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HomeMy WebLinkAboutNCG030234_Monitoring Report_20200403(gBENDEL March 31, 2020 NCDEQ Division of Land Resources 610 East Center Avenue, Suite 300 Moorseville, NC 28115 Subject: Monthly Discharge Monitoring Report Submittal for 2020 Bendel Tank & Heat Exchanger, LLC 4823 N. Graham Street, Charlotte, Mecklenburg County Stormwater Permit COC Number NCG030234 Dear Division of Land Resources: 704.596.5112 office 866.596.5112 toll -free 704.597.5069 fax 4823 North Graham Street Charlotte, NC 28269 As required by the referenced Stormwater Permit Certificate of Coverage, please find enclosed an original and one copy of the monthly Discharge Monitoring Report (DMR) for the referenced facility. These DMRs are being submitted as the following sample designated in the Tier III section of the permit: Year 2 - Period 1 As required in Tier III of the Stormwater Plan, Bendel will continue to monitor for all required parameters until such time as the site can demonstrate three consecutive samples that are below the benchmark value for all parameters in a Tier response. Based on the new general stormwater permit, this should be attainable for copper. Once attainment has been reached for copper, Bendel may seek a variance from the Department of Environmental Quality for zinc. Please call me at (704) 596-5112 if you have any questions or if you require any additional information. Sincerely, Jim Rozsa Vice President, Operations rD u 'C+: 3 m ro u a w v rD -I 0 < ro cm P v ro m° o C _ rt L h -I m 3 0 c c Gl ii v c v(D o- n O �' v N rD rt v n o 3_ rD rD N v - �. 3 ((DD Q 0° N r-r 0 Q rD is rD 0 �,°0na r� w a O n Oq Cr + ro rt r- _ rD ro C N ro 0 -+, to ro w ,-+ ro n 3 0 n S ro O ° n =; 0 C Cr Sv O � O °� tv O rD ? 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S2 7 O ? n -h ,� (D (D fV •P W 0 0 1' I f+ X- rD o� w N h CL W W s sv w N t.� -n Oo -0 r, 0 CD �^ rD (D -s G Ln W 0- (D v 0Oq Sv (ND 0 iz z n (D O (D rD CLs W 0 N Q C N v 0 f) S rD rr M CD 1.., (D (D O m N a (D cn 0 a C o o V N 0 0 O ! j CL n p� O fD G fed � s 0 W S O V g Nw H t1i 9 v ® SV W N 0 m Ln M � OrQ 0 A S^ N a O . R� lD ® 0 N o ri 0 o v r O p O CD CACL r , ! O ! O M N W G) n S r ( 0 s 2 A u, -o r O ® v 0 � f UOt r ty ® Ro w a 00 Z d D vQ a -a r 0 N X N A 0 m v n m m 0 O csi N W V W AA� d� r z D m SA m m S� m m m s sx DGNR-DEMLR j\AooresvM(,' Land Quality Sectlan�e(, P1e�l®nal D e� r- > m m G) m 0 •0 z ;u G) 0 ® m > VS ❑❑ o mp SD -�. 0 � m jcu❑❑❑ 3 m G (D o 0N0 �+ N 0 ID 0 6❑ 4 2 v y S 00 0 ❑m n' S D G5 � ❑S ID V) X w z V) t•J v v (D @ N 0 w (D (D G) @ O 0 M rD v -, -v 0 (Drt rD`rt sc 0 @ O It D. C!Q rt � (D (DrD 0. ((DD O (D (D t) @ 3 04 N rt (D n v r) Ov 0 0 Ln rDrD rD (D 3 0 rD 0 0 0 rD rD 0 0 n S 3 v v 0 (D p 0 W rb � n h 0 � O h zD w v e4 O' z CL (D L D " � W � 3 4 @ N v B O D(D c (A 3 W r', z -® O D aa:0, w C) of z ul 0) D (A � G) m g m 2 cr O 0 ® � B t o P� DO (D CL g i S is r CA [ O D 1° n Ln C C C 0 3 o o o F 3 ma� W (D � ® O v' F 'a @ to O N N O c' rD M o- =s 3 @ 4 o CDm g D � �. @ O ® IZN rb M �r S. �. @ O cl � � O v3 O .� m O S Z @ @ rt @ N rD O rD rb m @ o D'Q y r V co vi A Q ul X v ® ® IJ MO ® (DO rD @ (D > @ XX J w J � o S = O O pm rD rD S R r < 3 S R @ 0 i � u N (D (D @ 0- (D rD O -° 3 - CD 3 6 a @ (D vi 0 0 v o v s (D 0 (D " (D rt g- 0 0 Q (D O O w (D o rD � o s G O v @ 'a 3 �. 0 O rt O @ � °rt 5 < @ v 0 C (n O N vrD 0 ZT m 3 0 O n@ O n N < (D r+ o v c(D �+ (D (D (D O 3 � O (D n -< 0 3 = 0- .T O -0 1+ rTq C+ _" O O O a@ O (n M - rD rt O @ O ]" Q L. rD @ (D 00 w "n :3 0- O 3 O rt (D Q; rD -V o @ rt O Q 0o 0 S — rt O „-Or, N 0 c S O 0 n 2— @ -0 : h h 0 0 Q O uQ O 0 @ y 3 s iv (<D O �• @ <ID S O W O O D O N r r+ :3 (D n v S v v rD O 0. v Q 0 (D n n rt r+ CfQ o O C .v-r O 's uQ Uq (D ° o :3 ((D - • < O (n C) rD n n O r1 c o (D o obi O � ,y. n ry. ''(' 3 " (D m a -a -� 3 v O (DO (n `wG : (D 0. v 0 (D ,y: < 3 3 n O O M cL (D 33 ro s�' O � O rD �' 3 (D uci v O -° (DD + ` O O O :3m c = 2. (Dv (D rt 3rD v rD N �. 3 0 0 0 @ 3 (D v rt �+ @ rt @ O (D v Q rt < x 3' 0 O On x S A 0 rD 0' (D -I 0- o O 3 rr v O @ 0 v N O O � UU 0 3 o o o F 3 ma� W (D � ® O v' F 'a @ to O N N O c' rD M o- =s 3 @ 4 o CDm g D � �. @ O ® IZN rb M �r S. �. @ O cl � � O v3 O .� m O S Z @ @ rt @ N rD O rD rb m @ o D'Q y r V co vi A Q ul X v ® ® IJ MO ® (DO rD @ (D > @ XX J w J � o S = O O pm rD rD S R r < 3 S R @ 0 i � u N (D (D @ 0- (D rD O -° 3 - CD 3 6 a @ (D vi 0 0 v o v s (D 0 (D " (D rt g- 0 0 Q (D O O w (D o rD � o s G O v @ 'a 3 �. 0 O rt O @ � °rt 5 < @ v 0 C (n O N vrD 0 ZT m 3 0 O n@ O n N < (D r+ o v c(D �+ (D (D (D O 3 � O (D n -< 0 3 = 0- .T O -0 1+ rTq C+ _" O O O a@ O (n M - rD rt O @ O ]" Q L. rD @ (D 00 w "n :3 0- O 3 O rt (D Q; rD -V o @ rt O Q 0o 0 S — rt O „-Or, N 0 c S O 0 n 2— @ -0 : h h 0 0 Q O uQ O 0 @ y 3 s iv (<D O �• @ <ID S O W O O D O N r r+ :3 (D n v S v v rD O 0. v Q 0 (D n n rt r+ CfQ o O C .v-r O 's uQ Uq (D ° o :3 ((D - • < O (n C) rD n n O r1 c o (D o obi O � ,y. n ry. ''(' 3 " (D m a -a -� 3 v O (DO (n `wG : (D 0. v 0 (D ,y: < 3 3 n O O M cL (D 33 ro s�' O � O rD �' 3 (D uci v O -° (DD + ` O O O :3m c = 2. (Dv (D rt 3rD v rD N �. 3 0 0 0 @ 3 (D v rt �+ @ rt @ O (D v Q rt < x 3' 0 O On x S A 0 rD 0' (D -I 0- o O 3 rr v O @ 0 v N O O � UU roKm ro - v M rr o rt � N rip PDI CDro 4Z o OO :3 pj rs -o S 0 � O rr ro v v rD m v o c 0 O ro O OU W -s v ro o ro a v m v sz aca v ivy S � ro O 3 3 N 0 v o v 0 3 0 o c 0-_0 c (cn: 3 v Q 3 N Q ua O fD ❑- a)m -6 - (n , $ o 3 O O _ r+ :3 sz P.. N O O :3 o o ro -h 3 0 C 1) � o, , - � zr O ro S. -o � ID o' �Q(� O m o D ro =3 3 v o n ro 5 1 n :3Q O O 'z :3 O � (A (nD c zr P o ao v 3 v G, n v to rt v UQ r�D o ° 3 v� :3 S Q O ro ro O_ N �• n 3 ro 0- 70 3 rr N O O N v m D Q m 5 < o o — p N < C) n rr (D v o n A � - v N J A m G) O z D r O _T C) m C) O z D z D m N 3 W 0 c G7 N m n :j N D -G m M W m ;a X m enWm7 m C') D D M N Z D do m m n z x O m D m m _r) AO D > -r{ Z m G m m Q = 0 m m G) Q O " m n D lJ��-i :�o O m m (,mj m D w O m y m D n m 'o r = _.{ C O m 56 m 'I9 > Dm m 7z -'i m X = -ZI n m m rn vmi p D m m m m MIN Z (7 O m Z m C ® N TI -n — oO D -I m N D m rn E M M m :m O D N W M ryM m A D m > zm z z oN z' M rn O m C --� m m A Fol D � r -i v D m Z C) O O El Z W aceAnalytical www,pacelabs.com February 05, 2020 iVE Mr. Jim Rozsa and NR-D1Quality :MLF Sectio v 5o nry s�;rte Reg;o Bendel Corp. at on 4823 North Graham St. Charlotte, NC 28269 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 RE: Project: Bendel Pace Project No.: 92462402 Dear Mr. Rozsa: Enclosed are the analytical results for sample(s) received by the laboratory on January 27, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, n 1 Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer Wheat, AECOM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, 8 without the written consent of Pace Analytical Services, LLC, Page 1 of 12 Pace Analytical Services, LLC /+p �} /� eA 1 �Val,4ical 9800 Kincey Ave. Suite too Huntersville, NC 28078 www,pacelabs.com (704)875-9092 CERTIFICATIONS Project: Bendel Pace Project No.: 92462402 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Bendel Pace Project No.: 92462402 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92462402001 SW-001 EPA 1664E HH 1 PASI-C EPA 200.7 Rev 4.4 1994 IDS 3 PASI-A SM 2540D-2011 CJL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 1nt%lAna1j&ai® www.pacelabs.com Project: Bendel Pace Project No.: 92462402 ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SW-001 Lab ID: 92462402001 Collected: 01/24/20 08:15 Received: 01/27/20 12:19 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 4.8 1 01/31/20 16:18 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 12.3 ug/L 5.0 1 02/01/20 00:58 02/04/20 11:49 7440-50-8 Lead ND ug/L 5.0 1 02/01/20 00:58 02/04/2011:49 7439-92-1 Zinc 122 ug/L 10.0 1 02/01/20 00:58 02/04/20 11:49 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 38.0 mg/L 10.0 1 01/29/20 17:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC, Page 4 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Bendel Pace Project No.: 92462402 QC Batch: 522598 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92462402001 METHOD BLANK: 2795061 Matrix: Water Associated Lab Samples: 92462402001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 01/31/20 16:01 LABORATORY CONTROL SAMPLE: 2795062 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 16.9 84 64-132 MATRIX SPIKE SAMPLE: 2795063 92461814002 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.2 17.7 88 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Bendel Pace Project No.: 92462402 QC Batch: 522647 Analysis Method: EPA 200.7 Rev 4.41994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92462402001 METHOD BLANK: 2795460 Matrix: Water Associated Lab Samples: 92462402001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 02/04/2011:36 Lead ug/L ND 5.0 02/04/2011:36 Zinc ug/L ND 10.0 02/04/2011:36 LABORATORY CONTROL SAMPLE: 2795461 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 477 95 85-115 Lead ug/L 500 478 96 85-115 Zinc ug/L 500 465 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2795462 2795463 MS MSD 92462402001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 12.3 500 500 524 520 102 101 70-130 1 Lead ug/L ND 500 500 508 512 101 102 70-130 1 Zinc ug/L 122 500 500 624 626 100 101 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC, Page 6 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Bendel Pace Project No.: 92462402 QC Batch: 522170 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92462402001 METHOD BLANK: 2792927 Matrix: Water Associated Lab Samples: 92462402001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 01/29/20 17:31 LABORATORY CONTROL SAMPLE & LCSD: 2792928 2792929 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Total Suspended Solids mg/L 250 248 234 99 94 90-110 6 25 SAMPLE DUPLICATE: 2792930 92462422002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 29.0 31.0 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 laneAnalj4icalo www.pacelabs.com QUALIFIERS Project: Bendel Pace Project No.: 92462402 IRL=l4li'lt<1I4ILb9 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Bendel 92462402 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92462402001 SW-001 EPA1664B 522598 92462402001 SW-001 EPA 200.7 Rev 4.4 1994 522647 EPA 200.7 Rev 4.4 1994 522670 92462402001 SW-001 SM 2540D-2011 522170 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 12 Document Name: Document Revised: February 7, 2018 m AnalyftCal F Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: F•CAR•CS-033•Rev.06 Issuing Authority: Pace Carolinas Quality Office Laboratory receiving samples: Asheville ® Eden[] Greenwood ❑ Huntersvill Raleigh❑ Mechanicsvillen • ° Client Na : l 1(::. / 1 Project: Courier: T[]Fed Ex [❑UP5 ❑USPS FlCilent Q Commercial 10Pace []other: 92462402 Custody Seal Present? ❑Yes 134o Seals intact? ❑Yes )Ji (- 1 /7 { f Date/lnitiais Person Examining Contents:--------y Packing Material: JJBubble Wrap _0Bubble�Bags (None ❑ Other Biological Tissue rozen? Thermome,.k�e,r,:. ®Yes ❑No, -]N/A un 10: 42T058 Type of Ice: f {Wet j�eiue QNane Cooler Temp (°C): ) ✓ V Correction Factor: Add/Subtract (°C) 0.0°C Temp should be above freezing to 6°C Cooler Temp Corrected (°C); i� u QSampies out of temp criteria. Samples nn ice, cooling process hasbegun USDA Regulated Soil j N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate tram a foreign source lint atianally, Ves QNo f including Hawarr No ruerro nicolr Ures fsawv Comments/Discrepancy: Chain of Custody Present? .�.lres 'r aro ` NIA 1. _ Samples Arrived within Hold Time? k [lies []No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? Yes ZNo QN/A 3. 4. _ Rush Turn Around Time Requested? [3Yes n a []N/A 5iiffieient Volume? Ves QNo []N/A 6. Correct Containers Used? . ]Yes QNo QN/A -Pace Containers Used? JOYes QNo N/A Containers intact? IYes QNo []N/A 7. Dissolved analysis: Samples Field Flitered? Sample labels Match COC? -Includes Date/Time/ID/Analysis Matrix: QYes .,OYes QNo ❑No -,ETN/A QN/A 9. Heads ace in VOA Vials (>5-6mm)? QYes QNo EKIA 10. Trip Blank Present? Trip Blank Custody Seai:: Present? _ []Yes ❑Yes A390 QNo ❑N%/A NIA Si. COMMENTS/SAMPLE OIS6EPANCY ° Field Data Required? ❑Yes ❑No Lot ID of split containers: _ CLIENT NOTIFICATION/RESOLUTION Parson contacted: Date/Time: Project Manager SCURF Review: �L1 Date: _ is Project Manager SRF Review: gate: Page 10 of 12 Document Name: Document Revised: February 7, 2018 aCeAnalytical Sample Condition Upon Recei t(SCUR) Page 1 of 2 Document No,: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or clechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHS "Bottom half of box is to list number of bottle Project # PM: NMO Due Date: 02/05/20 CLIENT 92—AECOM CHA Ej 2 N a c .0 ro J E a m 2 N P c u J E a m 2 a Z c i s d E s rO ¢ V a d ;, a m tJ v S v J E In a m v a m 0 Z o a E {p� a m O 1s a Z J E {A a ^ r o M J E a m a `� 0 9 v i, °vi V I. ¢ t9 ¢ v S n u C§ L 11 d 2 9 a = E dJ of �A Um' Q v � N Q `v x t9 ¢ x = T Q .-f E tpA <f 1 a`+ o �ry t7 $ ¢ z Q E O O, t7 6f ¢ ; m O _? E in > d Z a E O Qf t7 9 cpt h > E o Obi LA ® .NS '^�" 9 > '& rz� ? 9 v +. S ¢ � :9 J E in M u tom" p� J E 0 ry t s q Ow Z Z J E d a m 2 a C E J ri ¢ z 5 D. c N Z CX E q `, XV 2\N\N N\ 3 4 5. . 7 8 9 F12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 8 Note: Whenever there is a discrepancy auecung ivory Lnroium w,,,N„e„L= DG„n1i a wrr �.,- .- --. •..,� _...._ __...... _-.... Out of hold, incorrect preservative, out of temp, Incorrect containers. Page 11 of 12 -40 tD 3: S Y a' Q N A K_ �C D (0 0) V/ v n a M Page 12 of 12 aceAnalyfiical www,pacelabs.com February 05, 2020 Mr. Jim Rozsa Bendel Corp. 4823 North Graham St. Charlotte, NC 28269 RE: Project: Bendel Pace Project No.: 92462402 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Rozsa: Enclosed are the analytical results for sample(s) received by the laboratory on January 27, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer Wheat, AECOM ACC O._ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, M without the written consent of Pace Analytical Services, LLC. Page 1 of 12 Project: Bendel Pace Project No.: 92462402 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 12 ac.Analylical www.pacelabs.com Project: Bendel Pace Project No.: 92462402 Lab ID Sample ID 92462402001 SW-001 SAMPLE ANALYTE COUNT Method EPA 1664B EPA 200.7 Rev 4.4 1994 SM 2540D-2011 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Analysts Reported Laboratory HH 1 PASI-C DS 3 PASI-A CJL 1 PASI-A Page 3 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Bendel Pace Project No.: 92462402 Sample: SW-001 Lab ID: 92462402001 Collected: 01/24/20 08:15 Received: 01/27/20 12:19 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 4.8 1 01/31/20 16:18 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper Lead 12.3 ug/L 5.0 1 02/01/20 00:58 02/04/20 11:49 7440-50-8 Zinc ND ug/L 5.0 1 02/01/20 00:58 02/04/20 11:49 7439-92-1 122 ug/L 10.0 1 02/01/20 00:58 02/04/20 11:49 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 38.0 mg/L 10.0 1 01/29/20 17:36 Date: 02/05/2020 09:25 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 12 accAnapical© www.pacelabs.com Project: Bendel Pace Project No.: 92462402 QC Batch: 522598 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92462402001 METHOD BLANK: 2795061 Matrix: Water Associated Lab Samples: 92462402001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 01/31/2016:01 LABORATORY CONTROL SAMPLE: 2795062 Spike LCS Parameter Units Cone. Result Total Petroleum Hydrocarbons mg/L 20 16.9 MATRIX SPIKE SAMPLE: 2795063 92461814002 Spike Parameter Units Result Cone. Total Petroleum Hydrocarbons mg/L ND 19.2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 84 64-132 MS MS % Rec Result % Rec Limits Qualifiers 17.7 88 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 aceAnalydcal wim.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bendel Pace Project No.: 92462402 QC Batch: 522647 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92462402001 METHOD BLANK: 2795460 Matrix: Water Associated Lab Samples: 92462402001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L NO 5.0 02/04/2011:36 Lead ug/L NO 5.0 02/04/2011:36 Zinc ug/L NO 10.0 02/04/2011:36 LABORATORY CONTROL SAMPLE: 2795461 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug/L 500 477 95 85-115 Lead ug/L 500 478 96 85-115 Zinc ug/L 500 465 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2795462 2795463 MS MSD 92462402001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L 12.3 500 500 524 520 102 101 70-130 1 Lead ug/L NO 500 500 508 512 101 102 70-130 1 Zinc ug/L 122 500 500 624 626 100 101 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 ,�aceAnalyfical(9 www.pacelabs.com Project: Bendel Pace Project No.: 92462402 QC Batch: 522170 QC Batch Method: SM 2540D-2011 Associated Lab Samples: 92462402001 METHOD BLANK: 2792927 Associated Lab Samples: 92462402001 Parameter Analysis Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/G ND 2.5- 01/29/201731 LABORATORY CONTROL SAMPLE& LCSD: 2792928 2792929 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. ' Result Result %Rec % Rec Limits RPD RPD Qualifiers Total Suspended Solids mg/L 250 248 234 99 94 90-110 6 25 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE DUPLICATE: 2792930 92462422002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 29.0 31.0 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 acepnalytical o www.pacelabs.com Project: Bendel Pace Project No.: 92462402 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/05/2020 09:25 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 aceAnaficai� www.pacelabs.cem Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bendel Pace Project No.: 92462402 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92462402001 SW-001 EPA1664B 522598 92462402001 SW-001 EPA 200.7 Rev 4.4 1994 522647 EPA 200.7 Rev 4.4 1994 522670 92462402001 SW-001 SM 2540D-2011 522170 Date: 02/05/2020 09:25 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 12 m aCE'A1780 Ca! Document Name: Sample Condition Upon Recelpt(SCUR) document Revised: February 7, 2018 Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.05 Pace Carolinas Quality Office Packing Material: ]Bubble Wrap ulrbie Bags (None [3 Other Thermometer` Type of fee! /ffWet [fBluo [2iR un ID: 9,21058 Cooler Temp ('C): ) ✓ V Correction Factor: Add/Subtract (°C) 0.0°C Cooler Temp Corrected (•C):--t=,-=- USDA Regulated 5o9 Q N/A, water sample) Did samples orlainatein a quarantine zone within the United States: CA, NY, or SC (check maps)? Biological Tissue. rozen? ❑None ®Yes ❑No,.-M/A Temp should be above freezing to VC []5ampies out of temp criteria. Samples nn ice, cooling process hasbegun Did samples originate from a foreign source (Igoptionaily, FlYes QNa including Hawaii MCI PuertO rncoN Uyes /r5.iwo Comments/Discrepancy: Chain of Custody Present? ..(r-rres ' 04a ;]N/A 1. Samples Arrived within Hold Time? ! :,ffYes []No ®N/A 2. Short Hold Time Analysis (<72 hr.)? E]Yes ErNo ®N/A 3. Rush Turn Around Time Requested? []Yes .,-fNa QN/A 4. SurficiantVolume7 )=i�10 N/A. ) 5. Correct Containers Used? Face Containers Used? ®Yes QNo yes ❑No ®N/A []NIA 6. Containers Intact?. d� iYes []No ®N/A' 7. _ Dissolved analysis: Samples Field_Fiitered? . []Yes []No >E N/A a. _ Sample Labels Match COC? -includes Date/Time/ID/Analysis Yes ON. Matrix: J 1 []N/A 9. Headspace in VOA Vials (>5-6mm)? (]Yes [JN_o i/A 10. Trip Blank present? Trip Blank Custody Sea'ss Present? ®Yes ,®No ❑Yes C]Na ©N/A/A N/A 11. COMMENTS/SAMPLE OI5CREPANCY e Field Data Required? ®Yes []NO Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Pgrson contacted: oate/rme: Project Manager SCURF Review: W(l) Date: / tJ N s 6 Project Manager SRF Review: Date: J �7 Page 10 of 12 •.. a .ceAnatytical Document Name: Sample Condition Ripon Recelpt(SCUR) document Revised: February 7, 2018 Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified. and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box Is to list number of bottle $ s 4 C U VEn a no 4 2 C 'D V }_' E a Q 2 �.. U 1^ a Co ? aroi ti j a a a Wm V.. x v O' U o' E- N H ®. V s rn z U .�yj� .# E- to O Cz „ ct 4 J E N w 6 u x x O tJ u� J € In f� to a m w a m — N ia,, 5 f 67 w E' a a s�-t 67 d ry a d M a ti 6 Z a a _ m �7 x c a _Q rui i7 d a O i� N .O -- M 67 Q a e E � N Q m m l°t dcl z Q J E 67 z, a 'N Q. o �.. >.. am t7 J E al 67 d O M O J. E. al 69 = Q f0 o > 6 % r z � ut E a 2 cu ,-,. {�.(yy , aV @ a a do' E J E L'9 a .�.. Vl E.: v. c u d E C7 '.. 2 i 6 ' 7NN a 9 zo 11 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon recelpt Date preservation adjusted Time preservation adjusted Amount of preservative added Lot 8 .n .,.,,: e...... ..auk...,.....,, .k-., n,....k nCLM0 r.Mr—finn riff — fi a Note: WheneverthereisamscrepancyanecnnglvuruiLu+ut".0w„Yna,.'.�o,.,r,,, ,,_. .._.------..---- -------------_ out of hold, incorrect preservative, out of temp, incorrect containers. Page 11 of 12 Page 12 of 12 laceAnalytical www,pacelabs.com February 14, 2020 Mr. Jim Rozsa Bendel Corp. 4823 North Graham St. Charlotte, NC 28269 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 RE: Project: Bendel Pace Project No.: 92463864 Dear Mr. Rozsa: Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer wheat, AECOM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 Project: Bendel Pace Project No.: 92463864 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 12 Project: Bendel Pace Project No.: 92463864 Lab ID Sample ID 92463864001 SW-001 SAMPLE ANALYTE COUNT Method EPA 1664E EPA 200.7 Rev 4.4 1994 SM 2540D-2011 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Analysts Reported Laboratory WAM 1 PASI-C SH1 3 PASI-A CJL 1 PASI-A Page 3 of 12 laneAnalj4ical@ www.pacelabs.com Project: Bendel Pace Project No.: 92463864 ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SW-001 Lab ID: 92463864001 Collected: 02/05/20 13:20 Received: 02/05/20 14:06 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 5.0 1 02/14/20 09:14 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper ND ug/L 5.0 1 02/11/20 00:57 02/13/20 00:02 7440-50-8 Lead ND ug/L 5.0 1 02/11/20 00:57 02/13/20 00:02 7439-92-1 Zinc 138 ug/L 10.0 1 02/11/20 00:57 02/13/20 00:02 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 12.2 mg/L 2.5 1 02/07/20 18:00 Date: 02/14/2020 04:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Bendel Pace Project No.: 92463864 QC Batch: 525180 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92463864001 METHOD BLANK: 2807148 Matrix: Water Associated Lab Samples: 92463864001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 02/14/20 09:14 LABORATORY CONTROL SAMPLE: 2807149 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.8 79 64-132 MATRIX SPIKE SAMPLE: 2807150 92463731002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 16.3 70 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 2111k\1111111VAP19P►III III Ze107�r�31 Project: Bendel Pace Project No.: 92463864 QC Batch: 524325 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92463864001 METHOD BLANK: 2803088 Matrix: Water Associated Lab Samples: 92463864001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 02/12/20 23:56 Lead ug/L ND 5.0 02/12/20 23:56 Zinc ug/L ND 10.0 02/12/20 23:56 LABORATORY CONTROL SAMPLE: 2803089 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper ug/L 500 498 100 85-115 Lead ug/L 500 472 94 85-115 Zinc ug/L 500 461 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2803090 2803091 MS MSD 92463864001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 524 484 104 96 70-130 8 Lead ug/L ND 500 500 500 499 100 100 70-130 0 Zinc ug/L 138 500 500 631 589 99 90 70-130 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Bendel Pace Project No.: 92463864 QC Batch: 523819 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92463864001 METHOD BLANK: 2800612 Matrix: Water Associated Lab Samples: 92463864001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 02/07/20 17:55 LABORATORY CONTROL SAMPLE: 2800613 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 248 99 90-110 SAMPLE DUPLICATE: 2800630 92463819001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 28.0 25.8 8 SAMPLE DUPLICATE: 2800631 92463831001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 5450 3320 49 D6 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 leAnalytical www.pacclabs.com QUALIFIERS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bendel Pace Project No.: 92463864 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC, Page 8 of 12 aceAnalytieal e www.pacefabs.com Project: Bendel Pace Project No.: 92463864 QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Nuntersville, NC 28078 (704)875-9092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92463864001 SW-001 EPA1664B 525180 92463864001 SW-001 EPA 200.7 Rev 4.4 1994 524325 EPA 200.7 Rev 4.4 1994 524346 92463864001 SW-001 SM 2540D-2011 523819 Date: 02/14/2020 04:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 12 Document Name: Document Revised: February 7, 2018 I'l-_i aCeAnalyf cal Sample Condition U on Recei t(SCUR) Page 1 of 2 Document No.: Issuing Authority. J F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood❑ Huntersvilleff e 11 Date/initials Person Examining Contents; Packing Material• -Bubble Wrap 39ubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes ❑No ❑N/A 92'T058 Type ofIce: ❑Wet ❑®Iua ONane R Gun ID: / Cooler Temp ('C): _AA `1J_ ____ Correction Factor: Add/Subtract ('C) 0.0°C iT Temp ski Auld be above freezing to 6'C Cooler Temp Corrected ('C): ©samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil 0 N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Intern "I oy, r—a..__ f7i— 1-11" inc uawaii and puartnRirnl? r-1Yes Comments/Discrepancy: Chain of Custody Present? 4es []NO ❑N/A 1. Samples Arrived within Hold Time? e®Yes ®No N A 2. Short Hold Time Analysts 1<72 hr.)? []Yes No ❑N/A 3. Rush Turn Around Time Requested? Ves o ❑N/A 4. Sufficient Volume? _ [lyes No N/A 5. Correct Containers Used? -Pace Containers Used? ewes ElVes []No (]No (]N/A [jN/A 6. Containers Intact? r Yes QNo (]N/A 7. Dissolved analysis: Samples Field Filtered? []Yes ONO (]N/A a. Sample Labels Match COC? Date/Time/ID/Analysis 10Yes Matrix:�_____ I-Includes []NO ON/a 9. Heads ace in VOA Vials (>S-6mm)? ❑Yes ❑No QN/A 10, Trip Blank Present? Trip Blank Custody Seals Present? []Yes FlVm ONO No ❑ N/A [f]f A il. d Data Requir d? Elves ONO COMMENTS/SAMPLE DISCREPANCY Field `- � � ' s U Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Y " 'l,`i� Date: ��t) Project Manager SRF Review: (V ? Date: (p Page 10 of 12 Document Name: Document Revised: February 7, 201E •ceAnalytical ,i a Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: / F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box If pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, t.tHg "Bottom half of box is to list number of bottle s z a k E N N a m Z z u Y}� id E O M a6~9U' to z a m a " y id E N m ez ` C C = w se .; •'4 rn a p iQ•j T v E N tiny Q 0 ? m O iz 2 " E M m 0r a Z N `-' E N NC m 5 c 's O 2 to E N to a a t7 5 a P�. 4 Z c, C to `av M 3 Q x a 4J °sFi d a s Q 2 n E N a a= a 4 `i N a w r1 4 A S J tpE� M tM,7 Q •V..• 2 $' E 'rt d rt L� Q Q z V a E a Q' m 0 N E C .`z., C a E p > v � E ® LA o > z T a } 4 s > u N J E vNi i a E O w m i Z m a E N Co z.. > . c E E E 4 C > c O E N > 1 ? a C 7 E q O I N\ 2- 3 A S 6 7 8 g 10 11 12 I.- IN NNN pH Adjustment log for Preserved Samples Sample lD Type of Preservative pit upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot a Note: Whenever there is a mscrepancy anecung warm c.arvar,d L-Ump-- �o,.,N ��rr •• •••• -•• Out of hold, incorrect preservative, out of temp, incorrect containers. Page 11 of 12 fN O A O 7 D I O n j A 3 @ 3: 7 Y N 3 Z O �1.,, G �(� N 1 O0 `f f V/ , c/� U 4U .� � 1 0 m .1 D � m ;U G (D 3 N (� N C w O {N n O W CD a a) 0 n C Q� fD �C Page 12 of 12 aceAnalical www.pacelabs.com February 14, 2020 Mr. Jim Rozsa Bendel Corp. 4823 North Graham St. Charlotte, NC 28269 RE: Project: Bendel Pace Project No.: 92463864 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Rozsa: Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, lZ r f.I ; XIIIL-2 L3cZ,2 Nicole Gasiorowski nicole.gasiorowski@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Jennifer Wheat, AEC OM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 12 amAnalytical www.pacelabs.com Project: Bendel Pace Project No.: 92463864 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 12 Q ac�AnaJyical www,pacclabs.com SAMPLE ANALYTE COUNT Project: Bendel Pace Project No.: 92463864 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analyses Method Analysts Reported Laboratory Lab ID Sample ID 92463864001 SW-001 EPA 1664B WAM 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 254OD-2011 CJL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 A�;a)xAnalydical@ www,pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Bendel Pace Project No.: 92463864 Sample: SW-001 Lab ID: 92463864001 Collected: 02/05/20 13:20 Received: 02/05/20 14:06 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 5.0 1 02/14/20 09:14 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper ND ug/L 5.0 1 02/11/20 00:57 02/13/20 00:02 7440-50-8 Lead ND ug/L 5.0 1 02/11/20 00:57 02/13/20 00:02 7439-92-1 Zinc 138 ug/L 10.0 1 02/11/20 00:57 02/13/20 00:02 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 12.2 mg/L 2.5 1 02/07/20 18:00 Date: 02/14/2020 04:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 12 '2 aceAnalj4ical www.pacclabs.com 0 i �' • tit _i Project: Bendel Pace Project No.: 92463864 QC Batch: 525180 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92463864001 METHOD BLANK: 2807148 Matrix: Water Associated Lab Samples: 92463864001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 02114/20 09:14 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2807149 Spike LCS LCS %Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.8 79 64-132 MATRIX SPIKE SAMPLE: 2807150 92463731002 Spike MS MS %Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 16.3 70 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 12 accAnalytical www.pacelabs.com Project: Bendel Pace Project No.: 92463864 QC Batch: 524325 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92463864001 METHOD BLANK: 2803088 Matrix: Water Associated Lab Samples: 92463864001 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper ug/L ND 5.0 02/12/20 23:56 Lead ug/L ND 5.0 02/12/20 23:56 Zinc ug/L ND 10.0 02/12/20 23:56 LABORATORY CONTROL SAMPLE: 2803089 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper ug/L 500 498 100 85-115 Lead ug/L 500 472 94 85-115 Zinc ug/L 500 461 92 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2803090 2803091 MS MSD 92463864001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Copper ug/L ND 500 500 524 484 104 96 70-130 8 Lead ug/L ND 500 500 500 499 100 100 70-130 0 Zinc ug/L 138 500 500 631 589 99 90 70-130 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 12 accAnalydicai" www,pacelabs.com !t _ . ` . ' f _ ,._ Project: Bendel Pace Project No.: 92463864 QC Batch: 523819 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92463864001 METHOD BLANK: 2800612 Matrix: Water Associated Lab Samples: 92463864001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 02/07/2017:55 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: ` 2800613 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 251 248 99 90-110 SAMPLE DUPLICATE: 2800630 92463819001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 28.0 25.8 8 SAMPLE DUPLICATE: 2800631 92463831001 Dup" Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 5450 3320 49 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12 �aceAnalyiical o www.pacolabs.com Project: Bendel Pace Project No.: 92463864 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 { a Huntersville, NC 28078 laceAnalydcal (704)875-9092 wvAv.paccelaabs.cam QUALITY CONTROLS DATA CROSS REFERENCE TABLE Project: Bendel Pace Project No.: 92463864 Analytical Batch Lab ID Sample ID QC Batch Method QC Batch Analytical Method ®— 92463864001 SW-001 EPA1664B 525180 200 7 Rev 4 41994 524346 92463864001 SW-001 92463864001 SW-001 EPA 200.7 Rev 4.4 1994 524325 EPA SM 2540D-2011 523819 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/14/2020 04:32 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 12 Document Name: document Revised; February 7, 2018 Sample Condition Upon Recelpt(SCUR) Page 1 of 2 aceAnalyflcdl Document No,: issuing Authority: F•CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: MEN Custody Seal Present? Dyes ,ONO Seals Intact? ®Yes -ONO Mechanicsville[] Date/initials Person Examining Contents: Packing Material: Bubble Wrap ten- ubble Bags [None [] Other Biological `tissue Frozen? Thermometer: s Elyes ®No ❑N/A C058 Type of ice: [wet QBlue ©None R sun ID: 42 Cooler Temp ('C): /1 Correction Factor: Add/Subtract (°C) O.0°C Temp �s ould be above freezing to 6°C Looter Temp Corrected ("C):. QSampies out of temp crite(ia. Samples on ice, cooling process USDA Regulated Soli NIA, water sample) has begun Did samples ❑ Originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internlo a y, Yes ,No Including Hawaii and Puerto Rico)? (-1Yes PI -NO l Chain of Custody Present? Cafes ONO ❑N/A 1 1. Sample .Arrivedwithin Hold Time? nusn t urn Around Time Requested? 'DYes o ❑N/A 4. nt Volume? it Yes QNo ❑N/Atl.,t Containers Used? �[7ves ®No (�N/A e Containers Used? Des QNo ONJA ers Intact? Yes ®No ❑N/A 7. ed analysis: Samples Field Filtered? ❑Yes ONO MIA e. labels Match COL? IBlank es L]No ❑N/A 9. udes Date/Time/ID/Analysis Matrix: ace in VOA Walt (>5-5mm)? DYes [No EJN/A 10, nk Present? ❑Yes No []NIA 11. nk Custody Seats Present? DYes ©No IAA COMMENTS/SAMPLL,EE��D��IS��CREPANC�Y Lot ID of split containers: CI.It;NT NOTIFICATiQN/RESOLUTION Person contacted: Date[fime: Field Data Required? Elves QNo Project Manager SCURF Review: N ' sz� Date: 1(p � Project Manager SRF Review; Aw `fir— Date: j(Q Page 10 of 12 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recelpt(SCUR) page 1 of 2 aceAnalyticar Document No.: Issuing Authority: f F-CAR-CS-O33•Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Ail and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle E a m a t,, m E N z n u m E O N m Q.0.m V , ski. u ro. FL E C0 N Z w a ,n- �Ma a 0. N va O u m E N �jjM �. N % p u E A 0.m 4ri �+ u m , E N 'I m ,-t A Q O sr 16 + �En N X w j m m �- v_ "C3 a E d Q/ N. 49 d v n a E Q r+ t9 4 d N c ,gyp E 4 E cr N U' 4 N v O a E ¢ oa 4 v N E S E f� N LA l7 Q u �. p N tnrn' l°I 4 T ¢ 0 E U` cs Z 4 0 -' E l'J > 2 a 0 J E t7 ? 2 rri T ¢ 0 E 0 2 0. ++ .Y a a ro a �' x ® a a X u �, a S �. 1 3 4 v", a uy E ,n Ni fly. w \ m a .c #v `� E o N ri '0. ut ct Ln u t% ° �' E 'n N M m z c .m G J E a O 9tR 4 S^v e N to ut z 0J a a p E Q E Ot. 1 / ! a 3' f 9' SO 11 12 pH Adjustment Log for preserved Samples sample iD Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added tot H _ _ _ _ �^nu nF thic rnrm will ha cant to tha Nnnh Carolina DUINR Certification Office (i.e. Note Note: Wheneverthere isadiscrepancy a ec ng or r , Out of hold, incorrect preservative, out of temp, incorrect containers. Page 11 of 12 jo =F CD :C > z C) C: ,CL rn' cn 03 r- 0 M 0 > M z 03 CD (D EL U) U) rH 0 os ro 0 Page 12 of 12