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HomeMy WebLinkAboutWQ0000485_Monitoring - 07-2020_20200824V=1 August 18, 2020 VALLEY PROTEINS, INC. Division of Water Resources Attn: Information Processing Unit 1617 Mail Service Center Q ^ Q q Raleigh, NC 27699-1617 C) ti Re: Ground Water Quality Monitoring Report (GWQMR) ti Valley Proteins Inc. — Rose Hill C, N 1 j 17 To whom it may concern, Please find enclosed the Groundwater Quality Monitoring Compliance Report for Surface Irrigation for the month of July 2020 for our Rose Hill Division. Should you require any additional information or wish to discuss this matter, please feel free to contact me at 910.289.2083 x 25119. Sincerely, V'ae-w nford General Manager cc: VP Corporate Office Making a Sustainable Difference. 469 Yellow Cut Road Rose Hill, NC 28458 0 540.8772590 0 866.558.0994 Transportation 0 866.651.8175 valleyproteins.com SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM •,• • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MWA Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 12.46 ft. Well Diameter: 2 in. pH4500HB 4.90 units Temp. 000lo: 21.4 °C DRY at Depth to Water Level 82546: 5.0 Screened Interval: 12.46 ft. to 2.46 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear / Tan Tint checlf—i Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here-t] LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.09 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 100.00 mg/L Al - Aluminum 01105 mg/L Sodium 6.64 mg/L pH (Lab) 00403 4.90 units Ba - Barium 01007 ug/L TOC omao 1.2 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 50 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 000lo <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Darrell Sanford - General Manager Permittee (or Authorized Apent) Name and Title - Please print or tvpe GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY OF ENVIRONMENT &NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: W0MDEPARTMENT DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: _ 3/31 /2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other. from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 31.00 ft. Well Diameter: 2 in. pH4500HB 6.20 units Temp. 000lo: 202 0C DRY at Depth to Water Level 82546: 11.9 ft. below measuring point Screened Interval: 30.15 ft. to 20.15 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear here: El Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES NO - LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn -,Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.08 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 274.00 mg/L Al - Aluminum of lo5 mg/L Sodium 9.99 mg/L pH (Lab) 00403 6.20 units Ba - Barium 01007 ug/L TOC 00680 1.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 13 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 8 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type (or Authorized Agent) IN GW-59 Rev, 812013 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM ••• • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 28.93 ft. Well Diameter: 2 in. pH4500HB 6.60 units Temp. 000lo: 18.9 °C DRY at Depth to Water Level 82546: 5.9 ft. below measuring point Screened Interval: 28.93 ft. to 18.93ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear check here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES Ej NO LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/2912020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.19 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids. -Total 70300 212.00 mg/L Al - Aluminum oilo5 mg/L Sodium 8.43 mg/L pH (Lab) 00403 6.60 units Ba - Barium 01007 ug/L TOC oo68o 0.80 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH,, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type Agent) GW-59 Rev.8/2013 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-907-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery — X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH45ooHe 5.10 units Temp. 000lo: 20.4 or DRY at Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.42 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 10.0 gallons Appearance Tan / White chec" Samples for metals were collected unfiltered: X YES n NO and field acidified: X YES ❑ NO here:µ LABORATORY INFORMATION Date sample analyzed: 07/1112020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.11 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 170.00 mg/L AI - Aluminum of lo5 mg/L Sodium 19.0 mg/L pH (Lab) 00403 5.10 units Ba - Barium 01007 ug/L TOC oo68o 0.6 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 77 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 19 mg/L Hg - Mercury 7190o ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo6lo <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NFjas N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N oo625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOcs: mg/L trnuent I otal vuus: mg/L vtn. Kemoval7o I certify that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a l DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Darrell Sanford - General Manager Pemtittee (or Authorized Agent) Name and Title - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name Field 5 - damaged by farm equip / to replace No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.60 units Temp. 00010: 20.4 °C DRY at Depth to Water Level 62546: 6.8 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00065: None sampling, Volume of water pumped/bailed before sampling: 10.0 gallons Appearance Tan / White chect] Samples for metals were collected unfiltered: X YES Q NO and field acidified: X YES ❑ NO here. LABORATORY INFORMATION Date sample analyzed: 07/1112020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead oio51 ug/L CoIrform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 315N /100mL Phosphorus: Total as P 00665 0.21 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): isso►ved Solids:Total 70300 61.00 mg/L Al - Aluminum o11o5 mg/L Sodium 2.05 mg/L pH (Lab) 00403 5.60 units Ba - Barium 01007 ug/L TOC oo68o 1.00 mg/L Ca - Calcium 00916 mg/L Chloride oog4o <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 26 mg/L Hg - Mercury 719M ug/L Lab Report Attached? E Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 76732: method # SM 6200C Total Ammonia oo6lo <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NIJ as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Darrell Sanford - General Manager Pennittee (or Authorized Agent) Name and Title - Please print or type mg/L Effluent Total VOCs: mg/L VOC Removal% • • . • DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 13.73 ft. Well Diameter: 2 in. pH4500HB 6.30 units Temp. 00010: 219 °C DRY at Depth to Water Level 82546: 6.3 ft. below measuring point Screened Interval: 13.73 ft. to 3,73 ft. Spec. Cond. 00094: )tMhos time of Measuring Point is 3.50 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: Sulfur sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan Tint checlf—n Samples for metals were collected unfiltered: X YES p NO and field acidified: X YES ❑ NO here LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 8 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.13 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 312.00 mg/L Al - Aluminum o11o5 mg/L Sodium 10.2 mg/L pH (Lab) 00403 6.30 units Ba - Barium 01007 ug/L TOC 00660 37.7 mg/L Ca - Calcium 00916 mg/L Chloride 00940 23 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug1L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 22 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 FtMhos K - Potassium 00937 mg/L VOC 78732 method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, N11as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 1.3 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Valley Proteins Inc.- Rose Hill Permit Name (if different): Facility Address: 469 Yellow Cut Rd. Rose Hill, NC 28458 County Duplin Contact Person: Corey Lanier Telephone#: (910) 660-1173 Well Location/Site Name No. of wells to be sampled: 11 (from Permit) DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIOH, NC 27699-1617 Phone: 919-607-6306 PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.60 units Temp. 000l( 201 °C DRY at Depth to Water Level 82546: 5.6 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000e5: Slight Sulfur sampling, Volume of water pumped/bailed before sampling: 10.0 gallons Appearance Reddish Tan chec ] Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here:µ LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead olo5i ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.23 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.77 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 592.00 mg/L Al - Aluminum oil o5 mg/L Sodium 71.8 mg/L pH (Lab) 00403 5.60 units Ba - Barium 01007 ug/L TOC oo68o 3.6 mg/L Ca - Calcium 00916 mg/L Chloride 0o94o 190 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron olo45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 119 mg/L Hg - Mercury 719oo ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 76732: method # SM 6200C Total Ammonia 00610 0.40 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NIJas N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 0.70 mg/L Ni - Nickel01067 ug/L method # Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type � DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: . DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807.8306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill _ Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.30 units Temp. 0001( 23.1 oC DRY at Depth to Water Level 82546: 7.3 Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 10.0 gallons Appearance Tan Tint checlF— Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO heret] LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 0.29 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 446.00 mg/L Al - Aluminum 01105 mg/L Sodium 56.9 mg/L pH (Lab) 00403 4.30 units Ba - Barium 01007 ug/L TOC 00680 3.00 mg/L Ca - Calcium 00916 mg/L Chloride oos4o 113 mg/L Cd - Cadmium 01027 ug/L Arsenic01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 144.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo6lo <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Ngas N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type mg/L Effluent Total VOCs: mg/L VOC Removal% DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM � 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-12B Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB: 4.20 units Temp. 000lo: 20.3 oC DRY at Depth to Water Level 82546: 7.0 ft. below measuring point Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur sampling, Volume of water pumped/bailed before sampling: 10.0 gallons Appearance Tan Tint checlf Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here:] LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc olo92 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.34 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 698.00 mg/L Al - Aluminum oil o5 mg/L Sodium 112 mg/L pH (Lab) 00403 4.20 units Ba - Barium 01007 ug/L TOC oo6eo 2.80 mg/L Ca - Calcium 00916 mg/L Chloride 00940 174 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron olo45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 274 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? N Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium o0937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nljas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type mg/L Effluent Total VOCs: mg/L VOC Removal% 0 0 DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery = - X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-13A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.00 units Temp. 000lo: 22.5 oC DRY at Depth to Water Level 82546: 6.9 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 10.0 gallons Appearance Tan Tint chec Samples for metals were collected unfiltered: X YES NO and field acidified: X YES F1 NO here: LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.32 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 47.00 mg/L Al - Aluminum 01105 mg/L Sodium 5.19 mg/L pH (Lab) 00403 5.00 units Ba - Barium o1oo7 ug/L TOC 00680 0.60 mg/L Ca - Calcium oo916 mg/L Chloride oo94o <5.0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 10.00 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nljas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: Darrell Sanford - General Manager Permittee (or Authorized Agent) Name and Title - Please print or type mg/L VOC Removal% �• DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: •• : DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-14A Date sample collected: 7/11/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.80 units Temp. 0001c 20.9 oC DRY at Depth to Water Level 92546: 6.1 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 10.0 gallons Appearance Reddish Tan chec" Samples for metals were collected unfiltered: X YES M NO and field acidified: X YES M NO here: J LABORATORY INFORMATION Date sample analyzed: 07/11/2020-07/29/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead oimi ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.10 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.46 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 908.00 mg/L Al - Aluminum otto5 mg/L Sodium 117 mg/L pH (Lab) 00403 5.80 units Ba - Barium 01007 ug/L TOC oo6ao 4,00 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 299 mg/L Cd - Cadmium o1o27 ug/L Arsenic 01002 ug/L Chromium: Total oto34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 170 mg/L Hg - Mercury 7190o ug/L Lab Report Attached? 0 Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 75732: method # SM 6200C Total Ammonia oomo <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NNas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.80 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: Darrell Sanford - General Manager Pennittee (or Authorized Agent) Name and Title - Please print or type mg/L VOC Removal% GW-59A COMPLIANCE REPORT FORM Permit # W00000485 (Submit one each monitoring period with GI4=59 forms.) I Enter date monitoring results were due. (08/3112020) Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? No Z Was any required information missing on the GW-59 report forms? No IF the answer to question 1 or 2 is "YES', list in the space provided below the well identification numbers) and explain the problems encountered in obtaining the required information. MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC, moving the replacement well 10' due North per DEQ direction. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missingidentification plate, area overgrown, etc.)'. If the answer is "Yes ", contact the Regional Office far guidance. No 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 5 For the constituents identified In question 4 above, have standards been exceeded previously for the same constituent(s) in the same well(s) in the last two years? YES If the answer to question 5 is "NO', skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES IF the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee Implementing previously approved actions required by the Division Involving this groundwater quality problem? YES If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility, Failure to do so may subject the permittee to a Notice of Violation fines and/or penalties. Additional monitoring was performed to identify constituents of TOC in MW No.9. The facility has been communicating with Mr. Geoff Kegley in the Wilmington Regional Office, 8 The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to thee/best of my knowledge. ' `"-Signature of Permittee (or A ed Agent) Date -11 Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report TDS 500 10A 12B 14A July-20 592 698 908 March-20 659 797 1180 November-19 637 908 1120 July-19 535 799 903 March-19 736 874 1220 November-18 659 621 1160 July-18 713 640 962 pH 6.5-8.5 1 2 7A 8A 9 10A 11A 12B 13A 14A July-20 4.90 6.20 5.10 5.60 6.30 5.60 4.30 4.20 5.00 5.80 March-20 5.00 4.00 5.40 5.90 4.90 5.10 5.00 4.90 5.20 November-19 5.29 5.42 4.98 5.03 4.62 5.55 5.39 July-19 5.78 1 5.33 5.41 4.88 5.93 1 5.93 March-19 5.60 5.51 3.83 5.59 6.17 4.18 4.60 4.21 5.23 4.95 November-18 5.63 5.74 4.78 5.25 5.72 4.90 4.78 4.34 5.47 4.90 July-18 6.14 4.81 5.50 5.28 5.00 4.88 5.89 5.03 Chloride 250 14A July-20 299 March-20 339 November-19 288 July-19 March-19 286 November-18 291 July-18 Sulfate 250 12B July-20 274 March-20 281 November-19 July-19 322 March-19 302 November-18 July-18 6r�envirochem ANALYTICAL & CONSULTING CHEMISTS Valley Proteins - Rose Hill Post Office Box 1026 Rose Hill NC Attention: Corey Lanier Lab ID Sample ID: 20-28823 Site: MW-1 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info'a environmentalchemists.com Date of Report: Jul 29, 2020 Customer PO #: 28458 Customer ID: 08100027 Report #: 2020-11475 Project ID: Monitoring Wells Method Collect Date/Time Matrix Sampled by 7/11/2020 1:40 PM Water jcb/envirochem Results Date Analyzed Color color Clear/Tan Tint 07/11/2020 Depth to water, ft. Depth to water, Ft. 5.0 feet 07/11/2020 Sodium EPA 200.7 6.64 mg/L 07/16/2020 Sulfate EPA 300.0 50 mg/L 07/14/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/11/2020 Odor Qualitative N/D 07/11/2020 Total Dissolved Solids (TDS) SM 2540 c 100 mg/L 07/13/2020 Temperature SM 2550 B 21.4 C 07/11/2020 Chloride SM 4500 Cl E 7 mg/L 07/18/2020 pH SM 4500 H B 4.9 units 07/11/2020 Total Phosphorus SM 4500 P F 0.09 mg/L 07/16/2020 Total Organic Carbon (TOC) SM 5310 B 1.2 mg/L 07/13/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 07/11/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 0.03 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method 0.03 mg/L 07/29/2020 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 07/20/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2020 Report #.: 2020-11475 Pagel of 11 Lenvirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infov environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28824 Site: MW-2 7/11/2020 2:05 PM Water jcb/envirochem Test Method Results Date Analyzed Color color Clear 07/11/2020 Depth to water, ft. Depth to water, Ft. 11.9 feet 07/11/2020 Sodium EPA 200.7 9.99 mg/L 07/16/2020 Sulfate EPA 300.0 8 mg/L 07/14/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.Ogallons 07/11/2020 Odor Qualitative N/D 07/11/2020 Total Dissolved Solids (TDS) SM 2540 C 274 mg/L 07/13/2020 Temperature SM 2550 B 20.2 C 07/11/2020 Chloride SM 4500 Cl E 13 mg/L 07/18/2020 pH SM 4500 H B 6.2 units 07/11/2020 Total Phosphorus SM 4500 P F 0.08 mg/L 07/16/2020 Total Organic Carbon (TOC) SM 5310 B 1.1 mg/L 07/13/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 07/11/2020 Nitrate Nitrogen (Caic) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020 Total Nitrogen (Caic) Total Kjeldahl Nitrogen (TKN) EPA 3512 < 0.5 mg/L 07/20/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2020 Report # . 2020-11475 Page 2 of 11 [envi7nochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info,a environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28825 Site: MW-4 7/11/2020 12:40 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 07/11/2020 Depth to water, ft. Depth to Water, Ft 5.9 feet 07/11/2020 Sodium EPA 200.7 8.43 mg/L 07/16/2020 Sulfate EPA 300.0 <5 mg/L 07/14/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/11/2020 Odor Qualitative N/D 07/11/2020 Total Dissolved Solids (TDS) SM 2540 C 212 mg/L 07/13/2020 Temperature SM 2550 B 18.9 C 07/11/2020 Chloride SM 4500 Cl E 5 mg/L 07/18/2020 pH SM 4500 H B 6.6 units 07/11/2020 Total Phosphorus SM 4500 P F 0.19 mg/L 07/16/2020 Total Organic Carbon (TOC) SM 5310 B 0.8 mg/L 07/13/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 07/11/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 07/20/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2020 Report #. 2020-11475 Page 3 of 11 F"0'07 Environmental Chemists, Inc. ' 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax sM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info!rtenvironmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28826 Site: MW-7A 7/11/2020 1:25 PM Water jcb/envirochem Test Method Results Date Analyzed Color color Tan/White 07111 /2020 Depth to water, ft. Depth to Water, Ft. 5.8 feet 07/11/2020 Sodium EPA 200.7 19.0 mg/L 07/16/2020 Sulfate EPA 300.0 19 mg/L 07/14/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 07/11/2020 Odor Qualitative N/D 07/11/2020 Total Dissolved Solids (TDS) SM 2540 c 170 mg/L 07/13/2020 Temperature SM 2550 B 20.4 C 07/11/2020 Chloride SM 4500 Cl E 77 mg/L 07/18/2020 pH SM4500H8 5.1 units 07/11/2020 Total Phosphorus SM 4500 P F 0.11 mg/L 07/16/2020 Total Organic Carbon (TOC) SM 5310 B 0.6 mg/L 07/13/2020 Fecal Coliform SM9222DMF <1 Colonies/100mL 07/11/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 3512 < 0.5 mg/L 07/20/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2020 Report # 2020.11475 Page 4 of 11 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab a 910.392.4424 Fax 710 8owsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infol'a environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28827 Site: MW-8A 7/11/2020 1:15 PM Water jcb/envirochem Test Method Results Date Analyzed Color color Tan/White 07/11/2020 Depth to water, ft. Depth to water, Ft. 6.8 feet 07/11/2020 Sodium EPA 200.7 2.05 mg/L 07/25/2020 Sulfate EPA 300.0 26 mg/L 07/14/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 07/11/2020 Odor Qualitative N/D 07/11/2020 Total Dissolved Solids (TDS) SM 2540 C 61 mg/L 07/13/2020 Temperature SM 2550 B 20.4 C 07111 /2020 Chloride SM 4500 Ci E < 5 mg/L 07/18/2020 pH SM 4500 H B 5.6 units 07111 /2020 Total Phosphorus SM 4500 P F 0.21 mg/L 07/16/2020 Total Organic Carbon (TOC) SM 5310 B 1.0 mg/L 07/13/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 07/11/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 07/20/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2020 Report # 2020-11475 Page 5 of 11 Lenvirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infou environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28828 Site: MW-9 7/11/2020 12:50 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan Tint 07/11/2020 Depth to water, ft. Depth to water, Ft. 6.3 feet 07/11/2020 Sodium EPA 200.7 10.2 mg/L 07/16/2020 Sulfate EPA 300.0 22 mg/L 07/14/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 07/11/2020 Odor Qualitative Sulfur 07/11/2020 Total Dissolved Solids (TDS) SM 2540 C 312 mg/L 07/13/2020 Temperature SM 2550 B 20.8 C 07/11/2020 Chloride SM 4500 Cl E 23 mg/L 07/18/2020 pH SM 4500 H B 6.3 units 07/11/2020 Total Phosphorus SM 4500 P F 0.13 mg/L 07/16/2020 Total Organic Carbon (TOC) SM 5310 B 37.7 mg/L 07/13/2020 Fecal Coliform SM 92220 MF 8 Colonies/100mL 07/11/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 3532 0.03mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351 2 1.3 mg/L 07/20/2020 Total Nitrogen Total Nitrogen 1.3 mg/L 07/29/2020 Report A 2020-11475 Page 6 of 11 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(a environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28829 Site: MW-10A 7/11/2020 12:20 PM Water jcb/envirochem Test Method Results Date Analyzed Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Color Reddish Tan 07/11/2020 Depth to water, Ft. 5.6 feet 07/11/2020 EPA 200 7 71.8 mg/L 07/16/2020 EPA 300.0 119 mg/L 07/20/2020 EPA 350.1 0.4 mg/L 07/15/2020 Gallons Bailed before sampling 10 gallons 07/11/2020 Qualitative Slight Sulfur 07/11/2020 SM 2540 C 592 mg/L 07/13/2020 SM 2550 B 20.1 C 07/11/2020 SM 4500 CI E 190 mg/L 07/18/2020 SM 4500 H B 5.6 units 07/11/2020 SM 4500 P F 0.77 mg/L 07/16/2020 SM 5310 B 3.6 mg/L 07/13/2020 SM 9222D MF <1 Colonies/100ml- 07/11/2020 EPA 353.2 < 0.02 mg/L 07/12/2020 EPA 353.2 0.23 mg/L 07/24/2020 Subtraction Method 0.23 mg/L 07/29/2020 EPA 351 2 Total Nitrogen 0.7 mg/L 07/20/2020 0.9 mg/L 07/29/2020 Report # 2020-11475 Page 7 of 11 SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infora environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28830 Site: MW-11A 7/11/2020 12:10 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan Tint 07/11/2020 Depth to water, ft. Depth to Water Ft 7.3 feet 07/11/2020 Sodium EPA 200.7 56.9 mg/L 07/16/2020 Sulfate EPA 300.0 144 mg/L 07/20/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 07/11/2020 Odor Qualitative N/D 07/11/2020 Total Dissolved Solids (TDS) SM 2540 C 446 mg/L 07/13/2020 Temperature SM 2550 B 23.1 C 07/11/2020 Chloride SM 4500 Cl E 113 mg/L 07/21 /2020 pH SM 4500 H B 4.3 units 07/11/2020 Total Phosphorus SM 4500 P F 0.29 mg/L 07/16/2020 Total Organic Carbon (TOC) SM 5310 B 3.0 mg/L 07/13/2020 Fecal Coliform SM9222DMF <1 Colonies/100mL 07/11/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2 < 0.5 mg/L 07/20/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2020 Report * 2020-11475 Page 5 of 11 F7-- ---.447 Environmental Chemists, Inc. nvirochem 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info�a environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28831 Site: MW-12B 7/11/2020 11:50 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Tan Tint 07/11/2020 Depth to water, ft. Depth to Water, Ft. 7.0 feet 07/11/2020 Sodium EPA 200.7 112 mg/L 07/25/2020 Sulfate EPA 300.0 274 mg/L 07/20/2020 Ammonia Nitrogen EPA 350.1 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 07/11/2020 Odor Qualitative Slight Sulfur 07/11/2020 Total Dissolved Solids (TDS) SM 2540 C 698 mg/L 07/13/2020 Temperature SM 2550 B 20.3 C 07/11/2020 Chloride SM 4500 Cl E 174 mg/L 07/21 /2020 pH SM 4500 H B 4.2 units 07/11/2020 Total Phosphorus SM 4500 P F 0.34 mg/L 07/17/2020 Total Organic Carbon (TOC) SM 5310 B 2.8 mg/L 07/13/2020 Fecal Coliform SM9222DMF <1 Colonies/100mL 07/11/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 < 0.02 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351 2 < 0.5 mg/L 07/20/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 07/29/2020 Report # 2020.11475 Page 9 of 11 renvirochem 6h ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(a environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28832 Site: MW-13A 7/11/2020 12:00 PM Water jcb/envirochem Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Method Results Date Analyzed Color Tan Tint 07/11/2020 Depth to Water, Ft. 6.9 feet 07111 /2020 EPA 200.7 5.19 mg/L 07/16/2020 EPA 300.0 10 mg/L 07/20/2020 EPA 350.1 < 0.2 mg/L 07/15/2020 Gallons Bailed before sampling 10 gallons 07/11/2020 Qualitative N/D 07/11/2020 SM 2540 C 47 mg/L 07/13/2020 SM 2550 B 22.5 C 07/11/2020 SM 4500 Cl E < 5 mg/L 07/21 /2020 SM 4500 H B 5.0 units 07/11/2020 SM 4500 P F 0.32 mg/L 07/17/2020 SM 5310 B 0.6 mg/L 07/13/2020 SM 9222D MF <1 Colonies/100mL 07/11/2020 EPA 353 2 0.03 mg/L 07/12/2020 EPA 353.2 < 0.02 mg/L 07/24/2020 Subtraction Method <0.02 mg/L 07/29/2020 EPA 351 2 Total Nitrogen < 0.5 mg/L 07/20/2020 <0.5 mg/L 07/29/2020 Report # 2020-11475 Page 10 of 11 [envi7nochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infola environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Jul 29, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Corey Lanier Report #: 2020-11475 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-28833 Site: MW-14A 7/11/2020 1:05 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color Reddish Tan 07/11/2020 Depth to water, ft. Depth to Water, Ft 6.1 feet 07/11 /2020 Sodium EPA 200 7 117 mg/L 07/16/2020 Sulfate EPA 300 0 170 mg/L 07/20/2020 Ammonia Nitrogen EPA 350 1 < 0.2 mg/L 07/15/2020 Gallons bailed before sampling Gallons Bailed before sampling 10 gallons 07/11 /2020 Odor Qualitative N/D 07/11 /2020 Total Dissolved Solids (TDS) SM 2540 C 908 mg/L 07/13/2020 Temperature SM 2550 B 20.9 C 07/11 /2020 Chloride SM 4500 Cl E 299 mg/L 07/21 /2020 pH SM 4500 H B 5.8 units 07/11 /2020 Total Phosphorus SM 4500 P F 0.23 mg/L 07/17/2020 Total Organic Carbon (TOC) SM 5310 B 4.0 mg/L 07/13/2020 Fecal Coliform SM 9222D MF <1 Colonies/100mL 07/11 /2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 3532 <0.02mg/L 07/12/2020 Nitrate+Nitrite-Nitrogen EPA 353 2 0.10 mg/L 07/24/2020 Nitrate Nitrogen Subtraction Method 0.10 mg/L 07/29/2020 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2 0.8 mg/L 07/20/2020 Total Nitrogen Total Nitrogen 0.9 mg/L 07/29/2020 Comment: Reviewed by: Report # 2020-11475 Page 11 of 11 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392.04123 `' (� Sample Recei t Checklist ClientM Date:?A� �� Report Number: Receipt of sample: DeliverecfZ UPS ❑ FedEx ❑ Other ❑ ❑ YES ❑ NO N/A 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt 'C Corrected temperature upon receipt •C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project M r./QA notified? YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO S. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? CZ YES 113 NO 8. Were tests to be performed listed on the COC? YES O NO 9. Did samples arrive in proper containers for each test? 10. Did samples arrive in good condition for each test? 11. Was adequate sample volume available?' YES ❑ NO YES ❑ NO YES ❑ NO 112. Were samples received within proper holding time for requested tests? YES 13 NO 13. Were acid preserved samples received at a pH of <27 • YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? • • ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 118. Were orthophosphate samples filtered in the field within 15 minutes? • TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. • • Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) by adding (circle one): were received incorrectly preserved and were adjusted accordingly H2SO, HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state tab if directed to analyzed by the customer who was notified, date and time Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Ana"cal & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 i nfo@environmentalchemists.com Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification p Collection m m E `" ~ m w °a o` 0 c 0 we _ ct9 :° o` o 0. " ` m rJ a r E " �W m m g D Z PRESERVATION ANALYSIS REQUESTED D to Time TempU w a i o Q1v _ = _ < _ _o _ w o MW: ( n 1;vo. L �' y MW C P X NO2, Chloride, TDS, Sulfate G G H Depth to water: �d C P X NO3, NH3, TP, TN calc G G / Gallons bailed: 01fj C P X Na G G H (field): W. 3' C P X Fecal Coliform G G Odor: C P X TOC G G LL Color: "Cw^/ �j ^�� C P X VOC November only) G G Gtsw C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: 3 C- Delivered By: Comments: Accepted: Rejected: Resam Received By: Time: ND: mington ENVIRONMENTAL CHEMISTS, I N C 6602 E: 9 0-392-0223'IFAX 910-392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well ST = Stream SO = Soil SL = Sludge Other: Sample Identification Collection E rm ~ a `o E o a a v o` m u E w m m g a Z PRESERVATION , , , ANALYSIS REQUESTED Time Temp w o Z =_ e o �, i o = w MW MW C P 8�d X NO2, Chloride, TDS, Sulfate G G y Depth to water: 3 C P Os X NO3, NH3, TP, TN calc G G Gallons bailed: ^ C P X lNa G G / H (field): C P X I Fecal Coliform G G Odor: o..c C P X TOG G G Color: C P I I X VOC (Novemberonly) G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. I emperature when Received "C: .3 Accepted: `,— Rejected: Resam le equested: Delivered By: Received By: zcz Date -IL av Time: 3s VO Comments: TURNAROUND: Windmill Way mington ENVIRONMENTAL CHEMISTS, I N C o f E: 9 0-392 0223'IFAX 910-392-44245 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentatchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: 1 = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m m S F a E S U m ct7 `o V a m �_J s U E W m z PRESERVATION ANALYSIS REQUESTED D to Time Temp() i z _ e o = "o x o o ~ w O MW: ��'' MW 8�as X NO2, Chloride, TDS, Sulfate G G Depth to water: .}� C P v'S A (CA 14 NO3, NH3, TP, TN calc G G Gallons bailed: C P X Na G G H (field): C P X Fecal Coliform G G Odor: c C P X TOC G G Color: an C P X I JVOC November only) G G C P G G C P G G C P G G Transfer Relinquished By: DatelTime Received By: Date/Time 1. 2. Temperature when Received °C: Accepted Rejected: Resam le equested: -! Delivered By: ECG Received By: Z.� DateiII IaQ Time:3= V0 Comments: TURNAROUND: Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: — l -t `, ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m m m s E 8tE c 82 m m0.Q PRESERVATION ANALYSIS REQUESTED Time Temp Z o o o o_ w MW: v �3L L MW C P of X NO2, Chloride, TDS, Sulfate G G k Depth to water: C P 'S 1 i0 X NO3, NH3, TP, TN calc G G Gallons bailed: C P X I JNa G G H (field): C P X Fecal Coliform G G Odor: J O^ C P X TOC G G // Color: �� '4.!+C C P X VOC (November only) G G C {w� C P G G C P G G C P G G Transfer Relinquished By: DatefTime Received By: Date/Time 1. 2. Temperature when Received °C: J Accepted:' Rejected: Resam le Requested: Delivered By: Received By: CT— Datel I h aD Time:5'. 40 Comments: TURNAROUND: Windmill Way ENVIRONMENTAL CHEMISTS, INC o E:910-3 202231FAX 910- 92-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info§environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: d - 7 ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONEIFAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludqe, Other: Sample Identification Collection m m w~ o 6o U m _ C U a U m C J t E U n W g? Z PRESERVATION ANALYSIS REQUESTED Date Time Temp o Z y = i 2 a Z = i O MW: L °' MW C P $7 X NO2, Chloride, TDS, Sulfate G G r Depth to water: �% C P D•� 4a44 X NO3, NH3, TP, TN calc G G Gallons bailed: �� C P X Na G G _ H (field): C P I X I IFecal Coliform G G Odor: ° ^ C P X TOC G G // Color: C P X1 VOC November only) G G c P G G C P G G C P G G Transfer Relinquished By: DatetTime Received By: Date/Time 1. 2. Temperature when Received °C: Accepted: ✓ Rejected: Resam le equested: Delivered By: Received By: e Date 12,a Time:3' Uy Comments: TURNAROUND: Way CM mington ENVIRONMENTAL CHEMISTS, I N C 6602 C : 910i1392 0223'IFAX 910-392-44245 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 114 ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m E F m a c `o m Ct7 `o v a m c o a u E ow m g z PRESERVATION ANALYSIS REQUESTED D t Time Temp _ z c = o x xo z o t w o MW: .iv La _J MW C P -1vtr «6O X NO2, Chloride, TDS, Sulfate G G Depth to water: '� X i!T NO3, NH3, TP, TN calc G G Gallons bailed: ��Ly C P X Na G G H (field): �• 1' C P X Fecal Coliform G G Odor: Sp l4' C P X TOC G G Color: fs ./>l �� ��✓ C P I X VOC November only) G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: 3 Accepted: Y Rejected: Resa le equested: Delivered By: Received By: Dat1 1 J • Time0 Comments: TURNAROUND: 4= Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: o— 1 i 7S ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge Other: Sample Identification Collection m m E~ 0 a E `o c l7 `o IL c E r o w m g Z PRESERVATION ANALYSIS REQUESTED D t Time TempN" z o m s~ o 0 o w z o M . %� / MW c P SIa/aa X 1402, Chloride, TDS, Sulfate G G Depth to water: } �' X NO3, NH3, TP, TN talc G G Gallons bailed: D C P X Na G G H (field): S• 5 5 C P X Fecal Coliform G G Odor: S4 41- 5-a/4- C P X ITOC G G /, Color: Xd�'f L � A.1 C P X VOC November only) G G C P G G C P G G C qGG Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received "C: J Delivered By: Comments: Accepted: '" Rejected: Resam le equested: Received By: C Datel 1 Timer : kjo TURNAROUND: t ENVIRONMENTAL CHEMISTS, I N C o E: 910 Windmill 910- 92-444mington, NC 28405 45 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 0 — % 75 ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection E °: in ~ a o o 0 W; y o V J o m L E m m Qf J Z PRESERVATION ANALYSIS REQUESTED t Time Temp" w Z Z u x o m = 0 = x x 0 o = w x 0 MW: �l KY•12, Z. 1 '. MW C P 6 � X NO2, Chloride, TDS, Sulfate G G v Depth to water: C P X IN03, NH3, TP, TN calc G G Gallons bailed: Q, C P X Na G G H (field): 'Lcl C P IX Fecal Coliform G G Odor: s c C P X TOC G G / Color: 4-,-, C P X I 1VOC November only) G G C P G G C P G G C P G G _in Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received 'C: Accepted: 6­ Delivered By: a C Z Received By: Comments: Resa 1 le equested: C �- Date Time:3. V9 TURNAROUND: :.. ENVIRONMENTAL CHEMISTS, I N C 6602 E: 9 0i1392 02l Way 231FAX 910' 92-"245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: IN ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m rn ~ 1 MJ o o` m C V a `o U a CDPRESERVATION C J o Q1 U E 0 UJ m g z ANALYSIS REQUESTED Date Time Temp Z z = o 0 0 w o MW: 2, { 1''�' '� MW C P c,�/ a air X NO2, Chloride, TDS, Sulfate « �i o G G a Depth to water: C P V's IN03, NH3, TP, TN calc G G Gallons bailed: I ° C P X I Na G G H (field): qAI- C P I X Fecal Coliform G G / Odor: (•f�'��i`�r C P I X TOC G G Color: L Cam/ -4,m C P I X I IVOC November only) G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: 3 Accepted: Rejected: Resample equested: Delivered By: F,c;;F- Received By: E C. DatedDI in Time: q Comments: TURNAROUND: a u Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info Ccoenvironmentalchomists.com Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: r,20 — 1 ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Siudae_ Other Sample Identification Collection E `� in ~ M o ° e fJ _ o c O. " 0 a L E " mQ� J Z PRESERVATION ANALYSIS REQUESTED Date Time Temp W ZO Z � 0 x o m = = x x a = o � IN02, MW: 13 LZ '� MW db3 X Chloride, TDS, Sulfate G G ., Depth to water: �; C P �'S X 1 °t NO3, NH3, TP, TN calc G G Gallons bailed: /O C P X Na G G H field : S• o C P X Fecal Coliform G G Odor: C P X TOC G G Color: N ho C P X VOC November only) G I G C P in G G C P G G I C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: J Accepted: ✓ Rejected: Resample equested: Delivered By: F_ Received By: Date7l h Time - li _ Comments: TURNAROUND: .. Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: O— 1 �� ADDRESS: CONTACT NAME: Susan Price PO NO: REPORT TO: Corey Lanier PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m m y~ m a o o 2 m _ cc� o `8 a " m c= o f L U ow m Z PRESERVATION ANALYSIS REQUESTED to Time Temp� i N _ o 0 z 0 W o MW: MW C P UM033 X NO2, Chloride, TDS, Sulfate G G ll •, De th to water: 73 . 9 C P X NO3, NH3, TP, TN calc G G Gallons bailed: C P X Na G G H (field): C P X Fecal Coliform G G Odor: 4► ^c C P Ix ITOC G G Color: �f .'s� {sa C P I X VOC November only) G G C�, f C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received °C: Accepted: Delivered By: f, CM Received By: Comments: ected: Resam� quests Date: 1 aD TURNAROUND: Time v