WQ0021577_Residual Annual Report 2018_20190221

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0021577
SUBMITTAL DATED: 2/21/2019
Project Contact Information
Rease provide information on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Neal Davis &Chris Williams
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0021577
Reviewer* Troy Doby
Phone Number*
252-533-6295
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Permittee * KapStone / WestRock Kraft Paper Corporation
Facility Name * KapStone / WestRock Kraft Paper Corporation Roanoke Rapids Mill
County* Halifax
Please provide comments/notes on your current submittal below.
Submitted Original and 3 copies February 18, 2019.
Did not distribute any residuals in 2018. Still ran analysis of residuals and included in the annual report
Please attach all information required or requested for this submittal to be review here.

Annual Kapstone WestRock Distributionof Residuals
4.54MB
Report 2018 WQ0021577.pdf
Application Form Engineering Rans, Specifications, Calculations, Etc.)
For neiv and modification permit applications, the paper copy is required to be subrrutted to the
Di,,isicn Be advised, applications ivill not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follo-kA*:
• Application Form
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineermg plan set
• 2 11-17" engineering plan sets
• 1 extra set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By U_S_ Postal Sen-ice:
Division of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh, NC 27699-1617
By Courier/Special Delivery:
Division of Wades Resources- Non -Discharge Branch
?: Nathaniel Thornburg- 9th Floor, Office #942WN
512 N_ Salisbury St_ Ralei NC 27604
For questions or problems contact Tessa Monday at 919.7073660 or TessaNlonday([ lcdcur-gov or
Sonia GraxTs at 919.707.3657 or SoniaLGraves(dpc&au.gov.
* I;W By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature Sign
Submission Date 2/21/2019

�� WestRock
February 12, 2019
NCDEQ-DWQ
Attention Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-01617
To Whom It May Concern:
100 Gaston Road
Roanoke Rapids, NC 27870
office: 252.533.6295
neal.davis@ westrock.com
Permit No. WQ0021577 requires that KapStone Kraft Paper Corporation, Roanoke Rapids Mill,
submit an annual Distribution of Residuals Solids report.
There were No Distribution of Residuals in 2018 All Solids were disposed of using the Kapstone
Kraft Paper Corporation Landfill Surface Disposal site (Permit # WQ000436) in 2018.
We did include the results from testing that was done in anticipation of the distribution of solids in
this Distribution of Residuals reports for 2018.
If there are any questions or concerns please contact me at 252-533-6295.
Sincerely,
ltt:ev
N Davis
Environmental Engineer
Enclosures
xc:
Ben White
Mike Knudson
Chris Williams
Central File

ANNUAL DISTRIBUTION OF RESIDUAL PERMIT REPORT 2018
PERMIT #WQ0021577
KAPSTONE KRAFT PAPER CORPORATION
ROANOKE RAPIDS, NC
TABLE OF CONTENTS
Page
Annual Land Application Certification Form........................................................................
Form DMSDF — Primary Clarifier Residuals Annual Certification 2018 ................... 1-2
Form RSSF — Primary Clarifier Residuals Sampling Summary..........................................3
Form RSSF-B — Primary Clarifier Residuals Sampling Summary B..................................4
Sample Analysis Primary Clarifier Residuals.............................................................5 —
28
TCLP — Sampling Analysis Primary Clarifier Residuals ......................................... 29 —
32
Form PVRF 02T — Primary Clarifier Residuals Annual Pathogen Reduction ........ 33 —
45
Form DMSDF — Flyash Residuals Annual Certification 2018........................................
46
Form RSSF — Flyash Residuals Sampling Summary ......................................................
47
Form RSSF-B — Flyash Residuals Sampling Summary B................................................
48
Sample Analysis Flyash Residuals.......................................................................... 49 —
72
TCLP— Flyash Residuals.......................................................................................... 73 —
76
Form PVRF 02T — Flyash Residuals Annual Pathogen Reduction Form ............... 77 —
89

ANNUAL LAND APPLICATION CERTIFICATION FORM
County:
Facility Name (as shown on permit):
Land Application Operator:
Year: "RQ%*
Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑ Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summarv:
Total number of application fields in the ermit:
Q
Total number of fields utilized for land application during the year:
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part n - Annuai ComDiance Statement:
Facility was compliant during calendar year
WQ Permit#:
with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ❑ Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Permittee Name and Title (typeRr print)
Signature of Permittee
Signalyle of Preparer* Date Signature of Land Applier
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
Date
Date
nFnIR FF'nphA ArIP /19/9nnrn

FORM DMSDF
PRIMARY CLARIFIER RESIDUALS
ANNUAL CERTIFICATION
2018

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2018 Kapstone Surface Disposal Unit Inputs
Permit # WQ0021577
x xo7t t
Primary
C`lar fier
Sludge,
)RyaNh
-
_ToW*
January
0.00
February
0.00
March
0.00
April
0.00
May
0.00
June
0.00
July
0.00
August
0.00
September
0.00
October
0.00
November
0.00
December
0.00
Total
0.00
Total amounts are the values per month listed on the surface disposal
form as Residual In.
These values are calculated, based on the amounts generated minus the amounts distributed as per
Distribution of Residuals permit # WQ0021577.
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Form RSSF
Primary Clarifier Residuals

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Form RSSF-8
Primary Clarifier Residuals Sampling
Summary 8

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Sampling Analysis
Primary Clarifier Residuals

Meritech, Inc.
Environmental Laboratory
` Laboratory Certification No.165
r •
Contact: Neal Davis Report Date: 1/22/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Project: Monthly
_ Date Sample Rcvd: 1/11/2018
Meritech Work Order #
011118114
Sample: Primary Clarifier Residuals Grab
1/11/18
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
Ammonia, Nitrogen
44.7 %
<22.4 mg/kg
1/12/18
1/18/18
0-100 %
22.4
SM2540B
TKN
Nitrate/Nitrite Nitrogen
763 mg/kg
1/15/18
mg/kg
40.5 mg/kg
g/
EPA 350.1
EPA 351.1
Nitrogen, total
<22.4 mg/kg
1;
763 mg/kg
1/12/18
1/18/18
22.4 mg/kg
20
EPA 353.2
Aluminum, total
10,400 mg/kg
g/ gS.
1/17/18
m
g/kg
mg/kg
EPA 353.2
EPA 200.7
Arsenic, total
Barium, total
7.91 mg/kg l;/ g
1/17/18
1.03 mg/kg
EPA 200.7
Cadmium, total
374 mg/kg
1.70 mg/kg
1/17/18
1/17/18
0.500 mg/kg
0.207
EPA 200.7
-Calcium, total
49 000 mg
mg/kg
1/17/18
mg/kg
10.0 mg/kg
EPA 200.7 '
EPA 200.7
Chromium, total
Copper, total
20.3 mg/kg
1/17/18
0.100 mg/kg g/ g
EPA 200.7
Lead, total
45.6 mg/kg
11.1 mg/kg
g
1/17/18
1/17/18
1.00 mg/kg
EPA 200.7
Magnesium, total
2,530 mg/kg
1/17/18
1.06 mg/kg
10.0 mg/kg
EPA Z00.7
EPA 200.7
Mercury, total
Molybdenum, total
0.022 mg/kg
< g/ g
0.559 mg/kg
1/15/18
1/17/18
0.02 mg/kg
EPA 245.1
Nickel, total
23.0 m
mg/kg
1/17/18
0,559 mg/kg
1.00 mg/kg
EPA 200.7
EPA
Phosphorous, total
1,110 mg/kg
1/17/18
2.00 mg/kg
200.7
EPA 200.7
Potassium, total
Selenium, total
2,600 mg/kg
1/17/18
20.0 mg/kg
EPA 200.7
Sodium, total
<1.12 mg/kg
mg/kg
4,140 mg/kg
1/17/18
1/17/18
1.12 mg/kg
20.0
EPA 200.7
Zinc, total
k
181 mg/kg g
1/17/18
mg/kg
g/ g
1.0 mg/kg
EPA 200.7
EPA 2001
SAR
3.30 -
1/17/18•
_
pH
CCE
7.7 S.U.
1/15/18
1.0 -14.0 S.U.
SM 4500 H B
6.20 %
1/16/18
1 %
AOAC 955.01
I hereby certify that I have reviewed and approve these data, �
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-I0.7013
.Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ0021577
M E RITECH, INC.
Client: Kapstone Kraft Paper Corp. Phone:_252-533-6295
Addre 100 Gaston Road Fax: [phone]
3
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC. Email:_ Neel. Davis@Kapstonepaper.c�
4
642 Tamco Rd.. Phone: [phone] .
27870 Project:_ Monthly I
Reidsville NC 27320 Fax: [phone]
P.O.#:'
Email: [e-mail]
Attention: Neal Davis Turn Around Time*
www.meritech-labs.com
How would you like our report sent? *RUSH work needs prior approval.
'Circle St 3-5 Da 24-48Hrs
all that apply: 0mal,s
preferred), Fax, Mail
a
Sampling Dates & TImes
Person Taking Sample (Si P nt): �
� s
-
La b�� Use:.
Sample Location
and/or ID #
Start
End
Comp?
Test(s).
Required
On Ice?
pH OK?
FTime
Date
Date
Time
Grab?
#of'Cont.
Yes No
Cl OK?
PRIMARY CLARIFIER RESIDUALS
%TOTAL SOLIDS, Ph, i
..
Metals: Ai, Ar, Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,.
Na,Ni, Se, Zn, Ptot, NH3, TKN; NO2, NO3
(�
P-A-N (by Calculation)
C-C-E (by Calculation)
`
Sodium Adsorption Ratio (by Calculation
Temperature Upon
Method Of
R ceipa'L,
*** Dechlonnation (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field priorto preservation.
Shipment:
Comments:
Compositor #
[� UPS
Jug #
Fed Ex
Are these resu s for regulatory purposes? Yeir
NQ Report results in: mg/L LI. mg/kg FJ ug/L
Hand Delivery
Relinquished by: D �:/ Time:
(j
Received ^ r� me:
Ti
Other
Relinquished b Da Time:
Received b .
y: Date: Time:
_
Relinquished by a Time:
Received by Time:
,— i
Loa

. w
- Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis Report Date: 2/21/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 2/8/2018
Meritech Work Order # 020818152 Sample: Primary Clarifier Residual Grab 2/8/18
Parameters
Results
Analysis Date
Re orting Limit
Method
% Total Solids
45.4 %
2/9/18
0-100 %
SM2540B
Arsenic, total
8.23 mg/kg
2/16/18
0.605 mg/kg
EPA 200.7
Barium, total
174 mg/kg
2/16/18
0.500 mg/kg
EPA 200.7
Chromium, total
15.5 mg/kg
2/16/18
0.100 mg/kg
EPA 200.7
Nickel, total
12.0 mg/kg
2/16/18
1.00 mg/kg
EPA 200.7
pH
8.8 S.U.
2/9/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data. `
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
7

5.9.2016 Chain of Custody Record (COC)
NPDES#: WQ002lS77 &WQ0000436-
Client; Kapstone Kraft Paper Corp Phone:_ 252-533-6295
Address:_ 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:_ Neal. Davis@ Kapstonepaper.cor
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email referred), Fax, ail Std(soda s) 3-5 Days 24-49Hrs
ME R I T E C H INC.
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone] '
Email: info@meritech[abs.com
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sam ign/P in /
'01,�/
Lab Use Only;
Start
End .
comp?
Grab?
#of
Cont.
Test(s) Required
On Ice?
Yes/No
pH OK?
Cl.OK?
Date
Time
Date
Time
Arsenic, Barium, Chromium, Nickel, pH, 1�
Total Solids
Temperature Upon.
Receipt: .
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation. ***
Comments:
Compositor$t
Jug #
UPS
Fed Ex
Are these results f r regulatory purposes? Yes No FJ
Report results in: mg/L mg/kg
ug/L
Hand Delivery
Relinquished by: D Time: /O 6�
I
Received by
te: Time- s
Other
Relinquish /+ J e: Time:
G���
Received by: Date: Time:
Relinquished Date: 'Time:
Received : (j

Meritech, Inc.
i Environmental Laboratory
H•�
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd:
3/21/2018
WQ0021577
WQ0000436
3/8/2018
Meritech Work Order #
030818151 Sample: Primary Clarifier Residuals Grab
3/8/18
Parameters
Results
Analysis Date
Reporting Limit
Method
Total Solids
38.6 %
3/9/18
0-100 %
SM2540B
Arsenic, total
5.23 mg/kg
3/15/18
0.605 mg/kg
EPA 200.7
Barium, total
264 mg/kg
3/15/18
0.500 mg/kg
EPA 200.7
Chromium, total
22.2 mg/kg
3/15/18
0.100 mg/kg
EPA 200.7
Nickel, total
21.9 mg/kg
3/15/18
1.00 mg/kg
EPA 200.7
pH
8.6 S.U.
3/9/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data. 4
. &"� �"
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
9

S-9-2016
Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
M E R I T E C H INC.
Client: Kapstone Kraft Paper Corp
Phone:_ 252-533-6295
1Address:_
100 Gaston Road
Fax: .[phone]
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870
Email:_ Neal. [e-mail]
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Neal Davis
Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
WWW.meritechlabs.com
Std soda s) 3-5 Days 24-48Hrs
Circle all that apply:(Ema' Fax,
(preferred),
ail
II Dates &Times
Person Taking Sampl(S' n/PrintSam
bU.,O" nl'y'"
Sample Location and/or ID # Start End
:_ -Z' -
Date
Comp? # of
Test(s) R
din.lce? p KOK�?.
q di red
Time Date Time
Grab? Cont.
Y60-No _ CI OK?:.
PRIMARY CLARIFIER RESIDUALS % . 3 '
� Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
i
Temperature upon, - •=-
Method of
Receipt -
*** Dechlorination (<0.5 ppm) of Ammdnia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Shipment:
Comments:
Compositor #_
UPS
-
rug # ,
Fed Ex
Are these results�qr regulatory purposes? - Yes
No Fj Report results in:
mg/L mg/kg ug/L
Wand Delivery..
Relinquished Date: / Time:
�� Received by:
Da / Tlme: O
Other
Relinquished h �B_at��� Time Received by:
Date: Time:
t
Relinquished by: Date: Time:
Received by L�
_ Date: time:
O
>J

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Project:
Date Sample Rcvd:
4/13/2018
WQ0021577
WQ0021577
00436
Monthly
4/5/2018
Meritech Work Order #
040518122 Sample: Primary Clarifier Residuals Grab
4/5/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
43.1 %
4/6/18
0-100 %
SM2540B
Ammonia, Nitrogen
<23.2 mg/kg
4/9/18
23.2 mg/kg
EPA 350.1
TKN
Nitrate/Nitrite Nitrogen
232 mg/kg
<23.2 mg/kg
4/6/18
4/6/18
40.5 mg/kg
23.2 mg/kg
EPA 351.1
EPA 353.2
Nitrogen, total
232 mg/kg
4/10/18
20 mg/kg
EPA 353.2
Aluminum, total
10,370 mg/kg
4/9/18
5.00 mg/kg
EPA 200.7
Arsenic, total
3.32 mg/kg
4/9/18
1.03 mg/kg
EPA 200.7
Barium, total
320 mg/kg
4/9/18
0.500 mg/kg
EPA 200.7
Cadmium, total
1.55 mg/kg
4/9/18
0.210 mg/kg
EPA200.7
Calcium, total
103,500 mg/kg
4/9/18
10.0 mg/kg
EPA 200.7
Chromium, total
21.6 mg/kg
4/9/18
0.100 mg/kg
EPA 200.7
Copper, total
89.3 mg/kg
4/9/18
1.00 mg/kg
EPA 200.7
Lead, total
6.31 mg/kg
4/9/18
1.06 mg/kg
EPA 200.7
Magnesium, total*
5600 mg/kg
4/9/18
10.0 mg/kg
EPA 200.7
Mercury, total
0.023 mg/kg
4/10/18
0.02 mg/kg
EPA 245.1
Molybdenum, total
<0.580 mg/kg
4/9/18
0.580 mg/kg
EPA 200.7
Nickel, total
18.6 mg/kg
4/9/18
1..00 mg/kg
EPA 200.7
Phosphorous, total
947 mg/kg
4/9/18
2.00 mg/kg
EPA 200.7
Potassium, total
3620 mg/kg
4/9/18
20.0 mg/kg
EPA 200.7
Selenium, total
<1.16 mg/kg
4/9/18
1.16 mg/kg
EPA 200.7
Sodium, total
4430 mg/kg
4/9/18
20.0 mg/kg
EPA 200.7
Zinc, total
116 mg/kg
4/9/18
1.0 mg/kg
EPA 200.7
SAR
1.81 -
4/9/18
_
-
pH
CCE
8.9 S.U.
4/6/18
1.0 -14.0 S.U.
SM 4500 H B
20.3 %
4/6/18
1 %
AOAC 955.01
19.
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-362013 Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ0021577
M E R I T E C H INC.
Client; Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre 100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES
T
Roanoke Rapids, NC. Email: Neal. Davis@Kapstonepaper.c
642 Tamco Rd. Phone: [phone]
27870 Project:_ Monthly
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Neal Davis Turn Around Time*
WWW.meritech—IGbs.com
: Ema• How would you like our report sent? *RUSH work needs prior approval.
Circle all thatappl (preferred), Fax, Mail Std(10 3-5 Days 24-49 Firs
days
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample (Sign/Print): /►-�
_
lab Use
Start
End
Comp?
Grab?
# of Cont.
Test(s) Required
On Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
Primary Clarifier Residuals
t(f�ZD►Q�
` j�
%TOTAL SOLIDS, Ph, C �-
Metals: Al, Ar, Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,
Na,Ni, Se, Zn, Ptot, NH3, TKN, NO2, NO3
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperature Upon
ecc
Method Of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Li _
Shipment: Comments: Compositor #
I UPS Jug #
�p Fed Ex Are these results for regulatory purposes? Yew Report results in: mg/L [I mg/kg FJ ug/L FJ
Hand Delivery
Other
Relinquished by: q Date:1� Jg Time:
Relinquished b W Dates Time: 00
Received by �^ D t/8 Time: O
Received by: Ti Date: me:
R nquished by: Date: Time:
Received by b: t^ in
N
U' /

• Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd:
5/21/2018
WQ0021577
WQ0000436
5/10/2018
Meritech Work Order #
051018150 Sample: Primary Clarifier Residuals Grab
5/10/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total -Solids
45.6 %
5/11/18
0=100 %
SM2540B
Arsenic, total
1.64 mg/kg
5/16/18
0.605 mg/kg
EPA 200.7
Barium, total
261 mg/kg
5/16/18
0.500 mg/kg
EPA 200.7
Chromium, total
39.3 mg/kg
5/16/18
0.100 mg/kg
EPA 200.7
Nickel, total
33.8 mg/kg
5/16/18
1.00 mg/kg
EPA 200.7
PH
7.6 S.U.
5/13/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: info@meritech[abs.com
www.meritechlabs.com
Sample Location and/or ID #
PRIMARY CLARIFIER RESIDUALS
Sampling Dates & Times
Start
End
Date
Time
Date
Time
7-W
Method of *** Dechlorination (<0.5 pl
Comments:
Ek UPS
F,dEx + Are these results for rq&la
Relinquished by: // %
Hand Delivery , // ,y{
Other IRelinquishe y. /
i
Relinquished by:
4
NPDES#:_
WQ 0021577 & WQ 0000436
Client: Kapstone Kraft Paper Corp
Phone:
252-533-6295
Address:_ 100 Gaston Road
Fax:
252-533-6264
Roanoke Rapids, NC 27870
Email:_
[e-mail]
Project:
P.O.#:
Attention:_ Neal Davis
Turn Around Time*
How would you like your report sent?
*RUSH work needs prior approval.
-Circle all that apply: Email (preferred), Fax,(Mail
Std 110 da s) 3-5 Da s
24-48Hrs
Person Taking Sample (Sign/Print
-
Lab Only
S -Use
Comp?
# of
Te/st(s)
On Ice?
Req u i red
pH OK?
Grab?
Cont.
Yes / No
Cl pK?
/
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
(purposes? Yes U No Q Reports results in: mg/L mg/kg
' Time: .� Received by
Time: �.�Dn Received by: Date:
Date: Time: Received y
C
Temperature Upon
Receipt:
• A 1�-
ug/L
Time:
Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis Report Date: 6/18/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 6/7/2018
Meritech Work Order # 060718137 Sample: Primary Clarifier Residuals Grab 6/7/18
Parameters Results Analysis Date Re orting Limit Method
% T-atal Solids
37.2 %
6/8/18
0-100 %
SM2540B
Arsenic, total
6.85 mg/kg
6/13/18
0.605 mg/kg
EPA 200.7
Barium, total
349 mg/kg
6/13/18
0.500 mg/kg
EPA 200.7
Chromium, total
31.2 mg/kg
6/13/18
0.100 mg/kg
EPA 200.7
Nickel, total
28.5 mg/kg
6/13/18
1.00 mg/kg
EPA 200.7
pH
8.6 S.U.
6/8/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data.
Labors ory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
15

59=0=6 Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436.
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email: Neal. Davis(@ Kapstonepaper.cor
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
*RUSH work needs. prior approval.
How would you li your report sent?
std da s) 3-5 Da s 24-48Hrs
Circle all that apply: m preferred) , Fa Mail
M E R I T E C H INC.-
1Address:_
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
'Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates & Times
p g
Person Taking Sam e(Sign/Pr' t):
�
Lab Use Only
start
End .
Comp?
Grab?
#of
Cont.
I
Tests)
Roq(uired
On Ice?
Yes / No:
pH OK?
Cl OK?
Date
Time
Date
Time
PRIMARY CLARIFIER RESIDUALS
7'�Q
%
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation.
Comments:
Compositor #
Jiag# _
UPS
Fed Ex
Are these resul for regulatory purposes? Yes No I
Report results in: mg/L U mg/kg [j
ug/L
Hand Delivery
ry
Other
Relinquished b Datej Time: O rO
.7
Relinquishe �_ r Date: Time: J
[� /
Received by: ate: Time:
O �
R ived by: Date: Time:
.-%
elinquished by: Date: Time:
Received by dab7at Ti
r i,� `�1, Y c-s-

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
1 A4.
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 071118166
Parameters Results
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorous, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
SAR
pH
CCE*
a
Report Date:
7/24/2018
NPDES#:
WQ0021577
WQ0000436
Project:
Monthly
Date Sample Rcvd:
7/11/2018
Sample: Primary Clarifier Residuals Grab
44.4
<20.2 mg/kg
283 mg/kg
<20.2 mg/kg
283 mg/kg
9,860 mg/kg
<1.13 mg/kg
376 mg/kg
1.68 mg/kg
82,900' mg/kg
24.3 mg/kg
67.8 mg/kg
9.23 mg/kg
4350 mg/kg
<0.023 mg/kg
<0.563 mg/kg
24.5 mg/kg
1745 mg/kg
2135 mg/kg
1.94 mg/kg
4300 mg/kg
208 mg/kg
2.63 -
7.6 S.U.
22.5 %
* Results not for regulatory purposes
Analysis Date
7/12/18
7/16/18
7/17/18
7/13/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/16/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/16/18
7/18/18
Reporting Limit
0-100 %
20.2 mg/kg
40.5 mg/kg
20.2 mg/kg
20 mg/kg
5.00 mg/kg
1.13 mg/kg
0.500 mg/kg
0.116 mg/kg
10.0 mg/kg
0.100 mg/kg
1.00 mg/kg
1.06 mg/kg
10.0 mg/kg
0.023 mg/kg
0.563 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
0.581 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 -14.0 S.U.
1%
7/11/18
Method
SM2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7 .
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500 H B
AOAC 955.01
I hereby certify that 1 have reviewed and approve these data.
Laborato epresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-2U-1033 Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQQ021577
M E R I T E C H, INC.
Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre 100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES
.Roanoke Rapids, NC. Email:_ Neal. Davis 6D Ka pstone pa per.ci
642 Tamco Rd. Phone: [phone]
27870 Project:_ Monthly I
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Neal Davis Turn Around Time*
www.meritech-labs.com
Sampling Dates & Times
Sample Location and/or ID # Start End -
Date Time Date Time
How would you like your report sent? *R work needs prior approval.
Circle all that apply: (preferred), Fax, Mai Sd(1 3-5 Da s 24-48Hrs
Ema'
' days
Person Taking Sample n/P Lab Use
comp?
°mp?
Grab?
# of Cont.
Test(s)
Required
� o
N
Yes No
pH OK?
C0
Primary Clarifier Residuals
It
'35
%TOTAL SOLIDS, Ph,
r
Metals: Ai, Ar; Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,
Na,Ni, Se, Zn, Ptot,_NH3, TKN, NO2, NO3
L--
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperature Upon
Receipt:
Method of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments: Compositor #
• '
Shipment:
UPS
Jug #
Fed Ex Are these results fgk regulatory purposes? Ye N Report results in: mg/L Ll mg/kg ug/L
Relinquished by:� D e: Time: :� Received b r at Hand Delivery
Other
Relinquished by: Time:
17- r ( f
Received by: D te: Time:
Relinquished b
q y Date: Time:
Receive a /L� T• g
( e• y .•j

Meritech, Inc.
Environmental Laboratory
* _ , Laboratory Certification No.165
i
Contact: Neal Davis
Client: Kapstone Paper & Packaging
Report Date:
8/20/2018
100 Gaston Rd.
NPDES#:
WQ0021577
Roanoke Rapids, NC 27870
Date Sample Rcvd:
WQ0000436
8/8/2018
Meritech Work Order #
080818109 Sample:
Primary Clarifier Residuals Grab
8/8/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
39.9 %
8/9/18
0-100 %
SM2540B
Arsenic, total
4.44 mg/kg
8/13/18
0.605 mg/kg
EPA 200.7
Barium, total
356 mg/kg
8/13/18
0.500 mg/kg
EPA 200.7
Chromium, total
29.3 mg/kg
8/13/18
0.100 mg/kg
EPA 200.7
Nickel, total
27.6 mg/kg
8/13/18
1.00 mg/kg
EPA 200.7
PH
6.8 S.U.
8/12/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data.
-1rZ;Loratoryy Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
19

s-9-20w Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
Client; I<apstone Kraft Paper Corp Phone:_ 252-533-6295
100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:_ Neal.Davis(cDKapstonepaper.cor
Project:
1 P.O.#:
Attention:_ Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all thatapply: preferred), Fax, Std 10da s) 3-5 Da s z4-4sHrs
Ei)
M E R I T E C H INC.
1Address:
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample ' /Pn
Lab- ,
Use Only -
Start
End
?
Comp.
Grab?
# of
Cont.
Tests)
Required
on Ice?
Yes./ No
pH OK?
Cl OK?
Date
Time
Date
Time
Primary Clarifier Residuals
?.f&Ani
&#5
Arsenic, Barium, Chromium, Nickel, pH, a
-
Total Solids
TemperatureUpon
Receipt:./��l
C'U
Method of
Shipment:
*** Dechlorination.(<0.5
ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation. ***
Comments:
Compositor #
jug#
UPS
Fed Ex
Are these results for regulatory purposes? Yes I No l
Report results in: mg/L mg/kg LJ ug/LLl
Hand Delivery
Relinquished by: te: Time:
/�
Received by: Time:
Other
Relinquish y: i Time: 5`"
Received by: Date: Time:
Relinquished by: Date: Time:
Received VI:✓ Time: I pr

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd:
9/24/2018
WQ0021577
WQ0000436
9/13/2018
Meritech Work Order #
091318102 Sample: Primary Clarifier Residuals Grab
9/13/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
45.9 %
9/14/18
0-100 %
SM2540B
Arsenic, total
3.18 mg/kg
9/19/18
0.605 mg/kg
EPA 200.7
Barium, total
329 mg/kg
9/19/18
0.500 mg/kg
EPA 200.7
Chromium, total
29.0 mg/kg
9/19/18
0.100 mg/kg
EPA 200.7
Nickel, total
25.9 mg/kg
9/19/18
1.00 mg/kg
EPA 200.7
pH
8.7 S.U.
9/14/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that 1 have reviewed and approve these data.
Laboratory epresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
21

S-9-2016 Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
M E R I T E C H INC.
1Address:_
100 Gaston Road Fax: [phone]
..
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email: [e-mail]
—
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs. prior approval.
www.meritechiabs.com
Circle all that apply: preferred) , Fa Mail Std 10 days) 3 - 5 Days Za-as Nrs
Email
Sampling Dates &Times
Person Taking Sample n/Print. b
Lab Use Only
Sample Location and/or ID #
ICJ
Start
End
�`
/Test(s)
On Ice?
pH OK?
Date
Time
Date
Time
Grab?
Cont.
Required
Yes / No
Cl OK?
PRIMARY CLARIFIER RESIDUALS
/J,��
7./67
6, O
Arsenic, Barium, Chromium, Nickel, pH,
%Total Solids
4 -
l
Temperature Upon
Receipt:
*** Dechlorination
(10.5 Ammonia, Cyanide, Phenol TKN
be done in the field
Method of
ppm) of and samples
must prior to preservation.
Comments:
Compositor #
Jug #
Shipment:
UPS
Fed Ex
Are these results 11 regulatory purposes? Yes a, No
Report results in: mg/L [ . mg/kg U
ug/L U
• Hand Delivery
Relinquished by: ` ,. Dare: Time:
@� J/%3 G
Received by: a Time:
.Other
Relinquished• �% 7 f% Time*- � %
� (J S
Received by: Date: Time:
Relinquished by: Date: Time:
Received by L at Tim
? lQ
L �Y
N

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 100418119 Sample: Primary Clarifier Residuals Grab
Parameters
Results
Analysis Date
Analyst,
0/8-Toal Solids
50.8 %
10/5/1-8
MR
Ammonia, Nitrogen
<19.7 mg/kg
10/9/18
NW
TKN
69.5 mg/kg
10/11/18
NW
Nitrate/Nitrite Nitrogen
<19.7 mg/kg
10/5/18
NW
Nitrogen, total
69.5 mg/kg
10/15/18
NW
Aluminum, total
6,080 mg/kg
10/11/18
ED
Arsenic, total
2.54 mg/kg
10/11/18
ED
Barium, total
482 mg/kg
10/11/18
ED
Cadmium, total
4.53 mg/kg
10/11/18
ED
Calcium, total
21,060 mg/kg
10/11/18
ED
Chromium, total
29.9 mg/kg
10/11/18
ED
Copper, total
109 mg/kg
10/11/18
ED
Lead, total
6.26 mg/kg
10/11/18
ED
Magnesium, total
7240 mg/kg
10/11/18
ED
Mercury, total
<0.020 mg/kg
10/9/18
MR
Molybdenum, total
<0.492 mg/kg
10/11/18
ED
Nickel, total
30.1 mg/kg
10/11/18
ED
Phosphorous, total
4000 mg/kg
10/11/18
ED
Potassium, total
3760 mg/kg
10/11/18
ED
Selenium, total
4.35 mg/kg
10/11/18
ED
Sodium, total
9040 mg/kg
10/11/18
ED
Zinc, total
675 mg/kg
10/11/18
ED
SAR
3.76 -
10/11/18
ED
pH
8.4 S.U.
10/5/18
BF
CCE*
33.0 %
10/22/18
LH
* Results not for regulatory purposes
I hereby certify that I have reviewed and approve these data.
Report Date:
10/24/2018
NPDES#:
WQ0021577
WQ0000436
Project:
Monthly
Date Sample Rcvd:
10/4/2018
Reporting Limit
0-100 Flo
19.7 mg/kg
40.5 mg/kg
19.7 mg/kg
20 mg/kg
5.00 mg/kg
0.581 mg/kg
0.500 mg/kg
0.116 mg/kg
10.0 mg/lcg
0.100 mg/kg
1.00 mg/kg
1.06 mg/kg
10.0 mg/kg
0.020 mg/kg
0.492 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
0.998 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 - 14.0 S.U.
1%
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
10/4/18
Method
SM234OB
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2,
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA Z00.7
EPA 245.1'
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500 H B
AOAC 955.01
23

3-20-2013
Chain of Custody Re; ord (COC)
N•PDES#: WQ0000436 & WQ00
Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC. Email:_ Neal. Davis@ Ka stone
27870 Project:_ Monthly
- P.O.#:
Attention: Neal Davis Turn Around Time
How would you like your report sent? *RUSH work needs prior a
Circle all that apply ED-11referred), Fax, Mai Std(10 3 z
days)
1577
�
a er.ci
M E R I T E C H, INC.
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
T•.
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW.meritech labs,com
3proval.
-49Hrs
Sample Location and/or ID #
Sampling Dates & Times
Person TakingSam ign/ i
4 S
Lab -
se.
start
End
Comp?
Grab?
#of Cont.
,
Test(s)
Required
On Ice?
Yes./'No
r
-:
H OK?
IOK?
Date
Time
Date
Time
PRIMARY CLARIFIER RESIDUALS
/
,' S
Z
%TOTAL SOLIDS, Ph,
Metals: Al, Ar, Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,
Na,Ni, Se, Zn, Ptot, NH3, TKN, NO2, NO3
P-A-N (by Calculation)
C-C-F (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperatur
Fee
Upon
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol
Comments:
Are these results f r r gulatory purposes? Yew",
e
Relinquished by: Dat Time:
Relinquished b v \ /�pafe��(+ Time:
( !/ G i
Relinquished by: Date: Time:
and .TKN-sampl'esifn:u'st be done in the field priorto preservation. *** ,
Compositor
Jug #
NIA _ •:.. ' Report results in: mg/L vo mg/kg I ug/L
Received by t ;
v to �p�_
Receivedb : r J
G Y Date: Time:
l
Receive Lj Tf e.
Ej UPS
Fed Ex
Hand Delivery
Other

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date: 11/20/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 11/8/2018
Meritech Work Order #
110818110
Sample: Primary Clarifier Residuals Grab
11/8/18
Parameters
Results
Analysis Date Analyst Reporting Limit
Method
% Total Solids
23.8 %
11/12/18
JM
0-100 %
SM2540B
Arsenic, total
<2.10 mg/kg
11/14/18
ED
2.10 mg/kg
EPA 200.7
Barium, total
525 mg/kg
11/14/18
ED
0.500 mg/kg
EPA 200.7
Chromium, total
37.3 mg/kg
11/14/18
ED
0.100 mg/kg
EPA 200.7
Nickel, total
35.6 mg/kg
11/14/18
ED
1.00 mg/kg
EPA 200.7
pH
7.8 S.U.
11/12/18
JM
1.0 - 14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data.
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
25

Chain of Custody Record (COC)'
NPDES#:_WQ0021577 & WQ0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
Address:_ 100 Gaston Road Fax: [phone]
Roanoke Rapids, NQ27870 Email:_ Neal. Davis@ Kapstonepaper.cor
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How -would you like your report sent? *RUSH work needs prior approval.
Circle all that apply Ema' (preferred), Fax(Mai Stcl 10da s) 3-5 Da s 24-48Hrs
' ME R I T E C H INC.
ENVIRONMENTAL LABORATORIES
5 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
- Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID#
am
Sampling Dates &Times
p g
Person Taking /Pr t
<S
rab•Use-:Ohly
Start
End
comp?
Grab?
#of
Cont.
Test
(s) Required
Onlce3._
yes-; No
'pH.OK?
.C; OK?
Date
Time
Date
Time
PRIMARY CLARIFIER RESIDUALS
/
Arsenic, Barium, Chromium; Nickel, pH,. (O
--�
Total Solids
Temperature Upon
Receipt:
1, ""-
Method -of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
_
Comp _ ositor #
Jug#
UPS
Fed Ex
Are these results f9J regulatory purposes? Yes No
Report results in: mg/L U mg/kg l
ug/L U
Hand Delivery
Other
Relinquished by: `� , Da lb Time: O L
Relinquished b _(J J r J7 Time: ` 67
eceived by: Time:
��/ a
Received.by Date: Time:
Relinquished by: Date: Time: _
Received b Ti 6

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date: 12/20/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 12/6/2018
Meritech Work Order # 12061896 Sample: Primary Clarifier Residuals Grab 12/6/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
38.6 %
12/18/18
0-100 %
SM2540B
Arsenic, total
<1.30 mg/kg
12/14/18
1.30 mg/kg
EPA 200.7
Barium, total
225 mg/kg
12/14/18
0.500 mg/kg
EPA 200.7
Chromium, total
18.2 mg/kg
12/14/18
0.100 mg/kg
EPA 200.7
Nickel, total
16.6 mg/kg
12/14/18
1.00 mg/kg
EPA 200.7
pH
8.4 S.U.
12/18/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data.
- " <4)-
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
27

59=0�6 Chain of -Custody Record (COC)
NPDES#: WQ0021577 & WQ0000436
Client; Kapstone Kraft Paper Corp Phorie:_ 252-533-6295
100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:_ Nea1.Davis @Kapstonepaper.cor
Project:
P.O.#:
Attention:_ Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: (preferred), Fax, Mail Std 1 da s) 3s 24
Ema'
M E R I TE C H INC,
1Address:
. ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
k
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW.meritechlab$.COm
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sa ple (Sign Print):
�S
Lab Use Only -
Start
EndComp?
Grab?
# of
Cont.
Tesf(sf
Required
on Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
PRIMARY CLARIFIER RESIDUALS
(Q111,
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
Temperature Upon
Receipt: J� LOrr-
/' -
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation. ***
Comments:
Compositor-#
Jugs#
LJ UPS
Fed Ex
Are these results fpr regulatory purposes? Yes No
Report results in: mg/L mg/kg J
ug/L L_J
ISr"and Delivery
�/1911
Relinquished by DayeTime: O�
Received by:at . Ti .
Other
Relinquished y: L_ q: = Time:
L 6 c
Recelv d by: Date: Time:
Relinquished by: Date: Time:
Rece b / to Tim
N J
00 - I`//

TCLP
Primary Clarifier Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Report Date: 10/25/2018
Contact: Neal Davis NPDES#: WQ0021577
Client: Kapstone Paper & Packaging WQ0000436
100 Gaston Rd. Project: Monthly
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 100418118 Sample: Primary Clarifier Residuals Grab 10/4/2018
1311- TCLP Metals
Parameter
Results
Analysis Date
An, alyst
Det. Limit
Reg. Limit
Method
Arsenic
<0.100 mg/L
10/15/2018
ED
0.100
5.0
EPA 200.7
Barium
0.575 mg/L
10/15/2018
ED
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
10/15/2018
ED
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
10/15/2018
ED
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
10/15/2018
ED
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
10/13/2018
MR
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
10/15/2018
ED
0.100
1.0
EPA 200.7 '
Silver
<0.050 mg/L
10/15/2018
ED
0.050
5.0
EPA 200.7
Parameter
Volatiles 8260
Semi Vol. 8270
TCLP Organics
Results Analysis Date Analyst Reporting Limit Method
Attached 10/15/2018 VV
Attached 10/23/2018 PM
8260
8270
Other Tests
Parameter Results Analysis Date Analyst Reporting Limit Method
Cyanide, total <0.500 mg/kg 10/10/2018 LH 0.500 mg/kg EPA 335.4
Sulfide <10.0 mg/kg 10/8/2018 LH 10 mg/kg SW 846 9038
Ignitability Will Not Ignite 10/22/2018 LH - EPA 1030
Corrositivity (pH) 8.4 S.U. 10/5/2018 BF 1.0 - 14.0 S.U. SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
,A Environmental Laboratory
Laboratory Certification No. 165
Page 2
Report Date: 10/25/2018
Contact: Neal Davis NPDES#: WQ0021577
Client: Kapstone Paper & Packaging WQ0000436
100 Gaston Rd. Project: Monthly
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 100418118 Sample: Primary Clarifier Residuals Grab 10/4/2018
1311- TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter Results Analysis Date Analyst Det, Limit Reg. Limit Dilution Factor
Endrin
<0.002 mg/L
10/22-23/18
MG
0.002
0.02 1
Chlordane
<0.003 mg/L
10/22-23/18
MG
0.003
0.03 1
Toxaphene
<0.05 mg/L
10/22-23/18
MG
0.05
0.5 1
Methoxychlor
<1.00 mg/L •
10/22-23/18
MG
1.00
10.0 1
Heptachlor
<0.0008 mg/L
10/22-23/18
MG
0.0008
0.008 1
Lindane
<0.040 mg/L
10/22-23/18
MG
0.040
0.4 1
Herbicides - SW-846 8151A
Parameter
Results
Analysis Date
Analyst
Det. Limit
- Reg. Limit
Dilution Factor
2,4-D
<1.00 mg/L
10/22-23/18
MG
1.00
10.0
1
2,4,5-TP (Silvex)
<0.100 mg/L
10/22-23/18
MG
0.100
1.0
1
I hereby certify that have reviewed and approve these data. Am L
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
Environmental Laboratories
I
Laboratory Certificate #165
Client: Kapstone Kraft Paper Corp.
Project: Monthly
Client Sample ID: Primary Clarifier Residuals
Sample Collection: 10/04/18
Meritech Sample ID: 100418118
1311 - TCLP Organics
Volatiles: SW-846 8260
Analysis: 10/15/18
Extraction:
10/08/18
Analyst: VVVrV
Report Date:
10/19/18
Parameter
Result
Units
Det. Limit
Ree. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1,1-Dichloroethene
< 0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone
<0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 10/23/18
Extraction:
10/08/18
Analyst: PM
Report Date:
10/23/18
Parameter
Result
Units
Det. Limit
ReE. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data.
L"� N/ ku,
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]
3

3-30-2M Chain of Custody Record.(000) .
NPDES#- WQ0000436 & WQ00 1577
ME R I TE C H, I �, Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295 '
Add're 100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES Roanoke Rapids, NC.. -
Email: Neal. Davis(a) Ka Pstone a er.cr
642 Tamco Rd. Phone: [phone] I
Project:_ Monthly
Reidsville- NC27320 Fax:[phone].
' P.O.#:
Email: [e-mail] Attention: Neal Davis Turn Around Time
How would you.like your report sent? *RUSH work needs prior a proval.
www.meritech-labs.com 5td(�o 3-5 Da s z - Hrs
Circle all that apply: mail preferred) , Fax, Mail -
da s
Sampling Dates & Times person Taking Sam i rint
Sample Location and/or ID # Starter -
End 'comp?
Date Time Date Time Grab? #of Cont. Test(s)Required .
IGNITABILITY, REACTIVITY,CORROSIVITy
TCLP TO INCLUDE:
Arsenic (5.0) 1,4 Dichlorobenzone
r—. Nfrolie 0'.
Barium 100:0
( ) 1,2-Dichloroetliane (0.5) Pentaelil'gtgpenbl.(1.0 .0)
Benzene 1,1-Dichloroethylene (0.7) Pyii
dineC .. ). S.0 .
'Cadmium (1.0) ' ' 2,4 Dinitrotdlueno (0:13) Selenium
(l.0)
Carbon:tetrachloride (0.5) FnNrin (002) :.. Salver,(50)
Chlordai%'(0;03) Hexachlorobenzene (Oiea) 4::, • Tetrachloroethylene_( :7)
Chlorobenzene (100.0) I3eptachlofaudfshydroxide): ' ' : ° =�
(0 00.8 Toxap$ene .,(0.5)
Chloroform 6:0
(; .. )' �Iea�achioro-l;3-butailierie:(0.5) i chl_oroethyee;(0. ")
Method of ( ppm) of Ammonia, Chromium 5 0 - *** Dechlorination <0.5 ( ) Hexachloroethaue (3:0) 2,4,5=Tricblorophenbl (As 0.0)
Shipment: Comments: m=Cresol.(20Dr0): Yiead SD : `
.. -(` ) - 2,4,!S. iehlorop7ienol}( )
o-Cresol 2Q0.0
r Ae
l}PS � (. -) � , . L?ndaue� (0,4) 2;45=TP (Silvex�t(1. )
Fed Ex Are these r suits for regulatory plCresol..(200.0) Mec _ 0;2 g N purpose, rl?!,( .-) . Vi1iy1 chloride (0.2)
Hand Delivery Relinquished b Cresol (200.0
�✓ i ) 1Vlethoxychl6r. (10.0)
.Relin uishe
Other q y Date: 2,4-D Methyl ethyl ketone (200:0) "
Relinquished by: Date: Time( ©5 - - - ^
' [ Received
Jai L to .,/�� 2 LT(
�— D —1 O Tim ...
N

Form PVRF 02T
Primary Clarifier Residuals
Annual Pathogen Reduction Form

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Kapstone Kraft Paper Corporation
WWTP Name: Roanoke Rapids Mill
Monitoring Period: From 1/1/2018 To
WQ Permit Number:
NPDES Number:
10/31/2018
WQ0000436
NC 0000752 PCR
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑ I
Alt. C (Prior Testing) p
A1t.D (No Prior Test) ❑ 1
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
I Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
time Stabilization ❑ 1
Ai Drying 0
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion 0
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
in
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -
ni ue
Minimum
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
< 177
215.67
535
col/g dry
0
QTR
Fecal
sm9222D
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC
02T.1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
v❑ "I certify, under penalty of law, that the pathogen requirements in 15A.NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Neal R. Davis Environmental Engineer None Distributed in 2018
Prep arer Name a T' e e or print) Land Applier Name and Title (if applicable)(type or print)
Signatu a of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
33
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Neal Davis Report Date: 1/22/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 1/11/2018
Meritech Work Order # 011118122 Sample: PCR 171-18 Grab 1/11/18
Parameters Results Analysis Date Reporting Limit, Method
% Total Solids 41.9 % 1/12/18 0-100 % SM 2540B
Fecal Coliform 217 col/ g dry 1/11/18 183 col/ g dry SM 9222 D
Meritech Work Order # 0.11118123 Sample: PCR 1-2-18 Grab 1/11/18
Parameters I Results Analysis Date Reporting Limit Method
% Total Solids 45.3 % 1/12/18 0-100 % SM 254013
Fecal Coliform <201 cal/ g dry 1/11/18 201 col/ g dry SM 9222 D
Meritech Work Order # 011118124 Sample: PCR 1-3-18 Grab 1/11/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
44.6 %
1/12/18
0-100 %
SM 2540B
.Fecal Coliform
<204 col/ g dry
1/11/18
204 col/-g dry
SM 9222 D
Meritech Work Order # 011118125 Sample: PCR 1-4-18 Grab
Parameters Results Analysis Date
% Total Solids 43.6 % 1/12/18
Fecal Coliform <209 col/ g dry 1/11/18
Meritech Work Order # 011118126 Sample: PCR 1-5-18 Grab
Parameters
Results Analysis Date
Reporting Limit Method
0-100 % SM 2540B
209 col/ g dry SM 9222 D
Reporting Limit Method
% Total Solids 44.7 % 1/12/18 0-100 % - SM 2540B
Fecal Coliform <203 col/ g dry 1/11/18 203 col/ g dry SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
A.
Environmental Laboratory
Laboratory Certification No.165
y
Page 2
Contact: Neal Davis Report Date: 1/22/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 1/11/2018
Meritech Work Order # 011118127 Sample: PCR 1-6-18 Grab 1/11/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 42.5 % 1/12/18 0-100 % SM 2540B
Fecal Coliform 428 col/ g dry 1/11/18 183 col/ g dry SM 9222 D
Meritech Work Order # 011118128 Sample: PCR 1-7-18 Grab 1/11/18
Parameters Results Analysis Date, Reporting Limit Method
% Total Solids
46.8 %
1/12/18
0-100 %
SM 2540B
Fecal Coliform
194 col/ g dry
1/11/18
183 col/ g dry
SM 9222 D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
35

Chain of Custody Record. (COC)
NPDES#:_ WQ 0021577 & WQ 0000486
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295 '
M E R ITE C H INC,
1Address:_
100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email:_ Neal.Davis Kapstonepaper.cor
642Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
www.meritechlabs.com
Circle all that apply: Email referred), Fax, Mail Stcl(10da s) 3-5 Da s 24
Sampling Dates & Times
Person Taking Sample rin
amp
�A ,4a
Sample Location and/or ID #
Start
End
,
Comp.
#of
Test(s-) Required
On`:ice?
�.�Yes;%'.No
p H; 0,1(?:!
Date
Time
Date
Time
Grab?
Cont.
CI OK?
PRIMARY CLARIFIER
PCR1-1-18
CLASS A FECAL COLIFORM ANALYSIS
PCR1-2-18
'GS
CLASS A FECAL COLIFORM ANALYSIS
PCR1-3-18
`%D
CLASS A FECAL COLIFORM ANALYSIS
PCR1-4-18
CLASS A FECAL COLIFORM ANALYSIS
PCR1-5-18
CLASS A FECAL COLIFORM ANALYSIS
PCR1-6-18
,'ZS
CLASS A FECAL COLIFORM ANALYSIS J�
I
PCR1-7-18!'3
D
CLASS A FECAL COLIFORM ANALYSIS
Temperature Upori
Receipt
** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation.
Method of
Comments:
! om7bsitor.#
Jug#
Shipment:
UPS
F x
Are these resul fcA regulatory purposes? Yes No
Report results in: mg/L [ mg/kg ug/L
Hand Delivery
Relinquished by: �� - Date: ` Time: j ©
'/
Received b to p` Time: O V
o
Other
Relinquish e: Time: l /(
Received by: Date:Q Time:
r'
Relinquished by: ate: Time:
Recei�y Lab j ` t tsi

n,.
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Meritech Work Order # 04051890 Sample: PCR-4-1 Grab
Parameters
Results Analysis Date
Page 1
Report Date: 4/16/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 4/5/2018
4/5/18
Reporting Limit Method
% Total Solids 45.3 % 4/6/18 0-100 % SM 2540B
Fecal Coliform <201 col/ g dry 4/5/18 201 col/ g dry SM 9222 D
Meritech Work Order # 04051891 Sample: PCR-4-2 Grab 4/5/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.4 % 4/6/18 0-100 % SM 254013
Fecal Coliform <200 col/ g dry 4/5/18 200 col/ g dry SM 9222 D
Meritech Work Order # 04051892 Sample: PCR-4-3 Grab 4/5/18
Parameters Results Analysis Date Reporting Limit Method
Wo-Total-Solids -- 47% ——/671-8 0=100�I`o SM 2540B
Fecal Coliform 193 col/ g dry 4/5/18 174 col/ g dry SM 9222 D
Meritech Work Order # 04051893 Sample: PCR-4-4 Grab 4/5/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.9 % 4/6/18 0-100 % SM 2540B
Fecal Coliform <198 col/ g dry 4/5/18 198 col/ g dry SM 9222 D
Meritech Work Order # 04051894 Sample: PCR-4-5 Grab 4/5/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.3 % 4/6/18 0-100 % SM 2540B
Fecal Coliform <201 col/ g dry 4/5/18 201 col/ g dry SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
_ Laboratory Certification No.165
a
Page 2
Contact: Neal Davis Report Date: 4/16/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 4/5/2018
Meritech Work Order # 04051895 Sample: PCR-4-6 Grab 4/5/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 44.5 % 4/6/18 0-100 % SM 2540B
Fecal Coliform <204 col/ g dry 4/5/18 204 col/ g dry SM 9222 D
Meritech Work Order # 04051896 Sample: PCR-4-7 Grab 4/5/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.0 % 4/6/18 0-100 % SM 254013
Fecal Coliform 404 col/ g dry 4/5/18 174 col/ g dry SM 9222 D
1 hereby certify that 1 have reviewed and approve these data. G
. &
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

59-2016
Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
M E R ITE C H1 INC.
Address:_ 100 Gaston Road Fax: [phone]
_
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email:_ Neal.Davis Kapstonepaper.cor
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Neal Davis Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
www.meritechiabs.com0EmaQ
Std l0da s) 3-5 Da 5 24-49Hrs
Circle all that apply:(preferred), Fax, Ma'' =
Sampling Dates & Times
Person Taking Sample (Sign/Print):
/Required
Lab Use Only
Sample
ocation and/or ID #
Start
End
comp?
#of
Test(s)
Req u i red
on Ice?
Yes / No
pH OK?
Date
Time
Time
Grab?
Cont.
Cl OK?—
r' %Date
PRIJ10ARY
CLARIFIER
PCR-4-1
t
CLASS A FECAL COLIFORM ANALYSIS
PCR-4-2
ZO
G
CLASS A FECAL COLIFORM ANALYSIS Gl
I
PCR-4-3
8 Z5-
CLASS A FECAL COLIFORM ANALYSIS
PCR-4-4
���0
�-
t'
CLASS A FECAL COLIFORM ANALYSIS
PCR-4-5=S^
c�
CLASS A FECAL COLIFORM ANALYSIS 7��^
PCR-4-6
g= r{D
CLASS A FECAL COLIFORM ANALYSIS�� J
PCR -4-7
6- T
I
CLASS A FECAL COLIFORM ANALYSIS
I
Temperature Upon
Receipt:
.7
Meth
I
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN
samples
must be done in the field prior to preservation. ***
of
Comments:
Compositor #
Shipm
nt:
Jug #
UP
Fed
x
Are these results for regulatory purposes? Yes No („
Report results in: mg/t_ [ mg/kg LJ ug/L
1-3;
\Hand
livery
Relinquished by: /L( 1 Date: r /,,b Time: D /
i ((/� 6
Received b at :�/ Time: Q
Oth
Relinquished b Date, Time: ��
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Da ;� t( Time:G

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 071118156 Sample: PCR 7-18 Grab
Parameters Results Analysis Date
% Total Solids 44.2 % 7/11/18
Fecal Coliform 206 col/ g dry 7/11/18
Page 1
Report Date: 7/19/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 7/11/2018
7/11/18
Reporting Limit Method
0-100 % SM 2540B
183 col/ g dry SM 9222 D
Meritech Work Order #
071118157
Sample: PCR 7-18 Grab
7/11/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
45.0 %
7/11/18
0-100 %
SM 2540B
Fecal Coliform
<202 col/
g dry 7/11/18
202 col/ g dry
SM 9222 D
Meritech Work Order #
071118158
Sample: PCR 7-18 Grab
7/11/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids 45.0 % 7/11/18 0-100 % SM 2540B
Fecal Coliform <202 col/ g dry 7/11/18 202 col/ g dry SM 9222 D
Meritech Work Order # 071118159 Sample: PCR 7-18 Grab 7/11/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.9 % 7/11/18 0-100 % SM 2540B
Fecal Coliform <198 col/ g dry 7/11/18 198 col/ g dry SM 9222 D
Meritech Work Order # 071118160 Sample: PCR 7-18 Grab 7/11/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 44.4 % 7/11/18 0-100 % SM 2540B
Fecal Coliform <205 col/ g dry 7/11/18 205 col/ g dry SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Neal Davis Report Date: 7/19/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 7/11/2018
Meritech Work Order # 071118161 Sample: PCR 7-18 Grab 7/11/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.4 % 7/11/18 0-100 % SM 2540B
Fecal Coliform <200 col/ g dry 7/11/18 200 col/ g dry SM 9222 D
Meritech Work Order # 071118162 Sample: PCR 7-18 Grab
Parameters Results Analysis Date
% Total Solids 45.0 % 7/11/18
Fecal Coliform <202 col/ g dry 7/11/18
7/11/18
Reporting Limit Method
0-100 % SM 2540B
202 col/ g dry SM 9222 D
I hereby certify that I have reviewed and approve these data. f��x
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016 Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436-
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
M E R ITE C H -INC.
1Address:
100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email: Neal. Davis(@Kapstonepaper.cor
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ Neal Davis Turn Around Time*
How would you like your report sent? *RUS or needs prior approval.
WWW.merltechiabs.cOm
Circle all that apply: mail Fax, ai Ad soda s) 3-s Days 24-48Hrs
i
referred),
��� c::—_)
Sampling Dates & Times
Person Taking Sample (5' n int): - '�
Lab -Use Only.
':on-lce?-_
Sample -Location and/or ID #
Start
End
Comp?
# of
/Te-st(s) Required
.pH:OK?
Date
Time
Date
Time
Grab?
Cont.
Yes-/ No
Cl OK?.
PRIMARY CLARIFIER
PCR-1-7-18
CLASS A FECAL COLIFORM ANALYSIS S C
PCR-2-7-18
CLASS A FECAL COLIFORM ANALYSIS
PCR-3-7-18
CLASS A FECAL COLIFORM ANALYSIS
PCR-4-7-18
CLASS A FECAL COLIFORM ANALYSIS
PCR-5-7-18
CLASS A FECAL COLIFORM ANALYSIS V
PCR-6-7-18
D�
1
CLASS A FECAL COLIFORM ANALYSIS i
PCR-7-7-18
nqi
CLASS A FECAL COLIFORM ANALYSIS l Ul
Temperature Upon
Receipt:
Method of
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation. ***
Comments:
IJUg
Compositor #
#
Shipment:
Q UPS
IJ Fed Ex
Are these results fA regulatory purposes? Yes No
Report results in: mg/L mg/kg _LJ
ug/L
Hand Delivery
Relinquished by: te: Time:
-^�
Received by t Time: ..�
_ _ _
Other
Relinquished te• Time 1
Received y: Date: Time:
-
Relinquished by: [)Aa- Time:
Rec i e: Tire
l J

Meritech, Inc.
Environmental Laboratory
d
- Laboratory Certification No.165
Page 1
Contact: Neal Davis Report Date: 10/12/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 10041898 Sample: PCR 1-10-18 Grab 10/4/18
Parameters
Results Anaiysis Date
Reporting Limit
Method
% Total Solids
48.2 % 10/5/18
0-100 %
SM 2540B
Fecal Coliform
<189 col/.g dry 10/4/18
189 col/ g dry
SM 9222 D
Meritech Work Order #
10041899 Sample: PCR 2-10-18 Grab
10/4/18
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
51.1 % 10/5/18
0-100 %
SM 2540B
Fecal Coliform
<178 col/ g dry 10/4/18
178 col/ g dry
SM 9222 D
Meritech Work Order #
100418100 Sample: PCR 3-10-18 Grab
10/4/18
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
49.9 % 10/5/18
0-100 %
SM 2540B
Fecal Coliform
<182 col/ g dry 10/4/18
182 col/ g dry
SM 9222 D
Meritech Work Order #
100418101 Sample: PCR 4-10-18 Grab
10/4/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
17.0 %
10/5/18
0-100 %
SM 2540B
Fecal Coliform
<535 col/ g dry
10/4/18
535 col/ g dry
SM 9222 D
Meritech Work Order # 100418102 Sample: PCR 5-10-18 Grab
Parameters
Results Analysis Date
10/4/18
Reporting Limit Method
% Total Solids
48.7 %
10/5/18
0-100 %
SM 2540B
Fecal Coliform
<187 col/ g dry
10/4/18
187 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
43

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
L� Page 2
Contact: Neal Davis Report Date: 10/12/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 100418103 Sample: PCR 6-10-18 Grab 10/4/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 48.8 % 10/5/18 0-100 % SM 2540B
Fecal Coliform <186 col/ g dry 10/4/18 186 col/ g dry SM 9222 D
Meritech Work Order # 100418104 Sample: PCR 7-10-18 Grab 10/4/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
51.4 %
10/5/18
0-100 %
SM 2540B
Fecal Coliform
<177 col/ g dry
10/4/18
177 col/ g dry
SM 9222 D
1 hereby certify that have reviewed and approve these data. f�t
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

�,zal6 Chain of Custody Record (COC)
NPDES#:_WQ0021577
Client: Kapstone Kraft Paper Corp Phone:_
&WQ0000436
252-533-6295
M E R ITE C H INC.
�
lAddress:
100 Gaston Road Fax:
252-533-6264
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email:_
Neal. [e-mail]
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:' Neal Davis
Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
www.meritechiabs.com
Circle all that apply: E ai preferred) , Fax, ail"
Std lOda s)
3-5 Da s 24-48Hrs
Sampling Dates & Times
Person TakingSamipl SiS' /P,..
/S
Lab Use Only
Sample Location and/or ID #
Start
End
Comp?
#of
Test(s) Req u i red
On Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
Grab?
Cont.
PRIMARY CLARIFIER
PCR-1-10-18
C)
?;
C�- II
CLASS A FECAL COLIFORM ANALYSIS
PCR-2-10-18
,��
C
(
CLASS A FECAL COLIFORM ANALYSIS
PCR-3-10-18
?;
I
CLASS A FECAL COLIFORM ANALYSIS
PCR-4-10-18.�(jtI
CLASS A FECAL COLIFORM ANALYSIS
�U
PCR-5-10-18
,'QS'
I
CLASS A FECAL COLIFORM ANALYSIS
r1�
PCR-6-10-18
g,'�D
Cy
CLASS A FECAL COLIFORM ANALYSIS
[G�
PCR-7-10-18 .
�.
C9'
CLASS A FECAL COLIFORM ANALYSIS
�Oi
Temperature Upon
Receipt: >�
Method of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
or#
Compositor #
Comments:
Shipment:
UPS,
Jug#
d Ex Are these results for/regulatory purposes?
Yes 1;
No I Report results in: mg/L
mg/kg Lj ug/L U
Relinquished by:
Time: j Received b
�Hand-Delivery
TiB/fJ)
Other Relinquished Da
Time Rec ivFd by:
Date:
Tme:
Relinquished by: Date:
Time: Re ed L b:
e II
Time: VI M I
U

Aol
FORM DMSDF
FL YASH
ANNUAL CERTIFICATION
2018

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0000436
PHONE: [phone]
FACILITY NAME: KAPSTONE KRAFT PAPER CORP. ROANOKE RAPIDS, NC
COUNTY: NORTHAMPTON OPERATOR: NEAL DAVIS
FACILITY TYPE (please check one): X Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? X Yes No —► If No skin Darts A. B. C and certifv form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient
Information
Amendment/ Bulking
Agent
- Residual In
Product Out
Name(s)
Volume (As
Is Tons
Intended use(s)
January
FLYASH
840.2
NO DISTRIBUTIONS
February
FLYASH
308.9
DURING 2018
March
FLYASH
1,066.90
April
FLYASH
0
May
FLYASH
1,111.20
June
FLYASH
146.7
July
FLYASH
929.4
August
FLYASH
728.2
September
FLYASH
391.5
October
FLYASH
220.5
November
FLYASH
606.8
December
FLYASH
866.8
Total from FORM DMSDF (sup)l
0
0
0
Totals: Annual (dry tons):1
0
7,217.0
0.0
0.00
Amendment(s) used: 1 0
Bulking Agent(s) used: 0
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar year with all conditions of the Distribution of Residuals permit (including but not limited to X Yes
items 1-3 below) issued by the Division of Water Quality: No --► If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and plete. I am aware that there are significant penalties for submitting false
infor ation, includin the p ssib" ity of fines and imprisonment for knowing violations."
02AO
Signatur of Permittee Date Signatur of Preparer** Date
(if di rent from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Form RSSF
Fl yash Residuals

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ000436
Facility Name: KapStone Kraft Paper Corporation
Residual Source WQ # or
NPDES #:
WWTP Name: KapStone Kraft Paper Corporation
Residual Analvsis Data
Laboratory: 1) Meritech, Inc. Reidsville, NC
2)
3)
4)
5) FLYASH
Parameter
Parameter
Ceiling
Conc.
Limit
Sample or Composite Date
1/11/18
2/8/18
3/8/18
4/5/18
5/10/18
6/7/18
7/11/18
8/8/18
9/13/18
10/4/18
11/8/18
12/6/18
Percent Solids M
NA
J, ), r
58.3
56.3
49.1
56.2
41.5
50.1
58.4
46.8
44.9
30.6
46
Arsenic
75
13.7
7.63
6.31
1 5.42
8.43
13.9
11.2
11.3
4.96
31.5
7.35
10.9
Cadmium
85
0.659
0.257
1
0.758
1 1.41
Copper
4,300
43
42.4
36.9
256
Chromium
NA
13
11.8
12.2
13.8
13.3
17.3
16.1
13.2
20.4
91.5
22.8
30.2
Lead
840
12.5
6.54
10.7
66.9
Mercury
57
0.067
1 0.041
0.1
1
0.171
Molybdenum
75
0.476
0.509
0.741
2.44
Nickel
420
16.5
10.8
13.9
15.6
19.2
24.6
21
12.8
23.9
105
30.9
35.7
Selenium
100
0.952
1.02
0.998
4.27
Zinc
71500
23
14.5
32.1
226
Total Phosphorus
NA
613
1 444
796
1
5840
TKN
NA
523
551.9
529
161
Ammonia -Nitrogen
I NA
1 19
20.4
20
85.5
Nitrate and Nitrite
I NA
1 19
20.4
20
85.5
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly
gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment
for tmowing violations." l
Signature of
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
.A
v

Form RSSF-8
Fl yash Residuals

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar
WQ Permit Number: WQ0000436
Facility Name: KAPSTONE KRAFT PAPER CORP
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
KAPSTONE KRAFT PAPER CORP
Laboratory: 1) Meritech, Inc. Reidsville, NC
2)
3)
4)
5) Flyash
Parameter (mg/kg)
Sample or Composite Date
1/11/18
2/8/18
3/8/18
4/5/18
5/10/18
6/7/18
7/11/18
8/8/18
9/13/18
10/6/18
11/8/18
12/6/18
Aluminum
14,600
11,730
11,520
41,200
Calcium
10,340
11,380
9,060
59,400
Magnesium
1,480
1 1,270
1,120
1
9,200
Sodium
1,780
1,530
1,400
8,900
Potassium
5,200
4,380
4,130
23,300
CCE
1%
1%
1%
1%
SAR
3.14
2.54
1
2.62
3.07
PAN
230.1
243.2
233.6
1
158.5
pH
8.7
8.6
9
7.2
8.3
8.7
7.8
8.2
8.8
8.9
9
9
cR. certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the p sibility of fines and imprisonment for knowing violations."
Signature of Plelfined
arer * Date
*Preparer is in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)

Sampling Analysis
Fl yash Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 011118113
Parameters
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total
Magnesium, -total
Mercury, total
Molybdenum, total
Nickel, total
Pgosphorous, total Y
Potassium, total
Selenium, total
Sodium, total
Zinc, total
SAR
PH
CCE
esult
Sample: Flyash Grab
52.5 %
<19.0 mg/lcg
523 mg/kg
<19.0 mg/kg
528 mg/kg
14,600 mg/kg
13.7 mg/kg
699 mg/kg
0.659 mg/kg
10,340 mg/kg
13.0 mg/kg
43.0 mg/kg
12.5 mg/kg
'1480 mg/kg
0.067 mg/kg
<0.476 mg/kg
� 16.55 mgLk
613 mg/kg
5200 mg/lcg
<0.952 mg/kg
1780 mg/kg
23.0 mg/kg
3.14 -
8.7 S.U.
<1.0 %
Analysis Date
Report Date:
1/22/2018
NPDES#:
WQ0021577
WQ0000436
Project:
Monthly
Date Sample Rcvd:
1/11/2018
Reporting Limit Method
1/12/18
0-100 %
SM2540B
1/18/18
19.0 mg/kg
EPA 350.1
1/15/18
40.5 mg/kg
EPA 351.1
1/12/18
19.0 mg/kg
EPA 353.2
1/18/18
20 mg/kg
EPA 353.2
1/17/18
5.00 mg/kg
EPA 200.7
1/17/.18
1.03 mg/kg
EPA 200.7
1/17/18
0,500 mg/kg
EPA 200.7
1/17/18
0.210 mg/kg
EPA 200.7 ,
1/17/18
10.0 mg/kg
EPA 200.7
1/17/18
0.100 mg/kg
EPA 200.7
1/17/18
1.00 mg/kg
EPA 200.7
1/17/18
1.06 mg/kg
EPA 200.7
1/17/18
10.0 mg/kg
*EPA 200.7
1/15/18
0.02 mg/kg
EPA 245.1
1/17/18
0.476 mg/kg
EPA 200.7
1/17/18
T 1-0-0-mg/kg ---
- - EP-A-200-7 - --
1/17/18
2.00 mg/kg
EPA 200.7
1/17/18
20.0 mg/kg
EPA 200.7
1/17/18
0.952 mg/lcg
EPA 200.7
1/17/18
20.0 mg/kg
EPA 200.7
1/17/18
1.0 mg/kg
EPA 200.7
1/17/18
_
-
1/15/18
1.0 -14.0 S.U.
SM 4500 H B
1/16/18
1 %
AOAC 955.01
I hereby certify that have reviewed and approve these data. 41,
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
#9

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
r
Contact: Neal Davis Report Date: 2/21/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 2/8/2018
Meritech Work Order # 020818149 Sample: Flyash Grab 2/8/18
Parameters Results Analysis Date Reporting Lirnit Method
% Total Solids
58.3 %
2/9/18
0-100 %
SM2540B
Arsenic, total
7.63 mg/kg
2/16/18
0.605 mg/kg
EPA 200.7
Barium, total
352 mg/kg
2/16/18
0.500 mg/kg
EPA 200.7
Chromium, total
11.8 mg/kg
2/16/18
0.100 mg/kg
EPA 200.7
Nickel, total
10.8 mg/kg
2/16/18
1.00 mg/kg
EPA 200.7
pH
8.6 S.U.
2/9/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that 1 have reviewed and approve these data. (�
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

59m=6 Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
Client. Kapstone Kraft Paper Corp Phone:_ 252-533-6295
Address:_ 10Q Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:_ [e-mail]
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: mail referred), Fax Mai Std(Soda s) 3-5 Days 124-48Hrs
ME R I T E C H INC.
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample Print:
� L �S
-
- LabfUse4Only} H_
:.
Start
End
Comp?
Grab?
#of
Cont.
Tests)
Required
Yes %"No
.,;.U`OK? '
Date
Time
Date
Time
12)
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor#
lug#
UPS
Fed Ex
Are these results or regulatory purposes? Yes No I
Report results in: mg/L mg/kg
ug/L
Hand Delivery
ry
Relinquished by: Time Chi
J �(J
Received by Date: Time:
Received b Y: - Date: Time:
Other
Relinquis b a Time:
� '
Relinquished b Date: Time:
Received b ' ,,a 7 �' Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Report Date:
3/21/2018
Client: Kapstone Paper
& Packaging NPDES#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd:
3/8/2018
Meritech Work Order #
030818150 Sample: Flyash Grab
3/8/18
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
56.3 % 3/9/18 0-100 %
SM2540B
Arsenic, total
6.31 mg/kg 3/15/18 0.605 mg/kg
EPA 200.7
Barium, total
300 mg/kg 3/15/18 0.500 mg/kg
EPA 200.7
Chromium, total
12.2 mg/kg 3/15/18 0.100 mg/kg
EPA 200.7
Nickel, total
13.9 mg/kg 3/15/18 1.00 mg/kg
EPA 200.7
pH
9.0 S.U. 3/9/18 1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data. �." &14�
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2026 Chain of Custody Record (COQ
NPDES#:_WQ0021577 & WQ0000436
Client; Kapstone Kraft Paper Corp Phone:_ 252-533-6295
Address:_ 100 Gaston Road Fax: — 252-533-6264
Roanoke Rapids, NC 27870 Email: Neal. [e-mail]
Project:
P.O.#:
Attention:_ Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply(Email preferred), Fax, Mail Std soda s) 3 - S Days 24-4sHrs
M E R IT E C H ' I N C.
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample ('gn/Pri t): Vz'/ ' ,
Lab Use Only.
Start
End
Comp? .
Grab?
#of
Cont.
Test(:s)
eq u i red
On Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
FLYASH
j
73�
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
'
Temperature, Upon
Receipt:
Method Of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN
samples
must be done in the field prior to preservation. ***
Comments:
lJug
Compositor#
#
Lk UPS
Fed Ex
Are these resWtsfol regulatory purposes? Yes No
Report results in: mg/L U mg/kg �J ug/L Ll
Hand Delivery
Relinquished b Da Time:
6 %�
Received by: D Time: o
�� '%s
Other
Relinq i d by: ate, Time: — /
S / uj
Received by: Date: Time:
Relinquishe y:' Date: Time:
Received by Lab: Date: Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
r
Report Date: 4/13/2018
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
NPDES#:
Project:
Date Sample Rcvd:
WQ0021577
WQ0000436
Monthly
4/5/2018
Meritech Work Order #
040518120 Sample: Flyash Grab
4/5/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
49.1 %
4/6/18
0-100 %
SM2540B
Ammonia, Nitrogen
<20.4 mg/kg
4/9/18
20.4 mg/kg
EPA 350.1
TKN
551.9 mg/kg
4/6/18
40.5 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
<20.4 mg/kg
4/6/18
20.4 mg/kg
EPA 353.2
Nitrogen, total
551.9 mg/kg
4/10/18
20 mg/kg
EPA 353.2
Aluminum, total
11,730 mg/kg
4/9/18
5.00 mg/kg
EPA 200.7
Arsenic, total
5.42 mg/kg
4/9/18
1.03 mg/kg
EPA 200.7
Barium, total
314 mg/kg
4/9/18
0.500 mg/kg
EPA 200.7
Cadmium, total
0.257 mg/kg
4/9/18
0.210 mg/kg
EPA 200.7
Calcium, total
11,380 mg/kg
4/9/18
10.0 mg/kg
EPA 200.7
Chromium, total
13.8 mg/kg
4/9/18
0.100 mg/kg
EPA 200.7
Copper, total
42.4 mg/kg
4/9/18
1.00 mg/kg
EPA 200.7
Lead, total
6.54 mg/kg
4/9/18
1.06 mg/kg
EPA 200.7
Magnesium, total
1270 mg/kg
4/9/18
10.0 mg/kg
EPA 200.7
Mercury, total
0.041 mg/kg
4/10/18
0.02 mg/kg
EPA 245.1
Molybdenum, total
<0.509 mg/kg
4/9/18
0.509 mg/kg
EPA 200.7
Nickel, total
15.6 mg/kg
4/9/18
1.00 mg/kg
EPA 200.7
Phosphorous, total
444 mg/kg
4/9/18
2.00 mg/kg
EPA 200.7
Potassium, total
4380 mg/kg
4/9/18
20.0 mg/kg
EPA 200.7
Selenium, total
<1.02 mg/kg
4/9/18
1.02 mg/kg
EPA 200.7
Sodium, total
1530 mg/kg
4/9/18
20.0 mg/kg
EPA 200.7
Zinc, total
14.5 mg/kg
4/9/18
1.0 mg/kg
EPA 200.7
SAR
IS4 -
4/9/18
-
-
pH
7.2 S.U.
4/6/18
1.0 -14.0 S.U.
SM 4500 H B
CCE
<1 %
4/6/18
1 %
AOAC 955.01
I hereby certify that I have. reviewed and approve these data. (G
&V
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

}2G-2013 Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ0021577
Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre '100 Gaston Road Fax: [phone]
Roanoke Rapids, NC. Email:_ Neal.Davis@Kapstonepaper.c
27870 Project:_ Monthly
P.O.#:
Attention: Neal Davis Turn around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all thatappl mail Epreferred), Fax, Mail stays)) 3-5 Da s �4-4gHrs
da s
ME R I T E C H INC. •
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
n
vvvv
W.mentech—labs.com
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample(Sign/Print): f i �1//�
Lab Use
Start
End
Comp?
Grab?
# of Cont.
Test(s) RequiredYes
on Ice?
/ No
pH OK?
Cl OK?
Date
Time
Date
Time
Flyash
�{�� Zola-
�(�
%TOTALSOLIDS, Ph, tJG
Metals: Al, Ar, Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,
Na,Ni, Se, Zn, Ptot, NH3, TKN, NO2, NO3
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
Temperature Upon
ece t
1 .
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and
TKN sam les must be done in the field priorto reservation. ***
Comments:
Compositor #
Jug #
[:j UPS
U , Fed Ex
Are these results for regulatory purposes? YeZ Q
Report results in: mg/L U mg/kg
FJ ug/L FJ
Hand Delivery
Relinquished by: )�Q` Date: /� Time: D
(/tJ
Received by ! at Tfine j O/
Other
Relinquished b
�^ G Date Tim / e:
700
Received b Date: Time:
RelifVruiishecl by: Date: Time:
Received b

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
i
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd:
5/21/2018
WQ0021577
WQ0O00436
5/10/2018
Meritech Work Order #
OS1018149 Sample: Flyash Grab
5/10/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
56.2 %
5/11/18
0-100 %
SM2540B
Arsenic, total
8.43 mg/kg
5/16/18
0.605 mg/kg
EPA 200.7
Barium, total
425 mg/kg
5/16/18
0.500 mg/kg
EPA 200.7
Chromium, total
13.3 mg/kg
5/16/18
0.100 mg/kg
EPA 200.7
Nickel, total
19.2 mg/kg
5/16/18
1.00 mg/kg
EPA 200.7
PH
8.3 S.U.
5/18/18
1.0 -14.0 S.U.
SM 4500 H B
K3
I hereby certify that 1 have reviewed and approve these data. �1'4vd
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5.9-2016
Chain of Custody Record (COC)
NPDES#:_ WQ 002lS77 & WQ 0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
Address:_ 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:_ Neal. [e-mail]
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like our report sent? *RUSH work needs prior approval.
Circle allthatapply: Email referred), Fax, Mail Std coda s) ads za
ME R I T E C H INC.
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW.f1'lerltechlabS.COt71
Sample Location and/or ID #
Sampling Dates & TimesPersonTakingSample(Sign/Prin
Lab Use Only
Start
_ End
Comp?
Grab?.
#of
Cont.
fe/st'(S') Required
On Ice?
Yes / No
pH.OK?
Cl OK?
Date
Time
Date
Time
FLYASH
�f' /
f%.'SO
Arsenic, Barium, Chromium, Nickel, pH, `
Total Solids
Temperature Upon . .
Receipt:
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol
and TKN samples must be done in the field prior to preservation.
Comments:
Compositor #
� __
Jug#-..=.._ _
UPS
ed Ex
Are these results fo' egulatory purposes? Yes
No I
Report results in: mg/L mg/kg IJ
ug/L a
Hand Delivery
-
Relinquished by: �a "/�� Time/ O
Received b Q
S, �t�/ (� Tme: /
1S
Other
Relinquish y: e` Tme:
V
J V
Receive - Date:
Date: Time:
Relinquished by: Date: Time:
Received ab: at / Y Time:
fJ
00

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Report Date:
6/18/2018
Client: Kapstone Paper
& Packaging NPDES#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd:
6/7/2018
Meritech Work Order #
060718135 Sample: Flyash Grab
6/7/18
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
41.5 % 6/8/18 0-100 %
SM2540B
Arsenic, total
13.9 mg/kg 6/13/18 0.605 mg/kg
EPA 200.7
Barium, total
547 mg/kg 6/13/18 0.500 mg/kg
EPA 200.7
Chromium, total
17.3 mg/kg 6/13/18 0.100 mg/kg
EPA 200.7
Nickel, total
24.6 mg/kg 6/13/18 1.00 mg/kg
EPA 200.7
pH
8.7 S.U. 6/8/18 1.0 -14.0 S.U.
SM 4500 H B
I hereby certify thatl have reviewed and approve these data. A " Mda " D(� lao 11
Labors ry Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
59.

5aza�6 Chain of Custody Record (COC)
NPDES#:_ WQ 0021577 & WQ 0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
Address: 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:_ Neal.Davis(cDKapstonepaper.cor
Project:
P.O.#:
Turn Around Time*
Attention:_ Neal Davis *RUSH work needs prior approval.
How would you like your report sent?
-48 Hrs
Circle all that appl Emai referred), Fax, Mail Std a s) 3-S Da s 24
M E R I T E C H I IV �, �
1
;.. ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
•
Person TakingSa /k ple (signint):
Lab Use Only
Start
End
Comp.
Grab?
#of
Cont.
Tests Required
1 `1
On Ice?
Yes/ No
pH OK?
ClCI OK.
Date
Time
Date
Time
FLYASH
,'3LO
A�_w
&
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
i
Temperature Upon
Receipt:
t V
Method of
Shipment:
*** Dechlorination (<0.S ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field priorto preservation. ***
Comments:
Compositor# '
lug#
UPS
Fed Ex
Are these results r regulatory purposes? Yes No
Report results in: mg/L mg/kg ug/L
Hand Delivery
Relinquished b te: Time: O
�� �S.
Received b / ate: Time: /O�O
G--
Other
Relinquish Gam_ 6 ate:7h,7 Time:/-gs,5
eceived y: Date: Time:
elinquished by: Date: Time:
Receiv a Dat 1 Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 071118165 Sample: Flyash Grab
Parameters Results Analysis Date
% Total Solids
Ammonia, Nitrogen
TKN
Nitrate/Nitrite Nitrogen
Nitrogen, total
Aluminum, total
Arsenic, total
Barium, total
Cadmium, total
Calcium, total
Chromium, total
Copper, total
Lead, total
Magnesium, total
Mercury, total
Molybdenum, total
Nickel, total
Phosphorous, total
Potassium, total
Selenium, total
Sodium, total
Zinc, total
SAR
pH
CCE*
50.1 %
<20.0 mg/kg
529 mg/kg
<20.0 mg/kg
529 mg/kg
11,520 mg/kg
11.2 mg/kg
477 mg/kg
0.758 mg/kg
9,060 mg/kg
16.1 mg/kg
36.9 mg/kg
10.7 mg/kg
1120 mg/kg
0.100 mg/kg
0.741 mg/kg
21.0 mg/kg
796 mg/kg
4130 mg/kg
<0.998 mg/kg
1400 mg/kg
32.1 mg/kg
2.62 -
7.8 S.U.
<1 %
* Results not for regulatory purposes
7/12/18
7/16/18
7/17/18
7/13/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/16/18
7/17/18
7/17/18
7/i7[18
7/17/18
7/17/18
7/17/18
7/17/18
7/17/18
7/16/18
7/18/18
Report Date:
7/24/2018
NPDES#:
WQ0021577
WQ0000436
Project:
Monthly
Date Sample Rcvd:
7/11/2018
Reporting Limit
0-100 %
20.0 mg/kg
40.5 mg/kg
20.0 mg/kg
20 mg/kg
5.00 mg/kg
0.581 mg/kg
0.500 mg/kg
0.116 mg/kg
10.0 mg/kg
0.100 mg/kg
1.00 mg/kg
1.06 mg/kg
10.0 mg/kg
0.012 mg/kg
0.290 mg/kg
1.00 mg/kg
2.00 mg/kg
20.0 mg/kg
0.998 mg/kg
20.0 mg/kg
1.0 mg/kg
1.0 -14.0 S.0
1%
7/11/18
Method
SM2540B
EPA 350.1
EPA 351.1
EPA 353.2
EPA 353.2
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
SM 4500 H B
AOAC 955.01
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
.11

3.213-2013 Chain of Custody Record (COC)
NPDES#: WQ0000436 & WQ00215h7
Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC. Email:_ Neal. Davis(@Kapstonepaper.ci
27870 Project:_ Monthly
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like _your report sent? *RUSH work needs prior approval,
Circle all that apply: mail 'referred), Fax, M II Stclda -5 Days �4r aBHis
M E R I T E C H, I IV C
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/. s
00�� 2 1"
Lab Use
Start
EndIce?
comp?
•#ofCont.
Tests)
Required
Yes / No
?
Cl OK?
Date
Time
Date
Time
Flyash
/i 1
1.�C�
%TOTAL SOLIDS, Ph,
Metals: AI,1Ar,;Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, Mg, Mo,
Na,Ni, Se, Zn, Ptot,'NH3, TKN, NO2, NO3
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
--F
Temperature Upon
Receipt:
,�}�_
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of
Ammonia, Cyanide,. Phenol and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor#
Jug #
UPS
Fed Ex
+
and Delivery
Other
Are these resu for regulatory purposes? Ye N
Relinquished by: Dax`` �3 Time:
// 3 'rrJ
Relinquishe / �at�� Time:
/
Report results in: mg/L mg/kg FJ ug/L
Received by a T
Received b : ✓/ J
Y Date: Time:
.Relinquished by: Date: Time:
Recei b Date:
� J
`

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date:
NPDES#:
Date Sample Rcvd:
8/20/2018
WQ0021577
WQ0000436
8/8/2018
Meritech Work Order #
080818107 Sample: Flyash Grab
8/8/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
58.4 %
8/9/18
0-100 %
SM2540B
Arsenic, total
11.3 mg/kg
8/13/18
0.605 mg/kg
EPA 200.7
Barium, total
649 mg/kg
8/13/18
0.500 mg/kg
EPA 200.7
Chromium, total
13.2 mg/kg
8/13/18
0.100 mg/kg
EPA 200.7
Nickel, total
12.8 mg/kg
8/13/18
1.00 mg/kg
EPA 200.7
pH
8.2 S.U.
8/12/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data. nA(IL
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016 Chain of Custody Record (COC)
NPDES#:_WQ0021577 & WQ0000436
Client; Kapstone� Kraft Paper Corp =•. Phone:_ 252-533-6295
100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:_ Neal.Davis(@Kapstonepaper.co
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Ema" (preferred) , Fax Mail Std to days) 3 - s Des 24-48 Hr5
M E R I T E C H INC.* �
1Address:_
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
6"i
Email: [e-mail]
www.meritechlabs-.com
Sample Location and/or ID #
Sampling Dates & Times
Person.TakingSa gn/ rin .
Lab Use Only
Start
End
,
Comp.
Grab?
#of
Co7nt.
Tests)
Required
on Ice?
Yes" / No'
pH OK?
.'Cl-OK?
Date
Time
Date
Time
Flyash
�$
T03
/
Arsenic, Barium, Chromium, Nickel, pH, 0
Total Solids
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN
samples must be done in the -field prior to preservation. ***
Comments:
Compositor #
Jug #-
UPS
Fed Ex
Are these results f regulatory purposes? Yes 1.T No rJ
Report results in: mg/L mg/kg ug/L a
Hand Delivery
Ti
Relinquished by: a me: �j
i
me: 2 -7
Received by: � 0p -rime:
� J )
Other
Relinquish by: Time: © _�
Received by: Date: Time.
Relinquished ! Date: Time:
Recei y Tim

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Report Date: 9/24/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 9/13/2018
Meritech Work Order #
091318100
Sample: Flyash Grab
9/13/18
Parameters
Results
Analysis Date Reporting Limit
Method
% Total Solids
46.8 %
9/1/18
0-100 %
SM2540B
Arsenic, total
4.96 mg/kg
9/19/18
0.605 mg/kg
EPA 200.7
Barium, total
449 mg/kg
9/19/18
0.500 mg/kg
EPA 200.7
Chromium, total
20.4 mg/kg
9/19/18
0.100 mg/kg
EPA 200.7
Nickel, total
23.9 mg/kg
9/19/18
1.00 mg/kg
EPA 200.7
PH
8.8 S.U.
9/14/18
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that have reviewed and approve these data. AMUCS
Laboratory epresentative
f
642 Tawco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016 Chain of Custody Record (COC)
NPDES#:_ WQ.0021577 & WQ 0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email:. [e-mail]_r
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your -report sent? *RUSH work needs prior approval.
Circle all that apply: mail% preferred) , Fax, 40 Std 10 da s) 3 - s Des 24
M E R I T E C H INC.
1Address:_
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Pr• y
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
t6st(s) Required
On Ice?
Yes /. No
pH OK?
CI OK?
Date
Time
Date
Time
FLYASH
g /,�
�'(�Yj
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
Temperature Upon
Receipt: j
Method Of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation.
Comments:
lJug
Compositor #
Q UPS
#
Fed Ex
Are these results for ffgulatory purposes? Yes No FJ
Report results in: mg/L - mg/kg
ug/L
Hand Delivery
Relinquished by: /
a/3 /� Time:
Received by atp:� Time: C
S Other
Relinquished Time:
Receive , by: Dat((e: Time:
Relinquished by: Date: ' Time:
Received by L �a y Time )�

Meritech, Inc.
Environmental Laboratory
t
Laboratory Certification No.165
Report Date:
Contact: Neal Davis NPDES#: WQ0021577
Client: Kapstone Paper & Packaging WQ0000436
100 Gaston Rd. Project: Monthly
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 100418114 Sample: Flyash Grab 10/4/18
Parameters Results Analysis Date Analyst Reporting Limit Method
% Total Solids
11.7 %
10/5/18
BF
0-100 %
SM2540B
Ammonia, Nitrogen
<85.5 mg/kg
10/5/18
NW
85.5 mg/kg
EPA 350.1
TKN
161 mg/kg
10/11/18
NW
40.5 mg/kg
EPA 351.1
Nitrate/Nitrite Nitrogen
<85.5 mg/kg
10/5/18
NW
85.5 mg/kg
EPA 353.2
Nitrogen, total
161 mg/kg
10/15/18
NW
20 mg/kg
EPA 353.2
Aluminum, total
41,200 mg/kg
10/11/18
ED
5.00 mg/kg
EPA 200.7
Arsenic, total
31.5 mg/kg
10/11/18
ED
0.581 mg/kg
EPA 200.7
Barium, total
1770 mg/kg
10/11/18
ED
0.500 mg/kg
EPA 200.7
Cadmium, total
1.41 mg/kg
10/11/18
ED
0.116 mg/kg
EPA 200.7
Calcium, total'
59,400 ing/kg
10/11/18
ED
10.O'mg/kg
EPA 200.7
Chromium, total
91.5 mg/kg
10/11/18
ED
0.100 mg/kg
EPA 200.7
Copper, total
256 mg/kg
10/11/18
ED
1.00 mg/kg
EPA 200.7
Lead, total
66.9 mg/kg
10/11/18
ED
1.06 mg/kg
EPA 200.7
Magnesium, total
9200 mg/kg
10/11/18
ED
10.0 mg/kg
EPA 200.7
Mercury, total
0.171- mg/kg
10/9/18
MR
0.012 mg/kg
EPA 245.1
Molybdenum, total
2.44 mg/kg
10/11/18
ED
0.290 mg/kg
EPA 200.7
Nickel, total
105 mg/kg
10/11/18
ED
1.00 mg/kg
EPA 200.7
Phosphorous, total
5840 mg/kg
10/11/18
ED
2.00 mg/kg
EPA 200.7
Potassium, total
23300 mg/kg
10/11/18
ED
20.0 mg/kg
EPA 200.7
Selenium, total
<4.27 mg/kg
10/11/18
ED
4.27 mg/kg
EPA 200.7
Sodium, total
8900 mg/kg
10/11/18
ED
20.0 mg/kg
EPA 200.7
Zinc, total
226 mg/kg
10/11/18
ED
1.0 mg/kg
EPA 200.7
SAR
3.07 -
10/11/18
ED
-
-
pH
8.9 S.U.
10/5/18
BF
1.0 - 14.0 S.U.
SM 4500 H B
CCE*
<1.0 %
10/22/18
LH
1 %
AOAC 955.01
* Results not for regulatory purposes
I hereby certify that I have reviewed and approve these data.
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
67

-20-2013 Chain of Custody Record (COC) NPDES#: WQ0000436 &
ME R I TE C H, ' N C Client: Kapstone Kraft Paper Corp. Phone:_ 252-533-6295
Addre 100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES Roanoke Rapids, NC. Email:_ Neal.DavisOKa
642 Tamco Rd. Phone: [phone]
woo 27870 Project:_ Monthly
Reidsville NC 27320 Fax: [phone] P.O.#:_
Email: [e-mail] Attention: Neal Davis
-www. meritech-labs, COm How would you like your report sent?
Circle all that apply: �a' preferred) , Fax, ail
Sampling Dates & Times Person Taking Sample (Si nt):
Sample Location and/or ID #
Start End comp?
Date I Time Date Time Grab? #of Cont. Tests) Required
FLYASH 700 �v / %TOTAL SOLIDS, Ph,
-77 Metals: Al, Ar, Ba, Cd, Ca, Cr,Cu,Hg, K, Pb, M
Na,Ni, Se, Zn, Ptot, NH3, TKN, NO2, NO3
Method of *** Dechlorination
Comments:
UPS
F Ex Are these results f
Hand Delivery Relinquished by:
Other Relinqulshedbb'
/
Relinquished by:
5 ppm) of Ammonia, C
2gulatory purposes?
Da
Date:
Phenol and TKN
Time:
Time:
Time:
P-A-N (by Calculation)
C-C-E (by Calculation)
Sodium Adsorption Ratio (by Calculation
must be done in the field prior to
Received by:
ort results in: mg/L
Turn Around Time
*RUSH work needs prior a 3proval.
std(10 3-5 Days -48Hrs
days)
Lablise.
On Ice? . H"OK?
Yes / No 1 OK?
Jug #
mg/kg Q1 ug/L
Time:
Upon
00

Meritech, Inc.
Environmental Laboratory
a
Laboratory Certification No.165
Contact: Neal Davis Report Date: 11/20/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 11/8/2018
Meritech Work Order # 110818109 Sample: Flyash Grab 11/8/18
Parameters Results Analysis Date Analyst Reporting Limit Method
% Total Solids
30.6 %
11/12/18
JM
0-100 %
SM2540B
Arsenic, total
7.35 mg/kg
11/14/18
ED
0.605 mg/kg
EPA 200.7
Barium, total
618 mg/kg
11/14/18
ED
0.500 mg/kg
EPA 200.7
Chromium, total
22.8 mg/kg
11/14/18
ED
0.100 mg/kg
EPA 200.7
Nickel, total
30.9 mg/kg
11/14/18
ED
1.00 mg/kg
EPA 200.7
pH
9.0 S.U.
11/12/18
JM
1.0 - 14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data.
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

5-9-2016 - ' Chain of Custody Record (COC)
NPDES#:_
WQ 0021577 & WQ0000436
M E R ITE C H, INC.
Client: Kapstone Kraft Paper Corp
Phone:_
252-533-6295
Address:_ 100 Gaston Road
Fax:
252-533-6264
ENVIRONMENTAL LABORATORIES
Roanoke Rapids; NC 27870
Email:
Neal. Davis@ Ka pstonepaper.cor
642Tamco Rd. Phone: [phone]
Project:
`
t Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Neal Davis
Turn AroundTlme*
`A `A `A
�/,/V1/VI/.meritechlabs.COm
Sampling Dates & Times
Sample Location and/or ID # Start End
Date Time Date Time
How would you like your -report sent? *RUSH work needs prior approval.
Circle all that apply: Email referred), Fax, Ma' Std loda s) 3-5 Da s 24-48Hrs
ampTaking Sample ri ��
' z�! ems' Lab Use Only
Comp?
Drab?
4,0
. # of
Cont.
/
'
Test(s) Required
Arsenic, Barium Chromium Nickel pH
On Ice?
Yes / No
pH OK?_.
:CI OIC?
FLYASH
/V /
71$(3
Method of
*** Dec
Comments:
UPS
Fed Ex
Are these
and Delivery
Relinquished b
Other
RelinquishB y: As
(Relinquished by:
0
<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN
regulatory purposes? Yes No
jF Time: 0 / /.
DD Timeills-
Date: Time:
Total Solids I O
must be done in the field prior to
Received by:
ort results in: mg/L
Temperature. Upon
Receipt:
Compositor #
Jug #
mg/kg IJ ug/L
Date: Tim O
Date: Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 12061892
Parameters Results
% Total Solids
Arsenic, total
Barium, total
Chromium, total
Nickel, total
pH
Sample: Flyash Grab
Analysis Date
46.0 %
12/18/18
<10.9 mg/kg
12/14/18
526 mg/kg
12/14/18
30.2 mg/kg
12/14/18
35.7 mg/kg
12/14/18
9.0 S.U.
12/18/18
Report Date: 12/20/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 12/6/2018
12/6/18
Reporting Limit
Method
0-100 %
SM2540B
10.9 mg/kg
EPA 200.7
0.500 mg/kg
EPA 200.7
0.100 mg/kg
EPA 200.7
1.00 mg/kg
EPA 200.7
1.0 -14.0 S.U.
SM 4500 H B
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
"1

5e��6 Chain of Custody Record (COC)
NPDES#:_WQ0021577 &'WQ0000436
Client: Kapstone Kraft Paper Corp Phone:_252-533-6295
Address: 100 Gaston Road Fax: [phone]
Roanoke Rapids, NC 27870 Email: [e-mail]
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Emai referred), Fax, al Stcl 10da 5) 3 24-48H.
- M E R I.T E C H I � �, �
1
ENVIRONMENTAL LABORATORIES
642Tamco.Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates & Times�S
Person Taking 5a le (Si P/int)-
Lab Use Only -
Start
End
Comp?
Grab?
#of
Cont.
Test(s)
Required
On
Orilce?•
No
pHOK?:
Cl OK?
Date
Time
Date
Time
FLYASH
Arsenic, Barium, Chromium, Nickel, pH,
Total Solids
Temperature. Upon
Receipt:-,
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and T-KN samples
must be done in the field prior to preservation. ***
Comments:
Cpositor•#-
_ om.-
Jug #
UPS
Fed Ex
Are these results for purposes? Yes No
Report results in: mg/c U mg/kg
ug/L Ll
Hand Delivery
Other
Relinquished by: / a Time q
3 V
Relinquished a Tim�:/
�. Z
Received by: te: Time:
-- O
Received b Y' ' Date: Time:
Relinquished by: Date: Time:
Receive y Lab: at . Time:
N v//

TCLP
F/ yash Residuals

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 100418115 Sample: Flyash Grab
1311- TCLP Metals
Page 1
Report Date:
10/25/2018
NPDES#:
WQ0021577
WQ0000436
Project:
Monthly
Date Sample Rcvd:
10/4/2018
10/4/2018
Parameter
Results
Anal, sY is Date
Analyst
Det. Limit
Reg. Limit
Method
Arsenic
<0.100 mg/L
10/15/2018
l ED
0.100
5.0
EPA 200.7
Barium
1.130 mg/L
10/15/2018
ED
0.050
100.0
EPA 200.7
Cadmium
<0.020 mg/L
10/15/2018
ED
0.020
1.0
EPA 200.7
Chromium
<0.050 mg/L
10/15/2018
ED
0.050
5.0
EPA 200.7
Lead
<0.100 mg/L
10/15/2018
ED
0.100
5.0
EPA 200.7
Mercury
<0.02 mg/L
10/13/2018
MR
0.02
0.2
EPA 245.1
Selenium
<0.100 mg/L
10/15/2018
ED
0.100
' 1.0
EPA 200.7
Silver
<0.050 mg/L
10/15/2018
ED
0.050
5.0
EPA 200.7
TCLP Organics
Parameter
Results
Analysis Date
Analyst Reporting Limit
Method
Volatiles 8260
Attached
10/15/2018
VV -
8260
Semi Vol. 8270
Attached
10/23/2018
PM -
8270
Other Tests
Parameter Results Analysis Date Analyst Reporting Limit Method
Cyanide, total
<0.500 mg/kg
10/10/2018 LH 0.500 mg/kg EPA 335.4
Sulfide
<10.0 mg/kg
10/8/2018 LH 10 mg/kg SW 846 9038
Ignitability
Will Not Ignite
10/22/2018 LH - EPA 1030
Corrositivity (pH)
8.9 S.U.
10/5/2018 BF 1.0 - 14.0 S.U. SM 4500 HB
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Report Date: 10/25/2018
Contact: Neal Davis NPDES#: WQ0021577
Client: Kapstone Paper & Packaging WQ0000436
100 Gaston Rd. Project: Monthly
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 100418115 Sample: Flyash Grab 10/4/2018
1311 - TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Parameter
Results
Analysis Date
Analyst
Det. Limit
Reg. Limit imit
Dilution Factor
Endrin
<0.002 mg/L
10/22-23/18
MG
0.002
0.02
1
Chlordane
<0.003 mg/L
10/22-23/18
MG
0.003
0.03
1
Toxaphene
<0.05 mg/L
10/22-23/18
MG
0.05
0.5
1
Methoxychlor
<1.00 mg/L
10/22-23/18
MG
1.00
10.0
1
Heptachlor
<0.0008 mg/L
10/22-23/18
MG
0.0008
0.008
1 •
Lindane
<0.040 mg/L
10/22-23/18
MG
0.040
0.4
1
Herbicides - SW-846 8151A
Parameter
Results
Analysis Date
Analyst
Det. Limit
Reg. Limit
Dilution Factor
2,4-D
<1.00 mg/L
10/22-23/18
MG
1.00
10.0
1
2,4,5-TP (Silvex)
<0.100 mg/L
10/22-23/18
MG
0.100
1.0
1
I hereby certify that I have reviewed and approve these data. (�
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
Environmental Laboratories
i
Laboratory Certificate #165
Client:
Kapstone Kraft Paper Corp.
Project:
Monthly
Client Sample ID:
Flyash
Sample Collection:
10/04/18
Meritech Sample ID:
100418115
1311 - TCLP Oraanics
Volatiles: SW-846 8260
Analysis: 10/15/18
Extraction:
10/08/18
Analyst: VWV
Report Date:
10/19/18
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
0.50
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
0.50
10
Chlorobenzene
< 0.0100
mg/L
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroethane
< 0.0100
mg/L
0.0100
0.50
10
1, 1 -Dichloroethene
<0.0100
mg/L
0.0100
0.70
10
Methyl Ethyl Ketone.
<0.100
mg/L
0.100
200
10
Tetrachloroethylene
< 0.0100
mg/L
0.0100
0.70
10
Trichloroethene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
Analysis: 10/23/18
Extraction:
10/08/18
Analyst: PM
Report Date:
10/23/18
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
1,4-Dichlorobenzene
<0.100
mg/L
0.100
7.5
10
Hexachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
Hexachloroethane
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
m&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
10
Pentachlorophenol
<0.500
mg/L
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5-Trichlorophenol
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenol
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby certify that I have reviewed and approve these data.
t�.
LU. / ,
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] * [e-mail]
75

3-7D-2M - Chain of Custody Record (COC) -
NPDES#i- WQ0000436 & WQOC 21577
M E R ITE C H, I I V CClient: Kapstorie Kraft Paper Corp. Phone:_ 252-533-6295
Add're 100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES Roanoke Rapids, NC.. Email:_ Neal.DavisCuDI(apstonE paper.c
642 Tamco Rd. Phone: [phone]
- Project:_ Monthly I
Reidsville- NC27320 Fax:[phone]-
P.O.#:
Email: [e-mail] Attention: Neal Davis Turn Around Time
`A n �/ ,� , How would you. like your report sent? *RUS ork needs prior a proval.
�/V w-meritech-Iabs.com Circle all that apply. Email referred), Fax, Std(10 3-5 Da s z =asHrs
Sampling Dates &. Times Person Taking•Sampl (Sign/P ' days
Sample Location and/or ID #�-
Start End comp?
Date Time Date Time Grab? • # of cost.
Test Required.
a
IGN•ITABILITY, REACTIVITY,CORROSIVITy
TCLP TO INCLUDE: _ I
:;Arsenic (5.0)2 1,4-D .icl lorobenzene -
(7..5) N;itrolienene;//2�0=
Barium 10010. -`
( ) 1,2 Dichloroetliane (0.5) P.entaolilorohenol.(j. , 0:0) .
•Benzene 0.5 -
�. . ). 1,1-Dichloroethylene. (0.7) Pyridine:(5.0).
'Cadmium.(1.0) 2,4--Dinitrotoluene (0.13) Selenium (1.0)
Carbon tetrachloride. 0.5
( ) Endrin (002) - Salver,(5:0)
Chloidarie 0.03 Tetrachloroethylene_( .7)
I3exachlorobebzene-(0:1..::; _
n ) "..
Chlorobenzene (100.0) Heptachlor (andril?saiydroxide)
0:0*08) Toxaphene ..(0.5) ,
Chloroform y <�; , n
(60) Hexachloio-]3-butaclierier(0.5) .•:Trichloroethyene (0,)
MethodOf *** Dechlorination (<0.5 ppm) of Ammonia, Chromium -5:0
(,.) Hexachloroetliane (3.0) • 2,4,-5�Trich1prophen61-(. 0.0)
Shipment: Comments: m-Cresol..(20D;0)'2,46=TYiehloroplienoh .0)
UPS 0-Cresol (200:0) Lindane r0
,4)
Fed Ex Are these.re is for regulatory piCresol (200.0) Me'rc _ 0;2 .; , g ry purpose. _. ; ury,( ...) . Vinyl chlgride'.(0.2
Hand Delivery Relinquistie /Y 'Cresol (200.0) . Methoxj'chlor.:(10.0)
Other Relinquish by: Date: 2,4-D�-(10:0) Methyl ethyl ketone (200:0)
Relinquished by: Date: •rime• _
�L. Rece ab: � ��

Form PVRF 02T
Fl yash Residuals
Annual Pathogen Reduction Form

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Kapstone Kraft Paper Corporation WQ Permit Number:
WWTP Name: Roanoke Rapids Mill NPDES Number:
Monitoring Period: From 1/1/2018 To 10/31/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative
Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testi
A1t.D (No Prior Test) ❑ 1 Process to Further Reduce Pathog
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogen
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophi]
Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑
Class B: JAR. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogen,
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Path
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic I
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class_ B) complete the following monitoriiI
Allowable Level Pathogen Density Number of Frequency
Parameter Excee- q y
in Sludge Minimum Geo. Mean Maximud Units dences of Analysis
2 x 10 to the MPN
6th power
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry < 162 190.97 380 col/g dry 0 QTR.
Weight)
Salmonella bacterial 3 MPN per 4 grams
(in lieu of fecal total solid (dry
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative nPrfnrmPr1-
WQ0000436
NC 0000752 FA
)erformed:
19) p
ngs ❑
»;
c ❑
gens":
igestion ❑
data:
Sample Analytic:
Tech -
Type I n;m—
Fecal ism9222D
Alt. 1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑+Alt.
4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) • ❑
No vector attraction reduction alternatives were performed 0
%-jv lc i it ll.ti t iur4 a i a i r.lvil r4 i kpiease cnecx the appropriate statement)
❑ - "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ . "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Neal R. Davis Environmental Engineer
Preparer Name an Title (ry or print)
Signature f Preparer* Date
None Distributed in 2018
Land Applier Name
and Title (if applicable)(type or print)
Gy/� I
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006) 77

Meritech, Inc.
Environmental Laboratory
t
Laboratory Certification No. 165
Contact: Neal Davis
Report Date:
Page 1
4/16/2018
Client: Kapstone Paper
& Packaging NPDES#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd:
4/5/2018
Meritech Work Order #
04051897 Sample: Flyash-4-1 Grab
4/5/18
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
49.3 % 4/6/18 0-100 %
SM 2540B
Fecal Coliform
<183 col/ g dry 4/5/18 183 col/ g dry
SM 9222 D
Meritech Work Order #
04051898 Sample: Flyash-4-2 Grab
4/5/18
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
49.7 % 4/6/18 0-100 %
SM 2540B
Fecal Coliform
183 col/ g dry 4/5/18 162 col/ g dry
SM 9222 D
Meritech Work Order #
040SI899 Sample: Flyash-4-3 Grab
4/5/18
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
47.0 % 4/6/18 0-100 %
SM 2540B
Fecal Coliform
<193 col/ g dry 4/5/18 193 col/ g dry
SM 9222 D
Meritech Work Order #
040518100 Sample: Flyash-4-4 Grab
.N�
4/5/18
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
49.7 % 4/6/18 0-100 %
SM 2540B
Fecal Coliform
<183 col/ g dry 4/5/18 183 col/ g dry
SM 9222 D
Meritech Work Order #
040518101 Sample: Flyash-4-5 Grab
4/5/18
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
51.6 % 4/6/18 0-100 %
SM 2540B
Fecal Coliform
<176 col/ g dry 4/5/18 176 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
78

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
a
Page 2
Contact: Neal Davis Report Date: 4/16/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ00004,36
Roanoke Rapids, NC 27870 Date Sample Rcvd: 4/5/2018
Meritech Work Order # 040518102 Sample: Flyash-4-6 Grab 4/5/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 49.7 % 4/6/18 0-100 % SM 254013
Fecal Coliform <183 col/ g dry 4/5/18 183 col/ g dry SM 9222 D
Meritech Work Order # 040518103 Sample: Flyash-4-7 Grab 4/5/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
50.5 %
4/6/18
0-100 %
SM 2540B
Fecal Coliform
<180 col/ g dry
4/5/18
180 col/ g dry
SM 9222 D
I hereby certify that have reviewed and approve these data. 1,
4a
Laboratory Representative
4
642 Tamco Road, Reidsv,* North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
NPDES#: WQ 0021577 & WQ 0000436
Client; Kapstone Kraft Paper Corp Phone:_ 252-533-6295
Address:_ 100 Gaston Road Fax: — 252-533-6264
Roanoke Rapids, NC 27870 Email: Neal. [e-mail]
Project:
P.O.#:
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email referred), Fax, Mail Std loda s) 35 IDs 24-48
t
M E R I T E C H INC.
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
WWW.meritech(abs.Com
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample (Sign/Print
lf�( �,,,•��- �
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
Test(s) Required
On Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
FLYASH FA-4-1A
S�ZCiia
-30
CLASS A FECAL COLIFORM ANALYSIS
FLYASH FA-4-2A
= 3
(T
CLASS A FECAL COLIFORM ANALYSIS b
FLYASH FA-4-3A
= t(D
(T
r
'CLASS A FECAL COLIFORM ANALYSIS
FLYASH FA-4-4A
CLASS A FECAL COLIFORM ANALYSIS I� U
FLYASH FA-4-5A
'57
Cj-
CLASS A FECAL COLIFORM ANALYSIS
FLYASH FA4-6A
i?D
(
CLASS A FECAL COLIFORM ANALYSIS ill
FLYASH FA-4-7A
)ZS'
(
CLASS A FECAL COLIFORM ANALYSIS k U3
Temperature Upon
Receipt: �✓
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation.
Comments:
Compositor #
UPS
Jug #
Fed Ex
Are these results for regulatory purposes? Yes No I
Report results in: mg/L [_—) mg/kg U
ug/L U
Hand Delivery/
Relinquished by ,,A �l Date: ` /Time:
r L.K Cam--- /
Receivedb : �' Dat . —/ Time: b/
Other
Relinquished b Date/ Time: O O
Received by� Date: Time:
Rel quished by: Date: Time:
Receive b b: D te: Time;, i
pp
O

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Neal Davis Report Date: 1/22/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 1/11/2018
Meritech Work Order # 011118115 Sample: FA 1-1-18 Grab 1/11/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 52.4 % 1/12/18 0-100 % SM 2540B
Fecal Coliform <173 col/ g dry 1/11/18 173 col/ g dry SM 9222 D
Meritech Work Order # 011118116 Sample: FA 1-2-18 Grab
Parameters
Results
Analysis Date
Reporting Limi
Method
% Total Solids
56.0 %
1/12/18
0-100 %
SM 2540B
Fecal Coliform
<162 col/ g dry
1/11/18
162 col/ g dry
SM 9222 D
Meritech Work Order #
011118117 Sample: FA 1-3-18 Grab
1/11/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
52.2 %
1/12/18
0-100 %
SM 2540B
Fecal Coliform
<174 col/ g dry
1/11/18
174 col/ g dry
SM 9222 D
Meritech Work Order # 011118118 Sample: FA 1-4-18 Grab
Parameters Results Analysis Date
% Total Solids
Fecal Coliform
51.5 % 1/12/18
<177 col/ g dry 1/11/18
Meritech Work Order # 011118119 Sample: FA 1-5-18 Grab
Parameters Results Analysis Date
% Total Solids
Fecal Coliform
51.7 % 1/12/18
<176 col/ g dry 1/11/18
1/11/18
Reporting Limit Method
0-100 % SM 2540B
177 col/ g dry SM 9222 D
1/11/18
Reporting ht:mt Method
0-100 % SM 2540B
176 col/ g dry SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
81

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech Work Order # 011118120 Sample: FA 1-6-18 Grab
Parameters
Results Analysis Date
Page 2
Report Date: 1/22/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 1/11/2018
Reporting Limit Method
% Total Solids 46.5 % 1/12/18 0-100 % SM 2540B
Fecal Coliform <196 col/ g dry 1/11/16 196 cal/ g dry SM 9222 D
Meritech Work Order # 011118121 Sample: FA1-7-18 Grab 1/11/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
51.2 %
1/12/18
0-100 %
SM 2540B
Fecal Coliform
<178 col/ g dry
1/11/18
178 col/ g dry
SM 9222 D.
I hereby certify that 1' have reviewed and approve these data. 6. JVX6�1
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
82

Chain of Custody Record (COQ
NPDES#:—
Client: Kapkone Kraft Paper. Corp Phone:—
Address:— 100 Gaston Road Fax:
Roanoke Rapids, NC 27870 Email:
Project:
P.O.#:
Attention: Neal Davis
How would you like your report sent?
Circle all that apply: referred), Fax, 4011
WQ 0021577 & WQ 0000436
252-533-6295
252-533-6264
Neal. Davis 0Ka pstonepa per:coi
Turn Around'rime*
*RUSH work needs prior approval.
y"49 Hrs
Std.JLQ das) 3-5 ,a 24 E: :
MERITECH INC@
ENVIRONMENTAL LABORATORIES
. N 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechiabs.com
Sample Location and/or ID #
Sampling Dates & Times.via
Person Taking Sample (Si nt):
Lab: Use OnlyV
Start
End
comp?
Grab?
#of
Cont.'v/Test(s)
Required
-ofi. ice?
"Yes: Yes:/.No
pH -OK?
Cl OK?
Date
Time
Date
Time
FLYASH FAI-1-18
All A
[K
0
1
CLASS A FECAL COLIFORM ANALYSIS
FAI-2-18, -
TZ5
I
)
CLASS A FECAL COLIFORM ANALYSIS
FAI-3-18
T3 D
CLASS A FECAL COLIFORM ANALYSIS
FAI-4-18
7!2:5.
CLASS A FECAL COLIFORM ANALYSIS
FAI-5-18
7" �
CLASS A FECAL COLIFORM ANALYSIS
FAI-6-18
7'11�
CLASS A FECAL COLIFORM ANALYSIS
FAI-7-18
CLASS A FECAL COLIFORM ANALYSIS
Temperature Upon -
Receipt.:,: j ok
Method of
Shipment:
Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation.
Comments:
ljui.#
Co!ppcis.ito.r.#.
ED UPS
(Zk F*Ex
Are these results r regulatory purposes? Yes 1:2(' No
Report results in: Mg/L [:J mg/kg J ug/L (a
Wand Delivery
Relinquished by: Datir Time: It. OK
Received L ffet Time: 0 .29
Other
Relinq Time:
DfIL
Received oe�' Date: Time:
�2 a
4 1
Relinquished by�te: Time:
Recelvek*6b-../' atef, t., -- . yTime:
00
UJ

.
Meritech, Inc.
Environmental Laboratory
-
Laboratory Certification No.
165
Contact: Neal Davis
Date:
Page 1Report
7/19/2018
Client: Kapstone Paper &Packaging
NPDES#:
WQ0021577
100 Gaston Rd.
WQ0000436
Roanoke Rapids, NC 27870
Date Sample Rcvd:
7/11/2018
Meritech Work Order #
071118149 Sample: Flyash 7-18 Grab
7/11/18
Parame1Mfigw
s AnalysiN Date _
Reporting Limit
Method
% Total Solids
51.4 % 7/11/18
0-100 %
SM 2540B
Fecal Coliform
<177 col/ g dry 7/11/18
177 col/ g dry
SM 9222 D
Meritech Work Order #
071118150 Sample: Flyash 7-18 Grab
7/11/18
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
49.8 % 7/11/18
0400 %
SM 2540B
Fecal Coliform
<183 col/ g dry 7/11/18
183 col/ g dry
SM 9222 D
Meritech Work Order #
071118151 Sample: Flyash 7-18 Grab
7/11/18
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
49.9 % 7/11/18
0-100 %
SM 2540B
Fecal Coliform
<182 col/ g dry 7/11/18
182 col/ g dry
SM 9222 D
Meritech Work Order #
071118152 Sample: Flyash 7-18 Grab
7/11/18
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
47.3 % 7/11/18
0-100 %
SM 2540B
Fecal Coliform
<192 col/ g dry 7/11/18
192 col/ g dry
SM 9222 D
Meritech WorkOrder #
071118153 Sample: Flyash 7-18 Grab
7/11/18
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
48.4 %
7/11/18
0-100 %
SM 2540B
Fecal Coliform
<188 col/ g dry
7/11/18
188 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
84

ti +
contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Meritech Work Order # 071118154 Sample: Flyash 7-18 Grab
Parameters Results Analysis Date
% Total Solids 47.4 % 7/11/18
Fecal Coliform <192 col/ g dry 7/11/18
Meritech Work Order # 071118155 Sample: Flyash 7-18 Grab
Parameters Results Analysis Date
% Total Solids 46.0 % 7/11/18
Fecal Coliform <198 col/ g dry 7/11/18
Page 2
Report Date: 7/19/2018
NPDES#: WQ0021577
WQ0000436
Date Sample Rcvd: 7/11/2018
7/11/18
Reporting Limit Method
0-100 % SM 254013
192 col/ g dry SM 9222 D
7/11/18
Reporting Limit Method
0-100 % SM 254013
198 col/ g dry SM 9222 D
I hereby certify that have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

sA6 Chain of Custody. Record (COC) ,
NPDES#: WQ0021577 & WQ0000436
Kapstone Kraft Paper Corp Phone:_ 252-533-6295
M E R ITE C H IINC.Client:
1Address:_
100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABORATORIES
Roanoke Rapids, NC 27870 Email:_ [e-mail]
b 642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC27320 Fax: 336L342-1522
P.O.#:
Email: [e-mail]
Attention: Neal Davis Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
www.meritechiabs.com
Std soda s) 3-5 Da s 24-48Hrs
Circle all that apply: Email (preferred), Fax, Mail
Sampling Dales &Times
Person Taking Sample (Sign/Print):
�
l.ab'Use Only
Sample Location and/or ID #
Start
End
Comp?
#of
Test(s)
Required
On Ice?
pIi OK?
Date
Time
Date
Time
Grab?
Cont.
Yes /. No:
Cl OK?
1 FLYASH 7-18
l j
!SO
,
CLASS A FECAL COLIFORM ANALYSIS
2 FLYASH 7-18
�l's�
CLASS A FECAL COLIFORM ANALYSIS l Sri
3 FLYASH 7-18
q"00
CLASS A FECAL COLIFORM ANALYSIS. 5
4 FLYASH 7-18
CLASS A FECAL COLIFORM ANALYSIS t
5 FLYASH 7-18
; Jb
CLASS A FECAL COLIFORM ANALYSIS k S
6 FLYASH 7-18
I
; J
CLASS A FECAL COLIFORM ANALYSIS
-
7 FLYASH 7-18
;ZO
CLASS A FECAL COLIFORM ANALYSIS �S
Temperature Upon
Receipt: V
-
Method of
*** Dechlorination
(<0.5 ppm) of AM, nonia, Cyanide, Phenol and TKN
samples must be done in the field prior to preservation.***
Comments:
Compositor#
Jug #
Shipment:
UPS
Fed Ex
Are these results for egulatory purboses? Yes U No Q.
Report results in: mg/L U mg/kg [J
ug/L
Me
and Delivery
Relinquished by: f . a e Time:
( / / 10 5
Received by: ,o at : Time . —
_ /D �,QS
Other
Relinquish Da T
Receive Y: Date: Time:
Relinquished by: Date: Time:
Recei y La j�atk: - Time:
Iji(( 1

Meritech, Inc.
Environmental Laboratory
Ai -
Page Laboratory Certification No.165
1
Contact: Neal Davis Report Date: 10/12/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 100418105 Sample: Flyash A 10-18 Grab 10/4/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.2 % 10/5/18 0-100 % SM 2540B
Fecal Coliform <201 col/ g dry 10/4/18 201 col/ g dry SM 9222 D
Meritech Work Order # 100418106 Sample: Flyash B 10-18 Grab 10/4/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.9 % 10/5/18 0-100 % SM 2540B
Fecal Coliform <198 col/ g dry 10/4/18 198 col/ g dry SM 9222 D
Meritech Work Order # 100418107 Sample: Flyash C 10-18 Grab 10/4/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 45.2 % 10/5/18 0-100 % SM 2540B
Fecal Coliform <201 col/ g dry 10/4/18 201 col/ g dry SM 9222 D
Meritech Work Order # 100418108 Sample: Flyash D 10-18 Grab 10/4/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
43.7 %
10/5/18
0-100 %
SM 2540B
Fecal Coliform
<208 col/ g dry
10/4/18
208 col/ g dry
SM 9222 D
Meritech Work Order # 100418109 Sample: Flyash E 10-18 Grab
Parameters
Results Analysis Date
10/4/18
Reporting Limit Method
% Total Solids
45.2 %
10/5/18
0-100 %
SM 2540B
Fecal Coliform
<201 col/ g dry
10/4/18
201 col/ g dry
SM 9222 D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]
87

Meritech, Inc.
Environmental Laboratory
R Laboratory Certification No.165
Page 2
Contact: Neal Davis Report Date: 10/12/2018
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 10/4/2018
Meritech Work Order # 100418110 Sample: Flyash F 10-18 Grab 10/4/18
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 47.8 % 10/5/18 0-100 % SM 2540B
Fecal Coliform 380 col/ g dry 10/4/18 183 col/ g dry SM 9222 D
Meritech Work Order # 100418111 Sample: Flyash G 10-18 Grab 10/4/18
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
46.2 %
10/5/18
0-100 %
SM 2540B
Fecal Coliform
<197 col/ g dry
10/4/18
197 col/ g dry
SM 9222 D
I hereby certify that 1 have reviewed and approve these data.
L boratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

I
5-92016 Chain of Custody Record (COC) .
I;
NPDES#:_WQ0021577 & WQ0000436
Client: Kapstone Kraft Paper Corp Phone:_ 252-533-6295
M E R I T' E C H
*C6,
•
JAddress:_
100 Gaston Road Fax: [phone]
ENVIRONMENTAL LABOR,ATORIES
Roanoke Rapids, NC 27870 Email: [e-mail]
—
;. 642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: info@meritechlal,
.com
Attention: Neal Davis Turn Around Time*
www.meritechiabs.com
How would you like our report sent? *RUSH work needs prior approval.
Std lOda s) 3-5 Da s 24-48Hrs
• Circle all that apply• ma' (preferred) , Fax, Nia'il
Sampling Dales &Times
S Tak
o ersn ang ampl i /Prn
ing
PA� w
�'457
Lab -Use -Only
Sample Location and/or ID #
Start
li End
Comp?
#of
Test(s) Required
On Ice?
pH OK?
Date
Time
„ Date
Time
Grab?
Cont.
Yes/No
CI OK?
FLYASH A 10-18
JI/r' /�
.'("
X
r'
CLASS A FECAL COLIFORM ANALYSIS , V
FLYASH B 10-18
i
�j
6S�
X
rr�� rr
CLASS A FECAL COLIFORM ANALYSIS V y
FLYASH C 10-18
.'��
X
CLASS A FECAL COLIFORM ANALYSIS G'
FLYASH D 10-18
7.15
X
CLASS A FECAL COLIFORM ANALYSIS
FLYASH E 10-18
, 2a
X
CLASS A FECAL COLIFORM ANALYSIS lY5
FLYASH F 10-18
,.
2,25
X
CLASS A FECAL COLIFORM ANALYSIS \ )
FLYASH G 10-18
--
�!p
1p � ..~
7. '3D'
X
CLASS A FECAL COLIFORM ANALYSIS � `I
�I
P"
Temperature Upon
Receipt:
Method of
*** Dechlorination
(<0.5 ppm) of A, mmonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation. ***
Comments:
Comppsitor #
Jug #
Shipment:
UPS
Fed Ex
Are these results for r gulatory pl�rposes? • Yes- a No
Report results in: mg/L mg/kg
ug/L 13.
and Delivery
Relinquished by: Date:/ /,� Time: ��—
1S
Received by: t)D Ttme-��L
(
Qt Other
Relinquishe y: D t Time:
;��
Received by. Date: Time:
Relinquished y: Date: Time:
Received b b: l�� �t : 1,6 T'im�' 1�