L 1 Pyrene U ND 0.283 0.943 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 1220 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene 1.73 0.300 1.00 ug/L 1 Ethylbenzene 5.32 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) 3.15 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR101 Project: SDCGO0213 Sample ID: 354692019 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 34.3 ug/L 47.2 72.8 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 35.4 ug/L 47.2 75.0 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 39.9 ug/L 47.2 84.6 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 54.9 ug/L 50.0 110 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 48.0 ug/L 50.0 95.9 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 50.1 ug/L 50.0 100 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW25 354692020 GW 13-AUG-14 10:50 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 43.2 0.300 1.00 ug/L 1 JMB3 08/21/14 0824 1412623 1 Acenaphthene J 0.300 0.300 1.00 ug/L 1 Acenaphthylene U ND 0.300 1.00 ug/L 1 Anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)anthracene U ND 0.300 1.00 ug/L 1 Benzo(a)pyrene U ND 0.300 1.00 ug/L 1 Benzo(b)fluoranthene U ND 0.300 1.00 ug/L 1 Benzo(ghi)perylene U ND 0.300 1.00 ug/L 1 Benzo(k)fluoranthene U ND 0.300 1.00 ug/L 1 Chrysene U ND 0.300 1.00 ug/L 1 Dibenzo(a,h)anthracene U ND 0.300 1.00 ug/L 1 Fluoranthene U ND 0.300 1.00 ug/L 1 Fluorene J 0.520 0.300 1.00 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.300 1.00 ug/L 1 Naphthalene 65.7 0.300 1.00 ug/L 1 Phenanthrene U ND 0.300 1.00 ug/L 1 Pyrene U ND 0.300 1.00 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 RXY1 08/27/14 1248 1414609 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene 5.41 0.300 1.00 ug/L 1 Ethylbenzene 8.41 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) 4.61 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis DXF4 08/20/14 0445 1412622 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW25 Project: SDCGO0213 Sample ID: 354692020 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 34.2 ug/L 50.0 68.3 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 39.5 ug/L 50.0 79.0 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 47.9 ug/L 50.0 95.7 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 56.3 ug/L 50.0 113 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 50.1 ug/L 50.0 100 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 52.9 ug/L 50.0 106 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR68 354692021 GW 13-AUG-14 10:50 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 18.0 0.280 0.935 ug/L 1 JMB3 08/21/14 0957 1412727 1 Acenaphthene U ND 0.280 0.935 ug/L 1 Acenaphthylene U ND 0.280 0.935 ug/L 1 Anthracene U ND 0.280 0.935 ug/L 1 Benzo(a)anthracene U ND 0.280 0.935 ug/L 1 Benzo(a)pyrene U ND 0.280 0.935 ug/L 1 Benzo(b)fluoranthene U ND 0.280 0.935 ug/L 1 Benzo(ghi)perylene U ND 0.280 0.935 ug/L 1 Benzo(k)fluoranthene U ND 0.280 0.935 ug/L 1 Chrysene U ND 0.280 0.935 ug/L 1 Dibenzo(a,h)anthracene U ND 0.280 0.935 ug/L 1 Fluoranthene U ND 0.280 0.935 ug/L 1 Fluorene U ND 0.280 0.935 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.280 0.935 ug/L 1 Naphthalene 30.3 0.280 0.935 ug/L 1 Phenanthrene U ND 0.280 0.935 ug/L 1 Pyrene U ND 0.280 0.935 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 GRB2 08/26/14 1826 1414685 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene J 0.690 0.300 1.00 ug/L 1 Ethylbenzene 1.79 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) J 0.570 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis sJwl 08/20/14 1210 1412726 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR68 Project: SDCGO0213 Sample ID: 354692021 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 35.3 ug/L 46.7 75.6 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 35.3 ug/L 46.7 75.5 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 41.6 ug/L 46.7 88.9 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 53.2 ug/L 50.0 106 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 41.8 ug/L 50.0 83.6 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 44.3 ug/L 50.0 88.7 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41 PR77 354692022 GW 13-AUG-14 12:15 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 1.13 0.280 0.935 ug/L 1 JMB3 08/21/14 1028 1412727 1 Acenaphthene J 0.308 0.280 0.935 ug/L 1 Acenaphthylene U ND 0.280 0.935 ug/L 1 Anthracene U ND 0.280 0.935 ug/L 1 Benzo(a)anthracene U ND 0.280 0.935 ug/L 1 Benzo(a)pyrene U ND 0.280 0.935 ug/L 1 Benzo(b)fluoranthene U ND 0.280 0.935 ug/L 1 Benzo(ghi)perylene U ND 0.280 0.935 ug/L 1 Benzo(k)fluoranthene U ND 0.280 0.935 ug/L 1 Chrysene U ND 0.280 0.935 ug/L 1 Dibenzo(a,h)anthracene U ND 0.280 0.935 ug/L 1 Fluoranthene U ND 0.280 0.935 ug/L 1 Fluorene U ND 0.280 0.935 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.280 0.935 ug/L 1 Naphthalene 3.49 0.280 0.935 ug/L 1 Phenanthrene U ND 0.280 0.935 ug/L 1 Pyrene U ND 0.280 0.935 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 GRB2 08/26/14 1855 1414685 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene 1.49 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis sJwl 08/20/14 1210 1412726 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41PR77 Project: SDCGO0213 Sample ID: 354692022 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 35.6 ug/L 46.7 76.1 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 35.4 ug/L 46.7 75.7 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 39.3 ug/L 46.7 84.1 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 52.8 ug/L 50.0 106 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 41.8 ug/L 50.0 83.6 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 44.4 ug/L 50.0 88.8 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: 41GW106 354692023 GW 13-AUG-14 11:20 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene 84.5 0.280 0.935 ug/L 1 JMB3 08/21/14 1059 1412727 1 Acenaphthene U ND 0.280 0.935 ug/L 1 Acenaphthylene U ND 0.280 0.935 ug/L 1 Anthracene U ND 0.280 0.935 ug/L 1 Benzo(a)anthracene U ND 0.280 0.935 ug/L 1 Benzo(a)pyrene U ND 0.280 0.935 ug/L 1 Benzo(b)fluoranthene U ND 0.280 0.935 ug/L 1 Benzo(ghi)perylene U ND 0.280 0.935 ug/L 1 Benzo(k)fluoranthene U ND 0.280 0.935 ug/L 1 Chrysene U ND 0.280 0.935 ug/L 1 Dibenzo(a,h)anthracene U ND 0.280 0.935 ug/L 1 Fluoranthene U ND 0.280 0.935 ug/L 1 Fluorene J 0.477 0.280 0.935 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.280 0.935 ug/L 1 Naphthalene 92.8 0.280 0.935 ug/L 1 Phenanthrene U ND 0.280 0.935 ug/L 1 Pyrene U ND 0.280 0.935 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 GRB2 08/26/14 1925 1414685 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene J 0.660 0.300 1.00 ug/L 1 Ethylbenzene 11.8 0.300 1.00 ug/L 1 Toluene J 0.380 0.300 1.00 ug/L 1 Xylenes (total) 18.4 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis sJwl 08/20/14 1210 1412726 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: 41GW106 Project: SDCGO0213 Sample ID: 354692023 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 28.2 ug/L 46.7 60.4 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 26.9 ug/L 46.7 57.7 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 34.4 ug/L 46.7 73.7 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 51.2 ug/L 50.0 102 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 41.1 ug/L 50.0 82.1 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 43.9 ug/L 50.0 87.8 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Equipment Rinsate 354692024 GW 13-AUG-14 15:00 14-AUG-14 Client Report Date: August 28, 2014 Project: SDCGO0213 Client ID: SDCG001 Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method Semi-Volatile-GC/MS 625 BNA Liquid "As Received" 2-Methylnaphthalene U ND 0.294 0.980 ug/L 1 JMB3 08/21/14 1130 1412727 1 Acenaphthene U ND 0.294 0.980 ug/L 1 Acenaphthylene U ND 0.294 0.980 ug/L 1 Anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)anthracene U ND 0.294 0.980 ug/L 1 Benzo(a)pyrene U ND 0.294 0.980 ug/L 1 Benzo(b)fluoranthene U ND 0.294 0.980 ug/L 1 Benzo(ghi)perylene U ND 0.294 0.980 ug/L 1 Benzo(k)fluoranthene U ND 0.294 0.980 ug/L 1 Chrysene U ND 0.294 0.980 ug/L 1 Dibenzo(a,h)anthracene U ND 0.294 0.980 ug/L 1 Fluoranthene U ND 0.294 0.980 ug/L 1 Fluorene U ND 0.294 0.980 ug/L 1 Indeno(1,2,3-cd)pyrene U ND 0.294 0.980 ug/L 1 Naphthalene U ND 0.294 0.980 ug/L 1 Phenanthrene U ND 0.294 0.980 ug/L 1 Pyrene U ND 0.294 0.980 ug/L 1 Volatile Organics SM 6200 B Volatile Organics "As Received" 1,2-Dichlorobenzene U ND 0.300 1.00 ug/L 1 GRB2 08/27/14 1958 1414685 2 1,3-Dichlorobenzene U ND 0.300 1.00 ug/L 1 1,4-Dichlorobenzene U ND 0.300 1.00 ug/L 1 Benzene U ND 0.300 1.00 ug/L 1 Ethylbenzene U ND 0.300 1.00 ug/L 1 Toluene U ND 0.300 1.00 ug/L 1 Xylenes (total) U ND 0.300 3.00 ug/L 1 The following Prep Methods were performed: Method Description Analyst Date Time Prep Batch EPA 625 BNA Liq. Prep -EPA 625 Analysis sJwl 08/20/14 1210 1412726 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analvsis Report Date: August 28, 2014 Company: SDC Group, Inc. Address : 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina 28533 Contact: Mr. Tom Landis Project: Analytical for Site 1083 Client Sample ID: Equipment Rinsate Project: SDCGO0213 Sample ID: 354692024 Client ID: SDCG001 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 625 2 SM 6200 B Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits 2-Fluorobiphenyl 625 BNA Liquid "As Received" 38.0 ug/L 49.0 77.5 (32%-102%) Nitrobenzene-d5 625 BNA Liquid "As Received" 35.7 ug/L 49.0 72.9 (36%-125%) p-Terphenyl-d14 625 BNA Liquid "As Received" 48.2 ug/L 49.0 98.4 (34%-135%) 1,2-Dichloroethane-d4 SM 6200 B Volatile Organics "As Received" 50.5 ug/L 50.0 101 (78%-124%) Bromofluorobenzene SM 6200 B Volatile Organics "As Received" 49.0 ug/L 50.0 98.0 (80%-120%) Toluene-d8 SM 6200 B Volatile Organics "As Received" 50.8 ug/L 50.0 102 (80%-120%) Notes: GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary SDC Group, Inc. 1 Cherry Point MCAS Bldg 4376T Cherry Point, North Carolina Contact: Mr. Tom Landis Workorder: 354692 Report Date: August 28, 2014 Page 1 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi-Volatile-GC/MS Batch 1412623 QC1203150863 LCS 2-Methylnaphthalene 50.0 36.1 ug/L 72.2 (33%-102%) JMB3 08/20/1417:27 Acenaphthene 50.0 41.3 ug/L 82.6 (40%-104%) Acenaphthylene 50.0 42.3 ug/L 84.6 (37%-107%) Anthracene 50.0 42.1 ug/L 84.1 (46%-110%) Benzo(a)anthracene 50.0 41.8 ug/L 83.5 (49%-111%) Benzo(a)pyrene 50.0 41.3 ug/L 82.6 (47%-110%) Benzo(b)fluoranthene 50.0 41.2 ug/L 82.4 (47%-117%) Benzo(ghi)perylene 50.0 51.1 ug/L 102 (33%-126%) Benzo(k)fluoranthene 50.0 42.0 ug/L 83.9 (46%-119%) Chrysene 50.0 41.3 ug/L 82.5 (44%-117%) Dibenzo(a,h)anthracene 50.0 47.1 ug/L 94.1 (36%-125%) Fluoranthene 50.0 38.8 ug/L 77.5 (45%-118%) Fluorene 50.0 42.9 ug/L 85.7 (43%-110%) Indeno(1,2,3-cd)pyrene 50.0 47.1 ug/L 94.3 (37%-125%) Naphthalene 50.0 37.1 ug/L 74.2 (31%-98%) Phenanthrene 50.0 41.7 ug/L 83.4 (47%-111%) Pyrene 50.0 57.5 ug/L 115 (38%-127%) **2-Fluorobiphenyl 50.0 40.7 ug/L 81.5 (32%-102%) **Nitrobenzene-6 50.0 40.3 ug/L 80.5 (36%-125%) **p-Terphenyl-dl4 50.0 45.6 ug/L 91.2 (34%-135%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 2 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi -Volatile -GUMS Batch 1412623 QC1203150862 MB 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene * *2-Fluorobiphenyl 50.0 * *Nitrobenzene-d5 50.0 **p-Terphenyl-dl4 50.0 QC1203150864 354692001 MS 2-Methylnaphthalene 100 U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L 43.2 ug/L 43.6 ug/L 58.8 ug/L 16.9 84.7 ug/L 86.5 (32%-102%) 87.2 (36%-125%) 118 (34%-135%) 67.7 (26%-103%) JM133 08/20/1416:56 08/20/14 22:06 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 3 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi -Volatile -GUMS Batch 1412623 Acenaphthene 100 J 0.420 80.5 ug/L 80 (31%-103%) JMB3 08/20/14 22:06 Acenaphthylene 100 U ND 82.0 ug/L 82 (33%-104%) Anthracene 100 U ND 83.0 ug/L 83 (33%-108%) Benzo(a)anthracene 100 U ND 84.0 ug/L 84 (35%-112%) Benzo(a)pyrene 100 U ND 85.9 ug/L 85.9 (34%-110%) Benzo(b)fluoranthene 100 U ND 86.7 ug/L 86.7 (34%-116%) Benzo(ghi)perylene 100 U ND 83.0 ug/L 83 (22%-122%) Benzo(k)fluoranthene 100 U ND 88.9 ug/L 88.9 (34%-119%) Chrysene 100 U ND 82.1 ug/L 82.1 (32%-116%) Dibenzo(a,h)anthracene 100 U ND 88.1 ug/L 88.1 (24%-123%) Fluoranthene 100 U ND 85.0 ug/L 85 (31%-118%) Fluorene 100 J 0.590 86.3 ug/L 85.7 (32%-111%) Indeno(1,2,3-cd)pyrene 100 U ND 82.9 ug/L 82.9 (25%-122%) Naphthalene 100 1.19 71.6 ug/L 70.4 (25%-100%) Phenanthrene 100 U ND 81.4 ug/L 81.4 (34%-112%) Pyrene 100 U ND 84.7 ug/L 84.7 (27%-126%) **2-Fluorobiphenyl 100 38.1 77.7 ug/L 77.7 (32%-102%) **Nitrobenzene-d5 100 39.3 75.4 ug/L 75.4 (36%-125%) **p-Terphenyl-dl4 100 29.9 82.4 ug/L 82.4 (34%-135%) QC1203150865 354692001 MSD 2-Methylnaphthalene 100 16.9 84.4 ug/L 0.355 67.4 (0%-30%) 08/20/14 22:37 Acenaphthene 100 1 0.420 76.8 ug/L 4.65 76.4 (0%-30%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 4 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi -Volatile -GUMS Batch 1412623 Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene **2-Fluorobiphenyl * *Nitrobenzene-d5 **p-Terphenyl-dl4 Batch 1412727 QC1203151211 LCS 2-Methylnaphthalene Acenaphthene 100 U ND 78.7 ug/L 4.03 78.7 (0%-30%) JMB3 08/20/14 22:37 100 U ND 78.0 ug/L 6.23 78 (0%-30%) 100 U ND 78.7 ug/L 6.47 78.7 (0%-30%) 100 U ND 79.5 ug/L 7.76 79.5 (0%-30%) 100 U ND 80.4 ug/L 7.57 80.4 (0%-30%) 100 U ND 71.4 ug/L 15.0 71.4 (0%-30%) 100 U ND 81.3 ug/L 9.02 81.3 (0%-30%) 100 U ND 76.9 ug/L 6.56 76.9 (0%-30%) 100 U ND 77.3 ug/L 13.2 77.3 (0%-30%) 100 U ND 80.8 ug/L 4.99 80.8 (0%-30%) 100 J 0.590 81.4 ug/L 5.80 80.8 (0%-30%) 100 U ND 72.6 ug/L 13.3 72.6 (0%-30%) 100 1.19 70.6 ug/L 1.38 69.4 (0%-30%) 100 U ND 76.6 ug/L 6.00 76.6 (0%-30%) 100 U ND 74.6 ug/L 12.7 74.6 (0%-30%) 100 38.1 75.5 ug/L 75.5 (32%-102%) 100 39.3 76.6 ug/L 76.6 (36%-125%) 100 29.9 72.4 ug/L 72.4 (34%-135%) 50.0 31.5 ug/L 50.0 37.1 ug/L 63 (33%-102%) JMB3 08/21/14 09:26 74.1 (40%-104%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 5 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi -Volatile -GUMS Batch 1412727 Acenaphthylene 50.0 38.9 ug/L 77.9 (37%-107%) Anthracene 50.0 39.1 ug/L 78.2 (46%-110%) JMB3 08/21/14 09:26 Benzo(a)anthracene 50.0 38.8 ug/L 77.6 (49%-111%) Benzo(a)pyrene 50.0 40.2 ug/L 80.5 (47%-110%) Benzo(b)fluoranthene 50.0 40.6 ug/L 81.2 (47%-117%) Benzo(ghi)perylene 50.0 39.4 ug/L 78.9 (33%-126%) Benzo(k)fluoranthene 50.0 41.5 ug/L 83 (46%-119%) Chrysene 50.0 38.2 ug/L 76.3 (44%-117%) Dibenzo(a,h)anthracene 50.0 41.7 ug/L 83.5 (36%-125%) Fluoranthene 50.0 37.5 ug/L 75 (45%-118%) Fluorene 50.0 40.9 ug/L 81.9 (43%-110%) Indeno(1,2,3-cd)pyrene 50.0 38.8 ug/L 77.5 (37%-125%) Naphthalene 50.0 31.1 ug/L 62.2 (31%-98%) Phenanthrene 50.0 38.0 ug/L 76.1 (47%-111%) Pyrene 50.0 46.9 ug/L 93.9 (38%-127%) **2-Fluorobiphenyl 50.0 40.5 ug/L 81 (32%-102%) **Nitrobenzene-d5 50.0 40.2 ug/L 80.3 (36%-125%) **p-Terphenyl-dl4 50.0 51.0 ug/L 102 (34%-135%) QC1203151210 MB 2-Methylnaphthalene U ND ug/L 08/21/14 08:55 Acenaphthene U ND ug/L Acenaphthylene U ND ug/L Anthracene U ND ug/L GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 6 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi -Volatile -GUMS Batch 1412727 Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(ghi)perylene Benzo(k)fluoranthene Chrysene Dibenzo(a,h)anthracene Fluoranthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene * *2-Fluorobiphenyl 50.0 * *Nitrobenzene-d5 50.0 **p-Terphenyl-dl4 50.0 QC1203151212 355006001 MS 2-Methylnaphthalene 100 U ND Acenaphthene 100 U ND Acenaphthylene 100 U ND Anthracene 100 U ND Benzo(a)anthracene 100 U ND U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L 33.2 ug/L 66.4 (32%-102%) 32.6 ug/L 65.1 (36%-125%) 45.7 ug/L 91.4 (34%-135%) 69.6 ug/L 69.6 (26%-103%) 78.0 ug/L 78 (31%-103%) 79.9 ug/L 79.9 (33%-104%) 80.9 ug/L 80.9 (33%-108%) 81.6 ug/L 81.6 (35%-112%) JMB3 08/21/14 08:55 08/21/14 12:33 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 7 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi -Volatile -GUMS Batch 1412727 Benzo(a)pyrene 100 U ND 83.8 ug/L 83.8 (34%-110%) JMB3 08/21/1412:33 Benzo(b)fluoranthene 100 U ND 87.1 ug/L 87.1 (34%-116%) Benzo(ghi)perylene 100 U ND 76.7 ug/L 76.7 (22%-122%) Benzo(k)fluoranthene 100 U ND 89.4 ug/L 89.4 (34%-119%) Chrysene 100 U ND 79.9 ug/L 79.9 (32%-116%) Dibenzo(a,h)anthracene 100 U ND 80.0 ug/L 80 (24%-123%) Fluoranthene 100 U ND 74.7 ug/L 74.7 (31%-118%) Fluorene 100 U ND 83.5 ug/L 83.5 (32%-111%) Indeno(1,2,3-cd)pyrene 100 U ND 74.0 ug/L 74 (25%-122%) Naphthalene 100 U ND 70.9 ug/L 70.9 (25%-100%) Phenanthrene 100 U ND 79.3 ug/L 79.3 (34%-112%) Pyrene 100 U ND 106 ug/L 106 (27%-126%) **2-Fluorobiphenyl 100 31.5 82.2 ug/L 82.2 (32%-102%) **Nitrobenzene-d5 100 30.1 82.3 ug/L 82.3 (36%-125%) **p-Terphenyl-dl4 100 47.7 110 ug/L 110 (34%-135%) QC1203151213 355006001 MSD 2-Methylnaphthalene 100 U ND 61.9 ug/L 11.6 61.9 (0%-30%) 08/21/1413:04 Acenaphthene 100 U ND 75.6 ug/L 3.10 75.6 (0%-30%) Acenaphthylene 100 U ND 77.8 ug/L 2.69 77.8 (0%-30%) Anthracene 100 U ND 81.2 ug/L 0.469 81.2 (0%-30%) Benzo(a)anthracene 100 U ND 82.2 ug/L 0.635 82.2 (0%-30%) Benzo(a)pyrene 100 U ND 84.0 ug/L 0.191 84 (0%-30%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 8 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Semi -Volatile -GUMS Batch 1412727 Benzo(b)fluoranthene 100 U ND 86.0 ug/L 1.29 86 (0%-30%) JMB3 08/21/1413:04 Benzo(ghi)perylene 100 U ND 79.5 ug/L 3.56 79.5 (0%-30%) Benzo(k)fluoranthene 100 U ND 85.9 ug/L 3.99 85.9 (0%-30%) Chrysene 100 U ND 80.4 ug/L 0.624 80.4 (0%-30%) Dibenzo(a,h)anthracene 100 U ND 83.5 ug/L 4.33 83.5 (0%-30%) Fluoranthene 100 U ND 80.6 ug/L 7.50 80.6 (0%-30%) Fluorene 100 U ND 82.1 ug/L 1.62 82.1 (0%-30%) Indeno(1,2,3-cd)pyrene 100 U ND 78.1 ug/L 5.31 78.1 (0%-30%) Naphthalene 100 U ND 58.7 ug/L 18.9 58.7 (0%-30%) Phenanthrene 100 U ND 79.4 ug/L 0.101 79.4 (0%-30%) Pyrene 100 U ND 87.5 ug/L 18.7 87.5 (0%-30%) **2-Fluorobiphenyl 100 31.5 79.2 ug/L 79.2 (32%-102%) **Nitrobenzene-d5 100 30.1 78.3 ug/L 78.3 (36%-125%) **p-Terphenyl-dl4 100 47.7 92.5 ug/L 92.5 (34%-135%) Volatile-GGMS Batch 1414609 QC1203155995 LCS 1,2-Dichlorobenzene 50.0 47.7 ug/L 95.4 (70%-130%) RXY1 08/26/14 08:24 1,3-Dichlorobenzene 50.0 48.7 ug/L 97.3 (70%-130%) 1,4-Dichlorobenzene 50.0 46.5 ug/L 93.1 (70%-130%) Benzene 50.0 45.9 ug/L 91.8 (70%-130%) Ethylbenzene 50.0 47.8 ug/L 95.5 (70%-130%) Toluene 50.0 46.8 ug/L 93.7 (70%-130%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 9 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Volatile -GUMS Batch 1414609 Xylenes (total) 150 150 ug/L 100 (70%-130%) RXY1 08/26/14 08:24 **1,2-Dichloroethane-d4 50.0 47.6 ug/L 95.2 (78%-124%) **Bromofluorobenzene 50.0 45.9 ug/L 91.8 (80%-120%) **Toluene-d8 50.0 49.0 ug/L 97.9 (80%-120%) QC1203156427 LCS 1,2-Dichlorobenzene 50.0 48.5 ug/L 96.9 (70%-130%) 08/26/14 20:05 1,3-Dichlorobenzene 50.0 48.8 ug/L 97.6 (70%-130%) 1,4-Dichlorobenzene 50.0 46.1 ug/L 92.2 (70%-130%) Benzene 50.0 47.6 ug/L 95.2 (70%-130%) Ethylbenzene 50.0 48.5 ug/L 97 (70%-130%) Toluene 50.0 47.9 ug/L 95.8 (70%-130%) Xylenes (total) 150 153 ug/L 102 (70%-130%) **1,2-Dichloroethane-d4 50.0 52.6 ug/L 105 (78%-124%) **Bromofluorobenzene 50.0 47.6 ug/L 95.2 (80%-120%) **Toluene-d8 50.0 48.0 ug/L 96 (80%-120%) QC1203156428 LCS 1,2-Dichlorobenzene 50.0 45.6 ug/L 91.2 (70%-130%) 08/27/14 08:35 1,3-Dichlorobenzene 50.0 46.3 ug/L 92.6 (70%-130%) 1,4-Dichlorobenzene 50.0 44.6 ug/L 89.2 (70%-130%) Benzene 50.0 44.6 ug/L 89.1 (70%-130%) Ethylbenzene 50.0 45.0 ug/L 89.9 (70%-130%) Toluene 50.0 44.7 ug/L 89.4 (70%-130%) Xylenes (total) 150 144 ug/L 95.9 (70%-130%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 10 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Volatile -GUMS Batch 1414609 **1,2-Dichloroethane-d4 50.0 * *Bromofluorobenzene 50.0 * *Toluene-d8 50.0 QC1203155992 MB 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzene Ethylbenzene Toluene Xylenes (total) ** 1,2-Dichloroethane-d4 50.0 * *Bromofluorobenzene 50.0 * *Toluene-d8 50.0 QC1203156425 MB 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzene Ethylbenzene Toluene Xylenes (total) **1,2-Dichloroethane-d4 50.0 51.7 ug/L 103 (78%-124%) RXY1 08/27/14 08:35 45.9 ug/L 91.7 (80%-120%) 48.1 ug/L 96.3 (80%-120%) U ND ug/L 08/26/1410:47 U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L 48.4 ug/L 96.8 (78%-124%) 49.6 ug/L 99.1 (80%-120%) 51.7 ug/L 103 (80%-120%) U ND ug/L 08/26/14 21:31 U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L 53.7 ug/L 107 (78%-124%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 11 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Volatile -GUMS Batch 1414609 **Bromofluorobenzene 50.0 49.4 ug/L 98.8 (80%-120%) RXY1 08/26/14 21:31 **Toluene-d8 50.0 49.8 ug/L 99.6 (80%-120%) QC1203156426 MB 1,2-Dichlorobenzene U ND ug/L 08/27/14 09:59 1,3-Dichlorobenzene U ND ug/L 1,4-Dichlorobenzene U ND ug/L Benzene U ND ug/L Ethylbenzene U ND ug/L Toluene U ND ug/L Xylenes (total) U ND ug/L **1,2-Dichloroethane-d4 50.0 53.9 ug/L 108 (78%-124%) **Bromofluorobenzene 50.0 47.9 ug/L 95.9 (80%-120%) **Toluene-d8 50.0 50.1 ug/L 100 (80%-120%) QC1203155993 354692005 PS 1,2-Dichlorobenzene 50.0 U ND 45.1 ug/L 90.2 (72%-120%) 08/27/14 13:16 1,3-Dichlorobenzene 50.0 U ND 45.9 ug/L 91.8 (70%-120%) 1,4-Dichlorobenzene 50.0 U ND 43.6 ug/L 87.3 (70%-120%) Benzene 50.0 U ND 44.6 ug/L 89.1 (75%-120%) Ethylbenzene 50.0 U ND 45.1 ug/L 90.3 (72%-120%) Toluene 50.0 U ND 45.2 ug/L 90.5 (72%-120%) Xylenes (total) 150 U ND 143 ug/L 95.6 (73%-120%) **1,2-Dichloroethane-d4 50.0 55.5 53.6 ug/L 107 (78%-124%) **Bromofluorobenzene 50.0 49.7 47.2 ug/L 94.4 (80%-120%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 12 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Volatile -GUMS Batch 1414609 **Toluene-d8 QC1203155994 354692005 PSD 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzene Ethylbenzene Toluene Xylenes (total) **1,2-Dichloroethane-d4 * *Bromofluorobenzene **Toluene-d8 Batch 1414685 - QC1203156176 LCS 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzene Ethylbenzene Toluene Xylenes (total) **1,2-Dichloroethane-d4 * *Bromofluorobenzene 50.0 51.9 49.4 ug/L 98.7 (80%-120%) RXY1 08/27/1413:16 50.0 U ND 44.6 ug/L 1.14 89.2 (0%-20%) 08/27/1413:44 50.0 U ND 44.7 ug/L 2.72 89.3 (0%-20%) 50.0 U ND 43.2 ug/L 1.06 86.3 (0%-20%) 50.0 U ND 42.9 ug/L 3.73 85.9 (0%-20%) 50.0 U ND 43.8 ug/L 3.04 87.6 (0%-20%) 50.0 U ND 44.3 ug/L 2.08 88.6 (0%-20%) 150 U ND 141 ug/L 1.85 93.8 (0%-20%) 50.0 55.5 54.1 ug/L 108 (78%-124%) 50.0 49.7 46.4 ug/L 92.8 (80%-120%) 50.0 51.9 50.1 ug/L 100 (80%-120%) 50.0 44.5 ug/L 89 (70%-130%) GRB2 08/26/1414:05 50.0 45.7 ug/L 91.3 (70%-130%) 50.0 44.0 ug/L 87.9 (70%-130%) 50.0 43.6 ug/L 87.1 (70%-130%) 50.0 45.9 ug/L 91.8 (70%-130%) 50.0 42.7 ug/L 85.4 (70%-130%) 150 141 ug/L 93.9 (70%-130%) 50.0 51.4 ug/L 103 (78%-124%) 50.0 41.2 ug/L 82.4 (80%-120%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 13 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Volatile -GUMS Batch 1414685 * *Toluene-d8 50.0 QC1203157685 LCS 1,2-Dichlorobenzene 50.0 1,3-Dichlorobenzene 50.0 1,4-Dichlorobenzene 50.0 Benzene 50.0 Ethylbenzene 50.0 Toluene 50.0 Xylenes (total) 150 ** 1,2-Dichloroethane-d4 50.0 * *Bromofluorobenzene 50.0 * *Toluene-d8 50.0 QC1203156173 MB 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Benzene Ethylbenzene Toluene Xylenes (total) ** 1,2-Dichloroethane-d4 50.0 * *Bromofluorobenzene 50.0 * *Toluene-d8 50.0 44.0 ug/L 88 (80%-120%) GRB2 08/26/1414:05 48.2 ug/L 96.3 (70%-130%) 08/27/1413:39 49.0 ug/L 98 (70%-130%) 47.5 ug/L 95 (70%-130%) 45.9 ug/L 91.8 (70%-130%) 49.0 ug/L 98.1 (70%-130%) 45.7 ug/L 91.4 (70%-130%) 151 ug/L 100 (70%-130%) 53.1 ug/L 106 (78%-124%) 45.9 ug/L 91.8 (80%-120%) 47.9 ug/L 95.9 (80%-120%) U ND ug/L 08/26/1417:28 U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L U ND ug/L 53.3 ug/L 107 (78%-124%) 41.8 ug/L 83.7 (80%-120%) 44.8 ug/L 89.7 (80%-120%) GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 14 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Volatile -GUMS Batch 1414685 QC1203157684 MB 1,2-Dichlorobenzene U ND ug/L 1,3-Dichlorobenzene U ND ug/L 1,4-Dichlorobenzene U ND ug/L Benzene U ND ug/L Ethylbenzene U ND ug/L Toluene U ND ug/L Xylenes (total) U ND ug/L **1,2-Dichloroethane-d4 50.0 50.7 ug/L 101 (78%-124%) **Bromofluorobenzene 50.0 44.6 ug/L 89.3 (80%-120%) **Toluene-d8 50.0 45.6 ug/L 91.2 (80%-120%) QC1203156174 354692021 PS 1,2-Dichlorobenzene 50.0 U ND 47.8 ug/L 95.7 (72%-120%) 1,3-Dichlorobenzene 50.0 U ND 51.0 ug/L 102 (70%-120%) 1,4-Dichlorobenzene 50.0 U ND 48.6 ug/L 97.3 (70%-120%) Benzene 50.0 J 0.690 52.8 ug/L 104 (75%-120%) Ethylbenzene 50.0 1.79 52.1 ug/L 101 (72%-120%) Toluene 50.0 U ND 51.6 ug/L 103 (72%-120%) Xylenes (total) 150 J 0.570 174 ug/L 115 (73%-120%) **1,2-Dichloroethane-d4 50.0 53.2 51.4 ug/L 103 (78%-124%) **Bromofluorobenzene 50.0 41.8 50.2 ug/L 100 (80%-120%) **Toluene-d8 50.0 44.3 53.0 ug/L 106 (80%-120%) QC1203156175 354692021 PSD GRB2 08/27/1417:32 08/27/14 22:24 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 15 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Volatile -GUMS Batch 1414685 1,2-Dichlorobenzene 50.0 U ND 48.8 ug/L 2.05 97.6 (0%-20%) 08/27/14 22:52 1,3-Dichlorobenzene 50.0 U ND 48.8 ug/L 4.41 97.6 (0%-20%) GRB2 1,4-Dichlorobenzene 50.0 U ND 47.7 ug/L 1.99 95.3 (0%-20%) Benzene 50.0 J 0.690 48.6 ug/L 8.28 95.8 (0%-20%) Ethylbenzene 50.0 1.79 50.1 ug/L 3.93 96.6 (0%-20%) Toluene 50.0 U ND 46.7 ug/L 10.1 93.3 (0%-20%) Xylenes (total) 150 1 0.570 151 ug/L 13.9 100 (0%-20%) **1,2-Dichloroethane-d4 50.0 53.2 47.8 ug/L 95.7 (78%-124%) **Bromofluorobenzene 50.0 41.8 47.5 ug/L 94.9 (80%-120%) **Toluene-d8 50.0 44.3 49.5 ug/L 99 (80%-120%) Notes: The Qualifiers in this report are defined as follows: ** Analyte is a surrogate compound < Result is less than value reported > Result is greater than value reported A The TIC is a suspected aldol-condensation product B The target analyte was detected in the associated blank. C Analyte has been confirmed by GUMS analysis D Results are reported from a diluted aliquot of the sample E Concentration of the target analyte exceeds the instrument calibration range H Analytical holding time was exceeded 1 Value is estimated JNX Non Calibrated Compound N Organics --Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest internal standard response factor N Presumptive evidence based on mass spectral library search to make a tentative identification of the analyte (TIC). Quantitation is based on nearest internal standard response factor N/A RPD or %Recovery limits do not apply. N1 See case narrative GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 354692 Page 16 of 16 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier P Organics --The concentrations between the primary and confirmation columns/detectors is >40% different. For HPLC, the difference is >70%. Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER. R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD. UJ Compound cannot be extracted X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound ^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more or %RPD not applicable. The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. APPENDIX B WELL ABANDONMENT RECORDS, WELL LOGS AND WELL CONSTRUCTION RECORDS DOD; 210022.08_1083_lnterim Report Dec2013-Feb2015_FlNAL CATLIN Engineers and Scientists CATLIN Project No. 210022.08 June 2015 WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: D.T. Chalmers, Jr. Well Contractor Name (or well owner personally abandoning well on his/her property) 4146A NC Well Contractor Certification Number CATLIN Engineers and Scientists Company Name 2. Well Construction Permit #: N/A List all applicable ice/l permits (i a Counir, State, Variance, byection, etc) if knairn 3. Well use (check well use): ❑ Agricultural ❑ MunicipaliPublic El Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑Industrial/Commercial ❑ Residential Water Supply (shared) ❑ Irrigation Non -Water Supply Well: ❑ Monitoring ❑ Recovery ❑ Aquifer Recharge ❑Aquifer Storage and Recovery ❑Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Gcothcnml (Heating/Cooling Return) ❑ Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑ Subsidence Control ❑ Tracer ❑ Other (explain under 7g) 4. Date well(s) abandoned: 12/9/2014 Sa. Well Location: For Internal Use ONLY: WELL ABANDONMENT DETAILS 7a. Number of wells being abandoned: 1 For nadliple uitecnon or nail-u•iaer supph [fells ONLY with the same cansinic tion ahandonnient you can.suhnnl one form 7b. Approximate volume of water remaining in well(s): N1A (gal•) FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: N/A 7d. Amount of disinfectant used: N/A 7e. Sealing materials used (check all that apply): ID Neat Cement Grout ❑Bentonite Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑Concrete Grout ❑Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑Bentonite Slurry ❑Other (explain under 7g) 7f. For each material selected above, provide amount of materials used: 7g. Provide a brief description of the abandonment procedure: Well overdrilled and completely removed then replaced with well 41 GW02R in same borehole. Building 1083 N/A Facility+'Owner Name Facility ID# (if applicable) 8• Certift ation: Building 1083, Havelock 28533 r— Physical Address, City, and Zip r Craven Unknown SYzallreofCert ted Well ontractoror Well Owner Date County Parcel Identification No. (PIN) Br signing this farm 1 hereby certify that the ivell(s) was (were) abandoned ill Sb. Latitude and longitude in degrees/minutes/seconds or decimal degrees accordance with 15A NCAC 02C.0100 a)- 2C Well Construction Standards and that a copy of this record has been provided to the well owner. (if well field, one lat/long is sufficient) 34.9418965 N -76.8632280 w CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well construction record(s) if available. For multiple iiyection or non -[rater supply well ONLY with the same coitstniction abandotnient, fait can .submit one fnnn 6a. Well ID#: 41GW02 6b. Total well depth: 20 (ft.) 6c. Borehole diameter: 2 (in.) 6d. Water level below ground surface: 10.5 (ft.) 6e. Outer casing length (if known): Not Applicable 6E Inner casing/tubing length (if known): 5 (ft.) 6g. Screen length (if known): 14.6 (ft) 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. MUNITZEUMMITWINIP 10a. For All Wells: Subnut this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Injection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c. For Water Supply & Injection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. Adapted from NCDFNR-DWR Form GW-30 North Carolina Department of Fm. ironment and Natural Resources - Dn ision of Water Resources Res iced August 2013 WELL CONSTRUCTION RECORD This form can be used for single or multiple wells 1. Well Contractor Information: D.T. Chalmers, Jr. Well Contractor Name 4146A 41 GW02R NC Well Contractor Certification Number Well Identification CATLIN Engineers and Scientists Company Name 2. Well Construction Permit #: N/A List all applicahle it ell permits (i a Counna State. Vanaine h jectnn, etc 1 fknoua 3. Well use (check well use): Water Supply Well: ❑ Agricultural ❑ Municipal.tPublic ❑Geothermal (Heating/Cooling Supply) El Residential Water Supply (single) ❑ Industrial/Commercial ❑ Residential Water Supply (shared) ❑ Irrigation ■ Monitoring ❑ Recovery Injection Well: ❑ Aquifer Recharge ■ Groundwater Remediation ❑ Aquifer Storage and Recovery ❑ Salinity Barrier ❑ Aquifer Test ❑ Stormvater Drainage ❑ Experimental Technology ❑ Subsidence Control ❑Geothermal (Closed Loop) ❑Tracer ❑Geothcnml (Heating/Cooling Return) ❑Other (explain under #21 Remarks) 4. Date Well(s) Completed: 12/10/2014 5a. Well Location: Building 1083 N/A FacilityiOwner Name Facility III# (if applicable) Building 1083, Havelock 28533 Physical Address, City, and Zip Craven County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 34.9418965 N -76.8632280 NY 6. Is (are) the well(s): ■Permanent or ❑Temporary 7. Is this a repair to an existing well: Yes or ■ No If this is a repair fill out known icell construction irfoiination and explain the nature ofthe repair under #21 remarks section or on the back of this form 8. Number of wells constructed: 1 For multiple intecaun or nun-autct supply it ells ONLY niih the saute construction. you can submit one form 9. Total well depth below land surface: 25 (ft.) For multiple irells list all depths ifdierent (example - 3 a,200' and 2 1) Inn) 10. Static water level below top of casing: 10.5 (ft. ) 1f ivater level is above use "+" 11. Borehole diameter: 12.25 (in.) 12. Well construction method: H.S. Augers (i a auger. rutaq, cable duaccipush. etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm):_ Method of test: 13b. Disinfection e: Amount: For Internal Use ONLY 22. C fication: Signature of Certified Well Contractor Date Br signing this form 1 hereby cerliJv that the well(s) was (were) constructed in accordance with 15.4 NCAC 02C.0100 or 2C Well Consiniction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Infection Wells: In addition to sending the form to the address in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 24c. For Water Supply & Infection Wells: Also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Adapted from NCDFNR-DWR Form GW-I North Carolina Department of Frtx ironment and Natural Resources - Dn ision of Water Resources Revised August 2013 WELL LOG CATLIN Engineers and Scientists 210022 Wilmngan, NC SHEET 1 OF 1 PROJECT NO.: 210022 STATE: NC COUNTY: Craven LOCATION: Havelock PROJECT NAME: Building 1083 LOGGED BY: Shane Chasteen WELL ID: DRILLER: D.T. Chalmers, Jr. 41 GW02R NORTHING: 440674.5600 EASTING:2640296.2400 CREW: CATLIN SYSTEM: NCSP NAD 83 ft BORING LOCATION: Replace well 41GW02 T.O.C. ELEV.: 14.87 DRILL MACHINE: CME 550 ATV METHOD: H.S. Augers 1 0 HOUR DTW: N/A TOTAL DEPTH: 25.0 START DATE: 12/09/14 FINISH DATE: 12/10/14 24 HOUR DTW: 10.5 WELL DEPTH: 25.0 BLOW COUNT OVA LAB. o L SOIL AND ROCK WELL DEPTH 0.5ft 0.5(t 0.5ft 0.5ft (PPm) ID. s c DEPTH DESCRIPTION ELEVATION DETAIL 0.0 LAND SURFACE 14.9 0.0 0.0 _ 3.0 3.0 11.9 4.7 M (SC) - Tan, Clayey SAND. HCO. a 4.0 5.0 9.9 rn e 8.0 8.0 6.9 8.0 11.1 M/W (CL) - Tan, CLAY. Soft w/med. plast. HCO. 10.0 4.9 10.0 13.0 13.0 1.9 24.4 Sat. (CUCH) - Gray, CLAY. Soft w/med. to high plast. Strong HCO. 15.0 _ _.� -0.1 o� oa oQ 18.0 18.0 8.1 Nt Q U N 29.0 Sat. px (CL) - Dark gray, CLAY. Soft. Strong HCO. 20.0 5.1 23.0 23.0 _ . _ •B.1 26.5 Sat. (CL) - S.A.A. 24.e 25.0 25.0 -10,1 25.0 25.0 Boring Terminated at Elevation -10.1 ft EPortland Cement MSentonite Pellets u #2 Medium Sand WELL ABANDONMENT RECORD This form can be used for single or multiple wells 1. Well Contractor Information: For Internal Use ONLY WELL ABANDONMENT DETAILS D.T. Chalmers, Jr. 7a. Number of wells being abandoned: 1 _ Well Contractor Name (or well owner personally abandoning well on his/her property) Fa multiple mtectian ar non•u'arersupph wells ONLY with the .same constinetia✓ahandmmhent, you can submit one form 4146A NC Well Contractor Certification Number CATLIN Engineers and Scientists Company Name 2. Well Construction Permit #: N/A List all applcable well pernnts (t a Count,. Stare, Variance. Injection, etc) i/known 3. Well use (check well use): Water Supply Well: ❑ Agricultural ❑ Municipal/Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑Industrial/Commercial ❑Residential Water Supply (shared) ❑ Irrigation Non -Water Supply Well: ❑ Monitoring ❑ Recovery Injection Well: ❑ Aquifer Recharge ❑ Groundwater Remediation ❑Aquifer Storage and Recovery ❑Salinity Barrier ❑Aquifer Test ❑Stormwater Drainage ❑Experimental Technology ❑Subsidence Control El Geothermal (Closed Loop) ❑Tracer ❑Geothennal (Heating/Cooling Return) ❑Other (explain under 7g) 4. Date well(s) abandoned: 12/10/2014 5a. Well Location: Building 1083 N/A Facility%Owner Name Facility 1D# (if applicable) Building 1083, Havelock 28533 Physical Address, City, and Zip Craven Unknown 7b. Approximate volume of water remaining in well(s): NIA (gal.] FOR WATER SUPPLY WELLS ONLY: 7c. Type of disinfectant used: N/A 7d. Amount of disinfectant used: N/A 7e. Sealing materials used (check all that apply): ❑Neat Cement Grout ❑Bentonnte Chips or Pellets ❑ Sand Cement Grout ❑ Dry Clay ❑Concrete Grout ❑Drill Cuttings ❑ Specialty Grout ❑ Gravel ❑ Bcntonite Slurry ❑ Other (explain under 7g) 7E For each material selected above, provide amount of materials used: 7g. Provide a brief description of the abandonment procedure: Well overdrilled and completely removed then replaced with well 41 GW03R in same borehole. 8. Cert' is ion: .1b_7z>1y Signature of Certified Well Contractor or Well Owner Date County Parccl Identification No. (PIN) Br signing this form I hereby certi%v that the ivell(s) was (were) abandoned in Sb. Latitude and longitude in degrees/minutes/seconds or decimal degrees accordance with 15A NCAC 02C.0100 at- 2C Well Construction Standards and that a copy ofthis record has been provided to the well owner. (if well field. one lat/long is sufficient) 34.9419216 N-76.8631403 W CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED Attach well corutrtiction recoi•d(s) if available. For multiple injection or non -pater .supply well ONLY with the sante cortsMicnon abandonnient, You can submit one form 6a. Well I D#: 41 GW03 6b. Total well depth: 20 (ft.) 6c. Borehole diameter: 2 (in.) 6d. Water level below ground surface: 13.26 (ft.) 6e. Outer casing length (if known): Not Applicable 611 Inner casing/tubing length (if known): 3 (ft.) 6g. Screen length (if known): 16.6 (ft) 9. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well abandonment details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 10a. For All Wells: Subnut this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 10b. For Injection Wells: In addition to sending the form to the address in 10a above, also submit one copy of this form within 30 days of completion of well abandonment to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636 10c, For Water Sullply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of completion of well abandonment to the county health department of the county where abandoned. Adapted from NCDFNR-DWR Fonn G W-30 North Carolina Department of Fm ironment and Natural Resources - Dn hston of Water Resources Res ised August 2013 WELL CONSTRUCTION RECORD This form can be used for single or multiple wells 1. Well Contractor Information: D.T. Chalmers, Jr. Well Contractor Name 4146A 41 GW03R NC Well Contractor Certification Number Well Identification CATLIN Engineers and Scientists Company Name 2. Well Construction Permit #: N/A 1 tat all applicable cell pernuts (i a Cowin State. Variance hyccuan etc) it Amour 3. Well use (check well use): Water SuDDIV Well: ❑ Agricultural ❑ Municipal, Public ❑Geothermal (Heating/Cooling Supply) ❑Residential Water Supply (single) ❑ Industrial 'Commercial ❑Residential Water Supply (shared) ❑ Irrigation ■ Monitoring 1-]Recovery ❑ Aquifer Recharge ■ Groundwater Remediation ❑ Aquifer Storage and Recovery ❑ Salinity Barrier ❑Aquifer Test ❑ Stormwater Drainage ❑ Experimental Technology ❑ Subsidence Control ❑Geothermal (Closed Loop) El Tracer ❑Geothermal (Heating/Cooling Return) ❑Other (explain under #21 Remarks) 4. Date Well(s) Completed: 12/10/2014 5a. Well Location: Building 1083 N/A Facility/Owner Name Facility ID# (if applicable) Buildinq 1083, Havelock 28533 Physical Address, City, and Zip Craven County Parcel Identification No. (PIN) 5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 34.9419216 N-76.8631403 W 6. Is (are) the well(s): ■Permanent or Temporary 7. Is this a repair to an existing well: ❑Yes or ■No /f this is a repair. Jill nut known ivell construction information and explain the native ofthe repair under #21 remarks sectinn or on the back ofthis form S. Number of wells constructed: 1 For multiple injection or non-natersupplp ixells ONLY kith the same construction roti cam submit one jornr. 9. Total well depth below land surface: 25 (ft.) For multiple hells list all depths ii'different (crample - 3 a 200' and 20 /00') 10. Static water level below top of casing: 13.26 (ft.) It water level is above tae "+" 11. Borehole diameter: 12.25 (in. For Internal Use ONLY. ft. ft. ft.1 ft. FROM I TO DIAMETER I THICKNESS I MATERIAL 0 ft. 10 ft. 4 in. Sch. 40 1 PVC ft. ft. in. 16. INNER CASING OR TUBING eothermal closed-I FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. ft. ft.i in. 17. SCMEN _ FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL 10 ft. 24.6 ft. 4 in. SIOt .010 Sch. 40 PVC ft.1 ft. in., FROM I TO MATERIAL EMPLACEMENT METHOD & AMOUNT' 0.3 ft. 4 ft. Portland cement Surface Pour 4 ft. 8 ft. Bent. Pellets Surface Pour ft. ft. 19: SAND/GRAVEL PA • K ifa able FROM TO I MATERIAL EMPLACEMENT METHOD 8 ft. 25 ft. #2 Med. Tor edo Sand Surface Pour ft. ft. 2n ,rign,&ING'LOG attach additional sheets if neceWilffl FROM TO DESCRIPTION ft. ft. ft. ft. PGH ft. ft. ft. ft. ft.1 fLl 22. Ltirication: Liz) -lov SigAature of Certified Well Contractor Date By signing this. form I herebv certify that the well(s) was (here) c onstncted in accordance with 15A NCAC 02C.0100 or 2C Well Construction Standards and that a copv of this record has been provided to the well otnner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTRUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Iniection Wells: In addition to sending the form to the address 12. Well construction method: H.S. Augers in 24a above, also submit one copy of this form within 30 days of completion of well construction to the following: (i.e. miger. rotnnt cable, direct push, etc) Division of Water Resources, Underground Injection Control Program, FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636 I 13a. Yield (gpm):. _ Method of test: 24c. For Water Supply & Iniection Wells: 13b. Disinfection e: Amount: Also submit one copy of this form within 30 days of completion of well construction to the county health department of the county where constructed. Adapted from NCDENR-DWR Form GW-I North Carolina Department of Fm ironment and Natural Resources- Dn axon of Water Resources Res iced August 2013 CATLIN WELL LOG Engineers and Scientists 210022 W Imo g?on, NC SHEET 1 OF 1 PROJECT NO.: 210022 STATE: NC I COUNTY: Craven LOCATION: Havelock PROJECT NAME: Building 1083 LOGGED BY: Shane Chasteen WELL ID: DRILLER: D.T. Chalmers, Jr. 41 GW03R NORTHING: 440684.2800 EASTING:2640322.3200 CREW: CATLIN SYSTEM: NCSP NAD 83 ft BORING LOCATION: Replace well 41GW03 T.O.C. ELEV.: 14.93 DRILL MACHINE: CME 550 ATV METHOD: H.S. Augers 0 HOUR DTW: 13.3 TOTAL DEPTH: 25.0 START DATE: 12/10/14 FINISH DATE: 12/10/14 124 HOUR DTW: N/A WELL DEPTH: 25.0 BLOW COUNT OVA LAB. o L SOIL AND ROCK WELL DEPTH 0.5tt 0.5a 0.5ft 0.5a (PPm) ID. s G DEPTH DESCRIPTION ELEVATION DETAIL 0.0 LAND SURFACE 14.9 0.0 0.0 _ 3.0 3.0 11.9 = - - 14.3 M (SC) - Tan, Clayey SAND. HCO. a 4.0 5.a 9-9 U 8.0 8.0 6.9 8.4 _ 9.5 M/W (CL) - Tan, CLAY. Soft w/med. plast. HCO. 10.0 4.9 10.0 13.0 13.0 19 3.1 Sat. ]_L5.0 (CUCH) - Gray, CLAY. Soft w/med. to high plast. Strong HCO. -0.1 of oa Oc 18.0 1B.0 •3,1 NL 2.3 Sat. (CL) - Dark gray, CLAY. Soft. Strong HCO. 20.0 •5.1 23.0 23.0 -8.1 _. 1.1 Sat. (CL) - S.A.A. 24.6 25.0 -10.1 25.0 25.0 25.0 Boring Terminated at Elevation -10.1 ft i EPortland Cement Benlonite Pellets F] #2 Medium Sand J( o� SITE LOCATION °ate Sao ROOSVEL-T-BL-VU 41 PR69 41GW105 ED NEUSE RIVER 268 66 41GW43 0 41 PR75 0 41 PR76 0 11 u v 41GW112 E 41 PR200 41 PR204 El 0 41 PR201 41PR72 ®41GW106 0 41PR203 0 41PR202 41 PR77 41GW05 ED 0 41 P 78 0 41GW36 41 PR79 El 41 PR80 E 41GW107 ED 41 PR81 0 N NEW WELL CONSTRUCTION MAP BUILDING 1083 MCAS CHERRY POINT, NC ®' <cii4esF�-�7ree�mgCommarn7 AR ANTIC OMS ICIM 41GW21 LEGEND ED Buildings Roads/Driveways ® New Recovery Well Location NOTES 41PR85 1. Existing 2" diameter wells 41 GW02 and 41 GW03 0 were completely removed then overdrilled and replaced with 4" diameter wells 41 GW02R and 41PR210 41PR212 41PR212 41GW03R. ❑ 0 0 41 PR82 41 PR215 ®1 GR213 41PR216 0 0 0 ❑041PR86 41PR217 41PR214 41 PR221 0 0 41PR2190 AlPR21 41GW03R 0 � 41 PR220 41 GW02R O 41 PR83""` ° \/ CATLIN Engineers and Scientists 41 PR87 FIGURE SITE PLAN WITH NEW WELL LOCATIONS 1 50 25 0 50 Feet Job No.: Date: Scale: Drawn By: Checked By: SCALE 210022.08 1 DEC 2014 AS SHOWN THW SAC