WQ0012404_Annual Report_20190301 (2)

February 19, 2019
North Carolina Department of Environmental Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Attention: Non -Discharge Compliance Unit
Reference: 2018 Annual Report
Land Application Program
CF Nitrogen, Inc.
Permit No. WQ0012404
S&ME Project No. 1040-98-044S
Non -Discharge Compliance Unit:
Mkt 01 2G19
RECEIVEDI► CN701DWR
MAR - 1 2019
Non -Discharge
Permitting Unit
S&ME, Inc. (S&ME) is submitting all monitoring and reporting requirements as specified in the above referenced permit for CF
Nitrogen, Inc. S&ME compiled this report using data gathered during the compliance year. This data includes: 1) Certification
Form, 2) Residual Sampling Summary Form, 3) 2018 Application Summary and Field Loading Rate Reports, 4) Field Application
Summaries, 5) Updated Attachment B, 6) Landowner Agreement Attachments & Lessee Agreement Attachments, and 7)
Groundwater Report.
CF Nitrogen, Inc. conducted land application events on current permitted fields in Bertie, Hertford, and Northampton Counties
within the year of 2018. A total of 12,758,000 gallons of nitrogen -enriched groundwater were land applied.
TCLP, Pathogen and Vector Monitoring, and Soil Analysis are not included in the report as these requirements are not
required by Permit based on the permitted operation of a groundwater recovery system only.
If there is any further information required or questions regarding this land application program please do not hesitate to
contact us for further assistance.
Sincerely,
S&ME, Inc.
Jason Volker, LSS Edmund Woloszyn, Jr., REM
Project Manager Principal Scientist/Project Manager
[e-mail] [e-mail]
cc: Mr. John A. Foster, CHMM (CF Nitrogen, Inc.)
Ms. Jeanette Stanley (NCDEQ — Superfund Section)
Mr. Jay Bryant (Granville Farms)
S&ME, Inc. 13201 Spring Forest Road I Raleigh, NC 27616 1 p 919.872.2660 1 www.smeinc.com

Water Resources
ENVIRONMENTAL QUALITY
PAT MCCRORY
Core°rnor
DONALD R. VAN DER VAART
S. JAY ZIMMERMAN
Director
January 25, 2016
JOHN A. FOSTER —MANAGER
CF NITROGEN, INC.
4 PARKWAY NORTH — SUITE 400
DEERFIELD, ILLINOIS 60015-2590
Dear Mr. Foster:
Subject: Permit No. WQ0012404
CF Nitrogen, Inc.
CF Nitrogen Site in Tunis, NC
Land Application of Nitrogen -
Enriched Ground Water
Hertford County
In accordance with your permit renewal request received June 22, 2015, and subsequent additional
information received January 4, 2016 and January 11, 2016, we are forwarding herewith Permit No.
WQ0012404 dated January 25, 2016, to CF Nitrogen, Inc. for the continued operation of the subject
nitrogen -enriched ground water land application program.
This permit shall be effective from the date of issuance until December 31, 2020, and shall be
subject to the conditions and limitations as specified therein. Please pay particular attention to the
monitoring requirements listed in Attachments A, B and C for they may differ from the previous permit
issuance. Failure to establish an adequate system for collecting and maintaining the required operational
information shall result in future compliance problems.
Please note the following permit conditions have been removed since the last permit issuance
dated December 9, 2011:
➢ Old Conditions II.1. & II.2. —These conditions are inherently covered under new Condition
II.1.
➢ Old Conditions III.3. & ITI.4. — These conditions are inherently covered under new Condition
III.5.
➢ Old Conditions III.5, 6 & 7 — These conditions are inherently covered under new Condition
ITI.7., which describes conditions which prohibit the application of nitrogen -enriched ground
water.
State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919 807 6464

Mr. John A. Foster
January 25, 2016
Page 2 of 2
Please note the following permit conditions are new since the last permit issuance dated
December 9, 2011:
➢ Condition I.3. —This condition requires the submission of an Operation and Maintenance Plan.
➢ Condition III.2. — This condition requires the maintenance of an Operation and Maintenance
Plan.
➢ Condition III.4. — This condition requires the presence of copies of the permit and the Operation
and Maintenance manual whenever an application event takes place.
➢ Condition VI.6. — This condition allows the permit to be revoked or modified under certain
circumstances.
➢ Condition VI.7. — This condition prohibits the expansion of the facilities if certain conditions
are present.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding.
If you need additional information concerning this permit, please contact David Goodrich at (919)
807-6352 or david.goodrichAncdenr. og_v.
Sincerely,
S. Jay Zimmerman, P.G., Director
Division of Water Resources
cc: Bertie County Health Department (Electronic Copy)
Hertford County Health Department (Electronic Copy)
Northampton County Health Department (Electronic Copy)
Washington Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Raleigh Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Files

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
LAND APPLICATION OF NITROGEN -ENRICHED GROUND WATER
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
CF Nitrogen, Inc.
Hertford County
FOR THE
continued operation of a nitrogen -enriched groundwater recovery system for CF Nitrogen, Inc. and
consisting of:
nine recovery wells with a transfer pump station and a one million gallon storage basin with a groundwater
transfer and loading system with dual loading bays for the tanker trucks; the operation of a nitrogen -
enriched ground water land application program consisting of the application of up to 20,000,000 gallons
per year of nitrogen -enriched ground water from the CF Nitrogen site in Tunis, NC; and all associated
piping, valves, control and appurtenances
to the approved sites listed in Attachment B in nearby counties with no discharge of wastes to surface
waters, pursuant to the application for permit renewal received June 22, 2015, and subsequent additional
information received by the Division of Water Resources, and in conformity with other supporting data
subsequently filed and approved by the Department of Environmental Quality and considered a part of this
permit. Additional land can be included into the program upon execution of the Landowner Agreement and
Lessee Agreement attached to this permit. This permit does not exempt the Permittee from complying with
the federal regulations.
This permit shall be effective from the date of issuance until December 31, 2020 shall void Permit No.
WQ0012404 issued December 9, 2011, and shall be subject to the following specified conditions and
limitations:
I. SCHEDULES
The nine monitoring wells and four piezometers at Site Number 11, shown on Figure 1 and listed in
Attachment C, shall be properly maintained. Well abandonment, if necessary, shall be coordinated
through the Division of Waste Management's Inactive Sites Branch. Within 30 days of abandonment,
a Well Abandonment Record (Form GW-30) listing this permit number and the appropriate monitoring
well identification number shall be completed for each well abandoned and mailed to the Division of
Water Resources, Water Quality Permitting Section, Non -Discharge Permitting Unit, 1617 Mail
Service Center, Raleigh, NC 27699-1617. A North Carolina Certified Well Contractor shall abandon
the monitoring wells according to the North Carolina Well Construction Standards (15A NCAC 02C
.0113) and local county rules. [15A NCAC 02C .0113, 02T .0108(b)(2)]
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No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application.
[15A NCAC 02T .0108(b)(2), 02T .105(d), 02T .0109]
3. The Permittee shall submit the Operation and Maintenance (O&M) plan as required in Condition 111.4.
to the Division within 90 days of the effective date of this permit. [15A NCAC 02T .0108(b)(2)]
II. PERFORMANCE STANDARDS
The subject nitrogen -enriched ground water land application program shall be effectively maintained
and operated at all times so there is no discharge to surface waters, nor any contravention of
groundwater or surface water standards. In the event the facilities fail to perform satisfactorily,
including the creation of nuisance conditions due to improper operation and maintenance, the Permittee
shall immediately cease land applying nitrogen -enriched ground water to the approved application area,
contact the appropriate regional office supervisor, and take any immediate corrective actions. [G.S.
143-215.1]
2. The nine monitoring wells (C-22, C-23, C-28, C-29, C-32, C-33, MWI-3, MWI-4, and MWI-6) and
four piezometers (PI-2, PI-11, PO-12 and PO-236) at Site Number 11, shown on Figure 1 and listed in
Attachment C, shall be properly maintained. Well abandonment, if necessary, shall be coordinated
through the Division of Waste Management's Inactive Sites Branch. Within 30 days of abandonment,
a Well Abandonment Record (Form GW-30) listing this permit number and the appropriate monitoring
well identification number shall be completed for each well abandoned and mailed to the Division of
Water Quality, Water Quality Permitting Section, 1617 Mail Service Center, Raleigh, NC 27699-1636.
A North Carolina Certified Well Contractor shall abandon the monitoring wells according to the North
Carolina Well Construction Standards (15A NCAC 02C .0113) and local county rules. Replacement
monitor wells shall be coordinated through the Division of Waste Management's Inactive Sites Branch
and approved by the Washington Regional Office, telephone number [phone], prior to their
installation. The regional office shall be notified at least 48 hours prior to the construction of any
monitoring well, and such notification to the Water Quality Regional Operations Section's regional
supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State
Holidays. The monitoring wells shall be constructed such that the water level in the monitoring well is
never above or below the screened (open) portion of the well at any time during the year, and in
accordance with 15A NCAC 02C .0108. [15A NCAC 02C .0113, .0108]
3. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this program. [15A NCAC 02B .0200, 02L .0100]
4. Only the land application sites owned by individuals or corporations who have signed a completed
Landowner Agreement Attachment and, if applicable, a Lessee Agreement Attachment, are approved
to receive nitrogen -enriched ground water as a nitrogen amendment for crop growth. A completed
Landowner Agreement and Lessee Agreement (see Attachments D and E) must be kept on file by the
Permittee and available for inspection. The appropriate Attachments (FORM: CF Industries LOAA
01072016 for landowners and FORM: CF Industries LAA 01072016 for lessees) will be signed and
submitted to the Division as part of the residuals annual report. [15A NCAC 02T .0108(b)(1)]
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5. Setbacks for the application areas shall be as follows:
Setback Description
Setback
(feet)
Private or public water supply
100
Surface waters (streams — intermittent and perennial, perennial waterbodies, and
100
wetlands
Surface water diversions (ephemeral streams, waterways, ditches)
25
Groundwater lowering ditches (where the bottom of the ditch intersects the
25
SHWT)
Wells with exception to monitoring wells
100
Bedrock outcrops
25
[15A NCAC 02T .1108]
6. Land application areas shall be clearly marked on each site prior to and during any nitrogen -enriched
groundwater application event. [15A NCAC 02T .0108(b)(1)]
7. Nitrogen -enriched ground water and other sources of Plant Available Nitrogen (PAN) shall not be
applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using
expected nitrogen requirements based on the determined Realistic Yield Expectations (RY ,) using any
of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http://nutrients.soil.ncsu.edp/yields/index.php). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(http://www.ncagrr.gov/SWC/tech/documents/9th Guidance Doc 100109.pdf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards (ftp://ftp-fc.sc.egov.usda.gov/NHO/practice-standards/standards/590.pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T .1109(b)(1)(k)]
If land application sites are to be over -seeded or double -cropped (e.g., Bermuda grass in the summer
and rye grass in the winter with both crops to receive nitrogen -enriched ground water), then the second
crop can receive an application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr).
This practice may be allowed as long as the second crop is to be harvested or grazed. If the second
crop is to be planted for erosion control only and is to be tilled into the soil, then no additional PAN
shall be applied. [15A NCAC 02T .0108(b)(1)]
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The use of spray irrigation equipment for application of the nitrogen -enriched ground water is approved
by this permit, provided all permit restrictions are met and appropriate backflow prevention, as
approved by the North Carolina Public Water Supply Division, is in place to protect the potable water
supply. [15A NCAC 02T .0108(b)(1)]
10. These nitrogen -enriched ground water application sites were individually permitted on or after
December 30, 1983; therefore, the compliance boundary is established at either 250 feet from the
residual land application area, or 50 feet within the property boundary, whichever is closest to the
nitrogen -enriched ground water application area. An exceedance of groundwater standards at or
beyond the compliance boundary is subject to remediation action according to 15A NCAC 02L
.0106(d) (2) as well as enforcement actions in accordance with North Carolina General Statute 143-
215.6A through 143-215.6C. Any approved relocation of the COMPLIANCE BOUNDARY will be
noted in Attachment B. [15A NCAC 02L .0107(a)]
11. The review boundary shall be established midway between the compliance boundary and the nitrogen -
enriched ground water application area. Any exceedance of groundwater standards at the review
boundary shall require action in accordance with 15A NCAC 02L .0106. [15A NCAC 02L .0108]
III. OPERATION AND MAINTENANCE REQUIREMENTS
1. The land application program shall be properly maintained and operated at all times. The program shall
be effectively maintained and operated as a non -discharge system to prevent any contravention of
surface water or groundwater standards. [15A NCAC 02T .1110]
2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan). Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan,
which pertains primarily to the land application equipment used at land application fields will, at a
minimum, include:
a. Operational functions that include the replacement or rehabilitation of recovery well components;
b. Maintenance schedules;
c. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
ii. Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
[15A NCAC 02T .1100]
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3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC
08G .0201. The ORC or his back-up shall visit the land application sites in accordance with 15A NCAC
08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition 11I. 2.), and
shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding
classification and designation requirements, please contact the Division of Water Resources' Protection
and Enforcement Branch at [phone]. [15A NCAC 02T .0117]
4. When the Permittee land applies nitrogen -enriched ground water, a copy of this permit and a copy of
O&M Plan shall be maintained at the land application sites during land application activities. [15A
NCAC 02T .0108(b)(1)]
Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying
nitrogen -enriched ground water from the surface disposal sites or storage sites onto adjacent properties
or into surface waters. [15A NCAC 02T .1109(c)(2)(C)]
6. With the exception of Site 11, no nitrogen -enriched ground water shall be stored at any land application
site, unless written approval has been requested and received from the Division. [G.S. 143-215.1]
Temporary storage in a 12,000 gallon tanker trailer at a specific land application site may be maintained
only during the application process. [15A NCAC 02T .0108(b)(1)]
7. Nitrogen -enriched ground water shall not be land applied under the following conditions:
a. If the nitrogen -enriched ground water is likely to adversely affect a threatened or endangered
species listed under section 4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the nitrogen -enriched ground water or the application causes the
contravention of surface water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
nitrogen -enriched ground water would occur;
e. Within the 100-year flood elevation, unless the nitrogen -enriched ground water is injected or
incorporated within a 24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied nitrogen -enriched groundwater, or if the slope
is greater than 18% for injected or incorporated nitrogen -enriched ground water;
h. If the land does not have an established vegetative cover unless the nitrogen -enriched ground water
is incorporated or injected within a 24-hour period following a nitrogen -enriched ground water
application event. Any field that is in a USDA no -till program shall be exempted from meeting this
vegetative cover requirement;
i. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
j. If the vertical separation of bedrock and the depth of residuals application is less than one foot;
k. Application exceeds agronomic rates.
[15A NCAC 02T .1109]
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Only the land application sites owned by individuals who have signed a completed Landowner
Agreement Attachment and, if applicable, a Lessee Agreement Attachment, are approved for nitrogen -
enriched ground water land application. A completed Landowner Agreement Attachment and Lessee
Agreement Attachment (see Attachments D and E) must be kept on file by the Permittee and available
for inspection. The appropriate Attachments (FORM: CF Industries LOAA 01072016 for landowners
and FORM: CF Industries LAA 01072016 for lessees) will be signed and submitted to the Division as
part of the residuals annual report. [ 15A NCAC 02T .1104(c)(4)]
9. The Permittee shall not land apply nitrogen -enriched ground water to a land application site owned by
others unless the agreement between the Permittee and the landowner/lessee or operators (see attached
forms) is in full force and effect. The Landowner Agreement Attachment (FORM: LOAA 01072016)
shall be considered renewed at the same time the permit is renewed. Should a landowner or lessee
terminate its agreement with the Permittee, the Permittee shall inform the Washington Regional Office,
Water Quality Regional Operations Section, to remove all of the sites associated with that owner or
lessee from the list of sites on Attachment B. If the Lessee has changed during a given permit cycle,
the Lessee Agreement Attachment (FORM: LAA 01072016). [15A NCAC 02T .I 104(c)(4)]
IV. MONITORING AND REPORTING REQUIREMENTS
1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses)
necessary to ensure groundwater and surface water protection shall be established, and an acceptable
sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
2. The nitrogen -enriched ground water shall be analyzed to demonstrate they are non -hazardous under the
Resource Conservation and Recovery Act (RCRA). Nitrogen -enriched ground water that tests or is
classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be used or disposed under this
permit. The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching
procedure (TCLP)] shall be performed at the frequency specified in Attachment A, and the Permittee
shall maintain these results for a minimum of five years. Any exceptions from the requirements in this
condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1, 1 -Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Heptachlor (and its hydroxide)
0.008
Toxaphene (0.5)
Chloroform (6.0)
Hexachloro-1,3-butadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
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[15A NCAC 13A .0102(b), 02T .1101, 02T .1105]
3. An analysis shall be conducted on the nitrogen -enriched ground water every 90 days, and the Permittee
shall maintain the results for a minimum of five years. The analysis shall include the following
parameters:
Aluminum
Nitrate -Nitrite Nitrogen
Plant Available Nitrogen
(by calculation)
Ammonia -Nitrogen
Total Kjeldahl Nitrogen
Potassium
Calcium
pH
Sodium
Magnesium
Phosphorus
[15A NCAC 02T .1101]
4. Analytical determinations made pursuant to the monitoring and reporting requirements of this permit
shall be made by a laboratory certified by the Division for the required parameters under 15A NCAC
2H .0800 or 15A NCAC 211.1100. Field analyses are exempted from this requirement. [15A NCAC
02H .0800 or .1100]
5. Monitoring wells shall be sampled at the frequencies and for the parameters specified in Attachment
C. The Permittee shall develop groundwater contour maps of the system and map this data as
groundwater contours. This is to be sufficient in aerial extent and density to describe the general pattern
of the water level elevation. The maps shall include access to the field and monitoring points, and cross -
sectional view maps that depict water levels across the slurry wall. [15A NCAC 02T .0105(m)]
6. Any monitoring (i.e., including groundwater, surface water, soil, or plant tissue analyses) deemed
necessary by the Division to ensure protection of the environment shall be established, and an
acceptable sampling and reporting schedule shall be followed.
7. Analytical determinations made pursuant to the monitoring and reporting requirements of this permit
shall be made by a laboratory certified by the Division for the required parameter(s) under 15A NCAC
2H .0800 or 15A NCAC 2H .1100. Field analyses are exempted from this requirement.
8. Proper records shall be maintained by the Permittee tracking all application events. These records shall
include, but are not necessarily limited to, the following information:
a. Date of nitrogen -enriched ground water application;
b. Location of nitrogen -enriched ground water application (site, field, or zone #);
c. Type of crop or crops to be grown on land application site;
d. Volume of nitrogen -enriched ground water applied in gallons per acre;
e. Continuous weekly, monthly, and year-to-date hydraulic (inches/acre) loadings for each land
application site; and
f. Annual totals, for each land application site, of plant available nitrogen (PAN) from the nitrogen -
enriched ground water (lbs/acre); annual totals, for each land application site, of phosphorous
applied from all sources (lbs/acre), fertilizers applied (other than from the nitrogen -enriched ground
water) (lbs. of PAN/acre); and annual totals, for each field, of PAN from all sources.
[15A NCAC 02T .0108(b)(1)]
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V.
9. Three copies of an annual report shall be submitted on or before March 1 St. The annual report shall
meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms.
Instructions for reporting and annual report forms are available at
http://portal.ncdenr.or web/wq/aps/lau/reporting, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T .1 I I l (a)]
10. Noncompliance Notification
The Permittee shall report by telephone to the Washington Regional Office, telephone number (252)
946-6481, as soon as possible, but in no case more than 24 hours or on the next working day following
the occurrence or first knowledge of the occurrence of any of the following:
a. Any failure of the nitrogen -enriched ground water application program resulting in a release of
material to surface waters.
b. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
c. Any process unit failure, due to known or unknown reasons rendering the facility incapable of
adequate residual treatment.
d. Any spill or discharge from a vehicle or piping system during nitrogen -enriched ground water
transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone]. Persons
reporting such occurrences by telephone shall also file a written report in letter from within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b) (1)]
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
groundwater recovery, storage and transfer system and shall be in accordance with the approved O&M
Plan. [15A NCAC 02T .0108(b)]
Prior to each nitrogen -enriched ground water application event, the Permittee or his designee shall
inspect the nitrogen -enriched ground water storage, transport and application facilities to prevent
malfunctions, facility deterioration and operator errors resulting in discharges, which may cause the
release of wastes to the environment, a threat to human health or a public nuisance. The Permittee shall
maintain an inspection log that includes, at a minimum, the date and time of inspection, observations
made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this
inspection log for a period of five years from the date of inspection, and this log shall be made available
to the Division upon request. [15A NCAC 02T .0108(b)]
WQ0012404 Version 3.0 Shell Version 151201 Page 8 of 9

3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or groundwater remediation
facilities permitted herein at any reasonable time for the purpose of determining compliance with this
permit; may inspect or copy any records required to be maintained under the terms and conditions of
this permit; and may collect groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)]
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to
143-215.6C. [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the nitrogen -enriched ground water application events are not
carried out in accordance with the conditions of this permit. [15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of the nitrogen -enriched ground
water described in the permit application and other supporting documentation. [G.S. 143-215.1 ]
4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Permit NCGO10000; any requirements pertaining to wetlands under 15A
NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [15A NCAC 02T .0105(c)(6)]
In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60 days' notice from the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [ 15A NCAC 02T .0110]
7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b).
[15A NCAC 02T .0120]
8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
.0105(e)(3)]
Permit issued this the 251 day of January 2016
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
S. Jay Zimmerman, P.G., Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0012404
WQ0012404 Version 3.0 Shell Version 151201 Page 9 of 9

ATTACHMENT A - Approved Residual Sources Certification Date: January 25, 2016
CF Nitrogen, Inc. Permit Number: WQ0012404 Version: 3.0
Nitrogen -Enriched Ground Water Source -Generating Facility
Approved
Monitoring
Monitoring
Monitoring
Mineralization
Permit
Biological
Maximum
Frequency for
Frequency for
Frequency for
Rate
Owner
FacilityName
County
ty
Number
Residuals
Gallons
Non -hazardous
Metals and
Pathogen &
og
[Raw = 0.4;
Per Year
Characteristics 2
Nutrients 3
Vector Attraction
Aerobic = 0.3;
Reductions
Anaerobic = 0.2;
compost = 0.1
CF Nitrogen, Inc.
CF Nitrogen in Tunis, NC
Hertford
WQ0012404
No
20,000,000
1 X Permit Cycle
4 X year
N/A
N/A
Total
20,000,000
I . Maximum Gallons per Year is the amount of nitrogen -enriched ground water approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition IV.3.
If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no
sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual
report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification.
WQ0012404 Version 3.0 Attachment A Page I of I

THIS PAGE BLANK

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Field/
Site
Owner
Lessee
County
Latitude
Longitude
Net
Acreage
Dominant Soil Series
Footnotes
29-1
Ronald Byrd
Bettie
36009'30"
-76057'54"
6.7
Leaf— Lf
29-2
Ronald Byrd
Bettie
36009'31"
-76058'02"
2.4
Leaf— Lf
29-3
Ronald Byrd
Bettie
36009'31"
-76058'09"
6.2
Exum — ExA
29-4
Ronald Byrd
Bettie
36009'27"
-76058'09"
9.8
Exum — ExA
29-5
Ronald Byrd
Bettie
36009'27"
-76058'20"
11.1
Exum —ExA
29-6
Ronald Byrd
Berie
36009'25"
-76058'34"
3.1
Leaf — Lf
29-7
Ronald Byrd
Bettie
36009'24"
-76058' 10"
4.6
Granthum — Gt
29-8
Ronald Byrd
Bettie
36009'21"
-76058'05"
9.9
Granthum — Gt
29-9
Ronald Byrd
Bettie
36009'24"
-76058'00"
0.5
Exum —ExA
29-10
Ronald Byrd
Bettie
36009'24"
-76057'56"
4.0
Exum — ExB
30-1
Kendred C. Williams, Jr.
Bettie
36008' 15"
-76057' 12"
15.4
Exum —ExA
30-2
Kendred C. Williams, Jr.
Bettie
36008'22"
-76057' 13"
6.1
Exum — ExA
30-3
Kendred C. Williams, Jr.
Bettie
36012'47"
-76056'35"
1.3
Craven — CrA
30-4
Kendred C. Williams, Jr.
Bettie
36012'45"
-76056'22"
26.3
Norfolk — NoB
30-5
Kendred C. Williams, Jr.
Bettie
36012'43"
-76056'OT'
32.4
Craven — CrB
30-6
Kendred C. Williams, Jr.
Bettie
36012'31"
-76056'09"
9.0
Craven — CrB
30-7
Kendred C. Williams, Jr.
Bettie
36012'38"
-76056'25"
12.9
Craven — CrB
30-8
Kendred C. Williams, Jr.
Bettie
36012'40"
-76056'34"
6.5
Craven — CrB
30-9
Kendred C. Williams, Jr.
Bettie
36012'41"
-76056'49"
16.4
Norfolk —NoA
30-10
Kendred C. Williams, Jr.
Bettie
36012'45"
-76056'47"
3.7
Norfolk —NoA
30-11
Kendred C. Williams, Jr.
Bettie
36012'48"
-76056'45"
1.4
Norfolk —NoB
30-12
Kendred C. Williams, Jr.
Bettie
36012'48"
-76056'39"
1.5
Norfolk —NoA
30-13
Kendred C. Williams, Jr.
Bettie
36012'51"
-76056'41"
5.1
Lenoir— Ln
WQ0012404 Version 3.0 Attachment B Page 1 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
30-14
Kendred C. Williams, Jr.
Bettie
36012'56"
-76056'38"
0.5
Lenoir— Ln
30-15
Kendred C. Williams, Jr.
Bettie
36013'03"
-76056'36"
8.9
Leaf— Lf
30-16
Kendred C. Williams, Jr.
Bettie
36013'09"
-76056'31"
4.5
Craven — CrA
30-17
Kendred C. Williams, Jr.
Bettie
36013'06"
-76057'03"
28.1
Craven — CrA
30-18
Kendred C. Williams, Jr.
Bettie
36012'55"
-76057'00"
20.9
Craven — CrA
30-19
Kendred C. Williams, Jr.
Bettie
36012'54"
-76056'48"
9.3
Goldsboro —GOA
30-20
Kendred C. Williams, Jr.
Bettie
36012'13"
-76056'51"
10.7
Craven — CrA
30-21
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012'23"
-76056'48"
7.0
Lenoir— Ln
30-22
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012' 16"
-76056'53"
7.5
Craven — CrA
30-23
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012' 16"
-76056'59"
9.2
Craven — CrA
30-24
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012' 18"
-76057'02"
3.8
Craven — CrA
30-25
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012' 19"
-76057'05"
1.5
Craven — CrA
30-26
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012'26"
-76057' 12"
4.3
Craven — CrA
30-27
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012'16"
-76057'08"
4.0
Craven—CrA
30-28
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012' 13"
-76057'09"
5.1
Craven — CrA
30-29
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bettie
36012'08"
-76057'OT'
13.3
Craven — CrA
30-30
Kendred C. Williams, Jr.
Bettie
36010'35"
-76057'25"
4.5
Nahunta — Na
30-31
Kendred C. Williams, Jr.
Bettie
36010'28"
-76057'24"
20.8
Exum — ExA
30-32
Kendred C. Williams, Jr.
Bettie
36010'24"
-76057' 15"
7.5
Goldsboro — GoA
30-33
Kendred C. Williams, Jr.
Bettie
36010' 18"
-76057' 19"
17.8
Goldsboro — GoA
30-34
Kendred C. Williams, Jr.
Bettie
36010' 18"
-76057' 18"
24.1
Goldsboro — GoA
30-35
Kendred C. Williams, Jr.
Bettie
36010'20"
-76057'37"
0.9
Exum — ExA
30-36
David C. Powell
Kendred C. Williams, Jr.
Bettie
36013' 13"
-76054'33"
19.9
Exum — ExA
30-37
E.M. Powell & Sons, Inc.
Kendred C. Williams, Jr.
Bettie
36013'07"
-76054'26"
21.2
Exum — ExA
30-38
E.M. Powell & Sons, Inc.
Kendred C. Williams, Jr.
Bettie
36012'49"
-76054'30"
23.4
Exum — ExA
WQ0012404 Version 3.0 Attachment B Page 2 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Field/
Site
Owner
Lessee
County
Latitude
Longitude
Net
Acreage
Dominant Soil Series
Footnotes
30-39
E.M. Powell & Sons, Inc.
Kendred C. Williams, Jr.
Bertie
36012'42"
-76054'24"
25.4
Exum —ExA
30-40
T.E. Ruffin
Kendred C. Williams, Jr.
Berne
36009'22"
-76057'24"
19.9
Exum — ExA
30-41
T.E. Ruffin
Kendred C. Williams, Jr.
Bertie
36009'23"
-76057'37"
7.0
Exum — ExA
30-42
T.E. Ruffin
Kendred C. Williams, Jr.
Bertie
36009'26"
-76057'43"
4.7
Exum —ExA
30-43
T.E. Ruffin
Kendred C. Williams, Jr.
Bertie
36009'23"
-76057'46"
7.0
Exum — ExA
30-44
James C. Askew
Kendred C. Williams, Jr.
Bertie
36011' 18"
-76057'21"
2.8
Exum — ExB
30-45
James C. Askew
Kendred C. Williams, Jr.
Bertie
36011' l8"
-76057' 1 T'
6.3
Exum — ExB
30-46
James C. Askew
Kendred C. Williams, Jr.
Bertie
36011' 1 T'
-76057' 10"
12.0
Gritney — Gt
30-47
Oliver B. Balance
Kendred C. Williams, Jr.
Bertie
36011' 12"
-76057'08"
11.6
Exum —ExA
33-17
Leonard L. Godwin
William Ward
Bertie
36013'38"
-77000'05"
11.2
Norfolk —NoA
33-18
Leonard L. Godwin
William Ward
Bertie
36013'31"
-76059'55"
11.2
Goldsboro — GoA
33-19
Ola Sanders
William Ward
Bertie
36012'15"
-76056'09"
16.8
Goldsboro—GoA
33-20
Ruth H. Metcalf
William Ward
Bertie
36014'16"
-76054'30"
3.3
Exum—ExA
33-21
Ruth H. Metcalf, et al
William Ward
Bertie
36014'02"
-76054'24"
12.9
Exum — ExA
33-22
Mildred Harris
William Ward
Bertie
36013'53"
-76054'12"
17.0
Exum—ExA
33-23
Agnes O. Moore, et al
William Ward
Bertie
36013'42"
-76054'09"
9.5
Goldsboro — GoA
County Total
Berne
653.6
Goldsboro — GoA
3-1
Wiley B. Gillam III
Hertford
36019'51"
-76050'39"
19.6
Lynchburg - Ly
3-2
Wiley B. Gillam III
Hertford
36019'44"
-76050'43"
37.2
Lynchburg - Ly
3-3
Wiley B. Gillam III
Hertford
36019'45"
-76050'28"
19.9
Norfolk — NoA
3-4
Wiley B. Gillam III
Hertford
36019'27"
-76048'06"
18.6
Wickham — WkB
3-5
Wiley B. Gillam III
Hertford
36019'02"
-76048'02"
31.9
Tarboro — TaB
6-1
Stuart Pierce Farms, Inc.
Hertford
36016'06"
-76056'20"
17.0
Craven — CrA
6-2
Stuart Pierce Farms, Inc.
Hertford
36016' 18"
-76056'20"
67.4
Caroline — CaA
6-3
Stuart Pierce Farms, Inc.
Hertford
36016'09"
-76055'58"
7.9
Caroline — CaA
WQ0012404 Version 3.0 Attachment B Page 3 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Sitd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
64
Stuart Pierce Farms, Inc.
Hertford
36015'54"
-76056' 16"
10.9
Caroline — CaA
6-5
Stuart Pierce Fauns, Inc.
Hertford
36015'47"
-76056'56"
54.0
Caroline — CaA
6-6
Stuart Pierce Farms, Inc.
Hertford
36015'36"
-76056'34"
23.3
Craven — CrB
6-7
Stuart Pierce Farms, Inc.
Hertford
36015'27"
-76056' 11"
42.2
Craven — CrB
6-9
Stuart Pierce Farms, Inc.
Hertford
36016'01"
-76057' 17"
38.9
Craven — CrA
6-10
Stuart Pierce Farms, Inc.
Hertford
36016'43"
-76055'34"
107.0
Caroline - CaA
6-11 A
Stuart Pierce Farms, Inc.
Hertford
36015'S2"
-77000'07"
41.0
Craven — CrB
6-11B
Stuart Pierce Farms, Inc.
Hertford
36015'41"
-76059'53"
72.2
Craven — CrB
6-11 C
Stuart Pierce Farms, Inc.
Hertford
36015'37"
-76059'40"
29.4
Craven — CrB
6-11 D
Stuart Pierce Farms, Inc.
Hertford
36015'24"
-76059'45"
41.2
Craven — CrB
6-1 1E
Stuart Pierce Farms, Inc.
Hertford
36015'36"
-76059'37"
47.7
Craven — CrA
6-12
Stuart Pierce Fauns, Inc.
Hertford
36018'30"
-77001'47"
40.4
Caroline — CaA
6-13
Stuart Pierce Farms, Inc.
Hertford
36018'27"
-76054'52"
41.4
Craven — CrA
6-14
Stuart Pierce Farms, Inc.
Hertford
36018' 10"
-76054'59"
30.9
Craven — CrA
6-15
Stuart Pierce Farms, Inc.
Hertford
36018' 14"
-76055' 18"
48.8
Craven — CrB
6-16
Stuart Pierce Farms, Inc.
Hertford
36016'51'
-76045'06"
46.1
Bonneau — BoB
6-17
Stuart Pierce Farms, Inc.
Hertford
36016'44"
-76045'38"
41.9
Bonneau — BoB
6-18
Stuart Pierce Farms, Inc.
Hertford
36017'04"
-76045'33"
21.0
Bonneau — BoB
6-19
Stuart Pierce Farms, Inc.
Hertford
36016'33"
-76043'56"
46.3
Goldsboro —GoA
6-20
Stuart Pierce Farms, Inc.
Hertford
36016'06"
-76044' 18"
21.4
Goldsboro — GoA
6-21
Stuart Pierce Fauns, Inc.
Hertford
36017'S0"
-76043' 10"
70.8
Bonneau — BoB
6-22
Stuart Pierce Farms, Inc.
Hertford
36016' 19"
-77002'38"
56.4
Craven - CrA
6-23
Stuart Pierce Farms, Inc.
Hertford
36016'32"
-77002'41"
94.9
Craven - CrA
6-24
Stuart Pierce Fauns, Inc.
Hertford
36016'20"
-77002'23"
41.6
Lenoir — Ln
WQ0012404 Version 3.0 Attachment B Page 4 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
9-2
Gray Pierce, et al
Hertford
36018'20"
-76051'l0"
18.5
Norfolk - NoA
9-3
Gray Pierce
Hertford
36018' 14"
-76051'20"
8.5
Norfolk - NoA
9-5
Carlyle Archer, et al
Gray Pierce
Hertford
36018'13"
-76051'37"
22.8
Norfolk—NoA
9-6
Gray Pierce
Hertford
36018' 15"
-76051'46"
4.5
Goldsboro — GoA
9-7
Gray Pierce
Hertford
36018'07"
-76051'28"
16.2
Norfolk — NoA
9-8
Gray Pierce
Hertford
36018'03"
-76051'36"
11.6
Norfolk — NoA
9-9
Gray Pierce
Hertford
36017' 15"
-76051'30"
18.1
Craven — CrB
9-10
Gray Pierce
Hertford
36017'59"
-76051'30"
5.6
Craven — CrB
9-11
Gray Pierce
Hertford
36017'45"
-76051' 19"
10.6
Craven — CrB
9-12
Gray Pierce
Hertford
36017'48"
-76051'05"
8.6
Conetoe—CoB
9-14
Gray Pierce
Hertford
36017'50"
-76050'58"
6.7
Tarboro — TaB
9-15
Gray Pierce
Hertford
36017'58"
-76050'50"
7.7
Tarboro — TaB
9-16
Gray Pierce
Hertford
36017'58"
-76051'22"
1.5
Craven — CrB
9-17
Gray Pierce
Hertford
36018'01"
-76051'21"
3.6
Craven — CrB
9-18
Gray Pierce
Hertford
36017'50"
-76051'25"
14.6
Wickham — WkA
9-19
Gray Pierce
Hertford
36017'59"
-76051'l0"
3.7
Tarboro—TaB
9-20
Gray Pierce
Hertford
36018'06"
-76051'13"
3.9
Bonneau — BoB
9-21
Gray Pierce
Hertford
36017'38"
-76051'49"
6.0
Craven — CrA
9-22
Gray Pierce
Hertford
36017'45"
-76051'49"
9.6
Lenoir — Ln
9-24
Gray Pierce
Hertford
36017'47"
-76051'43"
13.5
Craven — CrA
9-26
Gray Pierce
Hertford
36018'34"
-76051'45"
27.0
Craven — CrA
9-27
Gray Pierce
Hertford
36019' 12"
-76051'48"
24.9
Tarboro — TaB
9-28
Gray Pierce
Hertford
36018'51"
-76052'01"
15.0
Wickham — WkA
9-29
Gray Pierce
Hertford
36018'47"
-76051'57"
5.7
Wickham — WkA
9-30
Gray Pierce
Hertford
36° 18'44"
-76051'53"
11.9
Wickham — A"
WQ0012404 Version 3.0 Attachment B Page 5 of 16

i
ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
9-31
Gray Pierce, Merle Jones
Gray Pierce
Hertford
36017'48"
-76052'45"
11.4
Craven — CrA
9-32
Merle Jones
Gray Pierce
Hertford
36017'34"
-76052'36"
17.6
Lenoir— Ln
9-33
Gray Pierce
Hertford
36017'37"
-76052' 10"
16.7
Craven — CrA
9-34
Gray Pierce
Hertford
36017'52"
-76053'00"
7.6
Craven — CrA
9-35
Gray Pierce
Hertford
36017'58"
-76052'55"
13.4
Craven — CrA
9-37
R.C. Kennington
Gray Pierce
Hertford
36018'33"
-76052'45"
15.8
Craven — CrB
9-38
R.C. Kennington
Gray Pierce
Hertford
36018'27"
-76052'32"
7.6
Craven — CrB
9-40
Gray Pierce
Hertford
36019'21"
-76053'33"
11.2
Wickham — WkB
9-41
Gray Pierce
Hertford
36019'33"
-76053'28"
12.4
Wickham — WkA
9-42
Gray Pierce
Hertford
36019'23"
-77001'20"
26.4
Caroline — CaA
9-43
Gray Pierce
Hertford
36019' 16"
-77000'38"
39.4
Caroline — CaA
9-45
Gray Pierce
Hertford
36019' 11"
-77006'56"
73.7
Craven — CrA
9-46A
Gray Pierce
Hertford
36019' 19"
-77007'49"
36.7
Craven — CrA
9-46B
Gray Pierce
Hertford
36019' 15"
-77007'27"
42.5
Craven — CrA
9-47
Gray Pierce
Hertford
36019'33"
-77008'09"
18.8
Craven — CrA
948
Gray Pierce
Hertford
36018'32"
-77006'31"
45.1
Craven — CrA
9-50
Gray Pierce
Hertford
36018'53"
-77006'43"
63.8
Craven — CrA
9-52
Gray Pierce
Hertford
36018'57"
-77007'03"
27.4
Craven — CrA
9-53
Gray Pierce
Hertford
36019'06"
-77007'13"
26.7
Craven — CrB
10-1
J.H. Drewry, III
Hertford
36032'36"
-77009'01"
7.8
Tarboro — TaB
10-2
J.H. Drewry, III
Hertford
36032'30"
-77008'36"
34.1
Wickham — WkA
10-3
J.H. Drewry, III
Hertford
36032' 17"
-77008'33"
67.7
Autryville — AuB
104
J.H. Drewry, III
Hertford
36032'35"
-77008' 16"
6.9
Lynchburg — nLy
10-5
J.H. Drewry, III
Hertford
36032'58"
-77008' 17"
20.0
Norfolk — NoA
10-6
J.H. Drewry, III
Hertford
36052'21"
-77007'56"
35.0
Craven — CrA
WQ0012404 Version 3.0 Attachment B Page 6 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Field/
Site10-7
Owner
Lessee
County
Latitude
Longitude
a
Acreage
Dominant Soil Series
Footnotes
J.H. Drewry, III
Hertford
36032' 17"
-77008'07"
35.4
Norfolk — NoA
10-8
J.H. Drewry, III
Hertford
36032' 15"
-77008' 18"
42.3
Norfolk — NoA
10-9
J.H. Drewry, III
Hertford
36032'24"
-77007'46"
12.3
Autryville — AuB
10-10
J.H. Drewry, III
Hertford
36032'27"
-77007'41"
26.3
Bonneau — BoB
10-11
J.H. Drewry, III
Hertford
36032'01"
-77007'07"
4.9
Norfolk — NoA
11-1
CF Industries, Inc.
Granville Farms, Inc.
Hertford
36022' 19"
-76052' 10"
40.4
Craven — CrA
11-2
CF Industries, Inc.
Granville Farms, Inc.
Hertford
36022' 17"
-76051'47"
67.2
Craven — CrA
11-3
CF Industries, Inc.
Granville Farms, Inc.
Hertford
36022'01"
-76051'54"
41.4
Craven — CrA
12-1
Douglas R. White
Tuscarora Greens
Hertford
36023'03"
-76054'59"
8.3
Lenoir — Ln
12-2
Douglas R. White
Tuscarora Greens
Hertford
36022'57"
-76055' 11"
8.8
Lenoir — Ln
12-3
Douglas R. White
Tuscarora Greens
Hertford
36022'40"
-76054'57"
6.3
Craven — CrB
12-4
Douglas R. White
Tuscarora Greens
Hertford
36022'43"
-76054'46"
30.0
Craven — CrA
12-5
Douglas R. White
Tuscarora Greens
Hertford
36022'33"
-76054'51"
5.0
Craven — CrA
12-6
Douglas R. White
Tuscarora Greens
Hertford
36022'55
-76054'52"
18.0
Craven — CrA
23-1
Johnny Powell
Hertford
36017'01"
-76044'02"
24.9
Norfolk—NoA
23-2
Johnny Powell
Hertford
36016'42"
-76045' 12"
13.1
Norfolk — NoA
23-3
Thaddeus F. Scott
Johnny Powell
Hertford
36017'46"
-76045'44"
39.1
Norfolk — NoA
234
Thaddeus F. Scott
Johnny Powell
Hertford
36017'55"
-76045'44"
22.0
Norfolk — NoA
23-5
Johnny Powell
Hertford
36018' 19"
-76047' 17"
27.7
Norfolk — NoB
23-6
Johnny Powell
Hertford
36018'02"
-76050'25"
19.9
Conetoe—CoB
23-7A
Johnny Powell
Hertford
36017'42"
-76049'32"
33.5
Craven — CrA
23-713
Johnny Powell
Hertford
36018'03"
-76049' 10"
13.2
Bonneau — BoB
23-8
Johnny Powell
Hertford
36017' 12"
-76053'00"
29.8
Caroline — CaA
23-9
Johnny Powell
Hertford
36019'50"
-76051'05"
19.8
Craven — CrA
23-10
Johnny Powell
Hertford
36020'26"
-76049'47"
15.8
Craven — CrA
WQ0012404 Version 3.0 Attachment B Page 7 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
FSttd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
23-12
Johnny Powell
Hertford
36022'27"
-76054'50"
26.3
Craven — CrA
23-13
Johnny Powell
Hertford
36021'38"
-76054'02"
20.5
Craven — CrA
23-14
Johnny Powell
Hertford
36021'46"
-76054'23"
11.7
Craven — CrA
23-15
Johnny Powell
Hertford
36022'38"
-76056'02"
19.0
Norfolk — NoA
23-16
Johnny Powell
Hertford
36018'35"
-76055'42"
45.0
Craven — CrB
24-2
Chester Powell
Hertford
36019' 15"
-76050'40"
14.6
Norfolk — NoA
24-3
Chester Powell
Hertford
36019'28"
-76050'34"
11.6
Wickham — WkB
24-4
Chester Powell
Hertford
36018'56"
-76048'52"
10.8
Goldsboro — GoA
24-5
Chester Powell
Hertford
36018'43"
-76048'52"
13.0
Bonneau — BoB
24-6
Chester Powell
Hertford
36020'24"
-76051'54"
13.5
Craven — CrA
24-7
Chester Powell
Hertford
36020' 17"
-76051'46"
3.6
Craven — CrA
24-8
Chester Powell
Hertford
36015'50"
-76056'33"
6.3
Lenoir —Ln
24-9
Chester Powell
Hertford
36015'50"
-76053'54"
12.7
Craven — CrA
24-10
Shirley Deramus
Chester Powell
Hertford
36018'04"
-76043'20"
6.1
Bonneau — BoB
24-11
Shirley Deramus
Chester Powell
Hertford
36018'09"
-76043' 13"
10.5
Goldsboro — GoA
24-13
Chester Powell
Hertford
36015'23"
-76049'06"
14.8
Craven — CrA
25-1
Tommy Castelow
Hertford
36021'58"
-76053'54"
39.8
Caroline — CaA
25-2
Tommy Castelow
Hertford
36019'46"
-76049'06"
9.3
Norfolk — NoA
25-3
Tommy Castelow
Hertford
36020'02"
-76049'03"
32.2
Norfolk — NoA
25-4
Tommy Castelow
Hertford
36020' 17"
-76049'02"
30.2
Craven — CrA
25-5
Tommy Castelow
Hertford
36020'09"
-76048'42"
25.6
Craven — CrA
25-6
Tommy Castelow
Hertford
36020'00"
-76047'36"
27.2
Craven — CrA
25-7
Tommy Castelow
Hertford
36021' 16"
-76047'38"
12.3
Craven — CrA
25-8
Tommy Castelow
Hertford
36020'43"
-76054'05"
16.6
Craven — CrA
25-9
Tommy Castelow
Hertford
36020'37"
-76054'01"
34.7
1 Craven — CrA
WQ0012404 Version 3.0 Attachment B Page 8 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
F3rtd/
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
25-10
Tommy Castelow
Hertford
36020'26"
-76054'07"
11.3
Craven — CrA
25-11
Tommy Castelow
Hertford
36020'25"
-76054' 13"
4.8
Craven — CrA
25-12
Tommy Castelow
Hertford
36020'01"
-76054'28"
32.0
Craven — CrA
26-1
Beechwood Country Club
Hertford
36021'58"
-77000'38"
7.9
Caroline — CaA
26-2
Beechwood Country Club
Hertford
36021'53"
-77000'47"
10.5
Craven — CrB
26-3
Beechwood Country Club
Hertford
36021'37"
-77000'37"
8.3
Craven — CrB
26-4
Beechwood Country Club
Hertford
36021'43"
-77000'01"
18.2
Caroline — CaB
27-52
Lori S. Burgess
Steven Burgess
Hertford
36025'02"
-77006'01"
44.7
Norfolk — NoA
27-53
Lori S. Burgess
Steven Burgess
Hertford
36024'42"
-77005'55"
10.0
Norfolk — NoA
27-54
Steven Burgess
Hertford
36024'36"
-77006'06"
42.7
Norfolk — NoA
27-55
Steven Burgess
Hertford
36021' 18"
-77007'40"
6.6
Craven — CrA
27-56
Steven Burgess
Hertford
36021' 19"
-77007'31"
9.8
Craven — CrA
27-57
Steven Burgess
Hertford
36021'22"
-77007'21"
11.7
Craven — CrA
27-58
Steven Burgess
Hertford
36021' 11"
-77007' 17"
4.5
Lenoir — Ln
27-59
Steven Burgess
Hertford
36021'08"
-77007'23"
9.0
Lenoir — Ln
27-60
Steven Burgess
Hertford
36021'03"
-77007'07"
2.3
Lenoir — Ln
27-61
Steven Burgess
Hertford
36021'04"
-77006'59"
14.9
Craven — CrA
27-62
Steven Burgess
Hertford
36020'55"
-77007'02"
3.1
Craven — CrA
27-63
Adam & Wendy Burgess
Steven Burgess
Hertford
36021' 14"
-77006'55"
14.7
Craven — CrA
27-64
Adam & Wendy Burgess
Steven Burgess
Hertford
36021'24"
-77006'50"
29.5
Craven — CrA
28-1
Judith, Allison, & Walter Perry
Hertford
36019'31"
-77050'15"
17.6
Norfolk—NoA
28-2
Judith, Allison, & Walter Perry
Hertford
36019'27"
-76050'05"
17.5
Norfolk — NoA
28-3
Judith, Allison, & Walter Perry
Hertford
36019'48"
-76050' 10"
25.1
Norfolk — NoA
28-4
Judith, Allison, & Walter Pent'
Hertford
36019'21"
-76049'51"
10.8
Wickham — WkA
28-5
Judith, Allison, & Walter Perry
Hertford
36019'10"
-76049'34"
9.4
Conetoe— CoB
WQ0012404 Version 3.0 Attachment B Page 9 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
28-6
Judith, Allison, & Walter Perry
Hertford
36019'24"
-76050'24"
20.4
Norfolk — NoA
28-7
Judith, Allison, & Walter Perry
Hertford
36019'50"
-76051'03"
16.0
Norfolk — NoA
28-8
Judith, Allison, & Walter Perry
Hertford
36019'42"
-76051'06"
9.2
Goldsboro — GoA
28-9
Judith, Allison, & Walter Perry
Hertford
36019'42"
-76051'13"
9.9
Goldsboro — GoA
28-10
Judith, Allison, & Walter Perry
Hertford
36019'44"
-76051' 18"
1.7
Goldsboro — GoA
28-11
Judith, Allison, & Walter Perry
Hertford
36019'48"
-76051' 15"
3.7
Craven — CrB
28-12
Judith, Allison, & Walter Perry
Hertford
36019'47"
-76051' 11"
3.6
Craven — CrB
28-13
John Lock Mitchell
Walter Perry
Hertford
36017'42"
-76049'37"
8.7
Bonneau — BoB
28-14
John Lock Mitchell
Walter Perry
Hertford
36017'36"
-76049'45"
7.0
Bonneau — BoB
28-15
Betty Perry, John Mitchell, Eleanor Lane, Penny
Beasley, & Ken Mitchell
Walter Perry
Hertford
36017' 19"
-76050' 11"
17.4
Craven — CrA
28-16
John Mitchell, Eleanor Lane, Penny Beasley, Ken
Mitchell, & Wiccacon Properties, LLC
Walter Perry
Hertford
36018'02"
-76050'23"
18.9
Conetoe — CoB
28-17
Margaret Hall
Walter Perry
Hertford
36023'01"
-76056'51"
16.9
Craven — CrA
28-18
Betty Everette Perry
Walter Perry
Hertford
36017'30"
-76049'53"
7.4
Craven — CrA
31-1
Ray & Linda Chamblee
Hertford
36020'42"
-76055'26"
8.8
Craven — CrA
31-2
Jackie Chamblee
Ray Chamblee
Hertford
36020'40"
-76055'20"
9.6
Craven — CrB
31-3
Jackie Chamblee
Ray Chamblee
Hertford
36020'47"
-76055' 13"
15.9
Craven — CrA
31-4
Ray & Linda Chamblee
Hertford
36020'43"
-76055'04"
8.8
Craven — CrA
31-5
Ray &Linda Chamblee
Hertford
36017'31"
-76055'16"
5.9
Goldsboro—GoA
32-1
Janice Simmons Sessoms
William H. Sessoms
Hertford
36017'55"
-76048'53"
7.0
Wakulla WaB
32-2
William H. Sessoms
Hertford
36017'55"
-76048'42"
30.6
Lynchburg — Ly
32-3
William H. Sessoms
Hertford
36017'27"
-76048'38"
5.0
Craven — CrB
324
Joyce Ann Sessoms
William H. Sessoms
Hertford
36018'07"
-76048'45"
5.0
Bonneau — BoB
32-5
Joyce Ann Sessoms
William H. Sessoms
Hertford
36017'43"
-76049' 16"
5.5
Lynchburg — Ly
32-6
William H. Sessoms
Hertford
36017'42"
-76049'27"
2.7
Lynchburg — Ly
WQ0012404 Version 3.0 Attachment B Page 10 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
A eta
Dominant Soil Series
Footnotes
32-7
William H. & Joyce Ann Sessoms
Hertford
36017'24"
-76047'58"
28.9
Goldsboro
32-8
William H. & Delores Sessoms
Hertford
36017'33"
-76047'23"
23.2
Norfolk — NoB
32-9
William H. & Delores Sessoms
Hertford
36017'36"
-76047'36"
13.3
Norfolk — NoB
32-10
William H. & Delores Sessoms
Hertford
36017'42"
-76047'34"
7.3
Norfolk — NoB
32-11
Wiccacon Properties, LLC
William H. Sessoms
Hertford
36017'47"
-76049'32"
4.3
Craven — CrA
32-12
Ernest Chamblee
William H. Sessoms
Hertford
36015'23"
-76049'08"
14.0
Craven — CrA
33-1
William W & Nellie Ward
William Ward
Hertford
36014'36"
-76056'23"
3.0
Caroline — CaB
33-2
William W & Nellie Ward
William Ward
Hertford
36014'51"
-76056'23"
11.9
Craven — CrC2
33-3
William W & Nellie Ward
William Ward
Hertford
36014'47"
-76056'21"
15.1
Norfolk — NoB
33-4
William W & Nellie Ward
William Ward
Hertford
36014'48"
-76056' 12"
13.6
Norfolk — NoB
33-5
William W & Nellie Ward
William Ward
Hertford
36015' 10"
-76056'08"
14.2
Tarboro — TaB
33-6
William W & Nellie Ward
William Ward
Hertford
36014'43"
-76056' 10"
14.6
Norfolk — NoB
33-7
William W & Nellie Ward
William Ward
Hertford
36014'37"
-76056'08"
5.9
Craven — CrB
33-8
William W & Nellie Ward
William Ward
Hertford
36014'35"
-76056' 14"
3.0
Craven — CrB
33-9
Michael A. & Deborah Spalding
William Ward
Hertford
36014'23"
-76058'28"
14.2
Craven — CrA
33-10
Michael A. & Deborah Spalding
William Ward
Hertford
36014'28"
-76058'27"
8.0
Craven — CrB
33-11
Michael A. & Deborah Spalding
William Ward
Hertford
36014'26"
-76058' 17"
3.7
Craven — CrB
33-12
Michael A. & Deborah Spalding
William Ward
Hertford
36014'21"
-76058'17"
2.4
Craven — CrA
33-13
Rosa H. Sessoms
William Ward
Hertford
36015'09"
-77000'47"
25.0
Craven — CrA
33-14
Rosa H. Sessoms
William Ward
Hertford
36015'12"
-77000'36"
6.3
Leaf —Lf
33-15
Rosa H. Sessoms
William Ward
Hertford
36015' 15"
-77000'29"
2.8
Craven — CrA
33-16
Rosa H. Sessoms
William Ward
Hertford
36015'20"
-76000'31"
4.2
Craven — CrA
County Tots!
Hertford
4,230.4
15-1
J. Elliot Stephenson
Northampton
36028'42"
-77026'06"
19.2
Lynchburg — Ly
15-2
J. Elliot Stephenson
Northampton
36028'31"
-77025'43"
27.3
Craven — CrA
WQ0012404 Version 3.0 Attachment B Page 11 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
FSrtd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
15-3
J. Elliot Stephenson
Northampton
36028' 19"
-77026'06"
38.0
Caroline — CrB
154
J. Elliot Stephenson
Northampton
36025'47"
-77025'26"
41.3
Norfolk — NoA
15-5
J. Elliot Stephenson
Northampton
36026'06"
-77025'40"
71.3
Gritney — GxB
15-6
J. Elliot Stephenson
Northampton
36126' 17"
-77025'44"
37.1
Gritney — GxB
15-7
J. Elliot Stephenson
Northampton
36026' 12"
-77024'48"
13.1
Norfolk — NoA
15-8
J. Elliot Stephenson
Northampton
3602611911
-77028'39"
35.6
Goldsboro — GoA
15-9
J. Elliot Stephenson
Northampton
36026'49"
-77026'39"
15.1
Gritney — GxB
15-10
J. Bentley Stephenson
J. Elliot Stephenson
Northampton
36051'21"
-77026'21"
14.2
Gritney — GxB
15-11
J. Bentley Stephenson
J. Elliot Stephenson
Northampton
36126'44"
-77026'25"
14.5
Gritney — GxB
15-12
J. Elliot Stephenson
Northampton
36126'099'
-77026'36"
9.2
Gritney — GxB
15-13
J. Elliot Stephenson
Northampton
36026'03"
-77026'25"
17.2
Gritney — GxB
15-14
J. Elliot Stephenson
Northampton
36026921"
-77026'07"
19.9
Gritney — GxB
15-15
J. Elliot Stephenson
Northampton
36128'189'
-77025954"
24.3
Bonneau — BoB
15-16
J. Elliot Stephenson
Northampton
36028'2411
-770259419,
22.8
Bonneau — BoB
15-17
J. Elliot Stephenson
Northampton
36028'09"
-77025'52"
33.7
Craven — CrA
18-1
Thomas Williams
Northampton
36°29'41"
-77107'55"
12.0
Craven — CrB
18-2
Thomas Williams
Northampton
36129'52"
-77008'03"
15.0
Craven — CrA
19-1 W
C.C. Woodard
Northampton
36130'46"
-77020'27"
31.7
Norfolk — NoB
19-2W
C.C. Woodard
Northampton
36140'4799
-77020'48"
21.4
Norfolk — NoB
19-3W
C.C. Woodard
Northampton
36030'36"
-77020'56"
69.7
Norfolk—NoB
194W
C.C. Woodard
Northampton
36130'27"
-77020945"
76.7
Norfolk — NoB
19-5W
Cecil Whitehead
C.C. Woodard
Northampton
36030'18"
-77020'50"
12.8
Norfolk—NoB
19-6W
Amanda Cooke, et al
Cecil Whitehead
Northampton
36130'32"
-77020'33"
18.6
Norfolk — NoB
19-7W
C.C. Woodard
Northampton
36030' 18"
-77020' 10"
85.6
Norfolk — NoA
19-8W
C.C. Woodard
Northampton
36030'15"
-77°20'29"
10.9
WQ0012404 Version 3.0 Attachment B Page 12 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
19-9W
C.C. Woodard
Northampton
36030'35"
-77020'21"
15.7
Norfolk — NoB
19-10W
C.C. Woodard
Northampton
36031'25"
-77020'54"
3.9
Bonneau - BoB
19-11 W
C.C. Woodard
Northampton
36031'28"
-77020'44"
29.5
Bonneau - BoB
19-12W
C.C. Woodard
Northampton
3603114311
-77020'25"
4.6
Bonneau - BoB
19-13W
C.C. Woodard
Northampton
36031'12"
-77020'10"
7.9
Norfolk—NoB
19-14W
C.C. Woodard
Northampton
36031' 19"
-77120' 10"
9.3
Norfolk — NoB
19-15W
C.C. Woodard
Northampton
36031'26"
-77020' 10"
11.2
Norfolk — NoB
19-1 G
C.C. Woodard
Northampton
36032'09"
-77021'07"
48.6
Altavista - AtA
19-2G
C.C. Woodard
Northampton
36032' 17"
-77021'22"
13.6
Tarboro - TaB
19-3G
C.C. Woodard
Northampton
36032'26"
-77021'03"
36.2
Altavista - AtA
194G
C.C. Woodard
Northampton
36032'43"
-77020'57"
42.5
Wickham - WkA
19-5G
C.C. Woodard
Northampton
36032'39"
-77021' 13"
20.7
Roanoke - Ro
21-1
C.G. Perry
Northampton
36025'48"
-77020'OT'
19.6
Norfolk—NoB
21-2
C.G. Perry
Northampton
3602513911
-77020'45"
29.2
Caroline - CaB
21-3
C.G. Perry
Northampton
36025'38"
-77020' 17"
11.2
Caroline - CaB
214
C.G. Perry
Northampton
36025'29"
-77020'34"
3.3
Norfolk - NoA
21-5
C.G. Perry
Northampton
36025'31"
-77020'37
9.3
Norfolk—NoB
21-6
C.G. Perry
Northampton
36025'26"
-77020'31"
4.0
Norfolk—NoB
21-7
C.G. Perry
Northampton
36025'25"
-77020'25"
6.2
Norfolk — NoB
21-8
Robert Jones
Robert Jones
Northampton
36025' 12"
-77020'28"
50.4
Norfolk — NoA
21-10
C.G. Perry
Northampton
36023'41"
-77024'16"
44.3
Norfolk—NoB
21-11
C.G. Perry
Northampton
3602795T'
-77025'5T'
33.7
Craven - CrA
21-13
C.G. Perry
Northampton
36027'40"
-77025'35"
15.4
Norfolk - NoA
21-14A
C.G. Perry
Northampton
36027'28"
-77025'409'
13.8
Goldsboro - GoA
21-14B
C.G. Pent'
Northampton
36027'34"
-77025'39"
1 18.0
Goldsboro - GoA
WQ0012404 Version 3.0 Attachment B Page 13 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
Acreage
a
Dominant Soil Series
Footnotes
21-15
C.G. Perry
Northampton
36127'34"
-77025'16"
17.5
Goldsboro - GoA
21-16
C.G. Perry
Northampton
36127'28"
-77025' 16"
5.7
Goldsboro - GoA
21-17
C.G. Perry
Northampton
36025'40"
-77021'08"
4.5
Norfolk - NoA
21-18
Robert Jones
Robert Jones
Northampton
36025'28"
-77021'13"
6.7
Norfolk - NoA
21-20
Robert Jones
Robert Jones
Northampton
36125'23"
-77121'12"
3.7
Norfolk - NoA
21-21
Robert Jones
Robert Jones
Northampton
36025'34"
-77021'02"
31.4
Norfolk - NoA
21-22
Robert Jones
Robert Jones
Northampton
36025'25"
-77°21'02"
5.7
Goldsboro - GoA
22-1
Charles J. Stephenson
Northampton
36127'24"
-77024'58"
23.7
Goldsboro - GoA
22-2
Charles J. Stephenson
Northampton
36027'21"
-77024'49"
19.6
Goldsboro - GoA
22-3
Charles J. Stephenson
Northampton
36027' 17"
-77°24'38"
11.4
Goldsboro - GoA
22-4
Charles J. Stephenson
Northampton
36126'56"
-77024'31"
9.8
Goldsboro - GoA
22-5
Charles J. Stephenson
Northampton
36025'44"
-77023'58"
6.9
Goldsboro - GoA
27-1
Neil Burgess
Stephen Burgess
Northampton
36020'00"
-77112'50"
47.8
Norfolk—NoA
27-2
Neil Burgess
Stephen Burgess
Northampton
36026'00"
-771112'36"
56.4
Norfolk - NoA
27-3
Neil Burgess
Stephen Burgess
Northampton
36025'54"
-77012'27"
25.5
Rains — Ra
274
Neil Burgess
Stephen Burgess
Northampton
36025'41"
-77112'41"
27.5
Norfolk—NoA
27-5
Neil Burgess
Stephen Burgess
Northampton
36025' 18"
-77012'39"
16.0
Norfolk - NoA
27-6
Stephen Burgess
Stephen Burgess
Northampton
36126'07"
-77011'22"
53.4
Bonneau - BoB
27-7
Judi B. Burgess
Stephen Burgess
Northampton
36024'20"
-77013'28"
13.9
Craven - CrA
27-8
Judi B. Burgess
Stephen Burgess
Northampton
36123'59"
-77014' 10"
17.7
Norfolk — NoB
27-9
Lori S. Burgess
Northampton
36023'56"
-77113'57"
18.6
Caroline - CaA
27-10
Stephen Burgess
Northampton
36023'52"
-77013'51"
20.3
Craven - CrA
27-11
Stephen Burgess
Northampton
36023'42"
-77013'50"
23.4
Craven - CrA
27-12
Stephen Burgess
Northampton
36023'39"
-77013'40"
16.7
Craven - CrA
27-13
Stephen Burgess
Northampton
36°23'34"
-77113' 13"
5.2
Craven - CrA
WQ0012404 Version 3.0 Attachment B Page 14 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
Net A ea a
Dominant Soil Series
Footnotes
27-14
Lori S. Burgess
Stephen Burgess
Northampton
36024'34"
-77016'04"
14.7
Goldsboro - GoA
27-15
Stephen Burgess
Northampton
36026'31"
-77'l T l0"
6.5
Norfolk — NoB
27-16
Stephen Burgess
Northampton
36026'27"
-77°17'02"
5.1
Norfolk — NoB
27-17
Stephen Burgess
Northampton
36026'32"
-77016'52"
21,9
Norfolk—NoB
27-18
Lori S. Burgess
Northampton
36026'10"
-77114'39"
11.1
Goldsboro - GoA
27-19
Lori S. Burgess
Northampton
36126' 18"
-77014'24"
18.4
Goldsboro - GoA
27-20
Eloise T. Ward
Stephen Burgess
Northampton
36026'20"
-77014' 17"
12.9
Goldsboro - GoA
27-21
Eloise T. Ward
Stephen Burgess
Northampton
36026' 19"
-77114' 13"
3.8
Goldsboro - GoA
27-22
Eloise T. Ward
Stephen Burgess
Northampton
36026'34"
-77014' 15"
6.7
Goldsboro - GoA
27-23
Eloise T. Ward
Stephen Burgess
Northampton
36027'49"
-77015'27"
32.5
Bonneau - BoB
27-24
Eloise T. Ward
Stephen Burgess
Northampton
36028'07"
-77015' 16"
21.5
Bonneau - BoB
27-25
Eloise T. Ward
Stephen Burgess
Northampton
36028'04"
-77014'45"
35.2
Bonneau - BoB
27-26
Eloise T. Ward
Stephen Burgess
Northampton
36027'53"
-77014'41"
11.5
Norfolk - NoB
27-27
Eloise T. Ward
Stephen Burgess
Northampton
36028'02"
-77014'34"
14.4
Norfolk — NoB
27-28
Eloise T. Ward
Stephen Burgess
Northampton
36027'52"
-77014'25"
25.3
Norfolk — NoB
27-29
Eloise T. Ward
Stephen Burgess
Northampton
36027'45"
-77014' 1 T'
60.5
Norfolk — NoB
27-30
Eloise T. Ward
Stephen Burgess
Northampton
36028' 11"
-77014'51"
5.7
Autryville - AuA
27-31
Eloise T. Ward
Stephen Burgess
Northampton
36028' 16"
-77014'52"
10.5
Norfolk — NoA
27-32
Eloise T. Ward
Stephen Burgess
Northampton
36028'21"
-77014'52"
26.0
Bonneau — BoB
27-33
Eloise T. Ward
Stephen Burgess
Northampton
36028'21"
-77014'42"
9.9
Norfolk — NoA
27-34
Eloise T. Ward
Stephen Burgess
Northampton
36028'26"
-77014'30"
17.6
Bonneau — BoB
27-35
Eloise T. Ward
Stephen Burgess
Northampton
36028'30"
-77014' 18"
9.1
Goldsboro — GoA
27-36
Eloise T. Ward
Stephen Burgess
Northampton
36128'24"
-77013'5T'
9.3
Autryville — AuA
27-37
Eloise T. Ward
Stephen Burgess
Northampton
36028'23"
-77014' 12"
17.2
Autryville — AuA
27-38
Eloise T. Ward
Stephen Burgess
Northampton
1 36028' 10"
-77014'09"
3.0
Norfolk - NoA
WQ0012404 Version 3.0 Attachment B Page 15 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: January 25, 2016
Permit Number: WQ0012404 Version: 3.0
Fietd/
Owner
Lessee
County
Latitude
Longitude
A eta
Dominant Soil Series
Footnotes
27-39
Kevin B. Burgess
Stephen Burgess
Northampton
36026'40"
-77012140"
20.6
Norfolk - NoB
27-40
Kevin B. Burgess
Stephen Burgess
Northampton
36026'33"
-77012'35"
21.0
Norfolk - NoB
27-41
Stephen Burgess
Northampton
36027'33"
-77011'45"
9.8
Norfolk - NoB
2742
Stephen Burgess
Northampton
36027'43"
-77011'32"
93.5
Bonneau — BoB
2743
Stephen Burgess
Northampton
36027'35"
-7701 F21"
17.7
Norfolk — NoB
27-44
Stephen Burgess
Northampton
36027'43"
-77011,11"
29.2
Bonneau — BoB
27-45
Stephen Burgess
Northampton
36027'49"
-77011'04"
17.5
Norfolk — NoB
27-46
Stephen Burgess
Northampton
36027'27"
-77011' l 8"
13.9
Bonneau — BoB
27-47
Stephen Burgess
Northampton
36027'3611
-77011106"
20.8
Bonneau — BoB
27-48
Kevin B. Burgess
Stephen Burgess
Northampton
36027'31"
-77010'l5"
14.8
State— StA
27-49
Kevin B. Burgess
Stephen Burgess
Northampton
36027'27"
-77010'07"
6.1
Tarboro — TaB
27-50
Kevin B. Burgess
Stephen Burgess
Northampton
36027'38"
-77009159"
17.9
Altavista — AtA
27-51
Kevin B. Burgess
Stephen Burgess
Northampton
36027'38"
-77009'40"
52.7
Tarboro — TaB
27-65
Bobby Bridges
Neil Bridges
Northampton
36025'50"
-77015'01"
67.3
Bonneau — BoB
27-66
Neil & Donna B. Burgess
Northampton
360249509'
-77115' 10"
18.1
Norfolk — NoB
County Total
Northampton
2,630.5
Permit Total
7,514.5
WQ0012404 Version 3.0 Attachment B Page 16 of 16

ATTACHMENT C — Groundwater Monitoring and Limitations Permit Number: WQ0012404 Version: 3.0
CF Nitrogen, Inc.
ATTACHMENT C - GROUNDWATER LIMITATIONS AND MONITORING REQUIREMENTS
Permit No. WQ0012404 Version 3.0
CF Nitrogen, Inc.
Site 11 Monitor Wells C-22, C-23, C-28, C-29, C-32, C-33, MWI-3, MWI-4 and MWI-6
Site 11 Piezometers PI-11, PO-12, PI-2 and PO-236
Parameter
Limits
Monitoring Requirements
Daily Maximum
Daily
Units
Frequency
Measurement
Footnotes
Minimum
Water level, distance from
feet
4 x Year
Calculated
1
measuring point - 82546
1. 4 x Year monitoring shall be in January, April, July, and October.
WQ0012404 Version 3.0 Attachment C Page 1 of 1

MAR 01 2019
2018 Annual Report
Land Application Program
CF Nitrogen, Inc.
Permit No. WQ0012404
RECEIVEDINCDEQIDWR
MAR - 1 2019
Non -Discharge
Permitting Unit

2018 Annual Report
Land Application Program
CF Nitrogen, Inc. I I
S&ME Project No. Permit No. WQ0012404
TABLE OF CONTENTS:
SECTION NO.
I
II
III
IV
V
VI
VII
TITLE
Annual Land Application Certification Form
Residuals Sampling Summary and Analysis
2018 Application Summary and Field Loading Rate Reports
Field Application Summaries
Updated Attachment B
Landowner Agreement Attachments & Lessee Agreement
Attachments
Groundwater Data
February 19, 2019

2018 Annual Report
Land Application Program
CF Nitrogen, Inc.
S&ME Project No. Permit No. WQ0012404
CF Nitrogen, Inc.
Mr. John Foster
4 Parkway North, Suite 400
Deerfield, IL 60015-2590
847-405-2400
NC PERMIT # WQ0012404
Mr. Jay Bryant
Granville Farms, Inc.
100 Farmers Chemical Road
Cofield, NC 27922
252-358-2129
LAND APPLIERS:
Granville Farms, Inc.
8229 Highway 96 North
Oxford, North Carolina 27565
919-690-8000
February 19, 2019
13

Attachments

Annual Land Application Certification Form

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0012404 County: Hertford Year: 2019
Facility Name (as shown on permit): CF Nitrogen, Inc.
Land Application Operator. Granville Farms, Inc. Phone: [phone]"
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes ❑ No - If No, slip Part A, aad Part B and proceed to Part C. Also, If residuals were
generated but not lard applied, please attach an explanation on how the readaals were handled.
D�..� 1 _ U-.:drab A nnliroriu.w Cnmm9N•
Total number of application fields in the permit
392
Total number of fields utilized for land application during the year.
25
Total amount of dry tons applied during the year for all application sites:
MA Groundwater Recovery System
Total number of acres utilized for land application during the year.
798.7
Part B - Annual Comniance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. ® Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I I05(a) or the Pollutant
Loading Rates in 15A NCAC 02T .110*) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requiremei is in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T. i I I 1 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certif3ention•
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and.complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
CF Nitrogen, Inc. Tunis, NC Facility
Permittee Name itle or print)
ofPreparee Date
S&tlatuae of Penmittee Date
2-Z�-14
Applier Date
Jason Volker, S&ME, Inc. Jay Bryant, Granville Farms, Inc.
" Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (1212006)

Residuals Sampling Summary and Analysis

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analysed for over the past calendar year. Use additional terms as needed.
WQ Permit Number: W00012404
Facility Name: CF Nihogen, Inc.
NPDFS k or WQN: NA
Name Nihogen-Enriched Groundwater Recovery System
laboratory: 1) Waypoint Analytical
2)
3)
RESIDUAL ANALYSIS DATA
Date Sampled (grab) or Date 4/11/2018 6/19/2018 9W2018 11/28/2018
C
Percent Solids N/A N/A N/A N/A
TRN
271
225
255
241
Anvimnia-14ftrogen
270
242
249
240
Niftate-NWogen
255
273
262
272
Total Phosphorus
1.0
1.0
1.08
1.63
Aluminum
1.0
1.0
1.66
0.472
Calcium
136
121
122
99.1
Magnesium
19.9
17.2
18.0
15.9
Potassium
38.9
37.8
38.6
34.8
H
7.2
6.7
6.9
7.4
Sodium
37.1
33.1
35.6
33.2
"I certify, under penalty of law, that this document was prepared tinder my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
Imprisonment for knowing violations."

Report Number
18-103-0224 Page: 1 of 2
Account Number
46260
Send To: CF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield , NC 27922
Project: 052143
Waypoint
ANALYTICAL
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Purchase Order:
Report Date : 04/18/2018
Date Received : 04/13/2018
Date Sampled : 04/11/2018
Lab Number: 59746
Sample Id : 052143
Quantitation
Date and Time
Analysis
Result
Limit
Method
Test Started
Analyst
Total Kjeldahl Nitrogen , mg/L
271
10.0
SM-4500-NH3C-TKN
04/16/2018 09:00
R D
Total Phosphorus , mg/L
<1.00
1.00
6010C
04/16/2018 02:01
SMC
Total Potassium , mg/L
38.9
1.00
6010C
04/16/2018 02:01
SMC
Total Calcium , mg/L
136
1.00
6010C
04/16/2018 02:01
SMC
Total Magnesium , mg/L
19.9
1.00
6010C
04/16/2018 02:01
SMC
Total Sodium , mg/L
37.1
1.00
6010C
04/16/2018 02:01
SMC
Total Aluminum , mg/L
<1.00
1.00
6010C
04/16/2018 02:01
SMC
Ammonia Nitrogen, mg/L
270
5.00
SM-4500-NH3C
04/16/2018 09:00
R D
Nitrate+Nitrite-N , mg/L
255
100
4500NO3F-2011
04/17/2018 09:03
MMT
pH , s.u.
7.2
9045D
04/16/2018 10:40
JM
Pig;e, mV 1111~I✓
Pauric McGroary

Report Number
18-103-0224 Page: 2 of 2 Waypoint
Account Number
46260 ANALYTICAL
Send To: CIF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield , NC 27922
Project: 052143
Lab Number: 59746
Sample Id : 052143
Analysis
REPORT OF ANALYSIS
Quantitation
Result Limit
Method Reference:
Standard Methods for the Analysis of Water and Wastewater, 1997
Standard Methods for the Analysis of Water and Wastewater, 20th Ed. 1998
USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision
Comments:
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Purchase Order:
Report Date : 04/18/2018
Date Received : 04/13/2018
Date Sampled : 04/11/2018
Date and Time
Method Test Started Analyst
?W;4 X 60wr
Pauric McGroary

Report Number
18-170-0214
Account Number
46260
Send To: CF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield . NC 27922
Project : 055927
Waypoint(D
ANALYTICAL
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Purchase Order:
Report Date : 07/05/2018
Date Received : 06/19/2018
Date Sampled : 06/18/2018
Lab Number: 61256
Sample Id : 055927
Quantitation
Date and Time
Analysis
Result
Limit
Method
Test Started
Analyst
Total Kjeldahl Nitrogen , mg/L
225
10.0
SM-4500-NH3C-TKN
06/22/2018 08:30
R D
Phosphorus, mg/L
<1.00
1.00
601 OD
06/29/2018 11:59
BKN
Potassium , mg/L
37.8
1.00
601OD
06/28/2018 15:22
BKN
Calcium, mg/L
121
1.00
601OD
06/28/2018 15:22
BKN
Magnesium, mg/L
17.2
1.00
601OD
06/28/2018 15:22
BKN
Sodium, mg/L
33.1
5.00
601OD
06/28/2018 15:22
BKN
Aluminum, mg/L
<1.00
1.00
601OD
06/28/2018 15:22
BKN
Ammonia Nitrogen, mg/L
242
5.00
SM-4500-NH3C
06/22/2018 08:30
R D
Nitrate+Nitrite-N , mg/L
273
2.43
4500NO3F-2011
06/22/2018 13:42
MMT
pH , s.u.
6.7
9045D
06/20/2018 11:35
JM
Pam« mC 111 "I
Pauric McGroary
7'age 4 _-1

Report Number
18-170-0214
Account Number
46260
Send To: CF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield . NC 27922
Project : 055927
Lab Number: 61256
Sample Id : 055927
Analysis
Waypoint(D
ANALYTICAL
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Purchase Order:
Report Date : 07/05/2018
Date Received : 06/19/2018
Date Sampled : 06/18/2018
Quantitation Date and Time
Result Limit Method Test Started Analyst
Method Reference:
Standard Methods for the Analysis of Water and Wastewater, 1997
Standard Methods for the Analysis of Water and Wastewater, 20th Ed. 1998
USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision
Comments:
potir- X 6140rr
Pauric McGroary
image 5

Report Number
18-250-0207
Account Number
46260
Send To: CF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield , NC 27922
Project : 059467
Waypoint(D
ANALYTICAL
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Purchase Order:
Report Date : 09/18/2018
Date Received : 09/07/2018
Date Sampled : 09/06/2018
Lab Number: 62658
Sample Id : 059467
Quantitation
Date and Time
Analysis
Result
Limit
Method
Test Started
Analyst
Total Kjeldahl Nitrogen , mg/L
255
10.0
SM-4500-NH3C-TKN
09/13/2018 09:00
R D
Phosphorus, mg/L
1.08
1.00
6010D
09/14/2018 20:53
CCR
Potassium , mg/L
38.6
1.00
6010D
09/14/2018 20:53
CCR
Sulfur, mg/L
131
1.00
6010D
09/14/2018 20:53
CCR
Calcium, mg/L
122
2.00
601 OD
09/14/2018 20:53
CCR
Magnesium, mg/L
18.0
1.00
601 OD
09/14/2018 20:53
CCR
Sodium, mg/L
35.6
5.00
601 OD
09/14/2018 20:53
CCR
Aluminum, mg/L
1.66
1.00
601 OD
09/14/2018 20:53
CCR
Ammonia Nitrogen, mg/L
249
2.00
SM-4500-NH3C
09/12/2018 09:00
R D
Nitrate+Nitrite-N , mg/L
262
100
4500NO3F-2011
09/11/2018 12:19
MMT
pH , s.u.
6.9
9045D
09/12/2018 09:00
JM
Pif« If G�re
Pauric McGroary
image 4 cf �.

Report Number
18-250-0207
Account Number
46260
Send To: CF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield , NC 27922
Project: 059467
Lab Number: 62658
Sample Id : 059467
Analysis
Waypoint(D
ANALYTICAL
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Purchase Order:
Report Date : 09/18/2018
Date Received : 09/07/2018
Date Sampled : 09/06/2018
Quantitation
Result Limit Method
Method Reference:
Standard Methods for the Analysis of Water and Wastewater, 1997
Standard Methods for the Analysis of Water and Wastewater, 20th Ed. 1998
USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision
Comments:
Pot« X 6e"r
Pauric McGroary
page 5 c`
Date and Time
Test Started Analyst

Report Number
18-333-0211
Waypoint 7621 Whitepine Road, Richmond, VA 23237
Account Number Main 804-743-9401 ° Fax [phone]
46260 ANALYTICAL www.waypointanalytical.com
Send To: CF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield, NC 27922
Purchase Order: 60306
Project: 062594
Report Date: 12/12/2018
Date Received: 11/29/2018
REPORT OF ANALYSIS
Date Sampled: 11/28/2018
Lab Number: 63750
Sample ID: 062594
Quantitation
Date and Time
Analysis
Result
Limit
Method Test Started
Analyst
Total Kjeldahl Nitrogen , mg/L
241
10.0
SM-4500-NH3C-TKN 11/30/2018 08:30
R D
Phosphorus, mg/L
1.63
0.100
601 OD 12/05/2018 23:21
KKM
Potassium, mg/L
34.8
1.00
601 OD 12/06/2018 12:52
BKN
Calcium, mg/L
99.1
0.500
601 OD 12/05/2018 23:21
KKM
Magnesium, mg/L
15.9
0.100
601 OD 12/05/2018 23:21
KKM
Sodium, mg/L
33.2
0.500
601 OD 12/05/2018 23:21
BKN
Aluminum, mg/L
0.472
0.100
601 OD 12/05/2018 23:21
KKM
Ammonia Nitrogen, mg/L
240
2.00
SM-4500-NH3C 11/30/2018 08:30
R D
Nitrate+Nitrite-N , mg/L
272
100
4500NO3F-2011 11/30/2018 09:42
MMT
pH , s.u.
7.4
9045D 11/30/2018 08:30
R D
PO4t;4 XV 6bovr
Pauric McGroary
Page 4 of

Report Number
18-333-0211
Account Number Waypoint
46260 ANALYTICAL
Send To: CF Industries
John Foster
100 Farmers Chemical Rd
Suite 400
Cofield, NC 27922
Project: 062594
Lab Number: 63750
Sample ID: 062594
Analysis
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OF ANALYSIS
Result
Purchase Order: 60306
Report Date: 12/12/2018
Date Received: 11/29/2018
Date Sampled: 11/28/2018
Quantitation Date and Time
Limit Method Test Started Analyst
Method Reference:
Standard Methods for the Analysis of Water and Wastewater, 1997
Standard Methods for the Analysis of Water and Wastewater, 20th Ed. 1998
USEPA, SW-846, Test Methods for Evaluating Solid Wastes, Physical/Chemical Methods, 3rd Ed. Current Revision
Comments:
{ of;G it G0r
Pauric McGroary
Dage 5 ct

2018 Application Summary and Field Loading Rate Reports

2018 APPLICATION SUMMARY
CF NITROGEN, INC.
NITROGEN ENRICHED GROUNDWATER
PERMIT No. WQ0012404
NITROGEN ENRICHED GROUNDWATER SUMMARY
FARM
NAME
FIELD
NO.
APPL.
DATE
ACRES
UTILIZED
TOTAL
GALLONS
GAL'S./
ACRE
IN/
ACRE
PAN
(lbs/ac)
C.F. NITROGEN
Site 11
1
Q3-18
40.4
402,000
9,950
0.37
32.29
3
Q3-18
41.4
73 000
1763
0.06
5.71
STEVEN BURGESS
Site 27
1
Q2-18
47.8
778,000
16,276
0.60
53.01
2
Q2-18
56.4
1,162,000
20,603
0.76
67.11
42
Q3-18
93.5
1,133,000
12,118
0.45
54.22
43
Q2-18
17.7
225,000
12,712
0.47
56.88
44
Q1-18
29.2
265,000
9,075
0.33
40.61
Q2-18
29.2
101,000
3,459
0.13
15.48
45
Q1-18
17.5
236,000
13,486
0.50
60.35
46
Q2-18
13.9
177,000
12,734
0.47
56.98
47
Q2-18
20.8
230,000
11,058
0.41
49.48
67
Q1-18
33.7
481,000
14,273
0.53
63.87
68
Q4-18
58.0
919,000
15,845
0.58
51.63
70
QI-18
85.4
161000
1885
0.07
8.44
KENDRED C. WILLIAMS, JR.
Site 30
4
Q4-18
26.3
1,258,000
47,833
1.76
155.00
5
Q348
32.4
828,000
25,556
0.94
82.83
Q4-18
32.4
827,000
25,525
0.94
82.71
7
Q2-18
12.9
296,000
22,248
0.82
72.47
Q3-18
12.9
212,000
16,434
0.61
53.34
9
Q2-18
16.4
494,000
30,122
1.11
98.11
Q3-18
16.4
596,000
36,341
1.34
117.95
10
Q2-18
3.7
90,750
30,541
1.12
99.48
Q3-18
3.7
78,000
21,081
0.78
68.42
11
Q2-18
1.4
41,533
32,666
1.20
106.40
12
Q2-18
1.5
47,467
34,945
1.28
113.49
13
Q2-18
5.1
89,250
17,500
0.64
57.00
Q3-18
5.1
120,667
23,660
0.87
76.79
15
Q3-18
8.9
260,491
29,269
1.08
94.99
16
Q3-18
4.5
70,000
15,556
0.57
50.49
18
Q3-18
20.9
886,842
42,433
1.56
137.71
19
Q3-18
9.3
219,000
23,548
0.87
76.43
TOTALS 1 798.7 1 12,758,000 1
LAND APPLICATIONS 2018
MElYb[11•I 1m
s�
SEENUA iI1"
�IiTfi;[*�
• . � �'�
�757T W@41�
�9• �`��
Total Gallons Applied 12,758,000
GROUNDWATER RECOVERED 2018 TO HOLDING LAGOON
EEL
• : '�
11 TfSai'�ftek5f:i�I�)•
Total Gallons Recovered 12,355,200

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: CF Nitrogen, Inc.
OPERATOR: Granville Farms, Inc.
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 40.4 Cr Fescue Predominant Soil: Craven - CrA
FIELD
DATE
ACRES
LIT
TOTAL
GALLONS.
GALLONS
PER ACRE
Acre
in/ac
Nutrients 16s/ac
PAN
P
K
1
3-18
40.4
402,000
9,950
0.37
32.29
0.08
3.14
Site No.
11
Annual Totab
402,000
9,950
0.37
32.29
0.08
3.14
147 RYEL3mit
(IbsJacre/ ear)
(Siguaiure of Land Applier) Dite
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: CF Nitrogen, Inc.
OPERATOR: Granville Farms, Inc.
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 41.4 Crop: Fescue Predominant Sal: Craven - CrA
FIELD
DATE
ACRES
UTIII7.FD
TOTAL
GALLONS.
GALLONS
PERACRE
Acre
in/ac
Nutrients Ibs/ac
PAN
P
K
3
3-18
41.4
73,000
1,763
0.06
5.71
0.02
0.57
Site No.
11
Annual Totals
73,000
1,763
0.06
5.71
0.02
0.57
147 111YELimil
(%s Jacre/year)
,S� i Zl 14
(St = of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Neil Burgess
OPERATOR: Stephen Burgess
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 47.8 Crop: Wheat Predominant Soil: Norfolk - NoA
123 IRVIEUrtilt
(lbsJacre/year)
J3114
4PAure of Land Applier) Date
"I certify, under penalty of law, that this document Has prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there am
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Neil Burgess
OPERATOR: Stephen Burgess
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 56.4 Crop: Wheat Predominant Soil: Norfolk - NoA
FL13D
DATE
ACRES
ULHJMD
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients
bs/ac
PAN
P
K
2
2-18
56A
1,162,000
20 603
0.76
67.11
0.17
6.69
Site No.
27
Annual Totals
1,162,000
20,603
0.76
67.11
0.17
6.69
123 IRYELimit
(lbsJacre/ ear)
I Sr r S
(' of LandApplier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Stephen Burgess
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres: 93.5
Nitrogen Enriched Groundwater
Crops Wheat Predominant Soil: Bonneau - BoB
FLE1D
DATE
ACRES
UT ILEM
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac-
Nutrients Ibshc
PAN
P
K
42
1-18
93.5
1,133,000
12,118
0.45
54.22
0.10
3.78
Site No.
27
Annual Totals
1,133,000
12,118
0.45
54.22
0.10
3.78
91 IRYEUnit
ObsJacre/ ear)
<1;: 'S�b'4 I A 1/1 -k
ture of Land Applier) Efate
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aHare that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Stephen Burgess
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres:17.7
Nitrogen Enriched Groundwater
Cr Wheat Predominant Soil: Norfolk - NoB
M"
I DATE
ACRES
U111 mm
TOTAL
GALLONS
GALLONS
PER ACRE
Acre
in/ac
Nutrients IbsMe)
PAN
P
K
43
2-18
17.7
225,000
12 712
0.47
56.88
0.11
3.97
Site No.
27
Annual Totals 1
225,000
12,712
0.47
56.88
0.11
3.97
123 JRYELimit
(lbsJacrel ear)
13r �5
048malure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Stephen Burgess
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres: 29.2
Nitrogen Enriched Groundwater
Crop: Wheat Predominant Soil: Bonneau - BoB
FIELD
DATE
ACRES
UTIIDF.D
TOTAL
GALLONS
GALLONS
PFRACRE
Acre
in/ac
Nutrients 6s/2c
PAN
P
K
44
1-18
29.2
265,000
9 075
0.33
40.61
0.08
2.83
Site No.
27
Q2-18
29.2
101,000
3,459
0.13
15.48
0.03
1.08
Annual Totals
366,000
12,534
0.46
56.09
0.10
3.91
91 JRYEUndt
(lbsJacm/year)
7! ��- C-0 A kI l-,
atuueofLand Applier) to
"I certify, under penalty of law, that this document Has prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Stephen Burgess
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres:17.5
Nitrogen Enriched Groundwater
Crop: Wheat Predominant Soil: Norfolk - NoB
FIELD
I DATE
ACRES
V17LI7�D
TOTAL
GALLONS
GALLONS
PER ACRE
Acre
in/ac
NuMents
bs/ac
PAN
P
K
45
1-18
17.5
236,000
13,486
0.50
60.35
0.11
4.21
Site No.
27
Annual Totals
236,000
13,486
0.50
60.35
0.11
4.21
123 IRYEUmit
(lbsJacre/year)
3IAr,
ure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CIF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMrr # WQ0012404
OWNER: Stephen Burgess
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres:13.9
Nitrogen Enriched Groundwater
Croce Wheat Predominant Soil: Bonneau - BoB
m0©
91 IRYEUn4t
(lbsJacre/year)
<-��- - I ?( (�
W*QtureofLandApplier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Stephen Burgess
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres: 20.8
Nitrogen Enriched Groundwater
Crop: Wheat Predominant Soil: Bonneau - BoB
FM.D
DATE
ACRES
U17LI7FD
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients Ibs/ac
PAN
P
K
47
2-18
20.8
230,000
11,058
0.41
49.48
0.09
3.45
Site No.
27
Annual Totals
1
230,000
11,058
0.41
49.48
0.09
3.45
�To7bs
Limit
Jacte/year)
lure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possiMity of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Fannie Bryant
OPERATOR: Stephen Burgess
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 33.7 Cron Wheat Predominant Soil: Bonneau - BoB
FMD
I DATE
ACRES
uIrn
TOTAL
GALLONS
GALLONS
PER ACRE
Acre
in/ac
Nutrients hs/ac
PAN
P
K
67
1-18
33.7
481,000
14,273
0.53
63.87
0.12
4.45
Site No.
27
Annual Totals
481,000
14,273
0.53
63.87
0.12
4.45
91 IRYEUndt
(1bsJacre/year)
ature of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Martha Pearlman
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres: 58
Nitrogen Enriched Groundwater
Cron Wheat Predominant Soil: Goldsboro - GoA
HUD
I DATE
ACRES
UTIIJZED
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients Ibe/ac
PAN
P
K
68
4-18
58
919,000
15,845
0.58
51.63
0.18
4.83
Site No.
27
Annual Totals
919,000
15,845
0.58
51.63
0.18
4.83
136 IRVELIMIt
(lbs ✓acrelyear)
-�L -!5A A( S
(ftyf6ure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I an aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Ronald Woodard
OPERATOR:
RESIDUAL SOURCE:
Permitted Acres: 85.4
Nitrogen Enriched Groundwater
Crop: Wheat Predominant Soil: Lvnehhuro - Lv
MMEMMMEMOMmm
i v y7
y,
106 RYElimit
(IbsJacre/year)
ature of Land Applier) E6e
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 26.3 Crop: Soybeans Predominant Soil: Norfolk - NoB
FIELD
DATE
ACRES
L]TELE FD
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients Ibs/ac
PAN.
P
K
4
4-18
26.3
1,258,000
47 833
1.76
155.00
0.43
15.41
Site No.
30
Annual Totals
1,258,000
47,833
1.76
155.00
0.43
15.41
200 JRYELirnit
(lbsJacre/year)
�.�C A
(firdiure of Land Applier) date
"I certify, under penalty of law, that this document Has prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERNUT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 32.4 Crop: Soybeans Predominant Soil: Craven - CrB
FLELD
I DATE
ACRES
LIII[�
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients Ibs/ac
PAN
P
K
5
3-18
32.4
828,000
25,556
0.94
82.83
0.23
8.20
Site No.
30
Q4-18
32.4
827,000
25,525
0.94
82.71
0.23
8.22
Annual Totals
1,655,000
51,080
1.88
165.55
0.46
16.43
200 JRVELimit
(ibs Jacre/year)
�I I�
( gn a of Land Applier) D to
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 12.9 Crop: Soybeans Predominant Soil: Craven - CrB
FIELD
DATE
ACRES
UTH
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients lbs/ac
-PAN
P
K
7
2-18
12.9
296,000
22,248
0.82
72.47
0.19
7.22
Site No.
30
Q3-18
12.9
212,000
16,434
0.61
53.34
0.14
5.18
Annual Totals
1
508,000
38,682
1.42
125.80
0.32
12.41
200 JRVELimit
(lbsJacm/year)
(' of Land Applier) Date
"I certify, under -penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 16.4 Crop: Bermuda Predominant Soil: Norfolk - NoA
FLEID
DATE
ACRES
UTHIM
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients Ibslac)
PAN
P
K
9
2-18
16.4
494,000
30 122
1.11
98.11
0.25
9.78
Site No.
30
Q3-18
16.4
596,000
36,341
1.34
117.95
0.30
11.46
Annual Totals
1,090,000
66,463
2.45 1216.061
0.55
21.24
230 RYE Limit
(lbs Jacre/year)
�-5 1 311-�
(Sivrdure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 3.7 Crew Bermuda Predominant Soil: Nnrfnik - NnA
FIELD
DATE
ACRES
UTII�
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
NuMents lbs/ac
PAN
P
K
10
2-18
3.7
90,750
30 541
1.12
99.48
0.25
9.91
Site No.
30
Q3-18
3.7
78,000
21,081
0.78
68.42
0.18
6.65
Annual Total$
168,750
51,622
1.90
167.89
0.43
16.56
230 IRYELinflt
(lbs Jacm/year)
ature of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 1.4 Crop: Bermuda Predominant soil: Norfolk - NoR
FIIIDD
DATE
ACRES
iITIIzzm
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nntrients Ibehtc
PAN
P
K
11
2-18
1.4
41,533
32,666
1.20
106.40
0.27
10.60
Site No.
30
Annual Totals
41,533
32,666
1.20
106.40
0.27
10.60
225 jRYEUmlt
(bsJacre/year)
(. a of Land Applier) e
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres:1.5 Crop: Bermuda Predominant Sail: Norfolk - NnA
�MMMMMEMM
'
230 IRYELimit
(lbsJacre/year)
13l IS
lure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 5.1 Crop: Bermuda Predominant soil: Lenoir - Im
FIELD
DATE
ACRES
U1HIM
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients lba/ac
PAN
P
K
13
2-18
5.1
89,250
17,500
0.64
57.00
0.15
5.68
Site No.
30
Q3-18
5.1
120,667
23,660
0.87
76.79
0.20
7.46
Annual Totals
209,917
41,160
1.52
133.79
0.34
13.14
147 JRVE]Ljmit
(lbs Jacre/year)
i 3+ It
(Signiture of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 8.9 Crop: Bermuda Predominant Soil: Leaf - Lf
108 IRYEUnAt
(Nn Jacre/year)
(94P06re of Land Applier) Da e
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 4.5 Cr Bermuda Predominant Sall: Craven - CrA
FIIID
DATE
ACRES
UfII17D
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients Ibs
AC
PAN
P
K
16
3-18
4.5
70,000
15 556
0.57
50.49
0.13
4.91
Site No.
30
Annual Totals
70,000
15,556
0.57
50.49
0.13
4.91
168 JRYELImit
(lbsJacre/year)
lure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 20.9 Crop: Bermuda Predominant Soil: Craven - CrA
FMD
I DATE
ACRES'
UTII»
TOTAL
GALLONS
GALLONS
PERACRE
Acre
in/ac
Nutrients
bs/ac
PAN
P
K
18
3-18
20.9
886,842
42 433
1.56
137.71
0.35
13.39
Site No.
30
Annual Totals
886,842
42,433
1.56
137.71
0.35
13.39
168 JRYELimit
(lbsJacre/year)
(' ure of Land Applier) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

CF NITROGEN, INC. - TUNIS, NORTH CAROLINA
S&ME, INC.
Field Loading Rate Report - Nitrogen Enriched Groundwater
PERMIT # WQ0012404
OWNER: Kendred C. Williams, Jr.
OPERATOR:
RESIDUAL SOURCE: Nitrogen Enriched Groundwater
Permitted Acres: 9.3 Crop: Bermuda Predominant Soil: Goldsboro - GoA
FIELD
I DATE
ACRES
UTLIIMM
TOTAL
GALLONS
GALLONS
PERACRE
Acre
inlic
Nutrients Ihe/ac
PAN
P
K
19
3-18
9.3
219,000
23,548
0.87
76.43
0.20
7.43
Site No.
30
Annual Totals
1
219,000
23,548
0.87
76.43
0.20
7.43
230 IRYELimit
(]bs Jacrelyear)
Al.=;57 �<-�
/
fsi�ure of Land Applier) D to
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."

Field Application Summaries

GRANVILLE FARMS, INC.
FIELD APPLICATION SUMMARY
2018 APPLICATION YEAR
Granville Farms
FIELD
ACRES
CROP
1
40.4
fescue
3
41.4
fescue
8/7/2018
19,000
8/8/2018
88,000
8/ 10/2018
1 1 1,000
8/ 13/2018
49,000
8/ 14/2018
112,000
8/ 15/2018
23,000
9/ 1 1 /2018
39,000
9/ 12/2018
34,000
Totals
402,000
73,000
Q 1-2017
-
-
Q2-2017
-
-
Q3-2017
402,000
73,000
Q4-2017
-
-
CLIENT: CF NITROGEN, INC.
PERMIT # WQ0012404
APPLICATION METHOD: Surface
Site: I I

GRANVILLE FARMS, INC.
FIELD APPLICATION SUMMARY
2018 APPLICATION YEAR
Steven Burgess Site: 27
CLIENT: CF NITROGEN, INC.
PERMIT # WQOO 12404
APPLICATION METHOD: Surface
FIELD
ACRES
CROP
1
47.80
wheat
2
56.40
wheat
42
93.5
wheat
43
17.7
wheat
44
29.2
wheat
45
17.5
wheat
46
13.9
wheat
47
20.8
wheat
67
33.7
wheat
68
58
wheat
70
85.4
wheat
1/22/2018
118,000
1/23/2018
43,000
1/24/2018
122,000
1 /25/2018
119,000
1 /26/2018
107,000
1 /27/2018
81,000
1 /31/2018
52,000
2/ 112018
105,000
2/7/2018
62,000
2/8/2018
51,000
2/9/2018
39,000
2/ 1612018
42,000
2/22/2018
52,000
2/23/2018
52,000
2/24/2018
37,000
2/27/2018
54,000
2/28/2018
114,000
3/S/2018
114,000
3/6/2018
124,000
3/ 10/2018
99,000
3/ 15/2018
73,000
3/ 16/2018
115,000
3/ 17/2018
90,000
3/23/2018
85,000
3/24/2018
61,000
3/26/2018
44,000
3/27/2018
63,000
3/28/2018
69,000
3/29/2018
64,000
3/30/2018
25,000
4/2/2018
101,000
4/3/2018
119,000
/4/2018
106,000
/5/2O l e
142,000
/6/2018
F
88,000
/9/2018
87,000
/ 10/2018
90,000
4/ 11 /2018
92,000
4/ 1212018
92,000
4/ 1312018
83,000
4/14/2018
38,000
4/ 18/2018
118,000
4/19/2018
56,000
4/20/2018
81,000
4/23/2018
99,000
4/30/2018
119,000
5/ 1 /2018
132,000
5/2/2018
106,000
5/3/2018
81,000
5/4/2018
64,000
5/8/2018
114,000
5/9/2018
132,000
5/ 10/2018
131,000
S/ 12/2018
49,000
5/ 13/2018
37,000
5/ 14/2018
131,000
5/ 15/2018
142,000
5/ 16/2018
43,000
11 /8/2018
23,000
11 /912018
6,000
11 / 12/2018
55,000
I I/19/2018
50,000
11/20/2018
68,000
11121 /2018
83,000
1 1 /28/2018
35,000
11 /29/2018
62,000
11 /30/2018
44,000
12/5/2018
102,000
12/6/2018
75,000
12/7/2018
67,000
12/8/2018
74,000
12/ 14/2018
45,000
12/ 19/2018
43,000
12/27/2018
87,000
Totals
778,000
1,162,000
1,133,000
225,000
366,000
1 236,000
177,000
230,000
481,000
919,000
161,000
Q 1-2017
-
1,133,000
-
265,000
236,000
-
481,000
-
161,000
Q2-2017
778,000
1,162,000
-
225,000
101,000
-
177,000
230,000
-
-
Q3-2017
-
-
Q4-2017
919,000

GRANVILLE FARMS, INC.
FIELD APPLICATION SUMMARY
2018 APPLICATION YEAR
Kendred C. Williams, Jr. Site: 30
CLIENT: CF NITROGEN, INC.
PERMIT # W00012404
APPLICATION METHOD: Surface
FIELD
ACRES
CROP
4
26.30
soybeans
5
32.40
soybeans
7
12.90
soybeans
9
16.4
bermuda
10
3.7
bermuda
II
1.4
bermuda
12
1.5
bermuda
13
5.1
bermuda
15
8.9
bermuda
16
4.5
bermuda
18
20.9
bermuda
19
9.3
bermuda
6/8/2018
104,000
6/9/2018 1
100,000
6/ 10/2018
126,000
6/ 13/2018
54,000
6/ 14/2018
61,000
6/ 15/2018
49,000
6118/2018
61,000
6/ 19/2018
29,750
89,250
6/20/2018
41,533
47,467
6/26/2018
54,000
6/27/2018
117,000
6/28/2018
125,000
7/2/2018
115,000
7/3/2018
97,000
7/5/2018
106,000
7/6/2018
103,000
7/9/2018
113,000
7/ 10/2018
110,000
7/ 1 1 /2018
109,000
7/16/2018
110,000
7/ 1712018
166,000
7/20/2018
70,000
8/ 16/2018
117,000
8/ 17/2018
78,000
8/20/2018
108,000
8/21 /2018
105,000
8/22/2018
104,000
8/23/2018
104,000
8/24/2018
58,000
8/25/2018
102,000
8/26/2018
114,000
8/27/2018
63,000
8/28/2018
119,000
8/29/2018
63,158
56,842
8/30/2018
62,667
31,333
8/31/2018
58,000
9/4/2018
76,000
9/5/2018
58,000
9/6/2018
59,000
9/7/2018
38,000
9/ 10/2018
45,000
9/ 1 112018
18,000
9/25/2018
13,000
9/26/2018
57,000
9/27/2018
81,000
9/28/2018
118,000
9/29/2018
147,000
9/30/2018
118,000
1011 /2018
123,000
10/2/2018
103,000
1013/2018
124,000
10/4/2018
141,000
10/5/2018
105,000
1016/2018
116,000
10/8/2018
115,000
10/9/2018
116,000
10/10/2018
98,000
10/16/2018
31,000
10/ 1812018
105,000
10/19/2018
99,000
1012212018
122,000
10/23/2018
119,000
10/24/2018
74,000
10/25/2018
62,000
10/26/2018
25,000
10/29/2018
114,000
10/30/2018
106,000
10/31 /2018
80,000
1 1 / 112018
44,000
1 1 /2/2018
50,000
1 1 /312018
13,000
Totals
1 1,258,000
1,655,000
508,000
1,090,000
168,750
41,533
47,467
209,917
260,491
70,000
886,842
219,000
Q I -2017
-
-
-
-
-
-
-
Q2-2017
-
296,000
494,000
90,750
41,533
47,467
89,250
-
-
Q3-2017
828,000
212,000
596,000
78,000
-
120,667
260,491
70,000
886,842
219,000
Q4-2017
1 1,258,000
1 827,000
-
-
-
-
-

Updated Attachment B

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
29-1
Ronald Byrd
Bertie
36109'30"
-76°57'54"
6.7
Leaf—Lf
29-2
Ronald Byrd
Bertie
36°09'31"
-76*58-02"
2.4
Leaf— Lf
29-3
Ronald Byrd
Bertie
36009'31"
-76°58'09"
6
Exum — ExA
29-4
Ronald Byrd
Bertie
36009'27"
-76°58'09"
9.8
Exum — ExA
29-5
Ronald Byrd
Bertie
36°09'27"
-76058'20"
11.1
Exum—ExA
29-6
Ronald Byrd
Bertie
36°09'25"
-76°58'34"
3.1
Leaf— Lf
29-7
Ronald Byrd
Bertie
36°09'24"
-76°58'10"
4.6
Granthum G
29-8
Ronald Byrd
Bertie
36°09'21"
-76°58'05"
10
Granthum Gt
29-9
Ronald Byrd
Bertie
36°09'24"
-76058'00"
0.5
Exum — ExA
29-10
Ronald Byrd
Bertie
36°09'24"
-76°57'56"
4.0
Exum — ExB
30-1
Kendred C. Williams, Jr.
Bertie
36*08'15"
-76°57'12"
15.4
Exum — ExA
30-2
Kendred C. Williams, Jr.
Bertie
36°08'22"
-76°57'13"
6.1
Exum— ExA
30-3
Kendred C. Williams, Jr.
Bertie
36°12'47"
-76*56-35"
1.3
Craven — CrA
30-4
Kendred C. Williams, Jr.
Bertie
36°12'45"
-76°56'22"
26.3
Norfo k NoB
30-5
Kendred C. Williams, Jr.
Bertie
36°12'43"
-76°56'07"
32.4
Craven — CrB
30-6
Kendred C. Williams, Jr.
Bertie
36°1231"
-76°56'09"
9.0
Craven CrB
30-7
Kendred C. Williams, Jr.
Bertie
36°12'38"
-76056'25"
12.9
Craven CrB
30-8
Kendred C. Williams, Jr.
Bertie
36012'40"
-76°56'34"
6.5
Craven — CrB
30-9
Kendred C. Williams, Jr.
Bertie
36°1241"
-76°5649"
16.4
Norfolk — NoA
30-10
Kendred C. Williams, Jr.
Bertie
36012'45"
-76°56'47"
3.7
Norfolk—NoA
30-11
Kendred C. Williams, Jr.
Bertie
36°12'48"
-76o%'45"
1.4
Norfolk —NoB
30-12
Kendred C. Williams, Jr.
Bertie
36°12'48"
-76056'39"
1.5
Norfolk —NoA
30-13
Kendred C. Williams, Jr.
Bertie
36°12'51"
-76°56'41"
5.1
Lenoir— Ln
WQ0012404 Version: 3.0 Attachment B Page 1 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
30-14
Kendred C. Williams, Jr.
Bertie
36012'56"
-7605638"
0.5
Lenoir—Ln
30-15
Kendred C. Williams, Jr.
Bertie
36013'03"
-7605636"
8.9
Leaf—Lf
30-16
Kendred C. Williams, Jr.
Bertie
36°13'09"
-76*5631"
4.5
Craven—CrA
30-17
Kendred C. Williams, Jr.
Bertie
36°13'06"
-76°5703"
28.1
Craven—CrA
30-18
Kendred C. Williams, Jr.
Bertie
36°12'55"
-76°5700"
20.9
Craven — CrA
30-19
Kendred C. Williams, Jr.
Bertie
36°12'54"
-76°56'48"
9.3
Goldsboro - GoA
30-20
Kendred C. Williams, Jr.
Bertie
369213"
-76°56'51"
10.7
Craven—CrA
30-21
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
3692'23"
-76°56'48"
7.0
Lenoir— Ln
30-22
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36°12' 16"
-76°56'53"
7.5
Craven — CrA
30-23
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36012' 16"
-76056'59"
9.2
Craven — CrA
30-24
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36°12' 18"
-76°5702"
4
Craven — CrA
30-25
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36°12' 19"
-76°57'05"
1.5
Craven — CrA
30-26
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36°12'26"
-7605712"
4.3
Craven — CrA
30-27
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36°12' 16"
-76°5708"
4.0
Craven — CrA
30-28
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36°12'13"
-76°5709"
5.1
Craven—CrA
30-29
C.S. Hollomon, Jr.
Kendred C. Williams, Jr.
Bertie
36°12'08"
-76°5707"
13.3
Craven — CrA
30-30
Kendred C. Williams, Jr.
Bertie
36°10'35"
-76°5725"
4.5
Nahunta - Na
30-31
Kendred C. Williams, Jr.
Bertie
36*1928"
-76°5724"
20.8
Exum — ExA
30-32
Kendred C. Williams, Jr.
Bertie
36°10'24"
-76°5715"
7.5
Goldsboro— GoA
30-33
Kendred C. Williams, Jr.
Bertie
36010' 18"
-76°5719"
17.8
Goldsboro — GoA
30-34
Kendred C. Williams, Jr.
Bertie
36°10'18"
-76°5718"
24.1
Goldsboro—GoA
30-35
Kendred C. Williams, Jr.
Bertie
36°10'20"
-76°5737"
0.9
Exum — ExA
30-36
David C. Powell
Kendred C. Williams, Jr.
Bertie
36013' 13"
-76°54'33"
19.9
Exum— ExA
30-37
E.M. Powell & Sons, Inc.
Kendred C. Williams, Jr.
Bertie
36°13'07"
j -76°54'26"
21.2
Exum — ExA
30-38
E.M. Powell & Sons, Inc.
Kendred C. Williams, Jr.
Bertie
36°12'49"
1 7754'30"
r 23.4
Exum — ExA
WQ0012404 Version: 3.0 Attachment B Page 2 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
30-39
E.M. Powell & Sons, Inc.
Kendred C. Williams, Jr.
Bertie
36°12'42"
-76°54'24"
25.4
Exum—ExA
30-40
T.E. Ruffin
Kendred C. Williams, Jr.
Bertie
36109'22"
-76°5724"
19.9
Exum — ExA
30-41
T.E. Ruffin
Kendred C. Williams, Jr.
Bertie
36109023"
-76°5737"
7.0
Exum — ExA
30-42
T.E. Ruffin
Kendred C. Williams, Jr.
Bertie
36°09'26"
-7605743"
4.7
Exum — ExA
30-43
T.E. Ruffin
Kendred C. Williams, Jr.
Bertie
36°09'23"
-76°5746"
7.0
Exum — ExA
30-44
James C. Askew
Kendred C. Williams. Jr.
Bertie
3691'18"
-76°5721"
3
Exurri--ExB
30-45
James C. Askew
Kendred C. Williams, Jr.
Bertie
36°11' 18"
-7605717"
6.3
Exum — ExB
30-46
James C. Askew
Kendred C. Williams, Jr.
Bertie
3601 I' l 7"
-7605710"
12.0
Gritney — Gt
30-47
Oliver B. Balance
Kendred C. Williams, Jr.
Bertie
36°11' 12"
-76°5708"
11.6
Exum — ExA
33-17
Leonard L. Godwin
William Ward
Bertie
36°13'38"
-7700905"
11.2
Norfolk —NoA
33-18
Leonard L. Godwin
William Ward
Bertie
3693'31"
-76°59'55"
11.2
Goldsboro—GoA
33-19
Ola Sanders
William Ward
Bertie
36°12'15"
-76°56'09"
16.8
Goldsboro—GoA
33-20
Ruth H. Metcalf
William Ward
Bertie
36°14'16"
-76°54'30"
3.3
Exum—ExA
33-21
Ruth H. Metcalf, et all
William Ward
Bertie
36°14'02"
-76°54'24"
12.9
Exum — ExA
33-22
Mildred Harris
William Ward
Bertie
36°13'53"
-76°54'12"
17.0
Exum—ExA
33-23
Agnes 0. Moore, et all
William Ward
Bertie
36°13'42"
-76°54'09"
10
Goldsboro — GoA
County Total
Berke
653.6
3-1
Wiley B. Gillam III
Hertford
36°19'51"
j -76050'39"
19.6
Lynchburg - Ly
3-2
Wiley B. Gillam III
Hertford
369944"
-76°5943"
37.2
Lynchburg - Ly
3-3
Wiley B. Gillam III
Hertford
36°19'45"
-76°50'28"
19.9
Norfolk—NoA
3-4
Wiley B. Gillam III
Hertford
36°19'27"
-76°48'06"
18.6
Wickham— WkB
3-5
Wiley B. Gillam III
Hertford
36°19'02"
-76048'02"
31.9
Tarboro — TaB
6-1
Stuart Pierce Farms, Inc.
Hertford
36° 16'06"
-7605620"
17.0
Craven — CrA
6-2
Stuart Pierce Farms, Inc.
Hertford
369618"
-7605620"
67.4
Caroline — CaA
6-3
Stuart Pierce Farms, Inc.
Hertford
369609"
-76055'58"
7.9
Caroline — CaA
WQ0012404 Version: 3.0
Attachment B
Page 3 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
64
Stuart Pierce Farms, Inc.
Hertford
36015'54"
-76056'16"
10.9
Caroline — CaA
6-5
Stuart Pierce Farms, Inc.
Hertford
36° 15'47"
-76°56'56"
54.0
Caroline — CaA
6-6
Stuart Pierce Farms, Inc.
Hertford
36°15'36"
-76°56'34"
23.3
Craven— CrB
6-7
Stuart Pierce Farms, Inc.
Hertford
364527"
-76*56'11"
42.2
Craven — CrB
6-9
Stuart Pierce Farms, Inc.
Hertford
36°16'01"
-W57'17"
38.9
Craven — CrA
6-10
Stuart Pierce Farms, Inc.
Hertford
36°16'43"
-76°55'34"
107.0
Caroline — CaA
6-1 IA
Stuart Pierce Farms, Inc.
Hertford
36°15'52"
-77°00'07"
41.0
Craven — CrB
6-11B
Stuart Pierce Farms, Inc.
Hertford
36°1541"
-76°59'53"
72.2
Craven — CrB
6-1 IC
Stuart Pierce Farms, Inc.
Hertford
36015'37"
-76°59'40"
29.4
Craven — CrB
6-1 ID
Stuart Pierce Farms, Inc.
Hertford
36°15'24"
-7605945"
41.2
Craven--CrB
6-11 E
Stuart Pierce Farms, Inc.
Hertford
36015'36"
-76059'37"
47.7
Craven — CrA
6-12
Stuart Pierce Farms, Inc.
Hertford
36°18'30"
-77°Ol'47"
40.4
Caroline — CaA
6-13
Stuart Pierce Farms, Inc.
Hertford
36°18'27"
-76054'52"
41.4
Craven — CrA
6-14
Stuart Pierce Farms, Inc.
Hertford
36018'10"
-76°54'59"
30.9
Craven — CrA
6-15
Stuart Pierce Farms, Inc.
Hertford
36°18'14"
-76°55'18"
48.8
Craven — CrB
6-16
Stuart Pierce Farms, Inc.
Hertford
36°16'51"
-76045'06"
46.1
Bonneau — BoB
6-17
Stuart Pierce Farms, Inc.
Hertford
36° 16'44"
-76045'38"
41.9
Bonneau — BoB
6-18
Stuart Pierce Farms, Inc.
Hertford
36°17'04"
-76°45'33"
21.0
Bonneau — BoB
6-19
Stuart Pierce Farms, Inc.
Hertford
36°16'33"
-76 43'56"
46.3
Goldsboro — GoA
6-20
Stuart Pierce Farms, Inc.
Hertford
36° 16'06"
-76'44' 18"
21.4
Goldsboro — GoA
6-21
Stuart Pierce Farms, Inc.
Hertford
36°17'50"
-76'43'10"
70.8
Bonneau — BoB
6-22
Stuart Pierce Farms, Inc.
Hertford
36016'19"
-77°02'38"
56.4
Craven — CrA
6-23
Stuart Pierce Farms, Inc.
Hertford
36°16'32"
-77°02'41"
94.9
Craven — CrA
6-24
Stuart Pierce Farms, Inc.
Hertford
36° 16'20"
-77°02'23"
41.6
Lenoir — Ln
WQ0012404 Version: 3.0 Attachment B Page 4 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Field
Owner
Lessee
County
Latitude
Longitude
Ae�e t e
Dominant Soil Series
Footnotes
9-2
Gray Pierce, et at
Hertford
36018'20"
-76°51' 10"
18.5
Norfolk — NoA
9-3
Gray Pierce
Hertford
36° 18' 14"
-76°51'20"
8.5
Norfolk — NoA
9-5
Carlyle Archer, et at
Gray Pierce
Hertford
36°l8'13"
-76051'37"
22.8
Norfolk — NoA
9-6
Gray Pierce
Hertford
36°18'15"
-76°51'46"
4.5
Goldsboro GoA
9-7
Gray Pierce
Hertford
36°18'07"
-76*5F28"
16.2
Norfolk—NoA
9-8
Gray Pierce
Hertford
36°18'03"
-76°51'36"
11.6
Norfolk—NoA
9-9
Gray Pierce
Hertford
3601 T 15"
-76051'30"
18.1
Craven — CrB
9-10
Gray Pierce
Hertford
36°1759"
-76°5F30"
5.6
Craven—CrB
9-11
Gray Pierce
Hertford
3601 T45"
-76051' 19"
10.6
Craven — CrB
9-12
Gray Pierce
Hertford
369748"
-76°51'05"
8.6
Conetoe—CoB
9-14
Gray Pierce
Hertford
36°1750"
-76°50'58"
6.7
Tarboro—TaB
9-15
Gray Pierce
Hertford
3601T58"
-76050'50"
7.7
Tarboro—TaB
9-16
Gray Pierce
Hertford
36°1T58"
-76°5l'22"
1.5
Craven—CrB
9-17
Gray Pierce
Hertford
36°18'01"
-76°5l'21"
3.6
Craven — CrB
9-18
Gray Pierce
Hertford
36°1750"
-76051'25"
14.6
Wickham—WkA
9-19
Gray Pierce
Hertford
36°1T59"
-76°5l'10"
3.7
Tarboro—TaB
9-20
Gray Pierce
Hertford
36° 18'06"
-76°51' 13"
3.9
Bonneau — BoB
9-21
Gray Pierce
Hertford
36°1738"
-76°51'49"
6.0
Craven--CrA
9-22
Gray Pierce
Hertford
36° 1 T45"
-76°51'49"
9.6
Lenoir — Ln
9-24
Gray Pierce
Hertford
3601 T47"
-76°5l'43"
13.5
Craven — CrA
9-26
Gray Pierce
Hertford
36°18'34"
-76051'45"
27.0
Craven — CrA
9-27
Gray Pierce
Hertford
36° 19' 12"
-76°51'48"
24.9
Tarboro — TaB
9-28
Gray Pierce
Hertford
3698'51"
-76052'01"
15.0
Wickham— WkA
9-29
Gray Pierce
Hertford
36°18'47"
-76°51'57"
5.7
Wickham— WkA
9-30
Gray Pierce
Hertford
36018'44"
-76051'53"
11.9
Wickham— WkA
WQ0012404 Version: 3.0 Attachment B Page 5 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
9-31
Gray Pierce, Merle Jones
Gray Pierce
Hertford
36°17'48"
-76°52'45"
11.4
Craven — CrA
9-32
Merle Jones
Gray Pierce
Hertford
36° 17'34"
-76*52136"
176
Lenoir — Ln
9-33
Gray Pierce
Hertford
36'1737"
-76052'10"
16.7
Craven—CrA
9-34
Gray Pierce
Hertford
36°17'52"
-76°53'00"
8
Craven — CrA
9-35
Gray Pierce
Hertford
36° 17'58"
-76°52'55"
13
Craven — CrA
9-37
R.C. Kennington
Gray Pierce
Hertford
36°18'33"
-76°52'45"
16
Craven — CrB
9-38
R.C. Kennington
Gray Pierce
Hertford
36°18'27"
-76°52'32"
8
Craven — CrB
9-40
Gray Pierce
Hertford
36019'21"
-76053'33"
11.2
Wickham— WkB
9-41
Gray Pierce
Hertford
36019'33"
-76°53'28"
12.4
Wickham — WkA
9-42
Gray Pierce
Hertford
36019'23"
-77001'20"
26.4
Caroline — CaA
9-43
Gray Pierce
Hertford
36°19116"
-77°00'38"
39.4
Caroline —CaA
9-45
Gray Pierce
Hertford
36°19'11"
-77°06'56"
73.7
Craven — CrA
9-46A
Gray Pierce
Hertford
3699' 19"
-77°07'49"
36.7
Craven — CrA
9-46B
Gray Pierce
Hertford
36019'15"
-7700727"
42.5
Craven — CrA
9-47
Gray Pierce
Hertford
369933"
-77°08'09"
18.8
Craven — CrA
9-48
Gray Pierce
Hertford
36018 32'
-77006'31"
45.1
Craven CrA
9-50
Gray Pierce
Hertford
36°18'53"
-77°06'43"
63.8
Craven CrA
9-52
Gray Pierce
Hertford
36°18'57"
-77°07'03"
27.4
Craven CrA
9-53
Gray Pierce
Hertford
36019'06"
-77°0713"
26.7
Craven—CrB
10-1
J.H. Drewry, III
Hertford
36032'36"
-77°09'O1"
7.8
Tarboro —TaB
10-2
J.H. Drewry, III
Hertford
36032'30"
-77°08'36"
34.1
Wickham — WkA
10-3
J.H. Drewry, III
Hertford
369217"
-77°08'33"
67.7
Autryville —AuB
10-4
J.H. Drewry, III
Hertford
36°32'35"
-77°O8'16"
6.9
Lynchburg —Ly
10-5
J.H. Drewry, III
Hertford
36°32'58"
-77008'17"
20.0
Norfolk —NoA
10-6
J.H. Drewry, III
Hertford
36°52'21"
-77°OT56"
35.0
Craven—CrA
WQ0012404 Version: 3.0 Attachment B Page 6 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
10-7
J.H. Drewry, III
Hertford
36°32'17"
-77°08'07"
35.4
Norfolk—NoA
10-8
J.H. Drewry, III
Hertford
36°32'15"
-77*08'18"
42.3
Norfolk—NoA
10-9
J.H. Drewry, III
Hertford
36°32'24"
-77°07'46"
12.3
Autryville — AuB
10-10
J.H. Drewry, III
Hertford
36°32'27"
-77°07'41"
26.3
Bonneau—BoB
10-11
J.H. Drewry, III
Hertford
36°32'01"
-77°07'07"
4.9
Norfolk—NoA
11-1
CF Industries, Inc.
Granville Farms, Inc.
Hertford
36°22'19"
-76°52'10"
40.4
Craven CrA
11-2
CF Industries, Inc.
Granville Farms, Inc.
Hertford
36022' 17"
-76°5l'47"
67.2
Craven—CrA
11-3
CF Industries, Inc.
Granville Farms, Inc.
Hertford
36°22'01"
-76°51'54"
41.4
Craven — CrA
12-1
Douglas R. White
Tuscarora Greens
Hertford
36023'03"
-76°54'59"
8.3
Lenoir— Ln
12-2
Douglas R. White
Tuscarora Greens
Hertford
36°22'57"
-76°55' 11"
8.8
Lenoir — Ln
12-3
Douglas R. White
Tuscarora Greens
Hertford
36°22'40"
-76°54'57"
6.3
Craven — CrB
12-4
Douglas R. White
Tuscarora Greens
Hertford
36°22'43"
-76°54'46"
30.0
Craven — CrA
12-5
Douglas R. White
Tuscarora Greens
Hertford
36°22'33"
-76°54'51"
5.0
Craven — CrA
12-6
Douglas R. White
Tuscarora Greens
Hertford
36°22'55
-76054'52"
18.0
Craven—CrA
23-1
Johnny Powell
Hertford
36017'01"
-76044-02"
24.9
Norfolk—NoA
23-2
Johnny Powell
Hertford
3696'42"
-76°45' 12"
13.1
Norfolk — NoA
23-3
Thaddeus F. Scott
Johnny Powell
Hertford
36°17'46"
-76°45'44"
39.1
Norfolk—NoA
23-4
Thaddeus F. Scott
Johnny Powell
Hertford
36°17'55"
-76045-44"
22.0
Norfolk—NoA
23-5
Johnny Powell
Hertford
36018' 19"
-76°47' 17"
27.7
Norfolk — NoB
23-6
Johnny Powell
Hertford
36°18'02"
-76050'25"
19.9
Conetoe—CoB
23-7A
Johnny Powell
Hertford
36°17'42"
-76°49'32"
33.5
Craven — CrA
23-713
Johnny Powell
Hertford
36°18'03"
-76°49' 10"
13.2
Bonneau — BoB
23-8
Johnny Powell
Hertford
36°17' 12"
-76°53'00"
29.8
Caroline — CaA
23-9
Johnny Powell
Hertford
36°19'50"
-76°51'05"
19.8
Craven—CrA
23-10
Johnny Powell
Hertford
36°20'26"
-76°49'47"
15.8
Craven — CrA
WQ0012404 Version: 3.0 Attachment B Page 7 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
23-12
Johnny Powell
Hertford
36°22'27"
-76°54'50"
26.3
Craven — CrA
23-13
Johnny Powell
Hertford
36021'38"
-76°54'02"
20.5
Craven — CrA
23-14
Johnny Powell
Hertford
36°21'46"
-76°54'23"
11.7
Craven — CrA
23-15
Johnny Powell
Hertford
36°22'38"
-76°5602"
19.0
Norfolk—NoA
23-16
Johnny Powell
Hertford
36°18'35"
-76055'42"
45.0
Craven —CrB
24-2
Chester Powell
Hertford
36°19' 15"
-76°50'40"
14.6
Norfolk — NoA
24-3
Chester Powell
Hertford
36019'28"
-76°50'34"
11.6
Wickham - WkB
24-4
Chester Powell
Hertford
369 8'56"
-76°48'52"
10.8
Goldsboro — GoA
24-5
Chester Powell
Hertford
36018'43"
-76°48'52"
13.0
Bonneau — BoB
24-6
Chester Powell
Hertford
36°20'24"
-76051'54"
13.5
Craven — CrA
24-7
Chester Powell
Hertford
36*20' 17"
-76051'46"
3.6
Craven — CrA
24-8
Chester Powell
Hertford
36°15'50"
-76°56'33"
6.3
Lenoir— Ln
24-9
Chester Powell
Hertford
36°15'50"
-76053'54"
12.7
Craven — CrA
24-10
Shirley Deramus
Chester Powell
Hertford
36°18'04"
-76°43'20"
6.1
Bonneau — BoB
24-11
Shirley Deramus
Chester Powell
Hertford
36018'09"
-76°43'13"
10.5
Goldsboro —GoA
24-13
Chester Powell
Hertford
36° 15'23"
-76°49'06"
14.8
Craven — CrA
25-1
Tommy Castelow
Hertford
36°2l'58"
-76°53'54"
39.8
Caroline —CaA
25-2
Tommy Castelow
Hertford
3699'46"
-76°49'06"
9.3
Norfolk — NoA
25-3
Tommy Castelow
Hertford
36°2902"
-76°49'03"
32.2
Norfolk — NoA
25-4
Tommy Castelow
Hertford
36020' 17"
-76°49'02"
30.2
Craven — CrA
25-5
Tommy Castelow
Hertford
36°20'09"
-76048-42"
25.6
Craven — CrA
25-6
Tommy Castelow
Hertford
36°20'00"
-76047'36"
27.2
Craven — CrA
25-7
Tommy Castelow
Hertford
36°21' 16"
-76047'38"
12.3
Craven — CrA
25-8
Tommy Castelow
Hertford
36°20'43"
-76054'05"
16.6
Craven — CrA
25-9
Tommy Castelow
Hertford
36°20'37"
-76054'O1"
34.7
Craven — CrA
WQ0012404 Version: 3.0 Attachment B Page 8 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
25-10
Tommy Castelow
Hertford
36°20'26"
-76054'07"
11.3
Craven — CrA
25-11
Tommy Castelow
Hertford
36020'25"
-76°54' 13"
4.8
Craven — CrA
25-12
Tommy Castelow
Hertford
36°20'01"
1 -76054'28"
32.0
Craven — CrA
26-1
Beechwood Country Club
Hertford
36°21'58"
-770W38"
7.9
Caroline — CaA
26-2
Beechwood Country Club
Hertford
36°21'53"
-77°00'47"
10.5
Craven — CrB
26-3
Beechwood Country Club
Hertford
36°21'37"
-770W37"
8.3
Craven — CrB
26-4
Beechwood Country Club
Hertford
36021'43"
-77°00'01 "
18.2
Caroline — CaB
27-52
Lori S. Burgess
Steven Burgess
Hertford
36025'02"
-77°06'01 "
44.7
Norfolk — NoA
27-53
Lori S. Burgess
Steven Burgess
Hertford
36°24'42"
-77°05'55"
10.0
Norfolk—NoA
27-54
Steven Burgess
Hertford
36024'36"
-77°0606"
42.7
Norfolk—NoA
27-55
Steven Burgess
Hertford
36°2F18"
-7700740"
6.6
Craven—CrA
27-56
Steven Burgess
Hertford
36°21' 19"
-77°0731 "
9.8
Craven — CrA
27-57
Steven Burgess
Hertford
36021'22"
-7700721 "
12
Craven — CrA
27-58
Steven Burgess
Hertford
36°21' 11 "
-77007' 17"
4.5
Lenoir — Ln
27-59
Steven Burgess
Hertford
36021'08"
-77°07'23"
9.0
Lenoir— Ln
27-60
Steven Burgess
Hertford
36°2l'03"
-77°0707"
2
Lenoir— Ln
27-61
Steven Burgess
Hertford
36°21'04"
-77006'59"
14.9
Craven — CrA
27-62
Steven Burgess
Hertford
36020'55"
-7700702"
3.1
Craven — CrA
27-63
Adam & Wendy Burgess
Steven Burgess
Hertford
36021' 14"
-77°0655"
14.7
Craven — CrA
27-64
Adam & Wendy Burgess
Steven Burgess
Hertford
36021'24"
-77°0650"
29.5
Craven — CrA
28-1
Judith, Allison, & Walter Perry
Hertford
36°19131"
-77*50-15"
17.6
Norfolk—NoA
28-2
Judith, Allison, & Walter Perry
Hertford
36°19'27"
-76050'05"
17.5
Norfolk — NoA
28-3
Judith, Allison, & Walter Perry
Hertford
36°19'48"
-76050'10"
25.1
Norfolk—NoA
28-4
Judith, Allison, & Walter Perry
Hertford
36019021"
-76°49'51"
10.8
Wickham— WkA
28-5
Judith, Allison, &Walter Perry
Hertford
36°1910"
76°49'34"
9.4
Conetoe — CoB
WQ0012404 Version: 3.0 Attachment B Page 9 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
28-6
Judith, Allison, & Walter Perry
Hertford
36°19'24"
-76°50'24"
20.4
Norfolk—NoA
28-7
Judith, Allison, & Walter Perry
Hertford
36°19'50"
-76051'03"
16.0
Norfolk — NoA
28-8
Judith, Allison, & Walter Perry
Hertford
36°19'42"
-76051'06"
9.2
Goldsboro--GoA
28-9
Judith, Allison, & Walter Perry
Hertford
36°19'42"
-76051'13"
9.9
Goldsboro —GoA
28-10
Judith, Allison, & Walter Pent'
Hertford
36°19'44"
-76°51'l8"
1.7
Goldsboro — GoA
28-11
Judith, Allison, & Walter Perry
Hertford
36°19'48"
-76°51'15"
3.7
Craven — CrB
28-12
Judith, Allison, & Walter Perry
Hertford
36°19'47"
-76*51'l V
3.6
Craven — CrB
28-13
John Lock Mitchell
Walter Perry
Hertford
36017'42"
-76°49'37"
8.7
Bonneau — BoB
28-14
John Lock Mitchell
Walter Perry
Hertford
36°17'36"
-76049'45"
7.0
Bonneau — BoB
28-15
Betty Perry, John Mitchell, Eleanor Lane, Penny
Beasley, & Ken Mitchell
Walter Perry
Hertford
36° 17'19"
-76050-11"
17.4
Craven — CrA
28-16
John Mitchell, Eleanor Lane, Penny Beasley, Ken
Mitchell & Wiccacon Properties, LLC
Walter Pent'
Hertford
36°18'02"
76°50'23"
18.9
Conetce — CoB
28-17
Margaret Hall
Walter Perry
Hertford
36°23'01"
-76°56-51"
16.9
Craven — CrA
28-18
Betty Everette Perry
Walter Perry
Hertford
36°17'30"
-76°49'53"
7.4
Craven — CrA
31-1
Ray & Linda Chamblee
Hertford
36°20'42"
-76°55'26"
8.8
Craven — CrA
31-2
Jackie Chamblee
Ray Chamblee
Hertford
36*20*40"
-76°5520"
9.6
Craven— CrB
31-3
Jackie Chamblee
Ray Chamblee
Hertford
36°20'47"
-76°55'13"
15.9
Craven — CrA
314
Ray & Linda Chamblee
Hertford
36°20'43"
-76°55'04"
8.8
Craven — CrA
31-5
Ray & Linda Chamblee
Hertford
36°17'31"
-76°55'16"
5.9
Goldsboro--GoA
32-1
Janice Simmons Sessoms
William H. Sessoms
Hertford
36°17'55"
-76°48'53"
7.0
Wakulla - WaB
32-2
William H. Sessoms
Hertford
36°17'55"
-76048'42"
30.6
Lynchburg — Ly
32-3
William H. Sessoms
Hertford
36°17'27"
-76048'38"
5.0
Craven — CrB
324
Joyce Ann Sessoms
William H. Sessoms
Hertford
36018'07"
-76°48'45"
5.0
Bonneau — BoB
32-5
Joyce Ann Sessoms
William H. Sessoms
Hertford
36017'43"
-76*49'16"
5.5
Lynchburg — Ly
32-6
William H. Sessoms
Hertford
369742"
-76°49'27"
2.7
Lynchburg— Ly
WQ0012404 Version: 3.0 Attachment B Page 10 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
32-7
William H. & Joyce Ann Sessoms
Hertford
36°1 724"
-7604758"
28.9
Goldsboro - Go
32-8
William H. & Delores Sessoms
Hertford
369733"
-76°4723"
23.2
Norfolk —NoB
32-9
William H. & Delores Sessoms
Hertford
369736"
-76°4736"
13.3
Norfolk—NoB
32-10
William H. & Delores Sessoms
Hertford
369742"
-76°4734"
7.3
Norfolk—NoB
32-11
Wiccacon Properties, LLC
William H. Sessoms
Hertford
369747"
-76°49'32"
4.3
Craven—CrA
32-12
Ernest Chamblee
William H. Sessoms
Hertford
36°15'23"
-76°49108"
14.0
Craven—CrA
33-1
William W & Nellie Ward
William Ward
Hertford
36°14'36"
-76056'23"
3.0
Caroline— CaB
33-2
William W & Nellie Ward
William Ward
Hertford
36°14'51"
-76°56'23"
11.9
Craven — CrC2
33-3
William W & Nellie Ward
William Ward
Hertford
36°14'47"
-76056'21"
15.1
Norfolk—NoB
33-4
William W & Nellie Ward
William Ward
Hertford
36°14'48"
-76°56'12"
13.6
Norfolk —NoB
33-5
William W & Nellie Ward
William Ward
Hertford
36015'10"
-76°56O8"
14.2
Tarboro— TaB
33-6
William W & Nellie Ward
William Ward
Hertford
36014'43"
-76°5610"
14.6
Norfolk — NoB
33-7
William W & Nellie Ward
William Ward
Hertford
36°14'37"
-76°5608"
5.9
Craven — CrB
33-8
William W & Nellie Ward
William Ward
Hertford
3694'35"
-76°56'14"
3.0
Craven—CrB
33-9
Michael A. & Deborah Spalding
William Ward
Hertford
36°14'23"
-76058'28"
14.2
Craven — CrA
33-10
Michael A. & Deborah Spalding
William Ward
Hertford
3694'28"
-76°58'27"
8.0
Craven—CrB
33-11
Michael A. & Deborah Spalding
William Ward
Hertford
36°14'26"
-76°58'17"
3.7
Craven - CrB
33-12
Michael A. & Deborah Spalding
William Ward
Hertford
36'14'21"
-76°58'17"
2.4
Craven —CrA
33-13
Rosa H. Sessoms
William Ward Hertford
Hertford
36°15'09"
-77°00'47"
25.0
Craven — CrA
33-14
Rosa H. Sessoms
William Ward Hertford
Hertford
36015'12"
-7700936"
6.3
Leaf —Lf
33-15
Rosa H. Sessoms
William Ward
Hertford
36°15'15"
-77°0929"
2.8
Craven—CrA
33-16
Rosa H. Sessoms
William Ward
Hertford
36°15'20"
-76°0931"
4.2
Craven—CrA
County Total
Hertford
4,212.3
34-1
Nellie B. Brown
Martin
35°59'36"
-77°2910"
26.5
Goldsboro —GoA
34 2
Nellie B. Brown
Martin
35°59 30"
-77°20' 17"
19.1
Goldsboro — GoA
WQ0012404 Version: 3.0 Attachment B Page 11 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
(Tuner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
34-3
Nellie B Brown
Martin
35°59'26"
-77*20'17"
3.8
Lynchburg— Ly
34-4
Nellie B Brown
Martin
35°59120"
-77'20'16"
27.1
Lynchburg— Ly
County Total
Martin
76.5
15-1
J. Elliot Stephenson
Northampton
36°28'42"
-77°26'06"
19.2
Lynchburg— Ly
15-2
J. Elliot Stephenson
Northampton
36°28'31"
-77°25'43"
27.3
Craven — CrA
15-3
J. Elliot Stephenson
Northampton
36°28' 19"
-77°26'06"
38.0
Caroline — CrB
15-4
J. Elliot Stephenson
Northampton
36°25'47"
-77°25'26"
41.3
Norfolk - NoA
15-5
J. Elliot Stephenson
Northampton
36026'06"
-77125'40"
71.3
Gritney — GxB
15-6
J. Elliot Stephenson
Northampton
36°26' 17"
-77°25'44"
37.1
Gritney — GxB
15-7
J. Elliot Stephenson
Northampton
36°26' 12"
-77°24'48'
13.1
Norfolk - NoA
15-8
J. Elliot Stephenson
Northampton
36026' 19"
-77028'39"
35.6
Goldsboro — GoA
15-9
J. Elliot Stephenson
Northampton
36026'49"
-7702639"
15.1
Gritney — GxB
15-10
J. Bentley Stephenson
J. Elliot Stephenson
Northampton
36°51'21"
-77*2621"
14.2
Gritney — GxB
15-11
J. Bentley Stephenson
J. Elliot Stephenson
Northampton
36°26'44"
-77°26'25"
14.5
Gritney —GxB
15-12
J. Elliot Stephenson
Northampton
36026'09"
-77°26'36"
9.2
Gritney —GxB
15-13
J. Elliot Stephenson
Northampton
36°26'03"
-77°26125"
17.2
Gritney —GxB
15-14
J. Elliot Stephenson
Northampton
36026'21"
-77026'07"
19.9
Gritney —GxB
15-15
J. Elliot Stephenson
Northampton
36*28'18"
-77°25'54"
24.3
Bonneau—BoB
15-16
J. Elliot Stephenson
Northampton
36°28'24"
-77°25'41"
22.8
Bonneau—BoB
15-17
J. Elliot Stephenson
Northampton
36028'09"
-77°25'52"
33.7
Craven — CrA
18-1
Thomas Williams
Northampton
36029'41"
-77007'55"
12.0
Craven —CrB
18-2
Thomas Williams
Northampton
36°29'52"
-77008'03"
15.0
Craven — CrA
19-1W
C.C. Woodard
Northampton
36030'46"
-77120'27"
31.7
Norfolk—NoB
19-2W
C.C. Woodard
Northampton
36°40'47"
-77020'48"
21.4
Norfolk—NoB
19-3W
C.C. Woodard
Northampton
36°30'36"
-77020'56"
69.7
Norfolk —NoB
WQ0012404 Version: 3.0 Attachment B Page 12 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
19-4W
C.C. Woodard
Northampton
36030'27"
-77020'45"
76.7
Norfolk — NoB
19-5W
Cecil Whitehead
C.C. Woodard
Northampton
3603U'18"
-7702950"
12.8
Norfolk NoB
19-6W
Amanda Cooke, et al
Cecil Whitehead
Northampton
369932"
-7702933"'
18.6
Norfolk—NoB
19-7W
C.C. Woodard
Northampton
36030'18"
-7702910"
85.6
Norfolk—NoA
19-8W
C.C. Woodard
Northampton
3603915"
-77020'29"
10.9
Norfolk—NoB
19-9W
C.C. Woodard
Northampton
3603935"
-77020'21 "
15.7
Norfolk—NoB
19-IOW
C.C. Woodard
Northampton
36031'25"
-77020'54"
3.9
Bonneau - BoB
19-1 1W
C.C. Woodard
Northampton
36031'28"
-77021Y44"
29.5
Bonneau - BoB
19-12W
C.C. Woodard
Northampton
36031'43"
-77020'25"
4.6
Bonneau - BoB
19-13W
C.C. Woodard
Northampton
369142"
-7702910"
7.9
Norfolk NoB
19-14W
C.C. Woodard
Northampton
36031' 19"
-7702tY 10"
9.3
Norfolk — NoB
19-ISW
C.C. Woodard
Northampton
36°31'26"
-77020'10"
11
Norfolk NoB
19-1G
C.C. Woodard
Northampton
3603709"
-77°21'07"
48.6
Altavista -AtA
19-2G
C.C. Woodard
Northampton
3692'17"
-77021'22"
13.6
Tarboro - TaB
19-3G
C.C. Woodard
Northampton
36032'26"
-77021'03"
36.2
Altavista - AtA
194G
C.C. Woodard
Northampton
36032'43"
-77'20'57"
42.5
Wickham - WkA
19-SG
C.C. Woodard
Northampton
3603739"
-77021' 13"
20.7
Roanoke- Ro
21-1
C.G. Perry
Northampton
36n5'48"
-77°20'07"
19.6
Norfolk NoB
21-2
C.G. Perry
Northampton
36025'39"
-77020'45"
29.2
Caroline - CaB
21-3
C.G. Pent'
Northampton
36°25'38"
-77020'17"
11.2
Caroline- CaB
21-4
C.G. Perry
Northampton
36025'29"
-77020'34"
3.3
Norfolk - NoA
21-5
C.G. Perry
Northampton
36°25'31"
-7702937"
9.3
Norfolk—NoB
21-6
C.G. Perry
Northampton
36025'26"
-77020'31"
4.0
Norfolk—NoB
21-7
C.G. Perry
Northampton
36n5'25"
-77°20'25"
6.2
Norfolk—NoB
21-8
Robert Jones
Robert Jones
Northampton
36025' 12"
-7702928"
50.4
Norfolk — NoA
WQ0012404 Version: 3.0 Attachment B Page 13 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
21-10
C.G. Perry
Northampton
36°23'41"
-77*24'16"
44.3
Norfolk NoB
21-11
C.G. Perry
Northampton
36°27'57"
-77°25'57"
33.7
Craven - CrA
21-13
C.G. Pent'
Northampton
36°27'40"
-77°25'35"
15.4
Norfolk - NoA
21-14A
C.G. Perry
Northampton
3602728"
-77°25'40"
13.8
Goldsboro - GoA
21-14B
C.G. Perry
Northampton
36°27'34"
-77025'39"
18.0
Goldsboro -GoA
21-15
C.G. Perry
Northampton
3602734"
-77025'16"
17.5
Goldsboro -GoA
21-16
C.G. Perry
Northampton
3602728"
-77°25'16"
5.7
Goldsboro -GoA
21-17
C.G. Perry
Northampton
36°25'40"
-77°21'08"
4.5
Norfolk - NoA
21-18
Robert Jones
Robert Jones
Northampton
36°25'28"
-77°21'13"
6.7
Norfolk-NoA
21-20
Robert Jones
Robert Jones
Northampton
36°25'23"
-77°21' 12"
3.7
Norfolk - NoA
21-21
Robert Jones
Robert Jones
Northampton
36°25'34"
-77°21'02"
31.4
Norfolk - NoA
21-22
Robert Jones
Robert Jones
Northampton
36°25'25"
47°21'02"
5.7
Goldsboro - GoA
22-1
Charles J. Stephenson
Northampton
36°27'24"
-77°24'58"
23.7
Goldsboro - GoA
22-2
Charles J. Stephenson
Northampton
36°27'21"
-77124'49"
19.6
Goldsboro - GoA
22-3
Charles J. Stephenson
Northampton
36°2717"
-77°24'38"
11.4
Goldsboro - GoA
22-4
Charles L Stephenson
Northampton
36°26'56"
-77024-31"
9.8
Goldsboro - GoA
22-5
Charles J. Stephenson
Northampton
36°25'44"
-77023'58"
6.9
Goldsboro - GoA
27-1
Neil Burgess
Stephen Burgess
Northampton
36°20'00"
-77'12'50"
47.8
Norfolk—NoA
27-2
Neil Burgess
Stephen Burgess
Northampton
36*2600"
-77°12'36"
56.4
Norfolk—NoA
27-3
Neil Burgess
Stephen Burgess
Northampton
36025'54"
-77012'27"
25.5
Rains — Ra
27-4
Neil Burgess
Stephen Burgess
Northampton
36025'41"
-77°12'41"
27.5
Norfolk—NoA
27-5
Neil Burgess
Stephen Burgess
Northampton
36*25'18"
-77012'39"
16.0
Norfolk-NoA
27-6
Stephen Burgess
Stephen Burgess
Northampton
36°26'07"
-77011'22"
53.4
Bonneau - BoB
27-7
Judi B. Burgess
Stephen Burgess
Northampton
36°24'20"
-77°13'28"
13.9
Craven - CrA
27-8
Judi B. Burgess
Stephen Burgess
Northampton
36°23'59"
-77°14'10"
17.7
Norfolk—NoB
WQ0012404 Version: 3.0 Attachment B Page 14 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
Site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
27-9
Lori S. Burgess
Northampton
36023'56"
-77013'57"
18.6
Caroline - CaA
27-10
Stephen Burgess
Northampton
36023'52"
-77013-51"
20.3
Craven - CrA
27-11
Stephen Burgess
Northampton
36°23'42"
-77°13'50"
23.4
Craven - CrA
27-12
Stephen Burgess
Northampton
36°23'39"
-77°13'40"
16.7
Craven - CrA
27-13
Stephen Burgess
Northampton
36°23'34"
-77°13'13"
5.2
Craven - CrA
27-14
Lori S. Burgess
Stephen Burgess
Northampton
36°24'34"
-77°16'04"
14.7
Goldsboro - GoA
27-15
Stephen Burgess
Northampton
36026'31"
-77017'10"
6.5
Norfolk—NoB
27-16
Stephen Burgess
Northampton
36126'27"
-77°17'02"
5.1
Norfolk—NoB
27-17
Stephen Burgess
Northampton
36°26'32"
-77°16'52"
21.9
Norfolk—NoB
27-18
Lori S. Burgess
Northampton
36°26'10"
-77°14'39"
11.1
Goldsboro -GoA
27-19
Lori S. Burgess
Northampton
36°26'18"
-77°14'24"
18.4
Goldsboro -GoA
27-20
Eloise T. Ward
Stephen Burgess
Northampton
36°26'20"
-77° 14' 17"
12.9
Goldsboro - GoA
27-21
Eloise T. Ward
Stephen Burgess
Northampton
36026' 19"
-77° 14' 13"
3.8
Goldsboro - GoA
27-22
Eloise T. Ward
Stephen Burgess
Northampton
36126'34"
-77° 14' 15"
6.7
Goldsboro - GoA
27-23
Eloise T. Ward
Stephen Burgess
Northampton
36027'49"
-77° 15-27"
32.5
Bonneau - BoB
27-24
Eloise T. Ward
Stephen Burgess
Northampton
36028'07"
-7715' 16"
21.5
Bonneau - BoB
27-25
Eloise T. Ward
Stephen Burgess
Northampton
36°28'04"
-77°l4'45"
35.2
Bonneau - BoB
27-26
Eloise T. Ward
Stephen Burgess
Northampton
36°27'53"
-77°14'41"
11.5
Norfolk - NoB
27-27
Eloise T. Ward
Stephen Burgess
Northampton
36°28'02"
-77014'34"
14.4
Norfolk — NoB
27-28
Eloise T. Ward
Stephen Burgess
Northampton
36°2752"
-77° 14'25"
25.3
Norfolk — NoB
27-29
Eloise T. Ward
Stephen Burgess
Northampton
36°27'45"
-77014' 17"
60.5
Norfolk — NoB
27-30
Eloise T.Ward
Stephen Burgess
Northampton
36*28'11"
-7794'51"
5.7
Autryville -AuA
27-31
Eloise T. Ward
Stephen Burgess
Northampton
36°28'16"
-77°14'52"
10.5
Norfolk—NoA
27-32
Eloise T. Ward
Stephen Burgess
Northampton
36°28'21 "
-7794'S2"
26.0
Bonneau — BoB
r27-33
Eloise T.Ward
Stephen Burgess
Northampton
36°28'21"
-77-14-42"
9.9
Norfolk —NoA
WQ0012404 Version: 3.0 Attachment B Page 15 of 16

ATTACHMENT B - Approved Land Application Sites
CF Nitrogen, Inc.
Certification Date: February 14, 2018
Permit Number: WQ0012404 Version: 3.0
site/
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
27-34
Eloise T. Ward
Stephen Burgess
Northampton
3602826"
-7701430"
17.6
Bonneau — BoB
27-35
Eloise T.Ward
Stephen Burgess
Northampton
36128'30"
-77014'18"
9.1
Goldsboro —GoA
27-36
Eloise T. Ward
Stephen Burgess
Northampton
36028"24"
-77013'57"
9.3
Autryville — AuA
27-37
Eloise T. Ward
Stephen Burgess
Northampton
36028'23"
-77014'12"
17.2
Autryville — AuA
27-38
Eloise T. Ward
Stephen Burgess
Northampton
36128'10"
-77014'09"
3.0
Norfolk - NoA
27-39
Kevin B. Burgess
Stephen Burgess
Northampton
36026'40"
-7701240"
20.6
Norfolk-NoB
2740
Kevin B. Burgess
Stephen Burgess
Northampton
36026'33"
-77012'35"
21.0
Norfolk -NoB
2741
Stephen Burgess
Northampton
36127'33"
-77111'45"
9.8
Norfolk - NoB
2742
Stephen Burgess
Northampton
3612743"
-77' 11'32"
93.5
Bonneau — BoB
2743
Stephen Burgess
Northampton
36027'35"
-77011'21"
17.7
Norfolk—NoB
2744
Stephen Burgess
Northampton
3612743"
-77° 1 F] V
29
Bonneau — BoB
2745
Stephen Burgess
Northampton
36027'49"
-77°l 1'04"
18
Norfolk—NoB
2746
Stephen Burgess
Northampton
36027'27"
-77011'18"
13.9
Bonneau — BoB
27-47
Stephen Burgess
Northampton
3612736"
-77011'06"
20.8
Bonneau - BoB
2748
Kevin B. Burgess
Stephen Burgess
Northampton
36027'31"
-77010'15"
14.8
State —StA
27.49
Kevin B. Burgess
Stephen Burgess
Northampton
36027'27"
-77010'07"
6.1
Tarboro — TaB
27-50
Kevin B. Burgess
Stephen Burgess
Northampton
36027'38"
-77009'59"
17.9
Altavista— AtA
27-51
Kevin B. Burgess
Stephen Burgess
Northampton
36027'38"
-77009'40"
52.7
Tarboro—TaB
27-65
Bobby Bridges
Neil Bridges
Northampton
36025'50"
-77015101"
67.3
Bonneau— BoB
27-66
Neil & Donna B. Burgess
Northampton
36124'50"
-77015'10"
18.1
Norfolk - NoB
27-67
Fannie Bryant
Stephen Burgess
Northampton
3602746"
77010'47"
33.7
Bonneau - BoB
27-68
Martha Pearlman
Northampton
36030'5"
77011'14"
58.0
Goldsboro - GoA
27-69
Ronald Woodard
Northampton
36029'56"
77011'l8"
42.2
Gritney -GxB
27-70
Ronald Woodard
Northampton
36028'54"
7701225"
85.4
Lynchburg -Ly
County Total
Northampton
2,849.8
Permit Total
7,792.2
WQ0012404 Version: 3.0 Attachment B Page 16 of 16

Landowner Agreement Attachments & Lessee Agreement
Attachments
(NO NEW AGREEMENTS WERE OBTAINED IN 2018)

Groundwater Data

PREPARED ON EEHALF OF:
CF Industries Holdings, Inc.
4 Parkway North
Suite 400
Deerfield, IL
PREPARED BY:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, NC 27616
February 19, 2019

February 19, 2019
North Carolina Department of Environmental Quality
1636 Mail Service Center
Raleigh, NC 27699
Attention: Non Discharge Compliance Unit
Reference: Groundwater Monitoring Report Permit No. WQ0012404
January 1, 2018 thru December 31, 2018
CF Nitrogen, Inc.
Cofield, North Carolina
EPA ID No. NCD065288847
S&ME Project No. 1040-98-044R
To Whom It May Concern:
On behalf of CF Nitrogen, Inc. (CFN), a wholly -owned subsidiary of CF Industries Holding, Inc. (CFIH), S&ME, Inc.
(S&ME) is submitting the CY 2018 annual groundwater monitoring report for the CFN site located in Cofield,
North Carolina (Figure 1) as required by the Land Application Permit (Permit No. WQ0012404 dated of January 25,
2016). S&ME completed this annual report while under contract with CFIH.
Groundwater Recovery and Distribution Volumes
Weekly flow meter readings were recorded with monthly and quarterly volume. Based on flow meter readings
recorded from Transfer Pump Station #1 beginning January 1, 2018, and ending December 28, 2018,
approximately 12,355,200 gallons of groundwater were removed from the confined shallow aquifer in 2018.
Quarterly flow amounts for Transfer Pump Station #1 were as follows:
1st Quarter (January — March 2018): 1,872,400 gallons
2nd Quarter (April — June 2018): 3,985,900 gallons
3rd Quarter (July — September 2018): 3,235,800 gallons
4th Ouarter (October — December 2018): 3,261,100 alq Ions
Total Groundwater Recovery for 2018: 12,355,200 gallons
Based on flow meter readings from Transfer Pump Station #2, approximately 12,758,000 gallons of water were
transferred from the storage basin for land application. The nitrogen -enriched groundwater was applied to a
variety crops throughout the year including corn, wheat, soybeans, and fescue. The following volumes of
groundwater may differ slightly to those reported in the land application report, because meter readings were
S&ME, Inc. 13201 Spring Forest Road I Raleigh, NC 27616 1 p 919.872.2660 1 www.smeinc.com

r
Groundwater Monitoring Report Permit No. WQ0012404
January 1, 2018 thru December 31, 2018
CF Nitrogen, Inc.
Cofield, North Carolina
EPA ID No. NCD065288847
S&ME Project No. 1040-98-044R
read on dates when weekly inspections were conducted, which may have been on different days that were read
from the land application contractor. The flow volumes were recorded during weekly inspections and summed to
calculate quarterly volumes of groundwater that was land applied to agricultural fields.
Quarterly amounts for 2018 were as follows:
V Quarter (January — March 2018): 2,276,000 gallons
2n1 Quarter (April —June 2018): 3,732,000 gallons
3rd Quarter (July — September 2018): 3,419,000 gallons
4tn Quarter (October — December 2018): 3,331,000 gallons
Total Groundwater Applied for 2018: 12,758,000 gallons
Land application of nitrogen -enriched groundwater was recorded at 12,758,000 million gallons for CY 2018. Due
to a high frequency of rain events through the year, as well as two hurricanes (Florence and Michael), land
application efforts were not able to maintain the groundwater level within the slurry wall at an elevation below 30
feet relative to mean sea level (ft-msl). The total annual recorded rainfall at the Ahoskie site was 50.65 inches,
compared with the average of 46 inches for this area. The amount and frequency of rainfall in 2018 also resulted
in restricted land application caused by wet field conditions. Considerable efforts have been made to remove
groundwater when weather permits.
Groundwater elevations were also measured on a monthly basis during 2018. The monthly groundwater elevation
data from December 29, 2017 through December 28, 2018, are presented in Table 1. As required in the permit,
potentiometric maps showing quarterly interpretations of general groundwater elevations based on end of month
measurements for January, April, July and October 2018 are included as Figures 2, 3, 4 and 5.
As required in Attachment C of the Non -Discharge Permit, cross -sectional views of water levels measured in
piezometers PI-11 — PO-12 and PI-2 — PO-236 were prepared and are attached as Figures 2A, 3A, 4A and 5A for
each corresponding quarterly potentiometric map. Additional cross -sectional views of water levels measured in C-
designated wells C-23 — C-22, C-29 — C-28 are included as Figures 26, 36, 4B and 56, and cross -sectional views of
C-33-C-32 and monitor wells MWI-4 — MWI-6 are depicted in Figures 2C, 3C, 4C and 5C. The history of water
levels for piezometers PI-2, PI-11, PO-12 and PO-236 is graphically shown in Figure 6. The historical water level
data from the oldest C-designated wells on site (C-22, C-23, C-28, C-29, C-32 and C-33) are graphically shown in
Figure 7. Historical water level elevation data for MWI-3, MWI-4 and MWI-6 are depicted in Figure 8. Please note
that Figures 6, 7 and 8 represent groundwater data collected on a monthly basis representing month to month
changes in groundwater elevation, not quarterly changes.
February 19, 2019

Groundwater Monitoring Report Permit No. WQ0012404
January 1, 2018 thru December 31, 2018
CF Nitrogen, Inc.
Cofield, North Carolina
EPA ID No. NCD065288847
S&ME Project No. 1040-98-044R
Precipitation events were recorded by an on -site rain gauge. The amounts of precipitation for CY 2018 are
presented in Table 2. Monthly recorded rainfall on -site ranged from 1.30 inches in January 2018 to a season high
of 7.20 inches in July 2018. It is noted that Hurricane Florence made landfall in North Carolina on September 14,
2019, and Hurricane Michael passed through North Carolina October 11-12, 2019. During these high wind and
rain events, the on -site rain gauge was blown off the stand, therefore the full amount of rain during these events
was not captured. Weather reports estimated rainfall during Hurricane Florence at up to 30 inches along the North
Carolina coast. Rainfall estimated during Hurricane Michael averaged 10 inches. According to precipitation data
from the USA.com website (www.USA.com), the average rainfall amounts for Cofield, North Carolina is presented
in Table 2 and depicted in Figure 9.
The amount of rainfall in 2018 was 4.65 inches greater than the average rainfall for the region. However, the
frequency of rain events hindered land application due to permit conditions III.7.d and III.7.f. The land application
program is focused on reducing the groundwater elevation, weather permitting. Should you have any questions,
please do not hesitate to contact us at [phone].
Sincerely,
S&ME, Inc.
Jo Martin
Project Scientist
[e-mail]
Attachments:
Tables
Table 1: Groundwater Elevation Data
Table 2: Monthly Rainfall 2017 and 2018
Edmund Woloszyn, Jr., REM
Principal Scientist/Project Manager
[e-mail]
Figures
Figure 1:
Site Location Plan
Figure 2:
Groundwater Potentiometric Map for January 2018
Figure 2A:
Cross -sectional View PI-2 — PO-236 & PI-11 — PO-12 for January 2018
Figure 213:
Cross -sectional View C-23 — C-22 & C-29 — C-28 for January 2018
Figure 20
Cross -Sectional View C-33 — C-32 & MWI-4 — MWI-6 for January 2017
Figure 3:
Groundwater Potentiometric Map for April 2018
Figure 3A:
Cross -sectional View PI-2 — PO-236 & PI-11 — PO-12 for April 2018
February 19, 2019 3

Groundwater Monitoring Report Permit No. WQ0012404
January 1, 2018 thru December 31, 2018
CF Nitrogen, Inc.
Cofield, North Carolina
EPA ID No. NCD065288847
S&ME Project No. 1040-98-044R
Figure 36:
Cross -sectional View C-23 — C-22 & C-29 — C-28 for April 2018
Figure 3C:
Cross -Sectional View C-33 — C-32 & MWI-4 — MWI-6 for April 2018
Figure 4:
Groundwater Potentiometric Maps for July 2018
Figure 4A:
Cross -sectional View PI-2 — PO-236 & PI-11 — PO-12 for July 2018
Figure 413:
Cross -sectional View C-23 — C-22 & C-29 — C-28 for July 2018
Figure 4C:
Cross -Sectional View C-33 — C-32 & MWI-4 — MWI-6 for July 2018
Figure 5:
Groundwater Potentiometric Maps for October 2018
Figure 5A:
Cross -sectional View PI-2 — PO-236 & PI-11 — PO-12 for October 2018
Figure 56:
Cross -sectional View C-23 — C-22 & C-29 — C-28 for October 2018
Figure 5C:
Cross -Sectional View C-33 — C-32 & MWI-4 — MWI-6 for October 2018
Figure 6:
Groundwater Elevations for PI-2, PI-11, PO-12, and PO-236
Figure 7:
Groundwater Elevations for C-Designated Wells
Figure 8:
Groundwater Elevations for MWI-3, MWI-4 and MWI-6
Figure 9:
Monthly Rainfall 2018
cc: Mr. John A. Foster, CHMM (CF Nitrogen, Inc.)
Ms. Jeanette Stanley (NCDEQ — Superfund Section)
February 19, 2019 4

Attachments

Attachment I — Tables

TABLE 1
GROUNDWATER ELEVATION DATA
DECEMBER 2017 THROUGH DECEMBER 2018
CF NITROGEN - COFIELD, NORTH CAROLINA
S&ME PROJECT NO. 1040-98-044S
MWI-1 30.47
30.09
32.19
-12.37
31.67
b. -te-of WA
31.29
ervel Measurement
33.27
32.11
0
32.07
000
30.63
012/28/2018
32.39
34.11
31.31
MWI-2
30.46
30.78
31.72
32.04
31.74
31.04
31.12
34.06
32.28
32.26
30.46
32.12
33.42
MWI-3
30.13
30.01
31.51
31.90
31.21
31.01
30.75
32.55
32.15
31.83
30.15
31.49
33.09
MWI-4
30.61
30.55
31.45
31.63
31.73
31.35
31.39
31.55
32.03
31.53
30.27
28.35
32.55
MWO-5
25.32
25.44
25.94
26.38
26.18
26.54
25.92
26.44
26.34
25.96
25.42
25.64
26.40
MWI-6
29.97
30.91
31.79
31.45
31.69
31.01
31.21
34.01
32.13
33.09
30.91
32.61
33.83
MWI-7
28.76
29.12
30.56
30.54
30.02
29.52
29.56
31.62
30.34
31.14
29.00
31.66
32.34
MWO-8
26.15
27.41
26.91
27.31
26.15
27.05
26.13
31.09
26.71
28.71
28.45
29.11
30.21
PI-1
29.49
29.43
31.36
31.21
30.91
30.29
30.23
33.01
31.19
31.53
29.79
31.61
33.59
PI-2
29.60
29.82
30.82
31.12
30.58
30.48
30.10
32.80
30.70
30.74
28.98
31.06
32.92
PO-3
19.81
19.69
19.57
19.87
20.05
20.05
20.05
20.05
20.31
20.25
19.83
19.73
19.73
PI-4
29.83
30.05
31.01
31.31
31.15
30.85
27.87
33.05
31.55
31.41
29.79
32.01
32.85
PI-5
29.85
29.47
31.00
31.05
30.55
30.75
30.27
32.65
30.83
31.13
28.83
31.03
32.83
PO-6
24.48
24.38
24.48
24.96
24.96
25.06
24.82
24.84
24.98
24.88
24.56
24.48
24.80
PI-7
29.98
30.48
31.59
31.72
31.40
30.78
30.82
33.18
32.22
32.02
30.32
31.70
33.10
PI-8
28.26
28.44
29.92
30.12
29.68
29.16
29.08
30.16
29.46
30.58
28.56
30.74
31.88
PI-9
30.31
30.37
31.47
31.73
31.51
30.95
31.01
32.77
32.37
32.37
30.69
31.89
33.01
PI-10
30.54
30.38
31.72
31.98
31.52
31.38
31.36
32.24
32.44
32.40
30.50
31.66
32.76
PI-11
28.21
29.05
30.35
30.37
29.87
29.17
28.99
31.53
29.91
30.59
28.95
30.85
31.89
PO-12
16.22
16.70
16.60
16.82
16.50
16.78
16.52
16.80
16.60
16.38
16.02
16.50
16.52
PI-13R
30.35
31.07
3L91
32.25
30.89
31.35
31.43
33.25
32.93
32.49
31.03
32.23
33.27
PI-14
29.44
30.02
31.48
31.64
30.64
30.24
30.44
32.18
31.44
31.98
30.06
31.82
32.82
PO-15
24.70
24.76
25.66
26.00
26.28
26.00
25.74
25.26
25.66
25.78
25.10
25.24
25.80
PO-16
28.53
30.11
30.43
31.03
31.09
30.31
29.13
30.55
29.59
29.51
29.09
29.83
30.89
PI-17
30.26
32.28
32.60
33.00
32.22
32.00
31.90
35.02
32.66
32.78
30.14
33.00
33.90
PI-18
28.65
29.71
30.79
31.09
30.75
30.99
30.17
32.53
30.79
30.91
28.99
30.09
33.27
PI-19
29.11
28.63
29.65
29.73
29.77
29.67
29.19
31.31
29.83
30.19
28.23
30.69
31.81
PI-20
29.60
29.70
30.80
30.84
30.58
30.80
29.28
32.30
30.70
31.04
28.94
31.36
32.96
PI-21
29.39
29.53
30.55
30.81
30.35
30.79
30.17
32.15
31.15
31.25
28.95
31.15
33.21
PI-22
30.25
30.23
31.41
32.09
31.51
30.85
30.55
32.35
32.15
30.83
30.55
31.45
32.81
PI-23
30.54
30.96
32.54
32.88
32.38
31.96
32.14
34.28
33.06
32.78
31.98
32.33
34.24
PI-24
29.86
30.37
31.09
31.35
31.31
30.97
30.87
31.39
33.23
31.97
30.59
31.45
32.59
PO-25
26.05
26.15
26.67
26.87
26.95
26.83
26.47
27.01
26.87
26.57
26.17
26.51
27.33
PO-26
29.16
30.63
30.41
30.67
30.77
30.33
29.65
30.83
29.83
30.09
29.19
29.51
30.61
C-22
16.11
16.01
15.81
15.77
16.07
15.73
18.53
15.15
15.99
15.85
15.67
1.5.75
15.57
C-23 (Replaced 04/05)
28.76
29.30
30.98
30.68
30.76
30.80
29.48
31.98
30.56
31.34
28.70
31.08
33.00
C-28 (Repaired 08/03)
9.73
9.59
9.69
10.29
10.09
9.89
9.41
9.79
10.09
9.99
8.99
9.87
10.19
C-29
28.01
27.96
28.96
29.18
28.62
28.78
28.12
30.20
28.66
28.96
27.36
29.38
31.14
C-32
10.83
11.29
11.57
11.87
11.93
11.85
11.23
8.57
11.93
11.57
9.71
1.1.05
11.81
C-33
27.82
28.18
29.58
29.12
29.16
29.22
26.44
30.50
29.02
29.90
28.18
29.50
31.42
C-4
29.78
29.54
30.26
31.14
30.16
29.90
30.26
31.92
32.18
31.40
29.76
30.08
32.60
PO-235
16.32
15.93
15.87
16.15
16.31
16.17
16.15
16.11
16.39
16.47
15.91
16.03
16.31
PO-236
12.92
13.42
13.20
13.34
13.62
13.18
13.18
13.20
13.70
13.60
13.44
13.70
13.80
PO-237
29.13
30.31
30.45
30.55
30.45
30.35
29.65
30,71 T77771,29.83
29.51
29.95
30.31

MONTHLY
CF INDUSTRIES - I
S&ME PRC
Recorded2018 2017 Average Rainfall for
Month Rainfall Recorded
at CFI-Ahoskie Site (inches) at CFI-Ahoskie Site (inches) www.usa.com
January 1.30 3.95 3.60
February
3.55
0.65
3.10
March
5.40
5.95
4.10
April
3.90
3.20
3.50
May
6.75
4.55
3.80
June
7.15
4.70
4.10
July
7.20
7.75
4.80
August
3.35
2.55
4.80
September"
2.40
5.60
4.60
October"
2.45
3.85
3.20
November
4.50
2.50
3.10
December
2.70
3.50
3.30
Annual Total:
50.65
48.75
46.00
Monthly Average:
4.22
4.06
3.96
Recorded rainfall at site taken from on -site rain gauge
Data for average monthly rainfall obtained from the USA.com website for Cofield, NC
"Hurricane Florence made landfall in North Carolina on September 14, 2018, Hurricane Michael traveled
through South Carolina and North Carolina October 11-October 12, 2019.
Rain fall estimated for September and October due to gauge failure during hurricanes Florence and Michael

Attachment II — Figures

0 400
PO-235
(15.93)-
16
A pI-1
(29.43)
17
18
19
PO-3
PI-4
1
(19.69)
(30.05)
20
21
22
23
PI-7
24
(30.48)
PO-6
- !1d im
800
T (FEET)
Ll
MWI-2
® (30.78)
r d'
(13.42 p -2
IAPO-236 p�
RW-2
-1 RW-1
PI-5
9)
(29.4
\
jA
RW 3
(30.01)
pi
99
PI-10
(30 37) (30.38)
MWO-5
(25.44)
PO-25 PI-22
(30.23)
0(26.15)
PI-13R
1 27-11AW0-8 (31.07)
(27.41)
28
29
30
PO-237
PO-26
(30.31)
(30.63)
YI
ti
C22
C23 P
(29.30)
ti~
RW-5 Yo
7)
C28 ti
RW-7 (9.59)
RW-6 1
RW 8 -& C29
�W-4 (27.96)
C32
MWI-4
® (11.29) �1 V
(30.45) RW-9
C33 73
(28.18) ® A
n� pI-8 1
A (28.44) y W Q
® MWI-6
(30.91)
!���(30.37)
I-24
PIN
�y
PO-16 - ('32.28)
(30.11)
�j
yb
0
0 O
N
Z
PI;11 PO-12
(29.65) (16.70)
W
E~
p
M
V
w =
O
o
O
MWI-7 d)
®
�'-�
Z
(29.12)
z 0
d8
�,
V w
d.9
0
z
r
1
�
� PO'15
( 0.024 (24.76)
-16
LEGEND
RECOVERY WELL
® MONITOR WELL
SCALE:
PIEZOMETER
1 " = 400'
SLURRY WALL
DATE:
2-12-19
GROUNDWATER CONTOURS
PROJECT NUMBER
(30.09) GROUNDWATER ELEVATION (FEET ABOVE MEAN SEA LEVEL)
1040-98-044S
NOTE:
FIGURE NO.
PIEZOMETERS PI-18 TO PI-21 ARE GROUPED NEAR PI-5, WHICH IS
WITHIN THE RADIUS OF INFLUENCE; WATER LEVELS OF THESE
2
PIEZOMETERS ARE THUS EXCLUDED FROM THIS MAP.

45
PI-2 Pa236
42.60' MSL (T.O.C.)
43.62 MSL (T.O.C.)
40
35
SLURRY
WALL
30
—3Z 29.82 FT. MSL -30' MSL
25
20
15
—Q
13.42 FT. MSL
10
5
0
-5
SECTION PI-2 - PO-236
45
Pi-11
42.5T MSL (T.O.C.)
40
Pa12
39.29 MSL (T.O.C.)
35
SLURRY
WALL
0
—4 29.05 FT. MSL
-30' MSL
25
20
Ll
—Q 16.70 FT. MSL
15
10
5
0
-5
SECTION PI-11- PO-12
NOTE:
GROUNDWATER DATA COLLECTED ON JANUARY 30, 2018
CROSS - SECTIONAL VIEW
- PO-236 & PI-11- PO-12
SCALE:
FIGUJNO.PI-2
1" =DATE:E:2-11-2019
2
(�
CF NITROGEN, INC.
PROJECT NUMBER
1040-98-044S
COFIELD NORTH CAROLINA

N - '
a � �
PO-236-
(13.34 (31121) C22
(15.77)
PO-235 C23
(16.15) (321) } (30.68) p
RW-2
17
T ~`
18 ®MWI.1 RW-1 Pl3 RW-5 ti~
(32.37) N A (31.05)
19 # C28
RW-3 ® (10.29)
RW-6 RW7
PI-4 --22820 P-(31.31) RW8* titi
�RW-4 (91)
(19.87) C32
MWI-4
® (31.63) RW-9 (11.87) 13
21 C33
(29.12)0 yA
PI-8 W
A (30.12) Q
22 MWI-3 6 �
® (31.90) ti O Z O
FF o
z N ZU
23 MWI-2 (30I.37) A (6.82) I'- M l7
® (32.04) 1j O t~ Z
MWI-7
24 ®(30.54) ?8 W LLci
PI-7 I~ U uw
(31.72) MWI-6 19 u-
PO-6 ® (31.45) 2 OU
►z
1�
PI-10
(31.73) PI-9
(31.98) P1-14 1y
(31.64) ?
MWO-5 Po-15% S
(26.38) 3ti ®(31.14) (26.00) 36.
P1-24
(31.35)
PO-25 PI-22
(26.87) (32.09)
2� PI-13R LEGEND
(32.25)
Mwo-s PI-23 } RECOVERY WELL
(2.7 341) (32.88)
2929 30 PO-237 ® MONITOR WELL SCALE:
PO-26 (30.55) �y
A PIEZOMETER 1 " = 400'
(30.67)
DATE:
Po;16 P�=17 SLURRY WALL
(363')�,p33.00) �� 2-12-19
4 GROUNDWATER CONTOURS PROJECT NUMBER
3ti I W (3237) GROUNDWATER ELEVATION (FEET ABOVE MEAN SEA LEVEL) 1040-98-WS
It
NOTE: FIGURE NO.
0 400 800 PIEZOMETERS PI-18 TO PI-21 ARE GROUPED NEAR PI-S, WHICH IS
(FEET) WITHIN THE RADIUS OF INFLUENCE; WATER LEVELS OF THESE 3
PIEZOMETERS ARE THUS EXCLUDED FROM THIS MAP.

r v
N --
r
Ln
PO-236�
(13.20) PI-2
(32.80)
PO-235 P1_C23 2215) tia
(16.11) (33'1.Ol) (31.98)
RW-2 ti
17 y�
18 MWI-1 RW-1 pI-5 RW-5
® (33.27) A (32.65)
19 '�'
h � C28
RW-3 Y RW-7 (9.79)
-4 °j
RW-6
(33.05) RW_ 20 - PI g C29
P0;3 RW-4 (30.20) Q
(20.15) "
MWI-4 V
21
�ti ® (31.55) RW-9 C32 1�
C33 (8.57) y'y
(30.50)
PI-8 y yA �"
A (30.16) Z
22 ® MWI-3 �� 0
(32.55) 16 0-4 00
F- Z
o U
PO 12 W N Lu
Z
23 MWI=2 (31.53) A (16.80) 0O
(34.06)
3q MWI-7 j� a Z if
24 ® (31.62) 18 W i-- LL
PI-7 U w_
(33.18) MWI-6 ? Q LL
H P0�6 (34.01) 9 O
- (24.84) �O z
E
O
PI_9 . P1-10 13 L7
o (32.24)
(32.77) PI-24 PO-15
y� ® (32.18) - (2`26) -"?
MWO-5 �C4 �S
o(26.44) (31.92)
PI-24
A (31.39) 16
PO-2 5 (32.35)32/
(27.01) / PI-13R LEGEND
°` 1 MWO.8 (33.25)
o (31.09) PI-23 33} RECOVERY WELL
e ryo� o' - (34.28)` 1� ® MONITOR WELL SCALE:
�' n^y PO-237 34
p0-26 (30.71) PIEZOMETER 1 " = 400 '
c (30.83) 3g p1a F-1 SLURRY WALL DATE:
.��(35.02) 2-12-19
PO-16 �/ GROUNDWATER CONTOURS PROJECT NUMBER
.5o (305)
S
(3327) GROUNDWATER ELEVATION (FEET ABOVE MEAN SEA LEVEL) 1040-98-0445
NOTE: FIGURE NO.
0 400 800 PIEZOMETERS PI-18 TO PI-21 ARE GROUPED NEAR PI-5, WHICH IS
o (FEET) WITHIN THE RADIUS OF INFLUENCE; WATER LEVELS OF THESE 4
PIEZOMETERS ARE THUS EXCLUDED FROM THIS MAP.

PO-235
(15.93����
16
A
(29.79)
17
18
19
PI-4
20
—
Pa.
(29.79)
3
(19.13)
21
22
23
24
PI-7
(30.32)
- MAPO-C 6 G\
0 400 800
(FEET)
a "a
N
PO-236 PI-2 ~
(13.44) (28 98)' (1C2 ,yh
C23
(28.70)
RW-2
ti~
,YO
MWI-1 1
® (30.63) 28.83) RW-5
w RW-3 R6 R7 ® 8? 9)
RW-8 C29
RW- (27.36)
MWI-4 1 mod' ♦ ��
®(30.27) `RW:9 C33 93 1), �1
(28.18) ® ,�
PI-8 y�
(28.56) �A
MWI-2
® (30.46)
It, PI-9
(30.69)
MWO-5
(25.42)
MWI-3
® (30.15)
PI-22
(30.55)
130R- PLO PO-2
(26.17) 8(
W0;
PI123M(28,45) (3.98)
PO-237
PO-26
'*(29.19)
MWI-6
® (30.91)
PI-10
(30.50)
® C4
S
P1-24
A (30.59)
PI-11 PO-12
(28.95) (16.02)
MWI-7 ?
't8
jy
110
1S
PI-14
(30.06) 2
9
PO-151
(25.10) �S
1-1c
a
V
H
W
Q
Z
0
°O
m
U 0
P-4
E"
O
N
? Q
Z V
wj
[�
O
W
U H-
Oar
it
O
C
Z
Z cs
W
O
LL J
V Lu
°
0
3
U
z
a
0
c�
LEGEND
RECOVERY WELL
1j
SCALE:
® MONITOR WELL
/-"&
AL PIEZOMETER
1 " = 400 '
DATE:
� SLURRY WALL
PV17
2-12-19
PO-16 ('30.14)
GROUNDWATER CONTOURS
(29.09)
PROJECT NUMBER
(30.63) GROUNDWATER ELEVATION (FEET ABOVE MEAN SEA LEVEL)
1040-98-044S
NOTE:
FIGURE NO.
PIEZOMETERS PI-18 TO PI-21 ARE GROUPED NEAR PI-5, WHICH IS
WITHIN THE RADIUS OF INFLUENCE; WATER LEVELS OF THESE
5
PIEZOMETERS ARE THUS EXCLUDED FROM THIS MAP.

40.00
35.00
�. 30.00
4-0 25.00
O
. rl
M
y 20.00
rl
w
.1•r
3
15.00
0
0
10.00
5.00
0.00 _
00 00 O� O� O O ^ N N M M �Y v1 �O l� t� 00 00 as O� O O N N M M kn W) "D 0
O O O O O O O O O O O O O O O O O O ^ ^ ^ ^ ^ ^ ^ ^ ^
FIGURE 6
Groundwater Elevations for PI-2, PI-11, PO-12, PO-236
CF Nitrogen, Inc.
Cofield, North Carolina
S&ME Project No.1040-98-044S
PI-11
APO-12
PI-2
PO-236
Time

tM
I
1 11
35.00
30.00
25.00
20.00
15.00
11t
11'
0.00 _ _
00 00 � C" O O N N M M �/) �O l� [� 00 00 O O O O ^ N N M M d "t V) � \O r- r-
C� 1� O O O O O O O O O O O O O O O O O O O O -1 ^ 7 7
� M M
FIGURE 7
Groundwater Elevations for C- Designated Wells
CF Nitrogen, Inc.
Cofield, North Carolina
S&ME Project No.1040-98-044S
C-22
C-23
C-28
C-29
C-32
C-33
Time

'ii
FIGURE 8
Groundwater Elevations for MWI-3, MWI-4 & MWI-6
CF Nitrogen, Inc.
Cofield, North Carolina
S&ME Project No.1040-98-044S
M
35
M
25
20
15
10
5
0 00 00 O O ^ ^ N N M M d v W) "O 1.0 [- l- 00 N N M M IZT kn [�
O O O ^ ^ - I ^ ^ ^
Time
MWI-3
MWI-4
- MWI-6

s
Figure 9
Monthly Rainfall
' I
S CF Nitrogen, Inc.
Cofield, NC
S&ME Project 1040-98-O44S
9.00
8.00
7.00
6.00
t 5.00
U
f0
3.95
4.00
Cr-3.6
3.55
3.1
3.00
2.00
1.3
1.6
1.00
'
0.00
Jan Feb
5.95
Mar
6.75
7.75
7.15 7.21
5.60
70 114*114.814.1 1 1
3.90 3.8
3.5
2 3.35
- - .5
Apr May Jun Jul Aug Sep
■ 2018 Rainfall ■ 2017 Rainfall Average Monthly Rain for Cofield, NC
4.50
3.85
3.50
3.2 3.3
3.1
2.
2.4
Oct Nov Dec