WQ0035324_Complete File - Historical_20160226

(MkTc
ATC ASSOCIATES OF NORTH CAROLINA, P.C.
Engineering Individual Solutions
February 22, 2016
North Carolina Department of Environmental Quality
Division of Water Resources — Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: Quarterly Groundwater Results —December 2015
Former Pro Cleaners
8377 Creedmoor Road
Raleigh, Wake County, North Carolina
Groundwater Remediation. Permit No. WQ0035324
DSCA Site Identification No. DC920001
ATC Project No. DC9201 SL3 0
2725 East Millbrook Road
Suite 121
Raleigh, NC 27604
Tel: [phone]
Fax: [phone]
www.atcassociates.com
N.C. Engineering License No. C-1598
_4%
6�'
r C
q
V
ATC Associates of North Carolina, P.C. (ATC), under contract to the North Carolina Drycleaning
Solvent Cleanup Act (DSCA), is providing the December 2015 groundwater sampling results
required by Groundwater Remediation Permit No. WQ0035324 for the former Pro Cleaners site in
Raleigh, North Carolina.
The analytical results for the December 2015 post -injection sampling event are reported on the
enclosed GW-59 Groundwater Quality Monitoring Compliance Report Forms in Appendix A. The
required monitoring wells and water supply wells were sampled pursuant to the referenced
permit. Corresponding GW-I forms were submitted to NCDEQ in the Quarterly Groundwater
Results submitted August 29, 2012.
For the December 2015 reporting period, a GW-59A form is included in Appendix R Note that the
full scale compliance boundary, documented in the Injection Application Addendum submitted
to NCDEQ on March 23, 2011, is used in lieu of a review boundary. Analytical data tables are
included in Appendix C, and document groundwater analytical data from monitoring wells, water
supply wells, and natural attenuation parameters. Note that extraction wells EW-8 and EW-9
were formerly injection wells IW-8 and IW-9. Also note that the extraction well EW-8 was not
sampled during the December 2015 event due to an issue with the extraction pump at the time of
sampling. Monitoring wells MW- 1013, MW- I I B, and MW- 12 historically contain a low water
level. As such, field analyzed natural attenuation parameters were not able to be analyzed and are
listed as "NA" on the GW-59 forms. Complete laboratory reports for the December 2015
sampling event is included in Appendix D. The next quarterly sampling event is scheduled for
March 2016.

Former Pro Cleaners
Permit No. WQ0035324
February 22, 2016
Page 2
If you have any questions or require additional inforrnation, please contact our office at (919) 871-
0999.
Sincerely,
ATC Associates of North Carolina, P.C.
CLOL- —7— XJP4,&,-
Andrew McMillan
Staff Scientist
M
Justin C. Ballard, P.G.
Project Manager

Former Pro Cleaners
Permit No. WQ0035324
APPENDIX A
GW-59 COMPLIANCE REPORT FORMS
February 22, 2016
Page 3

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION
OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: J�;Y31,2016
Facility Name: , Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES
Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (St-1) NC
27613
County Wake
13
Lagoon 13 Remediation: infiltration Gallery
�Cifty) �St2le)
(zip)
El
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
11
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 3515016212ft.
4�57/67A
to
Spec. Cond. 00094: NA I.Whos
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478-90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA ___jaqefj&
minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered: Ell
YES 0
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N o0r,15 0.0029J
mg/L
Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum ollo5
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC oomo 1.8
mg/L
Ca - Calcium oo916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
il
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900_
ug/L
Lab Report Attached? El Yes (1) U No (0)
Specific Conductance 00095
ltMhos
K - Potassium 0 0937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
7::S'�s -r t �j L A-L-L*-z�
Permittee (or Authorized Agent) Name and Title - Please print ortype
GW-59 Rev. 8/2013

SUBMIT FORM ONYELLO PAPERONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM 9
FACILITY INFORMATION
Facility Name: Former Pro Cleaners
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
Raleigh (Street) NC 27613
(City) (State) (zip)
Contact Person: Justin Ballard
Well Location/Site Name: Former Pro Cleaners
County Wake
Telephone#: [phone]
No. of wells to be sampled: 20
)EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
NVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number: Expiration Date: July3l,2016
Non -Discharge WQ0035324 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon 13 Remediation: Infiltration Gallery
Spray Field Remediation: Pump and Treat
Rotary Distributor Land Application of Sludge
Water Source Heat Pump 13 Other:
3AMPLING INFORMAI 1UN
Date sample collected: 12/17/2015
NELL ID NUMBER (from Permit): EW-9 (formerly IW-9) Well Diameter: 2 in.
Nell Depth: 87 ft. Screened interval: 111162112 ft. to 45157167Aft.
Depth to Water Level 82546: _�A ft. below measuring point Relative M.P. Elevation: 478.90 ft.
Measuring Point is 0 ft. above land surface
Volume of water pumped/bailed before sampling: NA _11alle—minutes (to parameter stabilization)
qnmnlp- for metals were collected unfiltered: E0 YES El NO and field acidified: E] _YESE3 NO
s
kBORATORY INFORMATION Con -test Analytical Laboratory
, "I zul 5 Laboratory Name:
ite sample analyzed: 12118, — -
kRAMETERS NOTE:iwiaiues should
reflect ��jssojvedand colloidal Concentrations.
mg/L
1, 0.0029J
Nitrite (NO2) as N 006 1 -
mg/L
COD 00335
/100mL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Coliform: MF Fecal 31616
mg/L
Coliform: MF Total 31504
/100ML
Phosphorus: Total as P 00665_
(Note: Use MPN method for highly turbid samptes)
Orthophosphate 70507 NA
mg/L
Dissolved Solids:Total 70300_
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
mglL
Cd - Cadmium 01027
ug/L
ug/L
Chromium: Total 01034
ug/L
Arsenic 01002
mg/L
Cu - Copper 01042
mg/L
Grease and Oils 00552
Fe - Iron 01045 NA
ug/L
Phenol 32730
uglL
ug/L
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ltMhos
K - Potassium 00937
mg/L
Specific Conductance 00095
mg/L
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
(Ammonia Nitrogen; NH, as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L
TKIN as N 00625
mg/L
Ni - Nickel 01067
ug/L
For Remediation Systems Only (Attach Lab Reports):
-;s --, L,— 10
Permittee (or Authorized Agent) Name and Title - Please print or type
influent Total VOCS: 0.13194
mg/L
FIELD ANALYSES:
pH 004001 NA units
Spec. Cond. 00094: NA
Odor 00085:
Appearance
WAS DRY
at time of
Temp. 00010: NA oc sampling,
_PS/Cm' check
Certification No. 652
Pb - Lead o1051 ug/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
Tetrachioroethene: 0.16 mg/L
Trichloroethene: 0.0073 mg/I
cis-1,2-Dichloroethene: 0.0012 mg/l
trans-1,2-Dichloroethene: Not Detected
VinvI chloride: Not Detected
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method ATTACH LAB REPORT.)
Lab Report Attached? 0 Yes (1)
El No (0)
VOC 78732 method #
EPA 8260B
Total Organic Carbon method #
EPA 531 OC
Sulfate method #
ASTM D516-90
Ammonia, sulfide, nitrate, nitrite method #
EPA 4500
Effluent Total VOCS: 0
IN
mg/L VOC Removal% 100
-Z 17-7,1 /'r
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: J�ly 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE OF PERMITTED OPERATION BEING MONITORED
Raleigh (st­') NC
27613
County Wake
Lagoon Remediation: infiltration Gallery
(City) (State)
(zip)
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone* 919-871-0999
El Rotary Distributor El Land Application of Sludge
Well Location/Site Name. Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
at time of
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval : 35150162172 ft.
to 4515716U ft. Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478-90
ft. Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA
minutes (insufficient recharge
for purging) Appearance
Samples for metals were collected unfiltered: E0
YES El
NO and field acidified: 0 YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved
and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L Pb - Lead oio5i ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L JNA = Not analyzed due to lack of sufficient water.
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L utner (Specity Compounds and Concentration TnitsT
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg1L Tetra ch I oroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug1L Trichloroethene: 0.0073 mg1I
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045 NA
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? El Yes (1) 0 No (0)
Specific Conductance o0o95
IxMhos
K - Potassium 00937
mg/L VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: u Mg/L vut, Kemovai-/o
Af-�
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge W00035324 UIC
Permit Name (if different):
NPDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE OF PERMITTED OPERATION BEING MONITORED
Raleigh (st-0 NC
27613
County Wake
El Lagoon 13 Remediation: Infiltration Gallery
(City) �St.[�')
(zip)
11 Spray Field Rernediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
13 Rotary Distributor Land Application of Sludge
Well Location/Site Name. Former Pro Cleaners
No. of wells to be sampled: 20
77 Z-7
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WAS DRY
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
at time of
Well Depth: 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 35150162172ft.
to 45157167Aft.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Pelative M.P. Elevation: 478-90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA
minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered:
YES
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
652
Date sample analyzed: 12118,12121-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead olo5i ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg1L
INA = Not analyzed due to lack of sufficient water.
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
Mg/L
Other �SpeClry Uompounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Alurninurn oil o5
mg/L
Tetra ch loroeth ene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/1
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? 0 Yes (1) Ll No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927_
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite -, method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
_,4 -(, J
16 � U_44A>
Perm ittee (or Authorized Agent) Name and Title -Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPIDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (Street) NC
27613
County Wake
11
Lagoon 13 Remediation: infiltration Gallery
(City) (St,,ite)
�Zip)
11
Spray Field 0 Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
Rotary Distributor El Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 130ther:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 3tV1016�2 ft.
to
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478-90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA _Vaffffl.�-
minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered: E0
YES El
NO and field acidified: El YES El
NO
LABORATORY NFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 uglL
Coliform: MF Fecal 31616
1100mL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MFN method for highly turbid samples)
Orthophosphate 70507 NA
mg1L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Alurninum 01105
mg/L
Tetrachloroethene: 0. 16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/l
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
uglL
(Specify test and method #. ATTACH LAB REPORT)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) 13 No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
-ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
:� 1 r-j (a pf tAAz�
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
EIlT�FTIKMr._DEP
RTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
aim
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE OF PERMITTED OPERATION BEING MONITORED
Raleigh (s1­0 NC
27613
County W - ake
Lagoon Remediation: Infiltration Gallery
fcity) (SW�)
Op)
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
water source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION EW-9 (formerly IW-9)
WELL ID NUMBER (from Permit):
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
at time of
Well Depth: 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 35150162f72ft.
to 451571679ft. Spec. Cond. 00094: NA LtMhos
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft. Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA _____,�rninutes
(insufficient recharge
for purging) Appearance
Samples for metals were collected unfiltered: EH
YES
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12121-2312015
Laboratory Name: Con -test Analytical Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as IN 00615 0.0029J
mg/L Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L INA = Not analyzed due to lack of sufficient water.
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum o1105
mg/L Tetrachloroethene: 0. 16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L Trichloroethene: 0.0073 mg/I
TOC oom 1.8
mg/L
Ca - Calcium 00916
mg/L cis-1,2-Dichloroethene: 0.0012 mg/l
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L trans-1,2-Dichloroethene: Not Detected
Arsenic 01002 _ug/L
Chromium: Total 01034
ug/L Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
uglL Lab Report Attached? El Yes (1) 0 No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937---
mg1L VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0-93
ug/L Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: u.',J"J4 Mg/L tmueni ioiai vut-s. � V%J%O !Awiliuval /0 ­
6,4L—A4ZJ0
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
E1y�FT1
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPIDES
Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (Slmet) NC
27613
County Wake
Lagoon 13 Remediation: Infiltration Gallery
(City) (st.t�)
(zip)
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
Rotary Distributor El Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
water source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION EW-9 (formerly 1W-9)
WELL ID NUMBER (from Permit):
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
at time of
Well Depth: 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval : 35f5016212 ft.
to 451511671ft.
Spec. Cond. 00094: NA uMhos
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 000s5:
here:
Volume of water pumped/bailed before sampling:
NA
ga'191216 minutes (to Parameter stabilization)
Appearance
Samples for metals were collected unfiltered: Ell
YES 0
NO and field acidified: E3 YES M
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved
and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 ug/L
Coliform: MIF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: M F Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Soiids:Total 70300
mg/L
Al -Aluminum ol io5
mg/L
Tetra ch I oroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium01007
ug/L
Trichloroethene: 0.0073 mg1I
TOC 00680 1.8
mg/L
Ca - Calcium oo916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/l
ChlorideOO940
mg/L
Cd - CadmiumOI027
ug/L
trans- 1,2-Dichl oroeth ene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease andOiIS 00552
mg/L
Cu - Copper01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron o1o45 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? EZI Yes (1) 0 No (0)
Specific Conductance00095
[tMhos
K - PotassiumOO937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium00927
mg1L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3as N;Ammonia Nitrogenjotal)
Mn - Manganese 01055 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067_
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: U.1 31�,14 mg/L I:_-ttluent lotal vuus: u Mg/L vull memoval7o —
Permittee (or Authorized Agent) Name and Title - Please print ortype
Authorized
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION
OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]D6
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPIDES
Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (Strpet) NC
27613
County Wake
Lagoon Ell Remediation: Infiltration Gallery
(City) (St.le)
(zip)
Spray Field M Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone* 919-871-0999
Rotary Distributor El Land Application of Sludge
. Former Pro Cleaners
Well Location/Site Name.
No. of wells to be sampled: 20
-
Water Source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
at time of
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 000lo: NA cc
sampling,
Depth to Water Level 82546; NA ft. below measuring point
Screened Interval: W50162N2ft.
to 45157167Aft.
Spec. Cond. 00094: NA �tMhos
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 000m:
here:
Volume of water pumped/bailed before sampling:
NA
@allens minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered: Ell
YES
NO and field acidified: El YES 171
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved
and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminurn o1105
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
_ug/L
__ Trichloroethene: 0.0073 mg/I
TOC 00680 1-8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) U No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927 _mg1L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as IN 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Iota] VUUS: u —Mg/L vuL, Kenrl
I/-' B, A w-A VP
Permittee (or Authorized Agent) Name and Title - Please print or type
Signature of Permiftff (or
GW-59 Rev. 8/2013

SUBMlT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Former Pro Cleaners
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
Raleiqh (st-0 NC
(City)
-f De —on: Justin Ballard
Location/Site Name:
Former Pro Cleaners
(st.tp)
27613
(zip)
or
County Wale
Telephone#: [phone]
No. of wells to be sampled: 20
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number: Expiration Date: July 31, 2016
Non -Discharge WQ0035324 UIC
NPDES Other
YPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation: Pump and Treat
El Rotary Distributor El Land Application of Sludge
13 Water Source Heat pump [3 Other:
PLINU 1Nr*UKIVl1Al Jul"I EW-9 (formerly W-9) Date sample collected: 12/17/2015
L ID NUMBER (from Permit):
87 Well Diameter: 2 in.
Depth: 016212 ft. to 45157167A ft.
h to Water Level 82546: NA ft. below measuring point Screened Interval: 3-
3uring Point is 0 ft. above land surface Relative M.P. Elevation: 478.90 —ft.
me of water pumped/bailed before sampling: _LA_-qaI1GR6 minutes
Dies for metals were collected unfiltered: YES [I No and field acidified: El YES El NO
LABORATORY INFORMAI ILIN Laboratory Name: Con -test Analytical Laboratory
12/18 12/21-2312015
Date sample analyzed:
PARAMETERS NO : Values should reflect dissolved and colloidal concentrations.
mg/L
Nitrite (NO2) as N 006 15 0.0029J
mg/L
COD 00335_
/100mL
Nitrate (NO3) as N 00620 NotDetected
mg/L
Coliform: IMF Fecal 31616
mg/L
Coliform: MF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Dissolved Solids:Total 70300
mg/L
All -Aluminum oil o5
mg/L
pH (Lab) 00403
units
Ba - Barium 01007 —
ug/L
TOC 00680 1-8
mg/L
Ca - Calcium 00916_
mg/L
Chloride 00940
mg/L
Cd - Cadmium 01027 _
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034_
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe -Iron oio45 NA
_ug/L
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Specific Conductance 00095
�Whos
K - Potassium 00937
mg/L
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L
TKIN as N 00625
mg/L
Ni - Nickel 01067
ug/L
For Remediation Systems Only (Attach Lab Reports)
Permittee (or Authorized Agent) Name and Title - Please printortype
Influent Total VOCS: 0.13194
mg/L
FIELD ANALYSES:
pH 00400: NA units
Spec. Cond. 00094: NA
Odor 00085:
Appearance
Temp. 00010! NA oc
WS/Cm,
Certification No. 652
Pb - Lead 01051 ug/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
Tetrachloroethene: 0. 16 mg/L
Trichloroethene: 0.0073 mg/l
cis-1,2-Dichloroethene: 0.0012 mg/l
trans-1,2-Dichloroethene: Not Detected
Vinyl chloride: Not Detected
ORGANICS: (by GC, GC/i HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? E] yes (1) 10 No (0)
VOC 78732 method # EPA 8260B
Total Organic Carbon method # EPA 531 OC
Sulfate method # ASTM D516-90
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
Effluent Total VOCs: 0
WAS DRY
at time of
sampling,
check
here:
mg/L VOC Removal% 100
a
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
T . . .
14299aQui
. . i
DE RTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��*17
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPIDES
Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (Street) NC
27613
County Wake
Lagoon 13 Remediation: Infiltration Gallery
(City) (State)
(Zip)
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
Rotary Distributor Land Application of Sludge
Well Location/Site Name. Former Pro Cleaners
No. of wells to be sampled: 20
77
water source Heat Pump 13 Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
If WELL
WAS DRY
Well Depth: 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA 0C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 3515016212 ft.
to 451116111 ft.
Spec. Cond. 00094: NA ps/cm,
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA
92119,;s minutes
Appearance
Samples for metals were collected unfiltered:
YES
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
11 OOmL
Nitrate (NO3) as N 00620 NotDetected
_mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum o1io5
mg/L
etrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg1I
TOC 00680 1-8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) 10 No (0)
Specific Conductance 00095
ltMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH,as N;Ammonia Nitrogen, Total)
Mn - Manganese oio55 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as IN 00625
mg/L
Ni - Nickel o1067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 1UU
Permiftee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (st-0 NC
27613
County Wake
11
Lagoon 13 Remediation: Infiltration Gallery
(Cily) (Stat�)
�Zip)
El
Spray Field M Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
0
Rotary Distributor El Land Application of Sludge
Well Location/Site Name. Former Pro Cleaners
No. of wells to be sampled: 20
—M P-M
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WAS DRY
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES-
at time of
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 000lo: NA 0C
sampling,
Depth to Water Level 82546: NA ft. below measuring
point
Screened Interval: ­­Ul2ft.
to 4-7167A ft.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA _ja4eRs-minutes
(to parameter stabilization)
Appearance
0
Samples for metals were collected unfiltered:
YES
NO and field acidified: El YES 0
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-2312015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO.) as N 00620 Not Detected
_mg1L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg/L
Tetra ch I oroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/l
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans- 1,2-Di ch I oroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) 0 No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH,as N;Ammonia Nitrogenjotal)
Mn - Manganese 01055 0-93
ug/L
Sulfate method # ASTM D516-90
TKIN as N 00625
mg/L
Ni - Nickel o1o67
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 1UU
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date; July 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES
Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (SV-0 NC
27613
County Wake
11
Lagoon 13 Remediation: Infiltration Gallery
(C'ty) (st.l�)
(zip)
11
Spray Field M Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
Rotary Distributor El Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
if WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 3s(�MMft.
to 45/5716711ft.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surFace
Relative M.P. Elevation: 478.90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA ___:ga49RG-minutes
(to parameter stabilization)
Appearance
Samples for metals were collected unfiltered: ED
YES El
NO and field acidified: El YES 173
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as IN 00615 0.0029J
mg/L
Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Alurninum 01105
mg/L
Tetra ch loroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/
Cd - Cadmium 071027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) U No (0)
Specific Conductance 00095
RMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L
Sulfate method # ASTIM D516-90
TKIN as IN 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): I nfl uent Tota I VOCs: 0. 13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
Permittee (or Authorized Agent) Name and T-itle - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
. ' .
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (st-0 NC
27613
County Wake
Lagoon Remediation: Infiltration Gallery
(City)
(Zip)
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
Rotary Distributor El Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
water source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA C
at time of
sampling,
Depth to Water Level 82546; NA ft. below measuring point
Screened Interval: 3515016V72ft.
to 45157167ftft.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 00085: —
here:
Volume of water pumped/bailed before sampling:
NA _.@�rriinutes
Appearance
Samples for metals were collected unfiltered:
YES
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-2312015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg/L
Tetrachloroethene: 0. 16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/l
TOC 00680 1.8
mg/L
Ca - Calcium oog16
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? 0 Yes (1) U No (0)
Specific Conductance 00095
�IMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH3asN;Ammonia Nitrogenjotal)
Mn - Manganese 01055 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
'j T, auj� e'c-
Permittee (or Authorized Agent) Name and Title - Please print or type
Agent)
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
MITI
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION
OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT
Number: Expiration Date: July 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES
Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
(street) NC
27613
County Wake
Lagoon Remediation: infiltration Gallery
Raleigh
(Stele)
izip)
Spray Field Remediation: Pump and Treat
(City)
Contact Person: Justin Ballard
Telephone#: [phone]
El
Rotary Distributor 13 Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
13
water source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
at time of
Well Depth: 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
sampling,
NA
Depth to Water Level 82546: ft. below measuring point
Screened Interval: ­50162U2 ft.
—
to 4�571611�ft.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA _.q�minutes
Appearance
Samples for metals were collected unfiltered:
YES
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE. Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg1L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum ollo5
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403 —
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg1l
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552 —mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate oO945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) U No (0)
Specific Conductance 00095--
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Min - Manganese 01055 0-93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
_�S'JS 2
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES
Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (St-0 NC
27613
County Wake
Lagoon 13 Remediation: Infiltration Gallery
(City) (State)
(zip)
Spray Field 0 Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephol 919-871-0999
Rotary Distributor F-1 Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
at time of
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA C
sampling,
Depth to Water Level 82546: NA --ft. below measuring point
Screened Interval: 35(50/62U2 ft.
to 45/57167Aft.
Spec. Cord. 00094: NA PS/CM2
check
Measuring Point is 0 -_ ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA ___:ga4aFl,_minutl
Appearance
Samples for metals were collected unfiltered: EP
YES 0
NO and field acidified: El YES [M
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
1100l
Nitrate (NO3) as N 00620 Not Detected
_mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
mg/L
(Note: use Ml method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg1I
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/l
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
1
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
l
Lab Report Attached? El Yes (1) 0 No (0)
Slpecific Conductance 00095
lLMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH,as N;Ammonia Nitrogenjotal)
Mn - Manganese wo55 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: u mg/L VUU Kemovamo iuu
?, Pf"4q-_i>
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPIDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (St­l) NC
27613
County Wake
11
Lagoon 13 Remediation: infiltration Gallery
(City) (Stt.)
(zip)
11
Spray Field 0 Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: .[phone]
0
Rotary Distributor 13 Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled'. 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA 0C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring
point
Screened Interval: 3515016Z72 ft.
to 45/57/671ift.
Spec. Cond. 00094! NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 000m:
here:
Volume of water pumped/bailed before sampling:
NA _ja4GP,,,.minutes
Appearance
Samples for metals were collected unfiltered: 0
YES El
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12118,12/21-2312015
Laboratory Name: Con -test Analytical
Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 _mg/L
Coliform: IVIF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg/L
Tetra ch loroethene: 0. 16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 ni
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 ri
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002 _ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) 0 No (0)
Specific Conductance o0095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese oim 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
uglL
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
_S,1', -r, -.1 L�A IA-4-12,0
Permittee (or Authorized Agent) Name and Title - Please print or type
16
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
111115N PfIr-7117.
fr. M
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE OF PERMITTED OPERATION BEING MONITORED
Raleigh (Sr,aet) NC
27613
County Wake
El Lagoon CE Remediation: infiltration Gallery
(City) (Sti,l.)
(ZIP)
El Spray Field IM Remediation: Pump and -Treat
Contact Person: Justin Ballard
Telephone#: [phone]
Rotary Distributor 13 Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
(fr,m P­
t)
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
1W-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 3&5W62R2 ft.
to ­­6"ft.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478-90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA
gaileRs minutes
Appearance
Samples for metals were collected unfiltered: [9
YES El
NO and field acidified; El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-2312015
Laboratory Name: Con -test Analytical
Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead oimi ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO.) as IN 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum olim
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC 00680 1-8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg1I
Chloride00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) El No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055 0-93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625 -
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
--y' S T-1 J 85-4
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: JUIY31,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
NPIDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC
27613
TYPE OF PERMITTED OPERATION BEING MONITORED
11 Lagoon Remediation: Infiltration Gallery
Raleigh (S11-1 NC 27613 County Wake
,(0)
lzi,
El Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El Rotary Distributor El Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/1712015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter- 2 in.
pH 00400: NA units Temp. CoojQ: NA C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: --ft.
to ft. Spec. Cond. 00094, NA �I.Mhos
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA
minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered:
YES
NO and field acidified: El YES E]
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12121-23/2015
Laboratory Name: Con -test Analytical Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead olo5i u g/L
Coliform: MF Fecal 31616 _/100mL
Nitrate (NO3) as N ooc,20 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
11OOmL
Phosphorus: Total as P oo665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum oil o5
mg/L
Tetrachloroethene: 0.16 mg1L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichlorcethene: 0.0073 mg!l
TOC 00680 1.8
mg/L
Ca - Calcium oogl6
mg/L
cis-1,2-Dichloroethere: 0.0012 mg�
Chloride 00940
mg/L
Cd - Cadmium 01027
uglL
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and OilS 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
uglL
Lab Report Attached? E] Yes (1) El No (0)
Specific Conductance 00095
pMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH. as N; Ammonia Nttrogen, Total)
Mn - Manganese cio55 0-93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
uglL
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: - 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
Ar L
loemnittee (or Authorized Agent) Name and Title - Please print or type
GVI-59 Rev. 8/2013

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Former Pro Cleaners
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
(si-1) NC
I '�"
act Person: Jusfin Ballard
Location!Site Name: Former Pro Cleaners
SUBMlT FORM ON YELLOW PAPER ONLY
Clearly or
27613 County Wake
!Zipl
Telephoneg: 919-871-0999
No. of wells to be sampled: 20
)EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
31VISION OF WATER RESOURCES - INFORMATION PROCESSING UNlT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number: Expiration Date: JuIY31,2016
Non -Discharge W00035324 UIC
NPIDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Ell Remediation: Infiltration Gallery
Spray Field Remediation: Pump and Treat
Rotary Distributor L2ndApplicaticn of Sludge
Water Source Heat Pump Other: _
E>AMP_LING Date sample collected: 12/17/2015
INt-L)" 1 13
VVELL ID NUMBER (from Permit): EW-9 (formerly IW-9) Well Diameter: 2 in.
87
Well Depth: Screened interval: 1"111212ft. to ­M7A
Depth to Water Level 82546: NA ft. below measuring point Relative M.P. Elevation: 478.90
Measuring Point is 0 ft. above land surface
Volume of water pumped/bailed before sampling: NA _____9�minutes (to parameter stabilization)
El YES NO
.1;;;1rnnIP.,; for metals were collected unfiltered: [I YES El NO and field acidified:
kBORATORY INFORMATION Laboratory Name: Con -test Analytical Laboratory
" 12121-23/ZU15
ate sample analyzed ' 1- - ntrations.
kRAMETERS NWTE: —V.Iues should reflect dissolved and colloidal conce
mg/L
Nitrite (NO2) as IN 00615 0.0029J
mg/L
COD 00335
11OOmL
Nitrate (NO,) as N 00620 Not Detected
mg/L
Coliform: MF Fecal 31616
/1 OOmL
Phosphorus: Total as P 00665__
mg/L
Coliform: MF Total 31504
(Note use MPN method for K I turbid samples)
Orthophosphate 70507 NA
mg1L
Dissolved Solids:Total 70300
mg/L
Al -Alurninum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug1L
TOC 00680 1-8
mg/L
Ca - Calcium 00916
mg1L
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
ug/L
chromium: Total 01034
ug/L
Arsenic 01002
mg/L
Cu - Copper 01042
mg/L
Grease and Oils 00552
Fe - Iran 01045 NA
ug/L
Phenol 32730
ug/L
ug/L
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
specific Conductance 00095
IXMhos;
K - Potassium 00937
mg/L
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
(Ammon,a Nitrogen: NH,2s N:Ammonia Nitrogen. Total)
Mn - Manganese 01055 0.93
ugiL
TKIN as N 00625
mg/L
Ni - Nickel 01067
ug/L
For Remediation Systems Only (Attach Lab Reports)
_;� 1 -­1 �; Pr I-,-- -
-Fe—rmittee (or Authorized Agent) Name 2no I ]Tie - Please print or type
influent Total VOCs: 0.13194
mglL
FIELD ANALYSES:
pH 00400: NA units
Spec. Cond. 0OC94. NA
Odor 00085:
Appearance
If WELL
WAS DRY
at time of
Temp. 00010: NA
sampling,
—ps/cr check
Certification No. 652
Pb - Lead oio5i u g/L
Zn - Zinc 010C2 mgj'L
Other (specify Compounds and Concentration Units):
Tetra& I oroethe ne: 0.16 mg/L
Trichloroethene: 0.0073 mgA
cis-1,2-Dichloroethene: 0.0012 mg/i
trans-1,2-Dichloroethene: Not Detected
VinvI chloride: Not Detected
here:
11
ORGANICS: (by GC, GCtMS, HPLC)
(Specify test and method ATTACH LAB REPORT.)
Lab Report Attached? [D Yes (1)
L3 No (0)
VOC 78732 method #
EPA 8260B
Total Organic Carbon method #
EPA 531 OC
Sulfate method #
ASTM D516-90
Ammonia, sulfide, nitrate, nitrite , method # EPA 4500
Effluent Total VOCS: 0
(or
mg/L VOC Removal% 100
-Z /-7- Z'/ / '-
GW-59 Rev. 8/2013

JBMIT FORM ON YELLOW PAPER ONLY
&��E[VISION
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM ��%617
MAIL SERVICE CENTER. RALEIGH, NC 27699-1617 Phone, 91"07-6306
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: J�ly3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
-
Permit Name (if different):
NPDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE OF PERMITTED OPERATION BEING MONITORED
11 Lagoon Remediation: Infiltration Gallery
Raleigh NC 27613 County Wake
El Spray Field Pernediation: PumpandTreat
Contact Person: Justin Ballard Telephone#-. 919-871-0999
13 Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION
Permit): EW-9 (formerly IW-9) Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
WELL ID NUMBER (from
Well Depth: 87 ft. Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA cc
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point Screened Interval: 311—ft.
to 4511rffill�ft. Spec. Cond. 00094: NA ps/cm,
check
Measuring Point is 0 ft. above land surface Relative M.P. Elevation: 478.90
ft. Odor 00085:
here:
Volume of water pumped/bailed before sampling: NA minutes (insufficient recharge for purging) Appearance
Samples for metals were collected unfiltered: 0 YES El NO and field acidified: Ll YES El
NO
I
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-23120'5 Laboratory Name: Con -test Analytical Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
CC D 00335 mg/L Nitrite (NO2) as N 00615 0.0029J
mg/L Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 Not Detected
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665
mg/L =.=Not analyzed due to lack of sufficient water.
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 NA
mg/L Other (5pecity Compounds and Concentration Units):
Dissolved Solids:Total 70300 mg/L Al -Alurninum o1105
mg/L Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403 units Ba - Barium 01007
ug/L Trichloroethene: 0.0073 mgA
TOC 00680 1-8 mg/L Ca - Calcium 00916
mg/L cis-1,2-Dichlaroethene: 0.0012 mg1I
Chloride 00940 mg/L Cd - Cadmium 01027
ug/L trans-1,2-Dichloroethene: Not Detected
Arsenic 01002 ug/L Chromium: Total o1o34
ug/L Vinyl chloride: Not Detected
Grease and Oils 00552 mg/L Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L Fe - iron 01045 NA
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected mg/L Hg - Mercury 71900
ug/L Lab Report Attached? [D Yes (1) El No (0)
Specific Conductance 00095 RMhos K - Potassium 00937
mg/L VOC 78732 _, method # EPA 8260B
Total Ammonia 00610 Not Detected mg/L Mg - Magnesium 00927
mg/L Total Organic Carbo�i method # EPA 531 OC
(Ammonia Nitrogen; NH,as N;Ammonia Nitrogenjotal) Mn - Manganese o1o55 0.93
ugIL Sulfate method # ASTM D516-90
TKN as N 00625 mg!L Ni - Nickel 01067
ugfL Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: U-13194 mg/L Ettluent lotal vuus: 6 mgiL Vol- memOval7o I
Permittee (or Authorized Agent) Name and Tide -Please print or type
GW-59 Rev- 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
190jaMOLU
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��K617
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Piease Print Clearly or Type
PERMIT Number: Expration Date: J�ly3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
NPDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC
27613
TYPE OF PERMITTED OPERATION BEING MONITORED
11 Lagoon 13 Remediation: Infiltration Gallery
Raleigh (311-0 NC 27613 County Wake
(S"tn�
(7irl)
El Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft -
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA �C
at time of
sampl:ng,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 35�-212ft.
to """"'ft. Spec. Cond. 00094: 14A pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elctvation: 478.90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA
gaiieRs minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered: 0
YES F-1
NO and field acidified: 0 YES 0
NO
LABORATORY INFORMATION
Date sample analyzed: 12118. 12/21-2312015
Laboratory Name : Con -test Analytical Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L Pb - Lead oic5i ug/L
Coliform: MF Fecal 31616
11OOmL
Nitrate (NO3) as N 00620 Not Detected
mg!L Zn -Zinc 01092 mg/L
Coliform: MF Total 31504
/1 OOmL
Phosphorus: Total as P 00665
mg/L INA = Not analyzed due to lack of sufficient water.
(Note Use MPN method for highly turNd samples)
Orthophosphate 70507 NA
mg/L
utner (Specity Compounds and Uoncentration—Un-TisT7—
Dissolved Solids:Total 70300
mg/L
Al -Aluminum ollo5
mg1L
Tetrachloroethene: 0. 16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
—ug/L
Trichloroethene: 0.0073 mg/I
TOC oo6so 1-8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mgA
Chloride 00940 _mg/L
Cd - Cadmium 01027
ug/L
tr2ns-1.2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ut g/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
uq1L
Lab Report Attached? 0 Yes (1) U No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia om,,c Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH�as N;Ammonia Nitrogen.Total)
Mn - Manganese o1o55 0-93
ugfL Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
103MM2=1DEPARTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
P!ease Print Cleany or Type
PERMIT Number: Expiration Date: J11Y31.2016
Facility Name: Former Pro Cleaners
Non -Discharge %IVQ0035324 UIC
NPDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (S111-11) NC
27613
County Wake
11
Lagoon Remediation: Infiltration Gallery
fslnl��
�7'p�
El
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
P_
I I
Water Source Heat Pump C3 Other:
SAMPLING INFORMATION
If WELL
WAS DRY
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12117/2015
FIELD ANALYSES:
at time of
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: ­­-2ft.
to
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 0OC85:
here:
Volume of water pumped/bailed before sampling:
NA _VeHtrm�
minutes (to parameter stabilization)
Appearance
0
Samples for metals were collected unfiltered: Ell
YES El
N 0 and field acidified: 0 YES
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12121-23/2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 _mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead o1o5i
Coiform: MF Fecal 31616
11 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg!L
Zn - Zinc 01092 mg/L
Coliform: MF Total 315G4
/100mL
Phosphorus: Total as P OC665
mg/L
(Not�: Use IVPN medocl for highly turtoid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum w105
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC 00680 1.8
mg/L
Ca - Calcium oogi6
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002 —ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
CU - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug1L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug]L
Lab Report Attached? ID Yes (1) El No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 0061.0 Not Detected
mg!L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
�Ammonia Nitrogen: NH,as N:Ammoma Nitnogenjotal)
Mn - Manganese oio55 0-93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug1L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
:S , -,-r , � �3 P� LL4,z,�
Permittee (or Authorized Agent) Name and Tide - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPA TMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DWISION OF WATER RESOURCES � INFORMATION PROCESSING UNrT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
P�ease Print Dearty or Type
PERMIT Number: Expiration Date: J�IY31,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
Permit Name (if different):
NPIDES Other
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE OF PERMITTED OPERATION BEING MONITORED
Raleigh NC
27613
County Wake
11 Lagoon Remediation: Infiltration Gallery
(SW�)
(Lp)
11 Spray Field Remediaticn: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
13 Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled. 20
Water Source Heat Pump 13 Other:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA 0C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 3515MO-2ft.
to 151716"fL Spec. Cond. 00094: NA I(Mhos
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft. Odor occ85:
here:
Volume of water pumped/bailed before sampling:
NA _-g�minutes
(insufficient recharge
for purging) Appearance
Samples for metals were collected unfiltered: 0
YES El
NO and field acidified: 0 YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18.12/21-23t2015
Laboratory Name: Con -test Analytical Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as IN 006-,S 0.0029J
mg/L Pb - Lead o1o5i ug1L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L [—NA = Not analyzed due to lack of sufficient water.
(Note Use MPN method for highty turbid samples)
Orthophosphate 70507 NA
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
At - Aluminum oilm
mg/L Tetrachloroethene: 0. 16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug1L Trichloroethene: 0.0073 mg/I
TOC oo6w 1-8
mg/L
Ca - Calcium 00916
mg/L cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg1L
Cd - Cadmium 01027
ug1L trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
u g/L
Chromium: Total 01034
ug/L - Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ugfL (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not -Detected
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 0 Yes (1) Q No (0)
Specific Conductance 00095
�tMhos
K - Potassium 00937
mg/L VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg!L Total Orga . n . ;c Carbon method # EPA 531 OC
(Ammonia Ktrogen: NH,as N;Ammonia Nitrogenjotal)
Mn - Manganese 01055 0-93
ug/L Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel o1067
ug/L Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: u mg/L VL)L; Kemovav/. 106
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev- 812013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: J.iY31,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
NPDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC
27613
TYPE
E]
OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Raleigh (svldi NC 27613 County Wake
(C"y) (Sliili,�
�Zp)
11
Spray Field Remediat;on: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
If WELL
WAS DRY
Well Depth: 67
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: ­­12ft.
to --ft.
Spec. Cond. 00094: NA �tMhos
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor ocoa5:
here:
Volume of water pumped/bailed before sampling:
NA
9611ORS minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered: ER
YES El
NO and field acidified: 0 YES
NO
LABORATORY INFORMATION
Date sample analyzed: 12118,12t2l-23 / 2015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
—mg!L
Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616
11OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Noie: Use IAPN method for highly turbid sampl�)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mgL
Al -Aluminum o1105
mg/L
Tetra ch loroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
7richloroethene: 0.0073 mg/l
TOO owso 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroetnene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ugIL
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ugfL
(Specify test and method #, ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
—ug/L
Lab Report Attached? ID Yes (1) U No (0)
Specific Conductance 00095
�iMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium C0927
mg!L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH,as N;Ammon;a Nitrogen, Total)
Min - Manganese 01055 0-93
uglL
Sulfate method g ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: U mg/L VOC Removal/. luu
'5­s-k , J �3 A L-AR-51
Permittee (orAuthonzed Agent) Name and Title - Please Print ortype
Signature of
GW-59 Rev. 812013

SUBMIT FORM ON YELLOW PAPER ONLY
­�DEPARTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER. RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: JuIY31,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
NPIDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleig1h NC
27613
TYPE
1:1
OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Raleigh NC 27613 County Wake
IMP)
El
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump Other:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/1712015
FIELD ANALYSES:
WAS DRY
Well Depth: 87
Well Diameter: 2 in.
pH 00400� NA units Temp. 00010: NA oc
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval:
to �iiriiWrfl.
Spec- Cond- 00094. NA ltMhos
check
Measuring Point is o ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor coom:
here:
Volume of water pumped/bailed before sampling:
NA
g-� minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered: 0
YES
NO and field acidified: 0 YES
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12121-2312015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 uglL
Coliform: MF Fecal 31616_
/I OOmL
Nitrate (NO,) as N 00620 Not Detected
mg/L.
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 1100ml-
Phosphorus: Total as P 00665
mc/L
(Note: Use, MPN method for highly turbid �ri
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Tot8170300
mg/L
Al -Aluminum o1105
mg/L
Tetra chloroethene: 0.16 mg[L
pH (Lab) 00403
units
. Ba - Barium olow
ug/L
Trichlorcethene: 0.0073 mg/I
TOC oo68o 1-B
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug1L
Viny: chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. AT TACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) El No (0)
Specific Conductance 00095
P.Mhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 82606
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # . EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VUCS: u Mg/L vuu Removam. luu
_� , -,f I r_� � a LA_ A EP
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM asp Pr.nt aearly or
Facility Name: Former Pro Cleaners
Permit Name (if different): _
Facility Address: 8377 Creedmoor Road Ra
R21eiah (S-211 INC
11 1� �
act Person: Justin Ballard
Location/Site Name: Former Pro Cleaners
SUBMIT FORM ON YELLOW PAPER ONLY
h NC 27613
27613 County Wake
Telephone#: [phone]
No. of wells to be sample
SAMPLING INf-0KMAI JUN EW-9 (formerly IW-9) Date sample collected: 12MV2015
WELL ID NUMBER (from Permit):
67 Well Diameter: 2 in.
Well Depth: Screened Interval: 3560ffi-2 ft. to
Depth to Water Level 82546: NA it. below measuring point —
Measuring Point is 0 ft. above land surface Relative M.P. Elevation: 478.90
Volume of water pumped/bailed before sampling: NA ____:g�minutes C1 YES M, NO
Samples for metals were collected unfiltered: 0 YES [I NO .. and field acidified:
)EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
)IVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, No 27699-1617 Phone: [phone]
PERMIT Number: Expiration Date: July3l.2016
Non -Discharge WQ0035324 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
11 Lagoon Remediation: Infiltration Gallery
El Spray Field Remediation: Pump and Treat
Rotary Distributor Land Application of Sludge
Water Source Heat Pump Other.
�BORATORY INFORMAII 1UN
Laboratory Name: Con -test Analytical Laboratory
ate sample analyzed: 12/18,12121-2612015
kRAMETERS NOTE: Values sho I reflect
dissol ed and colloidal concentrations.
mg/L
Nitrite (NO2) as IN 00615 0.0029J
mg/L
COD 00335
1100mL
Nitrate (NO.3) as N 00620 Not Detected
mg/L
Coliform: MF Fecal 31616
mg/L
Coliform: MF Total 31504
/1 OOrnL
Phosphorus: Total as P 00665
(Note: Use IIPN methcd for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
Ug/L
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg!L
Chloride 00940
mg/L
Cd - Cadmium 01027
ugIL
Arsenic 01002
UgfL
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 0 1042
mg/L
Phenol 32730
ug/L
Fe - Iron 01045 NA
ug/L
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
specific Conductance 00095
VMI1cS
K - Potassium 00937
mg/L
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927_
mg1L
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogenjotal)
Mn - Manganese 01055 0-93
ug/L
TKN as IN 00625
mg/L
Ni - Nickel 01067
ug/L
�ttee(orAulhorized Agent) Name and ritle - Please print ortype
FIELD ANALYSES: AS DRY
at time of
pH OD400: NA units Temp. 00010: NA C sampling,
Spec. Cand. 00094. MA pS/CM2 check
here:
Odor 00085:
Appearance
Certification No. 652
Pb - Lead 01051 ug/L
Zn - Zinc 01092 mg1L
Other (Specify Compounds and Concentration Units):
Tetrachloroethene: 0.16 mg[L
Trichlaroethene: 0.0073 mgl
cis-1,2-D�rhloroethene: 0.0012 mg/I
trans-1,2-Dichlaroethene: Not Detected
Vinyl chloride: Not Detected
ORGANICS: (by GC, GCIMS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? [D Yes (1)
U No (0)
VOC 78732 method #
EPA 8260B
Total organic Carbon method #
EPA 531 OC
Sulfate method #
ASTM D516-90
Ammonia, sulfide, nitrate, nitrite , method # EPA 4500
ri 1'q1QA ­11 F-Mi tpnf Tot2l VOCS: 0
mg/L VOC Rernoval% 100
GW-59 Rev. 812013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print clearly or Type
PERMIT Number: Expiration Date: JIIY31.2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 L11C
NPDES Other
Permit Name (if different):
Facility Address: 8377Creedmoor Road Raleigh NC
27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Raleigh (SV-1) NC 27613 County Wake
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
r7
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87
Well Diameter- 2 in.
pH 00400: NA units Temp. 000io� NA oc
at time of
sampling,
Depth to Water Level 62546: NA ft. below measuring
point
Screened Interval: ­2­ft�
to 1111116"Ift.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478-90
ft.
Odor 000m:
here:
Volume of water pumped/bailed before sampling:
NA ___:g4le�minutes
Appearance
Ll
Samples for metals were collected unfiltered: ED
YES El
NO and field acidified: El YES
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18.12t2l-23,'2015
Laboratory Name: Con-teSt Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO,) as N 00615 0,0029J
mg/L
Pb - Lead 01051 ug1L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO,) as N 00620 Not[Detected
_mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note Uso MPN method for hIgNy turbid samples)
Orthophosphate 7C507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum ollo5
nrl
Tetra chl oroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ugIL
Trichloroethene: 0.0073 mg/i
TOC 00680
mg/L
Ca - Calcium cog16
mg/L
cis-1,2-Dichloroethene: 0.0012 nngil
Chloride 00940 _mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichicroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034 _ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552 _mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ugIL
(Specify test and method #. AT TACH LAB REPORT.)
Sulfate 00945 Not [)elected
mg/L
Hg - Mercury 71900
uglL
Lab Report Attached? El Yes (1) El No (0)
Specific Conductance 00095
pMhos
K - PotaSSiUM 00937 _mg/L
VOC 78732 - , method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammon73 Nitrogen; NHjas N;Amrtronia Nitrcgenjota')
Mn - Manganese 01055 0-93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOIDS: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Rierri 1uu
I& A LA-&-P
Perm ittee (or Authorized Ag ent) NameandTitle - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
L��DEPAIRTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Plione:919-807-6306
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: Jly 31. 2016
Facility Name: Former Pro Cleaners
Non -Discharge W00035324 UIC
NPDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC
27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Raleigh (sr�d) NC 27613 County Wake
fc'ry)
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
El
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
If WELL
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. ocoio: KIA C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 1-211ft.
to ­111-Ift.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
Odor 000m:
here:
Volume of water pumped/bailed before sampling:
NA __,��minutes
(to parameter stabiliZ2tion)
Appearance
Samples for metals were collected unfiltered: 0
YES F-1
N 0 and field acidified: El YES M
NO
LABORATORY INFORMATION
Date sample analyzed: 12il8,12121-2312015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 6-52
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg!L
Pb - Lead oim-, u 91L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
_mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: U�� MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentra'ion Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC omm 1.8
mg/L
Ca - Calcium oog16
mg/L
cis-1,2-Dir-hloroethene: 0.0012 mg!l
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans- 1, 2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 3273C
ug/L
Fe - Iron 01045 NA
ug1L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug[L
Lab Report Attached? 0 Yes (1) 0 No (0)
Specific Conductance 00095
[tMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 82605
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NH3as N;Ammonia Nitrogen.Total)
Min - Manganese oio55 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as IN 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: U mg!L VOC Removal% 'Llu
--S,
j !� Pc"—A-v-�
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number; Expiration Date: Ju�y 31, 2016
Facility Name: Former Pro Cleaners
Non -Discharge VVQ0035324 UIC
NPIDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 276113
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh NC
27613
County Wake
Lagoon Remediation: Infiltration Gallery
(sest"
Zp�
El
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cieaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WAS DRY
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
at time of
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. ocolo NA �C
sampling,
Depth to Water Level 82546: NA ft. below measuring point
Screened Interval: 111-1-2 ft.
to
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft, above land surface
Relative M.P. Elevation: 478-90
ft.
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA
gial!GRG minutes (to parameter stabilization)
Appearance
Samples for metals were collected unfiltered:
YES
NO and field acidified: 0 YES 23
NO
LABORATORY INFORMATION
Date sample analyzed: 12flB,12121-2312015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead o1o5i ug/L
Coliform: MF Fecal 31616_
1100ml-
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Alunninum 01105
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Tfthloroethene: 0.0073 m9i'l
TOC 00680
mg/L
Ca - Calcium oo916 _mg/L
cis-1,2-Dichloroethene: 0.0012 mg/l
Chloride 00940
mg/L
Cd - Cadmium 0-1027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
uglL
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
uglL
(Specify test and method #. ATTACH LAB REPORT)
Sulfate 00945 Not Detected
mglL
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) U No (0)
Specific Conductance 0009.5
uMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 5310C
(Ammonia Nitrogen; NHO is N; Ammonia Nitrogen. Total)
Min - Manganese 01055 0-93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0-13194 mg/L Effluent Total VOCs: U mg/L VOC Removal% 'uu
Fermittee (orAuthorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Cleanly or Type
PERMIT Number: Expiration Date: JJY31,2016
Facility Name: Former Pro Cleaners
Non-Disch2rge WQ0035324 UIC
NPDES — Other
-
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh fstl-(! NC
27613
County Wake
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
171
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87
Well Diameter: 2 i n.-
pH 0040C: NA units Temp. 000io: NA �c
at time of
sampling,
Depth to Water Level 82546- NA ft. below measuring
point
Screened Interval: ­r"'Ift.
to ­1111-Ift.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478-90
ft.
Odor 00085: -
here -
Volume of water pumped1bailed before sampling:
NA ___ja4aR,_minutes
Appearance
Samples for metals were collected unfiltered: D
YES 0
NO and field acidified: El YES 171
NO
LABORATORY INFORMATION
Date sample analyzed. 12/18.12/21-23/2015
Laboratory Name: Con -test Analytical
Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
l
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead olo5i ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620 NotDetected
_mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
11OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use l method for highly urtid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum oil o5
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) oo4o3
units
Ba - Barium 01,007
ug/L
Trichloroethene: 0.0073 mg1I
TOC oo68o 1.8
mg/L
Ca - Calcium oogiG
mg/L
cis-1,2-Dichloroethene: 0.0012 ri
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
u g/L
Vinyl chloride: No, Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
u glL
Lab Report Attached? El Yes (1) ID No (0)
Specific Conductance 00095
RMhos
K - Potassium 00937
mg/L
VOC 76732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; Nl N;Ammonia Nitrogenjotal)
Mn - Manganese olo55 0.93
u g/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 9IM07-6306
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: July3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge W00035324 UIC
NPDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh (SI-0 NC
27613
County Wake
El
Lagoon 13 Remediation: Infiltration Gallery
M " i"t'?�)
11
Spray Field M Remediation: P.rnp and Treat
Contact Person: Justin Ballard
Telephone#: [phone]
0
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump Other:
SAMPLING INFORMATION
If WELL
WAS DRY
WELL ID NUMBER (from Permit): EW-9 (formerly
IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA C
at time of
sampling,
Depth to Water Level 82546: NA ft, below measuring point
Screened Interval: 35'5­20�ft.
to iw"'s"'ft
Spec. Cond. OOOq4 NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA ____:ga4qR�_minutes
Appearance
Samples for metals were collected unfiltered: EE
YES El
NO and field acidified: El YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12118. 12/21-2312015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead oini ugIL
Coliform: M F Fecal 31616
/1 OOmL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
11OOmL
Phosphorus: Total as P 00665
mg/L
(No!e: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg1L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300_
mg/L
Al - Aluminum 01105
mg/L
Tetrachloroethene: 0. 16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
Trichloroethene: 0.0073 mg/I
TOC oo6so
mg/L
Ca - Calcium 00916 _mg/L
cis- 1, 2-Dich lorcethene: 0.0012 mg/I
Chloride 00940 _mg/L
Cd - Cadmium oio27
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and OiIS 00552
mg/L
Cu - Copper 01042 _mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug1L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg!L
Hg - Mercury 719CO
uglL
Lab Report Attached? 0 Yes (1) Q No (0)
Specific Conductance 00095
LtMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260 B
Total Ammonia 00610 Not [)elected
mg/L
Mg - Magnesium 00927 _mg/L
TCt21 Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055 0-93
ug1L
Sulfate - ASTM D516-90
method I
TKN as N 0:625
mg/L
Ni - Nickel 01067
u g1L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 mg/L Effluent Total VOCs: U mg/L VOC Removal% ''Ju —
Permittee (or AuthorizeC Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Pnnt Clearly or Type
PERMIT Number: ExPiration Date: J�Iy3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 — UIC
NPDES — Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Raleigh NC
27613
County Wake
Lagoon Remediation: Infiltration Gallery
El
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone#: [phone] - 99
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
r7
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected: 12/17/2015
FIELD ANALYSES:
If WELL
WAS DRY
Well Depth. 87
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA oc
at time of
sampling,
Depth to Water Level 82545: NA ft. below measuring
point
Screened Interval;
to
Spec. Cond. 00094: NA PS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor ooc85:
here:
Volume of water pumped/bailed before sampling:
NA __q�minutes
Appearance
Samples for metals were collected unfiltered: 3
YES El
N 0 and field acidified: C1 YES EI
N 0
LABORATORY INFORMATION
652
Date sample analyzed: 12)18,12/21-23120 ' 15
Laboratory Name. Con -test Analytical Laboratory
Certification No.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620 Not Detected
_mg1L
Zn - Zinc 01092 mg/L
Coliform: IVIF Total 3�,504
/1 OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum 01105
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
u g/L
Trichlorcethene: 0.0073 mg/I
TOC 00680 1-8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
uq1L
Chromium: Total 01034
ug/L
Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug1L
Fe - iron 01045 NA
ugIL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
uglL
Lab Report Attached? 0 Yes (1) 13 No (0)
Sppcific Conductance 00095
1AMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
_mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen: NH3asN;Ammonia Nitrogenjola!)
Mn - Manganese 01055 0-93
ug/L
Sulfate method # ASTM D516-90
TKN as N 03625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.113194 mg/L Effluent Total VOCs: U — mg/L VUG Renri luu
Permittee (or Authorized Agent) Name and Title - Please print or type
Signature 6fPXrn'liftee (or
GW-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
iF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING-
TER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
'ICE CENTER, RALEIGH, NIC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Ciparly or Type
PERMIT Number; Expiration Date: Jily3l.2016
Facility Name: Former Pro Cleaners
Non -Discharge WQ0035324 UIC
NPDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC
27613
TYPE
OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Raleigh NC 27613 County Wake
Spray Field Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephonet 919-871-0999
Rotary Distributor Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled:. 20
r7
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly
!W-9)
Date sample collected: 12/1712015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH X400: NA units Temp. 00010 NA C
at time of
sampling,
Depth to Water Level 82546: NA ft. below measuring
point
Screened Interval: 1`11-11ft.
to ­11-11�111ft.
Spec. Cond. 00094: NA pS/CM2
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft.
Odor 000w
here:
Volume of water pumped/bailed before sampling:
NA _____c�minutes
Appearance
Samples for metals were collected unfiltered: (I
YES El
NO and field acidified: Ll YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12121-2312015
Laboratory Name: Con -test Analytical Laboratory
Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite (NO.) as N 00615 0.0029J
mg/L
Pb - Lead oio5i ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620 Not Detected
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 NA
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids -.Total 70300 _mg1L
Al -Aluminum ollo5
mg/L
Tetrachloroethene: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
uq/L
Trichloroethene: 0.0073 mg/i
TOC 00680 1.8
mg/L
Ca - Calcium 00916
mg/L
cis-1,2-Dichloroethenei 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
ugIL
Chromium: Total 01034
uq1L
Vinyl cNoride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? El Yes (1) EI No (0)
Specific Conductance 00095_
I,LMhos
K - Potassium 00937
mg/L
VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L
Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen: NH� as N: Ammonia Nitrogen, Total)
Mn - Manganese m55 0.93
ug/L
Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
Ammonia, sulfide, nitrate, ritrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0-13194 _mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
BAL/LAZ��
Permittee, (or Authorized Agent) Name and Title - Please print or type
GIN-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
am
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��1617
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly
or Type
PERMIT Number: Expiration Date: July3l,2016
Facility Name: Former Pro Cleaners
Non -Discharge VVQC035324 UIC
NPDES Other
Permit Name (if different):
Facility Address: 8377 Creedmoor Road Raleigh NC 27613
TYPE OF PERMITTED OPERATION BEING MONITORED
Raleigh m11111) NC
27613
County Wake
El Lagoon EE Remediation: Infiltration Gallery
C'10
(Zio)
11 Spray Field M Remediation: Pump and Treat
Contact Person: Justin Ballard
Telephone* 919-871-0999
El Rotary Distributor El Land Application of Sludge
Well Location/Site Name: Former Pro Cleaners
No. of wells to be sampled: 20
Water Source Heat Pump 13 Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): EW-9 (formerly IW-9)
Date sample collected. 12/17/2015
FIELD ANALYSES:
WAS DRY
Well Depth: 87 ft.
Well Diameter: 2 in.
pH 00400: NA units Temp. 00010: NA C
at time of
Depth to Water Level 82546: NA ft. below measuring
point
Screened Interval: 1­1112ft.
to Spec. Cond. C0094: NA pS/CM2
sampling,
check
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: 478.90
ft. Odor 00085:
here:
Volume of water pumped/bailed before sampling:
NA _4ja�minutes
Appearance
Samples for metals were collected unfiltered:
YES El NO and field acidified: 0 YES El
NO
LABORATORY INFORMATION
Date sample analyzed: 12/18,12/21-2312015
Laboratory Name: Con -test Analytical
Laboratory Certification No. 652
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.0029J
mg/L Pb - Lead oio5i ug/L
Coliform: MF Fecal 31616
/1 OOmL
Nitrate (NO,) as N 00620 Not Detected
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665_
mg/L
(Note. Use MPN method for hioly turbid samples)
Orthophosphate 70507 NA
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg/L
Al -Aluminum oil o5
mg1L Tetra ch lo roethe ne: 0.16 mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L Trichlorcethene: 0.0073 mg/I
TOC 00680
mg/L
Ca - Calcium 009-6
mg/L cis-1,2-Dichloroethene: 0.0012 mg/I
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L trans-1,2-Dichloroethene: Not Detected
Arsenic 01002
u g/L
Chromium: Total 01034
ug/L Vinyl chloride: Not Detected
Grease and Oils 00552
mg/L
Cu - Copper 01042
_mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - iron 01045 NA
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 Not Detected
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ID Yes (1) 10 No (0)
Specific Conductance 00095
�tMhos
K - Potassium 00937
mg/L VOC 78732 method # EPA 8260B
Total Ammonia 00610 Not Detected
mg/L
Mg - Magnesium 00927
mg/L Total Organic Carbon method # EPA 531 OC
(Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55 0.93
ug/L Sulfate method # ASTM D516-90
TKN as N 00625
mg/L
Ni - Nickel 01067
ug[L Ammonia, sulfide, nitrate, nitrite method # EPA 4500
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.13194 . mg/L Effluent Total VOCs: 0 mg/L VOC Removal% 100
_::Y-<�7-/,J 8>4"JrO;'�
Permittee (OrAuthorized Agent) Name and Title - Please print or type
GW-59 Rev. 8/2013

Former Pro Cleaners
Permit No. WQ0035324
APPENDIX B
GW-59A COMPLIANCE REPORT FORM
February 22, 2016
Page 4

GW-59A COMPLUNCE REPORT FORM Permit # WQ0035324
(Submit one earl; itioniforing period with GJV-S9forms.)
Enter date monitoring results were due. ( 0/30/2015 ) Will this monitoring report (GW-59 and GW-59A)
_L_
YES
(�N�O
be submitted after the established due date?
2
IvVasany required information missing on the GNV-59 report forms?
�E
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
For water supply wells, well construction information is unavailable, including well diameter, depth, M.P. elevation, screened
interval, and depth to water.
3
Are anv of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
Y E S
Q_N
DO
identification plate, area overgrown, etc.)? Irthe ansiveris "Yes", contact the Regional 0giceforguidalice.
4
Are any monitored constituents equal to or above the established standards?
(Y_ E 7S
N- 0
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.- **ALL UNITS IN mg/L
MW-5: PCE(O.0038) MVV-16: PCE(O.006) MW-22S: PCE (0.0019)
MW-10B: PCE (0.08) MW-24S: PCE (0.0014) EVV-9: TCE (0,0073), PCE(O.16)
MVV-1 1A: PCE (0.0083) MW-24D: PCE (0.001) MW-12: PCE (0.00076)
EW-8 (formerly IW-8): Not sampled due to extraction pump not working at time of sampling event
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
(YES
-NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES" ' list in the space provided below. each well with constituent(s) exceeding
standards, concentration (s) reported, and sample collection date for each occurrence (for the last two years).
SEEATFACHED **ALL UNITS IN mg/L
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
QX E.
N- 0
if the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELYFOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
Wells located at or beyond the review boundary: MVV-5, MW-10A, MW-10B, MVV-1 1A, MVV-11B, MVV-16, MW-24S, EW-9
7
Is the permittee implementing previously approved actions required by the Division involving this
TE:�
No
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may b
reauired to determine the impact the waste disposal system is havina at the review and compliance
boundaries surroundinq this facility. Failure to do so maV subject the permittee to a Notice of Violation,
fines, andlor penalties.
In accordance with Groundwater Remediation Permit #WQ0035324, issued on April 16, 2012, a pump and treat system
was installed at the site in August 2012. Pilot scale operations began on August 29, 2012 and full scale operations began
on September 10, 2013. Pursuant to the permit, sampling of eleven pre -agreed upon monitoring wells will continue on a
quarterly basis. Note that Permit #WQ0035324 requests the sampling of twelve monitoring wells, however, one of these,
MW-4, was abandoned prior to 2008.
8
The person completing this porTion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
Signature of Permittee (or Authorized Agent) Date
GAV-59A 12/8/2003

GW-59A Question #5
MW-5: PCE — 12/16/2015 (0.0038), 9/17/2015 (0.0025), 6/16/2015 (0.0035), 3/19/2015
(0.0025), 12/18/2014 (0.0036), 9/25/2014 (0.0022), 6/18/14 (0.0012), 3/27/2014 (0.0014),
12/11/2013 (0.0033), 09/10/2013 (0.0041)
MW-10B: PCE — 12/15/2015 (0.08), 9/16/2015 (0.11), 6/18/2015 (0.11), 3/19/2015 (0.11),
12/18/2014 (0.18), 9/25/2014 (0.17), 6/18/14 (0.15), 3/27/2014 (0.19), 12/13/2013 (0.11),
09/12/2013 (0.046)
MW-11A: PCE — 12/15/2015 (0.0083), 9/17/2015 (0.0015), 6/18/2015 (0.002), 3/18/2015
(0.00086), 12/16/2014 (0.0012), (9/23/2014 (0.0033), 6/18/14 (0.0015), 3/26/2014 (0.00096),
09/12/2013 (0.0014), 05/29/2013 (0.0033)
MW-12: PCE — 12/17/2015 (0.0076), 9/16/2015 (0.00058), 6/17/2015 (0.00077), 3/20/2015
(0.00074)
MW-16: PCE — 12/15/2015 (0.006), 9/15/2015 (0.003), 6/18/2015 (0.0055), 3/19/2015
(0.0044), 12/18/2014 (0.0043), 9/25/2014 (0.0041), 6/18/14 (0.0019), 3/26/2014 (0.0024),
12/11/2013 (0.011), 09/10/2013 (0.0063), 05/30/2013 (0.0066)
MW-24S: PCE — 12/14/2015 (0.014), 9/15/2015 (0.0048), 6/15/2015 (0.021), 3/17/2015
(0.030), 12/17/2014 (0.038), 9/23/2014 (0.0.32), 6/16/14 (0.0099), 3/24/2014 (0.043),
12/10/2013 (0.0077), 09/10/2013 (0.004), 05/29/2013 (0.007)
MW-24D: PCE —12/16/2015 (0.001), 6/15/2015 (0.0012), 3/18/2015 (0.00090), 12/17/2014
(0.00078), 9/23/2014 (0.0.00087), 12/10/2013 (0.0014), 09/10/2013 (0.0021), 05/29/2013
(0.0016), 02/27/2013 (0.0015)
EW-8 (IW-8): PCE - 3/20/2015 (0.24), 12/18/14 (0.26), 9/25/2014 (0.29), 6/20/14 (0.28),
3/27/2014 (0.43), 12/11/2013 (0.47), 09/11/2013 (0.18), 05/30/2013 (0.093), 02/28/2013
(0.12), 11/30/12 (0.081); TCE - 9/25/2014 (0.0032J), 6/18/14 (0.0.0033J), 3/27/2014 (0.0040)
EW-9 (IW-9): PCE — 12/17/2015 (0.16), 9/15/2015 (0.099), 6/17/2015 (0.22), 12/18/2014 (0.2),
9/25/2014 (0.17), 3/27/2014 (0.32), 12/12/2013 (0.29), 09/11/2013 (0.087), 05/30/2013 (0.28),
02/28/2013 (0.31), 12/03/12 (0.31);TCE — 12/17/2015 (0.0073), 9/15/2015 (0.0035), 6/17/2015
(0.004), 12/18/2014 (0.0042), 3/27/2014 (0.0038), 02/28/2013 (0.0047), 12/03/12 (0.0052)

Former Pro Cleaners
Permit No. WQ0035324
APPENDIX C
ANALYTICAL DATA TABLES
February 22, 2016
Page 5

Table 1: Site Chronology
DSCA ID No.: DC920001
Chronology of Events
Instructions: Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility. Commence with the first date a problem was suspected and continue
through the most recent activity described in the current report.
Late 1994 or Early
A Phase I Environmental Site Assessment (ESA) was prepared by Smith Environmental Technologies (Smith). This
1995 (report not
provi
ESA identified Pro -Cleaners as a potential environmental concern.
A Phase H ESA was prepared by Smith. Three 2-inch monitoring wells (MW-1, MW-2, & MW-3) were installed at the
site and three hand auger borings (CS-01, CS-02, & CS-03) were advanced within the the former dry-cleaning location.
Groundwater samples collected from MW- I (located along the western wall of the building) indicated
June 1995
tetrachloroethylene (PCE) and trichloroethylene (TCE) at concentrations of 1,000 ppb and 24 ppb, respectively. The
average depth -to -groundwater was documented to be —29 feet bgs. PCE was detected in each of the soil borings
(advanced to 3 feet with samples collected from I foot bgs and at 3 feet bgs) at concentrations ranging from 240 ppb to
21 DDb.
An ESA was prepared by Southeastern Environmental Services, Inc. (SES). The field assessment included the
installation of four monitoring wells (MW-4 through MW-7), collection/analysis of shelby tube samples, and the
collection/analysis of groundwater samples. The four wells were installed to varying depths ranging from 68.5 feet bgs
(MW-5) to 70 feet bgs (MW-4, MW-6, & NM-7). Shelby tube samples were collected during the installation of MW-7
at depths of 29.5-31.5 feet bgs and 37.5-39.5 bgs and analyzed for vertical and horizontal hydraulic conductivity. The
analysis revealed horizontal and vertical hydraulic conductivities of 0.000091 cm/sec and 0.000018 cmi/sec, respectively,
December 1995
in the sample collected from above the water table; the analysis also revealed horizontal and vertical hydraulic
coinductivities of 0.0000 17 cm/sec and 0.0000079 crialsec, respectively, in the sample collected from below the water
table. Groundwater samples were also collected from five monitoring wells (MW-1 and MW-4 through MW-7) at the
site. PCE was detected in MW- 1 at a concentration of 34 10 ppb; PCE was detected in MW-4 at a concentration of 204
ppb; and, PCE was detected in MW-5, MW-6, MW-7 at concentrations ranging from 28 ppb to I I ppb. Groundwater
was also identified as a source for drinking water in the area of the site; a water supply well was identified approximately
250 feet north of the -ite
An ESA Addendum and Remedial Action Plan were prepared by SES and Walton Engineering (Walton). Two
additional monitoring wells were installed at the site: MW-8 was installed to a depth of 83 feet bgs and MW-9 was
installed to a depth of 63 feet bgs. Groundwater samples were collected from eight monitoring wells at the site. PCE
was detected in the samples collected from MW- 1 (2895 ppb), MW4 (663 ppb), and MW-8 (142 ppb). Samples
collected from MW-3, MW-5, MW-6 MW-7, and MW-9 did not contain PCE. Samples collected from MW- I and MW-
July 1996
4 included breakdown chlorinated compounds (TCE and cis-1,2-dichloroetylene [cis-1,2-DCE]). Water samples were
collected from three water supply wells; chlorinated solvents were not detected in these samples. The Remedial Action
Plan of this report discusses the implentation of several remedial technologies. The report concludes that the most
effective remediation technology for the site would be a combination of air sparging with vapor extraction. Design
schematics and operation and maintanence schedules were provided. The system became was installed and became
onerational on June 7- 1996
A Site Assessment Addendum was prepared by SES and Walton. Four additional monitoring wells were installed on the
north side of Strickland Road. Monitoring well MW-IOA was installed to a depth of 80 feet bgs; monitoring well MW-
IOB was installed at a depth of 45 feet bgs; MW-1 IA was installed to a depth of 104 feet bgs; and MW-1 1B was
installed to a depth of 35 feet bgs. PCE was detected in groundwater samples collected from MW-1 (1744 ppb), MW4
February 1997
(260 ppb), MW-5 (8.6 ppb), MW-7 (8.7 ppb), MW-8 (347 ppb), and MW-9 (2.2 ppb). Samples collected from MW-1,
MW4, and M`W-8 included breakdown chlorinated compounds (TCE and cis- 1,2-DCE). Chlorinated compounds were
not detected in MW-3, MW-6, MW-10A, MW-10B, MW-1 IA, MW-1 113, or the three residential water supply wells
sampled during this event. SES and Walton stated that the remediation system appeared to be reducing the solvent
concentrations in the s ree a
Hr Action Flan Addendum were prepared by SES and Walton. Six additional monitoring
A Site Assessment and?Ceorrective
wells (two were temporary and abandoned) were installed at the site. Monitoring well MW-8A was installed to a depth
ofl5lfeetbgs. Monitoring wells MW-12, MW-13, MW-14 (abandoned), NM-15 (abandoned), and NM-16 were
installed to a depth of 40 feet Laboratory analysis of groundwater samples revealed the presence of PCE in MW-1
(3380 ppb), MW4 (50.6 ppb), MW-5 (4.4 ppb), MW-7 (1.9 ppb), MW-8 (194 ppb), MW-8A (271 ppb), MW-9 (2.4
April 1997
ppb), NTW-14 (10 ppb), NIW-15 (29.6 ppb) and MW-16 (43.0 ppb). Breakdown chlorinated compounds were also
detected in MW-1, MW-8, MW-8A, and MW-15. Chlorinated solvents were not detected in MW-3, MW-10A, MW-
10B, MW-1 1A, MW-11B, MW-13, or the three residential water supply wells sampled during this event. Chlorinated
compounds were not detected in the soil samples collected during the installation of MW- 12, MW- 13, and MW- 14 from
20 feet bgs. Slug testing at the site during this assessment indicated an average hydraulic conductivity of 0.00067
cm/sec in the intermediate zones and 0.000425 in the deep zone. Two additional air sparge wells were constructed north
lof MW-8
pa'-'e I of(,

Table 1: Site Chronology
DSCA ID No'.-: DC920001
Chronology of Events
Instructions: Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility. Commence with the first date a problem was suspected and continue
through the mc, recent activity described in the current report.
A Final Corrective Action Plan Addendum was prepared by SES and Walton. This addendum was prepared to address
September 1997
concerns of the NCDENR regarding the off -site migration of the plume to the southwest and other various technical and
administrative issues.
A Groundwater Momtonng Report was prepared by SES and Walton. Monitoring well MW- 17 was sampled for the first
time during this sampling event, however a discussion regarding the installation was not provided. Groundwater
samples were collected from 18 monitoring wells and three water supply wells. Concentrations of chlorinated
March 1998
compounds increased drastically in samples collected from MWA. No significant changes in contaminant
concentrations were observed in samples collected from MW4 or noted for the remainder of the mornitoring wells or
water supply wells. It was noted in this report that Pro -Cleaners moved to another tenant space within Towne North
ShoDoing Center and dry-cleaning omrations ceased on the property.
An Active Remediation Groundwater Monitoring Report was prepared by SES and Walton. Groundwater samples were
June 1998
collected from 18 monitoring wells, three water supply wells, and one private utility supply well. Concentrations of
chlorinated compounds continued to show increasing values in MW-I. Additionally, samples collected from MW-8,
MW-8A, and MW-10A also showed increased concentrations of chlorinated comDounds.
An Active Remediation Groundwater Monitoring Report was prepared by SES and Walton. Groundwater samples were
January 1999
collected from 15 monitoring wells and three private water supply wells. The results revealed a decrease in
concentration of chlorinated compounds from the previous sampling event.
An Assessment Addendum and Active Remediation Groundwater Monitoring Report was prepared by SES and Walton.
Three temporary monitoring wells were installed (MW-18, MW-19, and MW-20). Monitoring well MW-18 was
April 1999
abandoned based on the analytical data; wells MW-19 and MW-20 were made permanent. Groundwater samples were
collected from 18 monitoring wells and three water supply wells. ne plume geometry remained unchanged and volatile
organic compounds (VOCs) were not detected in the samples collected from the three water supply wells.
An Active Remediation Groundwater Monitoring Report was prepared by SES and Walton. Groundwater samples were
August 1999
collected from 15 monitoring wells and three private water supply wells. The results indicated an unchanged plume
geometry and increase in concentrations in samples collected from monitoring wells MW-1013 and MW-I 113; VOCs
were not detected in the samples collected from the three water supply wells.
An Active Remediation Groundwater Monitoring Report was prepared by SES and Walton. Groundwater samples were
December 1999
collected from 15 monitoring wells and three water supply wells. The results indicated a narrowing of the groundwater
plume and unstable concentrations in samples collected from MW-1013 and MW-I 113; VOCs were not detected in the
samples collecteedd from tmhe three water supply wells.
An Active Remediation Groundwater Monitoring Report was prepared by SES and Walton. Groundwater samples were
collected from 15 monitoring wells and three water supply wells. The results indicated stable plume geometry and
May 2000
concentrations from the samples were generally consistant with the previous sampling event. The sample from the water
supply well located at 8401 Azalea contained a low concentration (1. 16 ppb) of 1,2,4-trimethyl benzene. No other
VOCs were detected in the samples collected from the three water supply wells.
An Active Remediation Groundwater Monitoring Report was prepared by SES and Walton. Groundwater samples were
October 2000
collected from 15 monitoring wells and three water supply wells. The results indicated stable plume geometry and
concentrations from the samples were either decreased or stable; VOCs were not detected in the samples collected from
the three water sunDly wells.
An Active Remediation and Groundwater Monitoring Report was prepared by SES and Walton. Groundwater samples
April 2001
were collected from 17 monitoring wells and three water supply wells. The results indicated stable plume geometry and
contaminant concentrations; VOCs were not detected in the samples collected from the three water supply wells.
August 2001
Northridge Partners filed a Petition for Certification of the site into the DSCA Program.
October 2001
The air sparge/soil vapor extraction system was taken out of service.
December 2001
The site was certified into the DSCA program.
A Groundwater Monitoring Report was prepared by MACTEC Engineering and Consulting, Inc. (MACTEC).
Groundwater samples were collected from ten monitoring wells and three water supply wells. The results indicated
October 2003
stable plume geometry and varying (increasing to the south-southwest and decreasing in the source and north of the
source area) concentrations of VOCs. TCE and cis-1,2-DCE were detected in the sample collected from the water
supply well located at 8400 Camellia Drive; VOCs were not detected in the samples collected from the other water
I supply wells.
December 2004
1 An Administrative Agreement for State -Directed Assessment and Remediation under the DSCA Program was executed.
Page 2 of6

Table 1: Site Chronology
DSCA ID No.: -DC920001
Chronology of Events
Instructions: Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility. Commence with the first date a problem was suspected and continue
through the mo, recent activity described in the current report.
A Groundwater Monitoring Report was prepared by MACTEC. Groundwater samples were collected from 16
monitoring wells and tIrree water supply wells. The results indicated stable plume geometry and varying concentations
April 2005
in samples collected from the monitoring wells. Contaminant concentrations increased in the sample collected from
8400 Camellia Drive� the remaining two water supply wells did not contain VOCs.
A Report of Water Supply Well Sampling Event was prepared by Engineering Consulting Services, Ltd. (ECS).
Groundwater samples were collected from ten water supply wells. No chlorinated compounds were detected in the
samples collected.
October 2005
Towne North Shopping Center, LLC purchased the Towne North Shopping Center property and became a DSCA
petitioner.
A Report of Soil Assessment and Groundwater Monitoring was prepared by MACTEC. Soil samples were collected
from soil borings S- I through S- 16 and from the boring associated with the installation of MW- I d; the soil samples were
collected from varying depths. The results indicated high concentrations ofPCE in soil outside the building in the area
of the rear door and along the sewer and water lines near the rear of the facility. One Type-11 monitoring well (MW-21)
Aprd 2006
was installed to replace MW-20; one Type -HI monitoring well (MW- I d) was installed immediately downgradient of the
sourcearea. Monitoring wells MW-6 and MW-20 were abandoned. Groundwater samples were collected from 12
monitoring wells and 18 water supply wells. 71be results indicated stable plume geometry and generally increasing
contaminant concentrations. The sample collected from the water supply well located at 8400 Camellia Drive contained
TCE and cis-1,2-DCE. The sample collected from the water supply well at 8404 Camellia Drive contained cis-1,2-DCE.
No other samples contained chlorinated solvent compounds.
A Report of Groundwater Monitoring was preapared by MACTEC. Groundwater samples were collected from I I
October 2006
momtoring wells and four water supply wells. The results indicated generally increasing contaminant concentrations in
the monitoring wells and the water supply well located at 8400 Camellia Drive. The remaining three water supply wells
sampled did not contain chlorinated solvent compounds.
June 2007
Towne North, LLC purchased the Towne North Shopping Center property.
June 2007
A Building Exterior Assessment was conducted by MACTEC. The report indicates that MACTEC was unable to detect
anv new distresses to the exterior of the facility after the excavation, which is discussed below.
A L r Report of Environmental Services was prepared by MACTEC. A soil excavation was conducted in June of
2007. A total of90.59 tons ofsoil were excavated from the site. Two soil samples (B-I & B-2) were collected from the
July 2007
base ofthe excavation. Sample B-2 contained 0.0087 ppm ofPCE based on laboratory analysis; sample B-I did not
contain PCE above a concentration ofO.001 1 ppm. The soil was transported to and disposed at Wayne Disposal, Inc. in
Belleville, Michigan.
A Water Supply Well Abandonment Report was prepared by ATC. Water supply wells were abandoned in accordance
November 2007
with applicable rules at 8400 Camellia Drive, 8401 Azalea Drive, and 8400 Azalea Drive. These residences had been
vreviouslv connected to City of Raleigh public water.
ATC collected groundwater samples from seven monitoring wells and 17 water supply wells. PCE was detected above
December 2007
2L Standards in samples collected from monitoring wells MW-8B and MW-16. Chlorinated compounds were detected
in samples collected from water supply wells located at 8404, 8408, and 9405 Camellia Drive below 2L Standards.
ATC collected groundwater samples from six monitoring wells and three water supply wells. PCE was detected above
March 2008
2L Standards in samples collected from monitoring wells MW-5, MW-17, and MW-10B. Chlorinated compounds were
detected in samples collected from water supply wells located at 8404, 8408, and 9405 Camellia Drive below 2L
Standards.
ATC collected groundwater samples from seven monitoring wells and three water supply wells. PCE was detected
June 2008
above 2L Standards in samples collected from monitoring wells MW-8B and MW-16. Chlorinated compounds were
detected in samples collected from water supply wells located at 8404 Camellia Drive below 2L Standards.
ATC collected groundwater samples from six monitoring wells and three water supply wells. PCE was detected above
September/October
2L Standards in samples collected from monitoring wells MW-5, MW-17, and MW-1013. Chlorinated compounds were
2008
detected in samples collected from water supply wells located at 8404, 8408, and 8405 Camellia Drive below 2L
Standards.
Monitoring wells MW-22S, MW-22D, and MW-23 and injection wells IW-1, IW-2, IW-3, IW-4, IW-5, fW-6, fW-7, IW-
November 2008
8, IW-9, and IW-10 were installed. ATC collected groundwater samples from eight monitoring wells. PCEwas
detected above 2L Standards in MW-5, MW-8B, MW- I OB, MW- 16, MW-22S, and MW-2 3.
December 2008
ATC collected groundwater samples from six monitoring wells. PCE was detected above the 2L Standard in MW-22S,
MW-23, IW-3, IW4, and rW-5.
January 2009
A pilot injection for enhanced reductive dechlorination was conducted. ABC+ was injected into IW-I and IW-2.
ATC collected groundwater samples from 12 monitoring wells and 17 water supply wells. PCE was detected in MW-5,
February 2009
MW-8B,MW-IOB,MW-16,MW-22S,MW-23, RV-3, IW4, and IW-5 at concentrations greater than the 2L Standard.
Chlorinated compounds were detected in samples collected from water supply well located at 8405 Camellia Drive
below the 2L Standards.
Page 3 of 6

Fable 1: Site Chronology
DSCA ID No.: DC920001
Chronology of Events
Instructions: Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility. Commence with the first date a problem was suspected and continue
through the mo recent activity described in the current report.
ATC collected groundwater samples from I I monitoring wells and three water supply wells. PCE was detected in MW-
April 2009
5, MW-813, MW- I OB, MW-16, MW-22S, MW-22D, MW-23, IW-3, IW4, and IW-5 at concentrations greater than the
2L Standard. Chlorinated compounds were detected in samples collected from water supply wells located at 8404 and
8408 Camellia Drive below 2L Standards.
ATC collected groundwater samples from 18 monitoring wells and 17 water supply wells. PCE was detected in MW-5,
July 2009
MW-813, MW-16, MW-17, MW-22S, MW-23, IW-3, IW4, and IW-5 at concentrations greater than the 2L Standard.
Chlorinated compounds were detected in samples collected from water supply wells located at 8404, 8408, and 8409
Camellia Drive below 2L Standards.
September 2009
ATC collected groundwater samples from eight monitoring wells. PCE was detected in MW-22S, MW-23, IW-1, IW-6,
IW-7, IW-8, and IW-9 at concentrations greater than the 2L Standard.
ATC collected groundwater samples from 12 monitoring wells and three water supply wells. PCE was detected in MW-
October 2009
5, MW-8B, MW-10A, MW-1013, MW-16, MW-22S, MW-23, IW-3, IW4, and rW-5 at concentrations greater than 2L
Standard. Chlorinated compounds were detected in samples collected from water supply wells located at 8404 and 8408
Camellia Drive below 2L Standards.
ATC conducted an air sampling event. The scope included the collection of air samples Indoor #1, Indoor #2 and an
January 2010
outdoor air sample. It also included the collection of sub -slab soil gas samples SGMP 4 1 and SGMP #2. The results of
the air sampling indicated no exceedances of the risk levels considered acceptable by the DSCA Program.
February 2010
ATC prepared an Injection Evaluation Report and a Groundwater Monitoring Report documenting sampling activities
from October 2008 to October 2009.
ATC collected groundwater samples firom 18 monitoring wells and 14 water supply wells. PCE was detected in MW-5,
February 2010
MW-813, MW-9, MW-1013, MW-16, MW-17, MW-22S, MW-23, IW-3, IW-4, and fW-5 at concentrations greater than
the 2L Standard. Chlorinated compounds were detected in samples collected from water supply wells located at 8404,
8405, and 8408 Camellia Drive below the 2L Standards.
ATC collected groundwater samples from 12 monitoring wells and three water supply wells. PCE was detected in MW-
April 2010
5 MW-813, MW-1013, MW-16, MW-22S, MW-23, IW-3, IW-4, and fW-5 at concentrations greater than the 2L
Si;�dard. Chlorinated compounds were detected in samples collected from water supply wells located at 8404 and 8408
Camellia Drive below the 2L Standards.
ATC collected groundwater samples from 21 monitoring wells and 10 water supply wells. PCE was detected in MW-
July 2010
813, MW- 16, MW-2 1, and MW-23 at concentrations greater than the 2L Standard. Chlorinated compounds were
detected in samples collected from water supply wells located at 8404, 8408, and 9409 Camellia Drive below the 2L
Standards.
August 20 10
ATC prepared a Soil Gas and Air Sampling Report documenting the January 20 10 vapor intrusion sampling.
ATC collected groundwater samples from 12 monitoring wells and three water supply wells. PCE was detected in MW-
October 20 10
5, MW-8B, MW-10B, MW-1 IA, MW-16, MW-22S, MW-23, IW-3, IW-4, and IW-5 at concentrations greater than the
2L Standard.
January 2011
ATC submitted an annual Groundwater Monitoring Report documenting groundwater sampling events conducted in
February 20 10, April 20 10, July 2010, and October 20 10.
ATC collected groundwater samples from 9 monitoring wells and 12 water supply wells. PCE was detected in MW-813,
MW-16, MW-21, and MW-23 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in
April 2011
samples collected from water supply wells located at 8404, 8405, 8408, and 8409 Camellia Drive and 8405 Azalea Place
below the 2L Standards. TCE, 1,2-dichloroethane, and carbon tetrachloride were detected in the water supply well
located at 9404 Azalea Place at concentrations greater than the 2L Standards.
ATC collected groundwater samples from 7 monitoring wells and 5 water supply wells. PCE was detected in MW-5,
MW-1013, and W-22S at concentrations greater than the 2L Standard. Chlorinated compounds were detected in
July 2011
samples collected from water supply wells located at 8405, 8408, and 8409 Camellia Drive below the 2L Standards.
PCE was detected in the water supply well located at 8404 Camellia Drive at a concentration greater than the 2L
Standard.
ATC collected groundwater samples from 8 monitoring wells and 9 water supply wells. PCE was detected in MW-813,
October/November
MW-1013, and MW-23 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in
2011
samples collected from water supply wells located at 8405 Azalea Place and 9404, 8405, 8408, and 8409 Camellia Drive
below the 2L Standards.
ATC collected groundwater samples from 10 monitoring wells, 2 injection wells and 5 water supply wells. PCE was
January/FebruaTy
detected in MW-5, MW-10B, MW-I IA, MW-16, MW-22S, MW-24S, MW-24D, IW-8, and RV-9 at concentrations
2012
greater than the 2L Standard. cis-1,2-DCE was detected in the sample collected from the water supply well located at
8409 Camellia Drive below the 2L Standards. PCE was detected in the sample collected from the water supply well
located at 8404 Camellia Drive at a concentration greater than the 2L Standard.
April 2012
ATC submitted an annual Groundwater Monitoring Report documenting groundwater sampling events conducted in
,April 2011, July 2011, November 2011, and February 2012.
pril 2012
lGroundwater Remediation Permit #WQ0035324 was issued by NCDENR on April 16,2012.
Page 4 of 6

Table 1: Site ChronologN
DSCA ID No.: 1)('920001
Chronology of Events
Instructions: Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility. Commence with the first date a problem was suspected and continue
through the most recent activity described in the current report.
ATC collected groundwater samples from 15 monitoring wells and 9 water supply wells. PCE was detected in MW-5,
July 2012
MW-813, MW-1013, MW-16, MW-22S, MW-23, MW-24S, MW-24D, IW4, RV-5, IW-8, and IW-9 at concentrations
greater than the 2L Standard. Chlorinated compounds were detected in samples collected from water supply wells
located at 8404 Azalea Place and 8405, 8408, and 8409 Camellia Drive below the 2L Standards.
July/August 2012
ATC supervised the installation of an In Situ Delivery (ISDTM) System for the injection of CarBstratem. The system
became operational on Wednesday, August 28, 2012.
August 2012
ATC began pilot phase activities on August 28, 2012. During the pilot phase, wells fW-I and IW-3 were used for
injection and well EW-2 was used for extraction.
ATC collected groundwater samples from 13 monitoring wells and 7 water supply wells. PCE was detected in MW-5,
November/
MW-813, MW-1013, MW-I IA, MW-16, MW-22S, MW-23, MW-24S, MW-24D, fW-4, IW-5, IW-8, and IW-9 at
December 2012
concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples collected from water
supply wells located at 8405 Azalea Place and 8404, 8405, 8408, and 8409 Camellia Drive below the 2L Standards.
ATC collected groundwater samples from 15 monitoring wells and 10 water supply wells. PCE was detected in MW-
813, MW-I 1A, MW-22S, MW-23, MW-24S, MW-24D, IW-4, IW-5, IW-8, and IW-9 at concentrations greater than the
February 2013
2L Standard. Chlorinated compounds were detected in samples collected from water supply wells located at 8405
Azalea Place and 9404, 8405, 8408, 8409, and 8412 Camellia Drive below the 2L Standards. Naphthalene was detected
in samples collected from water supply wells located at 8408 Azalea Place and 9401, 8404, 8412, and 8413 Camellia
Drive below the 2L Standards. On February 25, 2013, the pilot phase of the recirculation system was terminated.
February 2013
On February 25, 2013, pilot phase activities for the recirculation system were terminated.
May 2013
ATC collected Crawlspace Air #3.
ATC collected groundwater samples from 15 monitoring wells and 7 water supply wells. PCE was detected in MW-5,
MW-813, MW-1013, MW-1 1A, MW-16, MW-22S, MW-23, MW-24S, MW-24D, IW-4, lW-5, rW-8, and IW-9 at
May 2013
concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples collected from water
supply wells located at 8404 and 8405 Azalea Place and 8401, 8404, 8405, 9408 and 8409 Camellia Drive below the 2L
Standards. Naphthalene was detected in the sample collected from the water supply well located at 8401 Camellia Drive
below the 2L Standards.
August 2013
ATC submitted a Residential Indoor Air Sampling Report documenting the sampling of Crawlspace Air #3.
ATC collected groundwater samples from 15 monitoring wells and 10 water supply wells. PCE was detected in MW-5,
MW-813, MW-1013, MW-1 1A, MW-16, MW-22S, MW-23, MW-24S, MW-24D, IW4, IW-5, IW-8, and IW-9 at
concentrations greater than the 2L Standard. Concentrations TCE in MW-23 and bromodichloromethane in IW-5 were
September 2013
also detected above 2L Standards. Chlorinated compounds were detected in samples collected from water supply wells
located at 8404, 8405, and 8408 Azalea Place and 8404, 8405, 8408, 8409, 8412, and 8413 Camellia Drive below the 2L
Standards. Carbon tetrachloride and 1,2-dichloroethane were detected in the sample collected from the water supply well
located at 8408 Camellia Drive above the 2L Standards.
ATC supervised the implementation of full-scale activities for the ISDTm system for the continued injection of
September 2013
CarBstrateTm. The system became operational on Tuesday, September 10, 2013. During ftill-scale activities, wells IW-
IA, IW-2, TW-3, IW-4, IW-5A, TW-6, and fW-7A were used for injection and wells EW-8, EW-9, and EW-1 0 were used
for extraction.
ATC collected groundwater samples from I I monitoring wells, 2 injection wells, 2 extraction wells and 7 water supply
wells. PCE was detected inMW-5, MW-813, MW-1013, W-16,MW-22S,MW-23, MW-24S, MW-24D, IW-5, IW-7,
December 2013
EW-8, and EW-9 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples
collected from water supply wells located at 8404, and 8405 Azalea Place and 8404, 8405, 8408, and 8409 Camellia
Drive below the 2L Standards.
December 2013
ATC submitted an annual Groundwater Monitoring Report documenting groundwater sampling events conducted in July
2012, November 2012, February 2013, May 2013, and September 2013.
January 2014
ATC collected indoor air samples Indoor #I and Indoor #2.
ATC collected groundwater samples from 11 monitoring wells, 2 injection wells, 2 extraction wells and 9 water supply
wells. PCE was detected in MW-5, MW-8B, MW-1013, MW-I 1A, MW-16, MW-22S, MW-24S, IW-5, IW-7, EW-8,
March 2014
and EW-9 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples collected
from water supply wells located at 8404, and 8405 Azalea Place and 8404, 8405, 8408, 8409, 8412, and 8413 Camellia
Drive below the 2L Standards.
ATC collected groundwater samples from I I monitoring wells, 2 injection wells, 2 extraction wells and 9 water supply
wells. PCE was detected in MW-5, MW-813, MW-1013, MW-I IA, MW-16, MW-22S, MW-24S, IW-5, IW-7, and EW-8
June 2014
at concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples collected from water
supply wells located at 8404 and 8405 Azalea Place and 8404, 8405, 8408, and 8409 Camellia Drive below the 2L
Standards.
August 2014
1ATC collected indoor air samples Indoor #1 and Indoor #2.
Page 5 of 6

Table 1: Site ChronologN
DSCA ID No.: DC920001
Chronology of Events
Instructions: Brief description of all significant events that have occurred since a problem was
Date
suspected at the facility. Commence with the first date a problem was suspected and continue
through the mo recent activity described in the current report.
ATC collected groundwater samples from 12 monitoring wells, 2 injection wells, 2 extraction wells and 10 water supply
wells. PCE was detected in MW-5, MW-813, MW-10B, MW-11A, MW-16, MW-22S, MW-24S, MW-24D, IW-7, EW-8
September 2014
and EW-9 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples collected
from water supply wells located at 8404, 8405, 9408 Azalea Place and 9404, 8405, 8408, 8409, 8412, and 9413
Camellia Drive below the 2L Standards.
October 2014
ATC submitted an Indoor Air Sampling Report documenting the sampling of Indoor #I and Indoor #2 during the winter
and summer months of 2014.
ATC collected groundwater samples from 12 monitoring wells, I injection well, 2 extraction wells, and 7 water supply
wells. PCE was detected in MW-5, MW-813, MW-1013, MW-IIA, MW-16, MW-22S, MW-24S, MW-24D, EW-8, and
December 2014
EW-9 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples collected from
water supply wells located at 8404 and 8405 Azalea Place and 8404, 8405, 8408, and 8409 Camellia Drive below the 2L
Standards.
ATC collected groundwater samples from 13 monitoring wells, 2 (previously used) injection wells, I extraction well,
and 10 water supply wells. PCE was detected in MW-5, MW-813, MW-1013, MW-1 IA, MW-12, MW-16, MW-22S,
March 2015
MW-24S, MW-24D, IW-7, EW-8 and EW-9 at concentrations greater than the 2L Standard- Chlorinated compounds
were detected in samples collected from water supply wells located at 8404 and 8405 Azalea Place and 8404, 8405,
8408, and 8409 Camellia Drive below the 2L Standards.
ATC collected groundwater samples from 13 monitoring wells, 2 (previously used) injection wells, I extraction well,
and 7 water supply wells. PCE was detected in MW-5, MW-813, T�ff-1013, MW-11A, MW-12, MW-16, W-22S, MW-
June 2015
24S, MW-24D, IW-7, and EW-9 at concentrations greater than the 2L Standard. Chlorinated compounds were detected
in samples collected from water supply wells located at 8405 Azalea Place and 8404, 8405, 8408, and 8409 Camellia
Drive below the 2L Standards.
ATC collected groundwater samples firom 13 monitoring wells, 2 (previously used) injection wells, I extraction well,
and I I water supply wells. PCE was detected in MW-5, MW-813, MW-1013, MW-I IA, MW-16, MW-22S, MW-24S'
September 2015
EW-9, and IW-7 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples
collected from water supply wells located at 8405 Azalea Place and 8404, 8405, 8408, 8409, and 8412 Camellia Drive
below the 2L Standards.
ATC collected groundwater samples from 10 monitoring wells, 2 (previously used) injection wells, I extraction well,
and 7 water supply wells. PCE was detected in MW-5, MW-813, MW-1013, MW-IIA, MW-12, MW-IMW-24S, MW-
December 2015
24D, and EW-9 at concentrations greater than the 2L Standard. Chlorinated compounds were detected in samples
collected from water supply wells located at 8405 Azalea Place and 8404, 8405, and 8408 Camellia Drive below the 2L
-Standards.
Page 6 of 6

Table 6: Monitoring Well Construction Data
DSCA ID No.: DC920001 AL
Well ID
Date Installed
(mm/dd/yy)
Number of Samples
Well Depth
[feet]
Well Diameter
[inch]
Screen Interval
[feet]
Status
(Active/Inactive)
MW-1
5/1/95
20
36
2
26-36
Abandoned
MW-ID
11111105
2
140
2
130-140
Not Locatable
MW-2
6/1/95
1
28
2
18-28
Abandoned
NW-3
6/l/95
12
40
2
30-40
Active
NM-4
II/l/95
19
70
2
65-70
Abandoned
MW-5
II/l/95
43
68.5
2
63.5-68.5
Active
MW-6
Il/l/95
3
70
2
65-70
Destroyed
MW-7
II/l/95
24
70
2
65-70
Active
MW-8A
3/13/97
20
148
2
138-148
Active
MW-813
3/2/96
46
83
2
73-83
Active
MW-9
3/3/96
25
63
2
53-63
Active
MW-IOA
1/16/97
41
80
2
75-80
Active
MW-1013
1/16/97
48
45
2
25-45
Active
MW-IIA
I/l/97
44
105
2
100-105
Active
MW-IIB
I/l/97
23
35
2
25-35
Active
MW-12
3/11/97
20
40
2
3040
Active
MW-13
3/11/97
16
40
2
20-40
Active
MW-14
3/11/97
1
To
2
20-40
Abandoned
MW-15
3/12/97
1
40
2
20-40
Abandoned
NM-16
3/13/97
43
40
2
2040
Active
Nff-17
9/25/97
20
40
2
2040
Active
MW-18
3/30/99
1
35
2
30-35
Abandoned
MW-19
3/31/99
6
35
2
30-35
Not Locatable
MW-20
3/31/99
8
35
2
30-35
Abandoned
MW-21
11110105
9
28
2
13-28
Active
MW-22S
11/5/08
26
45
1
30-45
Active
MW-22D
11/5/08
24
85
1
80-85
Active
NM-23
11/4/08
26
2
30-45
Active
MW-24S
2MI2
14
50
1
30-50
Active
MW-24D
2n1l2
14
83
2
73-83
Active
Iw-I
11/3/08
2
47
2
29-39,4547
Inactive
IW-IA
7/27/13
0
47
4
29-39, 45-47
Active
IW-2
11/6/08
0
67
2
35-50, 54-60, 65-67
Active
IW-3
11/5/08
8
47
2
27-47
Active
IW4
11/11/08
14
87
2
3045, 55-60, 75-87
Active
IW-5
11/13/08
22
87
2
35-60, 70-87
Inactive
IW-5A
7/27/13
0
87
4
35-60, 70-87
Active
IW-6
11/14/08
1
87
2
40-50, 60-87
Active
IW-7
11/6/08
7
87
2
35-50, 60-70, 80-87
Inactive
IW-7A
7/27/13
0
87
4
35-50, 60-70, 80-87
Active
*EW-8
11/12/08
13
87
2
30-55, 60-65, 75-87
Active
*EW-9
11/11/08
14
87
2
3545, 50-57, 62-67, 72-
87
Active
*EW:10
11/17/08
1 2
1 87
1 2
30-55, 60-75, 80-87
Active
I*Formerly injection well (M).
Page I of I

Table 7: Groundwater Elevation Data
Groundwater
Sampling Point
Sampling Date
(ni-/dd/yy)
TOC Elevation
Ifeet]
Depth to Water
[feet bgs]
Groundwater
Elevation
Ifeet]
Depth to NAPL
Ifeet b9s]
NAPL Thickness
Ifeet]
Correcte
Groundwater
Elevation
MW-1
11/13/95
477 12
31.16
446.16
NA
NA
NA
4/18/96
29.40
447.92
NA
NA
NA
616/96
28.45
448.87
NA
NA
NA
6/20/96
27.95
449.47
NA
NA
NA
4/1/99
27.96
449.46
NA
NA
NA
10/19,99
28.50
448.82
NA_
NA
NA
3114100
27.70
449.62
NA
NA
NA
9/12/03
27.60
449.72
NA
NA
NA
3/9/05
25.42
451.90
NA
NA
NA
12/9/05
29.81
447.51
NA
NA
NA
8/8/06
29.82
447.50
NA
NA
NA
MW-ID
12/9105
477 63,
31.34
446.29
NA
NA
NA
9/8/06
6.12
471.51
NA
NA
NA
MW-2
11/13/95
21.90
71.08
NA
NA
NA
MW.3
11/13/95
479104
3L52
447.52
NA
NA
NA
4/18/96
30M
448.92
NA
NA
NA
6/6/96
29.67
449.37
NA
NA
NA
6/20/96
29.55
449.49
NA
NA
NA
4/1/99
28.15
450.89
NA
NA
NA
10/19,99
28.76
45019
NA
NA
NA
9/12/03
27.41
451.63
NA
NA
3NI05
28.97
450.07
NA
NA
-NA
NA
12/9105
30.27
448.77
NA
NA
NA
918/06
30.19
448.85
NA
NA
NA
3/11/08
32.07
446�97
NA
NA
NA
9/9/08
32.00
447.04
NA
NA
NA
1019/08
31.73
447.31
NA
NA
NA
I OMD9
31.05
447.99
NA
NA
NA
212/10
30.85
448.19
NA
NA
NA
7/13/10
29a5O
449.54
NA
NA
NA
10119/10
29.71
449.33
1 NA
NA
NA
4/25/11
30.99
448mO5
NA
NA
NA
7/26111
3L18
447.86
NA
NA
NA
11/1111
31.65
447.39
NA
NA
NA
1/25/12
32.15
446.89
NA
NA
NA
7/17/12
31.92
447.12
NA
NA
NA
11/28/12
32.41
446.63
NA
NA
NA
2125/13
32.66
446.38
NA
NA
NA
5/28/13
31.68
447.36
NA
NA
NA
9/9/13
30.30
44&74
NA
NA
NA
12/9/13
3L69
447.35
NA
NA
NA
3/24/14
31.56
447.48
NA
NA
NA
6116/14
30.28
448.76
NA
NA
NA
9/22/14
X04
449000
NA
NA
NA
12/15/14
30.33
448.71
NA
NA
NA
3/16/15
2 .78
449.26
NA
NA
NA
6115/15
29.04
450.00
NA
NA
NA
9/14/15
29,39
449.65
NA
NA
NA
12/14/15
29+26
449w7g
NA
NA
NA
1 %V4
11/13M
477 1"
3LO5
445.97
NA
NA
NA
4/19/96
29.22
447.90
NA
NA
NA
6/6/96
28.34
448.69
NA
NA
NA
6/20/96
57.79
419.23
NA
NA
NA
4/1/99
27.67
449.35
NA
NA
NA
10/19/99
28.11
448.91
NA
NA
NA
3/14/00
27.67
449.35
NA
NA
lq�-
9/12103
27.52
449�50
NA
NA
NA
3/14/05
28.08
449.94
NA
NA
NA
12/9/05
30.27
177
1414
1
NA
A
8/8/06
29w72
5!T
0
NA
NA
Pop I of 12

Table 7: Groundwater Elevation Data
DSCAIIVWO�r KDC92000
Groundwater
Sampling Point
Sampling Date
(mm/dd/yy)
TOC Elevation
[feet]
Depth to Water
[feet bgs]
Groundwater
Elevation
[feet]
Depth to NAPL
[feet bgs]
NAPL Thickness
[feet]
Corrected*
Groundwater
Elevation [feet]
MW-5
11/13/95
472.49
29r76
442r73
NA
NA
NA
4/18/96
29094
443.65
NA
NA
NA
4/1/99
22 65
449r84
NA
NA
NA
10/19/99
22.95
449.54
NA
NA
NA
3/14/00
2231
450A8
NA
NA
NA
8/12/03
21032
45LI7
NA
NA
NA
3/9/05
2118
44931
NA
NA
NA
12/9/05
24,76
44733
NA
NA
NA
8/8/06
24�59
447.90
NA
NA
NA
3/11/08
2635
445074
NA
NA
9/9/08
26r54
445�95
NA
NA
-NA
NA
10/8/09
26.54
445.95
NA
NA
NA
214/09
26.25
446�24
NA
NA
NA
4/2/09
2581
446068
NA
NA
NA
7/15/09
24.90
447,69
NA
NA
NA
10/6/09
25069
446080
NA
NA
NA
2/2/10
25066
446.83
NA
NA
NA
4/20/10
2461
44T88
NA
NA
NA
7/13/10
24.16
44833
NA
NA
NA
iO/20/10
24,68
447481
NA
NA
NA
4/25/11
26 09
446041
NA
NA
7/26/11
26,20
446029
NA
NA
-NA
NA
linni
2&73
445077
NA
NA
NA
1/26/12
26090
445.69
NA
NA
NA
7/17/12
26A2
446.07
NA
NA
NA
11/2 112
2553
446.96
NA
NA
NA
2/25/13
2T26
445023
NA
NA
NA
1/28/13
2636
446,13
NA
NA
NA
9/9113
26.65
445684
NA
NA
NA
12/9/13
25095
446�64
NA
NA
NA
3/24/14
25.07
44T42
NA
NA
NA
6116/14
2430
448619
NA
NA
NA
9/22/14
448.74
NA
NA
NA
12/15/14
24.02-1
449,47
NA
NA
NA
3/16115
23.54
448.95
NA
NA
NA
6/16/15
22.92
449.57
NA
NA
NA
9/14/15
24448
448.01
NA
NA
NA
12/14/15
23.91
448�59
NA
NA
MW-6
11/13/95
NA
31,36
65.10
NA
-NA
NA
NA
4/18/96
29950
6696
NA
NA
NA
616/96
28.19
68.28
NA
NA
NA
MW-7
1
11/-13/95
476.90
1
30486
446604
NA
NA
NA
4/18/96
29,13
447.77
NA
NA
NA
6/6/96
2960
448.30
NA
NA
NA
6/20/96
28636
448.54
NA
NA
NA
4/1/99
2726
449.64
NA
NA
NA
10/19/99
28020
448.70
NA
NA
NA
3/14/00
27.75
449v 15
NA
NA
NA
12/9/05
28073
448.17
NA
NA
NA
8/8/06
29.79
447011
NA
NA
NA
12/12/07
31.00
445.90
NA
NA
NA
io/s/08
31.52
445038
NA
NA
NA
7/16/09
30.00
446.90
NA
NA
NA
10/7/09
30052
446.38
NA
NA
NA
2/2/10
30.75
446.15
NA
NA
NA
4120/10
30926
446r64
NA
NA
NA
7/13/10
29086
447.04
NA
NA
NA
10/19/10
29.37
447m53
NA
NA
NA
4/25/11
30.93
445.97
NA
NA
NA
7/26/11
31409
445081
NA
NA
NA
11/1/11
31,0�
445.77
NA
NA
NA
7/17/12
31.77
445.13
NA
NA
NA
11/28/12
31946
445.44
NA
NA
NA
2/25/13
31990
445.00
NA
NA
NA
5/28/13
3L56
445.34
NA
NA
NA
9/9/13
30.85
446vO5
NA
NA_
NA
12/9/13
30.67
446023
NA
NA
NA
3124/14
31 14
44536
NA
NA
NA
6/16/14
1 -
1 445,85
NA
NA
NA
9/22/14
3036
1 446�54
NA
NA
NA
12/15/14
29948
44 7-4 2
NA
NA
NA
3/16/15
2222
447�60
NA
NA
NA
6/15/15
�� 5�
44640
NA
NA
NA
1 12/14/15
28 96
448.04
NA
_NA
NA
Page 2 of 12

Table 7: Groundwater Elevation Data
DSCA IOD No.: DC920001
Groundwater
Sampling Point
Sampling Date
(mm/dd/yy)
TOC Elevation
[feet]
Depth to Water
[feet bgs]
Groundwater
Elevatio
[feet]
DepthtoNAPL
[feet bgs]
NAPLThickness
[feet]
Correcte&
Groundwater
Elevation ffeet]
MW-8A
4/18/96
479,68
35087
443.81
NA
NA
NA
6/6/96
35010
444059
NA
NA
NA
6/20/96
33.08
446,60
NA
NA
NA
4/1/99
33.21
446.47
NA
NA
NA
10/19/99
35.35
444.33
NA
NA
NA
3/14/00
33.92
445�76
NA
NA
NA
9/12103
33006
446.62
NA
NA
NA
3/9/05
33.90
445.78
NA
NA
NA
12/9/05
35096
44172
NA
NA
NA
8/8106
36.27
443.41
NA
NA
NA
12/13/07
38,65
441003
NA
NA
NA
10/8/08
38.29
441.39
NA
NA
NA
7/16/09
36,14
443.54
NA
NA
NA
10/7/09
36021
443.47
NA
NA
NA
2/2/10
36,40
443.28
NA
NA
4/20/10
36006
443.62
NA
-NA
NA
NA
7/13/10
3539
444.29
NA
NA
NA
10/20/10
35,98
44170
NA
NA
NA
4/26/11
3660
44308
NA
NA
NA
7/26/11
37.74
441.94
NA
NA
NA
11/1/11
39 59
441.10
NA
NA
NA
7117/12
38�01
441.67
NA
NA
NA
11/28/12
3813
440.85
NA
NA
2/25/13
35,19
444.49
NA
NA
-NA
NA
1/28/13
38,22
44146
NA
NA
NA
9/9/13
36.83
442.85
NA
NA
NA
12/9/13
38,05
44L63
NA
NA
3124/14
38rol
441,67
NA
NA
-NA
NA
6/16/14
36�98
442.70
NA
NA
NA
9/22/14
39.51
441A7
NA
NA
NA
12/15/14
39A4
440054
NA
NA
NA
3/16/15
36�79
44189
NA
NA
NA
6/15/15
35003
444�65
NA
NA
NA
9/14/15
3 11),
444�65
NA
NA
NA
12114IT5
1� 36
444,32
NA
NA
MW-8B
4/1/99
479 71
37073
441.99
NA
NA
NA
10/19/99
36040
443.31
NA
NA
NA
3/14100
33.41
446630
NA
NA
NA
8/12/03
33059
446.12
NA
NA
NA
3/8/05
34.29
445942
NA
NA
NA
12/9/05
35.31
444.36
NA
NA
NA
8/8/06
35979
44192
NA
NA
NA
12/13/07
37 15
442,56
NA
NA
NA
2/4/09
37.75
441996
NA
NA
4/2/09
37015
442056
_NA
NA
NA
NA
7/16/09
35070
444.01
NA
NA
NA
9/15/09
36019
443652
NA
NA
NA
10/7/09
3547
444.24
NA
NA
NA
212/10
37.12
442,59
NA
NA
4120/10
35.78
443093
NA
-NA
NA
NA
7/13/10
35003
444.68
NA
NA
NA
10/20/10
35.64
444907
NA
NA
4125/11
37.34
44237
NA
NA
_NA
NA
7/26/11
37,35
442036
NA
NA
NA
11/1/11
38,22
441.49
NA
NA
NA
7/17/12
37.63
442 08
NA
NA
NA
11/28/12
38,51
441,20
NA
NA
NA
2/25/13
38.76
440.95
NA
NA
NA
5/28/13
37.92
441.79
NA
NA
NA
9/9/D
3800
441071
NA
NA
NA
12/9/13
376S9
442.12
NA
NA
NA
3/24/14
37026
44245
NA
NA
NA
6/16/14
36.46
443.25
NA
NA
NA
9/22/14
36017
441,54
NA
NA
NA
12/15/14
40.31
439.40
NA
NA
NA
3/16/15
3 7A 1
442.30
NA
NA
NA
6/17/15
35.03
444668
NA
NA
9/14/15
35.32
444.39
NA
i��
1 NA
12/14/15
r 35.14
444957
NA
NA
I NA
Page 3 of 12

Table 7: Groundwater Elevation Data
j),SCAMWK4.ik,,,,
DC920
Groundwater
Sampling Point
Sampling Date
(mm/dd/yy)
TOC Elevation
[feet]
Depth to Water
[feet bgs]
Groundwater
Elevation
[feet]
DepthtoNAPL
[feet bgs]
NAPLThickness
[feet]
Corrected*
Groundwater
Elevation [feet]
MW-9
4/18/96
477,01
29.35
447.66
NA
'�A
6/6/96
28.52
448.49
-NA
NA
NA
NA
4/1/99
27.77
449.24
NA
NA
NA
10119/99
28014
448,87
NA
NA
NA
3/14/00
27.61
449A0
NA
NA
NA
9/13/03
27.52
449.49
NA
NA
NA
12/9/Os
29095
447.16
NA
NA
NA
8/8/06
298
447,21
NA
NA
NA
12/12107
31,41
445.60
NA
NA
NA
10/8/08
31.77
445.24
NA
NA
NA
7/15/09
30,02
44699
NA
NA
NA
1016/09
3Oj87
446MI94
NA
NA
NA
2/2/10
31,00
446�01
NA
NA
NA
4120/10
29,90
477011
NA
NA
NA
7/13/10
29.36
447,65
NA
NA
NA
10/20/10
29+88
447.13
NA
NA
4/25/11
3L40
445,61
NA
NA
-NA
NA
7/26/11
31.42
44519
NA
NA
NA
11/1/11
32.05
444.96
NA
NA
NA
7/17/12
31.70
44531
NA
NA
NA
11/28/12
32.31
444070
NA
NA
NA
2/25/13
32658
444.43
NA
NA
NA
5/28/13
31.91
445.10
NA
NA
NA
9/9/13
30.76
446,25
NA
NA
NA
12/9/13
30.90
446.11
NA
NA
NA
3/24/14
30.55
446.46
NA
NA
NA
6/16/14
29.39
447,63
NA
NA
NA
9/22/14
28.91
448,20
NA
NA
NA
12/15/14
28j98
448,03
NA
NA
NA
3/16/15
28.59
448043
NA
NA
NA
6/15/15
2844
448.57
NA
NA
NA
9/14/15
29,43
44T58
NA
NA
NA
12/14/15
29,09
447.92
NA
NA
NA
MW-IOA
4/1/99
48063
3656
444.07
NA
NA
NA
10119/99
37665
442.99
NA
NA
NA
3/14/00
36,66
44197
NA
NA
NA
8/13/03
36 24
44439
NA
NA
NA
12/9/05
38692
441.71
NA
NA
NA
8/8/06
39.21
44142
NA
NA
NA
3/12/08
41.38
439.25
NA
NA
NA
9/9/08
41639
439.24
NA
NA
NA
1018/08
41,41
439.22
NA
NA
NA
7/14/09
39v 15
441648
NA
NA
NA
10/7/09
39692
440.71
NA
NA
NA
2/2/10
40v56
440.07
NA
NA
NA
4/20/10
39,11
441.52
NA
NA
NA
7/13/10
38.28
442.35
NA
NA
NA
10/20110
39.20
44L43
NA
NA
NA
4/25/11
40,69
439.94
NA
NA
NA
7/27/11
40.97
439.66
NA
NA
NA
11/1/11
41600
439063
NA
NA
NA
1125/12
41692
439.71
NA
NA
NA
7/17/12
41.09
439.54
NA
NA
NA
11128/12
42.09
438.54
NA
NA
NA
2125/13
42,37
438.26
NA
NA
NA
5/28/13
41.30
439.33
NA
NA
NA
9/9/13
40.10
440�53
NA
NA
NA
12/9/13
42,30
438033
NA
NA
NA
3/24/14
41648
439015
NA
NA
NA
6/16/14
40.26
440.37
NA
NA
NA
9/22/14
40.04
440b59
NA
NA
NA
12/15114
40,20
440.43
NA
NA
NA
39.43
2L
NA
NA
NA
�3/16/15
6/18/15
37682
442
NA
NA
NA
9/14/15
3T76
442.87
NA
NA
NA
12/14/15
38657
442.06
NA
NA
NA
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Table 7: Groundwater Elevation Data
DSCA ED No.: DC920001
Groundwatex
Sampling Point
Sampling Date
(mm/ddlyy)
TOC Elevation
V-1
Depth to Water
ffeet bgs]
Groundwater
Elevation
[fectl
Depth to NAPL
[feet bgs]
NAPL Thickness
[feet]
Corrected*
Gr dwater
oun
Elevation [feet]
TW-6
9/B/09
476.89
33.10
443.78
NA
NA
NA
10/20/io
32.32
444.56
NA
NA
NA
4/25/11
33.12
443.76
NA
NA
NA
11/29/12
35.21
441.67
NA
NA
NA
9/9/13
33.28
443.60
1 NA
NA
NA
1\� -7
9115/09
477.72
34.04
443.68
NA
NA
NA
10/20/10
33.28
444.34
NA
NA
NA
4/25/11
35.09
442.63
MA
NA
NA
11/28/12
36.23
441.49
NA
NA
NA
9/9113
34.50
443.22
NA
NA
NA
1219113
35.05
442.67
NA
NA
NA
3/24/14
34.59
443.14
NA
NA
NA
6116/14
33.48
444.24
NA
NA
NA
9/22/14
32.98
444.74
NA
-NA
NA
3/16115
32.92
444M
NA
NA
NA
&18/15
31.71
446.01
NA
NA
NA
9/14/15
31.64
446.09
NA
NA
NA
-EW-8
9/15/09
477.84
3535
44169
NA
NA
NA
10/20/10
34.45
443.39
NA
NA
NA
4/25/11
36.02
441.82
NA
NA
NA
1/25/12
37.22
440.62
NA
NA
NA
7/17/12
36.63
441.21
NA
NA
NA
11/28/12
37.40
440.44
NA
NA
NA
2/25/13
37.70
440.14
NA
NA
NA
5/29/13
36.97
440.97
-NA
-NA
-F -9
9/15/09
478.90
36.33
442.57
-NA
NA
NA
NA
10/20/10
35.78
443.12
NA
NA
NA
4/25/11
36.92
442.08
1 NA
NA
NA
1/25112
39.12
440.78
NA
NA
NA
7/17/12
3735
441.15
NA
NA
NA
MUM
A63
440.27
NA
NA
NA
2/25/13
39.88
440.02
NA
NA
NA
5/29/13
39.09
440.91
NA
NA
NA
-EWwIO
9/15/09
478.34
36,03
442.31
NA
NA
NA
10/20/10
35.49
442.85
NA
NA
NA
4/25111
37.40
440.94
1 NA
NA
NA
11/28/12
1 38.24
"0.1
NA
NA
NA
RW-1
2/1/98
NA
NA
NA
NA
NA
NA
6/25-26/98
NA
NA
NA
NA
NA
RW-2
2/1/98
NA
NA
NA
NA
A
tL
NA
6/25-
NA
NA
NA
NA
1 -
NA
MWC.1 A
2/6/06
NA
NA
NA
NA
NA
NA
*Foriiierly injection �11 (r*V).
Page 12 of 12

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ITable 10: Water Well(s) Survey Data �11 "
Distance
Direction
Property Owner
Well
Screen
Status
Ref. No./
Sampling Location
Tenant Name, Address,
from
Source of Well
(downgradient,
Name, Address, and
Depth
Interval
Use of Well
(Active/
We 11 ID
Name and Address
and Phone Number
Source
Identification
upgradient, etc.,
Phone Number
[feet]
[feet]
nactive
[feet]
to source area)
Kelli Barbour,
8400
Residence,
8400 Camellia Drive,
Same as Owner
480
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Abandon,'
Camellia
8400 Camellia Drive
Raleigh, NC, 27613,
919-772-5160
Charles & Carole Vish,
8401
Residence,
8401 Camellia Drive,
Same as Owner
680
ill
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8401 Camellia Drive
Raleigh, 27613,
919-847-7632
Andrew & Noma Kleitsch,
8404
Residence,
8404 Camellia Drive'
Same as Owner
68
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8404 Camellia Drive
Raleigh, NC, 27613,
919-848-0222
John M. Rogers,
8405
Residence,
8405 Camellia Drive'
Same as Owner
820
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8405 Camellia Drive
Raleigh, NC, 27613,
Unlisted
Daniel & Tara Whitley,
8408
Residence,
8408 Camellia Drive,
Same as Owner
880
200
Unknown
Drinking Water
Receptor Survey
Downgradient
Acti,, c
Camellia
8408 Camellia Drive
Raleigh, NC, 27613,
Unlisted
Gregory & Amanda
Williams,
8409
Residence,
8409 Camellia Drive,
Same as Owner
980
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8409 Camellia Drive
Raleigh, NC, 27613,
Unlisted
Frank & Brenda Ham,
8412
Residence,
8412 Camellia Drive'
Same as Owner
1040
210
Unknown
Drinking Water
Receptor Survey
Downgradient
Ach\c
Camellia
8412 Camellia Drive
Raleigh, NC, 27613,
919-847-4121
Gene R. & Sandra T.
8413
Residence,
Soyars,
8413 Camellia Drive,
Same as Owner
I i-10
Unknown
Unknown
DrinkingWater
Receptor Survey
Downgradient
Active
Camellia
8413 Camellia Drive
Raleigh, NC, 27613,
919-847-4142
Debian & Matthew
Thacker,
8416
Residence,
8416 Camellia Drive,
Same as Owner
1240
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8416 Camellia Drive
Raleigh, NC, 27613,
919-917-7393
Page 1 of 3

Table 10: Water Well(s) Survey Data
DSCA ID No.: DC920001 :A,
Distance
Direction
Property Owner
Well
Screen
Status
Ref. Nod
Sampling Location
Tenant Name, Address,
from
Source of Wel I
i
(downgradienFt,
Name, Address, and
Depth
Interval
UseofWell
,�us,
(Acti ve/
Well ID
Name and Address
and Phone Number
Source
Identification
upgradient, etc.,
.
Phone Number
[feet]
[feet]
Inactive)
[feet]
to source area)
Michael E. & Virginia H.
Richardson,
8417
Residence,
8417 Camellia Drive,
Same as Owner
1300
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8417 Camellia Drive
Raleigh, NC, 27613,
919-848-6743
Lorraine Tomasino,
8420
Residence,
8420 Camellia Drive'
Same as Owner
1200
>150
Unknown
Drinking Water
Receptor Survey
Downgradient
Acme
Camellia
8420 Camellia Drive
Raleigh, NC, 27613,
919-841-9338
James W., Jr. & Louise D.
8421
Residence,
Knox
8421 Camellia Drive,
Same as Owner
1440
139
Unknown
Drinking Water
Receptor Survey
Downgradient
Acti\c
Camellia
8421 Camellia Drive
Raleigh, NC, 27613,
919-847-5098
John & Goldie R.
Duperock,
8425
Residence,
8425 Camellia Drive,
Same as Owner
1440
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8425 Camellia Drive
Raleigh, NC, 27613,
919-847-5153
Betty Rogerson,
8429
Residence,
8429 Camellia Drive,
Same as Owner
1420
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8429 Camellia Drive
Raleigh, NC, 27613,
919-847-5613
Elizabeth M. Mercer,
8433
Residence,
8433 Camellia Drive,
Same as Owner
1440
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Camellia
8433 Camellia Drive
Raleigh, NC, 27613,
919-847-5754
Eugene Kermedy,
8400
Residence,
8400 Azalea Place
Same as Owner
400
150
Unknown
NA
Receptor Survey
Downgradient
Abandoned
Azalea
8400 Azalea Place
Raleigh, NC, 276 1
919-847-7575
Bruce Blackwell,
8401
Residence,
8401 Azalea Place,
Same as Owner
250
173
Unknown
NA
Receptor Survey
Downgradient
Abandoned
Azalea
8401 Azalea Placc
Raleigh, NC, 27613,
919-524-4765
Frederick Schwartz,
8404
Residence,
8404 Azalea Place
Same as Owner
600
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Azalea
8404 Azalea Place
Raleigh, NC, 27613,
919-676-1249
Page 2 of 3

Table 10: Water Well(s) Survey Data
DSCA ID No.: DC92000�
!
Distance
Direction
Property Owner
Well
Screen
Sta�tus
ta
Ref. No./
Sampling Location
Tenant Name, Address,
from
Source of Well
(downgradient,
Name, Address, and
Depth
Interval
Use of Well
(Active/
Well ID
Name and Address
and Phone Number
Source
Identification
upgradient, etc.,
Phone Number
[feet]
[feet]
Inactive)
[feet]
to source area)
Elias Schnegelberger,
8405
Residence,
8405 Azalea Place,
Same as Owner
600
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Azalea
8405 Azalea Place
Raleigh, NC, 27613,
919-847-4828
Richard Lemert,
8408
Residence,
8408 Azalea Place
Same as Owner
780
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Azalea
8408 Azalea Place
Raleigh, NC, 2761
919-846-0558
Jaswantrai Patel,
8409
Residence,
8409 Azalea Place,
Same as Owner
780
Unkuomi
t,nknomi
DrinkinQWater
Receptor Survey
Downgradient
Active
Azalea
8409 Azalea Place
Raleigh, NC, 27613,
919-846-7173
Vance Kennedy,
8412
Residence,
8412 Azalea Place
Same as Owner
980
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Azalea
8412 Azalea Place
Raleigh, NC, 27613,
919-847-4055
Richard & Danielle Lang,
Kenneth & Donna
Hunsinger,
8413
Residence,
9329 Tamarack Drive,
8413 Azalea Place,
960
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Azalea
8413 Azalea Place
Meadville, PA, 16335,
Raleigh, NC, 27613,
Unlisted
919-8474159
Annie B. Johnson
8416
Residence,
8416 Azalea Place,
Same as Owner
1140
Unknown
Unknown
Drinking Water
Receptor Survey
Downgradient
Active
Azalea
8416 Azalea Place
Raleigh, NC, 27613,
919-847-5675
Farlow & Metcalf LLC,
2949
Unknown,
7420 Matherly Drive,
Unknown
1000
Unknown
Unknown
Drinking Water
ENSR Receptor
Upgradrent
Active
Brennan
2949 Brennan Drive
Wake Forest, NC, 27587,
Survey
I
1 919-556-9677
1
1
rel is were all reportedly cased to oectrock surface and drilled into the beCIrOck until tne first zone capaM producing sufficient water flow was encounterea. Ine well at 2949 Brennan Drive was
rmeviously addressed as 8217 Creedmoor.
Page 3 of 3

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9 6
6 a
6 6
8 6
a &
a a
6 6
Naphthalene
8
tt
8 8
tig
8
9
9
R
8 8
8 a
8 8
z
Tetruchloroediyleric
6 8
8
9 4
6 4
a 9
.1
8 ddakk
a 6
a a
A 6
9 8
6
a a
A 6
a 8
Toluene
trans-1,2-Dichloroetli\
8
8
P
rrichloroethylene
z
A
a a
a 6
a
Vinyl chloride
8
a a
& a
a A
1.
A
g
g S
8
A
8 8
A
. 6
a 6
8 a
Xylenei; (total)
gag
8
8
8 9
- -
8 a
- -
8 &
- -
8 8
- -
i
8
- -
A
- -
- -
- -
- -
1,1,1-Trichlormthmic
a 8
8
s
s g
a 6
s s
a a
a
6 9
s
8 9
8 g
a 8
g s
a 9
& 8
9
g 8
a a
g s
a
8
1,1,2-Trichloroethw,
as
a 8
8
a 9
8 8
9
8 8
s 8
a
a
a
a a
9 9
9
a a
4 a
a A
a a
a a
a
lj-Dichlorocthan�
4; 81
A a
a a
.9 .8
9 a
a a
a a
a a
1,2-Dichloroethme
z
(EDC)
a a
A a
a a
8 g.
a
8
a A
8
8
a 8
A a
I I
A A
a I
Carbon tetrachloride
a
A A
9
9 A
8 A
a
a
a
s
a aga
s g
Chlorofom
z
z
o 6
a
a a
a a
a a
4 a
a a
a
a b
a 8
Brommethane
a
a
a
a a
z
z
z
>Z
z
>
>
>
z
>
> >
z �
>
. .
>
9
Dichlorodifluoromefli
we
9 9
9 9
4 8
8
a 4
a A
8
Chlorornethane
I
. .
. .
. .
.
. . I
I
I
L
I
-L—

Santple ID
Spling Date (mnVdd/,:
8
Benzene
CD
F
8 FIG
9
a a
11
ji.
1
I I
ION
8
m-1,2-13kh] ... thle
g a
g g
a a
A
A A
a A
6 a
A
Ethylbenzene
8 8
8 8
t a
g &
C, a
8 g
a
9 a
a 4
1, a
Meth I tert-butyl
y
ether
F S.3
S
G 5
G, G
(MTBE)
g a
a
a a
A
tg
Naphthalene
Tetrachloroeth� lenc
8's
8
8 s
8 8
8 8
8
Toluene
9
a 9
8
g a
a 4
a a
a
g 9
a 8
a
trans-1,2-DichlormthN
9 9
9
.
. .
. .
. .
. ..
rrichloroethylene
8 8
s 8
1 a
I E
g a
a a
a 4;
a b
a a
8 A
.8 a
g a
a a
a
Vmyl chlovide
86,
g
8; A
9P
9
6
g a
a 4
9
A a
-g-�g
�s
Xylenes (total)
9 9
9 9
9 a
z
>
�a
g
g
9 a
g g
A
g 8
A 8
s g
1,1,1-Trichloroeth�e
8
9
8
8 8
8 a
8 9
8 8is
1,
9
8
9 9
g
s a
A A
8 8
8�
s 8
a A
6 6
1,1,2-Trichloroethmic
G
15
9 9
9 8
9 9
],I-Dichloroethme
9
A 8
8
a a
a a
8� a
a a
9 a
.1 A.
1.
A
9,
1,2-Dichloroethme
9
G
9 9
8 9
g 8
g g
SH
9 9
9
9 9
-9 9
(EDC)
g g
g s
g g
8 8
A
8 8
a
a g
a a
Carbon tetrachlori&
A
I A
s g
9 9
g g
g g
g
g 9
—
9 9
—
9 8
- -
9 8
� -
9 b
� a
Chlorofom
6161
22
9
2
1 9
2 2
9 9
9 a
a 8
2
8 a
2
2 E
9 9
2 o
xv
Bromotnethane,
9
I z
zIz
z z
z
zlz.z
I
[z
z z
z 9
-11
6
Dichlorodifluorom,11,
> >
> >
> >
> >
> >
>
>
>
>
>
re
I
A
g gIg
;lg
A
. 8Ig
.
g .
O.A.418I.A
8
P1,1410161
8 8
Ilc hloromthan
- -
- —
—

Sample ID
r2
ct �t
5
Sampling Date (mrn/ddly:
9 9
8 9
9 9
9 s
Benzene
P
P
11
P .
11119.
. .
g.gJ916191919
. .
. .
. .
9.8
P p
8
8
6,-1,2-Dichloroethyle
A 8
g A
6 6
6 a
a a
4; a
8 9
a
a a
Ediylben,e.e
8- 9�
Methy tert-butyl
ether
(MTBE)
8888988gg
8 9
9
9 9
8 8
8 8
Naphthalene
retwhloroethviene
8i
4 a
roluene
8
trans-1,2-Dichlorced,
. .
. .
. .
. .
. .
.
8
8
Trichloroethylene
g g
8 a
8
4 6
4; It,
a 6
t, 8
a a
8 a
a
4;
a
g
Vinyl chloride
9 a
a a
4 A
a a
4;
6. 8
g g
9 9
a a
8 9
6 8
9 8
8 a
8 9�
Xylenes (total)
9 9
8 9
9 8
8 >
s
9 8
9
9
1,1,1-Trichloroethane
S6 8
8
t
9 9
A
8 9
A
9 9
&
9 9
8
A A
g g
1,1,2-Trichloroethwe
g g
g 8
8 a
8 8
lj-Dwhloroethan�
8 8
9
a 9
a 9
& A
9
a
8
a
9 8
a a
9 9
g a
9 8
8 a
a
a g
a.
a 4
s g
a a
g s
1,2-Dichloroethme
�9
(EDC)
arbon tetradiloride
8
9 8
8 9
1. A
9 9
9
8
8 8
g
g g
g
Chlorofom
A
9
a a
9 a
9 a
a 8
2 2
6 82
2
'a
2 2
2 2
- -
- -
x
0
Bromomethane
Dichlorodifluorometh
.9 .6
a 8
z
z
z z
z
z
. .
. z
z z
z z
z
>
>
> >
>
>
> >
> >
> >
Z
me
9�
9
g a
8 8
. 6
9 9
8 8
8
9 9
8
1 AR
I
8 g
"161
2hlorome:th e
an
-
-
-
-
�s —
— —

tv
Sarnple ID
Y,
Sarripling Date (mni/dd/y,
P)
EL
Ber�ene
8 a
S
z
cis-1,2-Dichloroeth% I e
— —
— —
— —
—
s s
—
— —
Ethylbenzene
8
8
g
y tert- uty
ther
(MTBE)
z
Naphthalene
a
Tetrachloroethylere
8
101,
ON,
Toluene
g
I I
g
I
A
A b
A a
6
a
4 a
a a
4; 8
a
a
6
traris-1,2-Dichloroi,th,
3 2
I P
A
Trichloroethylene
.
. .
. ...
.
. .
. .
8
6 . 8
Vin% I chloride
Xylenes (total)
8
a a
a a
g
a a
4;
g
8
8 g
a
g g
g a
g g
g
1,1,1-Trichloroethwie
.8
8
A
g
a
g
a
a a
.8
.8
's
1, 1,2-Trichloroethme
6
z
1,1-Dichloroethme
3
z
1,2-Dichloroethane
2 -8
-8
(EDC)
�9999
8 8
1, A
8 8
�g.gg.gi�
'arbon tetrachloride
. .
. .
. .
. .
. .
z
Chlorofbm
. .
. .
. .
. .
. .
b 6
- -
6 6
- -
6
- -
- -
- -
- -
Brommethane
z
> >
z
> >
z .
> >
z
>
z z
> >
I
>
z z
z
hl od fl 11,
c orodi uoron,,Il,
e
t9
Eh aner

Semple ID
e"
s
s
Sarnpling Date (mnVdd/y,
7
a a
a a
A a
A, a
a A
a A
A a
8
7
A
A
lal
A
11 11 1
�
I
1,
1*
Ia Ig
a
I
A 6
I
I
cis- 1,2-Dichloroethylc
S-1 2-Dich'or-ffiyl
a 6
6 6
a 4
A a
a a
a A
0 A
A A
a a
a 6
8 A
A a
a A
A A
4 A
a 6
A 4
'Y.be__e
Ethylbenzene
4 6'
a a
Ala
A 4
a a
a a
9 a
A a
8 8
. _buU"
Methyl tert-but,11
Me tjer
1
1
Ep
?
g
g g
S
8
effi
ether
I
.E
a a
a a
a A
9
a .9
.9 8
S. a
a
4
A a
9 a
a I
a a
.9 a
a a
NapInhalene
.9 .9
a
a a
A a
a
retrachloroethylene
A a
4
a
'a
a
roloene
w
85 8-
8-
E
E E
�
E
E
a a
8
8 8
a a
g
8
8 A
9 A
A
a a
8
a a
a a
A
8 Ip
?
? 2
9
8 a
9 9
a
9
A A
8 9
a a
9 §
tr, 1,2-Dichloroctli,
E
E
.
. .
9
. .
8
. .
. .
. .
. Z:
8 8
8 8
8
E E
8
Trichloroethylene
A a
a 8
g:g
a a
a a
a a
8 8
v Vinyl chloride
Xylenes (towl)
a
9 A
4 a
6 8
8
8 9
A A
8
9
A
a 4
a A
8
a a
A a
4;
a
8
a a
8 8
a 9
6
>
8
8 8
- I -
a a
a a
a 9
9
g
Z5
8'� �g�
>z 8
-
8 gig
- -
s
- -
8 s
- -I
1,1,1-Trichloroeth-
A I a
1A I A
11
a
8
a a
A a
A
8 a
a a
A a
6 a
1,1,2-Trichloroeth—
A
4; 1 A
a A
A
8 8
a
8
a 6
a
a .9
.9 .9
a
a
g
6
g
8 A
g
. a la
I I . A
IJ-Dichloroethane
9
a
A A
A
8
A
A
8
A
8 8
a
a
8
E
a
E E
a a
a A
A A
1,2-Dichloroethme
EDC)
ga�AOA
ga,�a
1
11, A
. _AAA
ga
Carbon tet—hlmd�
8
8
8
8
8 8
8 8
Chlorofonn
9
a
a 4,
a A
8 8
-
a a
- -
a a
- -
a a
- -
a a
- -
8
-
8
- -
- -
- -
- -
- -
Brornomethane
--
z z
> >
z z
z A
>
z
>
> >
> >
z z
>
. z
> >
z
>
z
>
z z
> >
z z
� >
z
>
>
Dichlomdifluoro.eih
we
a
glaIgIg
8
8 8
A
A
gig
g
8 8
g 8
a A
g g
a
g
a
Chlo,..,Ih.e

Sample ID
z
Sampling Date (mrnIdd/y,
7
Ben�ene
8
8 9
9
g 8
a 8
8
g
a
is-1,2-Dichloroethyl
9
Ethylbe=ne
a
Methyl tert-but,,l
g
g g
g g
g g
g
9 9
ether
(MTBE)
Naphthalene
le-chloroethylene
g
a a
a t�
A
Toluene
1
9
9 a
a 9
a
a &
a
6
6
A
trans-1,2-Dichloroelln
8
9
g
g g
g
s
g
g g
Trichloroethylene
g
8 g
a
8 a
1 1
1 1
Vinyl chloride
8
s 8
s
EP
a.
g g
g S
g
g g
Xylene, (total)
8
9
8
9 91
8
g
1, 1, 1-Trichloroethw,
g 8
g 8
g
E
g g
g g
g
g g
6 g
1,1,2-Trichloroethme
I,I-Dichloroedwe
EDC)
A 1.
Carbor, teuachlun&
g
Chloroforrn
P.
P!
2
2 21
o 6
b 2
2
o 2
2 a
�R 6
6 6
Bromomethane
z z
. z
z .
z z
z z
z z
z
z
. z
Dichlorudifluorometh
>
> >
> >
> >
>
> >
> >
>
>
> >
g
§
9C
4;
8
9
6
9
gl'lg
$1414
Chlorrnethane

Sarnple ID
—p—g Date (mmIdd/y,
'a
U,
z
Ben�enc
6-1
cr
I'l,
IZ1,1Z
Z.
611.1611.1.10,
I
z
z
z z
0
cis-1,2-Didiloroethyle
6
Ethylbenzene
Methyl tert-butNvI
ethff
z
z
z
6 .
(MTBE)
z
1
z
z I
>
Naphthalene
z
z
z 6
z
retTachloroeft lene
A
A
i, z
z
6 6
6 6
z 6
6 8
6 6
6
Toluene
6
6 6
6 6
6 6
6 6
6 6
6 6
6
trans-1,2-Didhiloroeth.
6
z. 6
6 6
6 6
616
6 6
6 6
6 6
Richloroethylene
11
u
u
+1
z.
Vinyl chloride
z.
z.
Xylenes (total)
z
1
z
6 6
6 6
6 6
1,1,1—chloroeth—
a
6 z.
6 6
6 6.
6 6
1,1,2-Trichloroethwic
x
z z
z Z
a
6
z Oz
6 6
I,I-Dichloroethme
P z
z
z z
0
z
z
z
.
z z
. .
2-Dichloroethme
EDC)
6 0
x z
0
z 6
0
z 6
6 6
6 6
6
6
Carbon tefr=hloride
zv
-W
z z.
z.
z. 6.
6 6
6 6.
6 6
Chlorofom
0 6
6 6
.
6 z
. .
6 6
. .
6 z
. .
6 6
. .
Bromomethane
.
Dichlonodifluorometh
we
z
>
z z
6. z.
'. 6.161"
I
z 6
6 z
z
6
6 6
6
z 6
6 6
ChIoro,-fl,,,-

Sample ID
z;
Z: a
S
2
;3 s-2
z
4,
.—pling Dare (nualdii/y.
z
z
Ben�ene
a
a A
a
-1
6 RIM
z z
. a
z
a
z
a
cis-1,2-Dichloroethyle
z:
OZ
Ethylbenzene
8
Zw �z
�z Z
IZ
Methyl tert-butyl
ether
. .
. .
. .
. .
(MTBE)
8
8 9
9 9
9 9
9
z
Z.
Oz
za 6
Z�
Naphthalene
4
0
A A
A z
z z
z
z z
z z
z z
z z
z
Tetrachloroethylere
8 s
8 8
Z
Z
Z.
Z.
Toluene
a
9 9
S
5
9
g 8
9 11
a a
a a
a a
A gkk
1;
A a
a
6
6 6
6
trans-1,2-Dichloroeth,
. .
. .
. .
I .
. .
. .
8
.
Z
1
6 6
6 6
6 6
6
Trichlormthylene
g
6 b
z
z
6 6
6 6
6 6
6 6
6 6
6
Vinyl chloride
g
8 g
a
8 a
g a
a A
a
g
5
6 6
6 6
Xylenes (total)
8
9
9 9
9 9
9
A 8
a
>
9 9
a
A
6
6
6
1,1,1-Trichloroethwe
8 2
8
8
8 8
8 8
Oz
z
0
z
0
z z
v
z z
0
z
.
1,1,2-Trichloroeth-
z
6 z
x z
6 6
x 6
z z
z 6
lj-Dichloroethane
A 9
? ?
a A
8 a
8
8-
a
8- 8
P a
z g
6 8
g 8
8
Oz
z
ei
z
a
z
z
.
z z
. .
z
a
1,2-13ichloroeth�e
. .
. .
. .
EDC)
4;,
A
9
a
8 8
a
z
z z
z
z
6 6
6 z
z z
z
Carbon tetrachloride
g
9
9 a
9 z
z z
z z
z z
z 6
z z
6
z
Chlorofom
Z
z Z
6
Z Z.
6
z z
ziz
z
Brommethme
6
9
6
a a
I>
6
zo Z.
6 6
z,6
z z
6 z
Dichlorodifluoromelli
me
a
6
66666666
z.
6 6
6
Chloromethane

S=p[e ID
Sarnpling Date knurivawy,
3
9 9
9 s
9 r
g
8 8
a 8
8 1
6 11
i
1
8
W I
8
cis- 1,2-Dichloroethyle
6 U
�
-
.
. .
Ethylbenzene
A
8
8
g
e y le - ut,
e
(MTBE)
a 8
Big
Naphthalene
z
yp
Tetrachloroethylene
9 8
9 9
9 9
8
8
a
8
g
g g
8 g!g
Toluene
8 8
8
.9
a a
lraru;-1,2.Dichloroejh,
rrichlorcethyleste
z
.
M-1111
—Vinyl chloride
g- g
g g
g
Z
g g
g g
Xylenes (total)
8
g
8
g
8M
z
z
> i
i 6
1,1,1-Trichl.roeih.,
8 8
9
g-
g s
s
Z. 8
-
8
g
Yp
1,1,2-Trichloroethmie
z 8
919
'A
1,1-Dichloroetharc
a a
a a
a
z 8
.9 0
.9
Z
9 gja
g
gjaJA
a
i� z
1,2-Dichloroethan�
1.6
8 9
9 9
15
9 9
a a
s s
s .
(EDC)
8 9
96
4 9
a a
9 a
9 z
u
Carbon tetrachloride
9
8
Chloroforin
z
8
9
8
9 6
2 -6
Brontomethane
Z z
>
z z
> >
z gIZIA
>
8.AJA
a
A
z
z
>
Z z
Z Z
> >
Z
>
Dichlorodifluorometi,
me
g
Chloromthme

Sairiple ID
9
IMM
i"3
8
Sarnpling Date (mni/dd/y.
>
�Jffl&
a
a a
a
a a
a 6
6 6
a 8
a
A 1.
a a
A a
Betucrie
cis-1,2-Dichloroediyle
6
alddo
6
a
a a
a a
4; A
a
a
Ethylbenzene
6
la
I a 1 8
a
a A
R
a
E
A a
9
a a
8 8
8 a
9
4 0
9 9
9 9
8 8
8
8 a
8 g
e y lert-butyl
ther
(MTBE)
8
1"I'd
a
8 8
I I a
a
1?
A a
s s
a a
a 8
a
6 a
. a
8
,
9 a
N*thalene
a
a
I a I a
a
8
Iz.z.
retrachloroethylene
A
8 b
ag
Toluene
s
s
a a
a a
A a
a
6 6
9 8
a
a a
a
a
trans-1,2-Dichloroctf,
a
9
A
9 8
8 a
9 9
.8
6 9
a a
9 A
A 9
8
A a
g g
a A
g 1
a
8 8
s
Trichloroethylene
6
a
a
a a
a a
6
a 4
a a
a a
a a
a
a a
Varyl chloride
T
ZQ—
A
8
aA
8
8 a
A
9 a
9 9
a 8
6. 9
a
9
A a
Xylenes (total)
a
9
8
9 9
a
8
A
a a
a a
a a
a
a
s s
8
s
a
1,1,1-Trichloroethm�
8
b
a 8
9 9
6 a
9 8
a
a a
A a
8 a
a a
gla
g
a 8
s g
8
8
a
1,1,2-Trichloroethw�
S
I,I-Dichl.roeth.c
a
a a
a a
a
a
8
8
8
9
a
g
a a
6 g
a
g
A
8
1,2-Dichloroethari,a
(EDC)
a
a a
a a
8 a
a a
a
kkla
a
a
8181,18
arbon tetrachloride
a a
6
9 a
a
A 8
a a
Chlorofom
a
a a
0
a a
0 6
a
6
8
G 6
9
6
a
8 8
9 a
B,...th.e
z
z .
z
z
z z
z z
z z
z
z
8 a
Diddorodifluorom 11,
z
> >
> W
>
> >
> >
>
> >
> >
>
0
me
9
8
8 8
a
A
a
'Isla
8
a
a a
s 9
9 8
8
a
9

'cable 11 1): Analytical Data for Water Su 51y Well(s)( l lser Specified Chemicals
DSCA ID NogSoJDC920001
A
'—
9
voC
c
9
o
u
N
o
t
.r
o
N C
0
N .0
k
3b
N
N
Q
E
y
w
m
L
HOME I
]29/199]
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
NA
ND
NA
HOME]
729/199]
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
NA
ND
NA
H0W I
]/29/199]
ND
ND
ND
ND
ND
ND,
ND
NA
ND
ND
ND
NA
ND
NA
Cny WAFF�
]29/199]
ND
ND
ND
ND
ND
ND
ND
NA
0.02
0.02
ND
NA
ND
NA
PW'-12
6/25d S
ND
O.WII
ND
ND
ND
ND
ND
NA
ND
ND
D.W22
NA
ND
NA
U16/19%
ND
NA
NA
NA
NA
NA
NA
ND
NA
ND
NA
NA
NA
A.05
1/2N199]
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
NA
NA
NA
v21/199]
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
NA
NA
NA
]/M/199]
ND
ND
ND
ND
ND
ND
ND
NA
ma
ND
ND
NA
NA
NA
2/1/1998
m
ND
ND
ND
ND
ND
ND
ND
ND
NA
NA
NA
6/2y12 2
ND
ND
ND
ND
ND
ND
ND
ND
ND
N/A
ND
NA
I IWI996
ND
ND
ND
ND
ND
ND
ND
ND
ND
NIA
NA
NA
N1/1999
ND
ND
ND
ND
ND
ND
INDNA
ND
ND
ND
NIA
ND
NA
Pa0n Ca�n�llia
6]I/199v
ND
ND
ND
ND
ND
ND
ND
ND
ND
N/A
ND
NA
IM11999
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
NA
NA
1/120ai
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
ND
NA
1012712-,
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
NA
NA
NA
LI/2001
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
NA
ND
NA
911312.3
NA
O.MS
'O.OWS
'O.OWS
ROWS
10.0W5
<D.OWS
NA
'0,0W5
A.0W5
<DUWS
NA
'O.WS
NA
LI]2005
NA
A.OWS
110.0005
'O.WS
A.OWS
<O.OWS
O.OWS
A.00D5
'0-5
AM5
A.M5
NA
A0025
NA
212V2006
M,
<O.OWO
<O.W03
A.WW
<O.OW2
A.O=
<O.W03
<M003
<O.W03
A.W03
<0.0002
-O0009
c0, 0
<0.0012
10/4,2006
10.0000
A.WOY
<0.0003
AD003
<O.OW2
A.0002
W.DW3
0M
<O.WW
<0.0003
A.0002
0.0008
0.OWO
<O.W12
Page 13 of24

PVT
S� P1, 11)
>
ieg
RR
ZZ
Sampling Date (mmIdd/y.
Chloroethwe
W
>
z
z z
z
z
sec-Butylben.ene
>
>
>
> >
>
>
ggggg888>z>1.1>z>z>z
z
>
> >
Hz-
> >
>
1,2-Dichlorobenzme
M.
z
z >
z z
> >
>
z
> >
z
> >
z z
> >
z
>
1,4-Dichlorobenzene
z z
Z Z
Z
> >
>
>
>z
z z
z
z z
z
z
1,2,3-
> >
> >
> >
> >
> >
> >
>
8
Tricltlorober�ene
8
9
z Z
> >
z z
> >
Z Z
> >
Z .
> >
z z
>
> >
>
1,2,4-
TrimethylbeIume
8
8 8
Carbon Disulfide
*3
9
9
Dibromochlorometha
ne
8
8
Chlorobenzene
9 86
a a
9
z z
> >
z
>
>z >z
4
>z 1>
z
> >
z z
> >
z
le.-Butylbenzene
6
2-Bu(mone
8
g
Meth, [me Chlond,
a 81
a a
a a
a a
a
>
Acetone

Smple ID
Sunpling Date
(mni/dd/y:
> o
9
CWoroethwe
911
> >
>
ITIZ
>
TIT
Iliz
> >
> >
z T
z
> >
z
>
> ZIZITM
>
z
sec-Butylbenzene
z
> >
z z
> >
> >
Z Z
> >
Z
> >
z
> >
I I
> >
I
>
z �
> >
Z Z
> >
z z
> >
1,2-Dichlorobenie..,
z z
> >
z z
> >
> >
I - z
z
> >z
-> >Z
> >
>
z
> >
z z
> >
z z
> >
1,4-Dichloroben/.C-
z
z z
- z
z Z
Z z
z
1,2,4-
> >
> >
> >
> >
> >
> >
>
> >
Trichloroben,ene
z z
z z
I zlzlz
>
z
> >
z Z
>
z z
> >
z z
> >
> >
z z
> >
z
> >
1,2,3-
> >
> >
>
z
TrichlorobenLene
z
z
z
z z
z
z z
z z
z z
Z z
z
z z
a a
1,2,4-
>
> >
> >
> >
> >
> >
> >
>
> >
>
> >
z
rrimetitylbenzene
M.
2
g 8
R
a 9
a a
R
a
a
E
Cwbon Disulfide
z
Dibromochlorometh.i
6a
ne
8
r r
�5 r
- -
- -
- -
- -
- -
z
Chlorobenzene
9
8 8
a 9
8 8
8 8
8 8
- -
- -
- -
- -
- -
- -
-
> >
>1 z
z
> >
z z
> >
z z
> >
Z Z
> >
Z I
>
Z I
>
I z
> >
------
z
8 a
a 8
a a
a a
4 a
g A
a a
9
2-Butmone
Z9 Z9
9
9
.4
9 .4
.9 .9
4 a
a a
A 8
a a
g A
Mediylene Chloride
z
Acetone
6
a
a a
a a
a a
a a
a
2
>

Sample ID
Sampling Date
(mm/dd/y,
A
a 6
g
a a
8
a 6
A a
A 8
a a
8
a A
. .
a a
. .
a a
. .
a a
. .
a
. .
Chloroethane
tv
tg
9 11
a
A
>
z1z
> >
z z
> >
z z1z
> >
zjzj�jz
> >
>
> >
>
>
> >
z z1a
> >
sec-Bnylben�ene
8
8
8 8
8 8
z z
> >
>
>
z z
> >
z z
> >
z z
> >
z
>
z
>
. z
> >
z z
> >
1,2-Dichlorobenzene
I
a
A
8
z
z z
z
z
z
x z
z z
z
z
z
z z
1,4-Dichlorobenzeiie
S
G 5
Z 5P
91
z z
z
z z
z
z
z z
z z
z z
z
1,2,4-
> >
> >
> >
� >
>
> >
>
> >
> >
> >
> >
I
Trichlorobenzene
z z
> >
z z
> >
z z
>
z g
> Z
>
z z
> >
>
z z
> >
z z
> >
z
> Z>
Z�
>z
1,2,3-
Trichlorobenzene
z z
> >
z
>
> >
HZIZ
> z
>
> z
>
z
>
z z
� >
z z
> >
z z
> >
z z
> >
z
>
1,2,4-
. .
. ...
.
. .
Trunethylbemene
81 A
4; Ala
8
9 9
a
A a
A A
a a
a 8
0 A
A a
a 6
a a
a a
A 0
9 z
88
R a
R
a a
a �
a
a
E a
R R
a a
a E
Carbon Disulfide
A
alair
14;
A
A a
4 A
a 9
a a
a a
6 9
a A
a a
a
A a
A z
z
Dibromochlorometha
ne
8 8
z
z
�3 8
8 8
8 8
Chlorobenzene
2 z
> >
z
tert-Butylbenzene
>
-
4 a
8 8
A
A A
a a
4
A a
a a
A 9
86 A
z
2-Butmone
a
a 8
a 4
a
a
a
A a
A A
Methylene Chloride
I
EPP
R a
a
E E
z
>
Acetone

Sample ID
Sampling Date (mmIrld/y,
Z:
3
G o
G
6
6
b
o 6
Chloroethane
v
z z
z z
z z
z z
z z
z z
z z
.-Btylbe,,,ne
> >
> >
> >
� >
> >
, >
> >
> >
> >
>
z
.
z z
z
z z
>
z > z
z z
>
z z
>
z z
> >
z z
> >
z z
> >
z
> >
> >
>
> >
> >
>
>
>
>
,2-Dichl.r.berr,-,
z
z z
z z
z z
z z
z z
z z
z
z Z
> >
z
>
>
>
>
>
> >
>
>
> >
> >
>
1,4-Dichlorobenzene
81
a a
4181$
z
. .
. z
z
z
z .
z z
1,2,4-
;95
s
r
9 8
� 9
8 s
9
z z
> >
z
> >
Z>
Z> >Z
z
>
> >
> >
> >
>
> >
>
Trichloroben/ene
7
7
z z
> >
z z
> >
z
>
z z
> >
z
> >
z z
> >
z z
> >
z
>
z
> >
z z
> >
z z
> >
z z
> >
z
1,2,3-
Trichloroben,ene
8
gjgjaj�
z z
z z
z z
z
z z
z .
z z
z
z
z
z z
z z
9
1,2,4-
8
> >
> >
> >
> >
> >
> >
> >
�
> >
> I
> >
>
Trimethylbenzene
a
9 6
6
g 6
a
A
a
8
A
6 A
A 'g'
a
�g 6g
81 Ag
z
—
.8
'a
Carbon MirIfide
g
6
g
a 4;
a 8
a z
Dibrormochlororned,a
s 8
8 8
8
8 8
8
I'l I
& 9
a 9
a
a a
9 a
9 a
4
a a
a a
9 a
a a
9
A 8
a A
a a
81
Chlorobenzene
9
9
9 8
z z
z
> >
z
>
z z
> >
z z
> >
z
>
Z>
z>
>
z
> >
tert-Butylbenzene
I
I'd
P.
2-But-o-
- -
- -
- -
- -
- -
Meth) lene Chloride
98 9
9 8.
9
g-
g
a a
a a
8
9
ao ac
8b
6
6 b
6 b
b 6
0
6
z
Acetone
>

Table 11 1 : Analytical Data for Water So J Ik Wells I scr S 3ecified Chemicals) NUULRUUI
DSCA ID NeAMC920001
0
`o
20
2
o
o
$
8
o
N
o
m
°
a
o
n
n
m
L
t/1/2WS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
2/2MW6
lbM4
<O.W04
<O.UW3
'0."3
<O.UW2
<U.UW2
<U.W03
<O.0003
'O.WU3
<U.OW3
L.WU]
L.OWA
O.OW4
<D.W12
12/1212W]
<0.01
NA
NA
NA
NA
NA
NA
<O.WS
<0D05
<O.W5
NA
0.0022J
<O.W5
<0.01
2/2l/]OW
<0.01
NA
NA
NA
NA
NA
NA
<U.WS
DW5
<O.W5
NA
'D.01
<D.W5
m05
"//IN2009
W.01
NA
NA
NA
NA
NA
N.4
m.W5
<O.W5
<O.WS
N.4
<D01
<O.WS
<0.05
7115/2010
©.01
NA
NA
NA
NA
NA
NA
®W3
1O.W5
<O.W5
NA
-0.01
W.WS
<O.OS
4/MOI1
<0.01
NA
NA
NA
NA
NA
NA
<D.W5
10.005
<O.W5
NA
'0.01
O.W12Ja
'1126 11
<0.01
NA
NA
NA
NA
NA
NA
<D.WS
<O.W5
<D.WS
N.4
�D 01
0.W]2J
lD.05
1011mil
<0.01
NA
NA
NA
NA
NA
NA
<0.W5
<U.W5
<O.W5
NA
D01
<D.WS
<0D5
IaV2012
'0.01
NA
NA
NA
NA
NA
NA
<O.W3
<O.WS
<O.W5
NA
-U.01
<O.WS
<0.05
T 18/2012
10.01
NA
NA
NA
NA
NA
NA
<D.W5
<D.WS
AWS
NA
•0,01
<D.W5
12/Y3012
<0.01
NA
NA
NA
NA
NA
NA
<O.WS
�.WS
<D.W5
NA
<D.01
<O.W5
<0.05
3!1/201)
c0.01
NA
NA
NA
NA
NA
NA
<O.WS
<O.WS
<0.W3
NA
W.01
<O.WS
5/31/2013
<0.01
NA
NA
NA
NA
NA
NA
m.W3
<U.W3
<D.W5
NA
©.01
O.OW5J
4.05
9/13=13
<0.01
NA
NA
NA
NA
NA
NA
<D.WS
<0 WS
<D.WS
NA
N.01
<O.WS
IVIIM13
<0.01
NA
NA
NA
NA
NA
NA
Q.WS
N.WS
D.WS
NA
Z.01
� ,005
10.05
3/21/WI4
V.O
<O.WlO
�.WIO
<D.WIO
�0.00I0
U.W50
<0.0010
<D.W4D
-D.W050
<D.WIO
<O.WIO
EOM
�.W50
W.050
6/2W2ON
W.OWO
<0W 10
<O..WIO
<O.WIO
<.W0
O..W IO
<0.0040
<O.OW50N.W
10
<O.W ID
0.020
<O.W30
<..O<
N00
AWIO
DWIO
N.WIO
DWSU
<4W50
<O.WIO
OWIO
'D.020
'D. W%
<O
12/19R014
NWW
NW10
<.WIU
aWU
<DW
<.WSU
DWSU
-0.WO
9.W0
! 0.W50D
3116*015
D.WIO
D.W50
D.WIO
O.WW
NM50
D.WIO
NW50D
.OD9SS2UUJ
WI5M!5
D 010
D.WW
<..WIO
O.O
DW50
N.WIO
<0010
<0050
N.05U
9/115
ADM
m.W10
O.WIO
<O.W
<O.W50
DWIO
<OW
W050
DWO
O<.00%9/32g1J
HMO
.
12/IN2015
NW20
-.W50
-MO
DW0
DW50
D.WO
'.020
<W0
<0.050
Page 19 of 24

S—ple ID
ZE a
7
z
2 2
S.pli.9 Date (..Vdd/y.
7�
9
9
9 9
2
2 2
9 4
o- 2
9 a
2 2
6
2
9 a
2 o-
9 8
o- 2
A i;
2 2
a 8
2 21
Chluoetluio,
tv
7'
Cr
>
>
z
>
z
>
>Z Z>
Z> :::4�4
z z
> >
> >
> >
IT
> >
z
> >z
sec-Butylben�ene
z .
> >
. .
> >
z 9
>
z
E >
z z
> >
z
> Z>
. .
.
. .
.
z �
> >
. .
z z
> >
. .
z
>
.
'>
>z >z
. .
1,2-Dichlorobenzene
.
z z
> >
z z
>
z
>
z
z
>
z z
> >
> �
z z1+1+1-
>
> >
>
z
> >
z
>
z z
> >
z
>
1,4 -Dichlorobenzere
z z
>
z
> >
z
>
z
>
> >
z z
> >
z
>
> z
z z
> >
z
>
z
> >
x z
> >
z z
> >
z z
>
z z
>
1,2,4-
rrichloroben7ene
z z
> >
z z
>
z
>
z
>
z
> >
> z>
z z
>
z z
>
z
>
z z
>
z z
>
z z
> >
z z
> >
z
> >
1,2,3-
rricWorobenzenc
z z
> >
z z
>
z
>
8 8
z
8 >
9
. z
> >
z z
> >
z z
> >
z z
> >
z
> 6
E
8
Z-, .8
8 8
5 8
z
>z z>
>z z>
>z '>
z
>z >
1,2,4-
Trimethylbenzene
Cubon Disulfide
E
9 9
9 8
8 8
a
4
9 A
8
6
6 a
A a
6
4 A
Dibromochlorometha
ne
8
a
z
4
6
A g
a
a a
a 9
a
a a
6 a
a
A .9
Chlorobenzene,
> >
z z
> >
z
>
a 8
8 8
8
z
>
z z
> >
> >
z z
> >
>
8 8
8 8
z
z
>
z
z z
> >
tert-Butylbmzme
2
2
Ag
2 2
2 21
2 -6
2
2-Buttvione
g a
a
a a
a g
A A
0
A
A
Methylene Chloride
z 8,
> 6
6 .
. .
6 6
. .
. 8
0 0
6 0
0 b
Acetone

Sarriple ID
3
Saimpling Date (mrn/dd�-,
No
2
2
2
2
Cbloroethane
0
I z
I z
z
z
z
z
>1
> >
> >
>
>
> �
>
> >
Butylbe—ene
z
> >
z
>
>
z .
> >
z z
>
z
>
z
>
-> >-
1,2-Dichlorobenzwe
z z
z z
z .
>
> >
z FH
>
> >
IzIzI
z
> >
z
>
z
z
>
lj-Dichloroben�ene
z z
z z
z z
z
z z
z
z
z z
1,2,4-
> >
> >
> >
> >
> >
> >
>
IITI
> >
I
Trichloroben.cre
z z
> >
z
> >
IzIz
z
> >
>
z I
z
>
� �
>
z z
> >
z g
>
z z
> >
� z
> >
1,2,3-
.
richlorobenzwe
zzz
lzlzlzl
-
�g��zl>z>
z z
z z
1,2,4-
> >
> >
> >
> >
> >
> >
Triniethylbenzerie
Carbon Disuffide
9
Dibromochloromethi
ne
g
8 81
g a
a I
Chlorobenzene
8
z
z z
z z
z z
> >
z
> >
z z
> >
z z
> >
z
>
z
>
z
> >
>
> >
> >
But%,Ibmzme
A a
a 4;
A
g
g
1� a
s
g
a
2-Butanone
Methylene Chloride
S: o
. .
.
Acetone

Sample ID
12
Sampling Date (mni/dd/y,
z Z
>
Chloroethane
6
6 6
6 6
6 6
'a z.
z.
z>
sm-Butyibenene
>
z
z. 6.
6. 6.
6 6
z
6
6 z.
S
1,2-Dichlorobenzene
>
z
z
Iz
z
.
.
6 z
z
. .
.
z z
a
. z
1,4-Dichlombenzene
z
z z
6
zo
Z.
1
>
6 1
Trichlorobenzene
>
z
z z
016
z
.
z
.
6 6
6 >
1,2,3-
Trichloroben�enc
>
z z
a a
z
z z
z z
z
z
>
1,2,4-
Trimediy1benzene
z z
>
z z
>
z z
� >
z z
> >
z
> >
I
>
> >
Carbon Disulfide
,ggg...66,666.6.6.66,666,
9 A
z z
z
A
Dibromoddoromethi
ne
g
I
gIdzIzIz.
a
z
v 0
z
0 w
z
z z.
6 i 5
6 6
6
Chlorobenzene
1
>
9
z
6
6 6
6 6
z z
z. 6
6 z
z z
>
tert-Butylbenme
Z Z
z
z z
z �5
25 'Z
z
Z Z
z
z 9
2-Butmone
Z.
>' 'a
6 >'
6 z.
z. z
.6 6
6 6
6 8
Meth) lene Chlonde
z
z
z z
z
z
z
>
>
> >
> �
>
>
> >
>
Acetone

Sarnple ID
Q
Q
zS
e
Sarnpling Date (mmIdd/y,
s
2
a a
2 2
a a
2 6—
4 a
2 2
A a
2 6
a a
2 2
a
2
>
> >
z
>
Chloroethane
V
8 a
6
1; a
8 a
> >zl>zlz>
�z >z
>T
>
> >
z g
a
a 6
a 6
z
z z
z z
sec-Butylbenzene
8 8
8 8
g s
> z>
� z
> >
. z
> >
z z
> >
z z
> >
z
> z
6
6
6 6
6 6
z z
z 6
z. Z.
Z. zv
>z
1,2-Dichlorobenzene
9 9
z
z
z z
> >
z
� Z>
z �
> >
z z
� >
z 9
z a
9 a
a
6
z z
6
z 6
z 6
6 6
9
1,4-Dichlorobenme
>z
z z
> >
z z
> >
z z
> >
z z
> >
z z
> >
z z
> �
z
>
z
v
z z
a v
z
v
z 6
z.
z. z.
1,2,4-
rrichlorobenzene
z z
>
> z
>
> >
IZI-
> >
> >
-
> >
>
z
0
I
6
01 Oz
-
0
H
6
+161+161Z
>
IT
T.
I I
Z
>' >'
-
9 >Z
z .
> >
z z
> >
z z
> >
I I
z z
> >
A
>
HI
x
6
. z
..E6zO,Oz.z.z..zz.6>z
g gig
g8l
g
a A
g
g
9
9 9
9 g
9 9
la I
8
z
z z
> >
z z
> >
z z
> >
z z
> >
z
>
z
>
6
Carbon Disulfide
8
a a
11 9
9 9
9 9
6 &
g
a
6 a
a A
a a
a
9
.
Dibromochloronwtha
E
8
9 8
E R
R
R
a
z
6
6 zu
z. 6
66 z
z z
. .
z z
. .
z
. .
6
ne
z
z x
z z
z
z
6,166.666
Chlorobenzene
8 s
s s
s 8
7,�
19
z>
X�
�z IX
1
z
6
6 z
a
w 6
6 6
z Z
0
6 z
0
z 6
Z
>
tert-Butylbenzene
z
z
z z
> >
z z
> >
z z
> >
a5
> >
> >
> >
+IzI-I>
>
z
>
2-Butanone
6^
8
Tls�
-
z
�z 6
z> 6
6 �
6 6
z 6
v
z z
> 0
x 6
al
z
Methylene Chloride
z
z
Z>
z
z
>
s >
>1 �
>z >z
>Z
>
Acetone

Sample ID
ZZ
.3
2
Sampling Date (mm/dd/y
>
0
Z; 7
g a
.6
A
9
9
Chloroethane
g a
a
z
z z
> >
z z
> >
>
> >
1z1z1z1
> >
>
sec-Butylbenzene
>
z z
> >
z
>
z>
>z >z
>z >
z z
>
1,2-Dichlorobenzme
z z
z z
IZI
z
z
z .
z z
z z
z z
1,4-Dichloroben.me
> >
> >
>
8
8 >
> >
> >
> >
>
a
z
z z
z
z z
1 �2,4-
>1
>
z
>
> >
> >
> 0
Trichloroberuene
z
z
Z 4
A
g A
A z
z zIzIzI-
z
1,2,3-
8 8
>
>
v 8
8 8
9
9 >
>
> >
>
>
Trichlo.=e
81ZIA.8
a
g g18
a
a
z
1,2,4-
, >
z z
> >
z
>
.
. .
. .
z
>
.
z z
> >
z z
> >
1
z
0
Trimethylbenme
C-bon Distr1lide
z
z
I
S S
g Lz
9 9
a
4; a
a a
a
A
A z
Dibrornochlorometha
1
1
ZIAIA
ne
8
8
9
a
A
z
ChlGrobewene
S S
8
g g
S 8
g 8
S
&
9
z
z z
8 8
z
> Z�
>1
>1
z
E
Epp
>
> >
> >
Izi-
tert-Butylben�ene
t,
g
a
z A
8 a
a 9
9
a 1.
6
A g
g g
8 *4
a
6
2-Butanone
o 6
b
2
6
G
G
S
Methylene Chloride
9
z
z
8
>
6
6 6
b
b >
Acetone

Sarnple ID
tv
r
G
23 S'pling Date (mm/dd/y,
2
2 E
2 2
2 2
Chloroethme
z
>
>
zrm,IWI�
> >
> >
z z
> >
9 z
>
sec-Butylberume
z
>
z z
> >
z z
> >
z
>
z
> >
z
> >
z
> >
b
z z
> >
z
>
1,2-Didilorobenzene
>
z z
> >
z
> >
>
Ilz
z z
> >
z z
> >
z z
>
z z
> >
z z
> >
z
>
>
1,4-Dichlorobenzwe
z z
>, >z
>'
>z z
z z
>
z z
>
'I a
I as
z z
> >
z z
> >
I
z
>
1,2,4-
Trichl.roben,ene
z
z
> >
z z
> >
z
>
z z
z z
> >
z z
> >
9
z �
> >
z z
> >
A
>
Z
>
z
>
z z
> >
z z
>
z
>
z z
> >
z �
> >
z z
> >
8
>z z
>
> >
zlzlzlllz
>
>
8
g
1,;
11 8
a a
A a
a a
A A
a
a a
8 a
8i a
Cubon DisWfide
g
A g
a a
A
a
Dibromochloromefl,
6
8 8
Chlorobenzene
Z
z
z
>
z
Z,
Z,
Z� I>
z z
Z z
> >
z
>
z
>
z
lert-Butylberrnne
g 4
a
8 a
2-Butanone
Methylene Chloride
z
6- 6-
6- 2
6-
b-
a a
a 2
a a
a a
a
a
Acetorre
>

Sarnpl� ID
>
L
z�
Z� Z�
�tl.
z!
!C!
�arnphng Date (—Vddly,
2 22
2
2
2 0
2
2
2 2
2 2
s 8
El
D-1-d ..Ygt. (DO)
> >
>
>Z
z
5.,
Z>
te
>Z
>
IzI
>
Izi+
Cali—
z z
> >
z
>
6
8 z
— >
z
>
Z>
A 8
�84
A,
I
6 8
1� Mth.-
>Z
>
>Z
F—, I..
z
a Oxaclation reduction
>
pountud (ORP)
z
>
z
>
F;
>Z
Z>
Z>
Z> Z>
>Z
z
>
z z
> >
z
>
Z
>
Z
>
Z
>
Z
>
A Ikahnity
z z
> >
>Z
Z Z
>
Z Z
T >
Z Z
IT
Z
>Z 7>
z
>
>Z Z>
z
>
Z>
Z>
Chloride (optimal)
-0
Z
>
Conductivity
P H
;5 Z:;
u,
Z;
P W.
U, Z
>
Z;; Zz
Z
>
Tenpotatun,
z
>
c,
A
51
9
S Total organic carbon
I(TOC)
u,
1
.
. .
. .
.
Z>
I'M
>
IZ
0�8
9 thane
8 A
A A
S
IN
!ft
,
!r
>
A
A
A
6 8
Ether,

Table 12: Analytical Data for Natural Attenuation Parameters
HE
�5
I
Uniu,
.211,
.29�
-9/L I
-WL I
mwL
RIL
V
R/L
mWL
pstcrr?
md urut I
C
mg/L I
mv/L
mg/L
3/10/2005
9.3
067
�1.0
NA
<0,026
288
10
10
'o
2.0
5.58
17.5
NA
<0.026
<.026
1111212008
6.54
NA
NA
NA
NA
NA
37803
NA
NA
A
182
6.05
17.62
2.6
NA
NA
2/4/2009
OIS8
NA
NA
NA
NA
NA
158
NA
A
NA
25
4a66
1127
0.385J
NA
NA
VM009
IN
NA
NA
NA
NA
NA
160.4
NA
NA
A
K
NA
4653
1834
<140
NA
NA
7/16/2009
2.96
NA
NA
NA
NA
NA
129.4
NA
NA
NA
NA
4.68
21.5
<160
NA
NA 1
9/15/2009
7.69
NA
NA
NA
NA
NA
127.8
NA
NA
NA
NA
4.73
21.68
<160
NA
NA
ion/2009
5.65
NA
NA
NA
NA
NA
4968
NA
NA
NA
22
3.96
20.81
<1.0
NA
NA
2/4/2010
7.94
NA
NA
NA
NA
NA
152.1
NA
NA
MA
4.7
15.07 1
0.24J
NA
NA
2
4/22/2010
6.77
NA
NA
NA
NA
NA
NA
246
NA
NA
NA
4.79
18.94
0.65J
MA
NA
7/14/2010_
6d58
NA
NA
NA
NA
NA
152.2
NA
NA
21
4191
2.78
NA
NA
NA
10/21/2010
0
7.41
NA
NA
NA
NA
NA
NA
180.6
NA
NA
NA
4495
22.31
NA
NA
NA
4/25/2011
NA-
NA
NA
NA
NA
NA
NA
139.4
NA
NA_
NA
4d98
22663
NA
NA
NA
11/212011
6.58
NA
RNA
NA
NA
NA
NA
190.2
NA
NA
NA
5.02
20.49
NA
MA
NA
7119f2012
6036
0.355
0.316
NA
<.]I
ND
51
NA
NA
22
4q93
26mO7
0.316J
<.23
-M431
MW-813
12/3/2012
6d 19
0.467
<5.0
NA
<0.00003
ND
210.2
NA
NA
50
4.97
1 19.02
<5.0
<0400023
<D400031
2/29/2013
5.79
NA
0. 127J
NA
<0.00011
ND
12244
NA
NA
20
5.34
15d I
0.78J
<0.00023
�M.00031
5/30/2013_
6,21
0.317
0.334
NA
NA
ND
96.2
NA
NA
22_
4472
26
0.39J
NA
NA
9/11/2013
5.71
0.348
0.397
NA
-Od00011
1.1
264.3
NA
NA
20
4.33
21.67
04218J
<.00023
<q00031
12/1212013
6.6
0.468J
0.419
NA
0.00011
ND
27043
NA
NA
16
4.47
13.54
0. 246J
<.00023
<.00031
3/25/2014
Od43
<.O
NA
<.0026
ND
74.5
NA
NA
33
5.35
12.58
�0.50
<0.0028
1 <,0038
6/19/2014
_4.44
3
Od4I
<mo
NA
0.006
ND
29667
NA
NA
24
3438-
30658
0628J
<0.0028
8
<.0038
9125/2014
L23
0.29
<.O
NA
0181
012
80.5
NA
NA
19
4.8
20.93
0.34J
W28
<.0028
<.0038
1211612014
0.7
0.30
<2.0
NA
2.5
-ND
180.2
2
'20.2
NA
NA
19
6163
17.96
0.43J
.2.
<.0028
<.0038
3/19J2015
1.61
0.35
NA
1.9
A
NA
20 2
NA
NA
24
4.94
15.93
0696
<0.0028
_2.
<.0038
6117/2015
0.57
0.26
0.94J
NA
2
ND
238.4
NA
NA
20
3.78
21.64
<.50
PW2
-Qd0028
<Ow0038
9/1612015
Oq64
0.27
16
NA
31000
0.15
185.0
NA
NA
27
5.21
22.11
0.42J
-*,0028
<Oq0038
12/16/2015
0.41
Oq 12
<.O
NA
6.4
OA
69q8
FNA127.7
NA
NA
25
5.28
20.83
0.98
�D60028
<.0038
3/17/2005
904
0.35
7.65
NA
<.026
ND
183
40
15
3.0
t 6.7
17.1
1 NA
-M.026
.0, .
-�04026
2/6f2OO6
9.57
NA
NA
NA
<0.0002
NA
NA
NA
NA
NA
NA
NA
NA
�0.0002
<.0003
7/15/2009
4.85
NA
NA
NA
NA
NA
NA
A
1
i 92
LIA
NA
MW-9
Z/1112
7.6
NA
A
A
A
NA
�69
NA
NA
24
H321
21T
NA
NA
NA
A.
NA
NA
"A
NA
�3
8;
NA
70
434
23 02
NA
NA
NA
H/1/2011
NA-
--M�
NA
NA
NA
NA
1 264
NA
NA
25
2069
NA
NA
NA
P.p 2 f 30

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Table 12: Analytical Data for Natural Attenuation Parameters l
DSCA ID No.: DC920001QQ
d
E
o
-
Units
m
/L
mV
mWL
vJL
PSICO
std it
° C
12/3/2012
5.09
NA
NA
NA
NA
NA
154.6
NA
NA
140
6.87
16.59
NA
NA
NA
2/252013
7.09
NA
NA
NA
NA
NA
116
NA
NA
164
6.94
12.66
NA
NA
NA
5/312013
6.9
NA
NA
NA
NA
NA
67.4
NA
NA
167
5.9
25.99
NA
NA
NA
9/132013
5.2
NA
NA
NA
NA
NA
106.9
NA
NA
158
6.98
28.32
NA
NA
NA
12/112013
8.27
NA
NA
NA
NA
NA
194
NA
NA
265.5
6.93
10.6
NA
NA
NA
8405
3272014
4.8
NA
NA
NA
NA
NA
103.7
NA
NA
165
6.95
14.79
NA
NA
NA
Azalea
6/202014
7.56
NA
NA
NA
NA
NA
171.8
NA
NA
170
5.12•
25.27
NA
NA
NA
9222014
6.86
NA
NA
NA
NA
NA
63.5
NA
NA
147
6.4
20.84
NA
NA
NA
IV192014
6.3
NA
NA
NA
NA
NA
151.5
NA
NA
115
7.71
13.29
NA
NA
NA
3/162015
9.77
NA
NA
NA
NA
NA
102.7
NA
NA
178
5.37
17,04
NA
NA
NA
6/15/2015
6.44
NA
NA
NA
NA
NA
65.1
NA
NA
257
8
22.27
NA
NA
NA
12/142015
4.83
NA
NA
NA
NA
NA
82.1
NA
NA
140
7.03
15.93
NA
NA
NA
2252013
5.49
NA
NA
NA
NA
NA
138.9
NA
NA
58
5.64
11.94
NA
NA
NA
8408
9/132013
3.61
NA
NA
NA
NA
NA
203
NA
NA
59
5.58
22.39
NA
NA
NA
Azalea
9222014
5.78
NA
NA
NA
NA
NA
171.6
NA
NA
56
5.42
21.11
NA
NA
NA
9/142015
6.90
NA
NA
NA
NA
NA
191.7
NA
NA
47
6.90
19.51
NA
NA
NA
8409 Azata
9/142015
6.02
NA
NA
NA
NA
NA
147.5
NA
NA
48
6.90
19.29
NA
NA
NA
8412 Azalea
3/162015
I0.85
NA
NA
NA
NA
NA
101.1
NA
NA
94
5.59
16.79
NA
NA
NA
*Indicates dissolves) oxygen and/or pH was not analyzed or enoneous due to instmmentation malfunction.
**Sample wm recollecte l on 4/1/2013 for nitrate and nitrite walysis.
"'Formerly injection well (I W ).
NA - Not Analyzed
NS - Sample not collected
Psge 15 of 30

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DSCA ID No.: DC920001
C
9
&
F�
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g
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g
�
ttthhhtl
Units
Im
m /L
m
mwJL
Im
mRfL
ImwL
m
m
mwL
mg/L
3/112005
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
2/62006
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
7/142009
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
10/72009
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
2/42010
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
4212010
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
7/132010
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
10202010
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
4/262011
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
7/272011
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
II/12011
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
1/252012
NA
NA
0.0171
a0.01
<.05
NA
NA
NA
NA
NA
NA
7/202012
<0.01
0.0123
0.245
<0.01
<0.05
ND
ND
0.07
ND
ND
NA
y1q.�UA
12/32012
d.002
0.0195
0.0161
m.01
<0.05
0.8
ND
ND
ND
ND
NA
2/272013
0.0436
00645
0.0141
0.324
�*.05
0.14
ND
ND
ND
ND
NA
5/292013
0.00195J
0.0245
0.0121
.0.01
<0.05
0.2
ND
ND
ND
ND
NA
9/122013
NA
0.0243
1 0.0321
0.907
1 <0.05
NA
NA
NA
NA
NA
NA
12/13/2013
0.0165
0.166
0.0081
<0.05
<0.05
0.14
ND
ND
ND
ND
NA
3/262014
0.0031
0.022
<0.30
<0.010
*.0
0.1
ND
ND
ND
ND
NA
6/172014
0.0012
0.02
<0.30
NA
<2.0
0.75
ND
ND
ND
ND
NA
9/252014
0.00181
0.029
m.30
0.0045J
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NA
NA
ND
ND
ND
NA
12/162014
.00131
0.0017
<0.30
0.00401
Q.0
ND
ND
ND
ND
ND
NA
3/182015
0.0097
0.031
0.151
0.00471
<2.0
ND
ND
ND
ND
ND
NA
6/182015
0.0012J
0.017
-10.30
1 0.0025J
<2.0
ND
I ND
ND
I ND
ND
NA
0.0101
0.013
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<.010QQ0.25
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NA
211.720115S
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0.0054
�.30
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000.000911
7.68
2/6/2006
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
MW-10B-A
2162006
NA
NA
NA
1 NA
1 NA
I NA
NA
NA
NA
NA
NA
Page 18 of 30

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Table 12(l): Analytical Data for Natural Aftenuation Parameten (User Specified Parameten)
DSCA ID No.: DC920001
it
z
Units
I mg/L
.2/1,
a/L
R/L
I mg/L
R/L
I mwL
mg/L
=/L
R/L
mg/L
I
1213/2012
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
A
NA
2/25/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
5f3l/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9/13/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
A
NA
NA
12/11/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
R
NA
3127/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
8404 C...Ili�
6120/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9f22/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12119/2014
NA
NA
A
NA
NA
NA
NA
NA
NA
NA
NA
NA
3/16/2015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
6/15/2015
NA
NA
A
NA
NA
NA
NA
NA
NA
NA
NA
NA
112011
NA
NA
NA
RNA
NA
NA
NA
NA
NA
NA
NA
NA
NA
T21
NA
NA
NA
NA
NA
NA
NA
NA
NA
MA
NA
NA
12/3/2012
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA_
NA
2/25/2013
NA
NA
NA
NA
NA
NA
A
NA
NA
NA
NA
NA
NA
5/31/2013
NA
NA
NA
NA
NA
NA
A
NA
NA
NA
NA
NA
NA
9/13/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12/11/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
3/27/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9405 C—Ilia
6/20/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9/22/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12/19/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
3/16/2015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
6/15/2015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9/14/2015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12/14/2015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12/312012
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
2/25/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
5/31/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA_
NA
9/13/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12/11/2013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
3/2712014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
8408 Co —Ilia
6/20/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9/22/2014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
A
12/19/2014
NA
NA
N
NA
NA
NA
NA
NA
NA
NA
A
1 3/16/2015
1 NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
L/!
1 NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
A
L
T5/22
9/ /.2
oj�
5
NA
NA
NA
NA
NA
NA
NA
NA
NA
_T__
A
NA
12114/2015
1 NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
P.p28.M

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Table 12 1 : Analytical Data for Natural Attenuation Parameters User S ecified Parameters 1
DSCA TD No.: DC920001
q
_
�
F
e
w
12
e
i5
3
Units
m
m /L
-WL
m
m
mwL
m
m
12/32012
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
2/252013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
5/312013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9/132013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12/112013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
8405
3272014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Azalea
6/202014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9222014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
12/192014
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
3/162015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
6/152015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
IV142015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
2252013
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
8408
9/OMB
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Azalea
92220I4
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9/142011
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
8409 A.W.
9/142015
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
9412 AM.
3/16/2015
NA
NA
NA
NA
NA
NA
NA
NA
NA
r NA
NA
*Indicates dissolved
oxygen and/or
pH was not
analyzed
or ertoneous
due to instrumentation
malfmaion.
"*Sample was r hoed on 4/1/2013 f nitmte end nitrite analysis.
—Formerly injection wc11(IW).
NA - Not Annlyecd
NS . Sample not collected
Page 30 of 30

PF,
Former Pro Cleaners
Permit No. WQ0035324
APPENDIX D
LABORATORY ANALYTICAL REPORTS
February 22, 2016
Page 6

Table of Contents
con-Ust"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 28, 2015
Justin Ballard
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: 8379 Creedmoor Rd., Raleigh
Client Job Number:
Project Number: DC92015L33
Laboratory Work Order Number: 15LO822
Enclosed are results of analyses for samples received by the laboratory on December 15, 2015. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
I Page 1

Table of Contents
Table of Contents
Sample Summary
4
Case Narrative
5
Sample Results
6
15LO822-01
6
15LO822-02
12
15LO822-03
14
15LO822-04
16
15LO822-05
18
15LO822-06
20
15LO822-07
22
15LO822-08
24
Sample Preparation Information
26
OC Data
28
Volatile Organic Compounds by GC/MS
28
B137934
28
Miscellaneous Organic Analyses
32
B138318
32
Metals Analyses (Total)
33
B137816
33
B138379
33
Metals Analyses (Dissolved)
34
B137936
34
B138389
34
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
35
B137818
35
I Page 2

Table of Contents
Table of Contents (continued)
B1 37822
B137915
B137921
B138131
B138190
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
35
35
35
35
36
37
38
41
I Page 3 o:f:4::4::::]

Table of Contents
con-ttst"')
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL, 413/525-2332
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121 REPORT DATE: 12/28/2015
Raleigh, NC 27604 PURCHASE ORDER NUMBER:
AM: Justin Ballard
PROJECT NUMBER: DC920151,33
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 15LO922
The results of analyses perfbrmed on the following samples submitted to the CON -TEST Analytical Laboratory are fiaund in this report.
PROJECT LOCATION: 8379 Creedmoor Rd., Raleigh
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
MW 24S
15LO922-01
Ground Water
3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 NI-13 C
SM21-22 450OS-F
SW-846 6020A
SW-846 8260B
8401 WSW
15LOS22-02
Water
SW-846 8260B
8404 CD WSW
15LO822-03
Water
SW-846 8260B
8405 CD WSW
15LO822-04
Water
SW-846 8260B
8408 WSW
15LO822-05
Water
SW-846 8260B
8409 WSW
15L0822-06
Water
SW-846 8260B
8405 WSW
15LO822-07
Water
SW-846 8260B
8404 WSW
15LO822-08
Water
SW-846 8260B
I Page 4

Table of Contents
41 con-UsV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL, 413/525-2332
CASE NARRATIVE SUNINIARI
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
SW-846 8260B
Qualifications:
V-20
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
A.ady. 8, Samples(s) Qualified:
Bromomethane
B 137934-BS 1, B 137934-BSD I
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I cer* that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best ofmy knowledge and belief, accurate and complete.
I
Johanna K. Harrington
Manager, Laboratory Reporting
I Page 5 of 44 1

Table of Contents
0 con -test ®R
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample#: NM 24S Sampled: 12/14/2015 17:30
Samvle ID: 15LOS22-01
Samvle Matrix: Ground Water
Volatile Organic Compounds by GUMS
Anslyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Date
Prepared
DatefTime
Analyzed
Analyst
Acetone
ND
0.050
0.0049
-91L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Benzene
ND
0.0010
0.000079
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
NWF
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/17/15
12119/15 9:04
MFF
Bromodichloromethane
ND
0.00050
0.000098
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Bromoform,
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
112/17/15
12/19/15 9:04
MFF
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Carbon Disulfide
ND
0.0040
0.0010
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Carbon Tetrachloride
ND
0.0050
0.00012
mg(L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Chlorobenzene
ND
0.0010
0.00016
mg(L
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Chloroethane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Chloroform
ND
0.0020
0.00022
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19115 9:04
MFF
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
1,2-DicMorobenzene
ND
0.0010
0.00010
-91L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
IIJ-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
1,2-Dichloroethane
ND
0.0010
0.00019
M91
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
IJ-Dichloroethylene
ND
0.0010
0.00021
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
cis- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19il5 9:04
MFF
trans- 1,2-Dichloroethylene
ND
0.0010
0.00015
-91
1
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
1,2-Dichloropropane
ND
0.0010
0.00013
M91
I
SW-846 9260B
12/17/15
12/19115 9:04
MFF
1,3-Dichloropropane
ND
0.00050
0.00011
1-9/1-
1
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12117/15
12/19/15 9:04
MFF
IJ-Dichloropropene
ND
0.0020
0.00013
mg;(L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
cis- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Ethylbenzene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
p4sopropyltoluene (p-Qymene)
ND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
4-Mediyl-2-pentanone (MlBK)
ND
0.010
0.0015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MIFF
I Page 6

con-tcsV'
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LOS22
Date Received: 12/15/2015
Field Sample#: MW 24S Sampled: 12/14/2015 17:30
SaInDle ID: 15LOS22-01
Samvle Matrix: Ground Water
Volatile Organic Compounds by GUMS
Date
DatetTime
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
n-Propylbenzene
ND
0.0010
0.00011
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Styrene
ND
0.0010
0.00015
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/17/15
12119/15 9:04
MFF
Tetrachloroethylene
0.014
0.00050
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Toluene
0.00031
0.0010
0.00010
mg/L
I
J
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
NWF
1, 1, 1 -Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Trichloroethylene
ND
0.0010
0.00020
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Trichlorofluoromedme (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-946 8260B
12117/15
12/19/15 9:04
MFF
1,2,3-Trichloropropane
ND
0.0020
0.00019
mgIL
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 9:04
MFF
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
WF
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
m+p Xylene
ND
0.0020
0.00025
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
o-Xylene
ND
0.0010
0.00013
mg(L
I
SW-846 8260B
12/17/15
12/19/15 9:04
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
99.8
70-130
12/19/15 9:04
Toluene-d8
100
70-130
12/19/15 9:04
4-Bromofluorobenzene
97.1
70-130
12/19/15 9:04
I Page 7

Table of Contents
con-tcst"�'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: %�orkOrdeF. IiI,0822
Date Received: 12/15/2015
Field Sample#: MW 24S Sampled: 12/14/2015 17:30
Samnle ID: 15LOS22-01
Samitile Matrix: Ground Water
Miscellaneous Organic Analyses
[hite
DatelTime
Analyte Results
RIL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00098
mg/L 1
3810-RSK175
12/22/15
12/22/1515:51
TPH
Ethene ND
0.0038
0.00099
Ing/L I
3910-RSK175
12/22/15
12/22/15 15:51
TPH
Methane ND
0.0026
0.0011
mg/L I
3810-RSK175
12/22/15
12/22/15 15:51
TPH
I Page 8

0 con-tcst'o'
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample #: NM 24S Sampled: 12/14/2015 17:30
Samole ED: 15LOS22-01
Samole Matrix: Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution FlngtQual Method Prepared Analyzed Analyst
Manganese 110 2.0 0.23 Pg/L 2 SW-846 6020A 12/23/15 12/24/1513:37 KSH
I Page 9 of 44 1

Table of Contents
0 con4esto
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA 01028 *FAX [phone] *TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LOS22
DateReceived: 12/15/2015
Field Sample#: MW 24S Sampled: 12/14/2015 17:30
Sanmle ED: 15LOS22-01
Samvle Matrix, Ground Water
Metals Analyses (Dissolved)
Date DatetTime
Analyte Results RL DL Units Dilution FlagtQual Method Prepared Analyzed Analyst
Manganese 20 2.0 0.23 pg/L 2 SW-846 6020A 12/23/15 12/28/15 10:51 MJH
I Page 10

Table of Contents
con -test'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 0 1028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO922
Date Received: 12/15/2015
Field Sample#: MW 24S Sampled: 12/14/2015 17:30
Samule ID: 15LOS22-01
Sample Matrix: Ground Water
Conventional Chenibtry Parameters by EPA/APHA/SW-846 Methods (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution FlagtQual
Method
Prepared
Analyzed
Analyst
Ammonia as N
0.26
0.30
0.22
mg/L
I J
SM19-22 4500 NH3 C
12/17/15
12/17/15 14:30
VAK
Nitrate as N
0.51
0.050
0.049
mg1L
I
SM 21-22 4500 NO3 F
12/17/15
12/17/15 14:10
JK
Nitrite as N
0.023
0.010
0.0020
mg/L
I
SM 21-22 4500 NO2 B
12/16/15
12/16/15 12:55
VAK
Sulfate
0.67
2.0
0.40
mg/L
I J
ASTM D516-07
12/21/15
12/21/15 13:10
NW11-1
Sulfide
ND
2.0
1.9
mg/L
I
SM21-22 450OS-F
12/16/15
12/16/15 15:15
DJM
Total Organic Carbon
ND
0.50
0.16
mg/L
I
SM 5310C
12/22/15
12/22/15 15:00
LL
I Page 11 of 44 1

Table of Contents
cont,testO
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order. 15LO822
Date Received: 12/15/2015
Field Sample #- 8401 WSW Sampled: 12/14/2015 15:10
Samole 111): 15LO822-02
SamDle Matrix: Water
Volatile Organic Compounds by GC/MS
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-946 8260B
12/17115
12/19/15 10:50
MFF
Benzene
ND
0.0010
0.000079
mg/L
SW-846 8260B
12/17/15
12/19115 10:50
MFF
Bromobenzene
NO
0.0010
0.00015
mg/L
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Bromochloromethane
NO
0.0010
0.00022
mg/L
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MIFF
Bromofbrm
ND
0.0010
0.00021
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
2-Butanone (MEK)
ND
0.020
0.0024
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
n-Butylbenzene
IND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MIFF
sec-Butylbenzene
NO
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Carbon Tetrachloride
NO
0.0050
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Chlorobenzene
NO
0.0010
0.00016
mg/L
1
SW-846 8260B
12/17/15
12119/15 10:50
MFF
Chlorodibromomethane
NO
0.00050
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Chloroethane
NO
0.0020
0.00028
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Chloroform
NO
0.0020
0.00022
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Chloromethane
NO
0.0020
0.00032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
2-Chlorotoluene
NO
0.0010
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
4-Chlorotoluene
NO
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg(L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
1,2-Dichlorobenzene
ND
0.0010
0.00010
mg(L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,3-Dichlorobenzene
ND
0.0010
0.00017
-91
1
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg(L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
I,I-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
IJ-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
cis- 1,2-Dichloroethylene
NO
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
trans- 1,2-DichlorDethylene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,2-Dichloropropane
NO
0.0010
0.00013
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,3-Dichloropropane
NO
0.00050
0.00011
Ing/L
I
SW-846 9260B
12/17/15
12/19/15 10:50
MFF
2,2-Dichloropropane
NO
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
IJ-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
cis- 1,3-Dichlorepropene
NO
0.00050
0.000062
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
trans- 1,3-Dichloropropene
NO
0.00050
0.00011
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
isopropylbenzene (Cumene)
NO
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
p-lsopropyltoluene (p-Cymene)
NO
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Methyl tert-Butyl Ether (MTBE)
Nb
0.0010
0.000090
mg/L
I
SW-846 8260B
12/17/15
12/19115 10:50
MFF
Methylene Chloride
NO
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
4-Methyl-2-pentanone (MIBK)
NO
0.010
0.0015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1 Page 12 of 44

Table of Contents
con-tcsV'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LOS22
Date Received: 12/15/2015
Field Sample#: 8401 WSW Sampled: 12/14/2015 15:10
Samole 111): ISLOS22-02
Sarmale Matrix: Water
Volatile Organic Compounds by GC/MS
Date
DatelTime
Analyte
Results
RL
DL
Units
Dilution Flag/Qua[
Method
Prepared
Analyzed
Analyst
Naphthalene
0.0020
0.0020
0.00012
-9/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
n-Propylbenzene
ND
0.0010
0.00011
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Styrene
ND
0.0010
0.00015
-9/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Toluene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
NffF
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,11.1-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1, 1,2-Trichloroethane
ND
0.0010
0.00012
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Trichloroethylene
ND
0.0010
0.00020
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
WF
Trichlorolluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
WF
Vinyl Acetate
ND
0.020
0.0014
Ing/L
1
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 10:50
MFF
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19/15 10:50
MFF
Surrogates
% Recovery
Recovery Limits
FlaglQual
1,2-Dichloroethane-d4
104
70-130
12/19/15 10:50
Toluene-d8
101
70-130
12/19/15 10:50
4-Bromofluorobenzene
95.6
70-130
12/19/15 10:50
I Page 13 of 44 1

Table of Contents
0 con-ttst's'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LOS22
Date Received: 12/15/2015
Field Sample#: 8404 CD WSW Sampled: 12/14/2015 14:45
Sample ID: 15LOS22-03
Sample Matrix: Water
Volatile Organic Compounds by GC/MS
Date
DatelTime
Amlyte
Results
RL
DL
Units
Dilution FlaglQuall
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Benzene
ND
0.0010
0.000079
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 11:17
WF
Brornobenzene
ND
0.0010
0.00015
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MIFF
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Bromodichloromethane
NID
0.00050
0.000088
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MIFF
Bromofbrm
ND
0.0010
0.00021
mgfL
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
2-Butanone (MEK)
ND
0.020
0.0024
M91L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MIFF
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
tert-Butylbenzene
ND
0.0010
0.00011
-9/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Carbon Tetrachloride
ND
0.0050
0.00012
mgfL
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Chlorobenzene
ND
0.0010
0.00016
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Chlorodibromornethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Chloroethane
ND
0.0020
0.00028
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
NFF
Chlorofbrm
0.00024
0.0020
0.00022
mgfL
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12117/15
12/19/15 11:17
MFF
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MIFF
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19115 11:17
MIFF
1,2-Dibromoethane (EDB)
ND
0.00050
0.000099
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
1,2-Dichlorobenzene
NID
0.0010
0.00010
mg1L
I
SW-846 8260B
12/17/15
12/19/15 11:17
NffF
1,3-Dichlorobenzene
NID
0.0010
0.00017
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg1L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
13-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
I,I-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12117/15
12/19/15 11:17
MFF
cis- 1,2-Dichloroethylene
0.010
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
NffF
trarL� 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MIFF
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
1,3-Dichloropropane
NID
0.00050
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
2,2-Dichloropropane
NID
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/19115 11:17
MFF
1,1-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
cig- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
?vlFF
trans- 1,3-Dichloropropene
ND
0.00950
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Diisopropyl Ether (DIPE)
NID
0.00050
0.00018
-9/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MIFF
Isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
p-isopropyltoluene (p-Cyrnene)
ND
0.0010
0.00012
-9/1-
1
SW-946 9260B
12/17/15
12/19/15 11:17
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Mediylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
4-Methyl-2-pentanone (MI13K)
ND
0.010
0.0015
-9/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
WF
I Page 1

0 con-UsV'
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/1512015
Field Sample #: 8404 CD WSW Sampled: 12/14/2015 14:45
Samule ID: 15LO822-03
Samvle Matrix: Water
Volatile Organic Compounds by GUMS
Date
Date(Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qua[
Method
Prepared
Analyzed
Analyst
Naphtha ene
ND
0.0020
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
S"e
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
1, 1,2,2-Tebrachloroethane
ND
0.00050
0.00013
mg/L
1
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
1
SW-846 8260B
12/17/15
12119/15 11:17
NWF
Toluene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFT
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
1,1,1-Trichloroethane
IND
0.0010
0.000094
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 11:17
WF
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-946 9260B
12/17/15
12/19/15 11:17
MFF
Trichloroethylene
0.0024
0.0010
0.00020
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
NWF
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
NUF
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:17
MFF
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
o-Xylene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:17
MFF
Surrogates % Recovery Recovery Limits FlngtQual
1,2-Dichloroethane-d4 103 70-130 12/19/15 11:17
Toluene-d8 100 70-130 12/19/15 11:17
4-BTomofluoTobenzene 96.7 70-130 12/19/15 11:17
I Page 15

Table of Contents
con-UstO
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO922
Date Received: 12/1512OY5
Field Sample #: 8405 CD WSW Sampled: 12/14/2015 13:05
Sample ED: 15LOS22-04
Sample Matrix: Water
Volatile Organic Compounds by GUMS
Date
DatetTime
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Benzene
ND
0.0010
0.000079
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Bromobenzene
ND
0.0010
0.00015
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
n-Butylbenzene
ND
0.0010
0.00010
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
tert-Butylbenzene
ND
0.0010
0.00011
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Carbon Disulfide
ND
0.0040
0.0010
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
NUF
Carbon Tetrachloride
ND
0.0050
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Chlorobenzene
ND
0.0010
0.00016
Ing/L
I
SW-946 8260B
12/17115
12/19/15 11:43
MFF
Chlorodibromomethane
ND
0.00050
0.00010
Ing/L
I
SW-846 9260B
12/17/15
12/19/15 11:43
MFF
Chloroethane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Chlorofbrm
ND
0.0020
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Chloromethane
ND
0.0020
0.00032
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
2-Chlorotoluene
ND
0.0010
0.00012
Ing/L
1
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
4-Chlorotoluene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
1,2-Dichlorobenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
NTF
IJ-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
IJ-Dichloroethylene
ND
0.0010
0.00021
mg1L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
cis- 1,2-Dichloroediylene
0.00056
0.0010
0.00015
mg/L
I J
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
trans- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,3-Dichloropropane
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MIFF
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
1, I-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
cis- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
Ethylbenzene
ND
0.0010
0.00013
mg/L
1
SW-846 8260B
12/17/15
12119/15 11:43
MFF
2-Hexanone (MBK)
ND
0.010
0.0015
mgfL
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
lsopropylbenzene (Cumene)
ND
0.0010
D.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0010
0.00012
mgfL
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
4-Methyl-2-pentanone (MlBK)
ND
0.010
0.0015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
I Page 16

Table of Contents
con-toto"
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028* FAX [phone]* TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample #: 8405 CD WSW Sampled: 12/14/2015 13:05
Sanmle 111): 15LOS22-04
Samvle Matrix: Water
Volatile Organic Compounds by GCtMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution FlagtQual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
n-Propylbenzene
ND
0.0010
0.00011
111911-
1
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1, 1,2,2-Tetrachloroefliane
ND
0.00050
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Toluene
ND
0.0010
0.00010
1119/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
1
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,1,1-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
Trichloroethylene
ND
0.0010
0.00020
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
WF
TTichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-946 8260B
12/17/15
12/19/15 11:43
MFF
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12119/15 11:43
MFF
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
WF
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 11:43
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qua]
1,2-Dichloroethane-d4
101
70-130
12/19/15 11:43
Toluene-d8
101
70-130
12/19/15 11:43
4-Bromofluorobenzene
96.6
70-130
12/19/15 11:43
I Page 17

Table of Contents
con-testo
ANALYTICAL LA130RATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: I SLO822
Date Received: 12/15/2015
Field Sample#: 8408 WSW Sampled: 12/14/2015 12:42
Sample 111): 15LOS22-05
Samvle Matrix: Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qua[
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Benzene
ND
0.0010
0.000079
mgtL
1
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Bromobenzene
ND
0.0010
0.00015
mgtL
1
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Bromoform,
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
tert-Butylbenzene
ND
0.0010
0.00011
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Carbon Disulfide
ND
0.0040
0.0010
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Carbon Tetrachloride
ND
0.0050
0.00012
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Chlorobenzene
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17115
12/19/15 12:10
MFF
Chlorodibromornethane
ND
0.00050
0.00010
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Chloroethane
ND
0.0020
0.00028
-8/1-
1
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Chloroform
0.00029
0.0020
0.00022
mg/L
I J
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Chloromethane
ND
0.0020
0.00032
mg(L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
2-Chlorotoluene
ND
0.0010
0.00012
mgtL
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
1
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
1,2-Dibromoediane (EDB)
ND
0.00050
0.000089
mg(L
1
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,2-Dichlorobenzene
ND
0.0010
0.00010
-9/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg(L
1
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
1
SW-846 8260B
12/17/15
12/19/15 12:10
NWF
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
I,I-Dichloroethane
ND
0.0010
0.00016
mg/L
1
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,2-Dichloroethane
ND
0.0010
0.00019
Ing/L
1
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
I,I-Dichloroothylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
cis- 1,2-Dichloroethylene
0.0037
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
ftms-1,2-Dichloroethylene
ND
0.0010
0.00015
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,3-Dichloropropane
ND
0.00050
0.00011
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
2,2-Dichloropropane
ND
0,0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
IJ-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MIFF
cis- 1,3-DichloTopropene
ND
0.00050
0.000062
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Ediylbcnzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
p-lsopropyltoluene (p-Cymene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
4-Methyl-2-pentanone (MlBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
I Page 18

Table of Contents
con-stest'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone]D5 * TEL. [phone]
project Location: 9379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample#: 8408 WSW Sampled: 12/14/2015 12:42
SamDle 111): 15LO822-05
Samnle Matrix: Water
Volatile Organic Compounds by GUMS
Date
Date(Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
MS/L
I
SW-846 8260B
12/17/15
12/19/1512:10
WF
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
NWF
Styrene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Toluene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-946 9260B
12/17/15
12/19/15 12:10
MFF
1, 1,1-Trichloroethaine
ND
0.0010
0.000094
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
1, 1,2-Trichloroethane
ND
0.0010
O.OD012
-9/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
Trichloroethylene
0.00068
0.0010
0.00020
Ing/L
I i
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 12:10
NWF
1,2,3-Trichloropropane
ND
0.0020
0.00019
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
NffF
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:10
MFF
Vinyl Chloride
ND
0.0020
0.00013
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
MFF
m+p Xylene
ND
0.0020
0.00025
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
NUF
o-Xylene
ND
0.0010
0.00013
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 12:10
NUF
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 103 70-130 12/19/15 12:10
Toluene-dg 101 70-130 12/19/15 12:10
4-Bromofluorobenzene 96.8 70-130 12/19/15 12:10
I Page 19 of 44

Table of Contents
con-tesV'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample #: 8409 WSW Sampled: 12/14/2015 12:20
Sanmle ID: 15LOS22-06
Samvle Matrix: Water
Volatile Organic Compounds by GUMS
Date
Date(Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NUF
Benzene
ND
0.0010
0.000079
-9/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
Bromoberizene
NO
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MIFF
Bromochloromethane
ND
0.0010
0.00022
mg/L
1
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 9260B
12/17/15
12/19/15 12:36
MFF
Bromoform
ND
0.0010
0.00021
mg1L
I
SW-946 8260B
12/17/15
12/19/15 12:36
NOF
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NUF
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
sec-Butylbenzene
NO
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
tert-Butylbenzene
ND
0.0010
0.00011
-91L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
Carbon Disulfide
NO
0.0040
0.0010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Carbon Tetrachloride
NO
0.0050
0.00012
1119/1-
1
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Chlorobenzene
NO
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NUF
Chlorodibromornethane
NO
0.00050
0.00010
mg1L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Chloroethane
NO
0,0020
0.00029
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Chlorofbrm
0.00049
0.0020
0.00022
mg/L
I J
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
2-Chlorotoluene
IND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
1,2-Dichlorobenzene
NO
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NUF
1,3-Dichlorobenzene
NO
0.0010
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NUF
Dichlorodifluoromethane (Freon 12)
NO
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NUF
IJ-Dichloroethane
NO
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NUF
1,2-Dichloroediane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
I,I-Dichloroethylene
NO
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
cis- 1,2-Dichloroethylene
0.0017
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
trans- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
1,3-Dichloropropane
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12119/15 12:36
MFF
2,2-Dichloropropane
ND
omio
0.00016
mg/L
I
SW-846 9260B
12/17/15
12/19/15 12:36
MFF
IJ-Dichloropropene
IND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
cis- 1,3-Dichloropropene
IND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MIFF
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
lsopropylbenzene (Cumene)
ND
0,0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
p-isopropyttol- (p-Cymene)
ND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MIFF
Methylene Chloride
ND
0.0050
0.0032
mg1L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
4-Methyl-2-pentanone (MMK)
ND
0.010
0.0015
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
I Page 20

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample#: 8409 WSW Sampled: 12/14/2015 12:20
Sanuale ID: 15LOS22-06
Samole M-strix: Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
Ing/L
I
SW-846 8260D
12/17/15
12/19/1512:36
NWF
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NffF
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-946 8260B
12117/15
12/19/15 12:36
MFF
Toluene
No
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
1,2,3-Trichlorobenzene
No
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
1,2,4-Trichlorobenzene
No
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
1, 1, 1 -Trichloroedianc
ND
0.0010
0.000094
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
klFF
1, 1,2-Tricliloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Trichloroethylene
No
0.0010
0.00020
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
1,2,3-Tricl-doropropane
ND
0.0020
0.00019
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 12:36
NlFF
1,2,4-Trimethylbenzene
No
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NlFF
1,3,5-Trimethylbenzene
NO
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
MFF
Vinyl Acetate
NO
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 12:36
NEF
Vinyl Chloride
NO
0.0020
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
MFF
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-946 8260B
12/17/15
12/19/15 12:36
NEF
o-Xylene
ND
0.0010
0.00013
mg/1-
I
SW-846 8260B
12/17/15
12119/15 12:36
NlFF
Surrogate,
*/. Recovery
Recovery Umits
Flag/Qual
1,2-Dichloroediane-d4
102
70-130
12/19/15 12:36
Toluene-d8
101
70-130
12/19/15 12:36
4-Bromofluorobenzene
98.3
70-130
12/19/15 12:36
I Page 21 of 44 1

Table of Contents
con-UsC'
ANALYTiCAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample 4: 8405 WSW Sampled: 12/14/2015 11:42
Sanmle ID: ISLO822-07
SaMDIC Matrix: Water
Volatile Org2nic Compounds by GC/MS
Date
Date/Timc
Analyte
Results
RIL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-846 260B
12/17/15
12/19/1513:03
MFF
Benzene
ND
0.0010
0.000079
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:03
WF
Bromochloromcdiane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
Bromomethane
ND
0,0020
0.00094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NIFF
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NIFF
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
sec-Butylbcnzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:03
MFF
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Carbon Tetrachloride
ND
0.0050
0.00012
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
Chlorobenzene
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/17/15
12119/15 13:03
MFF
Chloroethane
ND
0.0020
0.00028
mA
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Chloroform
ND
0.0020
0.00022
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NIFF
2-Chlorotoluene
ND
0.0010
0.00012
-g/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
N4FF
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/1-
I
SW-946 8260B
12/17/15
12/19/15 13:03
MFF
1,2-Dichlorobenzenc
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19115 13:03
N4FF
1,3-Dichlorobenzene
ND
0.0010
0.00017
-g4-
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
1,4-Dichlorobenzene
ND
0.0010
0.00015
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
IJ-Dichloroethane
ND
0.0010
0.00016
-9/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
1,2-Dichloroetbane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
IJ-Dichloroethylenc
ND
0.0010
0.00021
-g/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
cis- 1,2-Dichloroethylene
0.0023
0.0010
0.00015
-9/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
trans- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
1,2-Dichloropropane
ND
0.0010
0.00013
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
1,3-Dichloropropane
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
2,2-Dichloropropane
ND
0.0010
0.00016
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
IJ-Dichloropropenc
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
cis- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
IVIFF
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NffF
2-Hexanone (MBK)
ND
0.010
0.0015
-A
I
SW-846 8260B
12/17/15
12/19/15 13:03
NIFF
Isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:03
NIFF
p-Isopropyltoluene (p-Cymenc)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NEF
Page 2

Table of Contents
con -test 80
ANALYTICAL LABORATORY
39 Spruce Street - East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample 4: 8405 WSW Sampled: 12/14/2015 11:42
Saminle ID: 15LOS22-07
Samvle Mattix: Water
Volatile Organic Compounds by GUMS
Date
Dateffirne
Anallyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/1513:03
MFF
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NIFF
1,1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Toluene
ND
0.0010
0.00010
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 13:03
kffF
1,2,3-Triclilorobenzene
N D
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12119/15 13:03
MFF
1,1,1-Trichloroethane
ND
0.0010
0.000094
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
1,1,2-Trichloroetliane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Trichloroethylene
0.00035
0.0010
0.00020
mg/L
I J
SW-946 8260B
12/17/15
12/19/15 13:03
NffF
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:03
NfFF
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 13:03
NEF
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/1-
I
SW-946 8260B
12/17/15
12/19/15 13:03
MFF
1,3,5-Trimcthylbcnzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NIFF
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
WF
m+p Xylene
ND
0.0020
0.00025
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
NffF
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:03
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroetliane-d4
100
70-130
12/19/15 13:03
Toluene-d8
101
70-130
12/19/15 13:03
4-Bromofluorobenzene
96.6
70-130
12/19/15 13:03
I Page 23 of 44 1

Table of Contents
con-Usto"
ANALYTiGAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15L0822
Date Received: 12/15/2015
Field Sample 4: 8404 WSW Sampled: 12/14/2015 11:35
Samnle rD: 15LO822-08
Samole Matrix: Water
Volatile Organic Compounds by GC/MS
Date
DaterFime
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
Ing/L
I
SW-846 8260B
12117/15
12/19/1513:30
MFF
Benzene
ND
0.0010
0.000079
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 t3:30
MFF
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
Carbon Tetrachloride
ND
0.0050
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Chlorobenzene
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Chloroethane
ND
0.0020
0.00028
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Chloroform
0.0020
0.0020
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
2-Chlorotoluenc
ND
0.0010
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
4-Chlorotoluene
ND
0.0010
0.00013
MA
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1,2-Dibromoediane (EDB)
ND
0.00050
0.000089
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1,2-Dichlorobcnzene
ND
0.0010
0.00010
MA
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
1,3-Dichlorobenzene
ND
0.0010
0.00017
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Dichlorodifluoromedme (Freon 12)
ND
0.0020
0.00018
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
IJ-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
1,2-Dichloroethane
ND
0.0010
0.00019
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
I,I-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
cis- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
ftws-1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
1,2-Dichloropropanc
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1,3-Dichloropropanc
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
2,2-Dichloropropanc
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
IJ-Dichloropropene
ND
0.0020
0.00013
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
cis- 1,3-Dichloropropene
ND
0,00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 13:30
MFF
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NIFF
4-Methyl-2-pcntanone (MIBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
I Page 2

4 con-tcsto
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creedmoor Rd., Raleigh Sample Description: Work Order: 15LO822
Date Received: 12/15/2015
Field Sample#: 8404 WSW Sampled: 12/14/2015 11:35
S2nmle ID: 15LOS22-08
Samole Matrix: Water
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/1513:30
MFF
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NTF
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NIFF
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NIFF
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Toluene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1,2,3-Trictilorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1,1,1-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NIFF
Trichloroethylene
ND
0.0010
0.00020
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NIFF
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NfFF
1,2,3-Tricliloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
NfFF
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg4,
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Vinyl Acetate
ND
0.020
0.0014
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19115 13:30
WF
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/17/15
12/19/15 13:30
MFF
o-Xylene
IND
0.0010
0.00013
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 13:30
WF
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethanc-d4 103 70-130 12/19/15 13:30
Tolucne-d8 100 70-130 12/19/15 13:30
4-Bromofluorobenzene 97.4 70-130 12/19/15 13:30
P ---'I
age 25 of 44

Table of Contents
icon-tcsC'
ANALYTiCAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
3810-RSK175
Lab Number [Field ED] Batch Initial [mLj Final [mLl Date
15LO822-01 [MW 24S] B138318 1.00 1.00 12/22/15
ASTM D516-07
Lab Number [Field ID1 Batch Initial [mLJ Final ImLl Date
15LO822-01 [MW 24S] B 138190 100 100 12/21/15
SM 21-22 4500 NO2 B
Lab Number [Field ED] Batch Initial jmLJ Final [mLj Date
15L0822-01 [MW 24S] B137822 50.0 50.0 12/16/15
SM 21-22 4500 NO3 F
Lab Number [Field ED] Batch Initial [mLj Final [mLJ Date
15L0822-01 [MW 24S] B 137915 25.0 25.0 12/17/15
SM 5310C
Lab Number [Field ED] Batch Initial [mLj Final [mL] Date
15LO822-01 PAW 24S] B138131 50.0 50.0 12/22/15
SM19-22 4500 NH3 C
Lab Number [Field IDJ Batch Initial [mLj Final Inil-I Date
15L0822-01 [M-%V 24S] B137921 100 100 12/17/15
SM21-22 450OS-F
Lab Number [Field ED]
Batch
Initial [mLl
Final [mLj
Date
15LO822-01 [MW 24S]
B137818
100
100
12/16/15
Prep Method: SW-846 3005A-SW-846 6020A
Lab Number lField ED)
Batch
Initial [mLl
Final [mL]
Date
15LO822-OIREI [MW 24S]
B138379
50.0
50.0
12/23/15
Prep Method: SW-846 3005A Dissolved-SW-846 6020A
Lab Number [Field ED] Batch Initial JmL] Final [mLj Date
15LO822-0 IREI [MW 24S] B 138389 50.0 50.0 12/23/15
I Page 26 of 44

Table of Contents
con-atesto't
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 503OB-SW-846 8260B
Lab Number [Field ID] Batch Initial ImLl Final ImLl Date
15LOS22-01 [MW 24S]
B 137934
5
5.00
12/17/15
15LOS22-02 [8401 WSW]
B 137934
5
5.00
12/17/15
15LO822-03 [8404 CD WSW]
B 137934
5
5.00
12/17/15
15LO822-04 [9405 CD WSW]
B 137934
5
5.00
12/17/15
15LO822-05 [8408 WSW]
B 137934
5
5.00
12/17/15
15LO822-06 [9409 WSW]
B 137934
5
5.00
12/17/15
15LO822-07 [8405 WSW]
B137934
5
5.00
12/17/15
15LO822-08 [8404 WSW]
B137934
5
5.00
12/17/15
I Page 27

Table of Contents
con-atesV'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
QUALM CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source */oREC RPD
Analyte Result Limit Units Level Result %REC Limits RPID Limit Notes
Batch B137934 - SW-846 5030B
Blank (B137934-BLKI)
Acetone
ND
0.050
mg/L
Benzene
ND
0.0010
mg/L
Bromobenzene
ND
0.0010
mg/L
Bromochloromethane
ND
0.0010
mg/L
Bromodichloromethane
ND
0.00050
mg/L
Bromoform
ND
0.0010
mg/1-
Bromomethane
ND
0.0020
mg/L
2-Butanone (MEK)
ND
0.020
mg/L
n-Butylbenzene
ND
0.0010
mg/L
sec-Butylbenzene
ND
0.0010
mg/L
tcrt-Butylbenzene
ND
0.0010
mg/L
Carbon Disuffide
ND
0.0040
mg/L
Carbon Tetrachloride
ND
0.0050
mg/L
Chlorobenzenc
ND
0.0010
mg/L
Chlorodibromomcthane
ND
0.00050
mg/L
Chloroethane
ND
0.0020
-9/L
Chloroform
ND
0.0020
mg/L
Chloromethanc
ND
0.0020
mg/L
2-Chlorotoluene
ND
6.0010
mg/L
4-Chlorotoluene
ND
0.0010
mg/L
1,2-Dibromoetharie (EDB)
ND
0.00050
mg/L
1,2-Dichlorobenzene
ND
0.0010
mg/L
1,3-Dichlorobenzcne
ND
0.0010
1119/L
1,4-Dichlorobenzcne
ND
0.0010
mg/L
Dichlorodifluoromethane (Freon 12)
ND
0.0020
mg/L
I,I-Dichloroediane
ND
0.0010
mg/L
1,2-Dichloroethane
ND
0.0010
mg/L
1,1-Dichloroethylenc
ND
0.0010
mg/L
cis- 1,2-Dichloroediylene
ND
0.0010
mg/L
trans- 1,2-Dichloroethylene
ND
0.0010
-9/L
1,2-Dichloropropane
ND
0.0010
mg/L
1,3-Dichloropropane
ND
0.00050
mg/L
2,2-Dichloropropane
ND
0.0010
mg/L
IJ-Dichloropropene
ND
0.0020
mg/L
cis- 1,3-Dichloropropene
ND
0.00050
mg/1-
trms-1,3-Dichloropropene
ND
0.00050
mg/L
Diisopropyl Ether (DIPE)
ND
0.00050
1119/1-
Ethylbenzenc
ND
0.0010
mg/L
2-Hexanone (MBK)
ND
0.010
1119/1-
lsopropylbenzene (Cumene)
ND
0.0010
Ing/L
p-lsopropyltolucne (p-Cymene)
ND
0.0010
mg/L
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
1119/L
Methylene Chloride
ND
0.0050
mg/L
4-Medlyl-2-pentanone (MIBK)
ND
0.010
1119/L
Naphthalene
ND
0.0020
mg/L
n-Propylbenzene
ND
0.0010
mg/L
Styrene
ND
0.0010
Ing/L
1, 1,2,2-TetiAchloroethane
ND
0.00050
Ing/L
Tetrachloroethylene
ND
0.00050
mg/L
Toluene
ND
0.0010
1119/L
1,2,3-Trichlorobenzene
ND
0.0050
mg/L
1,2,41-Trichlorobenzene
ND
0.0010
mg/L
Prepared: 12/17/15 Analyzed: 12/19/15_ _ _ __
I Page 28 of 44 1

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALM CONTROL
Volatile Organic Compounds by GUMS - Quality Control
Reporting Spike Source %REC RPD
Utalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B137934 - SW-846 5030B
Blank (B137934-BLKI)
1,1, I-Trichloroediane
ND
0.0010
mg/L
1,1,2-Trichloroethane
ND
0.0010
mg/1-
Trichloroethylene
ND
0.0010
-9/1-
Trichlorofluoromediane (Freon 11)
ND
0.0020
mg/L
1,2,3-Trichloropropane
ND
0.0020
mg/L
1,2,4-Tximethylbenzenc
ND
0.0010
mg/L
1,3,5-Trimethylbenzene
ND
0.0010
Ing/L
Vinyl Acetate
ND
0.020
mg/L
Vinyl Chloride
ND
0.0020
mg/L
m+p Xylene
ND
0.0020
Ing/L
o-Xylene
ND
0.0010
-9/1-
Prepared: 12/17/15 Analyzed: 12/19/15
Surrogate: 1,2-Dichloroethanc-d4
Surrogate: Tolucn"8
Surrogate: 4-Bromofluorobcnzene
LCS (B137934-BS1)
0.0254
0.0254
0.0247
mg/L
-9/1-
mg/L
0.0250 101
0.0250 102
0.0250 98.8
Prepared: 12/17/15 Analyzed: 12/19/15
70-130
70-130
70-130
Acetone
0.0726
0.050
-9/1-
0.100
72.6
70-160
Benzene
0.0103
0.0010
mg/1-
0.0100
103
70-130
Bromobenzene
0.0104
0.0010
mg/L
0.0100
104
70-130
Bromochloromethane
0.0119
0.0010
mg/L
0.0100
119
70-130
Bromodichloromethane
0.00936
0.00050
-9/L
0.0100
93.6
70-130
Bromoform
0.00914
0.0010
mg/L
0.0100
91.4
70-130
Bromomethane
0.00739
0.0020
-9/1-
0.0100
73.9
40-160
V-20 t
2-Butanone (MEK)
0.0911
0.020
mg/L
0.100
91.1
40-160
t
n-Butylbenzene
0.00987
0.0010
-9/1-
0.0100
98.7
70-130
sec-Butylbenzene
0.0102
0.0010
Ing/L
0.0100
102
70-130
tert-Butylbenzene
0.00974
0.0010
Ing/L
0.0100
97.4
70-130
Carbon Disulfide
0.00921
0.0040
mg/L
0.0100
92.1
70-130
Carbon Tetrachloride
0.0104
0.0050
mg/L
0.0100
104
70-130
Chlorobenzene
0.00966
0.0010
Ing/L
0.0100
96.6
70-130
Chlorodibromomethane
0.00926
0.00050
mg/L
0.0100
92.6
70-130
Chloroethane
0.0114
0.0020
mg/L
0.0100
114
70-130
Chloroform
0.0102
0.0020
Ing/L
0.0100
102
70-130
Chloromethane
0.00864
0.0020
mg/L
0.0100
86.4
40-160
t
2-Chlorotoluene
0.0102
0.0010
mg/L
0.0100
102
70-130
4-Chlorotoluene
0.00967
0.0010
Ing/L
0.0100
96.7
70-130
1,2-Dibromoethanc (EDB)
0.0103
0.00050
mg/L
0.0100
103
70-130
1,2-Dichlorobcnzene
0.00925
0.0010
mg/L
0.0100
92.5
70-130
1,3-Dichlorobenzene
0.00977
0.0010
mg/L
0.0100
97.7
70-130
1,4-Dichlorobenzene
0.00927
0.0010
mg/L
0.0100
92.7
70-130
Dichlorodifluoromethane (Freon 12)
0.00434
0.0020
mg/L
0.0100
43.4
40-160
I,I-Dichloroethane
0.0106
0.0010
Ing/L
0.0100
106
70-130
1,2-Dichloroethane
0.00968
0.0010
Ing/L
0.0100
96.8
70-130
I,I-Dichloroethylene
0.00992
0.0010
1119/L
0.0100
99.2
70-130
cis- U-Dichloroethylene
0.0102
0.0010
Ing/L
0.0100
102
70-130
trans-1,2-Dichloroethylene
0.00993
0.0010
mg/L
0.0100
99.3
70-130
1,2-Dichloropropane
0.0104
0.0010
Ing/L
0.0100
104
70-130
1,3-Dichloropropane
0.0102
0.00050
mg/L
0.0100
102
70-130
2,2-Dichloropropanc
0.00855
0.0010
mg/L
0.0100
85.5
40-130
1,11-Dichloropropene
0.0101
0.0020
1119/1-
0.0100
101
70-130
cis- 1,3-Dichloropropene
0.00914
0.00050
mg/L
0.0100
91.4
70-130
trans- 1,3-Dichloropropene
0.00982
0.00050
1119/1-
0.0100
98.2
70-130
I Page 29

Table of Contents
con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source O/oREC RPD
Analyte Result Limit Units Level Result I/oREC Limits RPD Limit 'Note,
Batch B137934 - SW-846 5030B
LCS (Bl37934-BSI)
Prepared: 12/17/15 Analyzed: 12/19/15
Diisopropyl Ether (DIPE)
0.00974
0.00050
mg/L
0.0100
97.4
70-130
Ethylbenzenc
0.0102
0.0010
mg/1-
0.0100
102
70-130
2-Hexanone (M]BK)
0.0941
0.010
mg/1-
0.100
94.1
70-160
lsopropylbenzene (Cumene)
0.00999
0.0010
mg/L
0.0100
99.9
70-130
p-Isopropyltoluene (p-Cymene)
0.0107
0.0010
Ing/L
0.0100
107
70-130
Methyl tert-Butyl Ether (MTBE)
0.00976
0.0010
mg/L
0.0100
97.6
70-130
Methylene Chloride
0.00987
0.0050
mg/L
0.0100
98.7
70-130
4-Methyl-2-pentanone (MlBK)
0.0997
0.010
mg/L
0.100
99.7
70-160 t
Naphthalene
0.00857
0.0020
mg/L
0.0100
85.7
40-130 t
n-Propylbenzene
0.0101
0.0010
Ing/L
0.0100
101
70-130
Styrene
0.0101
0.0010
Ing/L
0.0100
101
70-130
1, 1,2,2-Tetrachloroethane
0.0106
0.00050
Ing/L
0.0100
106
70-130
Tetrachloroedlylene
0.00983
0.00050
mg/L
0.0100
98.3
70-130
Toluene
0.0102
0.0010
mg/L
0.0100
102
70-130
1,2,3-Trichlorobenzene
0.00852
0.0050
M8/L
0.0100
85.2
70-130
1,2,4-Trichlorobenzene
0.00911
0.0010
mg/L
0.0100
91.1
70-130
1, 1, 1 -Trichloroethane
0.00976
0.0010
mg/L
0.0100
97.6
70-130
1, 1,2-Trichloroethane
0.0103
0.0010
mg/L
0.0100
103
70-130
Trichloroethylene
0.0104
0.0010
-9/1-
0.0100
104
70-130
Trichlorofluoromethane (Freon 11)
0.00871
0.0020
Ing/L
0.0100
87.1
70-130
1,2,3-Trichloropropane
0.0107
0.0020
mg/L
0.0100
107
70-130
1,2,4-Trunediylbenzene
0.0102
0.0010
mg/L
0.0100
102
70-130
1,3,5-Tximethylbenzene
0.0105
0.0010
mg/L
0.0100
105
70-130
Vinyl Acetate
0.0943
0.020
mg/L
0.100
94.3
70-130
Vinyl Chloride
0.00785
0.0020
mg/L
0.0100
78.5
40-160
m+p Xylene
0.0202
0.0020
mg/L
0.0200
101
70-130
o-Xylene
0.00985
0.0010
mg/L
0.0100
98.5
70-130
Surrogate: 1,2-Dichloroethane-d4
Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene
LCS Dup (Bl37934-BSDI)
0.0255
0.0247
0.0248
mg/L
mg/L
mg/L
0.0250 102
0.0250 98.9
0.0250 99.0
Prepared: 12/17/15 Analyzed: 12/19/15
70-130
70-130
70-130
Acetone
0.0820
0.050
Ing/L
0.100
82.0
70-160
12.1
25
Benzene
0.0106
0.0010
Ing/L
0.0100
106
70-130
2.58
25
Bromobenzcne
0.0106
0.0010
Ing/L
0.0100
106
70-130
2.10
25
BromocWoromethane
0.0123
0.0010
mg/L
0.0100
123
70-130
3.47
25
Bromodichloromethane
0.00980
0.00050
Ing/L
0.0100
98.0
70-130
4.59
25
Bromoform,
0.00917
0.0010
-9/L
0.0100
91.7
70-130
0.328
25
Bromomethane
0.00761
0.0020
mg/L
0.0100
76.1
40-160
2.93
25
V-20
2-Butanone (MEK)
0.104
0.020
mg/L
0.100
104
40-160
13.4
25
n-Butylbenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
2.01
25
sec-Butylbenzenc
0.0102
0.0010
mg/L
0.0100
102
70-130
0.697
25
tert-Butylbenzene
0.00980
0.0010
mg/L
0.0100
98.0
70-130
0.614
25
Carbon Disulfide
0.00881
0.0040
mg/L
0.0100
88.1
70-130
4.44
25
Carbon Tetrachloride
0.0105
0.0050
mg/L
0.0100
105
70-130
0.382
25
CWorobenzenc
0.00965
0.0010
mg/L
0.0100
96.5
70-130
0.104
25
Chlorodibromomediane
0.00939
0.00050
mg/L
0.0100
93.9
70-130
1.39
25
Chloroethane
0.0109
0.0020
Ing/L
0.0100
109
70-130
5.02
25
Chloroform
0.0104
0.0020
Ing/L
0.0100
104
70-130
1.75
25
Chloromethane
0.00874
0.0020
Ing/L
0.0100
87.4
40-160
1.15
25
2-Cbiorotoluene
0.0102
0.0010
Ing/L
0.0100
102
70-130
0.0994
25
4-Chlorotoluene
0.0101
0.0010
-9/1-
0.0100
101
70-130
4.05
25
I Page 30 of 44 1

Table of Contents
con -test"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source 0/.REC RPD
Analyte Result Limit units Level Result 0/6REC Limits RPD Limit Notes
Batch B137934 - SW-846 5030B
LCS Dup (B137934-BSD1)
Prepared: 12/17/15 Analyzed: 12/19/15
1,2-Dibromoethane (EDB)
0.0101
0.00050
-9/1-
0.0100
101
70-130
1.87
25
1,2-Dichlorobenzene
0.00945
0.0010
1119/1-
0.0100
94.5
70-130
2.14
25
1,3-Dichlorobenzene
0.00975
0.0010
-9/1-
0.0100
97.5
70-130
0.205
25
1,4-Dichlorobenzene
0.00963
0.0010
-9/1-
0.0100
96.3
70-130
3.81
25
Dichlorodifluoromethane (Freon 12)
0.00460
0.0020
Mg/L
0.0100
46.0
40-160
5.82
25
IJ-Dichloroethane
0.0109
0.0010
Ing/L
0.0100
109
70-130
2.61
25
1,2-DicWoroethane
0.00952
0.0010
mg/L
0.0100
95.2
70-130
1.67
25
IJ-Dichloroethylene
0.0101
0.0010
mg/L
0.0100
101
70-130
2.09
25
cis- 1,2-Dichloroethylene
0.0101
0.0010
mg/L
0.0100
101
70-130
1.67
25
trans- 1,2-Dichloroethylene
0.0102
0.0010
mg/L
0.0100
102
70-130
2.29
25
1,2-Dichloropropane
0.0106
0.0010
mg/L
0.0100
106
70-130
2.67
25
1,3-Dichloropropane
0.0104
0.00050
mg/L
0.0100
104
70-130
2.43
25
2,2-Dichloropropane
0.00857
0.0010
mg/L
0.0100
85.7
40-130
0.234
25 t
IJ-Dichloropropene
0.0105
0.0020
mg/L
0.0100
105
70-130
3.78
25
cis- 1,3-Dichloropropene
0.00920
0.00050
mg/L
0.0100
92.0
70-130
0.654
25
trans- 1,3-Dichloropropene
0.0101
0.00050
-g/L
0.0100
101
70-130
2.61
25
Diisopropyl Ether (DIPE)
0.0100
0.00050
Ing/L
0.0100
100
70-130
3.03
25
Ethylbenzene
0.0103
0.0010
mg/L
0.0100
103
70-130
0.293
25
2-Hexanone (MBK)
0.107
0.010
mg/L
0.100
107
70-160
12.9
25
Isopropylbenzene (Cumene)
0.0101
0.0010
Ing/L
0.0100
101
70-130
0.798
25
p-Isopropyltoluene (p-Cymene)
0.0107
0.0010
mg/L
0.0100
107
70-130
0.187
25
Methyl tert-Butyl Ether (MTBE)
0.00995
0.0010
mg/L
0.0100
99.5
70-130
1.93
25
Methylene Chloride
0.0100
0.0050
Ing/L
0.0100
100
70-130
1.31
25
4-Methyl-2-pentanone (MIBK)
0.111
0.010
mg/L
0.100
111
70-160
11.0
25 t
Naphthalene
0.00994
0.0020
mg/L
0.0100
99.4
40-130
14.8
25 t
n-Propylbenzene
0.0101
0.0010
Ing/L
0.0100
101
70-130
0.297
25
Styrene
0.0102
0.0010
Ing/L
0.0100
102
70-130
1.29
25
1, 1,2,2-Tetrachloroethane
0.0110
0.00050
mg/L
0.0100
110
70-130
2.97
25
Tetrachloroethylene
0.00981
0.00050
Ing/L
0.0100
98.1
70-130
0.204
25
Toluene
0.0101
0.0010
Ing/L
0.0100
101
70-130
0.886
25
1,2,3-Trichlorobenzene
0.00943
0.0050
Ing/L
0.0100
94.3
70-130
10.1
25
1,2,4-Trichlorobenzene
0.00954
0.0010
mg/L
0.0100
95.4
70-130
4.61
25
1,11, I-Trichloroethane
0.00992
0.0010
Ing/L
0.0100
99.2
70-130
1.63
25
1, 1,2-Trichloroethane
0.0107
0.0010
mg/L
0.0100
107
70-130
3.24
25
Trichloroethylene
0.0104
0.0010
mg/L
0.0100
104
70-130
0.289
25
Trichlorofluoromethane (Freon 11)
0.00877
0.0020
Ing/L
0.0100
87.7
70-130
0.687
25
1,2,3-Txichloropropane
0.0111
0.0020
Ing/L
0.0100
111
70-130
3.68
25
1,2,4-Trimethylbenzene
0.0103
0.0010
mg/L
0.0100
103
70-130
0.782
25
1,3,5-Trimethylbenzene
0.0105
0.0010
-9/1-
0.0100
105
70-130
0.00
25
Vinyl Acetate
0.0984
0.020
mg/L
0.100
98.4
70-130
4.20
25
Vinyl Chloride
0.00772
0.0020
Ing/L
0.0100
77.2
40-160
1.67
25 t
m+p Xylene
0.0204
0.0020
mg/L
0.0200
102
70-130
1.04
25
o-Xylene
0.00999
0.0010
mg/L
0.0100
99.8
70-130
1.31
25
Surrogate: 1,2-Dichloroediane-d4
0.0258
Ing/L
0.0250
103
70-130
Surrogate: Toluene-d8
0.0248
Ing/L
0.0250
99.4
70-130
Surrogate: 4-Bromofluorobenzene
0.0245
-9/1-
0.0250
98.2
70-130
I Page 31 of �44

Table of Contents
con-testo"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Miscellaneous Organic Analyses - Quality Control
Reporting Spike Source */oREC RPD
Analyte Result Limit Units Level Result O/oREC Limits RPD Limit Note,
1318-3810-RSK175
Blank (B138318-BLKI) Prepared & Analyzed: 12/22/15
Ethane
Ethene
Methane
LCS (B139318-BSI)
IND 0.0029 mg/L
ND 0.0038 mg/L
ND 0.0026 mg�L
Prepared & Analyzed: 12/22/15
Ethane
2100
mg/L
2000
104
60-122
Ethene
2000
mg/L
2000
98.6
67-113
Methane
1900
mg/L
2000
96.3
56-121
I Page 32

Table of Contents
con-tiesto"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source */oREC RPD
Analyte Result Limit Units Level Result 9/6REC Limits RPD Limit Notes
Batch B137816 - SW-846 3005A
Blank (B137816-BLKI) Prepared: 12/16/15 Analyzed: 12/18/15
Manganese ND 2.0 Vg/L
LCS (B137816-BS1) Prepared: 12/16/15 Analyzed: 12/17/15
Manganese 241 5.0 Pg/L 250 96.6 80-120
LCS Dup (B137816-BSDI) Prepared: 12/16/15 Analyzed: 12/17/15
Manganese 246 5.0 Rg/L 250 98.4 80-120 1.90 20
Batch B138379 - SW4146 3005A
Blank (B138379-BLKI) Prepared: 12/23/15 Analyzed: 12/24/15
Manganese ND 2.0 Ag/L
LCS (Bl38379-BSI) Prepared: 12/23/15 Analyzed: 12/24/15
Manganese 234 5.0 Pg/L 250 93.6 80-120
LCS Dup (BI38379-BSDI) Prepared: 12/23/15 Analyzed: 12/24/15
Manganese 237 5.0 Pg/L 250 94.9 80-120 1.41 20
I Page 33

Table of Contents
Cl 0 con-testo
ANALYTICAL LABORATORY
39 Spruoe Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Metals Analyses (Dissolved) - Quality Control
Reporting Spike Source %REC RPD
Result Limit Units Level Result */.REC Limits RPD Limit Notes
Batch B137936 - SW-1146 3005A Dissolved
Blank (B137936-BLKI)
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
LCS (B137936-BSI)
ND
2.0
lLg/L
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
LCS Dup (B137936-BSD1)
255
5.0
Pg11-
250 102
Prepared: 12/17/15 Analyzed: 12/20/15
80-120
Manganese
Batch B139389 - SW-846 3005A Dissolved
262
5.0
Rg/L
250 105
80-120 2.75 20
Blank (B139389-BLKI)
Prepared: 12/23/15 Analyzed: 12/28/15
Manganese
LCS (B139389-BS1)
ND
2.0
ILg/L
Prepared: 12/23/15 Analyzed: 12/28115
Manganese
LCS Dup (B1393WBSDI)
249
5.0
Pg/L
250 99.6
Prepared: 12/23/15 Analyzed: 12/28/15
80-120
Manganese
248
5.0
Ag/L
250 99.2
80-120 0.466 20
I Page 34 of 44 1

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPAIAPRA/SW-846 Methods (Total) - QU21ity Control
Reporung Spike Source */.REC RPD -1
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B137818 - SM21-22 4500S-F
Blank (B137818-BLKI)
Prepared & Analyzed: 12/16/15
Sulfide
ND
2.0
mg/1-
LCS (B137818-BSI)
Prepared & Analyzed: 12/16/15
Sulfide
16
2.0
-9/1-
14.8 108
60.3-119
Batch B137822 - SM 21-22 4500 NO2 B
Blank (B137922-BLKI)
Prepared & Analyzed: 12/16/15
Nitrite as N
ND
0.010
mg/L
LCS(B137822-BS1)
Prepared & Analyzed: 12/16/15
Nitrite as N
0.11
0.010
-9/1-
0.100 105
90-111
LCS Dup (B137822-BSDI)
Prepared & Analyzed: 12/16/15
Nitrite as N
0.10
0.010
-9/1-
0.100 103
90-111 2.08 5.9
Batch B137915 - SM 21-22 4500 NO3 F
Blank (Bl37915-BLKI)
Prepared & Analyzed: 12/17/15
Nitrate as N
ND
0.050
mg/L
LCS (B137915-BS1)
Prepared & Analyzed: 12/17/15
Nitrate as N
3.6
0.050
mg/L
3.41 106
88.9-111
LCS Dup (B137915-BSD1)
Prepared & Analyzed: 12/17/15
Nitrate as N
3.6
0.050
mg/L
3.41 107
98.9-111 0.825 5.66
Batch B137921 - SM19-22 4500 NH3 C
Blank (B137921-BLKI)
Prepared & Analyzed: 12/17/15
Ammonia as N
ND
0.30
mg/L
LCS (B137921-BSI)
Prepared & Analyzed: 12/17/15
Ammonia as N
4.8
0.30
mg/L
5.00 95.8
82-106
LCS Dup (B137921-BSDI)
Prepared & Analyzed: 12/17/15
Ammonia as N
4.8
0.30
mg/L
5.00 95.8
82-106 0.00 8.24
Batch B138131 - SM 5310C
Blank (B138131-BLKI)
Prepared: 12/21/15 Analyzed: 12/22/15
Total Organic Carbon
ND
0.50
mg/1-
I Page 35

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-946 Methods (Total) - Quality Control
Reporting Spike Source */oREC RPD
Analyte Result Limit Units Level Result %REC Limits "D Limit Notes
Batch B138131 - SM 5310C
LCS (B138131-BSI)
Prepared: 12/21/15 Analyzed: 12/22/15
Total Organic Carbon
LCS Dup (B138131-BSDI)
9.70
0.50
-9/1-
10.0 97.0 90.1-114
Prepared: 12/21/15 Analyzed: 12/22/15
Total Orgamc Carbon
Batch B138190 - ASTM D516-07
9.66
0.50
-19/1-
10.0 96.6 90.1-114 0.403 7.72
Blank (B138190-BLKI)
Prepared & Analyzed: 12/21/15
Sulfate
LCS (B138190-BSI)
ND
2.0
mg/L
Prepared & Analyzed: 12/21/15
Sulfate
LCS Dup (111138190-111SIDI)
19
2.0
-9/1-
20.0 96.8 83.8-123
Prepared & Analyzed: 12/21/15
Sulfate
20
2.0
Ing/L
20.0 98.2 83.8-123 1.49 9.27
I Page 3

Table of Contents
con-test®R
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA 01028 *FAX [phone] *TEL. [phone]
FLAGIQUALIFIER SUMMARY
QC result is outside ofestablished limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
RL Reporting Limit
DL Method Detection Limit
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) arc determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
i Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
I Page 37 of 44 1

Table of Contents
con-toto
ANALYTICAL LABORATORY
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CERTIFICATIONS
Ccrtified Analyses included in this Report
Anslyte Certifications
3810-RSKI 7S in Water
Ethane
VA,NY,ME
Ethene
VA,NY,ME
Methane
VANY,ME
ASTMD516-07in Water
Sulfate
NY,NH,MACT,RI,VANC
SM 21-22 4500 NO2 B in Water
Nitrite as N
CT,NH,NY,MENC,VARl
SM21-22 4500 NO3 Fin Water
Nitrate as N
CTMANHNY,R1,ME,NC,VA
SM 531 OC in Water
Total Organic Carbon
NY,NC,CT,RI,ME,MA,VA
SM19-22 4500 NH3 C in Water
Ammonia as N
NY,MA,CT,R1,VA,NC,ME
SM21-22 4500S-F in Water
Sulfide
CTNHNY,R1,NCME,VA
SW-846 6020A in Water
Manganese
CT,NHNY,NC,ME,VA
Manganese
CT,NHNYNC,ME,VA
SW-846 8260B in Water
Acetone
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethanc
NC
Bromofornt
NC
Bromomethane
NC
2-Butanone (MEK)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzenc
NC
Chlorodibromomediane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibronioethane (EDB)
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
Dichlorodifluoromethane (Freon 12)
NC
I Page 38 of 44 1

con-testo"
ANALYTICAL LABORATORY
Certified Analyses included in this Report
Analyte
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certifications
SW-846 8260B in Water
IJ-Dichloroediane
NC
1,2-Dichloroethane
NC
I,I-Dichloroethylene
NC
cis- 1,2-Dichloroethylene
NC
h-ans- 1,2-Dichloroethylene
NC
1,2-Dichloropropane
NC
1,3-Dichloropropane
NC
2,2-Dichloropropane
NC
I,I-Dichloropropene
NC
cis- 1,3-DicWoropropene
NC
trans- 1,3-DicWoropropene
NC
Diisopropyl Ether (DIPE)
NC
Ethylbenzene
NC
2-Hexanone (MBK)
NC
Isopropylbenzene (Curnene)
NC
p-Isopropyholuene (p-Cyrnene)
NC
Methyl tert-Butyl Ether (MTBE)
NC
Methylene Chloride
NC
4-Methyl-2-pentanone (MIBK)
NC
Naphthalene
NC
n-Propylbenzene
NC
Styrene
NC
1, 1,2,2-Tetrachloroediane
NC
Tetrachloroethylene
NC
Toluene
NC
1,2,3-Trichlorobenzene
NC
1,2,4-Trichlorobenzene
NC
1, 1, I-Trichloroediane
NC
1, 1,2-Trichloroethane
NC
Trichloroethylene
NC
Trichlorolluoromethane (Freon 11)
NC
1,2,3-Trichloropropane
NC
1,2,4-Trimethylbenzene
NC
1,3,5-Trimethylbenzene
NC
Vinyl Acetate
NC
Vinyl Chloride
NC
m+p Xylene
NC
o-Xylene
NC
Table of Contents
I Page 39=

Table of Contents
conostesto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
Code
Description
Numbet
Expires
AIHA
AIHA-LAP, LLC
100033
02/1/2016
MA
Massachusetts DEP
M-MA100
06/30/2016
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2017
NY
New York State Department of Health
10899 NELAP
04/1/2016
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2016
RI
Rhode Island Department of Health
LAOOO 112
12/30/2015
NC
North Carolina Div. ofWater Quality
652
12/31/2016
NJ
New Jersey DEP
MA007 NELAP
06/30/2016
FL
Florida Department of Health
E871027 NELAP
06/30/2016
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2016
WA
State of Washington Department of Ecology
C2065
02/23/2016
ME
State of Maine
2011028
06/9/2017
VA
Commonwealth ofVirginia
460217
12/14/2016
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2016
I Page 40

Ph.ne: 413-525-2332 CHAIN OF CUSTODY RECORD 39 Spruce Street Page_1_,f
conmtEstc-) Fax: [phone] East Longmeadow, MA 01028
Email: [e-mail] -r4 r4N r4
ANALYTICAL LABORATORY I S # of Containers
44 http://Www.contestiabs.com ** Preservation
Company Name: ATC Telephone: ri *"Container Code
Address: tQ,-.1 fel Project # D C 72__OZ -3 3- Analysis R uested Dissolved Metals
N 0 Field Filtered
0— ci_ fe'; ZJ 6 1/-- 6" L9 &-Z Client PO#
A ntion: - �;A- B DATA DEUVERY (check all that apply) 0 Lab to Filter
tte , T, (, - . �, 0 FAX OEMAIL OWESSITE
Project Location: S51f rrZ54�&001_ ***Cont. Code:
-'t-
O'd
Sampled By:C,, - MO-Aie'-f gig, gr-,�Wq_ Email: A=amber glass
G=glass
Project Proposal Provided? (for billing purposes) Format: OPOF OEXCEL OGIS P=plastic
0 yes 0 OTHER q,, ST=sterile
proposal date
Collection -10 "Enhanced Data Package" V= vial
Con -Test Lab ID Client Sample ID/ Description *Matrix Conc S=summa can
J laboratory ust mly) Date/44"e- Bote Time Composite Gra,b Code Code 75C tx-) T=tedlar bag
O=Other
/V�
"/o
-GW=
**Preservation
I = Iced
H HCL
M Methanol
IN Nitric Acid
S = Sulfuric Acid
X=Nahydroxide
i T Na thiosulf ate
0 Other
grouicittrater
=�MEMMENEENEEMENWMatrixCode:
Comments:
... M I I I I I FFF WW= wastewater
use the following codes to let Con -Test know if a specific sample may be high Dw= drinking water
in concentration in Matrix/Conc. Code Box: A = air
...................................... - ............................................................ ...... I S = soil/solid
H - High; M - Medium; L - Low; C - Clean; U - Unknown SL = sludge
Relinquished by: (signature)
Date/Time:
1, 145-
J�ZljProgram
Turnaround
Detection
LIMABequi�ements
-_
Information
I
0 = other
. /-/ J
a 5.Day
North Carolina
s* natu
/Time:
0 5-7-Day
0 2L
0 DSCA 0 IHS8 Orphaned Landfill
1 �//5 Nq
Dgt
0 10-0.y
0 GWPC
0 SWS Landfill 0 UST 0 REC
si
._
Date/Time:
RUSH
0 SWSL
0 Other:
CD
0 '24-Hr r '48-Hr
0 OTHER
4
by: (�ignatu
7.
D t /Ti
IZ' TR -
0 72-Hrr 4-Day
ITA
AlHA NELAC & AIHA Certified
0
L-MJL_0=&
'TURNAROUNDTIME
taqc,
Requires Lab Approval
JA
= WBE/DBE Certified
—
4h.
(business days) STARTS AT 9:DD A.M. THE DAYAFTERSAmPLE RECEIPT UNLESSTHEREARE QUESTIONSON YOURCHAIN.
-0-
1 THIS FORM IS NOT FILLED OUT COMPLETELY OR IS INCORRECT, TURNAROUND TIME WILL NOT START UNTIL ALL QUESTIONS ARE ANSWERED.
PLEASE BE CAREFUL NOT TO CONTAMINATE THIS DOCUMENT
CD
0
0
0
�L
CD

Table of Contents
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Table of Contents
39 Spruce St.
East Longmeadow, MA. 01028
P: 413-525-2332
F: 413-525-6405
www.contestlabs.com
CLIENT NAME:
Page I of 2
Sample Receipt Checklist
-RECEIVED BY:
1) Was the chain(s) of custody relinquished and signed? �Y
ge No
2) Does the chain agree with the samples? es; No
If not, explain:
3) Are all the samples in good condition? oYes No
If not, explain:
lob-con-testo
, ANALYTICAL LABORATORY
No CoC Included
4) How were the samples received:
on Ice Direct from Sampling Ambient In Cooler(s)
Were the samples received in Temperature Compliance of (2-6'C)? 6i) No N/A
Temperature 'C, by Ternp blank 3-0 -Temperature 'C by Temp gun _
5) Are there Dissolved samples for the lab to filter? Yes
Who was notified Dn —fP - . Time
6) Are there any RUSH or ORT HOLDING TIME sa pies? No
Who was notified L Date Time
Permission to subcontract samples? Yes No
7) Location where samples are stored: (Walk-in clients only) if not already approved
Client Signat,
8) Do all samples have the proper Acid pH: Q No NIA
9) Do all samples have the proper Base pH: Ge No NIA
10) Was the PC notified of aiiy discrepancies with the CoC vs the samples: Yes
Containers received
at Con -Test
# of containers
# of containers
8 oz amber/clear iar
1 Liter Amber
4 oz amber/clear jar
500 mL Amber
2 oz amber/clear jar
250 mL Amber (8oz amber
Plastic Bag I Ziploc;
1 Liter Plastic
SOC Kit
500 mL Plastic
Non -ConTest Container
250
Perchlorate Kit
40 mL Vial - type listed bel
Flashpoint bottle
Colisure / bacteria bottle—
Other glass jar
Dissolved Oxygen bottle
Other
Encore
Laboratory Comments:
e-0
6C
_of C> C
40 mL vials: # HCI # Methanol
.277 Bisulfate # DI Water
......... . At-L
Time and Date Frozen:
ROV�.AAbqysf2U�3...-�.:' ft 'II'v,)uI1c'L'0 -- I Page 43

Table of Contents
Page 2 of 2
Login Sample Receipt Checklist
(Rejection Criteria Listing - Using Sample Acceptance Policy)
Any False statement will be brought to the attention of Client
Onp--ttion Answer (True/Falsej Comment
1) The cooler's custody seal., if present, is intact.
2) The cooler or samples do not appear to have
been compromised or tampered with.
T/F/NA
3) Samples were received on ice.
4) Cooler Temperature is acceptable.
5) Cooler Temperature isrecorded.
6) COC is filled out in ink and legible.
7) COC is filled out with all pe inent information.
8) Field Sampler's name present on COC.-
9) There are no discrepancies between the
sample IDs on the container and the COC.
10) Samples are received within Holding Time.
ll) Sample containers have legible labels.
12) Containers are not broken or leaking.
13) Air Cassettes are not broken/open.
14) Sample collection date/times are provided.
15) Appropriate sample containers are used.
16) Proper collection media used.
17) No headspace sample bottles are completely filled.
18) There is sufficient volume for all requsted
including any requested MS/MSDs.__
_77
-analyses,
19) Trip blanks provided if applicable.
20) VOA sample vials do not have head space or
bubble is <6mm (1/4") in diameter.
1) Samples do not require splitting or compositing.
Who notifled ot i-aise sxaxement5 f
Doc #277 Rev. 4 August 2013 Log -in Technician Initials: r Jjn
LPOLVI I Ii I 1%�-
Date/Time: n
16 (t 1�
I Page 44 of 44 1

con-tesV'
ANALYTICAL LA130RATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 28, 2015
Justin Ballard
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: Pro Cleaners
Client Job Number:
Project Number: Z045000389
Laboratory Work Order Number: 15LO823
Enclosed are results of analyses for samples received by the laboratory on December 15, 2015. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager

Table of Contents
Sample Summary
4
Case Narrative
6
Sample Results
7
15LO823-01
7
15LO823-02
13
15LO823-03
19
15LO823-04
25
15LO823-05
31
Sample Preparation Information
35
QC Data
37
Volatile Organic Compounds by GUMS
37
B137935
37
Miscellaneous Organic Analyses
41
B138318
41
Metals Analyses (Total)
42
B137816
42
B138379
42
Metals Analyses (Dissolved)
43
B137936
43
B138389
43
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
44
B137818
44
B137915
44
B137921
44
B137946
44

Table of Contents (continued)
B138131
B 138190
B138279
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
45
45
45
47
48
51

con-WW
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow MA01028 *FAX [phone] *TEL. [phone]
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121 REPORT DATE: 12/28/2015
Raleigh, NC 27604 PURCHASE ORDER NUMBER:
ATTN: Justin Ballard
PROJECT NUMBER: Z045000389
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 15LO823
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Pro Cleaners
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTI TEST SUB LAB
MWIIA
15LO823-01
Ground Water
3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 N113 C
SM21-22 450OS-F
SW-846 6020A
SW-846 8260B
MWIOA
15LO823-02
Ground Water
3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 N113 C
SM21-22 450OS-F
SW-846 6020A
SW-846 8260B
MWIOB
15L0823-03
Ground Water
3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM 19-22 4500 N113 C
SM21-22 450OS-F
SW-946 6020A
SW-846 8260B
MW16
15LO823-04
Ground Water
3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 N113 C
SM21-22 450OS-F
SW-946 6020A
SW-946 8260B

con-tcst'o
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121 REPORT DATE: 12/28/2015
Raleigh, NC 27604 PURCHASE ORDER NUMBER:
ATTN: Justin Ballard
PROJECT NUMBER: Z045000389
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 15LO823
The results ofanalyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Pro Cleaners
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUBLAB
MWIIB 15LO823-05 Ground Water 3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 N113 C
SM21-22 450OS-F
SW-846 8260B

con-tesC'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
SW-946 6020A
Qualifications:
R-04
Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that are <5 times the reporting
limit (RL).
Analyte & Samples(s) Qualified:
Manganese
B137816-DUPI
SW-846 8260B
Qualillications:
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFBALCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
Acetone
B137935-BSDI
Dichlorodffluoromethine (Freon 1,
B137935-BSDI
V-20
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte 8, Samples(s) Qualified:
Chloromethane
B137935-BSI, B137935-BSDI
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, die material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Johanna K. Harrington
Manager, Laboratory Reporting

con -tot ®R
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MAO 1028 *FAX [phone] *TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWIIA Sampled: 12/15/2015 10:00
SamDle ID: 15LOS23-01
Samnic Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Acetone
0.013
0.050
0.0049
mg/L
I J
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Benzene
ND
0.0010
0.000079
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Bromoform
ND
0.0010
0.00021
-91L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Bromomethanc,
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
2-Butanone (MEK)
ND
0.020
0.0024
-9/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
n-Butylbenzene
ND
0.0010
0.00010
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
sec-Butylbenzene
ND
0.0010
0.00011
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
tert-Butylbenzcne
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17115
12/19/15 22:49
LBD
Carbon Disuffide
ND
0.0040
0.0010
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Carbon Tetrachloride
ND
0.0050
0.00012
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Chlorobenzene
ND
0.0010
0.00016
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Chlorocthane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Chloroform
ND
0.0020
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
2-Chlorotolucne
ND
0.0010
0.00012
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
4-Chlorotolucne
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-846 8260B
12/17/15
12119/15 22:49
LBD
1,2-Dichlorobenzcne
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,3-Dichlorobenzcnc
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
IJ-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
I,I-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
cis- 1,2-Dichlorocthylene
0.00023
0.0010
0.00015
mg/L
I J
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
trans-1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,3-Dichloropropane
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1, 1 -Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
cis- 1,3-Dichloropropenc
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 22:49
LBD
Ethylbcnzcnc
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
2-Hexanone (MBK)
ND
0.010
0.0015
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
p-I-p-pyltol- (p-Cyrn-e)
ND
0.0010
0.00012
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 22:49
LBD
Mcthyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
4-Methyl-2-pentanone (MIBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD

con -test"'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW11A Sampled: 12/15/2015 10:00
Samole ID: 15LOS23-01
Samole Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
IND
0.0020
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/t5
12/19/15 22:49
LBD
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
Ing/L
I
SW-946 8260B
12/17/15
12/19/15 22:49
LBD
Tetrachloroethylene
0.0083
0.00050
0.00017
mg/l,
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Toluene
0.00054
0.0010
0.00010
mg/L
I
J
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,1,1-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Trichloroethylene
0.00038
0.0010
0.00020
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
L]BD
1,2,3-Trichloropropanc
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
L]BD
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
LBD
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 22:49
L]BD
Surrogates
% Recovery
Recovery lAmIts
Flag/Qual
1,2-Dichloroethane-d4
104
70-130
12/19/15 22:49
Toluen"8
99.5
70-130
12/19/15 22:49
4-Bromofluorobenzene
96.4
70-130
12/19/15 22:49

Ccon-NsC'
P ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWIIA Sampled: 12/15/2015 10:00
Sanmle ID: 15LOS23-01
Samole Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Date/Time
Analyte Results
RL
DL
Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
mg/L I
3810-RSK175
12/22/15
12/22/15 16:07
TPH
Ethene ND
0.0038
0.00099
mg/L I
3810-RSK175
12/22/15
12/22/15 16:07
TPH
Methane ND
0.0026
0.0011
mg/L I
3810-RSK175
12/22/15
12/22/15 16:07
TPH

con-UW
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MAO 1028 *FAX [phone] -TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW11A Sampled: 12/15/2015 10:00
Samule ID: 15LOS23-01
Sarnole Matrix: Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Mangan e 150 2.0 0.23 Ag/L 2 SW-846 6020A 12/23/15 12/24/15 13:41 KSH

con-tcsV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWIIA Sampled: 12/15/2015 10:00
Simmle ID: 15LOS23-01
Samole Matrix: Ground Water
Metals Analyses (Dissolved)
Date Dateffime
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 22 2.0 0.23 Ag/L 2 SW-846 6020A 12/23/15 12/28/15 10:54 MJH

con-UsV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL [phone]
Project Location: Pro Cleaners
Sample Description:
Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW11A
Sampled: 12/15/2015 10:00
Samnle ID: 15LO823-01
Samnle Matrix: Ground Water
Conventional Chemistry Parameters hy EPA/APHA/SW-846 Methods (Irotal)
Date
Date/Time
Analyte
Results RL DL Units
Dilution Flag/Qual Method
Prepared
Analyzed
Analyst
Ammonia as N
ND 0.30 0.22 mg/L
I SM19-22 4500 NH3 C
12/17/15
12/17/15 14:30
VAK
Nitrate as N
0.28 0.050 0.049 mg/L
I SM 21-22 4500 NO3 F
12/17/15
12/17/15 14:10
JK
Nitrite as N
0.0034 0.010 0.0020 mg/L
I J SM 21-22 4500 NO2 B
12/17/15
12/17/15 9:50
VAK
Sulfate
1.2 2.0 0.40 Ing/L
I J ASTM D516-07
12/21/15
12/21/15 13:10
MM11
Sulfide
ND 2.0 1.8 mg/L
I SM21-22 450OS-F
12/16/15
12/16/15 15:15
DJM
Total Organic Carbon
ND 0.50 OA6 11191L
I SM 5310C
12/22/15
12/22/15 15:00
LL

0 con-atest'�'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10A Sampled: 12/15/2015 12:00
S211111le ID: 15LOS23-02
Samole Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Benzene
ND
0.0010
0.000079
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260D
12/17115
12/19/15 23:16
LBD
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-946 8260B
12/17/15
12/19/15 23:16
LBD
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Bromomcthane
ND
0.0020
0.00094
mg/L
I
SW-946 8260B
12/17/15
12/19/15 23:16
LBD
2-Butanonc (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
n-Butylbenzene
ND
0.0010
0.00010
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Carbon Disuffide
ND
0.0040
0.0010
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Carbon Tetrachloride
ND
0.0050
0.00012
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Chlorobenzene
ND
0.0010
0.00016
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Chlorodibromomethane
ND
0.00050
0.00010
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Chloroethane
ND
0.0020
0.00028
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Chloroform
ND
0.0020
0.00022
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-946 8260B
12/t7/15
12/19/15 23:16
LBD
2-Chlorotoluene
ND
0.0010
0.00012
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
4-Chlorotoluene
ND
0.0010
0.00013
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-946 8260B
12117/15
12/19/15 23:16
LBD
1,2-Dichlorobenzene
ND
0.0010
0.00010
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,3-Dichlorobenzene
ND
0.0010
0.00017
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,4-Dichlorobenzene
ND
0.0010
0.00015
-9/1-
1
SW-946 8260B
12117/15
12/19/15 23:16
LBD
Dichlorodifluoromethane (Freon 12)
NID
0.0020
0.00018
mg/L
I
SW-946 8260B
12/17/15
12/19/15 23:16
LBD
1,1-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
I,I-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
cis- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
trans-1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,2-Dichloropropane
ND
0.0010
0.00013
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,3-Dichloropropanc
ND
0.00050
0.00011
-9/1-
1
SW-846 8260B
12117/15
12/19/15 23:16
]LBD
2,2-Dichloropropane
ND
0.0010
0.00016
-9/L
I
SW-946 8260B
12/17/15
12/19/15 23:16
LBD
1,1-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
cis- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
tmns-1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
2-Hexanone (MBK)
ND
0.010
0.0015
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Isopropylbenzene (Curnene)
ND
0.0010
0.00012
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
p-lsopropyltoluene (p-Cymene)
ND
0.0010
0.00012
-9/1-
1
SW-946 8260B
12/17/15
12/19/15 23:16
LBD
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/1-
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
4-Methyl-2-pentanone (Ml[BK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD

con -test"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10A Sampled: 12/15/2015 12:00
Samnle ID: 15LOS23-02
Samole Matrix: Ground Water
Volatile Organic Compounds by GUMS
Date
DatelTime
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/17/15
12/19/15 23:16
LBD
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Tetrachloroethylene
0.00047
0.00050
0.00017
mg/L
I
J
SW-846 8260B
12/17/15
12119/15 23:16
LBD
Toluene
0.00022
0.0010
0.00010
mg/L
I
J
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-946 8260B
12/17/15
12/19/15 23:16
LBD
1,1,1-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Trichloroethylene
ND
0.0010
0.00020
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
m+p Xylene
ND
0.0020
0.00025
mg1L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:16
LBD
Surrogates
% Recovery
Recovery Limits
Flag/Qua]
1,2-Dichlo I roethane-d4
105
70-130
12119/15 23:16
Toluene-dIi
99.4
70-130
12/19/15 23:16
4-Bromofluorobenzene
98.8
70-130
12/19/15 23:16

con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 0 1028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10A Sampled: 12/15/2015 12:00
Samole ID: 15LOS23-02
Samole Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Date/Time
Analyte Results
RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
mg/L I
3810-RSK175
12/22/15
12/22/1516:19
TPH
Ethene ND
0.0038
0.00099
mg/L I
3810-RSK175
IV22/15
12/22/15 16:19
TPH
Methane ND
0.0026
0.0011
mg/L I
3810-RSK175
12/22/15
12/22/15 16:19
TPH

con-toto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10A Sampled: 12/15/2015 12:00
Saumle ID: 15LO823-02
Samole Matrix: Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 5.4 2.0 0.23 Pg/L 2 SW-846 6020A 12/23/15 12/24/15 13:54 KSH

0 con-tcstO
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10A Sampled: 12115/2015 12:00
Samule ID: 15LO823-02
Samnle Matrix: Ground Water
Metals Analyses 0[)issolved)
Date Date/Time
Analyte Results RL DIL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 0.91 2.0 0.23 ILg/L 2 1 SW-846 6020A 12/23/15 12/28/15 10:57 MJH

con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners
Sample Description:
Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10A
Sampled: 12/15/2015 12:00
Saninle ID: 15LO823-02
Samole Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APHA/SW-946 Methods (rotal)
Date
Date/Time
Analyte
Results RL DL Units Dilution Flag/Qua] Method
Prepared
Analyzed
Analyst
Ammonia as N
ND 0.30 0.22 mg/L I SM19-22 4500 NH3 C
12/17/15
12/17/15 14:30
VAK
Nitrate as N
0.060 0.050 0.049 mg/L I SM 21-22 4500 NO3 F
12/17/15
12/17/15 14:10
JK
Nitrite as N
ND 0.010 0.0020 mg/L I SM 21-22 4500 NO2 B
12/17/15
12/17/15 9:50
VAK
Sulfate
ND 2.0 0.40 mg/L I ASTM D516-07
12/21/15
12/21/15 13:10
NffvlH
Sulfide
ND 2.0 1.8 mg/L I SM21-22 450OS-F
12/16/15
12/16/15 15:15
DJM
Total Organic Carbon
0.17 0.50 0.16 mg/L I J SM 53 1 OC
12/21/15
12/21/15 9:00
LL

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL� 413/525-2332
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWIOB Sampled: 12/15/2015 14:30
Samnle ID: 15LOS23-03
Samole Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
0.075
0.050
0.0049
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Benzene
ND
0.0010
0.000079
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
ILBD
Bromobenzenc
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Bromochloromethane
ND
0.0010
0.00022
-9/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:36
LBD
Bromoform,
ND
0.0010
0.00021
1119/1-
1
SW-846 8260B
12/17/15
12120/15 0:36
LBD
Bromomethane
ND
0.0020
0.00094
1119/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
2-Butanone (MEK)
ND
0.020
0.0024
mg/1-
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17115
12/20/15 0:36
LBD
Carbon Disulfide
ND
0.0040
0.0010
mg/1-
I
SW-846 8260B
12/17/15
12/20/15 0:36
LDD
Carbon Tetrachloride
ND
0.0050
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Chlorobenzene
ND
0.0010
0.00016
mg/L
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/17/15
1=0/15 0:36
LBD
Chloroethane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Chloroform
ND
0.0020
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:36
LBD
1,2-Dichlorobenzcne
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,3-Dichlorobenzene
ND
0.0010
0.00017
1119/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,4-Dichlorobenzene
ND
0.0010
0.00015
n1g/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
1119/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1, 1 -Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,2-Dichloroediane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
IJ-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
cis-1,2-Dichloroethylenc
0.00015
0.0010
0.00015
mg/L
I J
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
tmns-1,2-Dichloroethylcne
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12120/15 0:36
LBD
1,3-Dichloropropane
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LJBD
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
I,I-Dichloropropene
ND
0.0020
0.00013
mg/L.
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
cis-1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12117/15
12/20/15 0:36
LBD
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
lsopropylbenzene (Curnene)
ND
0.0010
0.00012
-9/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
p-lsopropyltoluene (p-Cyrnene)
0.00030
0.0010
0.00012
mg/L
I J
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12117/15
12/20/15 0:36
LBD
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/20115 0:36
LBD
4-Methyl-2-pentanone (MI]BK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD

con-test'0
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 0 1028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10B Sampled: 12/15/2015 14:30
Sanmle ID: 15LOS23-03
Sarnnle Matrix: Ground Water
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RIL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
rog/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
n-Propylbenzene
ND
0.0010
0.00011
rng/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Styrene
ND
0.0010
0.00015
1119/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LIBD
1,1,2,2-Tetrachloroethane
ND
0.00050
0.00013
1119/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Tetrachloroethylene
0.080
0.00050
0.00017
1119/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Toluene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,2,4-Ttichlorobenzene
ND
0.0010
0.00019
-9/1-
1
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,1,1-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:36
LBD
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Trichloroethylene
0.00047
0.0010
0.00020
mg/L
I J
SW-846 8260B
12/17/15
12/20/15 0:36
1-131)
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/20/1� 0:36
LBD
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:36
LBD
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:36
LBD
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:36
LBD
o-Xylenc
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/t7/15
12/20/15 0:36
LBD
Surrogates % Recovery Recovery Umits Flag/Qual
1,2-Dichloroethane-d4 105 70-130 12/20/15 0:36
Toluene-d8 101 70-130 12/20/15 0:36
4-Bromofluorobenzene 94.8 70-130 12/20/15 0:36

con-t(st"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample #: MW10B Sampled: 12/15/2015 14:30
Samule ID: 15LOS23-03
Sanmle Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Date/Time
Analyte Results
RIL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
mg/L I
3810-RSK175
12122/15
12/22/15 16:34
TPH
Ethene ND
0.0038
0.00099
mg/L I
3810-RSK175
12/22/15
12/22/15 16:34
TPH
Methane ND
0.0026
0.0011
mg/L I
3810-RSK175
12/22/15
12/22115 16:34
TPH.

con -test"
ANALYTICAL LABOPATORY
39 Spruce Street* East Longmeadow, MAO 1028 *FAX [phone] *TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWJOB Sampled: 12/15/2015 14:30
Samole ID: 15L0823-03
Samole Matrix: Ground Water
Metals Analyses (rotal)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 390 2.0 0.23 Pg/L 2 SW-846 6020A 12/23/15 12/24/15 13:57 KSH

con-Usto
ANALYTICAL LABOPATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWl0B Sampled: 12/15/2015 14:30
SRMDle ED: 151AS23-03
Samole Matrix: Ground Water
Metals Analyses (Dissolved)
Date Daterrime
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 220 2.0 0.23 gg/L 2 SW-846 6020A 12/23/15 12/28/15 11:01 MJH

con-stcst'0
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project LA)cation: Pro Cleaners
Sample Description:
Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW10B
Sampled: 12/15/2015 14:30
Samnle ID: 15LOS23-03
Sarnole Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APHAISW-846 Methods (Total)
Date
Date/Time
Analyte
Results
RL DL Units
Dilution Flag/Qual Method
Prepared
Analyzed
Analyst
Ammonia as N
ND
0.30 0.22 ing/l,
I SM19-22 4500 NH3 C
12/17/15
12/17/15 14:30
VAK
Nitrate as N
0.10
0.050 0.049 mg/L
I SM 21-22 4500 NO3 F
12/17/15
12/17/15 14:10
JK
Nitrite as N
0.0023
0.010 0.0020 mg/L
I J SM 21-22 4500 NO2 B
12/17/15
12/17/15 9:50
VAK
Sulfate
0.87
2.0 0.40 -9/1-
1 J ASTM D516-07
12/21/15
12/21/15 13:10
MMH
Sulfide
ND
2.0 1.8 -9/1-
1 SM21-22 45GOS-F
12/16115
12/16/15 15:15
DJM
Total Organic Carbon
ND
0.50 0.16 -91L
I SM 5310C
12/22/15
12/22/15 15:00
L.L

con-Usto
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
DateReceived: 12/15/2015
Field Sample#: MWI16 Sampled: 12/15/2015 15:50
Samnle ID: 15LO823-04
Samolc Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Quil
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Benzene
ND
0.0010
0.000079
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Bromobenzcnc
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBID
Bromochloromethanc
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Bromodichloromethane
ND
0.00050
0.000088
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-946 8260B
12/17/15
12/19/15 23:43
LBD
2-Butanone (MFK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Carbon Tetrachloride
ND
0.0050
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Chlorobenzene
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Chlorodibromomethane
ND
0.00050
0.00010
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Chlorocthanc,
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBID
Chloroform
ND
0.0020
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBID
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
4-Chlorotoluene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12117/15
12/19/15 23:43
LBD
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,2-Dichlorobenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBID
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/19/15 23:43
LBD
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,1-Dichloroethanc
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17115
12/19/15 23:43
LBID
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
IJ-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
cis-1,2-Dichloroediylene
NID
0.0010
0.00015
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
trans- 1,2-Dichloroethylene
ND
0.0010
0.00015
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,2-Dichloropropane
IND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LJ3D
1,3-Dichloropropane
ND
0.00050
0.00011
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
IJ-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
cis- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12117/15
12/19/15 23:43
LBD
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
-91L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Ethylbenzene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
2-Hexanone (MEBK)
ND
0.010
0.0015
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
lsopropylbenzene (Curnene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
p-Isopropyltoluene (p-Cymene)
IND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Methyl tert-Butyl Ether (MTBE)
0.0031
0.0010
0.000090
mg/L
I
SW-846 8260B
12/17/15
12/19115 23:43
LBD
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
4-Methyl-2-pentanone (MfBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/19115 23:43
LBD

con-tesV
ANALYTICAL LABOPATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: WorkOrder: ISLO823
Date Received: 12/15/2015
Field Sample#: MW16 Sampled: 12/15/2015 15:50
Samrile ID: 15LO823-04
Saniole Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17115
12/19/15 23:43
LBD
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Tetrachloroethylene
0.0060
0.00050
0.00017
111911-
1
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Toluene
0.00013
0.0010
0.00010
nig/L
I i
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
-9/1-
1
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
111911-
1
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1, 1, 1 -Trichloroethane
ND
0.0010
0.000094
111911-
1
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1, 1,2-Trichloroethane
ND
0.0010
0.00012
Ing/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Trichloroethylene
ND
0.0010
0.00020
111911-
1
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/19/15 23:43
LBD
Surrogates
% Recovery
Recovery Unilts
Flag/Qua]
1,2-Dichloroethane-d4
103
70-130
12/19/15 23:43
Toluene-d8
100
70-130
12/19/15 23:43
4-Bromofluorobenzene
97.0
70-130
12/19/15 23:43

con-kst'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW16 Sampled: 12/15/2015 15:50
Samole ID: 15LOS23-04
Samolc Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Date/Time
Analyte Results
RL
DL
Units Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
-9/1- 1
3810-RSK175
12/22/15
12/22/15 16:48
TPH
Ethene ND
0.0038
0.00099
-9/1- 1
3810-RSK175
12/22/15
12/22/15 16:48
TPH
Methane ND
0.0026
0.0011
mg/L I
3810-RSK175
12122/15
12/22/15 16:48
TPH

con-tesV
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW16 Sampled:- 12/15/2015 15:50
SRMDle ID: 15LO823-04
Samole Matrix: Ground Water
Metals Analyses (rotal)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 63 2.0 0.23 Pg/L 2 SW-846 6020A 12/23/15 12/24/15 14:01 KSH

con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Samplek MW16 Sampled: 12/15/2015 15:50
Samnle ID: 15LO823-04
Samnle Matrix: Ground Water
Metals Analyses (Dissolved)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qu2l Method Prepared Analyzed Analyst
Manganese 39 2.0 0.23 Pg/L 2 SW-846 6020A 12/23/15 12/28/15 11:04 MJH

con-tcsto
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow. MA01028 *FAX [phone] *TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW16 Sampled: 12/15/2015 15:50
SamDle ED: ISLOS23-04
Samnle Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods Crotal)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ammonia as N
IND
0.30
0.22
-911,
1
SM 19-22 4500 NH3 C
12/17/15
12/17/15 14:30
VAK
Nitrate as N
0.76
0.050
0.049
mg1l,
I
SM 21-22 4500 NO3 F
12/17/15
12/17/15 14:10
JK
Nitrite as N
0.0070
0.010
0.0020
mg/L
I J
SM 21-22 4500 NO2 B
12/17/15
12/17/15 9:50
VAK
Sulfate
3.2
2.0
0.40
-9/1-
1
ASTM D516-07
12/21115
12/21/15 13:10
MMH
Sulfide
ND
2.0
1.8
Ing/L
I
SM21-22 450OS-F
12/16/15
12/16/15 15:15
DJM
Total Organic Carbon
ND
0.50
0.16
Ing/L
I
SM 5310C
12/22/15
12/22/15 15:00
LL

con-UsC'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWllB Sampled: 12/15/2015 14:40
Sanmle ID: 15LO823-05
Samole Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Daterrime
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
0.12
0.050
0.0049
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Benzene
ND
0.0010
0.000079
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
L]BD
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LIBD
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17115
12/20/15 0:10
LBD
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Carbon Tetrachloride
NO
0.0050
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LEID
Chlorobenzene
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LIBD
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Chloroethane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/17115
12/20/15 0:10
LBD
Chloroform
0.0024
0.0020
0.00022
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
2-Chlorotolucne
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,2-Dibromoediane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-846 8260B
12/17115
12/20/15 0:10
LBD
1,2-Dichlorobenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LIBD
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
IJ-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1, 1 -Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
cis-1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
trans- 1,2-Dichloroethylenc
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,2-Dichloropropane
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/17115
12/20/15 0:10
LBD
1,3-Dichloropropanc
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
L]BD
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
IJ-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
cis- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Diisopropyt Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/17115
12/20/15 0:10
LBD
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Isopropylbenzcne (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
p-Isopropyltoluene (p-Cymene)
0.0043
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
4-Methyl-2-pentanone (MIBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15t2015
Field Sample#: MW1lB Sampled: 12/15/2015 14:40
SaulDle ID: 15LO823-05
Samnle Matrix: Ground Water
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
n-Propylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Svjrcne
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
Toluene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/17115
12/20/15 0:10
LBD
1,2,4-Trichlorobcnzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,1,1-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Trichloroethylene
ND
0.0010
0.00020
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,2,4-Trimethylbenzenc
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
-+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-946 8260B
12/17/15
12/20/15 0:10
LBD
o-Xylene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/17/15
12/20/15 0:10
LBD
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
104
70-130
12/20/15 0:10
Toluen"8
101
70-130
12/20/15 0:10
4-Bromofluorobenzene
96.3
70-130
12/20/15 0:10

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MWllB Sampled: 12/15/2015 14:40
Samule ID: 15LO823-05
Samole Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Date/Time
Analyte Results
RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
mg/L I
3810-RSK175
12/22/15
12/22/1517:00
TPH
Ethene ND
0.0038
0.00099
mg/L I
3810-RSK175
12/22/15
12/22/15 17:00
TPH
Methane 0.64
0.0026
0.0011
mg/L I
3810-RSK175
12/22/15
12/22/15 17:00
TPH

con-testo
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO823
Date Received: 12/15/2015
Field Sample#: MW11B Sampled: 12/15/2015 14:40
Samole 11D: 15LOS23-05
Sarnole Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APRA/SW-846 Methods (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Ammonia as N
ND
0.30
0.22
mg/L
I
SM 19-22 4500 NH3 C
12/17/15
12/17/15 14:30
VAK
Nitrate as N
ND
0.050
0.049
-91L
I
SM 21-22 4500 NO3 F
12/17/15
12/17/15 14:10
X
Nitrite as N
0.0034
0.010
0.0020
Ing/L
I J
SM 21-22 4500 NO2 B
12/17/15
12/17/15 9:50
VAK
Sulfate
ND
2.0
0.40
Ing/L
I
ASTM D516-07
12/21/15
12/21/15 13:10
MMH
Sulfide
ND
2.0
1.8
-9/L
I
SM21-22 450OS-F
12/16/15
12/16/15 15:15
DJM
Total Organic Carbon
0.78
0.50
0.16
Ing/L
I
SM 5310C
12/22/15
12/22/15 15:00
LL

con-atcsV'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Sample Extraction Data
3810-RSK175
Lab Number [Field ID]
Batch
Initial JmLj
Final [mL]
Date
15LO823-01 CMWIIA]
B138318
1.00
1.00
12/22/15
15LO823-02 [MW I 0A)
B138318
1.00
1.00
12/22/15
15LO823-03 [MW10B]
B138318
1.00
1.00
12/22/15
I SLO823-04 [MW16]
B138318
1.00
1.00
12/22/15
15LO823-05 [MW11B]
B 138318
1.00
1.00
12/22/15
ASTM D516-07
Lab Number [Field ID]
Batch
Initial [mL]
Final ImLl
Date
15L0823-01 R"LIAI
B138190
100
100
12/21/15
15LO823-02 P"10A)
B138190
100
100
12/21/15
15LO823-03 [MW10B]
B138190
100
100
12/21/15
15LO823-04 [MW16]
B138190
100
100
12/21/15
15LO823-05 [MW 11 B]
B138190
100
100
12/21/15
SM 21-22 4500 NO2 B
Lab Number [Field 1131
Batch
Initial [mL]
Final [mLj
Date
15LO823-01 [MWIIA]
B137946
50.0
50.0
12/17/15
15LO823-02 [MW I OA]
B137946
50.0
50.0
12/17/15
15L0823-03 [MW10B]
B137946
50.0
50.0
12/17/15
15LO823-04 [MW16]
B137946
50.0
50.0
12/17/15
15LO823-05 [MW I IBI
B137946
50.0
50.0
12/17/15
SM 21-22 4500 NO3 F
Lab Number [Field ED]
Batch
Initial [mLj
Final Inil-I
Date
15LO823-01 [MWIIA]
B137915
25.0
25.0
12/17/15
15LO823-02 [MW I OA]
B137915
25.0
25.0
12117/15
15LO823-03 [MWIOBI
B137915
25.0
25.0
12117/15
15L0823-04 [MW16]
B137915
25.0
25.0
12/17/15
15LO823-05 [MW I I BI
B137915
25.0
25.0
12/17/15
SM 5310C
Lab Number [Field ID]
Batch
Initial ImLl
Final [mL]
Date
15LO823-01 [MWIIA]
B138131
50.0
50.0
12/22/15
15L0823-03 [MW10B]
B138131
50.0
50.0
12/22/15
15L0823-04 [MW16]
B138131
50.0
50.0
12/22/15
15LO823-05 [MWIIB]
B138131
50.0
50.0
12/22/15
SM 5310C
Lab Number lField ID]
Batch
Initial [mL]
Final [mLj
Date
15LO823-02 [MWIOA]
B138279
50.0
50.0
12/21/15

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ANALYTICAL LABORATORY
SM19-22 4500 NH3 C
Lab Number lField ID]
39 Spruce Street* East Longmeadow, MA01028' FAX [phone]* TEL. [phone]
Sample Extraction Data
Batch Initial [mLl Final [mLl Date
15LO823-01 [MW11A]
B137921
too
100
12/17/15
15LO823-02 [MW10A]
B137921
100
100
12/17/15
15LO823-03 [MWIOBI
B137921
100
100
12/17/15
15L0823-04 [MW16]
B137921
100
100
12/17/15
15LO823-05 [MWlIBl
B137921
100
100
12/17/15
SM21-22 450OS-F
Lab Number [Field ID]
Batch
Initial [1111]
1 inal Ind.]
Date
15LO823-01 [MWIIAI
B137818
100
100
12/16/15
15LO823-02 [MW10A]
B137818
100
100
12/16/15
15LO823-03 [MW10B]
B137818
too
100
12/16/15
15LO823-04 [MW16]
B137818
too
100
12/16/15
15LO823-05 [MW I I B]
B137818
100
100
12/16/15
Prep Method: SW-846 3005A-SNV-846 6020A
Lab Number [Field ID] Batch Initial [mLl Final [mLl Date
15LO823-OIREI PAW11A]
B138379
50.0
50.0
12/23/15
15LO823-02REI [MWIOA]
B138379
50.0
50.0
12/23/15
15LO823-03REI UMWIOBJ
B138379
50.0
50.0
12/23/15
15LO823-04REI [MW16]
B138379
50.0
50.0
12/23/15
Prep Method: SW-846 3005A Dissolved-SW-846 6020A
Lab Number [Field ID] Batch Initial [mL] Final [mL] Date
15LO823-OIREI [MWIIA]
B138389
50.0
50.0
12/23/15
ISLO823-02REI [MWIOA]
B138389
50.0
50.0
12/23/15
15LO823-03REL [MWIOB]
B138389
50.0
50.0
12/23/15
15LO823-04REI [MWI61
B138389
50.0
50.0
12/23/15
Prep Method: SW-846 503011-SW-846 8260B
Lab Number [Field ID] Batch Initial [mLl Final [m-Ll Date
15LO823-01 [MWIIAI
B137935
5
5.00
12/17/15
15LO823-02 UMWIOAI
B137935
5
5.00
12/17/15
15LO823-03 W10B]
B137935
5
5.00
12/17/15
15LO823-04 ["161
B137935
5
5.00
12/17/15
15LO823-05 [MW I IBI
B137935
5
5.00
12/17/15

con-tiest"'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITYCONTROL
Volatile Organic Compounds by GOMS - Quality Control
Reporting Spike Source O/oREC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B137935 - SW-846 5030B
Blank (B137935-BLK1)
Prepared: 12/17/15 Analyzed: 12/19/15
Acetone
ND
0.050
mg/L
Benzene
IND
0.0010
mg/L
Bromobenzene
IND
0.0010
mg/L
Bromochloromcthane
ND
0.0010
Ing/L
Bromodichloromethane
ND
0.00050
Mg/L
Bromoform
ND
0.0010
Mg/L
Bromomethane
ND
0.0020
mg/L
2-Butanone (MEK)
ND
0.020
mg/L
n-Butylbenzene
ND
0.0010
-91L
sec-Butylbenzene
ND
0.0010
mg/L
tert-Butylbenzene
IND
0.0010
mg/L
Carbon Disulfide
IND
0.0040
mg/L
Carbon Tetrachloride
ND
0.0050
mg/L
Chlorobenzene
ND
0.0010
Mg/L
Chlorodibromomethane
ND
0.000SO
mg/L
Chloroethane
IND
0.0020
mg/L
Chloroform
IND
0.0020
mg/L
Chloromethane
ND
0.0020
mg/L
2-Chlorotoluene
ND
0.0010
mg/L
4-Chlorotoluene
ND
0.0010
mg/L
1,2-Dibromoethane (EDB)
IND
0.00050
Mg/L
1,2-Dichlorobenzene
ND
0.0010
mg/L
1,3-Dichlorobenzene
ND
0.0010
mg/L
1,4-Dichlorobenzene
ND
0.0010
mg/L
Dichlorodifluoromethane (Freon 12)
IND
0.0020
-9/1-
I,I-Dichloroethane
IND
0.0010
mg/L
1,2-Dichloroethane
ND
0.0010
mg/L
I,I-Dichloroethylene
ND
0.0010
mg/L
cis- 1,2-Dichloroethylene
ND
0.0010
mg/L
trans- 1,2-Dichlorocthylene
ND
0.0010
mg/L
1,2-Dichloropropane
ND
0.0010
mg/L
1,3-Dichloropropane
ND
0.00050
mg/L
2,2-Dichloropropane
IND
0.0010
mg/L
1,11-Dichloropropene
ND
0.0020
mg/L
cis- 1,3-Dichloropropcnc
ND
0.00050
mg/L
trans- 1,3-Dichloropropene
ND
0.00050
mg/L
Diisopropyl Ether (DIPE)
ND
0.00050
mg/L
Ethylbenzene
IND
0.0010
mg/L
2-Hexanone (MBK)
ND
0.010
mg/L
lsopropylbenzene (Cumene)
IND
0.0010
mg/L
p-Isopropyltoluene (p-Cymene)
ND
0.0010
mg/L
Methyl tert-Butyl Ether (MTBE)
IND
0.0010
mg/L
Methylene Chloride
ND
0.0050
mg/L
4-Methyl-2-pentanonc (MIBK)
ND
0.010
-91L
Naphthalene
IND
0.0020
mg/L
n-Propylbenzene
ND
0.0010
mg/L
Styrene
ND
0.0010
mg/L
1, 1,2,2-Tetrachloroethane
ND
0.00050
mg/L
Tetrachloroethylene
ND
0.00050
Ing/L
Toluene
ND
0.0010
Ing/L
1,2,3-Trichlorobenzcne
ND
0.0050
mg/L
1,2,4-Trichlorobenzene
ND
0.0010
1119/L

con -test"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GCIMS - Quality Control
Reporting Spike Source %REC RPD
Ualyte Result Limit Units Level Result %RFC Limits IZf1D Limit Notes
Batch B137935 - SW-846 5030B
Blank (B137935-BLK1)
Prepared: 12/17/15 Analyzed: 12/19/15_
1,1,1-Trichloroethane
ND
0.0010
mg/L
1, 1,2-Trichloroethane
ND
0.0010
1119/1-
Trichloroethylene
ND
0.0010
-9/1-
Trichlorofluoromethanc (Freon 11)
ND
0.0020
-9/1-
1,2,3-Trichloropropane
IND
0.0020
Ing/L
1,2,4-Trimethylbenzene
IND
0.0010
-9/1-
1,21,5-Trimethylbenzene
ND
0.0010
mg/L
Vinyl Acetate
ND
0.020
mg/L
Vinyl Chloride
ND
0.0020
mg/L
m+p Xylene
ND
0.0020
mg/L
o-Xylene
ND
0.0010
mg/L
Surrogate: 1,2-Dichloroethane-d4
0.0258
mg/L
0.0250
103
70-130
Surrogate: Toluene-M
0.0250
mg/L
0.0250
100
70-130
Surrogate: 4-Bromofluorobenzcne
0.0239
mg/L
0.0250
95.6
70-130
LCS (B137935-BSI)
Prepared: 12/17/15
Analyzed: 12/19/15
Acetone
0.0779
0.050
Ing/L
0.100
77.9
70-160
Benzene
0.0102
0.0010
mg/L
0.0100
102
70-130
Bromobenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
Bromochloromethane
0.0118
0.0010
mg/L
0.0100
118
70-130
Bromodichloromethane
0.00907
0.00050
mg/L
0.0100
903
70-130
Bromoform
0.00812
0.0010
mg/L
0.0100
81.2
70-130
Bromomethane
0.00648
0.0020
mg/L
0.0100
64.8
40-160
t
2-Butanone (MEK)
0.0962
0.020
1119/1-
0.100
96.2
40-160
t
n-Butylbenzene
0.00913
0.0010
mg/L
0.0100
91.3
70-130
sec-But7ylbenzene
0.00975
0.0010
mg/L
0.0100
97.5
70-130
tert-Butylbenzene
0.00942
0.0010
mg/L
0.0100
94.2
70-130
Carbon Disulfide
0.00834
0.0040
mg/L
0.0100
83.4
70-130
Carbon Tetrachloride
0.00992
0.0050
mg/L
0.0100
99.2
70-130
Chlorobenzene
0.00930
0.0010
mg/L
0.0100
93.0
70-130
Chlorodibromomethane
0.00851
0.00050
mg/L
0.0100
85.1
70-130
Chloroethane
0.0109
0.0020
mg/L
0.0100
109
70-130
Chloroform
0.00988
0.0020
mg/L
0.0100
98.8
70-130
Chloromethane
0.00793
0.0020
M911-
0.0100
793
40-160
V-20 t
2-Chlorotoluene
0.00948
0.0010
1119/1-
0.0100
94.8
70-130
4-Chlorotoluene
0.00942
0.0010
mg/L
0.0100
94.2
70-130
1,2-Dibromoethane (EDB)
0.00983
0.00050
-9/1-
0.0100
98.3
70-130
1,2-Dichlorobenzene
0.00909
0.0010
-9/1-
0.0100
90.9
70-130
1,3-Dichlorobenzene
0.00929
0.0010
mg/L
0.0100
92.9
70-130
1,4-Dichlorobenzene
0.00895
0.0010
mg/L
0.0100
89.5
70-130
Dichlorodifluoromethane (Freon 12)
0.00432
0.0020
mg/L
0.0100
43.2
40-160
t
1, 1 -Dichloroethane
0.0104
0.0010
mg/L
0.0100
104
70-130
1,2-Dichloroethane
0.00975
0.0010
mg/L
0.0100
97.5
70-130
IJ-Dichloroethylene
0.00967
0.0010
mg/L
0.0100
96.7
70-130
cis- 1,2-Dichloroethylene
0.0100
0.0010
mg/L
0.0100
too
70-130
aum-1,2-Dichloroethylene
0.00987
0.0010
mg/L
0.0100
98.7
70-130
1,2-Dichloropropane
0.0101
0.0010
mg/L
0.0100
101
70-130
1,3-Dichloropropane
0.0100
0.00050
1119/1-
0.0100
too
70-130
2,2-Dichloropropane
0.00701
0.0010
mg/L
0.0100
70.1
40-130
t
1, 1 -Dichloropropcne
0.00999
0.0020
11191L
0.0100
99.9
70-130
cis-1,3-Dichloropropene
0.00853
0.00050
1119/1-
0.0100
85.3
70-130
trans- 1,3-Dichloropropene
0.00918
0.00050
mg/L
0.0100
91.8
70-130

con-atcsV'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
,nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B137935 - SW-846 5030B
LCS (B137935-BSI)
Prepared: 12/17/15 Analyzed: 12/19/15
Diisopropyl Ether (DIPE)
0.00945
0.00050
mg/L
0.0100
94.5
70-130
Ethylbenzene
0.00967
0.0010
mg/L
0.0100
96.7
70-130
2-Hexanone (MBK)
0.0974
0.010
mg/L
0.100
97.4
70-160
t
Isopropylbenzene (Curnene)
0.00955
0.0010
mg/L
0.0100
95.5
70-130
p-Isopropyltoluene (13.-Cymene)
0.00992
0.0010
mg/L
0.0100
99.2
70-130
Methyl tert-Butyl Ether (MTBE)
0.00946
0.0010
mg/L
0.0100
94.6
70-130
Mediylcne Chloride
0.00915
0.0050
mg/L
0.0100
91.5
70-130
4-Methyl-2-pcntanone (MlBK)
0.104
0.010
mg/L
0.100
104
70-160
t
Naphthalene
0.00875
0.0020
mg/L
0.0100
87.5
40-130
t
n-Propylbenzene
0.00963
0.0010
1119/1-
0.0100
96.3
70-130
Styrene
0.00979
0.0010
1119/1-
0.0100
97.9
70-130
1, 1,2,2-Tetrachloroethane
0.0104
0.00050
mg/L
0.0100
104
70-130
Tetrachloroethylene
0.00922
0.00050
-9/L
0.0100
92.2
70-130
Toluene
0.00995
0.0010
mg/L
0.0100
99.5
70-130
1,2,3-Trichlorobenzene
0.00862
0.0050
mg/L
0.0100
86.2
70-130
1,2,4-Trichlorobenzene
0.00874
0.0010
mg/L
0.0100
87.4
70-130
1, 1, 1 -Trichloroethane
0.00952
0.0010
mg/L
0.0100
95.2
70-130
1, 1,2-Trichloroethane
0.00989
0.0010
mg/L
0.0100
98.9
70-130
Trichloroethylene
0.00995
0.0010
mg/L
0.0100
99.5
70-130
Trichlorofluoromethane (Freon 11)
0.00853
0.0020
1119/1-
0.0100
85.3
70-130
1,2,3-Trichloropropane
0.0107
0.0020
mg/L
0.0100
107
70-130
1,2,4-Trimethylbenzene
0.00976
0.0010
mg/L
0.0100
97.6
70-130
1,3,5-Trimethylbenzene
0.0100
0.0010
-9/L
0.0100
100
70-130
Vinyl Acetate
0.0876
0.020
mg/L
0.100
87.6
70-130
Vinyl Chloride
0.00695
0.0020
mg/L
0.0100
69.5
40460
t
m+p Xylene
0.0195
0.0020
mg/L
0.0200
97.6
70-130
o-Xylene
0.00975
0.0010
-9/L
0.0100
97.5
70-130
Surrogate: 1,2-Dichloroethanc-d4
0.0258
mg/L
0.0250
103
70-130
Surrogate: Toluene-d8
0.0247
mg/L
0.0250
98.8
70-130
Surrogate: 4-Bromofluorobenzene
0.0245
mg/L
0.0250
98.0
70-130
LCS Dup (B137935-BSDI)
Prepared: 12/17/15
Analyzed: 12/19/15
Acetone
0.0697
0.050
1119/1-
0.100
69.7 *
70-160
11.1
25
L-07 t
Benzene
0.00979
0.0010
mg/L
0.0100
97.9
70-130
4.59
25
Bromobenzene
0.00992
0.0010
mg/L
0.0100
99.2
70-130
1.80
25
Bromochloromethane
0.0115
0.0010
mg/L
0.0100
115
70-130
1.97
25
Bromodichloromethane
0.00950
0.00050
mg/L
0.0100
95.0
70-130
4.63
25
Bromoform
0.00790
0.0010
mg/L
0.0100
79.0
70-130
2.75
25
Bromomethane
0.00711
0.0020
mg/L
0.0100
71.1
40-160
9.27
25
t
2-Butanone (MEK)
0.0853
0.020
mg/L
0.100
85.3
40-160
12.0
25
t
n-Butylbenzene
0.00886
0.0010
mg/L
0.0100
88.6
70-130
3.00
25
sec-Butylberizene
0.00947
0.0010
mg/L
0.0100
94.7
70-130
2.91
25
tert-Butylbenzene
0.00927
0.0010
mg/L
0.0100
92.7
70-130
1.61
25
Carbon Disulfide
0.00787
0.0040
mg/L
0.0100
78.7
70-130
5.80
25
Carbon Tetrachloride
0.00975
0.0050
mg/L
0.0100
97.5
70-130
1.73
25
Chlorobenzene
0.00913
0.0010
mg/L
0.0100
91.3
70-130
1.84
25
Chlorodibromomethane
0.00883
0.00050
mg/L
0.0100
88.3
70-130
3.69
25
Chloroethane
0.0106
0.0020
mg/L
0.0100
106
70-130
2.99
25
Chloroform
0.00972
0.0020
mg/L
0.0100
97.2
70-130
1.63
25
Chloromethane
0.00949
0.0020
mg/L
0.0100
84.9
40-160
6.82
25
V-20 t
2-Chlorotoluene
0.00955
0.0010
mg/L
0.0100
95.5
70-130
0.736
25
4-Chlorotoluene
0.00926
0.0010
mg/L
0.0100
92.6
70-130
1.71
25

con-stiesto
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source 0/oREC RPD
knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B137935 - SW-846 5030B
LCS Dup (B137935-BSDI)
Prepared: 12/17/15 Analyzed: 12/19/15
1,2-Dibromoedianc (EDB)
0.00968
0.00050
mg/L
0.0100
96.8
70-130
1.54
25
1,2-Dichlorobenzene
0.00874
0.0010
mg/L
0.0100
87.4
70-130
3.93
25
1,3-Dichlorobenzene
0.00906
0.0010
mg/L
0.0100
90.6
70-130
2.51
25
1,4-Dichlorobenzcne
0.00886
0.0010
mg/L
0.0100
88.6
70-130
1.01
25
Dichlorodifluoromethane (Freon 12)
0.00399
0.0020
mg/L
0.0100
39.9
40-160
7.94
25
L-07
1, 1 -Dichloroethane
0.0101
0.0010
mg/L
0.0100
101
70-130
2.93
25
1,2-Dichlorocthane
0.00956
0.0010
mg/L
0.0100
95.6
70-130
1.97
25
I,I-Dichloroethylcne
0.00958
0.0010
mg/L
0.0100
95.8
70-130
0.935
25
cis- 1,2-Dichloroethylene
0.00990
0.0010
mg/L
0.0100
99.0
70-130
1.30
25
trans- 1,2-Dichloroethylene
0.00955
0.0010
mg/L
0.0100
95.5
70-130
3.30
25
1,2-Dichloropropane
0.0102
0.0010
mg/L
0.0100
102
70-130
1.38
25
1,3-Dichloropropane
0.00987
0.00050
mg1L
0.0100
98.7
70-130
1.51
25
2,2-Dichloropropane
0.00678
0.0010
mg/L
0.0100
67.8
40-130
3.34
25
t
I,I-Dichloropropene
0.00947
0.0020
mg/L
0.0100
94.7
70-130
5.34
25
cis- 1,3-Dichloropropene
0.00850
0.00050
mg/L
0.0100
85.0
70-130
0.352
25
U-ans-1,3-Dichloropropene
0.00903
0.00050
mg/L
0.0100
90.3
70-130
1.65
25
Diisopropyl Ether (DIPE)
0.00920
0.00050
111911-
0.0100
92.0
70-130
2.68
25
Ethylbenzene
0.00965
0.0010
mg/L
0.0100
96.5
70-130
0.207
25
2-Hexanone (MBK)
0.0864
0.010
mg/L
0.100
86.4
70-160
11.9
25
t
Isopropylbenzene (Curricne)
0.00939
0.0010
mg/L
0.0100
93.9
70-130
L69
25
p-Isopropyltoluene (p-Cymcne)
0.00981
0.0010
mg/L
0.0100
98.1
70-130
1.12
25
Methyl tert-Butyl Ether (MTBE)
0.00908
0.0010
mg/L
0.0100
90.8
7G- 130
4.10
25
Methylene Chloride
0.00910
0.0050
mg/L
0.0100
91.0
70-130
0.548
25
4-Methyl-2-pentanone (MIBK)
0.0943
0.010
mg/L
0.100
94.3
70-160
9.37
25
t
Naphthalene
0.00731
0.0020
mi/L
0.0100
73.1
40-130
17.9
25
t
n-Propylbcnzene
0.00955
0.0010
mg/L
0.0100
95.5
70-130
0.834
25
Styrene
0.00968
0.0010
mg/L
0.0100
96.8
70-130
1.13
25
1, 1,2,2-Tetrachloroethane
0.00984
O.OW50
mg/L
0.0100
98.4
70-130
6.01
25
Tetrachloroethylene
0.00918
0.00050
mg/L
0.0100
91.8
70-130
0.435
25
Toluene
0.00981
0.0010
mg/L
0.0100
98.1
70-130
1.42
25
1,2,3-Trichlorobenzene
0.00725
0.0050
mg/L
0.0100
72.5
70-130
17.3
25
1,2,4-Trichlorobenzene
0.00808
0.0010
mg/L
0.0100
80.8
70-130
7.85
25
1, 1, 1 -Trichloroethane
0.00940
0.0010
mg/L
0.0100
94.0
70-130
t.27
25
1, 1,2-Trichloroethane
0.00973
0.0010
mg/L
0.0100
97.3
70-130
1.63
25
Trichloroethylene
0.00977
0.0010
mg/L
0.0100
97.7
70-130
L83
25
Trichlorolluoromethane (Freon 11)
0.00817
0.0020
mg/L
0.0100
81.7
70-130
4.31
25
1,2,3-Trichloropropane
0.00957
0.0020
mg/L
0.0100
95.7
70-130
to.8
25
1,2,4-Trimethylbenzene
0.00950
0.0010
mg/L
0.0100
95.0
70-130
2.70
25
1,21,5-Trimethylberizene
0.00984
0.0010
mg/L
0.0100
98.4
70-130
1.61
25
Vinyl Acetate
0.0860
0.020
mg/L
0.100
86.0
70-130
1.77
25
Vinyl Chloride
0.00708
0.0020
mg/L
0.0100
70.8
40-160
1.85
25
m+p Xylene
0.0192
0.0020
mg/L
0.0200
95.9
70-130
1.81
25
o-Xylene
0.00952
0.0010
mg/L
0.0100
95.2
70-130
2.39
25
Surrogate: 1,2-Dichloroediane-d4 0.0253 mg/L 0,0250 101 70-130
Surrogate: Toluene-d8 0.0252 mg/L 0.0250 101 70-130
Surrogate: 4-Bromofluorobenzene 0.0244 mg/L 0.0250 97.4 70-130

con-NsC'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Miscellaneous Organic Analyses - Quality Control
Reporting Spike Source O/oREC RPD
Result Limit Units Level Result 0/6REC Limits RPD Limit Notes
Batch B138318 - 3810-RSK175
Blank (Bl383I8-BLK1) Prepared& Analyzed: 12/22/15
Ethane
ND
0.0028 mg/L
Ethene
ND
0,0038 mg/L
Methane
ND
0.0026 mg/L
LCS (11138318-BSI)
Prepared & Analyzed: 12/22/15
Ethane
2100
mg/L
2000 104 60-122
Ethene
2000
mg/L
2000 98.6 67-113
Methane
1900
mg/L
2000 96.3 56-121

con-aksto
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028* FAX [phone] *TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Result Limit Units Level ResWt %REC Limits "D Limit Notes
Batch B137816 - SW-846 3005A
Blank (B137816-BLK1)
Prepared: 12/16/15 Analyzed: 12/18/15
Manganese
LCS (Bl37816-BSI)
ND
2.0
Ag/L
Prepared: 12/16/15 Analyzed: 12/17/15
Manganese
LCS Dup (B137816-BSD1)
241
5.0
Pg/L
250 96.6
Prepared: 12/16/15 Analyzed: 12/17/15
80-120
Manganese
Duplicate (B137816-DUPI)
246
5.0
Source: 15LO823-02
Pg/L
250 98.4
Prepared: 12/16/15 Analyzed: 12118/15
80-120 1.90 20
Manganese
Matrix Spike (B137816-MSI)
0.852 2.0
Source: 15LO823-02
Ag/L
0.330
Prepared: 12/16/15 Analyzed: 12/18/15
911.5 20 R-04, J
Manganese
Batch B138379 - SW-846 3005A
242
5.0
;.Lg/I-
250 0.330 96.6
75-125
Blank (B138379-BLKI)
Prepared: 12/23/15 Analyzed: 12/24/15
Manganese
LCS (B138379-BS1)
ND
2.0
Ag/L
Prepared: 12/23/15 Analyzed: 12/24/15
Manganese
LCS Dup, (B139379-BSDI)
234
5.0
gg/L
250 93.6
Prepared: 12/23/15 Analyzed: 12/24/15
80-120
Manganese
237
5.0
gg/L
250 94.9
80-120 1.41 20

con-tcst"'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Metals Analyses (Dissolved) - Quality Control
Reporting Spike Source O/oREC RPD -1
Analyte Result Limit Units Level Result %REC Limits RPD Limit No,.
Batch B137936 - SW-846 3005A Dissolved
Blank (B137936-BLKI)
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
ND
2.0
Ig/L
LCS (B137936-BSI)
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
255
5.0
lig/L
250 102
80-120
LCS Dup (B137936-BSD1)
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
262
5.0
lug/L
250 105
80-120 2.75 20
Batch B138389 - SW-846 3005A Dissolved
Blank (B138389-BLKI)
Prepared: 12/23/15 Analyzed: 12/28/15
Manganese
ND
2.0
gg/L
LCS (B138389-BSI)
Prepared: 12/23/15 Analyzed: 12/28/15
Mang-M
249
5.0
119/1-
250 99.6
80-120
LCS Dup (Bl38389-BSDI)
Prepared: 12/23/15 Analyzed: 12/28/15
Manganese
248
5.0
gg/L
250 99.2
80-120 0.466 20

con-test�'
ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHAISW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit No,.
Batch B137818 - SM21-22 4500S-F
Blank (B137818-BLKl)
Prepared& Analyzed: 12/16/15
Sulfide
ND 2.0
Ing/L
LCS (Bl37918-BSI)
Prepared & Analyzed: 12/16/15
Sulfide
16 2.0
mg/L
14.8 108
60.3-119
Batch B137915 - SM 21-22 4500 NO3 F
Blank (B137915-BLK1)
Prepared & Analyzed: 12/17/15
Nitrate as N
ND 0.050
mg/L
LCS (B137915-BS1)
Prepared & Analyzed: 12/17/15
Nitrate as N
3.6 0.050
mg/L
3.41 106
88.9-111
LCS Dup (B137915-BSD1)
Prepared & Analyzed: 12/17/15
Nitrate as N
3.6 0.050
mg/L
3.41 107
88.9-111 0.825 5.66
Duplicate (B137915-DUP2)
Source: 15LOS23-02
Prepared &Analyzed: 12/17/15
Nitrate as N
ND 0.050
mg/L
0.060
NC 26.4
Matrix Spike (B137915-MS2)
Source: 15LOS23-02
Prepared & Analyzed: 12/17/15
Nitrate as N
4.2 0.050
1119/1-
3.98 0.060 105
55.9-136
Batch B137921 - SM19-22 4500 NH3 C
Blank (B137921-BLKI)
Prepared& Analyzed: 12/17/15
Ammonia as N
ND 0.30
-9/1-
LCS (Bl37921-BSI)
Prepared& Analyzed: 12/17/15
Ammonia as N
4.8 0.30
mg/L
5.00 95.8
82-106
LCS Dup (B137921-BSDI)
Prepared & Analyzed: 12/17/15
Ammonia as N
4.8 0.30
mg/L
5.00 95.8
82-106 0.00 8.24
Duplicate (Bl37921-DUP2)
Source: 15LOS23-04
Prepared & Analyzed: 12/17/15
Ammonia as IN
ND 0.30
mg/L
ND
NC 34.8
Matrix Spike (B137921-MS2)
Source: 15LOS23-04
Prepared & Analyzed: 12/17/15
Ammonia as N
1.9 0.30
mg/L
2.00 ND 93.0
71.6-116
Batch B137946 - SM 21-22 4500 NO2 B
Blank (B137946-BLK1)
Prepared & Analyzed: 12/17/15
Nitrite as N
ND 0.010
mg/L

con-tott,t)
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Irotal) - Quality Control
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B137946 - SNI 21-22 4500 NO2 B
LCS (B137946-BSI)
Prepared & Analyzed: 12/17/15
Nitrite as N
0.10 0.010
mg/L
0.100 101 90-111
LCS Dup (B137946-BSDI)
Prepared& Analyzed: 12/17/15
Nitrite as N
0.10 0.010
mg/L
0.100 99.7 90-111
1.43 5.9
Duplicate (B137946-DUPI)
Source: 15LO823-01
Prepared& Analyzed: 12/17/15
Nitrite as N
0.0034 0.010
mg/L
0.0034
0.00 23 1
Matrix Spike (B137946-MSI)
Source: 15LO823-01
Prepared &Analyzed: 12/17/15
Nitrite as N
0.099 0.010
1119/1-
0.100 0.0034 95.3 71.7-116
Batch B138131 - SM 5310C
Blank (B138131-BLKI)
Prepared: 12/21/15 Analyzed: 12/22/15
Total Organic Carbon
ND 0.50
-9/1-
LCS (B138131-BSI)
Prepared: 12/21/15 Analyzed: 12/22/15
Total Organic Carbon
9.70 0.50
-9/1-
10.0 97.0 90.1-114
LCS Dup (B138131-BSDI)
Prepared: 12/21/15 Analyzed: 12/22/15
Total Organic Carbon
9.66 0.50
mg/L
10.0 96.6 90.1-114
0.403 7.72
Duplicate (B138131-DUP2)
Source: 15LOS23-05
Prepared: 12/21/15 Analyzed: 12/22/15
Total Organic Carbon
0.802 0.50
mg/L
0.779
2.91 21.4
Matrix Spike (B138131-MS2)
Source: 15LOS23-05
Prepared: 12/21/15 Analyzed: 12/22/15
Total Organic Carbon
5.51 0.50
-9/L
5.00 0.779 94.6 66.4-114
Batch B138190 - ASTM D516-07
Blank (B138190-BLKI)
Prepared& Analyzed: 12/21/15
Sulfate
ND 2.0
-9/1-
LCS (B138190-BS1)
Prepared & Analyzed: 12/21/15
Sulfate
19 2.0
-9/1-
20.0 %.8 83.8-123
LCS Dup (B138190-BSD1)
Prepared & Analyzed: 12/21/15
Sulfate
20 2.0
-9/L
20.0 98.2 83.8-123
1.49 8.27
Batch B138279 - SM 5310C
Blank (B139279-BLKI)
Prepared & Analyzed: 12/21/15
Total Organic Carbon
ND 0.50
mg/L

con-Ust"'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result 0/oREC Limits RPD Limit Notes
Batch B138279 - SM 5310C
LCS (Bl38279-BSI) Prepared & Analyzed: 12/21115
Total Organic Carbon 9.88 0.50 mg/L 10.0 98.8 90.1-114
LCS Dup (B138279-BSDI) Prepared & Analyzed: 12/21/15
Total Organic Carbon 10.0 0.50 -9/1- 10.0 100 90.1-114 1.53 7.72
Duplicate (B138279-DUPI) Source: 15LO823-02 Prepared &Analyzed: 12/21/15
Total Organic Carbon ND 0.50 mg/L 0.171 NC 21.4
Matrix Spike (B138279-MSI) Source: 15LOS23-02 Prepared & Analyzed: 12/21/15
Total Organic Carbon 4.56 0.50 mg/L 5.00 0.171 87.7 66.4-114

con-tcst�'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadaw, MA01028 *FAX [phone]* TEL. [phone]
FLAG/QUAILIFIER SUMMARY
QC result is outside of established limits.
t Wide recovery limits established for difficult compound.
t Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
RL Reporting Limit
DL Method Detection Limit
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
i Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-07 Either laboratory fortified blank/laboratory, control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFBALCS results is within method specified criteria.
R-04 Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that
are <5 times the reporting limit (RL).
V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.

con-toto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
3810-RSKI 7S in Water
Ethane
VANYME
Ethene
VA,NYME
Methane
VA,NYME
ASTMD516-07in Water
Sulfate
NYNHMACTR1,VANC
SM21-22 4500 NO2 Bin Water
Nitrite as N
CTNH,NYMENC,VA,Rl
SM 21-22 4500 NO3 F in Water
Nitrate as N
CTMA,NH,NYR1,ME,NC,VA
SM531OC in Water
Total Organic Carbon
NYNC,CTJU,ME,MA,VA
SM19-22 4500 NH3 C in Water
Ammonia as N
NYMA,CTR1,VANCME
SM21-22 4SOOS-F in Water
Sulfide
CTNH,NYR1,NC,ME,VA
SW-846 6020A in Water
Manganese
CTNH,NYNC,ME,VA
Manganese
CTNH,NYNC,MEVA
SW-846 8260B in Water
Acetone
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Bromoform
NC
Bromomethane
NC
2-Butanone (MEK)
NC
n-Butylbenzene
NC
sec-Butylbcnzene
NC
tert-Butylbenzene
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethanc
NC
Chloroethane
NC
Chloroform
NC
Chloroincthane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromoethane (EDB)
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
Dichlorodifluoromethane (Freon 12)
NC

con-toto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8260B in Water
1, 1 -Dichloroethane
NC
1,2-Dichloroethane
NC
I,I-Dichloroethylene
NC
cis- 1,2-Dichloroethylene
NC
trans- 1,2-Dichloroethylene
NC
1,2-Dichloropropane
NC
1,3-Dichloropropane
NC
2,2-Dichloropropane
NC
1,1-Dichloropropene
NC
cis- 1,3-Dichloropropene
NC
trans- 1,3-Dichloropropene
NC
Diisopropyl Ether (DIPE)
NC
Ethylbenzene
NC
2-Hexanone (MBK)
NC
Isopropylbenzene (Cumene)
NC
p-Isopropyltoluene (p-Cymene)
NC
Methyl tert-Butyl Ether (MTBE)
NC
Methylene Chloride
NC
4-Methyl-2-pentanone (M113K)
NC
Naphthalene
NC
n-Propylbenzene
NC
Styrene
NC
1, 1,2,2-Tetrachloroethane
NC
Tetrachloroethylene
NC
Toluene
NC
1,2,3-Trichlorobenzene
NC
1,2,4-Trichlorobenzene
NC
1, 1, 1 -Trichloroethane
NC
1,1,2-Trichloroethane
NC
Trichloroethylene
NC
Trichlorofluoromethane (Freon 11)
NC
1,2,3-Trichloropropanc
NC
1,2,4-Trimethylbenzene
NC
1,3,5-Trimethylbenzene
NC
Vinyl Acetate
NC
Vinyl Chloride
NC
m+p Xylene
NC
o-Xylene
NC

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA01028 * FAX [phone] * TEL. [phone]
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP� LLC
100033
02/1/2016
MA
Massachusetts DEP
M-MAIOO
06/30/2016
CT
Connecticut Department of Publile Health
PH-0567
09/30/2017
NY
New York State Department of Health
10899 NELAP
04/1/2016
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2016
RI
Rhode Island Department of Health
LAOOO 112
12/30/2015
NC
North Carolina Div. ofWater Quality
652
12/31/2016
NJ
New Jersey DEP
MA007 NELAP
06/30/2016
FL
Florida Department of Health
E871027 NELAP
06/30/2016
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2016
WA
State of Washington Department of Ecology
C2065
02/23/2016
ME
State of Maine
2011028
06/9/2017
VA
Commonwealth ofVirginia
460217
12/14/2016
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2016

(iD Phone: [phone] CHAIN OF CUSTODY RECORD 39 Spruce Street
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Address: ii,-,it-L16ROOOC� Ri. �Oi-t Project # LA 00c
F—k V\ Client PO#
Attention:
DATA DELIVERY (check all that apply)
0 FAX VEMAIL OWEBSITE
7-
Project Location:
Fax #
Sampled By: g,0SZTy z Cori) 10061f)
Email: BAillW(.0, �Ar-Dtt<,,
Format: PPDF APEXCEL OGIS
0
Z
t
Project Proposal Provided? (for billing purposes)
0 yes proposal date -L
Collection
- OTHER
0 "Enhanced Data Package"
Q,
-
M k)
5- k) --D
IC
I-E
Con -Test Lab ID
Client Sample ID / Description
-Beg—Mir
_f_ffnK_`
*Matrix
Conc
(laboratory use only�
Date/Time-
aate�Time
Composite
Grab
Code
Code
I
A
I Y_
I V\I
k
/,l vv( t a A
-�d
7
'rl L
A W q " 11/6
MEManno
mmmmmmc
MEEMEMN
Page I of--L
It of Containers
** Preservation
*"Container Code
Dissolved Metals
0 Field Filtered
0 tab to Filter
***Cont. Code:
A=amber glass
G=glass
P=plastic
ST=sterile
V= vial
S=summa can
T=tedlar bag
O=Other
"Preservation
I = Iced
H HCL
M Methanol
N Nitric Acid
5 Sulfuric Acid
B Sodium bisulfate
X Na hydroxide
T Na thiosulfate
0 Other
*Matrix Code:
GW= groundwater
WW= wastewater
Please use the following codes to let Con -Test know if a specific sample m "y be high DW= drinking water
A= air
pro,;ec-4 )t
��
in concentration in Matrix/Conc. Code Box;
............. I ................................... I ......................................................................................... �
S = soil/solid
H - High; M - Medium; L - Low; C - Clean; U - Unknown
SL sludge
Relinquished by: (signature)
C-C:V-A9'
Date/Time:
Turnaround
Detection
Limit Reguirements
Program Information
0 h
0 5-Day
North Carolina
Receeiged by: (s!Watu
?4z
Date[Time:
0 5-7-Day
0 2L
DSCA 0 IHSB Orphaned Landfill
0 10-Day
0 GWPC
0 SWS Landfill 0 LIST 0 REC
Rerli,shed 4#02�
Date/Time:
$
BO.H.
'24-Hr
0 SWSL
0 Other:
tg
0 r'48-Hr
0 OTHER
A LCo�� /I
R ce * d by: (si Ir C_VDte/T[e:
0 '72-Hr r'4-Day
M, NELAC & ANA Certified
�.!t AII-IN
Z
A01 Z�161'
Requires Lab Approval
WBE/DBE Certified
11 TURNAR66N6 TIME (6usiness days) STARTS AT 9:00 A.M. THE DAY AFTER SAMPLE RECEIPT UNLESS THERE ARE QUESTIONS ON YOUR CHAIN.
IF THIS FORM IS NOT FILLED OUT COMPLETELY OR IS INCORRECT, TURNAROUND TIME WILL NOT START UNTIL ALL QUESTIONS ARE ANSWERED.
PLEASE BE CAREFUL NOT TO CONTAMINATE THIS DOCUMENT

12/16/2015
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39 Spruce St.
East Longmeadow, MA. 01028
P: 413-525-2332
F: 413-525-6405
www.contestiabs.com
CLIENT NAME:
Page 1 of 2
Sample Receipt Checklist
RECEIVED B Y: L)
1) Was the chain(s) of custody relinquished and signed? e No
2) Does the chain agree with the samples? Y �es' N c,
If not, explain:
3) Are all the samples in good condition? 0yes No
If not, explain:
4) How were the samples received:
con test"
ANALY"FICAL LABORATORY
No CoC Included
On Ice [14""_ Direct from Sampling El Ambient 0 In Cooler(s) Eg--'
Were the samples received in Temperature Compliance of (2-6'C)? 6�� N o N/A
Temperature 'C by Temp blank 3-0 -Temperature oC by Temp gun
5) Are there Dissolved samples for the lab to filter? Yes -1
60
Who was notified D a —te Time
E3affiples? No
6) Are there any RUSH or ORT HOLDING TIME 6�
Who was notified Date Time er ission to subcontract samples? Yes No
7) Location where samples are stored: (Walk-in clients only) if not already approved
Client Signature:
8) Do all samples have the proper Acid pH: Q No N/A
9) Do all samples have the proper Base pH: Ge No NIA
1M Waq the PC notified of a,,. discreow-1-Jes with the CoC vs the samples: Yes N o nN1
Containers received at Con -Test
# of containers
# of containers
1 Liter Amber
8 oz amber/clear jar
500 mL Amber
4 oz amber/clear jar
250 mL Amber (8oz amber)
2 oz amber/clear jar
1 Liter Plastic
Plastic Bag / Ziploc
500 mL Plastic
SOC Kit
250 mL plastic
Non-ConTest Container
40 mL Via[ - type listed below
3141
Perchlorate Kit
Colisure / bacteria bottle
Flashpoint bottle
Dissolved Oxygen bottle
Other glass jar
Encore
Other
Laboratory Comments:
/1% A
S nc)+ a C-lb
40 mL vials: # Methanol
# HCI
664 271 .. # Bisulfate # DI Water
..v . A A. . m­t 9n1,1 Thiosulfate Unpreserved
Time and Date Frozen:

Page 2 of 2
Login Sample Receipt Checklist
(Rejection Criteria Listing - Using Sample Acceptance Policy)
Any False statement will be brought to the attention of Client
Question Answer (True1F_ e Comment
T1F/NA
1) The cooler's. custody seal, if present, is intact.
2) The cooler or samples do not appear to have
been compromised or tampered with.
3) Samples were received on ice.
4) Cooler Temperature is acceptable.
5) Cooler Temperature is recorded.
6) COC is filled out in ink and legible.
7) COC is filled out with all pertinent information.
8) Field Sampler's name present on COC.
9) There are no discrepancies between the
sami)le IDs on the container and the COC.
10 Samples are received within Holding Time.--
11) Sample containers have legible labels.
12) Containers are not broken or leaking.
13) Air Cassettes are not brokenlopen.
ru
14) Sample collection date/times are provided.
I-
15) Appropriate sample containers are used.--
16) Proper collection media used.
17) No headspace sample bottles are comLetely filled.
18) There is sufficient volume for all reclusted
analyses, including any requested MS/MSDs.
19) Trip blanks_provided if applicable.
20) VOA sample vials do not have head space or
bubble is <6mm (1/4") in diameter.
21) Samplesdo not require splitting or compositing.
Who notitied ot 1malse statements r e:
Doc #277 Rev. 4 August 2013 Log -in Technician Initials: M) Date[Time:

Table of Contents
con-ksto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 29, 2015
Justin Ballard
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: Pro Cleaners
Client Job Number:
Project Number: DC920 I SL33
Laboratory Work Order Number: 15L0906
Enclosed are results of analyses for samples received by the laboratory on December 16, 2015. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
I Page 1

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
15LO906-01
15LO906-02
15LO906-03
Sample Preparation Information
QC Data
Volatile Organic Compounds by GUMS
B138109
B138121
Miscellaneous Organic Analyses
B138318
Metals Analyses (Total)
B138299
B138642
Metals Analyses (Dissolved)
B137936
B138641
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B138048
B138214
B138250
B138306
B138312
4
5
6
6
12
18
24
26
26
26
30
34
34
35
35
35
36
36
36
37
37
37
37
37
38
I Page 2

Table of Contents
Table of Contents (continued)
B138422
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
38
39
40
43
I Page 3 of 46 1

Table of Contents
con-tcsV'
ANALYTICAL LABORATORY
39 Spruce Street East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121 REPORT DATE: 12/29/2015
Raleigh, NC 27604 PURCHASE ORDER NUMBER:
ATTN: Justin Ballard
PROJECT NUMBER: DC9201SL33
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 15LO906
The results ofanalyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Pro Cleaners
FIELD SAMPLE 4 LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
MW-5 15LO906-01 Ground Water 3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 NI-13 C
SM21-22 450OS-F
SW-846 6020A
SW-846 8260B
MW-24D 15LO906-02 Ground Water 3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 NE3 C
SM21-22 450OS-F
SW-846 6020A
SW-846 8260B
MW-8B 15LO906-03 Ground Water 3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 NH3 C
SM21-22 4500S-F
SW-846 6020A
SW-846 8260B
I Page 4

Table of Contents
con-t(SV
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
SW-846 8260B
Qualifications:
1-04
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery arc outside ofcontrol limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
Dichlarodifluoromcthane (Freon 1.
15L0906-01 [MW-51, 15LO906-03 [MW-8B], B 138109-BLK 1, B I 38109-BS 1, B I 38109-BSD I
RL-1 I
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
15LO906-03W-SB]
V-05
Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is
associated with the reported value which is likely to be biased on the low side.
Amilyte & Samples(s) Qualified:
1,2,3-Trichlorobenzene
15LO906-02[MW-24D), B138121-BLKI, B138121-BSI, B138121-BSDI
Naphthalene
15LO906-02V"-24D], B138121-BLKI, B138121-BSI, B138121-BSDI
V-20
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was'. no' detected" for this compound.
A..Ilyle & Samples(s) Qualified:
Bromomethane
B138121-BSI, B138121-BSDI
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, ifany, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry ofthose individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best ofmy knowledge and belief, accurate and complete.
IL
Johanna K Harrington
Manager, Laboratory Reporting
I Page 5 =

Table of Contents
con-tcsV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample 4: MW-5 Sampled: 12/16/2015 10:10
Samnle ID: 15LO906-01
Sanwle Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Acetone ND 0.050 0.0049 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Benzene ND 0.0010 0.00012 -9/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Bromobenzene ND 0.0010 0.00015 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Bromochloromethane ND 0.0010 0.00022 -9/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Bromodichloromethane ND 0.00050 0.000088 mg/1- I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Bromoform ND 0.0010 0.00021 -9/1- 1 SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Bromomethane ND 0.0020 0.00094 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
2-Butanone (MEK) ND 0.020 0.0024 m9/1- I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
n-Butylbcnzene ND 0.0010 0.00015 -g4, I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
see-Butylbenzene ND 0.0010 0.00013 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
tert-Butylbenzene IND 0.0010 0.00011 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Carbon Disulfide ND 0.0040 0.0010 -9/1- 1 SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Carbon Tetrachloride ND 0.0050 0.00012 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Chlorobcnzene ND 0.0010 0.00016 -9/1- 1 SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Chlorodibromomethane ND 0.00050 0.00010 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Chloroethane ND 0.0020 0.00028 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Chloroform 0.00026 0.0020 0.00022 mg/L I J SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Chloromethane ND 0.0020 0.00032 mg/L I SW-946 8260B 12/20/15 12/20/15 22:31 EEH
2-Chlorotoluene ND 0.0010 0.00012 mg/L I SW-946 8260B 12/20/15 12/20/15 22:31 EEH
4-Chlorotoluene ND 0.0010 0.00014 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
1,2-Dibromoethane (EDB) ND 0.00050 0.00012 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
1,2-Dichlorobenzene ND 0.0010 0.00017 -91 1 SW-846 8260B 12/20/15 12/20/15 22:31 EEH
1,3-Dichlorobenzene ND 0.0010 0.00017 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
1,4-Dichlorobenzene ND 0.0010 0.00015 Ing/L 1 SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Dichlorodifluoromethane (Freon 12) ND 0.0020 0.00018 mg/L I L-04 SW-846 8260B 12/20/15 12/20/15 22:31 EEH
IJ-Dichloroethane ND 0.0010 0.00016 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
1,2-Dichloroediane ND 0.0010 0.00019 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
I,I-Dichloroethylenc ND 0.0010 0.00021 Ing/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
cis- 1,2-Dichloroethylene 0.00085 0.0010 0.00015 Ing/L I J SW-846 8260B 12/20/15 12/20/15 22:31 EEH
trans- 1,2-Dichlorocthylene ND 0.0010 0.00015 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
1,2-Dichloropropane IND 0.0010 0.00013 Ing/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
1,3-Dichloropropane ND 0.00050 0.00013 -9/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
2,2-Dichloropropane ND 0.0010 0.00016 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
IJ-Dichloropropene ND 0.0020 0.00013 mg/L I SW-846 8260B 12120/15 12/20/15 22:31 EEH
cis- 1,3-Dichloropropene ND 0.00050 0.00012 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
trans- 1,3-Dichloropropene ND 0.00050 0.00011 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Diisopropyl Ether (DIPE) ND 0.00050 0.00018 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Ethylbenzene IND 0.0010 0.00013 mg/L I SW-946 8260B 12/20/15 12/20/15 22:31 EEH
2-Hexanone (MBK) ND 0.010 0.0015 mg/L I SW-846 8260B 12t20/15 12/20/15 22:31 EEH
lsopropylbenzene (Cumene) ND 0.0010 0.00012 Ing/L I SW-946 8260B 12/20/15 12/20/15 22:31 EEH
p-Isopropyltoluene (p-Cymene) ND 0.0010 0.00015 mg/L I SW-946 8260B 12/20/15 12/20/15 22:31 EEH
Methyl tert-Butyl Ether (MTBE) ND 0.0010 0.000090 mg/L I SW-846 8260B 12/20/15 12/20/15 22:31 EEH
Methylene Chloride ND 0.0050 0.0032 11191 1 SW-946 8260B 12/20/15 12/20/15 22:31 EEH
4-Methyl-2-pentanone (MlBK) ND 0.010 0.0015 mg/L I SW-846 8260D 12/20/15 12/20/15 22:31 EEH
I Page 6 of 46

Table of Contents
con -test"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadaw, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample#: MW-5 Sampled: 12/16/2015 10:10
Samnle ID: 15LO906-01
SamDle Matrix: Ground Water
Volatile Organic Compounds by C.C/MS
Date
DatelTime
Analyte
Results
RL
DL
Units
Dilution
Flag/Qua]
Method
Prepared
Analyzed
Analyst
Naphth ene
ND
0.0020
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
n-Propylbcnzcne
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:31
EEH
Styrene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12420/15
12/20/15 22:31
EEH
1, 1,2,2-Tetrachloroctliane
ND
0.00050
0.00016
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:31
EEH
Tetrachloroethylenc
0.0038
0.00050
0.00017
-9/L
1
SW-946 8260B
12/20/15
12/20/15 22:31
EEH
Toluene
0.00019
0.0010
0.00017
mg/L
I
i
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
1, 1, 1 -Trichloroediane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
Trichloroethylene
0.00030
0.0010
0.00020
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
Trichlorofluoromediane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
1,2,3-Tricldoropropane
ND
0.0020
0.00019,
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:31
EEH
1,3,5-Trimethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:31
EEH
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:31
EEH
-+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
o-Xylcne
ND
0.0010
0.00013
mg4-
I
SW-846 8260B
12/20/15
12/20/15 22:31
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dicliloroediane-d4
106
70-130
12/20/15 22:31
Toluene-d8
IDO
70-130
12/20/15 22:31
4-Bromofluorobenzenc
%.6
70-130
12/20/15 22:31
I Page 7 :of 4::6::::]

Table of Contents
con-toto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL, 413/525-2332
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample#: MW-5 Sampled: 12/16/2015 10:10
SaMDle ID: 15L0906-01
Samnle Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Daterfime
Analyte Results
RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
-9/1- 1
3810-RSK175
12/22/15
12/22/15 17:51
TPH
Ethene ND
0.0038
0.00099
-9/1- 1
3810-RSK175
12t22/15
12/22/15 17:51
TPH
Methane ND
0.0026
0.0011
mg/L I
3810-RSK175
12/22/15
12/22/15 17:51
TPH
I Page 8

Table of Contents
61 con-Usto
ANALYTICAL LABOPATORY
39 Spruce Street * East Longmeadaw, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/1&2015
Field Sample #: MW-5 Sampled: 12/16/2015 10:10
Samnle ID: 15LO906-01
Samnle Matrix: Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua[ Method Prepared Analyzed Analyst
Manganese 21 2.0 0.23 Ag/L 2 SW-846 6020A 12/28/15 12/29/15 11:43 MJH
I Page 9 of 46 1

Table of Contents
A ALMLAK&
Milli cannwlv
�LIAA
Wrl ANALYMAIL LABORATMY 39 Spruoe Street * East Longmeadow, MA 01028 * FAX [phone] TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample 4: MW-5 Sampled: 12/16/2015 10:10
SamDle ID: 151-8906-01
Samole Matrix: Ground Water
Metals Analyses (Dissolved)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Manganese 6.2 10 0.23 PgIL 2 SW-846 6020A 12/28/15 12/29/15 12:14 MJH
I Page10of46 I

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
project Location: Pro Cleaners Sample Description: Work Order: ISLO906
Date Received: 12/16/2015
Field Sample N: NfW-5 Sampled: 12/16/2015 10:10
Samole ID: 15LO906-01
Samnle Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APRA/SW-846 Methods (Total)
Date
Datetrime
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ammonia as N
ND
0.30
0.22
1119/L
I
SM19-22 4500 NH3 C
12/22/15
12/23/15 14:00
VAK
Nitrate as N
ND
0.050
0.049
mg/L
I
SM 21-22 4500 NO3 F
12/22/15
12/23/15 15:45
AG
Nitrite as N
0.0058
0.010
0.0020
mg/L
I i
SM 21-22 4500 NO2 B
12/18/15
12/18/15 10:10
MM11
Sulfate
5.3
2.0
0.40
mg/L
I
ASTM D516-07
12/22/15
12/22/15 13:53
MI%*1
Sulfide
ND
2.0
1.8
mg/L
I
SM21-22 450OS-F
12/21/15
12/21/15 18:45
DJM
Total Organic Carbon
0.32
0.50
0.16
mg/L
I i
SM 5310C
12/23/15
12/23/15 15:30
LL
I Page 11

Table of Contents
con-test'9
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample #: NM-24D Sampled: 12/16/2015 11:30
Samnle ID: 15LO906-02
SamDle Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RIL
DL
Units
Dilution Flag/Qual
Method
Prepared Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Benzene
ND
0.0010
0.000079
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Bromobenzene
ND
0.0010
0.00015
-9/1-
1
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Bromochloromethanc
ND
0.001-0
0.00022
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Brornomethane
ND
0.0020
0.00094
mg/1-
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
n-Butylbenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
sec-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
Carbon Tetrachloride
ND
0.0050
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Chlorobcnzenc
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Chlorocthane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Chloroform
ND
0.0020
0.00022
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
2-Chlorotolucne
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
4-Chlorotoluene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,2-Dibromoethane (EDB)
ND
0.00050
0.000089
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,2-Dichlorobenzene
ND
0.0010
0.00010
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,3-Diclilorobetizene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,4-Dichlorobenzcne
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
IJ-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/21115
12/21/15 14:18
EEH
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
IJ-Dichloroetitylene
ND
0.0010
0.00021
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
cis- 1,2-Dichlorocthylene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
traw- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,2-Dichloropropanc
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,3-Dichloropropane
ND
0.00050
0.00011
mg/L
I
SW-946 8260B
12/21/15
12t2l/15 14:18
EEH
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
IJ-Dichloropropcne
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/21/t5
12/21/15 14:18
EEH
cis- 1,3-Dichloropropene
ND
0.00050
0.000062
mg/L
I
SW-846 8260B
12421/15
12/21/15 14:18
EEH
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-846 8260B
12t2l/15
12/21/15 14:18
EEH
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Ethylbenzene
ND
0.0010
0.00013
-9/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
2-Hexanone (MBK)
ND
0.010
0.0015
-9/1-
1
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
lsopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
p-Isopropyltoluene (p-Cymene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
4-Mediyl-2-pentanone (MIBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
I Page 12

0 con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 0 1028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample 4: MW-24D Sampled: 12/16/2015 11:30
S2mnle ID: 15LO906-02
Sanmlc Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mg/L
I
V-05
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
n-Propylbenzene
ND
0.0010
0.00011
mg/L
1
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Styrene
ND
0.0010
0.00015
-9/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00013
-9/1-
1
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Tetrachloroethylene
0,0010
0.00050
0.00017
-9/1-
1
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Toluene
0.00030
0.0010
0.00010
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,2,3-Trichlorobenzene
NO
0.0050
0.00014
mg/L
I
V-05
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
1,1,1-Trichloroedmc
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,1,2-Trichloroetliane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Trichloroethylene
NO
0.0010
0.00020
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Trichlorolluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,2,3-Ttichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-946 8260B
12/21/15
12/21/15 14:18
EEH
1,3,5-Trimethylbenzene
ND
0.0010
0.00010
mg/L
1
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Vinyl Acetate
ND
0.020
0.0014
Ing/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Vinyl Chloride
ND
0.0020
0.00013
m9/1-
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
m+p Xylene
ND
0.0020
0.00025
Ing/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
o-Xylene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/21/15
12/21/15 14:18
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qtul
1,2-Dichloroediane-d4
97.4
70-130
12/21/15 14:18
Toluene-d8
99.1
70-130
12/21/15 14:18
4-Bromofluorobenzene
98.1
70-130
12/21/15 14:18
I Page 13 of 46 1

con-stestw
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample#: MW-24D Sampled: 12/16/2015 11:30
Sgmnle ID: 15LO906-02
Samole Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Date/Time
Analyte Results
RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
mg/L I
3810-RSK175
12/22/15
12/22/15 18-03
TPH
Ethene ND
0.0038
0.00099
-9/L I
3810-RSK175
12/22/15
12/22/15 18:03
TPH
Methane ND
0.0026
0.0011
-9/1- 1
3810-RSK175
12/22/15
12/22/15 18:03
TPH
I Page 14

con-UsV
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street* East Longmeadow, MA 01028 *FAX [phone] *TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample 4: MW-24D Sampled: 12/16/2015 11:30
Samnle ID: ISLO906-02
SamDle Matrix-:- Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] method - — Prepared Analyzed Analyst
Mangan se 710 2.0 U3 Vg/L 2 SW-946 6020A 12/28/15 12/29/1511:47 MJH
I Page 1Eo:f=46

Table of Contents
0 con-tcstO
ANALYTICAL LABOPATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample#: MW-24D Sampled: 12/16/2015 11:30
Sanmle ID: 15L0906-02
Samole Matrix: Ground Water
Metals Analyses (Dissolved)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 2.2 2.0 0.23 Pg/L 2 SW-846 6020A 12/28/15 12/29/1512:17 MJH
I Page 16 of 46

Table of Contents
con-NsC'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample#: MW-24D Sampled: 12/16/2015 11:30
SaInDle ID: 15LO906-02
SarnDle Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APRA/SW-846 Methods (Total)
Date
Date/Time
Analyte
ftesults
RL
DL
Units
Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Ammonia as N
ND
0.30
0.22
mg/L
I
SMI 9-22 4500 NH3 C
12/22/15
12/23/15 14:00
VAK
Nitrate as N
0.14
0.050
0.049
mg/L
I
SM 21-22 4500 NO3 F
12/22/15
12/23/15 15:45
AG
Nitrite as N
0.0077
0.010
0.0020
mg/L
I J
SM 21-22 4500 NO2 B
12/18/15
12/18/15 10:10
NOAH
Sulfate
ND
2.0
0.40
-9/1-
1
ASTM D516-07
12/22/15
12/22/15 13:53
MMH
Sulfide
4.0
2.0
1.8
Ing/L
I
SM21-22 450OS-F
12/21/15
12/21/15 18:45
DJM
Total Organic Carbon
0.28
0.50
0.16
mg/L
I J
SM 5310C
12/23/15
12/23/15 15:30
LL
I Page 7�

Table of Contents
con-tesV'
ANALYTICAL LABOPATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] TEL. [phone]
Project Location: Pro Cleaners
Sample Description:
Work Order: 15LO906
Date Received: 12/16/2015
Field Sample 4: MW-8B
Sampled: 12/16/2015
14:10
Samnle ID: 15L0906-03
Samole Matrix: Ground Water
Sample Flags: RL- I I
Volatile
Organic Compounds
by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
0.019
0.10
0.0097
-9/1-
2 J
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Benzene
ND
0.0020
0.00024
Ing/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Bromobcnzene
NO
0.0020
0.00030
Ing/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
Bromochloromethane
ND
0.0020
0.00045
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Bromodichloromethane
ND
0.0010
0.00018
Ing/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
Bromoform
ND
0.0020
0.00042
Ing/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Bromomethane
NO
0.0040
0.0019
Ing/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
2-Butanone (MEK)
ND
0.040
0.0047
Ing/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
n-Butylbenzene
NO
0.0020
0.00030
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
sec-Butylbenzene
NO
0.0020
0.00026
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
tert-Butylbenzene
ND
0.0020
0.00022
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Carbon Disulfide
ND
0.0080
0.0020
mg/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
Carbon Tetrachloride
ND
0.010
0.00024
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Chlorobenzene
ND
0.0020
0.00032
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Chlorodibromomethane
ND
0.0010
0.00020
mg/L
2
SW-846 9260B
12/20/15
12/21/15 6:04
EEH
Chlorocthane
ND
0.0040
0.00056
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Chloroform
0.0026
0.0040
0.00044
mg/L
2 J
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Chloromethane
ND
0.0040
0.00065
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
2-Chlorotoluene
ND
0.0020
0.00024
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
4-Chlorotoluene
ND
0.0020
0.00028
Ing/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,2-Dibromoethane (EDB)
ND
0.0010
0.00024
-9/1-
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,2-Dichlorobenzene
ND
0.0020
0.00034
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,3-Dichlorobenzene
ND
0,0020
0.00034
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,4-Dichlorobenzene
ND
0.0020
0.00030
mg/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
Dichlorodifluoromethane (Freon 12)
NO
0.0040
0.00036
mg/L
2 L-04
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1, I-Dichloroethane
ND
0.0020
0.00032
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,2-Dichloroethane
ND
0.0020
0.00039
mg/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
IJ-Dichloroethylenc
ND
0.0020
0.00042
mg/L
2
SW-846 8260B
l2a0/1 5
12/21/15 6:04
EEH
cis- 1,2-Dichloroedlylene
0.0061
0.0020
0.00029
Ing/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
trans- 1,2-Dichloroethylene
ND
0.0020
0.00030
Ing/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
1,2-Dichloropropane
ND
0.0020
0.00026
Ing/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,3-Dichloropropane
ND
0.0010
0.00026
-9/1-
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
2,2-Dichloropropane
ND
0.0020
0.00032
-91L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
IJ-Dichloropropene
ND
0.0040
0.00026
-9/1-
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
cis- 1,3-Dichloropropene
ND
0.0010
0.00024
Ing/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
trans- 1,3-Dichloropropene
ND
0.0010
0.00022
Ing/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Diisopropyl Ether (DIPE)
ND
0.0010
0.00036
-9/1-
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Ethylbenzene
ND
0.0020
0.00026
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
2-Hexanone (MBK)
ND
0.020
0.0030
mg/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
Isopropylbenzene (Cumene)
ND
0,0020
0.00024
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
p-Isopropyltoluene (p-Cymene)
ND
0.0020
0.00030
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.0020
0.00018
Ing/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
Methylene Chloride
ND
0.010
0.0064
-9/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
4-Mediyl-2-pentanone (MlBK)
ND
0.020
0.0029
mg/L
2
SW-946 8260B
12/20/15
12/21/15 6:04
EEH
I Page 1

Table of Contents
con-tot"o
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample 4: MW-8B Sampled: 12/16/2015 14:10
S2mnle ID: 15LO906-03
Samole Matrix: Ground Water
Sample Flags: RL- I I Volatile Organic Compounds by C.C/MS
Date
Daterrime
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
NaphdW ne
ND
0.0040
0.00024
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
n-Propylbenzene
ND
0.0020
0.00026
mg/L
2
SW-846 8260H
12/20/15
12/21/15 6:04
EEH
Styrene
ND
0.0020
0.00030
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1, 1,2,2-Tetimchloroethane
ND
0.0010
0.00032
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Tetrachloroethylene
0.19
0.0010
0.00034
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Toluene
0.00036
0.0020
0.00034
mg/L
2 1
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,2,3-Tjichlorobenzene
ND
0.010
0.00028
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,2,4-Trichlorobenzene
ND
0.0020
0.00038
mg/L
2
SW-846 8260B
12/20/15
12t2l/15 6:04
EEH
1,1,1-Trichloroethanc
ND
0.0020
0.00019
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1, 1,2-Trichloroediane
NO
0.0020
0.00023
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Trichloroethylene
0.0040
0.0020
0.00040
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Trichlorofluoromediane (Freon 11)
ND
0.0040
0.00029
mg/L
2
SW-846 8260B
12/20/15
12t2l/15 6:04
EEH
1,2,3-Trichloropropane
ND
0.0040
0.00038
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,2,4-Trimedlylbenzene
ND
0.0020
0.00036
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
1,3,5-Trimediylbenzene
ND
0.0020
0.00026
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Vinyl Acetate
ND
0.040
0.0029
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
Vinyl Chloride
ND
0.0040
0.00027
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
m+p xylene
ND
0.0040
0.00050
mg/L
2
SW-846 8260B
12/20/15
12/21/15 6:04
EEH
o-Xylene
ND
0.0020
0.00026
mg/L
2
SW-846 8260B
12420/15
12/21/15 6:04
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dicl-doroethane-d4
104
70-130
12/21/15 6:04
Toluene-dg
100
70-130
l2t21115 6:04
4-Bromofluorobcnzene
96.4
70-130
l2t21115 6:04
I Page 19

Table of Contents
con-tcsV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample W: MW-SB Sampled: 12/16/2015 14:10
Samnle El): 15LO906-03
SaMDle Matrix: Ground Water
Miscellaneous Organic Analyses
Date
DatelTime
Analyte Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
-9/1-
1
3810-RSK175
l2n2/15
12/22/15 18:16
TPH
Ethene ND
0.0038
0.00099
1-9/1-
1
3810-RSK175
12/22/15
12/22/15 18:16
TPH
Methane 6.4
0.013
0.0056
-9/1-
5
3810-RSK175
12/22/15
12/22/15 18:30
TPH
I Page 20

..........
Table of Contents
con-test`�'
ANALYTICAL LABORATORY
39 Spruce Street - East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12116/2015
Field Sample#: MW-SB Sampled: 12/16/2015 14:10
Samnle ID: 15L0906-03
Samole Matrix: Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Manganese 86 2.0 0.23 Pg/L 2 SW-846 6020A 12/28/15 12/29/15 11 50 MJH
I Page 21 of �46

R
con4o
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12AU2015
Field Sample*: MW-8B Sampled: 12/16/2015 14:10
Samnle ID: ISLO906-03
Sarnole Matrix: Ground Wate
Metals Analyses (Dissolved)
Manganese
Date Datefrime
Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
86 2.0 0.23 Pgq- 2 SW-846 6020A 12/28/15 12/29/15 12:21 MJH
I Page 2

Table of Contents
con-tesV
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadaw, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Pro Cleaners Sample Description: Work Order: 15LO906
Date Received: 12/16/2015
Field Sample 4: MW-8B Sampled: 12/16/2015 14:10
SaInDle ID: 15LO906-03
Samole Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APHAISW-846 Methods (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ammonia as N
ND
0.30
0.22
mg/L
I
SM19-22 4500 NH3 C
12/22/15
12/23/15 14:00
VAK
Nitrate as N
0.12
0.050
0.049
mg/L
I
SM 21-22 4500 NO3 F
12/22/15
12/23/15 15:45
AG
Nitrite as N
0.031
0.010
0.0020
Ing/L
I
SM 21-22 4500 NO2 B
12/18/15
12/18/15 10:10
K0,M
Sulfate
ND
2.0
0.40
mg/L
I
ASTM D516-07
12/22/15
12/22/15 13:53
MMH
Sulfide
ND
2.0
1.8
mg/L
I
SM21-22 450OS-F
12/21/15
12/21/15 18:45
DJM
Total Organic Carbon
0.98
0.50
0.16
mg/L
I
SM 5310C
12/23/15
12/23/15 15:30
LL
ARNOW-
RL
WIN*
I Page 23

Table of Contents
con-atesV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
3810-RSK175
Lab Number [Field ID)
Batch
Initial [mLl
Final [mL]
Date
15LO906-01 [MW-51
B138318
1.00
1.00
12/22/15
15LO906-02 [MW-24D]
B138318
1.00
1.00
12/22/15
15L0906-03 [MW-8B)
B138318
1.00
1.00
12/22/15
15LO906-03REI [MW-8131
B 138318
1.00
1.00
12/22/15
ASTM D516-07
Lab Number [Field ID]
Batch
Initial JmLl
Final JmLj
Date
15LO906-01 [MW-5]
B138306
100
100
12/22/15
15LO906-02 [N4W-24D]
B138306
100
100
12/22/15
15LO906-03 [MW-813]
B138306
100
100
12/22/15
SM 21-22 4-100 NO2 B
Lab Number [Field ID1
Batch
Initial [mL]
Final [mL]
Date
15L0906-01 V"-51
B 138048
50.0
50.0
12/18/15
15L0906-02 [MW-24D]
B138048
50.0
50.0
12/18/15
15LO906-03 W-813)
B138048
50.0
50.0
12/18/15
SM 21-22 4500 NO3 F
Lab Number lField ID]
Batch
Initial [mL]
Final lmLj
Date
15LO906-01 W-5]
B 138312
25.0
25.0
12/22/15
15L0906-02 [MW-24D]
B 138312
25.0
25.0
12/22/15
15LO906-03 W-813]
B 138312
25.0
25.0
12/22/15
SM 5310C
Lab Number [Field ID1
Batch
Initial [nit,]
Final [mLl
Date
ISLO906-01 [MW-5]
B 138422
50.0
50.0
12/23/15
15LO906-02 W-24131
B 138422
50.0
50.0
12/23/15
15LO906-03 P"-8131
B 138422
50.0
50.0
12/23/15
SM19-22 4500 NH3 C
Lab Number [Field IDJ
Batch
Initial [mL]
Final [mLl
Date
15LO906-01 W-51
B138250
100
100
12/22/15
15LO906-02 W-241)]
B138250
too
100
12/22/15
15L0906-03 [MW-8B]
B138250
100
100
12/22/15
SM21-22 450OS-F
Lab Number [Field ID]
Batch
Initial [mL]
Final [mLj
Date
15LO906-01 P"-51
B 138214
100
100
12/21/15
15LO906-02 W-24131
B 138214
100
100
12/21/15
15LO906-03 W-8131
B 138214
100
100
12/21/15
I Page 24

Table of Contents
con-tesV'
ANALYTICAL LABORATORY
39 Spruce Street - East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Lxti-action Data
Prep Method: SW-846 3005A Dissolved-SW-846 6020A
Lab Number [Field ID1
Batch
Initial JmLj
Final ImLl
Date
15L0906-OIREI [MW-51
B 138641
50.0
50.0
12/28/15
15LO906-02REI [MW-24D]
B138641
50.0
50.0
12/28/15
15LO906-03REI [MW-8B]
B 138641
50.0
50.0
12/28/15
Prep Method: SW4146 3005A-SW-846 6020A
Lab Number [Field ED]
Batch
Initial jmLj
Final [mLj
Date
15LO906-OIREI [MW-51
B 138642
50.0
50.0
12/28/15
15LO906-02REI [MW-24D]
B 138642
50.0
50.0
12/28/15
15LO906-03REI [N4W-8B]
B 138642
50.0
50.0
12/28/15
Prep Method: SW-846 5030B-SW-846 8260B
Lab Number [Field ID1
Batch
Initial [mLj
Final [mLj
Date
15LO906-01 [MW-5]
B138109
5
5.00
12/20/15
15LO906-03 [MW-8B]
B138109
15
5.00
12/20/15
Prep Method: SW-846 503OB-SW-846 8260B
Lab Number [Field ID]
Batch
Initial [mLj
Final JmLj
Date
15LO906-02 [MW-24D]
B 138121
5
5.00
12/21/15
I Page 25

Table of Contents
con-skst'-�'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 0 1028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source */oREC RPD
Result Limit Units Level Result %REC Limits RPD Limit Not.
Batch B138109 - SW-846 5030B
Blank (B138109-BLKI)
Prepared & Analyzed: 12/20/15
Acetone
ND
0.050
-9/1-
Benzene
ND
0.0010
-9/L
Bromobenzene
ND
0.0010
-911-
Bromochloromethane
ND
0.0010
mg/L
Bromodichoromethane
ND
0.00050
mg/L
Bromoform
ND
0.0010
mg/L
Bromomethane
ND
0.0020
mg/L
2-Butanone (MEK)
ND
0.020
mg/L
n-Butylbenzene
ND
0.0010
mg/L
sec-Butylbenzene
ND
0.0010
mg/L
tcrt-Butylbenzene
ND
0.0010
mg/L
Carbon Disulfidc
ND
0.0040
mg/L
Carbon Tetrachloride
ND
0.0050
mg/1-
Chlorobenzene
ND
0.0010
mg/1-
Chlorodibromomethane
ND
0.00050
mg/L
ChlorGethanc
ND
0.0020
mg/L
Chloroform
ND
0.0020
mg/L
Chloromethane
ND
0.0020
mg/L
2-Chlorotolucne
ND
0.0010
mg/L
4-Chlorotolucne
ND
0.0010
mg/L
1,2-Dibromoethane (EDB)
ND
0.00050
mg/L
1,2-Dichlorobenzene
ND
0.0010
mg/L
1,3-Dicldorobcnzene
ND
0.0010
mg/L
1,4-Dichlorobenzene
ND
0.0010
mg/L
Dichlorodifluoromethane (Freon 12)
ND
0.0020
mg/L L-04
IJ-Dichloroethanc
ND
0.0010
mg/L
1,2-Dichloroethane
ND
0.0010
mg/L
IJ-Dichloroethylene
ND
0.0010
mg/L
cis- 1,2-Dichlorocthylenc
ND
0.0010
mg/L
ti-ans- 1,2-Dichloroethylene
ND
0.0010
Ing/L
1,2-Dichloropropanc
ND
0.0010
mg/L
1,3-Dichloropropane
ND
0.00050
mg/L
2,2-Dichloropropanc
ND
0.0010
mg/L
I,I-Dichloropropcne
ND
0.0020
mg/L
cis- 1,3-Dichloropropene
ND
0.00050
1119/L
trans-1,21-Dichloropropene
ND
0.00050
-9/L
Diisopropyll Ether (DIPE)
ND
0.00050
-9/1-
Ethylbcnzene
ND
0.0010
-9/1-
2-Hexanone (MBK)
ND
0.010
-9/1-
Isopropylbenzene (Cumene)
ND
0.0010
Ing/L
p4sopropyltoluene (p-Cymene)
ND
0.0010
-91L
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
m9/1-
Methylene Chloride
ND
0.0050
mg/L
4-Mcdiyl-2-pentanone (MIBK)
ND
0.010
mg/L
Naphthalene
ND
0.0020
mg/L
n-Propylbenzene
ND
0.0010
mg/L
Styrene
ND
0.0010
mg/L
1, 1,2,2-Tetrachloroethane
ND
0.00050
mg/L
Tetrachloroethylene
ND
0.00050
mg/L
Toluene
ND
0.0010
mg/L
1,2,3-Trichlorobenzene
ND
0.0050
mg/L
1,2,4-Trichlorobenzene
ND
0.0010
mg/L
I Page 26 of 46 1

Table of Contents
con-t(sto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
knalyte Result Limit units Level Result */oREC Limits RPD Limit Notes
Batch B138109 - SW-846 503013
Blank (B138109-BLKI)
Prepared & Analyzed: 12/20/15
1,1,1-Trichloroethane
ND
0.0010
mg/L
1,1,2-TricWoroethane
ND
0.0010
mg/L
Trichloroethylene
ND
0.0010
mg/L
TrieWorofluoromediane (Freon 11)
ND
0.0020
Ing/L
1,2,3-Trici-Joropropane
ND
0.0020
mg/L
1,2,4-Trimcthylbenzene
ND
0.0010
Ing/L
1,3,5-Trimediylbenzene
ND
0.0010
Ing/L
Vinyl Acetate
ND
0.020
Ing/L
Vinyl Chloride
ND
0.0020
Ing/L
m+p Xylene
ND
0.0020
-9/1-
o-Xylene
ND-
0.0010
mg/L
Surrogate: 1,2-Dichloroediane-d4
Surrogate: Toluene-d8 '
Surrogate: 4-Bromofluorobenzene
LCS (B1381WBSI)
0.0265
0.0250
0.0240
mg/L
mg/L
mg/L
0.0250 106
0.0250 99.9
0.0250 95.9
Prepared & Analyzed: 12/20/15
70-130
70-130
70-130
Acetone
0.0849
0.050
-9/1-
0.100
84.9
70-160
t
Benzene
0.0106
0.0010
-9/1-
0.0100
106
70-130
Bromobcnzenc
0.0101
0.0010
-9/1-
0.0100
101
70-130
Bromochloromctlianc
0.0121
0.0010
-9/1-
0.0100
121
70-130
Bromodichloromethane
0.00967
0.00050
-9/1-
0.0100
96.7
70-130
Bromoform
0.00891
0.0010
mg/L
0.0100
89.1
70-130
Brornornethane
0.00727
0.0020
mg/1-
0.0100
72.7
40-160
t
2-Butanone (MEK)
0.108
0.020
mg/L
0.100
108
40-160
t
n-Butylbenzene
0.00982
0.0010
mg/L
0.0100
98.2
70-130
sec-Butylbenzene
0.0103
0.0010
-9/1-
0.0100
103
70-130
tert-Butylbenzene
0.00971
0.0010
mg/L
0.0100
97.1
70-130
Carbon Disulfide
0.00946
0.0040
mg/L
0.0100
94.6
70-130
Carbon Tetrachloride
0.0102
0.0050
mg/L
0.0100
102
70-130
Chlorobenzene
0.00955
0.0010
-9/L
0.0100
95.5
70-130
Chlorodibromomediane
0.00937
0.00050
mg/L
0.0100
93.7
70-130
Chloroethane
0.0104
0.0020
mg/L
0.0100
104
70-130
Chloroform
0.0105
0.0020
mg/L
0.0100
105
70-130
Chloromethane
0.00829
0.0020
mg/L
0.0100
82.9
40-160
2-Chlorotoluene
0.00960
0.0010
mg/L
0.0100
%.0
70-130
4-Chlorotoluene
0.00988
0.0010
mg/L
0.0100
98.8
70-130
1,2-Dibromoedme (EDB)
0.0105
0.00050
mg/L
0.0100
105
70-130
1,2-Dichlorobenzene
0.00939
0.0010
mg/L
0.0100
93.9
70-130
1,3-Dicldorobenzene
0.00967
0.0010
mg/1-
0.0100
96.7
70-130
1,4-Dichlorobenzene
0.00905
0.0010
mg/L
0.0100
90.5
70-130
Dichlorodifluoromethane (Freon 12)
0.00372
0.0020
mg/L
0.0100
37.2
40-160
L-04
1,11-Dichloroethane,
0.0109
0.0010
mg/L
0.0100
109
70-130
1,2-Dichlorocthane
0.00989
0.0010
mg/L
0.0100
98.9
70-130
I,I-Dichloroethylene
0.0101
0.0010
mg/L
0.0100
101
70-130
cis� 1,2-Dichloroethylene
0.0107
0.0010
-9/1-
0.0100
107
70-130
trans- 1,2-Dichloroethylene
0.0102
0.0010
mg/L
0.0100
102
70-130
1,2-Dichloropropane
0.0102
0.0010
mg/L
0.0100
102
70-130
1,3-Dichloropropane
0.0102
0.00050
mg/L
0.0100
102
70-130
2,2-Dichloropropane
0.00872
0.0010
mg/L
0.0100
87.2
40-130
1,11-Dichloropropene
0.0104
0.0020
mg/L
0.0100
104
70-130
cis, 1,3-Dichloropropene
0.00893
0.00050
mg/L
0.0100
89.3
70-130
trara-1,3-Dichloropropene
0.00949
0.00050
mg/L
0.0100
94.9
70-130
I Page 27 of

Table of Contents
con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
nalyte Result Limit units Level Result O/oREC Limits RPD Limit Notes
Batch B138109 - SW-846 5030B
LCS (B138109LBSI) Prepared & Analyzed: 12/20/15
Diisopropyl Ether (DIPE)
0.00999
0.00050
mg/L
0.0100
99.9
70-130
Ethylbenzene
0.00995
0.0010
mg/L
0.0100
99.5
70-130
2-Hexanone (MBK)
0.104
0.010
Ing/L
0.100
104
70-160
lsopropylbcnzene (Cumene)
0.00978
0.0010
Ing/L
0.0100
97.8
70-130
p4sopropyltoluene (p-Cymene)
0.0107
0.0010
rug/L
0.0100
107
70-130
Methyl tert-Butyl Ether (MTBE)
0.00998
0.0010
mg/L
0.0100
99.8
70-130
Methylene Chloride
0.0102
0.0050
mg/L
0.0100
102
70-130
4-Methyl-2-pentanone (MlBK)
0.107
0.010
mg/L
0.100
107
70-160
Naphthalene
0.00912
0.0020
mg/L
0.0100
91.2
40-130
n-Propylbenzene
0.00993
0.0010
mg/L
0.0100
99.3
70-130
Styrene
0.00990
0.0010
mg/L
0.0100
99.0
70-130
1, 1,2,2-Tctrachloroethane
0.0107
0.00050
Ing/L
0.0100
107
70-130
Tetrachloroediylene
0.00966
0.00050
mg/L
0.0100
96.6
70-130
Toluene
0.00998
0.0010
mg/L
0.10100
99.8
70-130
1,2,3-Tricblorobenzene
0.00879
0.0050
mg/L
0.0100
87.9
70-130
1,2,4-Trichlorobenzene
0.00953
0.0010
mg/L
0.0100
95.3
70-130
1, 1, 1 -Trichloroethane
0.0102
0.0010
mg/L
0.0100
102
70-130
1, 1,2-Trichloroethane
0.0101
0.0010
mg/L
0.0100
101
70-130
Trichloroethylene
0.0103
0.0010
Ing/L
0.0100
103
70-130
:�ehloroflnorornethanc (Freon LQ-�-
0.0086-9,
0.0020
Ing/L
0.0100
86.9
70-130
0.0020
mg/L
0.0100
106
70-130
r,2-,4-Trimethylbenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
1,3,5-Trimethylbenzene
0.0103
0.0010
mg/L
0,0100
103
70-130
Vinyl Acetate
0.0922
0.020
mg/L
0.100
92.2
70-130
Vinyl Chloride
0.00729
0.0020
mg/L
0.0100
72.9
40-160
m+p Xylene
0.0198
0.0020
mg/L
0.0200
99.2
70-130
o-Xylene
0.00981
0.0010
mg/L
0.0100
98.1
70-130
Surrogate: 1,2-Dichloroethane-d4
0.0270
Ing/L
0.0250
108
70-130
Surrogate: Toluene-d8
0.0248
mg/L
0.0250
99.0
70-130
Surrogate: 4-Bromofluorobcnzenc
0.0246
mg/L
0.0250
98.2
70-130
LCS Dup (B138109-BSDI)
Prepared & Analyzed: 12/20/15
Acetone
0.0845
0.050
mg/L
0.100
84.5
70-160
0.555
Benzene
0.0102
0.0010
mg/L
0.0100
102
70-130
4.14
Bromobenzene
0.00982
0.0010
mg/L
0.0100
98.2
70-130
2.91
Bromochloromethane
0.0126
0.0010
mg/L
0.0100
126
70-130
3.80
Bromodichloromedme
0.00980
0.00050
mg/L
0.0100
98.0
70-130
1.34
Bromoform
0.00869
0.0010
mg/L
0.0100
86.9
70-130
2.50
Bromomethane
0.00721
0.0020
mg/L
0.0100
72.1
40-160
0.829
2-Butanone (MEK)
0.109
0.020
mg/L
0.100
109
40-160
0.926
n-Butylbcnzene
0.00951
0.0010
mg/L
0.0100
95.1
70-130
3.21
sec-Butylbenzene
0.00975
0.0010
mg/L
0.0100
97.5
70-130
5.78
tert-Butylbenzene
0.00940
0.0010
Ing/L
0.0100
94.0
70-130
3.24
Carbon Disulfide
0.00892
0.0040
mg/L
0.0100
89.2
70-130
5.88
Carbon Tetrachloride
0.0100
0.0050
mg/L
0.0100
100
70-130
2.17
Chlorobenzene
0.00912
0.0010
-9/1-
0.0100
91.2
70-130
4.61
Chlorodibromomethane
0.00923
0.00050
mg/L
0.0100
92.3
70-130
1.51
Chloroethane
0.0103
0.0020
mg/L
0.0100
103
70-130
0.867
Chloroform
0.0102
0.0020
mg/L
0.0100
102
70-130
3.77
Chloromethane
0.00830
0.0020
mg/L
0.0100
83.0
40-160
0.121
2-Chlorotoluene
0.00952
0.0010
mg/L
0.0100
95.2
70-130
0.937
4-Chlorotoluene
0.00943
0.0010
mg/L
0.0100
94.3
70-130
4.66
t
t
25 t
25
25
25
25
25
25 t
25 t
25
25
25
25
25
25
25
25
25
25
25
25
1 Page 28 of �46

Table of Contents
con -kW
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MAO 1028 *FAX [phone] *TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reportmg Spike Source 0/oREC RPD
Result Limit Units Level Result O/oREC Limits RPD Limit Notes
Batch B138109 - SW-846 5030B
LCS Dup (B138109-BSDI)
hepared & Analyzed: 12/20/15
1,2-Dibromoedme (EDB)
0.0103
0.00050
-9/L
0.0100
103
70-130
2.50
25
1,2-Dichlorobenzene
0.00930
0.0010
mg/L
0.0100
93.0
70-130
0.963
25
1,3-Dichlorobenzene
0.00953
0.0010
-9/1-
0.0100
95.3
70-130
1.46
25
1,4-Diclilorobcnzene
0.00913
0.0010
mg/L
0.0100
91.3
70-130
0.880
25
Dichlorodifluoromethane (Freon 12)
0.00375
0.0020
mg/L
0.0100
37.5
40-160
0.803
25
L-04 t
1, 1 -Dichloroethane
0.0105
0.0010
Ing/L
0.0100
105
70-130
3.83
25
1,2-Dichloroctliane
0.00970
0.0010
mg/L
0.0100
97.0
70-130
1.94
25
1, 1 -Dichloroethylene
0.00960
0.0010
mg/L
0.0100
Wo
70-130
4.68
25
cis- 1,2-Dichloroethylcne
0.0102
0.0010
mg/1-
0.0100
102
70-130
4.20
25
b-ans-1,2-Dichloroediylene
0.00976
0.0010
-9/1-
0.0100
97.6
70-130
4.41
25
1,2-DicWoropropane
0.0103
0.0010
mg/L
0.0100
103
70-130
0.585
25
1,3-Dichloropropane
0.00999
0.00050
mg/L
0.0100
99.9
70-130
2.37
25
2,2-Dicliloropropanc
0.00819
0.0010
mg/L
0.0100
81.9
40-130
6.27
25
t
1, 1 -Dichloropropene
0.00990
0.0020
mg/L
0.0100
99.0
70-130
5.21
25
cis- 1,3-Dichloropropene
0.00879
0.00050
mg/L
0.0100
87.9
70-130
1.58
25
trazu, 1,3-Dichloropropene
0.00962
0.00050
mg/L
0.0100
%.2
70-130
1.36
25
Diisopropyl Ether (DIPE)
0.00995
0.00050
mg/L
0.0100
99.5
70-130
0.401
25
Ethylbenzene
0.00976
0.0010
Ing/L
0.0100
97.6
70-130
1.93
25
2-Hcxanone (MBK)
0.105
0.010
mg/1-
0.100
105
70-160
1.40
25
t
lsopropylbenzene (Cumene)
0.00941
0.0010
mg/L
0.0100
94.1
70-130
3.86
25
p-lsopropyltoluene (p-Cymene)
0.0103
0.0010
mg/L
0.0100
103
70-130
3.81
25
Methyl tert-Butyl Ether (MTBE)
0.00981
0.0010
mg/L
0.0100
98.1
70-130
1.72
25
Methylene Chloride
0.0102
0.0050
mg/L
0.0100
102
70-130
0.980
25
4-Mediyl-2-pentanone (MlBK)
0.110
0.010
mg/L
0.100
110
70-160
2.62
25
t
Naphthalene
0.00927
0.0020
mg/L
0.0100
92.7
40-130
1.63
25
t
n-Propylbenzcne
0.00939
0.0010
mg/L
0.0100
93.9
70-130
5.59
25
Styrene
0.00%2
0.0010
mg/L
0.0100
96.2
70-130
2.87
25
1, 1,2,2-Tetrachloroethanc
0.0108
0.00050
mg/L
0.0100
108
70-130
0.841
25
Tetrachloroethylene
0.00915
0.00050
mg/L
0.0100
91.5
70-130
5.42
25
Toluene
0.00970
0.0010
mg/L
0.0100
97.0
70-130
2.85
25
1,2,3-Trichlorobenzene
0.00906
0.0050
Ing/L
0.0100
90.6
70-130
3.03
25
1,2,4-Trichlorobenzenc
0.00940
0.0010
Ing/L
0.0100
94.0
70-130
1.37
25
1,1,1-TricWoroethane
0.00966
0.0010
Ing/L
0.0100
%.6
70-130
5.24
25
1,1,2-Trichloroediane
0.0102
0.0010
mg/L
0.0100
102
70-130
0.0986
25
Trichloroethylene
0.00997
0.0010
mg/L
0.0100
99.7
70-130
3.06
25
Trichlorofluoromediane (Freon 11)
0.00842
0.0020
mg/L
0.0100
94.2
70-130
3.16
25
1,2,3-Trichloropropane
0.0108
0.0020
mg/1-
0.0100
108
70-130
1.78
25
1,2,4-Trimethylbenzene
0.00994
0.0010
mg/L
0.0100
98.4
70-130
2.51
25
1,3,5-Trimethylbenzene
0.00998
0.0010
mg/L
0.0100
99.8
70-130
3.16
25
Vinyl Acetate
0.0926
0.020
mg/L
0.100
92.6
70-130
0.335
25
Vinyl Chloride
0.00689
0.0020
mg/L
0.0100
68.9
40-160
5.64
25
m+p Xylene
0.0191
0.0020
mg/L
0.0200
95.4
70-130
3.91
25
o-Xylene
0.00956
0.0010
mg/L
0.0100
95.6
70-130
2.58
25
Surrogate: 1,2-Dichloroethane-d4
0.0265
mg/L
0.0250
106
70-130
Surrogate: Tolucne-d8
0.0250
mg/L
0.0250
100
70-130
Surrogate: 4-Bromofluorobenzene
0.0242
mg/1-
0.0250
%.6
70-130
I Page 29 of �46

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALM CONTROL
Volatile Organic Compounds by GUMS - Quality Control
Reportmg Spike Source O/oREC RPD
Analyte Result Limit Units Level Result O/oREC Limits RPD Limit Notes
Batch B138121 - SW-846 5030B
Blank (111138121-BLIKI) Prepared & Analyzed: 12/21/15
Acetone
ND
0.050
mg/L
Benzene
ND
0.0010
mg/L
Bromobenzene
ND
0.0010
mg/L
Bromochloromethane
ND
0.0010
m9/1-
Bromodicl-doromethane
ND
0.00050
Ing/L
Bromoform
ND
0.0010
mg/L-
Bromomethane
ND
0.0020
Ing/L
2-Butanone (MEK)
ND
0.020
mg/L
n-Butylbenzene
ND
0.0010
mg/L
sec-Butylbcnzene
ND
0.0010
mg/L
tert-Butylbenzene
ND
0.0010
mg/L
Carbon Disulfide
ND
0.0040
mg/L
Carbon Tetrachloride
ND
0.0050
mg/L
Chlorobenzene
ND
0.0010
019/1,
Chlorodibromomediane
ND
0.00050
Ing/L
Chloroethane
ND
0.0020
mg/1-
Chloroform
ND
0.0020
m9/1-
Chlorometharle
ND
0.0020
mg/L
2-Chlorotoluene
ND
0.0010
-19/1-
4-Chlorotoluene
ND
0.0010
mg/1-
1,2-Dibromoethane (EDB)
ND
0.00050
mg/L
1,2-DieMorobcnzene
ND
0.0010
-19/L
1,3-Dichlorobenzcne
ND
0.0010
mg/L
1,4-Dichlorobenzcne
ND
0.0010
-9/1-
Dichlorodifluoromethane (Freon 12)
ND
0.0020
m9/1-
IJ-Dichloroethane
ND
0.0010
mg/L
1,2-Dicliloroctliane
ND
0.0010
mg/L
1,1-Dichloroethylene
ND
0.0010
Ing/L
cis- 1,2-Dichloroethylene
ND
0.0010
mg/L
trans- 1,2-Dichloroethylene
ND
0.0010
-9/1-
1,2-Dichloropropane
ND
0.0010
Ing/L
1,3-Dichloropropane
ND
0.00050
-9/1-
2,2-Dichloropropane
ND
0.0010
mg/1-
IJ-Dichloropropene
ND
0.0020
Ing/L
cis- 1,3-Dichlaropropene
ND
0.00050
m9/1-
trans- 1,3-Dichloropropene
ND
0.00050
-9/1-
Diisopropyl Ether (DIPE)
ND
0.00050
-9/1-
Ethylbenzenc
ND
0.0010
mg/L
2-Hexanone (MBK)
ND
0.010
mg/1-
Isopropylbenzene (Cumene)
ND
0.0010
-9/1-
p4sopropyltoluene (p-Cymene)
ND
0.0010
-9/1-
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
-9/1-
Methylene Chloride
ND
0.0050
-9/1-
4-Methyl-2-pentanone (MIBK)
ND
0.010
-9/1-
Naphthalene
ND
0.0020
-9/1-
a-Propylbenzene
ND
0.0010
m9/1-
Styrene
ND
0.0010
mg/L
1, 1,2,2-Tetrachloroethane
ND
0.00050
mg/1-
Tetrachloroethylene
ND
0.00050
m9/1-
Toluene
ND
0.0010
mg/L
1,2,3-Trichlorobenzene
ND
0.0050
m9/1-
1,2,4-Trichlorobenzene
ND
0.0010
mg/1-
V-0�
V-0�
Page 30 of 46

0 con-tcst'�'
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Report-g Spike Source I/oREC RPD
Analyte Result Limit Units Level Result 0/oREC Limits RPD Limit Notes
Batch B138121 - SW-846 5030B
Blank (11138121-BLKI)
Prepared & Analyzed: 12/21/15
1, 1, 1 -Trichloroethane
ND
0.0010
mg/L
1, 1,2-Trichloroethane
ND
0.0010
D19/1-
Trichloroethylene
ND
0.0010
mg/L
Trichlorofluoromethane (Freon 11)
ND
0.0020
mg/1-
1,2,3-Txichloropropane
ND
0.0020
Ing/L
1,2,4-Trimethylbenzene
ND
0.0010
mg/L
1,3,5-Trimediylbenzene
ND
0.0010
mg/L
Vinyl Acetate
ND
0.020
mg/1-
Vinyl Chloride
ND
0.0020
D19/1-
m+p Xylcne
ND
0.0020
mg/L
o-Xylene
ND
0.0010
mg/L
Surrogate: 1,2-Dichloroethane-d4
0.0259
mg/L
0.0250 103 70-130
Surrogate: Toluene-d8
0.0253
mg/L
0.0250 101 70-130
Surrogate: 4-Bromofluorobenzene
0.0243
mg/L
0.0250 97.2 70-130
LCS (B138121-BSI)
Prepared & Analyzed: 12/21/15
Acetone
0.0836
0.050
mg/L
0.100
83.6
70-160
Benzene
0.0108
0.0010
mg/L
0.0100
108
70-130
Bromobenzene
0.0104
0.0010
mg/L
0.0100
104
70-130
Bromochloromethanc
0.0126
0.0010
mg/L
0.0100
126
70-130
Bromodichloromethane
0.0101
0.00050
-9/1-
0.0100
101
70-130
Bromoform
0.00893
0.0010
Ing/L
0.0100
89.3
70-130
Bromomethane
0.00761
0.0020
Ing/L
0.0100
76.1
40-160
2-Butanone (MEK)
0.104
0.020
Ing/L
0.100
104
40-160
n-Butylbenzene
0.0107
0.0010
mg/L
0.0100
107
70-130
sec-Butylbenzene
0.0106
0.0010
mg/L
0.0100
106
70-130
tert-Butylbenzene
0.0101
0.0010
-9/L
0.0100
101
70-130
Carbon Disulfide
0.0105
0.0040
-9/1-
0.0100
105
70-130
Carbon Tetrachloride
0.0107
0.0050
Ing/L
0.0100
107
70-130
Chlorobenzene
0.00973
0.0010
Ing/L
0.0100
97.3
70-130
Chlorodibromomethane
0.00952
0.00050
Ing/L
0.0100
95.2
70-130
Chloroethane
0.0115
0.0020
mg/L
0.0100
115
70-130
Chloroform
0.0107
0.0020
mg/L
0.0100
107
70-130
Chloromethane
0.00900
0.0020
mg/L
0.0100
90.0
40-160
2-Chlorotoluene
0.0103
0.0010
mg/L
0.0100
103
70-130
4-Chlorotoluene
0.0104
0.0010
mg/L
0.0100
104
70-130
1,2-Dibromoedme (EDB)
0.0108
0.00050
mg/L
0.0100
108
70-130
1,2-Dichlorobenzene
0.00955
0.0010
Ing/L
0.0100
95.5
70-130
1,3-Dichlorobenzene
0.00998
0.0010
-9/1-
0.0100
99.8
70-130
1,4-Dichlorobenzene
0.00992
0.0010
mg/L
0.0100
99.2
70-130
Dichlorodifluoromethanc (Freon 12)
0.00558
0.0020
mg/L
0.0100
55.8
40-160
I,I-Dichloroetliane
0.0114
0.0010
mg/L
0.0100
114
70-130
1,2-Dichlorocthane
0.0106
0.0010
mg/L
0.0100
106
70-130
I,I-Dichloroethylene
0.0106
0.0010
mg/L
0.0100
106
70-130
cis- 1,2-Dichloroethylene
0.0108
0.0010
mg/L
0.0100
108
70-130
trans- 1,2-Dichloroethylent
0.0106
0.0010
Ing/L
0.0100
106
70-130
1,2-Dichloropropane
0.0108
0.0010
Ing/L
0.0100
108
70-130
1,3-Dichloropropane
0.0104
0.00050
-9/1-
0.0100
104
70-130
2,2-Dichloropropane
0.0109
0.0010
Ing/L
0.0100
109
40-130
IJ-Dichloropropene
0.0107
0.0020
Ing/L
0.0100
107
70-130
cis- 1,3-Dichloropropenc
0.00979
0.00050
-9/1-
0.0100
97.9
70-130
ums-1,3-Dichloropropene
0.0108
0.00050
mg/L
0.0100
108
70-130
V-20
T
t
t
t
I Page 31 of 46

Table of Contents
0 con-NsV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source */oREC Rill)
knalyte Result Limit Units Level Result 1/*REC Limits RPD Limit Notes
Batch B138121 - SW-846 5030B
LCS (BI38121-BS1)
Prepared & Analyzed: IMI115
Diisopropyl Ether (DIPE)
0.0102
0.00050
mg/L
0.0100
102
70-130
Ethylbenzene
0.0102
0.0010
mg/L
0.0100
102
70-130
2-Hcxanone (MBK)
0.103
0.010
mg/L
0.100
103
70-160
Isopropylbenzene (Cumene)
0.0102
0.0010
mg/L
0.0100
102
70-130
p-Isopropyholuene q�Cymene)
0.0112
0.0010
mg/L
0.0100
112
70-130
Methyl tert-Butyl Ether (MTBE)
0.0103
0.0010
mg/L
0.0100
103
70-130
Methylene Chloride
0.0106
0.0050
mg/L
0.0100
106
70-130
4-Methyl-2-pentanone (MIBK)
0.109
0.010
mg/L
0.100
109
70-160
t
Naphthalene
0.00872
0.0020
mg/L
0.0100
87.2
40-130
V-05 t
n-Propylbenzene
0.0104
0.0010
-9/1-
0.0100
104
70-130
Styrene
0.0104
0.0010
mg/L
0.0100
104
70-130
1, 1,2,2-Tetrachloroethane
0.0109
0.00050
mg/L
0.0100
109
70-130
Tetrachloroethylene
0.0103
0.00050
-9/1-
0.0100
103
70-130
Toluene
0.0106
0.0010
mg/L
0.0100
106
70-130
1,2,3-Trichlorobenzene
0.00899
0.0050
mg/L
0.0100
89.9
70-130
V-05
1,2,4-Trichlorobenzene
0.00939
0.0010
mg/L
0.0100
93.9
70-130
1, 1, 1 -Trichloroethane
0.0103
0.0010
mg/L
0.0100
103
70-130
1, 1,2-Trichloroethane
0.0104
0.0010
mg/L
0.0100
104
70-130
Trichloroethylene
0.0107
0.0010
mg/L
0.0100
107
70-130
Trichlorofluoromethane (Freon 11)
0.00952
0.0020
mg/L
0.0100
95.2
70-130
1,2,3-Trichloropropane
0.0109
0.0020
-9/1-
0.0100
109
70-130
1,2,4-Trimediylbcnzene
0.0106
0.0010
-19/1-
0.0100
106
70-130
1,3,5-Trimethylbenzene
0.0108
0.0010
Ing/L
0.0100
108
70-130
Vinyl Acetate
0.0989
0.020
-19/1-
0.100
98.9
70-130
Vinyl Chloride
0.00816
0.0020
mg/L
0.0100
81.6
40-160
m+p Xylene
0.0207
0.0020
mg/L
0.0200
104
70-130
o­Xylene
0.0104
0.0010
-9/1-
0.0100
104
70-130
Surrogate: 1,2-Dichloroethane-d4
0.0264 Ing/L
0.0250 106 70-130
Surrogate: Toluene-d8
0.0252 mg/L
0.0250 101 70-130
Surrogate: 4-Bromofluorobeftzene
0.0250 -19/1-
0.0250 99.9 70-130
LCS Dup (B138121-BSDI)
Prepared & Analyzed: 12/21/15
Acetone
0.0838
0.050
mg/L
0.100
83.8
70-160
0.263
Benzene
0.0106
0.0010
-9/L
0.0100
106
70-130
2.71
Bromoben�ene
0.0103
0.0010
mg/L
0.0100
103
70-130
1.26
BromocWorometliane
0.0126
0.0010
1119/1-
0.0100
126
70-130
0.635
Bromodichloromethane
0.00938
0.00050
mg/1-
0.0100
93.8
70-130
7.79
Bromoform
0.00851
0.0010
mg/1-
0.0100
85.1
70-130
4.82
Bromomethane
0.00795
0.0020
mg/L
0.0100
79.5
40-160
4.37
2-Butanone (MEK)
0.104
0.020
1-9/1-
0.100
104
40-160
0.106
n-Butylbenzene
0.00997
0.0010
mg/L
0.0100
99.7
70-130
6.97
see-Butylbenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
4.82
tert-Butylbenzene,
0.00963
0.0010
mg/L
0.0100
96.3
70-130
4.76
Carbon Disulfide
0.00996
0.0040
Ing/L
0.0100
99.6
70-130
4.90
Carbon Tetrachloride
0.0104
0.0050
mg/L
0.0100
104
70-130
2.37
Chlorobenzene
0.00957
0.0010
Ing/L
0.0100
95.7
70-130
1.66
Chlorodibromomethane
0.00922
0.00050
-9/1-
0.0100
92.2
70-130
3.20
Chloroethane
0.0111
0.0020
mg/L
0.0100
111
70-130
3.19
Chloroform
0.0106
0.0020
Ing/L
0.0100
106
70-130
1.41
Chloromethane
0.00904
0.0020
mg/L
0.0100
90.4
40-160
0.443
2-Chlorotoluene,
0.00959
0.0010
mg/L
0.0100
95.9
70-130
6.75
4-Chlorotoluene
0.00993
0.0010
mg/L
0.0100
99.3
70-130
4.33
25
25
25
25
25
25
25 V-20 t
25 t
25
25
25
25
25
25
25
25
25
25
25
25
1 Page 32

Table of Contents
con-tcsV
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source O/oREC RPD
Analyte Result Limit Units Level Result */oREC Limits RPD Limit Notes
Batch B138121 - SW-S46 5030B
LCS Dup (B138121-BSD1)
Prepared & Analyzed: 12/21/15
1,2-Dibromoethane (EDB)
0.0103
0.00050
-9/1,
0.0100
103
70-130
4.91
25
1,2-Dichlorobenzene
0.00920
0.0010
-9/1-
0.0100
92.0
70-130
3.73
25
1,3-Dichlorobenzene
0.00971
0.0010
mg/1-
0.0100
97.1
70-130
2.74
25
1,4-Dichlorobenzcne
0.00961
0.0010
11191L
0.0100
96.1
70-130
3.17
25
Dichlorodifluoromethane (Freon 12)
0.00550
0.0020
-9/1-
0.0100
55.0
40-160
1.44
25
I,I-Dichloroethane
0.0112
0.0010
-9/1-
0.0100
112
70-130
1.24
25
1,2-Dichloroethane
0.00985
0.0010
Ing/L
0.0100
98.5
70-130
6.96
25
I,I-Dichloroediylene
0.0101
0.0010
mg/L
0.0100
101
70-130
5.20
25
cis- 1,2-Dichloroethylene
0.0104
0.0010
mg/L
0.0100
104
70-130
3.86
25
trans- 1,2-Dichloroethylene
0.0104
0.0010
mg/L
0.0100
104
70-130
2.01
25
1,2-Dichloropropane
0.0104
0.0010
mg/L
0.0100
104
70-130
3.97
25
1,3-Dichloropropane
0.0102
0.00050
mg/L
0.0100
102
70-130
1.93
25
2,2-Dichloropropanc
0.0103
0.0010
mg/L
0�0100
103
40-130
5.36
25
IJ-Dichloropropenc
0.0107
0.0020
mg/L
0.0100
107
70-130
0.187
25
cis- 1,3-Dichloropropene
0.00927
0.00050
mg/L
0.0100
92.7
70-130
5.46
25
U'ans-1,3-Dichloropropene
0.00997
0.00050
mg/L
0.0100
99.7
70-130
8.36
25
Diisopropyl Ether (DIPE)
0.0102
0.00050
mg/L
0.0100
102
70-130
0.587
25
Ethylbenzene
0.00997
0.0010
mg/L
0.0100
99.7
70-130
2.48
25
2-Hexanone (MBK)
0.0998
0.010
-19/1-
0.100
99.8
70-160
3.00
25
Isopropylbenzene (Cumene)
0.00983
0.0010
-9/1,
0.0100
98.3
70-130
3.40
25
p-lsopropyltoluene (p-Cymcne)
0.0106
0.0010
-9/1,
0.0100
106
70-130
5.61
25
Methyl tort -Butyl Ether (MTBE)
0.00999
0.0010
-9/1-
0.0100
99.9
70-130
3.15
25
Methylene Chloride
0.0106
0.0050
-9/1-
0.0100
106
70-130
0.755
25
4-methyl-2-pentanone (MIBK)
0.106
0.010
-9/1-
0.100
106
70-160
2.54
25
Naphthalene
0.00859
0.0020
-19/1-
0.0100
85.9
40-130
1.50
25
V-05
n-Propylbenzene
0.0101
0.0010
-9/1-
0.0100
101
70-130
3.11
25
Styrene
0.00988
0.0010
-9/1-
0.0100
98.8
70-130
4.74
25
1, 1,2,2-Tetrachloroethane
0.0105
0.00050
-9/1-
0.0100
105
70-130
3.65
25
Tetrachloroethylene
0.00978
0.00050
mg/L
0.0100
97.8
70-130
5.08
25
Toluene
0.0102
0.0010
mg/L
0.0100
102
70-130
3.65
25
1,2,3-Trichlorobenzene
0.00997
0.0050
mg/L
0.0100
89.7
70-130
0.223
25
V-05
1,2,4-Trichlorobenzene
0.00922
0.0010
mg/L
0.0100
92.2
70-130
1.83
25
1,1,1-Trichloroethane
0.0101
0.0010
-9/1-
0.0100
101
70-130
1.18
25
1, 1,2-Trichloroediane
0.0102
0.0010
mg/L
0.0100
102
70-130
2.42
25
Trichloroethylene
0.00998
0.0010
-9/1-
0.0100
99.8
70-130
6.59
25
Trichlorofluoromethane (Freon 11)
0.00915
0.0020
mg/L
0.0100
91.5
70-130
3.96
25
1,2,3-Trichloropropane
0.0109
0.0020
Ing/L
0.0100
109
70-130
0.00
25
1,2,4-Trimethylbenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
5.02
25
1,3,5-Trimethylbenzene
0.0101
0.0010
1119/1-
0.0100
101
70-130
6.03
25
Vinyl Acetate
0.0963
0.020
mg/L
0.100
96.3
70-130
2.61
25
Vinyl Chloride
0.00792
0.0020
mg/L
0.0100
79.2
40-160
2.99
25
m+p Xylene
0.0202
0.0020
-9/1-
0.0200
101
70-130
2.69
25
o-Xylcnc
0.00994
0.0010
mg/1-
0.0100
98.4
70-130
5.24
25
Surrogate: 1,2-Dichloroethant-d4
0.0269
mg/1-
0.0250
107
70-130
Surrogate: Toluene-d8
0.0249
mg/L
0.0250
99.4
70-130
Surrogate: 4-Bromofluorobenzene
0.0244
-9/1.
0.0250
97.8
70-130
I Page 33

Table of Contents
con-UW
ANALYTICAL LABOPATORY
Batch B138318 - 3810-RSK175
Blank (B138318-BLKI)
Ethane
Ethene
Methane
LCS (B138318-BSI)
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
QUALITY CONTROL
Miscellaneous Organic Analyses - Quality Control
Reporung Spike Source 0/6REC RPD
Result Limit Units Level Result O/oREC Limits RPD Limit Notes
Prepared & Analyzed: 12/22/15
ND 0.0028 E-9/1-
ND 0.0038 -9/1-
ND 0.0026 mg/L
Prepared & Analyzed: 12/22/15
Ethane 2100
Ethene 2000
Methane 1900
mg/L 2000 104 60-122
mg/L 2000 98.6 67-113
mg/L 2000 96.3 56-121
I Page 34

6 con-tcstRo
ANALYTICAL LABORATORY
1138299 - SW-846 3005A
Blank (Bl38299-BLKI)
Manganese
LCS (B138299-USI)
39 Spruce Street* East Longmeadow, MA01028* FAX [phone]* TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Table of Contents
Reportuig Spike Source O/oREC RPD
Result Limit Units Level Result 0/6REC Limits RPD Limit Notes
Prepared: 12/22/15 Analyzed: 12/23/15
ND 2.0 Pg/L
Prepared: 12/22/15 Analyzed: 12/23/15
Manganese 242 5.0 Ig/l- 250 96.8 80-120
LCS Dup (B138299-BSDI) Prepared: 12/22/15 Analyzed: 12/23/15
Manganese 243 5.0 Pg/L 250 97.1 80-120 0.327 20
Batch B138642 - SW-846 3005A
Blank (B138642-BLKI) Prepared: 12/28/15 Analyzed: 12/29/15
Manganese ND 2.0 IL911-
LCS (B138642-BS1) Prepared: 12/28/15 Analyzed: 12/29/15
Manganese 229 5.0 Itg/L 250 91.6 80-120
LCS Dup (B138642-BSDI) Prepared: 12/28/15 Analyzed: 12/29/15
Manganese 230 5.0 Fg/L 250 91.9 80-120 0.310 20
I Page 35 of 46 1

Table of Contents
con-tcsto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALFFY CONTROL
Metals Analyses (Dissolved) - Quality Control
Reporting Spike Source O/oREC RPD
Result Limit Units Level Result '/JZEC Limits RPD Limit Notes
Batch B137936 - SW-846 3005A Dissolved
Blank (B137936-BLKI)
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
LCS (B137936-BS1)
ND
2.0
Vg/L
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
LCS Dup (0137936-BSD1)
255
5.0
Rg/1-
250 102 80-120
Prepared: 12/17/15 Analyzed: 12/20/15
Manganese
Batch B138641 - SW-846 3005A Dissolved
262
5.0
Pg/L
250 105 80-120 2.75 20
Blank (B138641-BLKI)
Prepared: 12/28/15 Analyzed: 12/29/15
Manganese
LCS (BI39641-BSI)
ND
2.0
Itg/L
Prepared: 12/28/15 Analyzed: 12/29/15
Manganese
LCS Dup (B138641-BSDI)
213
5.0
Itg/1-
250 85.4 80-120
Prepared: 12/28/15 Analyzed: 12/29/15
Manganese
232
5.0
Pg/L
250 93.0 80-120 8.57 20
I Page 3

Table of Contents
con-UsV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APRA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit units Level Result %REC Limits RPD Limit Notes
Batch B138048 - SM 21-22 4500 NO2 B
Blank (B138048-BIKI)
Prepared & Analyzed: 12/18/15
Nitrite as N
LCS (B138048-BSI)
ND
0.010
mg/L
Prepared & Analyzed: 12/18/15
Nitrite as N
LCS Dup (11138048-BSDI)
0.10
0.010
Ing/L
0.100 101
Prepared & Analyzed: 12/18/15
90-111
Nitrite as N
Duplicate (11138048-DUPI)
0.10 0.010
Source: 15LO906-01
mg/L
0.100 102
Prepared & Analyzed: 12/18/15
90-111 0.359 5.9
Nitrite as N
Matrix Spike (B138048-MSI)
0.0062 0.010
Source: 151A906-01
-9/1-
0.0058
Prepared & Analyzed: 12/18/15
6.05 23
Nitrite as N
Batch B138214 - SM21-22 450OS-F
0.089
0.010
-9/1-
0.100 0.0058 82.8
71.7-116
Blank (B138214-BLKI)
Prepared & Analyzed: 12/21/15
Sulfide
LCS (B138214-BSI)
ND
2.0
-9/1-
Prepared & Analyzed: 12/21/15
Sulfide
Batch 11138250 - SM19-22 4500 NH3 C
15
2.0
-9/1-
14.8 100
60.3-119
Blank (B138250-BLKI)
Prepared: 12/22/15 Analyzed: 12/23/15
Ammonia as N
LCS(B138250-BSI)
ND
0.30
mg/L
Prepared: 12/22/15 Analyzed: 12123/15
Ammonia as N
LCS Dup (B139250-BSDI)
4.8
0.30
mg/L
5.00 95.2
Prepared: 12/22/15 Analyzed: 12/23/15
82-106
Ammoma as N
Batch B138306 - ASTM D516-07
4.6
0.30
-9/1-
5.00 92.4
82-106 2.99 9.24
Blank (B138306-BLKI)
Prepared & Analyzed: 12/22/15
Sulfate
LCS (B139306-BSI)
ND
2.0
mg/L
Prepared & Analyzed: 12/22/15
Sulfate
21
2.0
mg/L
20.0 104
83.9-123
I Page 3

Table of Contents
0 con -toot"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source 0/oREC RPD
Result Limit units Level Result %REC Limits RPD Limit Notes
Batch B138306 - ASTM D516-07
LCS Dup (111138306-BSDI)
Prepared & Analyzed: 12/22/15
Sulfate
Batch B138312 - SM 21-22 4500 NO3 F
21
2.0
Ing/L
20.0 105 83.8-123 1.05 8.27
Blank (B138312-BLKI)
Prepared: 12/22/15 Analyzed: 12/23/15
Nitrate as N
LCS (111138312-BS1)
ND
0.050
Ing/L
Prepared: 12/22/15 Analyzed: 12/23/15
Nitrate as N
LCS Dup (111138312-BSDI)
4.6
-9/1-
4.27 108 88.9-111
Prepared: 12/22/15 Analyzed: 12/23/15
Nitrate as N
Batch B138422 - SM 5310C
4.6
-9/1-
4.27 108 88.9-111 0.00 5.66
Blank (111138422-BLIKI)
Prepared & Analyzed: 12/23/15
Total Organic Carbon
LCS (B139422-BS1)
ND
0.50
-9/1-
Prepared & Analyzed: 12/23/15
Total Organic Carbon
LCS Dup (B138422-BSDI)
10.5
0.50
mg/L
10.0 105 90.1-114
Prepared & Analyzed: 12/23/15
Total Organic Carbon
10.3
0.50
-9/1-
10.0 103 90.1-114 1.85 7.72
I Page 38 of 46 1

confater, to
ON1111111
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
QC result is outside ofestablished limits.
t Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
Data exceeded client recommended or regulatory level
RL Reporting Limit
DL Method Detection Limit
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
I Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside ofcontrol limits.
Reported value for this compound is likely to be biased on the low side.
RL-1 I Elevated reporting limit due to high concentration oftarget compounds.
V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Increased uncertainty is associated with the reported value which is likely to be biased on die low side.
V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
Table of Contents
I Page 39 of 6

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
381 6-RSK1 75 in Water
Ethane
VA,NY,ME
Ethene
VANY,ME
Methane
VANY,ME
ASTMD516-07in Water
Sulfate
NYNH,MA,CT,R1,VANC
SM 21-22 4500 NO2 B in Water
Nitrite as N
CTNH,NY,Nffi,NC,VA,Rl
SM 21-22 4500 NO3 F in Water
Nitrate as N
CT,MANH,NY,R1,ME,NC,VA
SM5310Cin Water
Total Organic Carbon
NYNC,CT,R1,ME,MA,VA
SM19-22 4500 NH3 C in Water
Anunortia as N
NYMA,CT,R1,VANC,ME
SM21-22 450OS-F in Water
Sulfide
CT,NH,NYJU,NC,ME,VA
SW-846 6020A in Water
Manganese
CTNHNY,NC,ME,VA
Manganese
CTNHNYNC,ME,VA
SW-846 8260B in Water
Acetone
NC
Benzene
NC
Brornobenzene
NC
Bromochloromethane
NC
Brornodichlorornethane
NC
Brornoform
NC
Brornornethane
NC
2-Butanone (MEK)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromoethane (EDB)
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
Dichlorodifluoromediane (Freon 12)
NC
I Page 4

Table of Contents
con-Ptest.0
ANALYTICAL LABORATORY
Certified Analyses included in this Report
Analyte
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certifications
SW-846 8260B in Water
I,I-Dichloroediane
NC
1,2-Dichloroethane
NC
I,I-Dichloroedlylene
NC
cis- 1,2-Dichloroethylene
NC
trans- 1,2-Dichloroethylene
NC
1,2-Dicliloropropane
NC
1,3-Dichloropropanc
NC
2,2-Dicidoropropane
NC
IJ-Dichloropropene
NC
cis- 1,3-Dichloropropene
NC
trans- 1,3-Dichloropropcne
NC
Diisopropyl Ether (DIPE)
NC
Ethylbenzcne
NC
2-Hexanonc (MBK)
NC
lsopropylbcnzene (Cumene)
NC
p-Isopropyltoluene (p-Cymene)
NC
Medlyl tert-Butyl Ether (MTBE)
NC
Methylene Chloride
NC
4-Medlyt-2-pentanone (MlBK)
NC
Naphthalene
NC
n-Propylbenzene
NC
Styrene
NC
1, 1,2,2-TetiAchloroedianc
NC
Tetrachloroethylenc
NC
Toluene
NC
1,2,3-Trichlorobenzene
NC
1,2,4-Txichlorobenzene
NC
1, 1, I-Trichloroethane
NC
1,1,2-Tricblorocdiane
NC
Trichloroethylene
NC
Trichlorofluoromethane (Freon 11)
NC
1,2,3-Trichloropropane
NC
1,2,4-Trimethylbenzene
NC
1,3,5-Trimethylbenzene
NC
Vinyl Acetate
NC
Vinyl Chloride
NC
m+p Xylenc
NC
o-Xylene
NC
I Page 41 of �46

Table of Contents
A1111 i co -must'
wrAN&YTC& LASOMTM
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AlHA-LAP, LLC
100033
02/1/2016
MA
Massachusetts DEP
M-MAIOO
06/30/2016
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2017
NY
New York State Department ofHealth
10899 NELAP
04/1/2016
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2016
RI
Rhode Island Department of Health
LAOOO 112
12/30/2015
NC
North Carolina Div. of Water Quality
652
12/31/2016
NJ
New Jersey DEP
MA007 NELAP
06/30/2016
FL
Florida Department of Health
E871027 NELAP
06/30/2016
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2016
WA
State of Washington Department ofEcology
C2065
02/23/2016
ME
State ofMainc
2011028
06/9/2017
VA
Commonwealth of Virginia
460217
12/14/2016
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2016
I Page 42

Phone: [phone]Z CHAIN OF CUSTODY RECORD 39 Spruce Street Page- I Of
conmtEsto Fax:[phone] East Longmeadow, MA 01028
ANALYTICAL LABORATORY Email: [e-mail] I# of Containers
44 http://www.contestlabs.com I** Preservation
Company Name: A.'rC Telephone: _111.8+1-099c:1 'Container Code
Address: 'a_5 f 'Solt it?,l 0 C— -1 A0 I 5L33 Dissolved Metuls
,A5f Project # a i Re uested
fo,,ICW� N(_ Q_,��04 Client PO#
0 Field Filtered
DATA DELIVERY (check all that apply) < 0 Lab to Filter
Attention: — r-11 1 40
0 FAX EMAIL OWEBSITE
Project Location: ff-0 C I CA0VIF-S Fax #
t, L" I— I �g C W 'Cont. Code-
A=amber glass
Sampled By: 94br_0 ZPW -d- r!l AJo JS
Erna i 1: 'T05f.-i. A I P�p) (J-10. covll� G=glass
Project Proposal Provided? (for billing purposes) Format: GPDF 41EXCEL OGIS B *Z! -e P=piastic
0) r ST=sterile
C) yes proposalclate 0 OTHER
0 "Enhanced Data Package" S=summa can
Beginning Ending *Matrix Conc
Con -Test Lab ID ri
Client Sample ID Description zr 1 0
ilaboratary uw ar�yj Date/+W^e- D&WTime Composite Grab Code Code 4 0 WIN T=tedlar bag
F Coll E V= vial
0 O=Other
X
M Lk V Preservation
nla LA �10 I = Iced
H HCL
M Methanol
IN Nitric Acid
S = Sulfuric Acid
8 = Sodium bisulfate
X = Na hydroxide
T = Na thiosulfate
0 = Other
*MatrixCaft
VM= wastewater
GW= groundwater
Comments: Please use the following codes to let Con -Test know if a specific sample may be high DW= drinking water
in concentration in Matrix/Conc. Code Box: A air
............... .................................... ........ I ............................................................................ S soil/solid
D5c A L'.5+ + *
H - High;
Relinquish sign
Date/Time:
Turnaround
Detection
Limit Requirement
North Carolina
0 2L
WWI
5-Day
S-7-Day
0
Recei& by: ($2!9"
Date/Time:
I a// 6 /��
0 10-Day
RUSH
0 GWPC
0 SWSL
-D
teli iZd�b: !i
Date/Time:
0)
.0
(D
Z_ -
1-1/V/ �_ X1 151
0 '24-Hr r'48-Hr
'72-Hr r '4-Day
0 OTHER
-0,
teceiVe3l b 3,0"CD
t /Ti
[
Requires Lab Approval
4�C) --
TURNAROUND TIME 1business days) STARTS AT 9:00 A.M. THE DAY AFTER SAMPLE RECEIPT UNLESS THERE ARE QUESTIONS ON YOUR CHAIN.
' IF THIS FORM IS NOT FILLED OUT COMPLETELY OR IS INCORRECT, TURNAROUND TIME WILL NOT START UNTIL ALL QUESTIONS ARE ANSWERED
M - Medium; L - Low; C - Clean; U - Unknown aL. = sluuge
0 =other
Program, Information
0 DSCA () IHS8 Orphaned Landfill
0 SWS Landfill 0 LIST REC
0 Other:
L
NELAC & AIHA Certified
WBE/DBE Certified
PLEASE BE CAREFUL NOT TO CONTAMINATE THIS DOCUMENT
(D
0
C)
0
n
(D
�L
(n

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Table of Contents
39 Spruce St.
East Longmeadow, MA. 01028
P: 413-525-2332
F: 413-525-6405
www.contestiabs.com
CLIENT NAME:
14D
con-Usto
I
ANAL"CALLABORATORY
Page I of 2
Sample Receipt Checklist
RECEIVED BY: LEM D
1) Was the chain(s) of custody relinquished and signed? No No CoC Included
2) Does the chain agree with the samples? 19 No
If not, explain:
3) Are all the samples in good condition? IS No
If not, explain:
4) How were the samples received:
On Ice LK_ Direct from Sampling Ambient El In Cooler(s)
Were the samples received in Temperature Compliance of (2-6*C)? 6D N o N/A
Temperature 'C by Temp blank 3,c) -Temperature 'C by Temp gun
11_�)
5) Are there Dissolved samples for the lab to filter? Yes (No)
Who was notified Date Time
6) Are there any RUSH or S ORT HOL - ING TIME samples? No
Who was notified ate Time
ermission to subcontract samples? Yes No
7) Location where samples are stored: (Walk-in clients only) if not already approved
Client Signature:
8) Do all samples have the proper Acid pH: ee No N/A
s
9) Do all samnles have the proper Base pH: Yes No NIA
10) Was the k �, notified o, any discrepancies with the CoC vs the samples: Yes
Contai ners received at Con -Test
# of containers
X.
1 Liter Amber
8 oz amber/clear jar
500 mL Amber
4 oz amber/clear jar
250 mL Amber (8oz amber
2 oz amber/clear jar
1 Liter Plastic
Plastic Bag / Ziploc
500 mL Plastic
SOC Kit
250 mL plastic
Non-ConTest Container
40 mL Vial - type listed below
Perchlorate Kit
Colisure / bacteria bottle
Flashpoint bottle
Dissolved Oxygen bottle
Other glass jar
Encore
Other
Laboratory Comments:
40 mL vials: # HCI 10
.. D .... ..
6c# 277: # Bisulfate
ReVA Auquist �().1.3. # Thiosulfate
# Methanol
# DI Water
Unpreserved
# of containers
Time and Date Frozen:
I Page 45

Table of Contents
Page 2 of 2
Login SaMDle Receipt Checklist
(Rejection Criteria Listing - Using Sample Acceptance Policy)
Any False statement will be brought to the attention of Client
r)"aafinn Answer (True/ A!Ue Comment
T/FJNA
1) The cooler's custody seal, if present, is intact.
2) The cooler or samples do not appear to have
been compromised or tampered with.
3) Samples were received on ice.
4) Cooler Temperature is acceetable.
5) Cooler Temperature is recorded.
COC is filled out in ink and legible.
7) COC is filled out with all pertinent information.
8) Field Sampler's name present on COC.
9) There are no discrepancies between the
sample IDs on the container and the COC.
10) Samples are received within Holding Time.
11) Sample con.ainers have legible labels.
12) Containers are not broken or leaking.
13) Air Cassettes are not broken/open.
14) Sample collection date/times are provided.
-15) Appropriate sample containers are used.__
16) Proper collection media used.
17) No headspace sample bottles are completely filled.
18) There is sufficient volume for all requsted
analvses, including any,.reque ted MS/MSDs._
19) Trip blanks provided if applicable.
20) VOA sample vials do not have head space or
bubble is <6m
21) Samplesdo not require splitting or compositing.
rr:
Who notitieU 01 I -Me staxe evits. LLICIUM? I I 1�
Doc #277 Rev. 4 August 2013 Log -In Technician Initials: KNII DatelTime: ol(457
/D-�Y
I Page 4

con-Usto"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 24, 2015
Justin Ballard
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: 8379 Creeedmoor Rd., Raleigh
Client Job Number:
Project Number: DC9201SL33
Laboratory Work Order Number: 15LO991
Enclosed are results of analyses for samples received by the laboratory on December 17, 2015. If you have any questions
conceming this report, please feel free to contact me.
Sincerely,
I, �4/U44�
Lisa A. Worthington
Project Manager

Table of Contents
Sample Summary
Case Narrative
Sample Results
15LO991 -01
15LO991-02
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/MS
B138233
Miscellaneous Organic Analyses
B138318
Metals Analyses (Total)
B138299
Metals Analyses (Dissolved)
B138303
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B138157
B138214
B138250
B138306
B138312
B138422
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
11
17
19
19
19
23
23
24
24
25
25
26
26
26
26
26
27
27
28
29
32

con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121 REPORT DATE: 12/24/2015
Raleigh, NC 27604 PURCHASE ORDER NUMBER:
ATTN: Justin Ballard
PROJECT NUMBER: DC9201SL33
ANALYTICAL SUMMARY
WORK ORDER NUM13ER: 15LO991
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 8379 Crecedmoor Rd., Raleigh
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAIB
EW9 15LO991-01 Ground Water 3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 5310C
SM19-22 4500 NH3 C
SM21-22 450OS-F
SW-846 6020A
SW-846 8260B
MW12 15LO991-02 Ground Water 3810-RSK175
ASTM D516-07
SM 21-22 4500 NO2 B
SM 21-22 4500 NO3 F
SM 53 IOC
SM19-22 4500 NI-13 C
SM21-22 450OS-F
SW-846 6020A
SW-846 8260B

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
The results ofanalyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals inunediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: WorkOrder: ISLO991
Date Received: 12/17/2015
Field Sample#: EW9 Sampled: 12/17/2015 14:00
SamvlelD: 15LO"1-01
Samole Matrix: Ground Water
Volatile Organic Compounds by GUMS
Date
Date/Time
Anslyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
0.037
0.050
0.0049
Ing"L
I J
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Benzene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Bromodichoromethane
ND
0.00050
0.000088
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/21/15
12122/15 16:01
EEH
2-Butanone IMEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EER
n-Butylbenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
sec-Butylbenzene
ND
0.0010
0.00013
mg1L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
tert-Butylbenzene
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Carbon Tetrachloride
ND
0.0050
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Chlorobenzene
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Chlomethane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Chloroform
0.00086
0.0020
0.00022
mg/L
1 J
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
2-Chlorotoluene
ND
0.0010
0.00012
mg1L
1
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
4-Chlorotoluene
ND
0.0010
0.00014
mg/L
I
SW-846 8260B
12121/15
12/22/15 16:01
EEH
1,2-Dibromoethane (EDB)
ND
0.00050
0.00012
-9/1-
1
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,2-Dichlorobenzene
ND
0.0010
0.00017
mg1L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,3-Dichlorobenzene
ND
0.0010
0.00017
1119/1-
1
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,4-Dichlorobenzene
ND
0.0010
0.00015
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
I,I-Dichloroethane
ND
0.0010
0.00016
mg(L
I
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
1,2-Dichloroethane
ND
0.0010
0.00019
-9(L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
I,I-Dichloroethylene
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
cis- 1,2-Dichloroethylene
0.012
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
tmns-1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,2-Dichloropropane
ND
0.0010
0.00013
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,3-Dichloropropane
ND
0.00050
0.00013
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
IJ-Dichloropropene
ND
0.0020
0.00013
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
cis- 1,3-Dichloropropene
ND
0.00050
0.00012
mg/L
1
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg(L
I
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg(L
I
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
Ethylbenzene
ND
0.0010
0.00013
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
2-Hexanone (MBK)
ND
0.010
0.0015
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
lsopropylbenzene (Cumene)
ND
0.0010
0.00012
-911-
1
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
p-Isopropyltoluene (p-Cymene)
ND
0.0010
0.00015
mg(L
I
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12121/15
12/22/15 16:01
EEH
4-Methyl-2-pentanone (MlBK)
ND
0.010
0.0015
mg(L
I
SW-946 8260B
12/21/15
12/22/15 16:01
EEH

con-tesc'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Field Sample#: EW9 Sampled: 12/17/2015 14:00
Samule ID: 15L0991-01
SaroDle Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mg/L
1
SW-946 8260B
12/21/15
12/22/1516:01
EEH
n-Propylbenzene
ND
0.0010
0.00013
mg/L
1
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
Styrene
IND
0.0010
0.00015
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00016
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Tetrachloroethylene
0.16
0.00050
0.00017
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Toluene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1, 1, 1 -Trichloroethane
ND
0.0010
0.00DO94
mg1L
1
SW-946 8260B
12/21/15
12/22/15 16:01
EEH
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg1L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Trichloroethylene
0.0073
0.0010
0.00020
mg/L
I
SW-946 8Z60B
12/21/15
12/22/15 16:01
EEH
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
1,3,5-TTimethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8160B
12/21/15
12/22/15 16:01
EEH
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
m+p Xylene
ND
0.0020
0.00025
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:01
EEH
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 105 70-130 12/22/15 16:01
Toluenc-d8 98.0 70-130 12/22/15 16:01
4-Bromofluorobenzene 98.7 70-130 12/22/15 16:01

0 con-testo"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Fleld Sample#: EW9 Sampled: 12117/2015 14:00
Sample ID: 15LO"1-01
Samnle Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Dateffime
Analyte Results
. RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
mg/L I
3810-RSK175
12/22/15
12/22/15 18:48
TPH
Ethene NID
0.0038
0.00099
mg/L I
3810-RSK175
12/22/15
12/22/15 18:48
TPH
Methane 4.1
0.0053
0.0022
mg/L 2
3810-RSK175
12/22/15
12/22/15 19:04
TPH

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413t525-6405 * TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Field Sample#: EW9 Sampled: 12/17/2015 14:00
Satanic, ID: 15LO991-01
Sanmle Matrix: Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 930 2.0 0.23 Pg/L 2 SW-846 6020A 12/22/15 12/23/15 12:55 MJH

0 con-tcst'o
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Field Sample#: EW9 Sampled: 12/17/2015 14:00
Samvle ID: 15LO991-01
Samvle Matrix: Ground Water
Metals Analyses (Dissolved)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganese 910 2.0 0.23 Rg/L 2 SW-846 6020A 12/22/15 12/23/15 13:57 MJH

con-atcst'9
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Field Sarnple#: EW9 Sampled: 12/17/2015 14:00
Samule ID: 15LO"1-01
Samnle Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APRA/SW-846 Methods (total)
Date
Date/Time
Analyte
Results
RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ammonia as N
ND
0.30
0.22
mg/L I
SM19-22 4500 N113 C
12/22/15
12/23/1514:00
VAK
Nitrate as N
ND
0.050
0.049
mg/L I
SM 21-22 4500 NO3 F
12/22/15
12/23/15 15:45
AG
Nitrite as N
0,0029
0.010
0.0020
mg/L I J
SM 21-22 4500 NO2 B
12/18/15
12/18/15 11:30
MMH
Sulfate
ND
2.0
0.40
mg/L I
ASTM D516-07
12/22/15
12/22/15 13:53
MMH
Sulfide
ND
2.0
1.8
mg1L I
SM21-22 450OS-F
12/21/15
12/21/15 18:45
DJM
Total Organic Carbon
1.8
0.50
0.16
mg/L 1
SM 5310C
12/23/15
12/23/15 15:30
ILL

con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Crecedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Fleld Sample#: MW12 Sampled: 12/17/2015 13:20
Samole ID: 15LO991-02
Sanmle Matrix: Ground Water
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
0.0065
0.050
0.0049
mg1L
I J
SW-846 8260B
12/21/15
12/22/1516:28
EEH
Benzene
ND
0.0010
0.00012
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Bromobenzene
ND
0.0010
0,00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Bromochloromethane
IND
0.0010
0.00022
Ing/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Bromodichloromethane
ND
0.00050
0.000088
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Bromoform
ND
0.0010
0.00021
mg(L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Bromomethane
ND
0.0020
0.00094
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
n-Butylbenzene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
sec-Butylbenzene
ND
0,0010
0.00013
111911,
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
tcrt-Butylbenzcne
ND
0.0010
0.00011
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Carbon Tetrachloride
ND
0.0050
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Chlorobenzene
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Chlorodibromomethane
ND
0.00050
0.00010
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Chloroethane
ND
0.0020
0.00028
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Chloroform
ND
0.0020
0.00022
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Chloromethane
ND
0.0020
0.00032
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
4-Chlorotoluene
ND
0.0010
0.00014
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2-Dibromocthanc (EDB)
ND
0.00050
0.00012
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,3-Dichlorobenzene
IND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,4-Dichlorobenzcne
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
I,I-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2-Dichloroethane
ND
0.0010
0.00019
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
I,I-Dichloroethylene
ND
0.0010
0.00021
mg(L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
cis- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
trans- 1,2-Dichlorocthylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,3-Dichloropropane
ND
0.00050
0.00013
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
I,I-Dichloropropene
ND
0.0020
0.00013
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
cis- 1,3-Dichloropropene
ND
0.00050
0.00012
mg(L
I
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
-g(L
I
SW-946 8260B
12J21/15
12/22/15 16:28
EEH
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Ethylbcnzene
ND
0.0010
0.00013
1119/1-
1
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
2-Hexanonc (MIBK)
ND
0.010
0.0015
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
Isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
p-Isopropyltoluenc (p-Cymcnc)
IND
0.0010
0.00015
mg(L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Mcthylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
4-Mcthyl-2-pentanone (MlBK)
ND
0.010
0.0015
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:28
EEH

con-toto
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Field Sample#: MW12 Sampled: 12/17/2015 13:20
SamnleID: 15LO"1-02
Sarnvle Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RIL
DL
Units
Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mgfL
I
SW-846 8260B
12/21/15
12/22/1516:28
EEH
n-Propylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00016
1119/1-
1
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
Tetrachloroethylene
0.00076
0.00050
0.00017
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
Toluene
ND
0.0010
0.00017
-9/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
-91L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1, 1, 1 -Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
Trichloroethylene
ND
0.0010
0.00020
mgfL
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2,3-Trichloropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,2,4-Trimcthylbenzene
ND
0.0010
0.00018
mg/L
1
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
1,3,5-Trimethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/21/15
12/22/15 16:28
EEH
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
m+p Xylene
ND
0.0020
0.00025
ing/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/21/15
12/22/15 16:28
EEH
Surrogates
% Recovery
Recovery Limits
nag/Qua]
1,2-Dichlorocthane-d4 102 70-130 12/22/15 16:28
Toluene-d8 101 70-130 12/22/15 16:28
4-Bromofluorobenzene 99.5 70-130 12/22/15 16:28

con-Usto
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Field Sample #: MW12 Sampled: 12/17/2015 13:20
Sample ID: 15LO991-02
Samole Matrix: Ground Water
Miscellaneous Organic Analyses
Date
Date/Time
Analyte Results
- RJL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ethane ND
0.0028
0.00088
mg/L I
3810-RSK175
12/22/15
12/22/15 19:22
'f?H
Ethcnc ND
0.0038
0.00099
mgfL I
3810-RSK175
12/22/15
12/22/15 19:22
TPH
Methane ND
0.0026
0.0011
mg/L I
3810-RSK175
12/22/15
12/22/15 19:22
TPH

con-NsC'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Santple Description: Work Order: 15LO991
Date Received: 12/17/2015
Field Sample#: MW1 2 Sampled: 12/17/2015 13:20
Samule ID: 15LO991-02
Samole Matrix: Ground Water
Metals Analyses (Total)
Date Date/Time
Analyte Results RIL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Manganesc 420 2.0 0.23 Rg/L 2 SW-846 6020A 12/22/15 12/23/15 12:58 MJH

con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA01028 * FAX 4`13/525-6405 * TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Held Sample#: MW12 Sampled: 12/17/2015 13:20
Sarrmle ID: 15LO991-02
Samole Matrix: Ground Water
Metals Analyses (Dissolved)
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qua] Method Prepared Analyzed Analyst
Manganese 430 2.0 0.23 ilg/L 2 SW-846 6020A 12/22/15 12/23/15 14:01 MJH

con-test`�'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8379 Creeedmoor Rd., Raleigh Sample Description: Work Order: 15LO991
Date Received: 12/17/2015
Held Sample #: MW12 Sampled: 12/17/2015 13:20
Sainvie ID: 15LO991-02
Samule Matrix: Ground Water
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (rutal)
Date
Date/Time
Analyte
Results
RL
DL
Units Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Ammonia as N
ND
0.30
0.22
mg1L 1
SM 19-22 4500 NH3 C
12/22/15
12/23/15 14:00
VAK
Nitrate as N
0.74
0.050
0.049
mg/L I
SM 21-22 4500 NO3 F
12/22/15
12/23/15 15:45
AG
Nitrite as N
0.0062
0.010
0.0020
mg1L I J
SM 21-22 4500 NO2 B
12/18/15
12/18/15 11:30
MMH
Sulfate
ND
2.0
0.40
mg/L I
ASTM D516-07
12/22/15
12/22/15 13:53
MMH
Sulfide
ND
2.0
1.8
mg/L I
SM21-22 450OS-F
12/21/15
12/21/15 18:45
DJM
Total Organic Carbon
1.6
0.50
0.16
Ing/L I
SM 5310C
12/23/15
12/23/15 15:30
ILL

con-Ust'9
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
3810-RSK175
Lab Number [Field ID] Batch Initial JmLl Final [mL] Date
15LO991-01 [EW9]
B138318
1.00
1.00
12/22/15
15LO991-OIREI [EW91
B138318
1.00
1.00
12122/15
15LO991-02 [MW12]
B138318
1.00
1.00
12/22/15
ASTM D516-07
Lab Number [Field ID]
Batch
Initial [mLj
Final [mL]
Date
15LO991-01 [EW9]
B138306
100
too
12/22/15
15LO991-02 [MW12]
B138306
too
100
12/22/15
SM 21-22 4500 NO2 B
Lab Number [Field ID]
Batch
Initial [mL]
Final [mLl
Date
15L0991-01 [EW91
B138157
50.0
50.0
12/18/15
15LO991-02 [MW12]
B138157
50.0
50.0
12/18/15
SM 21-22 4500 NO3 F
Lab Number JIField ID]
Batch
Initial [mL]
Final JmLj
Date
15LO991-01 [EW91
B138312
25.0
25.0
12/22/15
15LO991-02 [MW121
B138312
25.0
25.0
12/22/15
SM 5310C
Lab Number [Field ID]
Batch
Initial [mLl
Final JmL]
Date
15LO991-01 [EW91
B138422
50.0
50.0
12/23/15
15LO991-02 [MW 121
B138422
50.0
50.0
12/23/15
SM19-22 4500 NH3 C
Lab Number [Field ID] Batch Initial [mLl Final JmL] Date
15LO991-01 [EW9] B138250 100 100 12/22/15
15LO991-02 [MW121 B 138250 100 100 12/22/15
SM21-22 450OS-F
Lab Number [Field ID]
Batch
Initial JmL] Final [mLl
Dote
15LO991-01 [EW9]
B 138214
100 100
12/21/15
15LO991-02 (MW12]
B 138214
100 100
12121/15
Prep Method: SW-846 3005A-SW-846 6020A
Lab Number [Field ID]
Batch
Initial JmLl
Final lint.]
I)ate
ISLO991-01 [EW91
B138299
50.0
50.0
12/22/15
15LO991-02 W12]
B138299
50.0
50.0
12/22/15

con-tcst'9
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3005A Dissolved-SW-846 6020A
Lab Number []Field ID]
Batch
Initial [mLl
FInal JmLl
Date
15L0991-01 [EW91
B138303
50.0
50.0
12/22/15
15LO991-02 [MW12]
B 138303
50.0
50.0
12/22/15
Prep Method: SW-846 5030B-SW-846 8260B
Lab Number 11711eld ID]
Batch
Initial JmLj
FInal [mL]
Date
ISLO991-01 [EW91
B138233
5
5.00
12/21/15
15LO991-02 [MW121
B138233
5
5.06
12/21/15

con-sksto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
nalyte Result Limit Units Level Result O/oREC Limits RPD Limit Notes
Batch B138233 - SW-846 5030B
Blank (11138233-11M) Prepared & Analyzed: 12/22/15
Acetone
ND
0.050
mg(L
Benzene
ND
0.0010
mg/L
Bromobcnzene
ND
0.0010
mg1L
Bromochloromethane
ND
0.0010
Mg/L
Bromodichloromethane
ND
0.00050
mg/L
Bromolorm
ND
0.0010
-9/1-
Bromomcthanc
ND
0.0020
mg/L
2-Butanonc (MEK)
ND
0.020
mg/L
n-Butylbcnzene
ND
0.0010
mg/L
sec-Butylbenzene
ND
0.0010
mg/L
tert-Butylbenzene
ND
0.0010
mg/L
Carbon Disullide
ND
0.0040
mg/L
Carbon Tetrachloride
ND
0.0050
mg/L
Chlorobenzcnc
ND
0.0010
mg/L
Chlorodibromomethanc
ND
0.00050
mg/L
Chlorocthane
ND
0.0020
mg/L
Chloroform
ND
0.0020
mg/L
Chloromethane
ND
0.0020
mg/L
2-Chlorotoluene
ND
0.0010
mg/L
4-Chlorotolucnc
ND
0.0010
mg/L
1,2-Dibromocthanc (EDB)
ND
0.00050
mg/L
1,2-Dichlorobenzene
ND
0.0010
mg/L
1,3-Dichlorobenzene
ND
0.0010
mg/L
1,4-Dichlorobenzene
ND
0.0010
mg1L
Dichlorodifluoromcthanc (Freon 12)
ND
0.0020
mg/L
1, 1 -Dichlorocthanc
ND
0.0010
mg/L
1,2-Dichloroethanc
ND
0.0010
mg/L
I,I-Dichloroethylene
ND
0.0010
mg(L
cis- 1,2-Dichloroethylene
ND
0.0010
mg/L
trans- 1,2-Dichlorocthylene
ND
0.0010
mg/L
1,2-Dichloropropane
ND
0.0010
mg/L
1,3-Dichloropropanc
ND
0.00050
mg/L
2,2-Dichloropropane
ND
0.0010
mg/L
IJ-Dichloropropene
ND
0.0020
mg/L
cis- 1,3-Dichloropropene
ND
0.00050
mg(L
tmns-1,3-Dichloropropene
ND
0.00050
mg/L
Diisopropyl Ether (DIPE)
ND
0,00050
mg/L
Ethylbenzene
ND
0.0010
mg/L
2-Hexanonc (MBK)
ND
0.010
mg/L
Isopropylbenzene (Cumcne)
ND
0.0010
mg/L
p-lsopropyltoluene (p-Cymenc)
ND
0.0010
mg/L
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
mg/L
Methylenc Chloride
ND
0.0050
mg/L
4-Methyl-2-pentanone (NHBK)
ND
0.010
mg/L
Naphthalene
ND
0.0020
mg/L
n-Propylbenzene
ND
0.0010
mg/L
Styrene
ND
0.0010
mg/L
1, 1,2,2-Tctrachlorocthane
ND
0.00050
mg/L
Tetrachloroethylenc
ND
0.00050
M&/L
Toluene
ND
0.0010
-9/1-
1,2,3-Trichlorobenzenc
ND
0.0050
mg/L
1,2,4-Trichlorobcnzcne
ND
0.0010
-gfL

con-atestO
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
QUALITY CONTROL
Nlolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source O/oREC RPD
Lnalyte Result Limit Units Level Result 0/9REC Limits RPD Limit Notes
Batch B138233 - SW-846 5030B
Blank (B138233-BLK1) Prepared& Analyzed: 12/22/15
1,1,1-Trichloroethane
ND
0.0010
mg/1-
1, 1,2-Trichloroethane
ND
0.0010
mg/L
Trichloroethylene
ND
0.0010
mg/L
Trichlorofluoromethane (Freon 11)
ND
0.0020
mg/L
1,2,3-Trichloropropane
ND
0.0020
mg/L
1,2,4-Trimethylbenzene
ND
0.0010
mg/L
1,3,5-Trimethylbenzene
ND
0.0010
mg/L
Vinyl Acetate
ND
0.020
mg/L
Vinyl Chloride
ND
0.0020
mg(L
m+p Xylene
ND
0.0020
mg/L
o-Xylene
ND
0.0010
mg/L
Surrogate: 1,2-Dichloroethane-d4
0.0257
mg/L
0.0250 103 70-130
Surrogate: Toluene-d8
0.0252
mg/L
0.0250 101 70-130
Surrogate: 4-Bromotluorobenzene
0.0243
mgfL
0.0250 97.2 70-130
LCS (B138233-BS1)
Prepared& Analyzed: 12/22/15
Acetone
0.0718
0.050
mg/L
0.100
71.8
70-160
Benzene
0.0106
0.0010
mg/L
0.0100
106
70-130
Bromobenzene
0.0103
0.0010
-9/1-
0.0100
103
70-130
Bromochloromcthane
0.0122
0.0010
mg/L
0.0100
122
70-130
Bromodichloromethane
0.00971
0.00050
mg/L
0.0100
97.1
70-130
Bromoform
0.00839
0.0010
mg/L
0.0100
83.9
70-130
Bromomethane
0.00701
0.0020
mg/L
0.0100
70.1
40-160
2-Butanone (MEK)
0.0869
0.020
mg/L
0.100
86.9
40-160
n-Butylbenzene
0.0105
0.0010
nig/L
0.0100
105
70-130
sec-Butylbenzene
0.0105
0.0010
mg/L
0.0100
105
70-130
tert-Butylbenzene
0.0102
0.0010
mg/L
0.0100
102
70-130
Carbon Disulfide
0.00910
0.0040
mg/L
0.0100
91.0
70-130
Carbon Tetrachloride
0.0106
0.0050
mg/L
0.0100
106
70-130
Chloroberizene
0.00946
0.0010
mg/L
0.0100
94.6
70-130
Chlorodibromomethanc
0.00904
0.00050
mg/L
0.0100
90.4
70-130
Chloroethane
0.0109
0.0020
mg/L
0.0100
109
70-130
Chloroform
0.0104
0.0020
mg/L
0.0100
104
70-130
Chloromethane
0.00901
0.0020
mg/L
0.0100
90.1
40-160
2-Chlorotoluene
0.00960
0.0010
mg/L
0.0100
96.0
70-130
4-Chlorotoluene
0.00961
0.0010
mg/L
0.0100
96.1
70-130
1,2-Dibromoethane (EDB)
0.0101
0.00050
mg/L
0.0100
101
70-130
1,2-Dichlorobenzene
0.00936
0.0010
mg/L
0.0100
93.6
70-130
1,3-Dichlorobenzene
0.0100
0.0010
mg/L
0.0100
100
70-130
1,4-Dichlorobenzene
0.00971
0.0010
mg/L
0.0100
97.1
70-130
Dichlorodifluoromethane (Freon 12)
0.00546
0.0020
mg/L
0.0100
54.6
40-160
I,I-Dichloroethane
0.0112
0.0010
mg/L
0.0100
112
70-130
1,2-Dichloroethane
0.00996
0.0010
mg/L
0.0100
99.6
70-130
1, 1 -Dichloroethylene
0.0102
0.0010
mg/L
0.0100
102
70-130
cis- 1,2-Dichloroethylene
0.0104
0.0010
mg/L
0.0100
104
70-130
trans- 1,2-Dichloroethylene
0.0102
0.0010
mg/L
0.0100
102
70-130
1,2-Dichloropropane
0.0108
0.0010
mg/L
0.0100
108
70-130
1,3-Dichloropropane
0.0104
0.00050
mg/L
0.0100
104
70-130
2,2-Dichloropropane
0.0108
0.0010
mg/L
0.0100
108
40-130
IJ-Dichloropropene
0.0106
0.0020
mg/L
0.0100
106
70-130
cis- 1,3-Dichloropropene
0.00937
0.00050
mg1L
0.0100
93.7
7G- 130
trans- 1,3-DichloTopropene
0.00984
0.00050
mg/L
0.0100
98.4
70-130
t
t
t
t

con-atcsto"
ANALYTICAL LABORATORY
Batch B138233 - SW-846 5030B
LCS (Bl38233-BSI)
Diisopropyl Ether (DIPE)
Ethylbenzene
2-Hexanone (MBK)
Isopropylbenzene (Cumene)
p-Isopropyltoluene (p-Cyinene)
Methyl tert-Butyl Ether (MTBE)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Naphthalene
n-Propylbenzene
styrene
1, 1,2,2-TetrachloroethaDe
Tetrachloroethylene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1 -Trichloroethane
1, 1,2-Trichloroethanc
Trichloroethylene
Trichlorofluoromcthane (Freon 11)
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Acetate
Vinyl Chloride
m+p Xylene
o-Xylene
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source 0/6REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Prepared& Analyzed: 12/22/15
0.00978
0.00050
mg(L
0.0100
97.8
70-130
0.0100
0.0010
mg/L
0.0100
100
70-130
0.0872
0.010
mg/L
0.100
87.2
70-160
0.00991
0.0010
mg/L
0.0100
99.1
70-130
0.0110
0.0010
mg/L
0.0100
110
70-130
0.00939
0.0010
mg/L
0.0100
93.9
70-130
0.0102
0.0050
mg/L
0.0100
102
70-130
0.0948
0.010
1119/1-
0.100
94.8
70-160 t
0.00710
0.0020
1119/1-
0.0100
71.0
40-130 t
0.0101
0.0010
1119/1-
0.0100
101
70-130
0.00981
0.0010
mg(L
0.0100
98.1
70-130
0.00978
0.00050
mg/L
0.0100
97.8
70-130
0.0104
0.00050
mg(L
0.0100
104
70-130
0.0104
0.0010
mg1L
0.0100
104
70-130
0.00734
0.0050
mg1L
0.0100
73.4
70-130
0.00840
0.0010
mg/L
0.0100
84.0
70-130
0.0102
0.0010
mg(L
0.0100
102
70-130
0.0103
0.0010
mg/L
0.0100
103
70-130
0.0102
0.0010
mg/L
0.0100
102
70-130
0.00919
0.0020
mg/L
0.0100
91.9
70-130
0.00987
0.0020
mg/L
0.0100
98.7
70-130
0.0105
0.0010
mg(L
0.0100
105
70-130
0.0103
0.0010
mg(L
0.0100
103
70-130
0.0869
0.020
mg/L
0.100
86.9
70-130
0.00810
0.0020
mg/L
0.0100
81.0
40-160
0.0198
0.0020
mg/L
0.0200
98.9
70-130
0,00981
0.0010
mgfL
0.0100
98.1
70-130
Surrogate: 1,2-Dichloroethane-d4
0.0261 Ing/L
0.0250 104 70-130
Surrogate: Toluene-d8
0.0252 mg/L
0.0250 101 70-130
Surrogate: 4-Bromofluorobenzcnc
0.0244 mg/L
0.0250 97.6 70-130
LCS Dup (Bl38233-BSD1)
Prepared & Analyzed: 12/22/15
Acetone
0.0758
0.050
mg/L
0.100
75.8
70-160
5.42 25
Benzene
0.0107
0.0010
mg/L
0.0100
107
70-130
1,32 25
Bromobenzene
0.0102
0.0010
mg/L
0.0100
102
70-130
0.488 25
Bromochloromcthanc
0.0125
0.0010
mg1L
0.0100
125
70-130
2,76 25
Bromodichloromethane
0.00951
0.00050
mg/L
0.0100
95.1
70-130
2.08 25
Bromoform
0.00823
0,0010
mg/L
0.0100
82.3
70-130
1.93 25
Bromomcthane
0.00792
0.0020
mg/L
0.0100
79.2
40-160
12.2 25
2-Butanone (MEK)
0.0905
0.020
mg/L
0.100
90.5
40-160
4.06 25
n-Butylbenzene
0.00987
0.0010
mg/L
0.0100
98.7
70-130
6.38 25
sec-Butylbenzene
0.0102
0.0010
mg/L
0.0100
102
70-130
3.39 25
tert-Butylbcnzene
0.00967
0.0010
mg1L
0.0100
96.7
70-130
5.24 25
Carbon Disulfide
0.00871
0.0040
mg/L
0.0100
87.1
70-130
4.38 25
Carbon Tetrachloride
0.0107
0.0050
mg/L
0.0100
107
70-130
1.41 25
Chlorobenzene
0.00943
0.0010
11119/1-
0.0100
94.3
70-130
0.318 25
Chlorodibromomcthanc
0.00889
0.00050
mg/L
0.0100
88.9
70-130
1.67 25
Chloroethane
0.0113
0.0020
mg/L
0.0100
113
70-130
3.52 25
Chloroform
0.0104
0.0020
Ing/L
0.0100
104
70-130
0.576 25
Chloromethane
0.00938
0.0020
mg/L
0.0100
93.8
40-160
4.02 25
2-Chlorotoluene
0.00980
0.0010
mg1L
0.0100
98.0
70-130
2.06 25
4-Chlorotoluene
0.00973
0.0010
ing/L
0.0100
97.3
70-130
1.24 25
t
t
t

0 con-atcsV'
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by CXIMS - Quality Control
Reporting Spike Source %REC RPD
.nalyte fzesult Limit Units Level Result 0/.REC Limits RPD Limit Notes
Batch B138233 - SW-846 5030B
LCS Dup (B138233-BSDI)
Prepared& Analyzed: 12/22/15
1,2-Dibromoethane (EDB)
0.0102
0.00050
mg/L
0.0100
102
70-130
1.87
25
1,2-Dichlorobenzene
0.00904
0.0010
mg1L
0.0100
90.4
70-130
3.48
25
1,3-Dichlorobenzene
0.00952
0.0010
mg/L
0.0100
95.2
70-130
4.92
25
1,4-Dichlorobenzene
0.00915
0.0010
mg/L
0.0100
91.5
70-130
5.94
25
Dichlorodifluoromethane (Freon 12)
0.00566
0.0020
mg/L
0.0100
56.6
40-160
3.60
25 t
I,I-Dichloroethane
0.0110
0.0010
mg/L
0.0100
110
70-130
2.25
25
1,2-Dichloroethane
0.00993
0.0010
nig/L
0.0100
99.3
70-130
0.302
25
I,I-Dichloroethylene
0.0103
0.0010
mg/L
0.0100
103
70-130
0.488
25
cis- 1,2-Dichloroethylene
0.0107
0.0010
mg/L
0.0100
107
70-130
2.66
25
trans- 1,2-Dichloroethylene
0.0103
0.0010
mg/L
0.0100
103
70-130
1.76
25
1,2-Dichloropropane
0.0100
0.0010
mg/L
0.0100
100
70-130
7.32
25
1,3-Dichloropropane
0.00989
0.00050
mg/L
0.0100
98.9
70-130
5.51
25
2,2-Dichloropropane
0.0107
0.0010
mgfL
0.0100
107
40-130
1.39
25 t
I,I-Dichloropropene
0.0106
0.0020
mg/L
0.0100
106
70-130
0.472
25
cis- 1,3 -Dichloropropene
0.00932
0.00050
mg/L
0.0100
93.2
70-130
0.535
25
trars- 1,3-Dichloropropene
0.00996
0,00050
mg/L
0.0100
99.6
70-130
1.21
25
Diisopropyl Ether (DIPE)
0.00976
0.00050
mgfL
0.0100
97.6
70-130
0.205
25
Ethylbenzene
0.0102
0.0010
mg/L
0.0100
102
70-130
1.58
25
2-Hexanone (MBK)
0.0872
0.010
mg/L
0.100
87.2
70-160
0.0344
25 t
Isopropylbenzene (Cumene)
0.00981
0.0010
nig/L
0.0100
98.1
70-130
1.01
25
p-lsopropyltoluene (p-Cymene)
0.0106
0.0010
mg/L
0.0100
106
70-130
4.16
25
Methyl tert-Butyl Ether (MTBE)
0.00957
0.0010
mg/L
0.0100
95.7
70-130
1.90
25
Methylenc Chloride
0.0103
0.0050
mg/L
0.0100
103
70-130
1.56
25
4-Methyl-2-pentanone (MIBK)
0.0956
0.010
mg/L
0.100
95.6
70-160
0.777
25 t
Naphthalene
0.00711
0.0020
mg/L
0.0100
71.1
40-130
0.141
25 t
n-Propylbenzene
0.0100
0.0010
mg/L
0.0100
100
70-130
0.698
25
Styrene
0.00995
0.0010
mg/L
0.0100
99.5
70-130
1.42
25
1, 1,2,2-Tetmchloroethane
0.00995
0.00050
mg/L
0.0100
99.5
70-130
1.72
25
Tetrachloroethylene
0.0100
0.00050
mg/L
0.0100
100
70-130
3.91
25
Toluene
0.0101
0.0010
mg/L
0.0100
101
70-130
2.82
25
1,2,3-Trichlorobenzene
0.00745
0.0050
mg/L
0.0100
74.5
70-130
1.49
25
1,2,4-Trichlorobenzene
0.00815
0.0010
mg1L
0.0100
81.5
70-130
3.02
25
1, 1, 1 -Trichloroethane
0.0102
0.0010
mg/L
0.0100
102
70-130
0.197
25
1, 1,2-Trichloroethane
0.00946
0.0010
mg/L
0.0100
94.6
70-130
8.31
25
Trichloroethylene
0.0105
0.0010
mg/L
0.0100
105
70-130
3.09
25
Trichlorolluoromethane (Freon 11)
0,00943
0.0020
mg/L
0.0100
94.3
70-130
2.58
25
1,2,3-Trichloropropane
0.00970
0.0020
mg/L
0.0100
97.0
70-130
1.74
25
1,2,4-Trimethylbenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
3.69
25
1,3,5-Trimethylbenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
1.76
25
Vinyl Acetate
0.0885
0.020
mg/L
0.100
88.5
70-130
1.86
25
Vinyl Chloride
0.00815
0.0020
mg/L
0.0100
81.5
40-160
0.615
25 t
m+p Xylene
0.0203
0.0020
mg/L
0.0200
101
70-130
2.45
25
o-Xylene
0.0100
0.0010
mg/L
0.0100
100
70-130
2.02
25
Surrogate: 1,2-Dichloroethane-d4
0.0265
mg/L
0.0250
106
70-130
Surrogate: Toluene-dg
0.0245
mg/L
0.0250
98.0
70-130
Surrogate: 4-Bromofluorobenzene
0.0246
mg/L
0.0250
98.4
70-130

0 con-tcst'o
ANALYTICAL LABORATORY
Batch B138318 - 3810-RSK175
Blank (B138318-BlXl)
Ethane
Ethene
Methane
LCS (11138318-BS1)
Ethane
Ethene
Methane
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
QUALITY CONTROL
Miscellaneous Organic Analyses - Quality Control
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
ND
ND
ND
0.0028 1119/1-
0.0038 mg/L
0.0026 mg/L
Prepared &Analyzed: 12/22/15
Prepared & Analyzed: 12/22115
2100 mg/L 2000 104 60-122
2000 mg/L 2000 98.6 67-113
1900 mg/L 2000 96.3 56-121

con-tesV'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source 9/6REC RPD
Analyte Result Limit Units Level Result 0/6REC Limits RPD Limit Notes
Batch B138299 - SW-846 3005A
Blank (B138299-BLKI) , Prepared: 12/22/15 Analyzed: 12/23/15
Manganese ND 2.0 Ag/L
LCS (B1382"-BSI) Prepared: 12/22/15 Analyzed: 12/23/15
Manganese 242 5.0 Rg/L 250 96.8 80-120
LCS Dup (B1382"-BSD1) Prepared: 12/22/15 Analyzed: 12/23/15
Manganese 243 5.0 Itg/L 250 97.1 80-120 0.327 20

con-tiesto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Metals Analyses (Dissolved) - Quality Control
Reporting Spike Source */.REC RPD
lAnalyte Result Limit Units Level Result %REC Limits RPD Limit Note,
Batch B138303 - SW-946 3005A Dissolved
Blank (B138303-BLK1)
Manganese
LCS (B138303-BS1)
Manganese
LCS Dup (B138303-BSD1)
Prepared: 12/22/15 Analyzed: 12/23/15
ND 2.0 Rg/L
Prepared: 12/22/15 Analyzed: 12/23/15
250 5.0 Rg/L 250 99.9 80-120
Prepared: 12/22/15 Analyzed: 12/23/15
Manganese 251 5.0 Pg/L 250 100 80-120 0.418 20

con-atcsC'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APEWSW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Result Limit Units Level Result 0/6REC Limits RPD Limit Notes
Batch B138157 - SM 21-22 4500 NO2 B
Blank (B138157-BLKI)
Prepared & Analyzed: 12/18/15
Nitrite as N
LCS (B138157-BS1)
ND
0.010
mg/L
PrepaTed &Analyzed: 12/18/15
Nitrite as N
LCS Dup (111138157-BSDI.)
0.10
0.010
mg/L
0.100 101 90-111
Prepared &Analyzed: 12/18/15
Nitrite as N
Batch B138214 - SM21-22 450OS-F
0.10
0.010
mg/L
0.100 102 90-111 0.359 5.9
Blank (Bl38214-BLKI)
Prepared & Analyzed: 12/2 1/15
Sulfide
LCS (B138214-BS1)
ND
2.0
mg/L
Prepared & Analyzed: 12/21/15
Sulfide
Batch B138250 - SM19-22 4500 NH3 C
15
2.0
mg/L
14.8 100 60.3-119
Blank (B138250-BLKI)
Prepared: 12/22/15 Analyzed: 12/23/15
Ammonia as N
LCS (B138250-BS1)
ND
0.30
mg/L
Prepared: 12/22/15 Analyzed: 12/23/15
Ammonia as N
LCS Dup (8138250-BSD1)
4.8
0.30
mg/L
5.00 95.2 82-106
Prepared: 12/22/15 Analyzed: 12/23/15
Ammonia as N
Duplicate (B138250-DUP2)
4.6 0.30
Source: 15L0991-01
mg1L
5.00 92.4 82-106 2.99 8.24
Prepared: 12/22/15 Analyzed: 12/23YIS
Ammonia as N
Matrix Spike (B138250-MS2)
ND 0.30
Source: 15LO991-01
mg/L
ND NC 34.8
Prepared: 12/22/15 Analyzed: 12/23/15
Ammonia as N
Batch B138306 - ASTM D516-07
2.1
0.30
mg/L
2.00 ND 105 71.6-116
Blank (Bl38306-BLKI)
Prepared & Analyzed: 12/22/15
Sulfate
LCS (B138306-BS1)
ND
2.0
mg/L
Prepared & Analyzed: 12/22/15
Sulfate
21
2.0
1119/1-
20.0 104 83.8-123

con-test'g'
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHAISW-846 Methods (Total) - Quality Control
Reporting Spike Source 0/6REC RPD
Analyte Result Limit Units Level Result I/ouc Limits "D Limit Notes
Batch B138306 - ASTM D516-07
LCS Dup (Bl38306-BSDI)
Prepared & Analyzed: 12/22/15
Sulfate
Batch B138312 - SM 21-22 4500 NO3 F
21
2.0
-9/1-
20.0 105 83.8-123 1.05 8.27
Blank (11138312-BLIKI)
Prepared: 12/22/15 Analyzed: 12/23/15
Nitrate as N
LCS (B139312-BSI)
ND
0.050
mg/L
Prepared: 12/22/15 Analyzed: 12/23/15
Nitrate as N
LCS Dup (Bl383l2-BSD1)
4.6
mg/L
4.27 108 88.9-111
Prepared: 12/22/15 Analyzed: 12/23/15
Nitrate as N
Batch B138422 - SM 5310C
4.6
mg/L
4.27 108 88.9-111 0.00 5.66
Blank (Bl38422-BLK1)
Prepared& Analyzed: 12/23/15
Total Organic Carbon
LCS (B138422-BSI)
ND
0.50
mg1L
Prepared& Analyzed: 12/23/15
Total Organic Carbon
LCS Dup (B138422-BSDI)
10.5
0.50
mg/L
10.0 105 90.1-114
Prepared& Analyzed: 12/23/15
Total Organic Carbon
10.3
0.50
-9/1-
10.0 103 90.1-114 1.85 7.72

0 con -test"
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFEER SUMMARY
QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
RL
Reporting Limit
DL
Method Detection Limit
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).

0 con-tEsto
ANALYTiCAL LABORATORY
39 Spruce Street* East Longmeadow, MAO 1028 *FAX [phone]* TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
3810-RSKI 75 in Water
Ethane
VANYME
Ethene
VA,NYME
Methane
VA,NYME
ASTMD516-07in Water
Sulfate
NYNHMA,CTR1,VANC
SM 21-22 4500 NO2 B in Water
Nitrite as N
CTNHNYMENC,VARI
SM 21-22 4500 NO3 F in Water
Nitrate as N
CTMANH,NYR1,MENCVA
SM 531 OC in Water
Total Organic Carbon
NYNC,CTR1,MF,MA,VA
SM19-22 4500 NH3 C in Water
Ammonia as N
NYMA,CTR1,VANC,ME
SMII-22 450OS-F in Water
Sulfide
CTNHNYR1,NC,ME,VA
SW-846 6020A in Water
Manganese
CTNHNYNC,MEVA
Manganese
CTNHNYNC,MEVA
SW-846 8260B in Water
Acetone
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Bromofiarm
NC
Bromomethane
NC
2-Butanone (MEK)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluenc
NC
4-Chlorotoluene
NC
1,2-Dibromoethane (EDB)
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
Dichlorodifluoromethane (Freon 12)
NC

con -test"
ANALYTICAL LABORATORY
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone]* TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Anslyte Certifications
SW-846 8260B in Water
lj-Dichloroethane
NC
1,2-Dichloroethane
NC
I,I-Dichloroethylene
NC
cis- 1,2-Dichloroethylenc:
NC
tmns-1,2-Dichloroethylene
NC
1,2-Dichloropropane
NC
1,3-Dichloropropane
NC
2,2-Dichloropropane
NC
1, 1 -Dichloropropene
NC
cis- 1,3-Dichloropropene
NC
trans- 1,3-Dichloropropene
NC
Diisopropyl Ether (DIPE)
NC
Ethylbenzene
NC
2-Hcxanonc (M13K)
NC
Isopropylbenzene (Curnene)
NC
p-Isopropyltoluiene (p-Cymene)
NC
Methyl tert-Butyl Ether (MTBE)
NC
Methylene Chloride
NC
4-Methyl-2-pentanone (NHBK)
NC
Naphthalene
NC
n-Propylbenzene
NC
Styrene
NC
1, 1,2,2-Tetrachloroethane
NC
Tetrachloroethylene
NC
Toluene
NC
1,2,3-Trichlorobenzene
NC
1,2,4-Trichlorobenzene
NC
1, 1, 1 -Trichloroethane
NC
1, 1,2-Trichloroethane
NC
Trichloroethylene
NC
Trichlorofluorornethane (Freon 11)
NC
1,2,3-Trichloropropane
NC
1,2,4-Trimethylbenzene
NC
1,3,5-Trimethylbenzene
NC
Vinyl Acetate
NC
Vinyl Chloride
NC
m+p Xylene
NC
o-Xylene
NC

con -tor
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413t525-6405 * TEL. [phone]
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIRA
AIHA-LAP, LLC
100033
02/1/2016
MA
Massachusetts DEP
M-MAIOO
06/30/2016
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2017
NY
New York State Department of Health
10899 NELAP
04/1/2016
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2016
RI
Rhode Island Department of Health
LAOOO 112
12/30/2015
NC
North Carolina Div. of Water Quality
652
12/31/2015
NJ
New Jersey DEP
NUO07 NELAP
06/30/2016
Fl,
Florida Department of Health
E871027 NELAP
06/30/2016
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2016
WA
State of Washington Department ofEcology
C2065
02/23/2016
ME
State of Maine
2011028
06/9/2017
VA
Commonwealth of Virginia
460217
12/14/2016
NH-P
New Hampshire Environmental Lab
2557 NELAP
0916/2016

Phone: [phone] CHAIN OF CUSTODY RECORD
conwtesr Fax: [phone]
Email: [e-mail] (IfN
op ANALYTICAL LABORATORY http://www.contestlabs.com ISL,099 I -z
Company Name:AT C, Telephone: qiq 611_oqqq �,D
I jct# (19-01 St 33
Address: 2- 1 -157 E lircolc 4, st,4e, I 0-1p-ro
,0_,:�,4ei �1\_ /V 16 0 q Client PON
Attention: Tv_A1.t\- 6a_11--zreW_- DATA DELIVERY (check all that ap,
0 FAX *EMAIL OWESSITE
Project Location: P_ezJef� 96 1$
Sampled By: C , No b / e-,: �, 121 - d, e t, 150,1i'z4g
Project Proposal Provided? (for billing purposes) Format: 6PDF *EXCEL OGIS
0 yes proposal date A- 0 OTHER
Collection 0 "Enhanced Data Package"
Con -Test Lab ID
ilaboratory �e only)
Client Sample ID Description
4ft-9-
DatehT+me-
_f_ftrT_
-&etr�Time
Composite
Grab
*Matrix
Code
Conc
Code
r7
tie)
(5
k * i
) ic A
Relinquished byi (signat
Dp.e/ ime;
Turnaround
Detection
Limit RgqMjtqMgrLt
14JC)
0 5-Day
0 5-7-Day
North Carolina
4D 2L
RKIved by: (�vgpatur
Date/Time:
tyl -7/1 :) A�J
0 10�Day
RUSH
0 GWPC
0 swst
Date/Time:
t�lj 7/05' "'I
0 '24-Hr r'48-Hr
0 '72-Hr r'4-Day
0 OTHER
RecON9 by: (signature)
iDate/Time:
-CA,
Requires Lab Approval
39 Spruce Street
East Longmeadow, MA 01028
Anaiysis
- 14
co
S,
Page ) Of I
# of Containers
** Preservation
***Container Code
Dissolved Metals
0 Field Filtered
0 Lab to Filter
** *Cent. Code:
A=amber glass
G=glass
P=plastic
ST=sterile
V= vial
S=summa can
T--tedlar bag
O=Other
"Preservation
I = Iced
H HCL
M Methanol
N Nitric Acid
S Sulfuric Acid
B Sodium bisulfate
X Na hydroxide
T Na thlosulfate
0 Other
*Matrix Code:
GW= groundwater
[T -J I WW= wastewater
Please use the following codes to let Con -Test know if a specific sample may be high DW= drinking water
in concentration in Matrix/Conc. Code Box: A= air
.................. I ............................................................................. .................... ........................ S = soil/solid
H - High; M - Medium; L - Low; C - Clean; U - Unknown SL = sludge
- 1 0 h
Program Information
0 DSCA 0 IHSB Orphaned Landfill
0 SWS Landfill 0 UST 0 REC
0 Other:
AIHA
NELAC & AIHA Certified
WBE/DBE Certified
TURNAROUNb TIME (busineis days) STARTS AT 9-.06 A.M. THE DAY AFTER SAMPLE RECEIPT UNLESS THERE ARE QUESTIONS ON YOUR CHAIN.
IF THIS FORM IS NOT FILLED OUT COMPLETELY OR IS INCORRECT, TURNAROUND TIME WILL NOT START UNTILAU. QUESTIONS ARE ANSWERED. PLEASE BE CAREFUL NOT TO CONTAMINATE THIS DOCUMENT

12/W2015
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39 Spruce St.
East Longmeadow, MA 01028
P: 413-525-2332
F: 413-525-6405
www.contestiabs.com
CLIENT NAME:
i) Was the chain(s) of custody relinquished and signed?
2) Does the chain agree with the samples?
If not, explain:
3) Are all the samples in good condition?
If not, explain:
No No CoC Included
No
(YLes__) No
4) How were the samples received:
On Ice E�-' Direct from Sampling Ambient F1 In Cooler(s)
Were the samples received in Temperature Compliance of (2-6*C)? ce-!,� No NIA
,--;. , C-
Temperature *C by Temp blank Temperature *C by Temp gun
6) Are there Dissolved samples for the lab to filter? Yes 2N_�I
Who was notified Date Time �Yes No
6) Are there any RUSH or ORT HOLDING'TI!4E samples?
Who was notified LC jC' Date Time - Permission to subcontract samples? Yes No
7) Location where samples are stored: (Walk-in clients only) if not already approved
,Client Signat, —
8) Do all samples have the proper Acid pH: (:�4s' No N/A
9) Do all samples have the proper Base pH: (Ee; _-, No N/A
-1 - - ----- I �- ^ .._ 41,­ --- 1�a- Vae- Nn rNIA
iu) was ine r-%j nutilivu %if 41
Containers received at -Con -Test
# of containers
8 oz amber/clear'
j2r-
4 oz am ber/clear jar
# of containers
1 Liter Amber
500 mL Amber
250 mL Amber �8oz amber)
2 oz amber/clear iar
1 Liter Plastic
Plastic Bag / Ziploc
500 mL Plastic
SOC Kit
250 mL plastic
Non-ConTest Container
40 mL Vial - type listed below
Perchlorate Kit
Flashpoint bottle
Colisure / bacteria bottle_
Other glass jar
Dissolved Oxygen bottle
Encore
Other
Laboratory Comments:
40 mL vials: # HCI k # Methanol
........ ....
. ...... # Bisulfate # DI Water
... ............ .. ..
Time and Date Frozen:

Page 2 of 2
Login Sample Receipt Checklis
(Rejection Criteria Listing - Using Sample Acceptance Policy)
Any False statement will be brought to the attention of Client
Question
1) The cooler's custody seal, if present, is intact.
Answer (Truel..... I
T/F/NA
2) The cooler or samples do not appear to have
been compromised or tampered with.
3) Samples were received on ice.
4) Cooler Temperature is acceptable.
5) Cooler Temperature is recorded.
6) COC is filled out in ink and legible.
7) COC is filled out with all pertinent information.
8) Field Sampler's name present on COC.
9) There are no discrepancies between the
sample IDs on the container and the COC.
10) Samples are received within Holding Time.
11) Sample containers have legible labels.
_T
Containers are not broken or leaking.
_T
13) Air Cassettes are not broken/open.
14) Sample collection date/times are provided.
15) Appropriate sample containers are used.
_T
16) Proper collection media used.
_T
17) No headspace sample bottles are completely filled.
18) There is sufficient volume for all requsted
analyses, including any requested MS/MSDs.
_T
19) Trip blanks provided if applicable.
I\"A
20) VOA sample vials do not have head space or
bubble is <6mm (1/4") in diameter.
21) Samples do not require splitting or compositing.
Who notified of False statements? Daterrime:
Doc #277 Rev. 4 August 2013 Log -in Technician Initials: Date/Time:
iM k& � C2�3 � QJ\

Table of Contents
con-test08
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 23, 2015
Justin Ballard
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: 8377 Creedmoor Road, Raleigh, NC
Client Job Number:
Project Number: DC92015L33
Laboratory Work Order Number: 15LO909
Enclosed are results of analyses for samples received by the laboratory on December 16, 2015. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
. �-' �V�'V�
Lisa A. Worthington
Project Manager
Pagel of2721

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
15LO909-01
15LO909-02
15LO909-03
Sample Preparation Information
QC Data
Volatile Organic Compounds by GUMS
B138109
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
7
9
11
12
12
12
16
17
19
I Page 2 =of22=]

con-tfst"
ANALYTICAL LABORATORY
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Justin Ballard
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
PURCHASE ORDER NUMBER:
PROJECT NUMBER: DC92015L33
ANALYTICAL SUMMARY
Table of Contents
REPORT DATE: 12/23/2015
WORK ORDER NUMBER: 15LO909
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 8377 Creedmoor Road, Raleigh, NC
FIELD SAMPLE #
LAB ID:
MATRIX SAMPLE DESCRIPTION
TEST SUB LAB
Prc-Carbon
15LO909-01
Water
SW-846 8260B
Mid -Carbon
15L0909-02
Water
SW-846 8260B
Post -Carbon
15LO909-03
Water
SW-846 8260B
I Page 3

Table of Contents
con-testo't
ANALYTiCAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
FA�IIEZDIEKIIE
Qualifications:
L,04
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside ofcontrol limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
Dichlorodifluoramediane (Freon 1:
15LO909-OI[Pre-Carbon], 15LO909-02[Mid-Carbon], 15LO909-03[Post-Carbon], B138109-BLKI, B138109-BSI, B138109-BSDI
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, ifany, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best ofmy knowledge and belief, accurate and complete.
Johanna K. Harrington
Manager, Laboratory Reporting
I Page 4

Table of Contents
con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] TEL. [phone]
Project Location: 8377 Creedmoor Road,
Raleigh, N
Sample Description:
Work Order: 15LO909
Date Received: 12/16/2015
Field Sample #: Pre -Carbon
Sampled: 12/16/2015
15:25
S2mDle ID: ISLO909-01
Samnle Matrix: Water
Volatile Organic Compounds by GC/MS
Date
Dateffime
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared Analyzed
Analyst
Acetone
ND
0.050
0.0049
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Benzene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Bromobenzene
ND
0.0010
0.00015
-g/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Bromochloromethane
ND
0.0010
0.00022
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
n-Butylbenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
sec-Butylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
text-Butylbenzene
ND
0.0010
0.00011
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Carbon Disulfide
ND
0.0040
0.0010
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:51
EEH
Carbon Tetrachloride
ND
0.0050
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Chlorobenzenc
ND
0.0010
0.00016
-9/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Chlorodibromomethane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Chloroethane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Chloroform
ND
0.0020
0.00022
-g/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Chloromcthane
ND
0.0020
0.00032
Ing/L
I
SW-946 8260B
12/20/15
12/20/15 23:51
EEH
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
4-Chlorotoluene
ND
0.0010
0.00014
mgA-
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,2-Dibromoethane (EDB)
ND
0.00050
0.00012
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,2-Dichlorobenzenc
ND
0.0010
0.00017
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,4-Dichlorobenzene
ND
0.0010
0.00015
n1g/L
I
SW-846 8260B
12/20115
12/20/15 23:51
EEH
Dichlorodifluoromcthane (Freon 12)
ND
0.0020
0.00018
mg/L
1 L-04
SW-846 8260B
l2t20115
12/20/15 23:51
EEH
I,I-Dichloroctliane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1, I-Dichloroethylene
0.00058
0.0010
0.00021
mg/L
I J
SW-846 8260B
12/20115
12/20/15 23:51
EEH
cis- 1,2-Dichloroethylene
0.13
0.0010
0.00015
mg/L
I
SW-846 8260B
l2t20/15
12/20/15 23:51
EEH
trarLs- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
l2t20/15
12/20/15 23:51
EEH
1,3-Dichloropropane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
2,2-Dichloropropane
ND
0.0010
0.00016
n1g/L
I
SW-846 8260B
l2t20/15
12/20/15 23:51
EEH
I,I-Dichloropropenc
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
cis- 1,3-Dichloropropene
ND
0.00050
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
-9/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
2-Hexanonc (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
lsopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
p-isopropyltoluene (p-Cymene)
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:51
EEH
Methylene Chloride
ND
0.0050
0.0032
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
4-Methyl-2-pentanone (MlBK)
ND
0.010
0.0015
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
I Page 5

Table of Contents
con -tor
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8377 Crecdmoor Road, Raleigh, N Sample Description: Work Order: 15LO909
Date Received: 12/16/2015
Field Sample#: Pre -Carbon Sampled: 12/16/2015 15:25
Samnic ID: 15LO909-01
Samole Matrix: Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
n-Propylbenzene
ND
0.0010
0.00013
mg/L
I
SW-946 9260B
12/20/15
12/20/15 23:51
EEH
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1, 1,2,2-Teti2chlorocthanc
IND
0.00050
0.00016
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Tetrachloroethylenc
0.00064
0.00050
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Toluene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
Ing/L
I
SW-846 8260B
12/20115
12/20/15 23:51
EEH
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:51
EEH
1, I,I-Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1, 1,2-Trichloroediane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Trichloroethylene
ND
0.0010
0.00020
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,2,3-Tricliloropropanc
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
1,3,5-Trimethylbenzene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Vinyl Acetate
ND
0.020
0.0014
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Vinyl Chloride
0.00045
0.0020
0.00013
mg/L
I J
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
o-Xylene
0.0010
0.00013
mg/L
I J
SW-846 8260B
12/20/15
12/20/15 23:51
EEH
Surrogates % Recovery Recovery Limits Flag/Qua]
1,2-Dichloroetliane-d4 105 70-130 12/20/15 23:51
Toluene-d8 100 70-130 12/20/15 23:51
4-Bromofluorobenzene %.7 70-130 12/20/15 23:51
I Page 6

Table of Contents
con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8377 Creedmoor Road, Raleigh, N Sample Description: Work Order: 15LO909
Date Received: 12/16/2015
Field Sample #: Mid -Carbon Sampled: 12/16/2015 15:35
Sample ID.- 15L0909-02
Sample Matrix: Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
R1,
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Benzene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Bromochloromethane
ND
0.0010
0.00022
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Bromodichloromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/20115
12/20/15 22:58
EEH
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:59
EEH
2-Butanone (MEK)
0.0063
0.020
0.0024
mg/L
I J
SW-946 8260B
12/20/15
12/20/15 22:58
EEH
n-Butylbenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
sec-Butylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
tert-Butylbenzene
IND
0.0010
0.00011
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Carbon Disulfide
ND
0.0040
0.0010
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Carbon Tetrachloride
ND
0.0050
0.00012
Ing/L
I
SW-846 8260B
12/20/15
12120/15 22:58
EEH
Chlorobenzene
ND
0.0010
0.00016
-9/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Cl-dorodibromomediane
ND
0.00050
0.00010
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Chloroethane
ND
0.0020
0.00028
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Chloroform
ND
0.0020
0.00022
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Chloromethane
NID
0.0020
0.00032
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
4-Chlorotoluene
NID
0.0010
0.00014
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,2-Dibromoediane (EDB)
ND
0.00050
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,2-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,4-Dichlorobenzene
NID
0.0010
0.00015
-811L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
Ing/L
I IL-04
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1, I-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,2-Dichloroediane
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
IJ-Dichoroedlykne
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
cis- 1,2-Dichloroedlytene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
trans- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,2-Dichloropropane
NID
0.0010
0.00013
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,3-Dichloropropane
ND
0.00050
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
2,2-Dichloropropane
NID
0.0010
0.00016
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
I,I-Dichloropropcne
ND
0.0020
0.00013
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
cis- 1,3-Dichloropropene
ND
0.00050
0.00012
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
ums-1,3-Dichloropropene
ND
0.00050
0.00011
mg/1-
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/1-
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Ethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
2-Hexanone (MEK)
IND
0.010
0.0015
mg/1-
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
lsopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
p-Isopropyltoluene (p-Cymene)
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Methylene Chloride
ND
0.0050
0.0032
mg/1-
I
SW-946 8260B
12/20/15
12/20/15 22:58
EEH
4-Mediyl-2-pentanone (MIBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
I Page 7

Table of Contents
con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 8377 Creedmoor Road, Raleigh, N Sample Description: Work Order: 15LO909
Date Received: 12/16/2015
Field Sample #: Mid -Carbon Sampled: 12/16/2015 15:35
Sample ID: 15LO909-02
Samole Matrix: Water
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
n-Propylbenzene
ND
0.0010
0.00013
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Styrene
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:58
EEH
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00016
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Tetrachloroethylene
ND
0.00050
0.00017
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Toluene
ND
0.0010
0.00017
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,2,3-Trichlorobenzene
ND
0.0050
0.00014
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:58
EEH
1,2,4-Trichlorobenzene
ND
0.0010
0.00019
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,1,1-Trichloroedianc
ND
0.0010
0.000094
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1, 1,2-Trichloroediane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Trichloroethylene
ND
0.0010
0.00020
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
mg/1-
I
SW-946 8260B
12/20/15
12/20/15 22:58
EEH
1,2,3-Trichloropropane
ND
0.0020
0.00019
-9/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:58
EEH
1,3,5-Trimethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
m+p Xylenc
ND
0.0020
0.00025
mg/L
I
SW-846 8260B
12/20/15
12/20/15 22:58
EEH
o-Xylene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 22:58
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroediane-d4
107
70-130
12/20/15 22:58
Toluene-d8
102
70-130
12/20/15 22:58
4-Bromofluorobenzene
98.6
70-130
12/20/15 22:58
I Page 8 of 22 1

Table of Contents
con-tEW
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/52&6405 * TEL. [phone]
Project Location: 8377 Creedmoor Road, Raleigh, N Sample Description: Work Order: 15LO909
Date Received: 12/16/2015
Field Sample #: Post -Carbon Sampled: 12/16/2015 15:45
Samnle ID: 15LO909-03
SarnDle Matrix: Water
Volatile Organic Compounds by GUMS
Date
DatelTime
Analyte
Results
RL
DL
Units
Dilution Flag/Qua]
Method
Prepared
Analyzed
Analyst
Acetone
ND
0.050
0.0049
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Benzene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Bromobenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Bromochloromethane
ND
0.0010
0.00022
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Bromodichoromethane
ND
0.00050
0.000088
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Bromoform
ND
0.0010
0.00021
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Bromomethane
ND
0.0020
0.00094
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
2-Butanone (MEK)
ND
0.020
0.0024
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
n-Butylbenzene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
sec-Butylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
tert-Butylbenzene
ND
0.0010
0.00011
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Carbon Disulfide
ND
0.0040
0.0010
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Carbon Tetrachloride
ND
0.0050
0.00012
-91L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Chlorobenzene
ND
0.0010
0.00016
-A
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
Chlorodibromomethane
ND
0.00050
0.00010
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Chloroethane
ND
0.0020
0.00028
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Chloroform
ND
0.0020
0.00022.
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Chloromethanc
ND
0.0020
0.00032
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
2-Chlorotoluene
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
4-Chlorotoluene
ND
0.0010
0.00014
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,2-Dibromoethane (EDB)
ND
0.00050
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,2-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,3-Dichlorobenzene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,4-Dichlorobenzene
ND
0.0010
0.00015
Ing/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Dichlorodifluoromethane (Freon 12)
ND
0.0020
0.00018
-9/1-
1 L-04
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
IJ-Dichloroethane
ND
0.0010
0.00016
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,2-Dichloroethane
ND
0.0010
0.00019
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
IJ-Dichloroethylene
ND
0.0010
0.00021
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
cis- 1,2-Dichloroethylene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
trans- 1,2-Dichloroediylcne
ND
0.0010
0.00015
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
1,2-Dichloropropane
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
1,3-Dichloropropane
ND
0.00050
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
2,2-Dichloropropane
ND
0.0010
0.00016
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
IJ-Dichloropropene
ND
0.0020
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
cis- 1,3-Dichloropropene
ND
0.00050
0.00012
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
trans- 1,3-Dichloropropene
ND
0.00050
0.00011
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
Diisopropyl Ether (DIPE)
ND
0.00050
0.00018
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Ethylbenzene
ND
0.0010
0.00013
-9/1-
1
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
2-Hexanone (MBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Isopropylbenzene (Cumene)
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
p-lsopropyltoluene (p-Cymene)
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.0010
0.000090
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Methylene Chloride
ND
0.0050
0.0032
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
4-Methyl-2-pentanone (NHBK)
ND
0.010
0.0015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
I Page 9

Table of Contents
con-stor
ANALYTICAL LABORATORY
39 Spruoe Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. 413/52&2332
Project Location: 8377 Creedmoor Road, Raleigh, N Sample Description: Work Order: 15LO909
Date Received: 12/16/2015
Field Sarnple*: Post -Carbon Sampled: 12/16/2015 15:45
S2MDie ID: 15LO909-03
Sanmle Matrix: Water
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/QuAl
Method
Prepared
Analyzed
Analyst
Naphthalene
ND
0.0020
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
n-Propylbenzene
ND
0.0010
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
Styrene
ND
0.0010
0.00015
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1, 1,2,2-Tetrachloroethane
ND
0.00050
0.00016
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Tetrachloroethylene
ND
0.00050
0.00017
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Toluene
ND
0.0010
0.00017
mg/L
I
SW-846 8260B
12/20115
12/20/15 23:24
EEH
1,2,3-TricMorobenzene
ND
0.0050
0.00014
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,2,4-Tricldorobenzene
ND
0.0010
0.00019
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
1, 1, 1 -Trichloroethane
ND
0.0010
0.000094
mg/L
I
SW-846 9260B
12/20/15
12/20/15 23:24
EEH
1, 1,2-Trichloroethane
ND
0.0010
0.00012
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Trichloroethylene
ND
0.0010
0.00020
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Trichlorofluoromethane (Freon 11)
ND
0.0020
0.00015
-8/1-
1
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,2,3-TricMoropropane
ND
0.0020
0.00019
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,2,4-Trimethylbenzene
ND
0.0010
0.00018
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
1,3,5-Trimethylbenzene
ND
0.0010
0.00013
mg/L
I
SW-846 8260B
12/20/15
12/20/15 23:24
EEH
Vinyl Acetate
ND
0.020
0.0014
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
Vinyl Chloride
ND
0.0020
0.00013
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
m+p Xylene
ND
0.0020
0.00025
mg/L
I
SW-946 8260B
12/20/15
12/20/15 23:24
EEH
o-Xylenc
ND
0.0010
0.00013
Ing/L
I
SW-W 8260B
12/20/15
12/20/15 23:24
EEH
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethanc-dil 106 70-130 12/20/15 23:24
Toluene-d8 101 70-130 12/20/15 23:24
4-Brornofluorobenzene 98.7 70-130 12/20/15 23:24
I Page 10

Table of Contents
con-testO
ANALYTICAL LABORATORY
39 Spruce Street - East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 503OB-SW-846 8260B
Lab Number [Field ID] Batch Initial [mL] Final [mLl Date
15LO909-01 [Pre -Carbon)
B 138109
5
5.00
12/20/15
15LO909-02 [Nfid-Carbon]
B 138109
5
5.00
12/20/15
15LO909-03 [Post -Carbon]
B 138109
5
5.00
12/20/15
I Page 11 of

Table of Contents
con-tcst'9
ANALYTICAL LABORATORY
Batch B138109 - SW-846 5030B
Blank (111138109-BLKI)
Acetone
Benzene
Bromobenzene
Bromochloromediane
Bromodichloromethane
Bromoforin
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chlorodibromomediane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzenc
Dichlorodifluoromethane (Freon 12)
IJ-Dichloroethane
1,2-Dichloroediane
I,I-Dichloroethylene
cis- U-Dichloroethylene
trans- 1,2-Dichloroethylene
1,2-Dichloropropane
1,3-Dieliloropropane
2,2-Dichloropropane
IJ-Dichloropropene
cis- 1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl Ether (DIPE)
Ethylbenzene
2-Hcxanone (MBK)
lsopropylbenzene (Cumene)
p-lsopropyltoluene (p-Cymene)
Methyl tert-Butyl Ether (MTBE)
Methylene Chloride
4-Methyl-2-pentanone (MlBK)
Naphthalene
n-Propylbcnzene
Styrene
1, 1,2,2-Tetrachloroethane
Tetrachloroethylene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source */oREC RPD
Result Limit Units Level Result G/oREC Limits RPD Limit Notes
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
IND
ND
ND
IND
ND
ND
ND
ND
ND
IND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MD
ND
ND
ND
ND
ND
0.050 m9/1-
0.0010 mg/L
0.0010 mg/L
0.0010 mg/L
0.00050 mg/L
0.0010 mg/L
0.0020 mg/L
0.020 mg/1-
0.0010 mg/1-
0.0010 Ing/L
0.0010 mg/L
0.0040 mg/L
0.0050 mg/L
0.0010 mg/L
0.00050 mg/L
0.0020 -19/1-
0.0020 mg/L
0.0020 mg/L
0.0010 mg/L
0.0010 mg/L
0.00050 Ing/L
0.0010 mg/1-
0.0010 mg/1-
0.0010 mg/1-
0.0020 Ing/L
0.0010 mg/L
0.0010 mg/L
0.0010 mg/L
0.0010 Ing/L
0.0010 mg/L
0.0010 mg/L
0.00050 mg/L
0.0010 Mg/L
0.0020 mg/1-
0.00050 -9/1-
0.00050 mg/L
0.00050 mg/L
0.0010 m9/1-
0.010 mg/L
0.0010 -19/1-
0.0010 -9/1-
0.0010 1119/1-
0.0050 mg/L
0.010 mg/L
0.0020 mg/1-
0.0010 mg/L
0.0010 mg/L
0.00050 Ing/L
0.00050 mg/L
0.0010 mg/L
0.0050 mg/L
0.0010 Ing/L
prepared & Analyzed: 12/20/15
L-04
I Page 12 of 22 1

Table of Contents
con-tot"o
ANALYTICAL LABORATORY
39 Sprure Street * East Longmeadow, MA 01028 * FAX [phone] * TEL [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source */.REC RPD
Lnalyte Result Limit Units Level Result */oREC Limits RPD Limit Notc,
Batch B138109 - SW-946 5030B
Blank (B138109-BLKI)
Prepared & Analyzed: 12/20/15
1,1,]-Trichloroediane
ND
0.0010
mg/L
1, 1,2-Trichloroethane
ND
0.0010
mg/L
Trichloroethylene
ND
0.0010
mg/L
Trichlorofluoromediane (Freon 11)
IND
0.0020
mg/L
1,2,3-Trichloropropane
ND
0.0020
mg/L
1,2,4-Trimethylbenzene
IND
0.0010
m9/1-
1,3,5-Trimcdiylbenzene
ND
0.0010
mg/L
Vinyl Acetate
ND
0.020
mg/L
Vinyl Chloride
IND
0.0020
mg/L
m+p Xylene
ND
0.0020
mg/L
o-Xylene
ND
0.0010
mg/L
Surrogate: 1,2-Dichloroethane-d4
Surrogate: Toluene-d8
Surrogate: 4-Bromofluorobenzene
LCS (B139109-BS1)
0.0265
0.0250
0.0240
mg/L
mg/L
mg/L
0.0250 106
0.0250 99.9
0.0250 95.9
prepared & Analyzed: 12/20/15
70-130
70-130
70-130
Acetone
0.0849
0.050
mg/L
0.100
94.9
70-160
Benzene
0.0106
0.0010
mg/L
0.0100
106
70-130
Bromobenzene
0.0101
0.0010
mg/L
0.0100
101
70-130
Bromocliloromcthane
0.0121
0.0010
mg/L
0.0100
121
70-130
Bromodichloromethane
0.00967
0.00050
mg/L
0.0100
96.7
70-130
Bromoform
0.00891
0.0010
mg/L
0.0100
89.1
70-130
Bromomethane
0.00727
0.0020
mg/L
0.0100
72.7
40-160
t
2-Butanone (MEK)
0.108
0.020
mg/L
0.100
108
40-160
t
n-Butylbenzene
0.00982
0.0010
mg/L
0.0100
98.2
70-130
sec-Butylbenzene
0.0103
0.0010
-9/L
0.0100
103
70-130
tert-Butylbenzene
0.00971
0.0010
mg/L
0.0100
97.1
70-130
Carbon Disulfide
0.00946
0.0040
1119/1-
0.0100
94.6
70-130
Carbon Tetrachloride
0.0102
0.0050
-9/L
0.0100
102
70-130
Chlorobenzenc
0.00955
0.0010
mg/L
0.0100
95.5
70-130
Chlorodibromomediane
0.00937
0.00050
mg/L
0.0100
93.7
70-130
Chloroethane
0.0104
0.0020
mg/L
0.0100
104
70-130
Chloroform
0.0105
0.0020
mg/L
0.0100
105
70-130
Chloromethane
0.00829
0.0020
mg/L
0.0100
82.9
40-160
2-Chlorotoluene
0.00960
0.0010
mg/L
0.0100
96.0
70-130
4-Chlorotoluene
0.00988
0.0010
-9/1-
0.0100
98.8
70-130
1,2-Dibromoediane (EDB)
0.0105
0.00050
mg/L
0.0100
105
70-130
1,2-Dichlorobenzene
0.00939
0.0010
-9/1-
0.0100
93.9
70-130
1,3-DicliJorobenzene
0.00967
0.0010
mg/L
0.0100
96.7
70-130
1,4-Dichlorobenzene
0.00905
0.0010
mg/L
0.0100
90.5
70-130
Dichlorodifluoromethane (Freon 12)
0.00372
0.0020
mg/L
0.0100
37.2
40-160
L-04
IJ-Dichloroethanc
0.0109
0.0010
mg/L
0.0100
109
70-130
1,2-Dichlorocdiane
0.00989
0.0010
mg/L
0.0100
98.9
70-130
1,11-Dichloroctilylenc:
0.0101
0.0010
mg/L
0.0100
101
70-130
cis- 1,2-Dichloroethylene
0.0107
0.0010
mg/L
0.0100
107
70-130
traro, 1,2-Dichlorocthylene
0.0102
0.0010
mg/L
0.0100
102
70-130
1,2-Dichloropropane
0.0102
0.0010
mg/L
0.0100
102
70-130
1,3-Dichloropropanc
0.0102
0.00050
mg/L
0.0100
102
70-130
2,2-Dichloiropropanc
0.00872
0.0010
-9/L
0.0100
87.2
40-130
I,I-Dichloropropenc
0.0104
0.0020
mg/L
0.0100
104
70-130
cis- 1,3-Dichloropropene
0.00893
0.00050
1119/1-
0.0100
89.3
70-130
trans- 1,3-Dichloropropene
0.00949
0.00050
mg/L
0.0100
94.9
70-130
I Page 13 of 22 1

Table of Contents
con-Usto
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source O/oREC RPD
Lnalyte Result Limit Units Level Result O/oREC Limits RPD Limit Notes
Batch B138109 - SW-846 5030B
LCS (B138109-BSI)
Prepared & Analyzed: 12/20/15
Diisopropyl Ether (DIPE)
0.00999
0.00050
Ing/L
0.0100
99.9
70-130
Ethylbenzene
0.00995
0.0010
Ing/L
0.0100
99.5
70-130
2-Hexanone (NMK)
0.104
0.010
Ing/L
0.100
104
70-160
lsopropylbenzenc (Cumene)
0.00978
0.0010
Ing/L
0.0100
97.8
70-130
p-lsopropyltoluene (p-Cymene)
0.0107
0.0010
Ing/L
0.0100
107
70-130
Methyl tert-Butyl Ether (MTBE)
0.00998
0.0010
-9/1-
0.0100
99.8
70-130
Methylene Chloride
0.0102
0.0050
Ing/L
0.0100
102
70-130
4-Methyl-2-pentanone (MIBK)
0.107
0.010
Ing/L
0.100
107
70-160 t
Naphthalene
0.00912
0.0020
Ing/L
0.0100
91.2
40-130 t
n-Propylbenzcnc
0.00993
0.0010
mg/L
0.0100
99.3
70-130
Styrene
0.00990
0.0010
Ing/L
0.0100
99.0
70-130
1, 1,2,2-Tetrachloroethanc
0.0107
0.00050
-9/1-
0.0100
107
70-130
Tetrachloroethylene
0.00966
0.00050
Ing/L
0.0100
96.6
70-130
Toluene
0.00998
0.0010
Ing/L
0.0100
99.8
70-130
1,2,3-Trichlorobenzene
0.00879
0.0050
Ing/L
0.0100
97.9
70-130
1,2,4-Trichlorobenzenc
0.00953
0.0010
mg/L
0.0100
95.3
70-130
1, 1, 1 -Tricliloroethane
0.0102
0.0010
Ing/L
0.0100
102
70-130
1, 1,2-Trichloroethane
0.0101
0.0010
Ing/L
0.0100
101
70-130
Trichloroethylene
0.0103
0.0010
Ing/L
0.0100
103
70-130
Trichlorofluoromethane (Freon 11)
0.00969
0.0020
Ing/L
0.0100
86.9
70-130
1,2,3-Trichloropropane
0.0106
0.0020
mg/L
0.0100
106
70-130
1,2,4-Trimethylbenzene
0.0101
0.0010
Ing/L
0.0100
101
70-130
1,3,5-Tzimethylbenzene
0.0103
0.0010
mg/L
0.0100
103
70-130
Vinyl Acetate
0.0922
0.020
Ing/L
0.100
92.2
70-130
Vinyl Chloride
0.00729
0.0020
Ing/L
0.0100
72.9
40-160
m+p Xylene
0.0198
0.0020
Ing/L
0.0200
99.2
70-130
o-Xylenc
0.00981
0.0010
mg/L
0.0100
98.1
70-130
Surrogate: 1,2-Dichloroethane-d4
0.0270
Mg/L
0.0250
108
70-130
Surrogate: Toluene-d8
0.0248
mg/L
0.0250
99.0
70-130
Surrogate: 4-Bromofluorobcnzene
0.0246
mg/L
0.0250
98.2
70-130
LCS Dup (B138109-BSDI)
Prepared & Analyzed: 12/20/15
Acetone
0.0945
0.050
Ing/L
0.100
94.5
70-160
0.555
Benzene
0.0102
0.0010
mg/L
0.0100
102
70-130
4.14
Bromobenzene
0.00982
0.0010
mg/L
0.0100
98.2
70-130
2.91
Brornochloromethane
0.0126
0.0010
mg/L
0.0100
126
70-130
3.80
Bromodichloromethane
0.00980
0.00050
mg/L
0.0100
98.0
70-130
1.34
Bromoform
0.00869
0.0010
mg/L
0.0100
86.9
70-130
2.50
Bromomethane
0.00721
0.0020
Ing/L
0.0100
72.1
40-160
0.829
2-Butanone (MEK)
0.109
0.020
-91L
0.100
109
40-160
0.926
n-Butylbenzene
0.00951
0.0010
mg/L
0.0100
95.1
70-130
3.21
sec-Butylbenzene
0.00975
0.0010
-9/1-
0.0100
97.5
70-130
5.78
tert-Butylbenzene
0.00940
0.0010
mg/L
0.0100
94.0
70-130
3.24
Carbon Disulfide
0.00892
0.0040
Ing/L
0.0100
89.2
70-130
5.88
Carbon Tetrachloride
0.0100
0.0050
mg/L
0.0100
100
70-130
2.17
Chlorobenzene
0.00912
0.0010
Mg/L
0.0100
91.2
70-130
4.61
Chlorodibromomethane
0.00923
0.00050
mg/L
0.0100
92.3
70-130
1.51
Chloroethane
0.0103
0.0020
mg/L
0.0100
103
70-130
0.867
Chloroform
0.0102
0.0020
mg/L
0.0100
102
70-130
3.77
Chloromethane
0.00830
0.0020
mg/L
0.0100
83.0
40-160
0.121
2-Chlorotoluene
0.00952
0.0010
mg/L
0.0100
95.2
70-130
0.837
4-Chlorotoluene
0.00943
0.0010
mg/L
0.0100
94.3
70-130
4.66
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25 +
25
25
1 Page 14
j

Table of Contents
con-stesto
ANALYTICAL LABOPATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source ONoREC RPD
nalyte Result Limit Units Level Result */oREC Limits RPD Limit Now,
Batch B138109 - SW-846 5030B
LCS Dup (B138109-BSDI) Prepared & Analyzed: 12/20/15
1,2-Dibromoediane (EDB)
0.0103
0.00050
mg/L
0.0100
103
70-130
2.50
25
1,2-Dichlorobenzene
0.00930
0.0010
mg/L
0.0100
93.0
70-130
0.963
25
1,3-Dichlorobenzenc
0.00953
0.0010
mg/L
0.0100
95.3
70-130
1.46
25
1,4-Dichlorobenzene
0.00913
0.0010
MA
0.0100
91.3
70-130
0.880
25
Dichlorodifluaromethane (Freon 12)
0.00375
0.0020
mg/L
0.0100
37.5
40-160
0.803
25
L-04 t
I,I-Dichloroethane
0.0105
0.0010
mg/L
0.0100
105
70-130
3.83
25
1,2-Dichloroediane
0.00970
0.0010
mg/L
0.0100
97.0
70-130
1.94
25
1,1-Dichloroediylene
0.00960
0.0010
MA
0.0100
96.0
70-130
4.68
25
cis- 1,2-Dichloroethylene
0.0102
0.0010
mg/L
0.0100
102
70-130
4.20
25
trans- 1,2-Dichlaroethylene
0.00976
0.0010
mg/L
0.0100
97.6
70-130
4.41
25
1,2-Dicliloropropane
0.0103
0.0010
mg/L
0.0100
103
70-130
0.585
25
1,3-Dichloropropane
0.00999
0.00050
mg/L
0.0100
99.9
70-130
2.37
25
2,2-Dicliloropropane
0.00819
0.0010
mg/L
0.0100
81.9
40-130
6.27
25
t
I,I-Dichloropropenc
0.00990
0.0020
mg/L
0.0100
99.0
70-130
5.21
25
cis- 1,3-Dichloropropene
0.00879
0.00050
mg/L
0.0100
87.9
70-130
1.58
25
hms-1,3-Dichloropropene
0.00962
0.00050
mg/L
0.0100
96.2
70-130
1.36
25
Diisopropyl Ether (DIPE)
0.00995
0.00050
mg/L
0.0100
99.5
70-130
0.401
25
Ethylbenzene
0.00976
0.0010
Ing/L
0.0100
97.6
70-130
1.93
25
2-Hexanonc (MBK)
0.105
0.010
mg/L
0.100
105
70-160
1.40
25
t
lsopropylbenzene (Cumene)
0.00941
0.0010
mg/L
0.0100
94.1
70-130
3.86
25
p-isopropyltoluene (p-Cymene)
0.0103
0.0010
mg/L
0.0100
103
70-130
3.81
25
Methyl tert-Butyl Ether (MTBE)
0.00981
0.0010
mg/L
0.0100
98.1
70-130
1.72
25
Methylene Chloride
0.0102
0.0050
mg/L
0.0100
102
70-130
0.980
25
4-Methyl-2-pentanone (MIBK)
0.110
0.010
Ing/L
0.100
110
70-160
2.62
25
t
Naphthalene
0.00927
0.0020
mg/L
0.0100
92.7
40-130
1.63
25
t
n-Propylbenzene
0.00939
0.0010
mg/L
0.0100
93.9
70-130
5.59
25
Styrene
0.00962
0.0010
mg/L
0.0100
96.2
70-130
2.87
25
1, 1,2,2-Tetrachlorocthane
0.0108
0.00050
mg/L
0.0100
108
70-130
0.841
25
Tetrachloroethylene
0.00915
0.00050
mg/L
0.0100
91.5
70-130
5.42
25
Toluene
0.00970
0.0010
mg/L
0.0100
97.0
70-130
2.85
25
1,2,3-Trichlorobenzenc
0.00906
0.0050
mg/L
0.0100
90.6
70-130
3.03
25
1,2,4-Trichlorobenzene
0.00940
0.0010
mg/L
0.0100
94.0
70-130
1.37
25
1, 1, I-Trichloroethanc
0.00966
0.0010
Ing/L
0.0100
96.6
70-130
5.24
25
1, 1,2-Trichloroethane
0.0102
0.0010
MA
0.0100
102
70-130
0.0996
25
Trichloroediylene
0.00997
0.0010
mg/L
0.0100
99.7
70-130
3.06
25
Trichlorofluoromethane (Freon 11)
0.00942
0.0020
mg/1-
0.0100
84.2
70-130
3.16
25
1,2,3-Trichloropropane
0.0108
0.0020
mg/L
0.0100
108
70-130
1.78
25
1,2,4-Trimethylbenzene
0.00984
0.0010
mg/L
0.0100
98.4
70-130
2.51
25
1,3,5-Trimethylbenzene
0.00998
0.0010
mg/L
0.0100
99.8
70-130
3.16
25
Vinyl Acetate
0.0926
0.020
mg/1-
0.100
92.6
70-130
0.335
25
Vinyl Chloride
0.00689
0.0020
mg/L
0.0100
68.9
40-160
5.64
25
m+p Xylene
0.0191
0.0020
mg/L
0.0200
95.4
70-130
3.91
25
o-Xylenc
0.00956
00010
mg/L
0.0100
95.6
70-130
2.58
25
Surrogate: 1,2-Dichloroethane-d4 0.0265 mg/L 0.0250 106 70-130
Surrogate: Toluene-dg 0.0250 mg/L 0.0250 too 70-130
Surrogate: 4-Bromofluorobenzene 0.0242 -9/L 0.0250 96.6 70-130
I Page 15 of �22

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
QC result is outside ofestablished limits.
t Wide recovery limits established for difficult compound.
Wide RPD Emits established for difficult compound.
# Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
i Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP I -Flag).
L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside ofcontrol limits.
Reported value for this compound is likely to be biased on the low side.
Table of Contents
I Page 16 of

Table of Contents
con-atest®R
ANALYTICAL LABORATORY
Certified Analyses included in this Report
Anslyte
39 Spruce Street* East Longmeadow, MA01028 *FAX [phone] *TEL. [phone]
CERTIFICATIONS
Certifications
S W-846 8260B in Water
Acetone
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
BromodicWoromethane
NC
Bromoform
NC
Bromomethane
NC
2-Butanone (MEK)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromocdiane (EDB)
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
Dichlorodifluoromediane (Freon 12)
NC
I,I-Dichloroethane
NC
1,2-Dichloroethane
NC
IJ-Dichloroethylene
NC
cis- 1,2-Dichloroethylene
NC
ums-1,2-Dichloroethylene
NC
1,2-Dichloropropane
NC
1,3-Dichloropropanc
NC
2,2-Dichloropropane
NC
IJ-Dichloropropenc
NC
cis- 1,3-Dichloropropene
NC
trans-1,3-Dichloropropene
NC
Diisopropyl Ether (DIPE)
NC
Ethylbenzenc
NC
2-Hexanone (MBK)
NC
Isopropylbenzene (Cumene)
NC
p-Isopropyltoluene (p-Cymene)
NC
Methyl tert-Buryl Ether (MTBE)
NC
Methylene Chloride
NC
4-Methyl-2-pentanonc (MlBK)
NC
Naphthalene
NC
n-Propylbcnzene
NC
Styrene
NC
I Page 17 of 22 -1

Table of Contents
con -tor
ANALYTICAL LABORATORY
39 Spruce Street - East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8260B in Water
1, 1,2,2-Tctracliloroediane
NC
Tctrachloroethylene
NC
Toluene
NC
1,2,3-Triclilorobcrtzene
NC
1,2,4-Trichlorobenzene
NC
1, 1, I-Trich1loroethane
NC
1, 1,2-Trieldoroettiane
NC
Trichloroethylene
NC
TrieWorofluoromethane (Freon 11)
NC
1,2,3-Trichloropropane
NC
1,2,4-Trimethylbenzene
NC
1,3,5-Trimethylbcnzene
NC
Vinyl Acetate
NC
Vinyl Chloride
NC
m+p Xylene
NC
o-Xylene
NC
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
0
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC
100033
02/1/2016
MA
Massachusetts DEP
M-MAIOO
06/30/2016
CT
Connecticut Department of Publitc, Health
PH-0567
09/30/2017
NY
New York State Department of Health
10899 NELAP
04/1/2016
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2016
RI
Rhode Island Department of Health
LA000112
12/30/2015
NC
North Carolina Div. of Water Quality
652
12/31/2015
NJ
New Jersey DEP
MA007 NELAP
06/30/2016
FL
Florida Department of Health
E871027 NELAP
06/30/2016
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2016
WA
State of Washington Department of Ecology
C2065
02/23/2016
ME
State ofMaine
2011028
06/W2017
VA
Commonwealth of Virginia
460217
12/14/2016
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2016
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Company Name: A T C 5W Telephone: C/ a * "Container Code
Address: ;7— 7.��5 F , /^j; ji�r­C,0.k Q, , ; I e- 1,�- I Project # C 2-013 Analysis Requested Dissolved Metals
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(laboratory use onlyJ DateAF*mL- --Bvte�Time Composite Grab *Code -Code T--tedlar bag
Pr C m r b 15 .';-5 O=Other
C. i
35
"Preservation
I = Iced
... P0 C t5 q5
H = HCL
M Methanol
N Nitric Acid
S =Sulfuric Acid
B = Sodium bisulfate
X = Na hydroxide
T = Na thiosulfate
0 = Other
*Mald-Code:
GW= groundwater
VVW= wastewater
ments: Please use the following codes to let Con -Test know if a specific sample m DW= drinking water
in concentration in Matrix/Conc. Code Box.
A Li .................. I .............. 11 ........................... 1.11 .... ................ __ ....................................... S = soil/solid
H - High; M - Medium; L - Low; C - Clean; U - Unknown SL = sludge
Relinquished by� (signature)
Date/Time:
Turnaround ft
Detection
Limit Re-quirements
r
Program Information
5-Day
North Carolina
egei4d by: f�i,
Date/Time:
0 5-7-Day
0 2L
0 DSCA 0 IHSI3 Orphaned Landfill
C) 10-D.y
0 GWPC
0 SWS Landfill C) UST 0 REC
teinoished b Sig
Date/Time;
RUSH'
0 SWSL
0 Other:
CD
0 24-Hr r'48-Hr
0 OTHER
t ' d (sl
Date/Tirne:
0 72-Hr r'4-Day
AIHA NELAC & AIHA Certified
0
'
'TURNAROUND
�1:
Requires Lab App roval
WBE/DBE Certified
N
TIME lbusiness days) STARTS AT 9:00 A.M. THE DAY AFTER SAMPLE RECEIPT UNLESS THERE ARE QUESTIONS ON YOUR CHAIN.
'-'IF
THIS FORM IS NOT FILLED OUT
COMPLETELY OR IS INCORRECT, TURNAROUND TIME WILL NOT
START UNTIL ALL QUESTIONS ARE ANSWERED.
PLEASE BE CAREFUL NOT TO CONTAMINATE THIS DOCUMENT
(D
0
C)
0
=3
(D
Cn

12/17/2015
Ship Track Manage
FedEX �rackinc,
Travel History
Table of Contents
Track your package or shipfnent with FedEx Tracking
1`4 Profilk My FedEx Rewards Support Locatiom 114C�i' English
Learn FeclEx Office (D
A Date/Time Activity
Location
- 12/17/2015 - Thursday
10-24 am Delivered
FASI LONC41WADOR M. i
810 an" On Fad Ex vehicle for delivery
OWDSM LCkhS C1
8:04 am At local FedEx facility
%W..D$Or LCCVS. C T
6:23 am At destination sort facility
E�Sl GFIV6Y� t T
4:59 am Departed FedEx location
RDWNPOL� N
12:15 am Arrived at FedEx location
NOIANAFLX-E IN
— 1211612015 - Wednesday
9:38 pm Left FedEx. origin facility
7-11 pm Picked up
5-38 pm Shipment information sent to FedEx
Shipment Facts
Tracking
775228909203
Service FedEx Priority Overnight
number
Weight 16 lbs 6.8 k9s
Master tracking
number
775228909096
Total pieces 4
Delivered To
Shipping/Receiving
Shipper 80
reference
Total shipment
Weight
15 lbs " 6.8 kgs
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Deliver Weekday
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Table of Contents
Page 2 of 2
Login Sample Receipt Checklist
(Rejection Criteria Listing - Using Sample Acceptance Policy)
Any False statement will be brought to the attention of Client
wyespon
1) The cooler's custody seal, if present, is intact.
Answer (i ru
uomment
T1F/NA
2) The cooler or samples do not appear to have
been compromised or tampered with.
3) Samples were received on ice.
4) Cooler Temperature is acceptable.
5) Cooler Temperature is recorded.
6) COC is filled out in ink and legible.
T
7) COC is filled out with all pertinent information.
T
8) Field Sampler's name present on COC.
9) There are no discrepancies between the
sample IN on the container and the COC.
10) Samples are received within Holding Time .
11) Sample containers have legible labels.
_,_ Containers are not broken or leaking.
13) Air Cassettes are not broken/open.
_14� Sample collection date/times are provided.
15) Appropriate sample containers are used.
16) Proper collection media used.
17) No headspace sample bottles are completely filled.
18) There is sufficient volume for all requsted
analyses, including any requested MS/MSDs,
19) Trip blanks provided if applicable.
20) VOA sample vials do not have head space or
bubble is <6mm (1/4") in diameter.
21) Samples do not require splitting or compositing.
Who notified of False statements? Date/Time:
Doc #277 Rev. 4 August 2013 Log -in Technician Initials: Vlk_� DaterTime:
I Page 21 of

39 Spruce St.
East Longmeadow, MA. 01028
P: 413-525-2332
F: 413-525-6405
www.contestlabs.corn
CLIENT NAME: (RAt-C" 0
Table of Contents
con -test
ANALYMAL I ABORATORY
Page 1 of 2
Sample Receipt Checklist
RECEIVED BY:
DATE: IQ 1-211
1) Was the chain(s) of custody relinquished and signed?
2) Does the chain agree with the samples?
If not, explain:
3) Are all the samples In good condition?
If not, explain:
4) How were the samples received:
On Ice Eb Direct from Sampling Ambient El
Were the samples received in Temperature Compliance of (2-60C)?
Temperature 'C by Temp blank
Q No No CoC Included
(jd:j No
:Ye:s ) N o
In Cooler(s)'�E
CY6S) No N/A
Temperature 'C by Temp gun
5) Are there Dissolved samples for the lab to filter? Y e s ( N­d�
Who was notified Date Time
6) Are there any RUSH or SHORT HOLDING TIME samples? Yes
Who was notified Date Time
Permission to subcontract samples? Yes No
7) Location where samples are stored: (Walk-in clients only) if not already approved
Client Signature:
8) Do all samples have the proper Acid pH: Yes No
9) Do all samples have the proper Base pH: Yes No
10) Was the PC notified of any discrepancies with the CoC vs the samDles: Yes No Gii-k
Containers received at Con -Test
# of containers
# of containers
1 Liter Amber
8 oz amber/clearjar
500 mL Amber
4 oz amber/clear jar
250 mL Amber (8oz amber)
2 oz amber/clear iar
1 Liter Plastic
Plastic Bag / Ziploc
500 mL Plastic
SOC Kit
Non-ConTest Container
Perchlorate Kit
250 mL plastic
40 mL Vial - type listed below
Colisure / bacteria bottle
Fl;4ehnninf Knff
Dissolved Oxygen bottle
Othpr HnQr. iar
Encore
Other
Laboratory Comments:
40 mL vials: # HCI # Methanol
Bisulfate # DI Water
R.ev.:A A0ust . 2 . 0.1,3. Thiosulfate Unpreserved
Time and Date Frozen:
Page 22 of