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HomeMy WebLinkAboutWQ0009949_Monitoring (Report)_20160121 2015 ANNUAL DOWNGRADIENT AREA1611 MONITORING REPORT Site: edit GEIGY CHEMICAL CORPORATION CERCLA SITEal. ABERDEEN, MOORE COUNTY, NORTH CAROLINA COMMITTEE CORRESPONDENCE Submitted To: MR. JON BORNHOLMPir USEPA REGION IV 61 FORSYTH STREET, SW MAIL CODE: 9T25 ATLANTA, GA 30303-8960 all Prepared By: 110in _. ENVIROTRAC LTD. 7343 WEST FRIENDLY AVENUE, SUITE J GREENSBORO, NC 27410 (336) 763-6025 RECEWEDINCDEQIDWR JAN 2 ' 2016 JANUARY 2016 Water(��E.':'' �;`;;onal Operatiar n A Full Service Environmental Consulting and Contracting Firm L 1 Eii46IFac Environmental Services January 19, 2016 Mr. Jon Bornholm Remedial Project Manager USEPA Region IV 61 Forsyth Street, SW Mail Code: 9T25 Atlanta, GA 30303-8960 RE: October 2015 Sampling Event Downgradient Area Monitoring Report Geigy Chemical Corporation CERCLA Site Aberdeen, North Carolina Dear Mr. Bornholm: On behalf of Olin Corporation and Syngenta Crop Protection (the Companies), the purpose of this letter is to transmit analytical results for the October 2015 monitoring event associated with the Geigy Site downgradient area monitored natural attenuation remedy. The monitoring event includes the collection of groundwater and surface water samples. Samples for the annual monitoring event were collected October 20 through 22, 2015, and were submitted to TestAmerica Laboratories, Inc. in Savannah, Georgia for analysis. Laboratory analytical results are summarized in Tables 1, 2, 3, and 4 (Attachment 1). Sample locations are shown in Figures 1, 2, 3 and 4 (Attachment 2). Copies of the analytical reports are included in Attachment 3. To facilitate your review, findings of the October 2015 downgradient area monitoring event are summarized below. Upper Black Creek Aquifer Groundwater Samples BHC isomers were detected at concentrations exceeding the performance standards in four of the seven Upper Black Creek monitoring wells (MW-11 D, MW-18D, MW-20D, MW-22D, MW-23D, MW-26D, and MW-30). Monitoring wells MW-11 D and MW-20D could not be sampled due to insufficient water in the wells. Alpha-BHC exceeded the performance standard in MW- 18D and MW-30D. Beta-BHC exceeded the performance standard in MW-18D, MW-22D, and MW-30D. Delta-BHC exceeded the performance standard in MW-18D, MW-22D and MW-30D. The BHC isomer concentrations in the five monitoring wells sampled remain within the range of historical results. Upper Black Creek Aquifer October 2015 groundwater data are summarized in Table 1 and in Figure 2. Historical sample results are summarized in Table 4. Lower Black Creek Aquifer Groundwater Samples No pesticides were detected at levels exceeding the performance standards in groundwater samples collected from monitoring wells MW-32L, MW-36L, MW-38L, MW-39L, or MW-40L located adjacent to Aberdeen Creek, Ray's Mill Creek, and McFarland Branch. No pesticides 7434 W. Friendly Ave., Suite J, Greensboro, NC 27410 I Office: (336) 763-6025 I Fax: (336) 763-6035 www.envirotrac.com • E. r151 QE Environmental Services were detected in the groundwater sample collected from monitoring well MW-36L, which serves as a sentinel monitoring point for Town Well No. 2. BHC isomer concentrations generally have decreasing trends. The BHC isomer concentrations detected in the monitoring wells remain within the range of historical concentrations. Lower Black Creek Aquifer October 2015 groundwater data are summarized in Table 2 and in Figure 3. Historical sample results are summarized in Table 4. Surface Water Samples Estimated concentrations of BHC isomers below the laboratory reporting limit were detected in the McFarland's Branch surface water samples SW-01, SW-02 and SW-03. The concentrations of BHC isomers in McFarland's Branch continue to be consistent with historical levels. Estimated concentrations of alpha-BHC isomers below the laboratory reporting limit were detected in the Aberdeen Creek surface water sample SW-07. Estimated concentrations of beta-BHC isomers below the laboratory reporting limit were detected in the Aberdeen Creek surface water samples SW-05, SW-07 and SW-08. The concentrations of BHC isomers in Aberdeen Creek continue to be consistent with historical levels. No pesticides were detected in the surface water sample collected from Ray's Mill Creek (SW- 09). Surface water October 2015 data are summarized in Table 3 and in Figure 4. Should you have questions concerning the monitoring results, please contact Chris Hay at (336)763-6025. Sincerely, ENVIROTRAC LTD. Annamarie Blauser Senior Scientist . Christopher IN. Hay, E.I. Principal Enclosure Cc: Doug Rumford, NCDEQ Superfund Section, w/enc. Michael Rogers, NCDEQ DWR, w/enc. Garland Hilliard, Olin Corporation, w/enc. George Crouse, Syngenta, w/enc. 7434 W. Friendly Ave., Suite J, Greensboro, NC 27410 I Office: (336) 763-6025 I Fax: (336) 763-6035 www.envirotrac.com ATTACHMENT 1 ANALYTICAL DATA SUMMARY TABLES OCTOBER 2015 MONITORING EVENT TABLE 1: UPPER BLACK CREEK AQUIFER GROUNDWATER MONITORING SUMMARY PARAMETER ANALYTICAL DATA PERFORMANCE SAMPLE LOCATION MW-11 D MW-18D MW-20D MW-22D MW-23D MW-26D MW-30D STANDARD DATE COLLECTED 10/21/15 10/21/15 10/21/15 10/20/15 10/22/15 10/21/15 10/21/15 Aldrin NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U 0.05 alpha-BHC NS 0.098 NS 0.028 J 0.021 J 0.049 U 0.081 0.05 beta-BHC NS 1.5 NS 0.18 0.022 J 0.049 U 1.7 0.05 delta-BHC NS 0.39 NS 0.11 0.048 U 0.049 U 0.27 0.05 gamma-BHC (Lindane) NS 0.1 NS 0.022 J 0.015 J 0.019 J 0.067 0.2 alpha-Chlordane NS 0.05 U NS 0.051 U 0.048 U 0.016 J 0.05 U NE gamma-Chlordane NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE Dieldrin NS 0.26 NS 0.051 U 0.048 U 0.049 U 0.17 0.1 4,4'-DDD NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE 4,4'-DDE NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE 4,4'-DDT NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE Endosulfan I NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE Endosulfan II NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE Endosulfan sulfate NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.017 Jp NE Endrin NS 0.05 U NS 0.051 U 0.048 U * 0.049 U 0.05 U NE Endrin aldehyde NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE Endrin ketone NS 0.16 NS 0.051 U 0.048 U 0.049 U 0.17 0.1 Heptachlor NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE Heptachlor epoxide NS 0.05 U NS 0.051 U 0.048 U 0.016 J 0.019 Jp NE Methoxychlor NS 0.05 U NS 0.051 U 0.048 U 0.049 U 0.05 U NE Toxaphene NS 4.5 J NS 5.1 U 4.8 U 4.9 U 2.6 J 1 Trichloroethene NS 1.9 NS NA NA NA 1.0 U ** NOTES Results are presented in micrograms per liter NE = No standard established J = Estimated value less than the reporting limit but greater than the method detection limit NA= Not analyzed for this compound *= LCS and LCSD exceeds the control limits NS = Not sampled **=Trichloroethene is not a COC for the Geigy site. U = Indicates the analyte was not detected p= The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported. Bold = Concentration exceeds performance standard or method detection limits if no standard is established MW-11 D and MW-20D were not sampled due to insufficient amount of water in the wells. 11.990010.00 ©2016 EnviroTrac January 2016 TABLE 2: LOWER BLACK CREEK AQUIFER GROUNDWATER MONITORING SUMMARY PARAMETER ANALYTICAL DATA PERFORMANCE SAMPLE LOCATION MW-22L MW-25L MW-27L MW-31L MW-32L MW-36L MW-37L MW-38L MW-39L MW-40L PZ-2 PZ-3 PZ-5 STANDARD DATE COLLECTED 10/20/15 10/21/15 10/21/15 _ 10/21/15 10/22/15 10/21/15 10/21/15 10/22/15 10/21/15 10/22/15 10/21/15 10/21/15 10/21/15 Aldrin 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U 0.05 alpha-BHC 0.17 0.7 0.92 0.4 0.053 U 0.049 U 0.88 0.053 U _ 0.051 U 0.048 U 0.31 0.25 1.0 0.05 beta-BHC 0.71 0.56 2.0 0.62 0.053 U 0.049 U 0.68 0.053 U 0.051 U 0.043 J 0.17 0.088 0.31 0.05 delta-BHC 0.44 0.97 2.1 0.86 0.053 U 0.049 U 1.5 0.053 U 0.051 U 0.048 U 0.23 0.15 0.48 0.05 gamma-BHC (Lindane) 0.12 0.1 0.17 0.084 0.053 U 0.049 U 0.18 0.053 U 0.051 U 0.048 U 0.2 0.17 0.36 0.2 alpha-Chlordane 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE gamma-Chlordane 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Dieldrin 0.071 0.015 J _ 0.1 0.028 J _ 0.053 U 0.049 U 0.018 J 0.053 U 0.051 U 0.048 U 0.011 J 0.052 U 0.051 U 0.1 4,4'-DDD 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE 4,4'-DDE 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE 4,4'-DDT 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Endosulfan I 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Endosulfan II 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Endosulfan sulfate 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U _ 0.052 U 0.051 U NE Endrin 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U* 0.049 U 0.049 U 0.053 U* 0.051 U 0.048 U* 0.053 U 0.052 U 0.051 U* NE Endrin aldehyde 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Endrin ketone 0.072 0.027 J 0.18 0.049 0.053 U 0.049 U 0.046 J 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.031 J 0.1 Heptachlor 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Heptachlor epoxide 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Methoxychlor 0.049 U 0.05 U 0.05 U 0.048 U 0.053 U 0.049 U 0.049 U 0.053 U 0.051 U 0.048 U 0.053 U 0.052 U 0.051 U NE Toxaphene 1.9 J 5.0 U 0.89 Jp 0.22 Jp _ 5.3 U 4.9 U 0.75 J 5.3 U 5.1 U 4.8 U 5.3 U _ 5.2 U 5.1 U 1 NOTES Results are presented in micrograms per liter J = Estimated value less than the reporting limit but greater than the method detection limit *= LCS and LCSD exceeds the control limits may be flagged with a D. NE = No standard established NA= Not analyzed for this compound U = Indicates the analyte was not detected p= The %RPD between the primary and confirmation column/detector is>40%. The lower value has been reported. Bold = Concentration exceeds performance standard or method detection limits if no standard is established 11.990010.00 ©2016 EnviroTrac January 2016 TABLE 3: SURFACE WATER ANALYTICAL SUMMARY PARAMETER ANALYTICAL DATA McFARLANDS BRANCH ABERDEEN CREEK RAY'S MILL SAMPLE LOCATION CREEK SW-01 SW-02 SW-03 SW-04 SW-05 SW-06 SW-07 SW-08 SW-11-2 SW-09 DATE COLLECTED 10/21/15 10/21/15 10/21/15 10/21/15 10/21/15 10/21/15 10/21/15 10/21/15 10/21/15 10/21/15 Aldrin 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U alpha-BHC 0.05 U 0.05 U 0.01 J 0.05 U 0.051 U 0.051 U 0.0086 J 0.049 U 0.051 U 0.049 U beta-BHC 0.018 J 0.017 J 0.029 J 0.05 U 0.013 Jp 0.051 U 0.016 Jp 0.013 Jp 0.051 U 0.049 U delta-BHC 0.05 U 0.05 U 0.029 J 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U gamma-BHC (Lindane) 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U alpha-Chlordane 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U gamma-Chlordane 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Dieldrin 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U 4,4'-DDD 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U 4,4'-DDE 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U 4,4'-DDT 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Endosulfan I 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Endosulfan II 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Endosulfan sulfate 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Endrin 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Endrin aldehyde 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Endrin ketone 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Heptachlor 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Heptachlor epoxide 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Methoxychlor 0.05 U 0.05 U 0.05 U 0.05 U 0.051 U 0.051 U 0.054 U 0.049 U 0.051 U 0.049 U Toxaphene 5.0 U 5.0 U 5.0 U 5.0 U 5.1 U 5.1 U 5.4 U 4.9 U 5.1 U 4.9 U Total Suspended Solids' 2.0 U 2.0 U 2.0 U 8.0 14.0 2.2 U 2.0 U 2.9 2.1 U 1.7 NOTES: Results are presented in micrograms per liter unless otherwise noted J = Estimated value less than the reporting limit but greater than the method detection limit U = Indicates the analyte was not detected p=The%RPD between the primary and confirmation column/detector is>40%. The lower value has been reported. =Total suspended solids are measured as milligrams per liter 11.990010.00 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS C = V a c 0 @ 0 U 0 I = -o co 2c 0 us I- c c as r o 0 o r c m i m m ccu E a a 0 w o m s o i, -c a) PARAMETER o m a0 E a QTL) 0 y a " m cco .x x a 2 o co Q a m N E cu rn L it v v -°a "0 w c aai N N . x o To _o CO t U v v c c Lis -a c 2 2 a) I- o rn c. W Ta W Lu us H PERFORMANCE STANDARD 0.05 0.05 0.05 0.05 I 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** MW-4S 04/21/98 2.5U 2.5U,O 16 2.5U 2.5U 2.5U 2.5U _ 2.OJ _ 5.OU 1 5.OU 5.OU 2.5U 5.OU 5.OU 5.OU 5.OU 5.OU I 2.5U 2.5U 25U 50U NA 1998 3rd Quarter not sampled 10/29/98 0.55 U 0.55 0,R 4.2 2.8 0.55 U 1 0.55 U ] 0.55 U _ 0.27 J 1.1 U I 1.1 U 1.1 U 0.55 U 1.1 U 1.1 U I 1.1 U 1.1 U 1.1 U 1 0.55 U 0.55 U I 5.5 U 11 U NA 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 10/14/99 0.05 U 1 0.05 U I 0.36 0.23 0.05 U _ 0.05 U 1 0.05 U 1 0.027 J 1 0.1 U 0.1 U 0.1 U 0.05 U I 0.1 U _ 0.1 U I 0.1 U I 0.1 U 0.031 J 0.05 U 0.05 U 0.5 U ) 2.0 U NA 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 2000 3rd Quarter not Sampled 10/13/00 0.25 U,Q 0.25 U 1.5 0.66 0.25 U 0.25 U 0.25 U 0.5 U 0.5 U I 0.5 U 0.5 U 0.25 U 0.5 U 1 0.5 U 1 0.5 U 0.5 U 0.5 U 1 0.25 U 1 0.25 U 2.5 U 1.0 U NA 2001 Semi-Annual not Sampled 10/10/01 0.05U 0.05U 0.013J 0.05U 0.05U 0.05U _ 0.05U 0.1 U 0.1 U 0.1 U 1 0.1 U 0.05U 0.1 U 0.1 U 1 0.1 U 0.1 U 0.1 U 1 0.05U 0.05U 0.5U 2.OU I NA 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 2007 Annual Sampling Event not Sampled 10/24/08 0.19 U 1 0.19 U 1 3.9 D* 10.079 J,D,P_ 0.044 J,D 0.19 U 0.19 U I 0.57 D 0.39 U 1 0.39 U 0.39 U 0.19 U _ 0.39 U 0.39 U 1 0.39 U 0.39 U 0.46 D 0.19 U 0.073 J,D,P 1.9 U 19 U I NA 2009 Annual Sampling Event not Sampled 10/12/10 0.047 U 0.047 U 0.9 1.3 0.047 U 0.047 U 0.047 U 0.099 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U* 0.094 U 0.094 U 0.053 J 0.047 U 0.047 U 0.094 U 4.7 U 1.0 U 10/11/11 0.050 U 0.013 J 1.1 D 0.21 D 0.018 Jp 0.050 U 0.050 U 0.13 0.099 U 0.067 Jp 0.099 U 0.050 U 0.099 U , 0.099 U 0.099 U, 0.099 U 0.086 J _0.050 U 0.050 U 0.099 U_ 5.0 U 1.0 U 10/23/12 0.23 U 0.23 U 1.2 D 0.29 D 0.23 U 0.23 U 0.23 U 0.18 JD 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 0.23 U 23 U 1.0 U 10/16/13 0.05 U 0.041 J 6.7 Ep _ 1.3 Ep 0.067 p 0.05 U 0.05 U 1.6 E 0.05 U 0.05 U 0.05 U 0.05 U _ 0.05 U 0.05 U 0.05 U 0.05 U 1.1 E 0.05 U 0.27 0.05 U 7.4 p NA 10/21/14 0.048 U 0.048 U 0.5 0.19 , 0.048 U 0.048 U 0.016 J 0.13 0.048 U 0.048 U 0.011 J 0.048 U 0.048 U 0.0092 J 0.048 U 0.048 U 0.049 0.048 U 0.016 Jp 0.048 U 1.2 J NA 10/20/15 0.049 U 0.049 U 0.75 0.31 0.049 U 0.049 U _ 0.01 Jp 0.25 0.049 U 0.049 U 0.049 U _ 0.049 U 0.049 U 0.049 U 0.049 U, 0.049 U 0.073 0.049 U 0.026 Jp 0.049 U 2.7 J NA MW-5S 04/21/98 0.5U 0.5U 2.50 0.59 0.05J 0.5U 0.5U 0.44J 1.OU I 1.OU 1.OU 0.5U 1.OU y 1.OU 1 1.OU 1.OU 0.27J 0.5U 0.07J 1 5.OU 15 NA 1998 3rd Quarter not sampled 10/29/98 0.59U 0.31J,O,R 8.6 2.0 0.25J 0.08J I 0.59U 0.79J 1.2U 1 1.2U 1.2U 1 0.59U 1.2U 1.2U I 1.2U 1 1.2U 1.2U 0.59U 0.18J 5.9U 12 NA 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 10/14/99 0.25U,Q 0.25U 1.4 _ 0.7 I 0.25U 1 0.25U 0.25U 0.5U 0.5U 1 0.5U 0.5U 0.25U 0.5U 1 0.5U 1 0.5U 0.5U 0.12J 1 0.25U 0.25U 1 2.5U 10U 1 NA 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 2000 3rd Quarter not Sampled 10/13/00 1 0.25U,Q 0.042J 3.2 I 1.4 0.25U _ 0.25U 0.25U 1 0.35J I 0.5U 0.5U 0.5U 1 0.25U 0.5U 0.5U 0.5U 1 0.5U 0.29J 1 0.25U 1 0.25U _ 2.5U 10U 1 NA - 2001 Semi-Annual not Sampled 10/10/01 j 0.25U 0.25U 1.3 0.17J 0.25U 0.25 U 0.25U 0.1J 0.5U 1 0.5U L 0.5U 0.25 U 1 0.5U 0.5U 1 0.5U 0.5U 0.13J 0.25U 0.25U I 2.5U 10U NA 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 11.990010.00 Page 1 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) 0 c - = a) a) c = 2 2 m m c c a W I- cc m w a> c a)- o c `o 0 r c s • m m , O O a1 .c o a a wN L L U a) PARAMETER -o ris m m 6 �o s E -a -o 9 9 9 > > ti . - m .X x n o Q a a) E . s m U 0 sF �f v o c W c 73 a) a m m xo t a a) a) m N W W W W c I I 2 H .` H PERFORMANCE - 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 **STANDARD 2007 Annual Sampling Event not Sampled 10/24/08 I 0.47 U 0.47 U 3.5 D 1 0.18 J,D,P 0.47 U I 0.47 U 0.47 U 0.51 J,D 0.94 U 10.94 U 0.94 U I 0.47 U I 0.94 U I 0.94 U 10.94 U 10.94 U 1 0.36 J,D 0.47 U I 0.47 U 4.7 U 47 U NA 2009 Annual Sampling Event not Sampled _ 10/12/10 0.049 U 0.030 Jp _ 2.4 Ep 0.65 p 0.048 Jp 0.049 U 0.049 U 0.73 p 0.098 U 0.098 U . 0.098 U 0.049 U 0.098 U 0.098 U* 0.098 U 0.098 U 0.37 p 0.049 U 0.049 U 0.098 U 4.9 U 1.0 U 10/11/11 0.053 U 0.053 U , 0.93 D 0.10 0.053 U _ 0.053 U 0.053 U 0.13 0.11 U 0.11 U 0.11 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.10 J 0.053 U 0.053 U 0.11 U 1.7 J 1.0 U 10/23/12 0.22 U 0.22 U 1.0 D 0.22 U 0.22 U 0.22 U 0.22 U 0.33 D 0.22 U 0.061 JD 0.22 U 0.22 U 0.22 U 0.22 U 0.22 U 0.22 U 0.099 JD 0.22 U 0.22 U 0.22 U 22 U 1.0 U 10/15/13 0.048 U 0.046 J 2.2 Ep 0.17 0.041 Jp 0.048 U 0.048 U 0.95 Ep 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.33 p 0.048 U 0.048 U _0.048 U 18 p NA 10/21/14 0.17 0.035 J 3.7 _ 0.5 0.035 Jp _ 0.049 U 0.049 U 1.5 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.4 p 0.049 U 0.049 U 0.049 U 1.7 NA 10/20/15 0.051 U 0.018 J 2.8 0.28 0.028 Jp 0.051 U _ 0.051 U 0.54 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.3 0.051 U 0.051 U 0.051 U 9.6 NA MW-6S 04/21/98 1 0.5 U 2.9 6.6 6.0 2.4 0.5 U _ 0.5 U 0.58 J 1.0 U I 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U I 1.0 U 1.0 U 0.62 J _ 0.5 U 0.5 U 5.0 U 20 NA 1998 3rd Quarter not sampled 10/29/98 I 0.56 U 1.8 O,R 7.1 4.6 1.1 0.56 U I 0.56 U 0.25 J 1 1.1 U 1 1.1 U 1.1 U I 0.56 U I 1.1 U 1.1 U 1.1 U I 1.1 U 1.1 U 0.56 U _ 0.12 J 5.6 U I 11 I NA 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 10/14/99 I 1.0 U,Q 3.9 6.9 1 18 2.0 1 1.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U I 2.0 U 2.0 U 2.0 U I 1.0 U 1.0 U 10U 40 U I NA 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 2000 3rd Quarter not Sampled 10/13/00 0.05 U 0.05 U 0.05 U I 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U I 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U I 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U I 2.O U NA 2001 Semi-Annual not Sampled 10/11/01 1.2 U 3.5 10 1 15 0.91 J 1.2 U 1.2 U 2.5 U 2.5 U I 2.5 U _ 2.5 U _ 1.2 U 2.5 U 2.5 U I 2.5 U 2.5 U 2.5 U 1.2 U 1.2 U 12 U 50 U NA 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 2007 Annual Sampling Event not Sampled 10/23/08 0.49 U 0.23 J,D 4.4 D 1.6 D 0.091 J,D 0.49 U 0.49 U _ 0.10 J,D 0.97 U 10.97 U 0.97 U I 0.49 U 0.97 U I 0.97 U 10.97 U 10.97 U __ 0.97 U 0.49 U 0.49 U 4.9 U 49 U I NA 2009 Annual Sampling Event not Sampled 10/12/10 0.047 U 0.14 p 5.9 Ep 1.8 Ep 0.047 U 0.047 U 0.047 U 0.35 p 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U* 0.094 U 0.094 U 0.40 p 0.047 U 0.047 U 0.094 U 4.7 U 1.0 U 10/11/11 0.049 U , 0.098 5.9 D 1.1 D 0.054 p 0.049 U 0.049 U 0.33 0.099 U 0.099 U 0.099 U 0.049 U 0.099 U 0.099 U 0.099 U 0.099 U 0.32 0.049 U 0.049 U 0.099 U 6.9 1.0 U _ 10/23/12 0.55U 0.55U 5.1 D 1.8D 0.065JD 0.55U 0.55U 0.57D 0.55U 0.55U 0.55U 0.55U 0.55U 0.55U 0.55U 0.55U 0.28JD 0.55U 0.55U 0.55U 55U 1.OU 10/15/13 0.048 U 0.1 3.1 Ep 1.4 Ep 0.048 U _ 0.048 U 0.048 U 0.36 p 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.34 0.048 U 0.048 U 0.048 U 5.2 p NA _ 10/21/14 0.0099 Jp 0.043 J 1.9 0.62 0.05 U 0.05 U 0.035 J 0.12 p 0.05 U 0.05 U . 0.05 U . 0.05 U 0.05 U 0.026 J 0.05 U 0.05 U 0.11 0.05 U 0.05 U 0.05 U 2.1 Jp NA 10/20/15 0.05 U 0.11 7.3 1.7 0.3 0.05 U 0.05 U 0.43 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.39 0.05 U 0.05 U 0.05 U 7.6 p NA MW-10S 04/21/98 0.5 U 0.39 J 7.0 1.6 1.34 J I 0.5 U 0.5 U 0.9 J 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.8 0.5 U 0.5 U 5.0 U 8.4 J 5.0 U 1998 3rd Quarter not sampled 10/29/98 0.56 U 0.085 J,O,R 4.5 1 0.41 J 0.11 J I 0.56 U 0.56 U 0.27 J 1.1 U 1 1.1 U 1.1 U 0.56 U ] 1.1 U 1.1 U 1 1.1 U _ 1.1 U 1 1.1 U 0.56 IJI 0.56 U 5.6 U 11 U 1.0 U 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 10/14/99 0.25U,Q 0.045J 1 2.3 0.21J 0.064J I 0.25U 0.25U _ 0.17J 0.5U I 0.5U 0.5U 0.25U 0.5U 0.5U I 0.5U _ 0.5U 0.40J I 0.25 U 0.25U 2.5U 10U 10U 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 11.990010.00 Page 2 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS 0 as a) a) c 0 U U I ", a a) 0 W H c c m s o 0 0 c a) c m I I m e o �0 m •c a a o w ;a w a) c a) : s -p o a) PARAMETER m m as r E Q Q 9 ° v�i Y @ X X a Q a `JS/ 0 m t v v v a o ° v3, c ° c n ' °n. ° f6 2 �o fa -a as t U v v v c c w c I I ° I° o m a w •c m L L H PERFORMANCE STANDARD 0.05 0.05 0.05 0.05 ' 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** 2000 3rd Quarter not Sampled 10/13/00 10.25U,Q I 0.25U 108 1 0.077J 0.25U I 0.25 U I 0.25U 0.21J 0.5U 0.5U 0.5U 0.25U I 0.5U 0.5U 1 0.5U I 0.5U I 0.24J 0.25U I 0.25U I 2.5U I 10U I 1.OU 2001 Semi-Annual not Sampled 10/11/01 I 0.25U I 0.17JD 1.0 0.65 0.058J I 0.25 U 0.25U I 0.5U 0.5U I 0.5U 0.5U 0.25 U 0.5U I 0.5U I 0.5U 0.5U 0.5U 0.25U I 0.25U 2.5U I 10U 1.OU 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 2007 Annual Sampling Event not Sampled 10/21/08 I 0.19U 0.19U I 1.7D 0.19U 0.19U I 0.19U 0.19U I 0.26J,D 0.38U 10.38U 0.38U 0.19U 0.38U I 0.38U 10.38U 0.38U 0.36J,D 0.19U 0.19U I 1.9U 19U 1.OU 2009 Annual Sampling Event not Sampled 10/12/10 0.49 U 0.49 U 5.8 D 0.49 U 0.49 U ' 0.49 U . 0.49 U 0.51 0.97 U 0.97 U 0.97U 0.49 U 0.97 U 0.97 U 0.97 U 0.97 U 0.98 D 0.49 U 0.49 U 0.97 U 49 U NA 10/11/11 0.051 U 0.013J 1.6D 0.047J 0.0098Jp 0.51 U 0.51 U 0.17 0.10U 0.10U 0.10U 0.051 U 0.10U 0.10U 0.10U 0.10U 0.28 0.051 U 0.051 U 0.10U 1.6Jp 1.OU 10/23/12 0.054 U 0.054 U 0.38 0.012 J 0.054 U 0.054 U 0.054 U 0.061 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.056 0.054 U 0.054 U _ 0.054 U 5.4 U 1.0 U 10/15/13 0.048 U 0.013 J 0.88 E* 0.026 Jp 0.021 J , 0.048 U 0.048 U 0.067 0.048 U 0.048 U 0.048 U 0.012 J 0.048 U 0.048 U 0.048 U 0.048 U 0.16 0.048 U 0.014 Jp 0.048 U 0.53 Jp 1.0 U 10/21/14 0.048 U 0.0056 J 0.56 0.02 J 0.009 Jp 0.048 U 0.0067 J 0.074 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.098 0.048 U 0.0083 Jp 0.048 U 0.47 Jp 1.0 U 10/20/15 0.048 U 0.048 U 0.88 0.02 J 0.015 J 0.048 U 0.048 U 0.12 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.17 0.048 U 0.012 Jp 0.048 U 0.97 J 1.0 U MW-16S 04/21/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U I 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U I 0.5 U 1.0 U 5.0 U 1998 3rd Quarter not sampled 10/29/98 I 0.05U 0.05U,R 0.05U 0.05U 0.05U I 0.05U 0.05U 0.1 U I 0.1 U I 0.1 U I 0.1 U 0.05U 0.1 U I 0.1 U I 0.1 U I 0.1 U 0.1 U 10.05U 0.05U 10.52U I 1.OU 1.OU 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 10/14/99 I 0.05 U 0.05 U 0.05 U I 0.05 U 0.05 U 0.05 U 0.05 U I 0.1 U 0.1 U 0.1 U 0.1 U I 0.05 U I 0.1 U 0.1 U I 0.1 U 0.1 U 0.1 U 0.05 U I 0.05 U I 0.5 U 2.O U 1.O U 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled - 2000 3rd Quarter not Sampled 10/13/00 0.05U I 0.05U I 0.05U 0.05U I 0.05U I 0.05U 0.05U 0.1 U I 0.1 U I 0.1 U 0.1 U 0.05U 0.1 U 0.1 U I 0.1 U 0.1 U 0.1 U 0.05U 0.05U 0.5U I 2.OU 5.OU 2001 Semi-Annual not Sampled 10/11/01 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.1 U 0.1 U I 0.1 U I 0.1 U 0.05U 0.1 U 0.1 U I 0.1 U I 0.1 U 0.1 U 10.05U I 0.05U 10.52U 2.OU I 1.OU 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 2007 Annual Sampling Event not Sampled 10/21/08 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 10.047 U 0.047 U 0.047 U 0.047 U 10.047 U 0.047 U 10.047 U 10.047 U 10.047 U 10.047 U 0.047 U 0.047 U 0.047 U I 0.047 U 0.047 U I 4.7 U I 1.0 U 2009 Annual Sampling Event not Sampled 10/11/10 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U 0.095 U 0.095 U* 0.095 U 0.095 U 0.095 U 0.048 U 0.048 U 0.095 U 4.8 U 1.0 U 10/11/11 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.10 U 0.10 U 0.10 U _ 0.10 U 0.050 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.050 U 0.050 U 0.10 U 5.O U 1.O U 10/23/12 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 u 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 4.7 U 1.0 U 10/15/13 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 5.2 U 1.0 U 10/21/14 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U 1.0 U 10/20/15 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 5.4 U 1.0 U 11.990010.00 Page 3 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS m 0 m _ = v a) 8 c = U 0 = N a) c W I- c c a3 r p O o t a) c m I = m = ° m � . 0 o 0 w � � C a) . U U V > s a) PARAMETER v 00 m as L E Q Q m uI) ,- 45 Y 0 0 - > n 2 s@ Q Q Ev U ch as O -p N W .0 •` n fl Q t X o CO 0 v j W LL c w I I 2 ~PERFORMANCE STANDARD 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** MW-17S 04/21/98 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.1 U 0.1 U I 0.1 U 0.1 U 0.05U 0.1 U 0.1 U I 0.1 U 0.1 U 0.1 U 0.05U _ 0.05 U 0.5U 1.OU 5.OU 1998 3rd Quarter not sampled 10/29/98 0.05 U 0.05 U,R 0.05 U I 0.05 U 0.05 U 0.05 U _ 0.05 U 0.1 U I 0.1 U I 0.1 U 0.1 U 0.05 U 0.1 U I 0.1 U I. 0.1 U 0.1 U I 0.1 U 0.05 U I 0.05 U 0.5 U I 1.O U _ 1.O U 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 10/14/99 0.05 U 0.05 U 0.05 U I 0.05 U I 0.05 U 1 0.05 U 0.05 U _ 0.1 U 0.1 U 0.1 U I 0.1 U 0.05 U I 0.1 U 0.1 U I 0.1 U I 0.1 U 0.1 U _ 0.05 U 0.05 U _ 0.5 U I 2.O U I 1.O U 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 2000 3rd Quarter not Sampled 10/13/00 0.05U _ 0.05U 0.05U 0.05U I 0.05U 1 0.05U _ 0.05U 0.1 U I 0.1 U 1 0.1 U 0.1 U 0.05U 0.1 U 0.1 U I 0.1 U 0.1 U 0.1 U 10.05U 0.05 U 0.5U I 2.OU I 1.OU 2001 Semi-Annual not Sampled 10/11/01 I 0.05 U 0.05 U 0.05 U 0.05 U I 0.05 U I 0.05 U 0.05 U 0.1 U I 0.1 U 1 0.1 U 0.1 U I 0.05 U 0.1 U I 0.1 U 0.1 U I 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U I 2.O U 1.O U 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 2007 Annual Sampling Event not Sampled 10/21/08 0.049 U 0.049 U 0.049 U _ 0.049 U I 0.049 U 1 0.049 U 0.049 U I 0.013 J 0.097 U 0.097 U I 0.097 U 0.049 U 0.097 U 0.097 U 10.097 U 10.097 U_ 0.097 U 0.049 U I 0.049 U 0.49 U 4.9 U 1.0 U 2009 Annual Sampling Event not Sampled 10/11/10 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.10U 0.10U 0.10U 0.10U 0.05U 0.10U 0.10U* 0.10U 0.10U 0.10U 0.05U 0.05U 0.10U 5.OU 1.OU 10/11/11 0.048 U 0.048 U 0.048 U 0.048 U , 0.048 U _ 0.048 U , 0.048 U 0.096 U 0.096 U 0.096 U_ 0.096 U , 0.048 U 0.096 U 0.096 U 0.096 U 0.096 U 0.096 U 0.048 U 0.048 U _0.096 U 4.8 U 1.0 U 10/23/12 0.054 U 0.054 U 0.054 U . 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U` 0.054 U 0.054 U 5.4 U 1.0 U 10/15/13 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U 1.0 U 10/21/14 0.048 U 0.048 U 0.014 J 0.048 U 0.048 U 0.048 U 0.048 U 0.0081 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.01 J 0.048 U 0.048 U 0.048 U 4.8 U 1.0 U 10/20/15 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U_ 0.053 U 0.053 U 5.3 U 1.0 U MW-18S 04/21/98 0.05U 0.05U 0.05U 0.05U I 0.05U 0.05U 0.05U 0.1 U 0.1 U I 0.1 U I 0.1 U 0.05U 0.1 U 0.1 U I. 0.1 U 0.1 U 0.1 U 0.05U _ 0.05U 0.5U 1.OU 5.OU 1998 3rd Quarter not sampled 10/29/98 I 0.05 U 0.05 U,R 0.05 U 0.05 U 0.05 U I 0.05 U 0.05 U _ 0.1 U 0.1 U 1 0.1 U 0.1 U 0.05 U I 0.1 U _ 0.1 U I 0.1 U I 0.1 U I 0.1 U 10.05 U 0.05 U 0.5 U 1 1.O U 1.O U 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 10/14/99 0.05U 0.05U 0.05U 0.05U 0.05U I 0.05U 0.05U I 0.1 U 0.1 U I 0.1 U I 0.1 U I 0.05U 0.1 U 0.1 U I 0.1 U 0.1 U 0.1 U 0.05U 0.05U I 0.5U I 2.OU 1.OU 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 2000 3rd Quarter not Sampled 10/13/00 0.05U 0.018J 0.05U 0.05U 0.24 0.05U I 0.05U I 0.1 U I 0.1 U 0.1 U 0.1 U 0.05U 0.1 U I 0.1 U I 0.1 U 0.1 U _ 0.1 U 0.05U I_ 0.05U I 0.5U I 2.OU 10U 2001 Semi Annual not Sampled 10/11/01 0.05U 0.05U 0.05U 0.05U I 0.05U _ 0.05U _I 0.05U 0.1 U I 0.1 U 0.1 U I 0.1 U 1 0.05U 0.1 U 0.1 U I 0.1 U 0.1 U 0.1 U 10.05U 0.05U 0.5U 2.OU 1.OU 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 11.990010.00 Page 4 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) _ _ a) a> U as - c >, c O a) c 0 0 0I = a> a c c 0 W I- @ C c� C O o 0 0 t c _c C I m m c O a3 'C o 0 0 w- _ .0.. .0 y L L 'O U a) PARAMETER `o m m E o p u°i ° v, w -o - m m 'x x c. 2 Q a m E v ca co v a° -°° v°i w S CI) a°i CI) L X ° m _o a as -C U v v c c W -o c 2 2 N 0 o rn o w Lu w w M ~ H PERFORMANCE STANDARD 0.05 0.05 I 0.05 0.05 I 0.2 NE , NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** 2007 Annual Sampling Event not Sampled 10/21/08 I 0.047 U I 0.047 U I 0.032 J,p I 0.047 U I 0.047 U 10.047 U ( 0.047 U I 0.21 J I 0.094 U 10.094 U I 0.094 U 0.047 U 0.094 U 10.094 U 10.094 U 0.094 U I 0.026 J 10.047 U I 0.047 U 10.47 U I 4.7 U I 1.0 U 2009 Annual Sampling Event not Sampled 10/12/10 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U _ 0.05U 0.10U 0.10U 0.10U 0.10U 0.05U 0.10U _ 0.10U* 0.10U 0.10U 0.10U 0.05U 0.05U _ 0.10U 5.OU 1.OU 10/11/11 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U _ 0.049 U 0.049 U_ 0.098 U 0.098 U 0.098 U 0.098 U 0.049 U 0.098 U 0.098 U 0.098 U_0.098 U 0.098 U 0.049 U 0.049 U 0.098 U 4.9 U 1.0 U 10/23/12 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U _ 0.052 U_ 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 5.2 U 1.0 U 10/15/13 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U _ 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 5.2 U 1.0 U 10/21/14 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U*_0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U 1.0 U 10/20/15 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U _ 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U 1.0 U MW-11 D 04/21/98 I 0.14 0.52 I 0.1 0.045 J 0.05 U I 0.05 U I 0.05 U I 0.053 J 0.1 U 0.1 U 0.1 U I 0.05 U I 0.1 U 0.1 U I 0.1 U 0.1 U I 0.056 J 0.05 U I 0.05 U I 0.5 U 1.0 U NA 1998 3rd Quarter not sampled 10/27/98 0.53 U 1.6 O,R 4.9 0.98 0.52 J 0.53 U 0.53 U 0.21 J 1.1 U 1.1 U 1.1 U 0.53 U 1.1 U 1.1 U 1.1 U 1.1 U 1.1 U 0.53 U 0.53 U 5.3 U 11 U NA 04/13/99 0.5 U 1.8 Q 6.9 1.3 0.33 Q 0.5 U 0.5 U 0.28 J 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.43 J 0.5 U 0.5 U 5 U 20 U NA 08/13/99 1.OU 3.3 16.0 2.6 _ 0.39J 1.0U 1.0U 0.78J 0.24J 2.OU 2.OU 1.OU 2.OU 2.OU 2.OU 2.OU 1.1J 1.OU 1.OU _ 10U 40U NA 10/14/99 1.OU 2.5 13.0 1.9 0.26J 1.OU 1.OU 0.54J 2.OU 2.OU 2.OU 1.OU 2.OU 2.OU _ 2.OU 2.OU 0.93J 1.OU 1.OU 10U 40U NA 02/04/00 1.OU 2.1 14.0 _ 2 0.31 1.OU 1.OU 0.65J 2.OU 2.OU 2.OU 1.OU 2.OU 2.OU 2.OU 2.OU 1.2J 1.OU 1.OU 10U 40U NA 04/12/00 1.OU 2.4 13.0 _ 2.3 0.91 1.OU 1.OU 0.73 2.OU 2.0U 2.0U 1.OU 2.OU 2.OU 2.OU 2.OU 0.93J 1.OU 1.OU 10U _ 40U NA 07/24/00 0.5 U,Q 2 8.1 1.6 0.86 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.63 J 0.5 U 0.5 U 5.0 U 20 U NA 10/15/00 0.5 U,Q 1.1 6.5 1.1 0.39 J 0.5 U 0.5 U 0.39 J 1.0 U 1.0 U 1.0 U 0.5U 1.0 U 1.0 U 1.0 U 1.0 U 0.42 J 0.5 U 0.5 U 5.0 U 20 U NA 01/12/01 0.5U 0.72Q 5.5Q 0.85Q 0.33JQ 0.5U 0.5U 0.26J,Q 1.OU 1.OU 1.OU 0.5U _ 1.OU 1.OU 1.OU 1.OU 0.36J 0.5U 0.5U 5.OU 20U NA 2001 4th Quarter not Sampled 10/23/06 I 0.05 U I 0.37 I 2.6 0.51 I 0.16 0.1 U 0.1 U 0.05 U I 0.1 U I 0.1 U I 0.1 U 0.05 U I 0.1 U I 0.1 U 0.05 U 1 0.1 U NA 10.05 U I 0.05 U I 0.5 U I 1.0 U NA 2007 Annual Sampling Event not Sampled 2008 Annual Sampling Event not Sampled 2008 Annual Sampling Event not Sampled 2009 Annual Sampling Event not Sampled 2010 Annual Sampling Event not Sampled 2011 Annual Sampling Event not Sampled 2012 Annual Sampling Event not Sampled 2013 Annual Sampling Event not Sampled 2014 Annual Sampling Event not Sampled 2015 Annual Sampling Event not Sampled MW-16D 04/21/98 0.05U I 0.05U 0.05U I 0.05U I 0.05U I 0.05U 0.05U I 0.1 U 0.1 U 0.1 U 0.1 U 10.05U I 0.1 U 0.1 U 0.1 U I 0.1 U _ 0.1 U 0.05U I 0.05U 1 0.5U I 1.OU 2900 1998 3rd Quarter not sampled 10/29/98 I 0.05U 10.05U,R 0.05U I 0.05U I 0.05U I 0.05U I 0.05U I 0.1 U 0.1 U 0.1 U I 0.1 U 0.05U I 0.1 U 0.1 U 1 0.1 U I 0.1 U I 0.1 U 10.05U 0.05U I 0.5U I 1.OU I 270 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 1999 4th Quarter not Sampled _ 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 2000 3rd Quarter not Sampled 10/13/00 I 0.05U 10.05U,R I 0.05U I 0.05U I 0.05U I 0.05U I 0.05U 0.1 U 0.1 U I 0.1 U I 0.1 U 10.05U I 0.1 U I 0.1 U _ 0.1 U I 0.1 U 0.1 U 10.05U 0.05U I 0.5U I 2.OU I 260E 2001 Semi-Annual not Sampled 10/10/01 I 0.05U I 0.05U I 0.05U I 0.05U I 0.05U I 0.05U 0.05U I 0.1 U I 0.1 U I 0.1 U 0.1 U 10.05U I 0.1 U I 0.1 U I 0.1 U I 0.1 U I 0.1 U 10.05U I 0.05U I 0.5U I 2.OU I 190Q 11.990010.00 Page 5 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) a) m 0 c - = -o a) c U U N c c T C o a) a) U 2f� y i s 0 W F- c _c s o 0 o t c pp 2 m j@ o N c 0 0 0 w w. w c o N U U �, = ) PARAMETER a CO@ con -0 9 9 9 > > U) 4- a 'e co X X 0_ 2 Q a N V N t v O -0 0 W .0 •C Q Q o. t X o V co = �U v v v c c aj a c 2 = 0 0 o c=i 0 0) o. W W c w g F- •c N W H PERFORMANCE- 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** STANDARD1 i 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 2007 Annual Sampling Event not Sampled 10/21/08 I 0.019 U I 0.16 J,D 1.O D 10.057 J,D,P I 0.14 J,D I 0.19 U I 0.19 U 1 0.093 J,D I 0.39 U 10.19 U I 0.39 U I 0.17 U I 0.39 U I 0.39 U 10.39 U 10.39 U 10.17 J,D 10.19 U I 0.19 U I 1.9 U I 19 U 9.4 2009 Annual Sampling Event not Sampled 10/12/10 NS NS NS NS NS NS NS NS NS NS , NS NS , NS NS NS NS NS NS NS NS NS 55 10/11/11 NA NA NA NA NA NA NA NA NA NA NA NA NA _ NA NA NA NA NA NA NA NA 99 10/23/12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 100 10/16/13 NA NA r NA NA NA NA NA NA NA NA NA NA NA NA NA NA _ NA NA NA NA NA 62 10/22/14 NA NA NA NA NA NA NA NA NA NA _ NA NA NA _ NA NA NA NA NA NA NA NA 57 10/20/15 NA NA NA NA NA NA NA NA NA NA NA y NA NA NA _ NA NA NA NA NA NA NA 56 MW-17D 04/21/98 I 0.05U 0.05U 0.05U I 0.05U I 0.05U 0.05U 0.05U I 0.1 U I 0.1 U 0.1 U 0.1 U 0.05U I 0.1 U 0.1 U I 0.1 U 0.1 U I 0.1 U 0.05U I 0.05U I 0.5U I 1.OU I 3200 1998 3rd Quarter not sampled 10/29/98 I 0.05U I 0.05U,R 0.05U I 0.05U I 0.05U 0.05U 0.05U 0.1 U I 0.1 U I 0.1 U I 0.1 U 10.05U I 0.1 U I 0.1 U 1 0.1 U 0.1 U I 0.1 U 10.05U I 0.05U 0.5U 1.OU 350 1999 1st Quarter not Sampled 1999 2nd Quarter not Sampled 1999 3rd Quarter not Sampled 1999 4th Quarter not Sampled 2000 1st Quarter not Sampled 2000 2nd Quarter not Sampled 2000 3rd Quarter not Sampled 10/13/00 I 0.05 U I 0.05 U,R I 0.05 U 0.05 U I 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U I 0.1 U 0.05 U I 0.1 U I 0.1 U I 0.1 U I 0.1 U I 0.1 U 10.05 U I 0.05 U I 0.5 U 2.O U I 290 Q 2001 Semi-Annual not Sampled 10/10/01 I 0.05U I 0.05U I 0.05U 0.05U I 0.05U 0.05U I 0.05U 0.1 U I 0.1 U I 0.1 U 0.1 U 10.05U I 0.1 U I 0.1 U I 0.1 U I 0.1 U I 0.1 U 10.05U I 0.05U I 0.5U I 2.OU I NA 2002 Semi&Annual Sampling Event not Sampled 2003 Annual Sampling Event not Sampled 2004 Annual Sampling Event not Sampled 2005 Annual Sampling Event not Sampled 2006 Annual Sampling Event not Sampled 2007 Annual Sampling Event not Sampled 10/21/08 I NA I NA NA I NA I NA I NA I NA I NA I NA I NA I NA _ NA I NA I NA I NA I NA I NA I NA I NA I NA I NA I 250 2009 Annual Sampling Event not Sampled 10/14/10 NS NS NS NS NS NS NS NS _ NS NS NS NS NS NS NS NS NS NS NS _ NS NS 280 10/11/11 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 190 10/23/12 NA NA NA NA NA NA NA NA NA , NA NA NA NA NA NA NA NA NA NA NA NA 150 10/16/13 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 80 10/22/14 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA _ NA NA 190 10/20/15 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 190 MW-18D 04/21/98 I 0.5 U ( 1.7 6.5 I 1.6 I 1.1 I 0.5 U 1 0.5 U I 0.66 J 1.0 U I 1.0 U 1.0 U I 0.5U l 1.0 U I 1.0 U I 1.0 U L 'Lou 1.1 I 0.5 I 0.08 J I 5.0 U I 10 U 1 6.2 1998 3rd Quarter not sampled 10/29/98 I 1.0 U I 1.6 0 I 8.2 1 1.9 I 1.0 I 1.0 U I 1.0 U I 0.5 J I 2.0 U L 2.0 U 2.0 U I_ 1.0 U I 2.0 U I 2.0 U I 2.0 U 2.0 U 2.0 U 1.0 U I 1.0 U I 10 U I 20 U I 4.2 1999 1st Quarter not Sampled 11.990010.00 Page 6 of 18 ©2016 EnviroTrac January 2016 • TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) _ m m U c = v a) c U V U = N c o w 1-- c m s o 0 o s c s co c m I m m e o (6 .c o o 0 w .0 .` 00 .0 E -0 o a PARAMETER a @ CO cis r o Q Q y N a @ " .X X a 2 ca Q a a� m E U f° s CD p v v v_ o -oa cn ti c •� n a s z X 0 Ja -a co s U 1 v c c w a c = 2 N F-- o a) co w w c w g H PERFORMANCE 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** STANDARD 04/15/99 0.5Q 1.0 4.9 0.78 0.7 0.5U 0.5U 0.29J 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 0.57J 0.5U 0.5U 5U 20U NA 08/13/99 0.25U 1.2 3.8 0.77 0.94 0.25U 0.25U 0.23J 0.049J 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.37J 0.25U 0.25U 2.5U 10U NA 10/14/99 0.25U 1.0 3.0 0.64 0.84 0.25U 0.25U 0.16J 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.35J 0.25U 0.25U 2.5U 10U 20 02/04/00 0.25U 1.2 3.0 0.68 1.0 0.25U 0.25U 0.17J 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.37J 0.25U 0.25U 2.5U 10U NA 04/12/00 0.25U,Q 1.0 2.5 0.56 0.92 0.25U 0.25U 0.17J 0.5U 0.5U _ 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.35J 0.25U 0.25U 2.5U 10U NA 07/24/00 0.25 U,Q 0.97 2.7 0.81 0.86 0.25U 0.25U _ 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.31 J 0.25 U 0.25 U 2.5 U 10 U NA 10/15/00 0.25U,Q 0.81 2.6 0.64 0.7 0.5U _ 0.5U 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 0.26J 0.5U 0.5U 5U 20U 29Q 01/12/01 0.25 U 0.76 2.5 0.63 0.71 0.25 U 0.25 U 0.12 J 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.226 J 0.25 U 0.25 U 2.5 U 10 U NA 10/10/01 0.05 U 0.43 0.7 0.17 0.4 0.05 U 0.05 U 0.058 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.072 J 0.05 U 0.05 U 0.5 U 2 U 46 Q 10/21/08 0.19 U 0.016 J,D 1.O D 0.057 J,D,P 0.14 J,D _ 0.19 U 0.19 U 0.093 J,D 0.39 U 0.39 U 0.39 U 0.19 U 0.39 U 0.39 U 0.39 U 0.39 U 0.17 J,D 0.19 U 0.19 U 1.9 U 19 U 20 10/20/09 0.05 U 0.27 1.3 E 0.27 0.22 0.05 U 0.05 U 0.12 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.18 0.05 U 0.05 U 0.1 U 5 U 18 10/12/10 0.049 U 0.3 2.1 E 0.47 0.27 0.049 U 0.049 U 0.18 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U* 0.097 U 0.097 U 0.26 0.049 U 0.049 U 0.097 U 4.9 U 26 10/11/11 0.048 U 0.28 1.1 D 0.24 0.24 0.048 U 0.048 U 0.090 J 0.096 U 0.096 U_ 0.096 U 0.048 U 0.096 U 0.096 U 0.096 U 0.096 U 0.17 0.048 U 0.048 U 0.096 U 1.2 Jp 24 1 10/23/12 0.049 U 0.18 0.51 0.12 0.16 0.049 U 0.049 U 0.053 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.072 0.049 U 0.049 U 0.049 U 4.9 U 42 10/16/13 0.048 U 0.19 1.7 E* 0.55 0.21 0.048 U 0.048 U 0.15 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.13 0.048 U 0.048 U 0.048 U 1.5 Jp 23 10/21/14 0.011 Jp 0.093 0.64 0.14 0.048 U 0.025 Jp 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.034 J 0.048 U 0.048 U 0.16 0.048 U 0.048 U 0.048 U 3.9 Jp 5.9 10/21/15 0.05 U 0.098 1.5 0.39 0.1 0.05 U 0.05 U _ 0.26 0.05 U _ 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.16 0.05 U 0.05 U 0.05 U 4.5 J 1.9 MW-20D 05/05/98 0.25 U 0.710 0.46 0.9 0.77 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 5U NA 07/23/98 0.05 U 0.61 0.35 0.8 0.66 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U _ 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1 U NA 10/27/98 0.535 U 0.56 0,R 0.4 J 0.71 0.61 0.53 U 0.53 U 1.1 U 1.1 U 1.1 U 1.1 U 0.53 U 1.1 U 1.1 U 1.1 U 1.1 U 1.1 U 0.53 U 0.53 U 5.3 U 11 NA 01/13/99 0.05 U 0.6 0.36 0.77 0.63 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 04/13/99 0.2U 0.61 Q 0.41 0.82 0.63 0.2U 0.2U 0.4U 0.4U 0.4U 0.4U 0.2U 0.4U 0.4U 0.4U 0.4U 0.4U 0.2U 0.2U 2U 8U NA 08/10/99 0.2 U 0.66 0.48 0.81 0.68 0.2 U 0.2 U 0.4 U 0.4 U 0.4 U 0.4 U 0.2 U 0.4 U 0.4 U 0.4 U 0.4 U 0.4 U 0.2 U 0.2 U 2U 8U NA 10/13/99 0.05 U 0.51 0.37 0.72 0.51 0.0088 J 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 02/03/00 0.1 U 0.71 0.52 0.93 0.68 0.1 U 0.1 U 0.2 U 0.2 U 0.2 U 0.2 U 0.1 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.1 U 0.1 U 1U 4U NA 04/11/00 0.25 U 0.81 0.67 1.1 0.8 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 07/23/00 0.25 Q 0.69 0.62 0.92 0.67 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 10/11/00 0.25Q 0.8 0.75 1.0 0.75 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 01/10/01 0.25U 0.73Q 0.75Q 0.99Q 0.75Q 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U _ 0.5U 0.5U 0.25U 0.25U 2.5U 11 U NA 10/09/01 0.05 U 0.45 0.41 0.63 0.45 0.05 U 0.05 U 0.1 U _ 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U _ 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 04/09/02 0.05 U 0.36 0.37 0.51 0.35 0.05 U 0.1 G 0.042 J 0.1 U 0.1 U 0.2 G 0.05 U 0.2 G 0.1 U 0.1 U 0.2 G 0.041 J 0.05 U 0.1 G 0.5 U 2 U NA 10/23/02 0.05 U 0.31 0.33 0.45 0.31 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 10/06/03 0.1 U 0.1 0.19 0.18 0.12 0.1 U 0.1 U 0.2 U 0.2 U 0.2 U 0.2 U 0.1 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.1 U 0.1 U 1U 4U NA 10/20/04 0.05 U 0.089 0.11 0.12 0.096 0.05 U 0.05 U 0.011 J 0.1 U 0.1 U 0.012 J 0.05 U 0.1 U 0.1 U 0.1 U 0.0054 J 0.016 J 0.05 U 0.05 U 0.031 J 2 U NA 10/14/05 0.05 U 0.086 0.095 0.12 0.075 0.05 U 0.05 U 0.0081 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 J 0.1 J 0.05 U 0.0071 J 0.5 U 2 U NA - 10/23/06 0.05 U 0.076 0.14 0.15 0.074 0.05 U 0.05 U 0.0094 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 10/16/07 0.052 U 0.081 _ 0.15 0.17 0.078 0.052 U 0.052 U 0.0064 J 0.1 U 0.1 U 0.1 U 0.052 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.052 U 0.052 U 0.52 U 2.1 U NA 10/14/08 0.047 U 0.043 J,PG 0.072 PG 0.11 0.047 0.047 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.047 U 0.47 U 4.7 U NA 10/20/09 0.05 U 0.047 J 0.13 0.12 0.047 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5 U NA 10/13/10 0.05 U 0.045 J 0.14 p 0.12 0.045 J 0.05 U 0.05 U 0.10 U 0.10 U 0.10 U 0.10 U 0.05 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.05 U 0.05 U 0.10 U 5.0 U NA 2011 Annual Sampling Event not Sampled 2012 Annual Sampling Event not Sampled 2013 Annual Sampling Event not Sampled 2014 Annual Sampling Event not Sampled 2015 Annual Sampling Event not Sampled 11.990010.00 Page 7 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS c = a) 0 U - a a) C m = = m N C W H N C w L O o N L O PARAMETER � m co m cis a s a To Y o m X X La o Q Q Ev U coE s o v v_ O o -co o w c a na s co o o .0 a co a cm 0 Nr v v W W Lu c w i i o m W it PERFORMANCE 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 **STANDARD MW-22D 04/21/98 0.5 U 1.7 6.5 1.6 1.1 0.5 U 0.5 U 0.66 J 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.1 0.5 U 0.08 J 5.0 U 10 U 6.2 05/05/98 0.05 U 0.59 0.43 0.64 0.56 0.05 U 0.05 U 0.021 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.024 J 0.05 U 0.0081 J 0.5 U 1.0 NA 07/23/98 0.05 U 0.43 _ 0.33 0.56 0.41 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1 U NA 10/27/98 0.26 U 0.49 0.4 0.63 0.46 0.26 U 0.26 U 0.51 U , 0.51 U _ 0.51 U 0.51 U 0.26 U 0.51 U 0.51 U 0.51 U 0.51 U 0.51 U 0.26 U 0.26 U 2.6 U 5.1 U 4.2 01/13/99 0.25 O,U 0.75 0.57 0.93 0.71 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 04/13/99 0.2 U 0.59 Q 0.45 0.75 0.55 0.2 U 0.2 U 0.4 U 0.4 U 0.4 U 0.4 U 0.2 U 0.4 U 0.4 U 0.4 U 0.4 U 0.4 U 0.2 U 0.2 U 2 U 8 U 4.2 08/12/99 0.05 U 0.38 0.33 0.53 _ 0.34 0.05 U 0.05 U 0.1 U 0.013 J 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 10/14/99 0.05 U 0.41 0.35 0.61 0.35 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 02/03/00 0.05 U 0.43 0.42 0.66 0.37 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.023 J 0.05 U 0.05 U 0.5 U 2 U NA 04/12/00 0.05 U 0.39 0.39 0.58 0.31 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 07/21/00 0.056 V 0.36 0.36 0.57 _ 0.29 0.056 U 0.056 U 0.11 U 0.11 U 0.11 U 0.11 U 0.056 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.056 U 0.056 U 0.56 U 2.2 U NA 10/11/00 0.05 U 0.43 0.45 0.69 0.35 0.05 U 0.05 U 0.035 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.03 J 0.05 U 0.05 U 0.5 U 2 U NA 01/10/01 0.1 U 0.48Q 0.61Q 0.85Q 0.43Q 0.1 U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1U 4U NA 10/09/01 0.05 U 0.44 0.61 0.78 0.37 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U_ 0.05 U 0.5 U 2 U NA 04/09/02 0.1 G 0.36 0.65 0.72 0.32 0.05 U 0.1 G 0.059 J 0.1 U 0.2 G 0.2 G 0.05 U 0.2 G 0.1 U 0.1 U 0.2 G 0.1 U 0.05 U 0.1 G 0.5 U 2 U NA 10/23/02 0.05 U 0.26 0.5 0.5 _ 0.21 0.05 U 0.05 U . 0.022 J 0.1 U _ 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.029 J 0.05 U 0.05 U 0.5 U 2 U NA 10/07/03 0.1 U 0.43 0.89 0.96 0.4 0.1 U 0.1 U 0.044 J 0.2 U 0.2 U 0.2 U 0.1 U 0.2 U 0.2 U 0.2 U 0.2 U 0.089 J 0.1 U 0.1 U 1 U 4 U NA 10/22/04 0.25 U 0.16 J 0.35 0.32 0.16 J 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.057 J 0.25 U 0.25 U 0.11 J 10 U NA 10/11/05 0.05 U 0.066 0.12 0.13 0.065 0.05 U 0.05 U 0.0083 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U _ 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 10/23/06 0.05 U 0.045 J 0.091 0.082 0.041 J 0.05 U 0.05 U 0.0065 J,PG 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U _ 0.049 J,PG 0.5 U 2 U NA 10/16/07 0.048 U 0.038 J 0.11 0.088 0.033 J 0.048 U 0.048 U 0.096 U 0.096 U 0.096 U 0.096 U 0.048 U 0.096 U 0.096 U 0.096 U 0.096 U 0.096 U 0.048 U 0.048 U 0.48 U 1.9 U NA 10/14/08 0.047 U 0.032 J,PG 0.099 PG 0.091 0.029 J,PG 0.047 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.047 U 0.47 U 4.7 U NA 10/20/09 0.05 U 0.011 J 0.039 J 0.026 J 0.0068 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5 U NA 10/13/10 0.048 U 0.032 J 0.17 p 0.1 _ 0.029 J 0.048 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U_ 0.048 U 0.095 U 4.8 NA 10/12/11 0.053 U 0.032 J 0.14 p 0.11 0.018 Jp 0.053 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U_ 0.053 U 0.11 U 5.3 U NA 10/24/12 0.049 U 0.04 J 0.2 0.081 0.039 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 4.9 U NA 10/16/13 0.048 U 0.03 J 0.17 p 0.097 0.024 J 0.0074 Jp 0.01 J 0.018 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.018 J 0.048 U 0.048 U 0.048 U 4.8 U NA 10/22/14 0.049 U 0.03 J 0.19 0.098 0.023 J 0.049 U 0.049 U 0.015 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U* 0.049 U 0.018 J 0.049 U 0.049 U 0.049 U 4.9 U NA 10/20/15 0.051 U 0.028 J 0.18 0.11 0.022 J 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U _ 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 5.1 U NA MW-23D 04/21/98 0.5 U 1.1 4.8 1.0 0.73 0.5 U 0.5 U 0.51 J 1.0 U " 1.0 U 1.0 U 0.5U 1.0 U 1.0 U 1.0 U 1.0 U 0.81 J 0.5U 0.5U 5 U 10 U NA 05/05/98 0.05 U 0.29 0.16 0.072 0.19 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1.0 U NA 07/22/98 0.05 U _ 0.29 0.17 0.067 0.2 0.05 U . 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1.0 U NA 10/27/98 0.26 U 0.32 0.2 J 0.062 J 0.26 U 0.26 U 0.26 U 0.51 U 0.51 U 0.51 U 0.51 U 0.26 U 0.51 U 0.51 U 0.51 U 0.51 U 0.51 U 0.26 U 0.26 U 2.6 U 5.1 U NA _ 01/13/99 0.05 U 0.32 0.18 0.071 0.21 0.05 U 0.05 U , 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/99 0.05 U 0.33 0.14 0.073 0.21 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.05 U 2.0 U NA 08/13/99 0.05 U 0.37 0.21 0.083 0.24 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/12/99 0.05 U 0.31 0.16 0.066 0.2 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 02/03/00 0.05 U 0.3 0.16 0.062 0.19 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/12/00 0.05 U 0.3 0.16 0.063 0.19 0.05 U 0.05 U 0.1 U 0.1 U . 0.1 U 0.1 U _ 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 07/23/00 0.05 U 0.29 0.16 0.062 0.19 0.05 U . 0.05 U 0.1 U 0.1 U . 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/14/00 0.05 U 0.28 0.15 0.056 0.17 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 01/10/01 0.05 U 0.34 0.2 0.072 0.22 0.05 U 0.05 U 0.1 U 0.1 U , 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U _ 0.05 U 0.05 U 0.5 U 2.0 U NA 10/11/01 0.05U 0.23 0.13 0.037J 0.14 0.05U _ 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.05U 0.5U 2.OU NA 04/09/02 0.05 U 0.21 0.15 0.056 0.13 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U _ 0.05 U 0.1 G 0.5 U 2.0 U NA 10/23/02 0.05 U 0.2 0.14 0.04 J 0.11 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 11.990010.00 Page 8 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a> a) a> 0 c = a o c U c9 - c a c L o U U 2 a c 0 w H @ c co t o 0 0 o t c s c m = = m e o f6 ca •c 0 0 0 9,- w a� c a) o L a U a) a) PARAMETER � @ o U E o y oP w° m m m o o 2 Q a Ti) E v m o) 0 v v v a a -a c 2 2 a) i U rn a w w `c w 2 - PERFORMANCE 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** STANDARD 10/08/03 0.1 U 0.19 0.15 0.042J 0.13 0.1 U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1U 4.OU NA 10/21/04 0.05 U 0.18 0.17 0.041 J 0.12 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.0032 J 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.011 J 2.0 U NA 10/13/05 0.05 U 0.15 0.11 0.041 J 0.098 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.0053 J 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 2006 Annual Sampling Event not Sampled 10/16/07 0.053 U 0.13 0.11 0.03 J 0.084 J 0.053 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U _ 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.053 U 0.53 U 2.1 U NA 10/15/08 0.049 U 0.062 PG 0.041 J,PG 0.017 J 0.054 J 0.049 U 0.049 U _ 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.49 U 4.9 U NA 10/20/09 0.05 U _ 0.0099 J 0.05 U 0.05 U 0.0073 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5.0 U NA 10/14/10 0.05 U 0.062 , 0.039 Jp 0.05 U 0.045 J 0.05 U 0.05 U 0.10 U 0.10 U 0.10 U 0.10 U 0.05 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.05 U 0.05 U 0.10 U 5.0 U NA 10/12/11 0.049 U 0.033 J 0.028 Jp . 0.049 U , 0.020 Jp 0.049 U 0.049 U 0.098 U 0.098 U 0.098 U 0.098 U 0.049 U 0.098 U 0.098 U 0.098 U 0.098 U 0.098 U 0.049 U 0.049 U 0.098 U 4.9 U NA 10/24/12 0.054 U 0.017 J 0.024 J _ 0.054 U 0.013 J 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 0.054 U 5.4 U NA 10/16/13 0.051 U 0.047 J _ 0.037 Jp 0.012 Jp 0.033 J 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 5.1 U NA 10/23/14 0.049 U 0.035 J 0.033 J 0.049 U 0.025 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U* 0.049 U 0.049 U 0.049 U_ 0.049 U 0.049 U 4.9 U NA 10/22/15 0.048 U 0.021 J 0.022 J 0.048 U 0.015 J 0.048 U 0.048 U 0.048 U _ 0.048 U _0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U* 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U NA MW-26D 04/30/98 0.05 U 0.019 J 0.021 J 0.013 J 0.042 J 0.071 J 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U , 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.0076 J 0.5 U 1.0 U NA 07/23/98 0.05 U 0.018 J 0.019 J 0.012 J 0.043 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1.0 U NA 10/27/98 0.054 U 0.016 J,R 0.02 J 0.0089 J 0.041 J 0.054 U 0.054 U 0.11 U 0.11 U 0.11 U 0.11 U 0.054 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.054 U 0.054 U 0.54 U 1.1 U NA 01/19/99 0.05 U 0.025 J 0.025 J 0.015 J 0.052 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/99 0.05 U 0.021 J 0.021 J 0.012 J 0.047 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U , 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 08/12/99 0.055 U 0.022 J 0.024 J 0.013 J 0.049 J 0.055 U 0.055 U 0.11 U 0.11 U 0.11 U 0.11 U 0.055 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.055 U 0.055 U 0.55 U 2.2 U NA 10/13/99 0.05 U 0.021 J 0.024 J 0.012 J 0.05 0.0071 J 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 02/04/00 0.05 U 0.022 J 0.02 J 0.015 J 0.046 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/00 0.05 U 0.033 J 0.029 J 0.019 J 0.057 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 07/22/00 0.05 U 0.05 0.05 0.026 J 0.081 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U _ 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/14/00 0.05 U 0.048 J 0.038 J 0.029 J 0.07 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 01/10/01 0.05 U 0.065 0.066 0.043 J 0.097 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/11/01 0.05 U 0.056 0.082 0.11 0.085 0.05 U 0.05 U 0.1 U 0.1 U _ 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/10/02 0.05 U 0.061 0.074 0.051 0.086 0.19 J 0.015 J 0.031 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.028 J 0.05 U 0.016 J 0.5 U 2.0 U NA 10/24/02 0.05 U 0.069 0.09 0.052 0.1 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/06/03 0.05 U 0.037 J _ 0.086 _ 0.038 J , 0.073 0.05 U 0.05 U 0.0055 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U . 0.1 U 0.1 U 0.05 U 0.015 J 0.5 U 3.0 U NA 10/21/04 0.05 U 0.027 J 0.046 J 0.034 J 0.054 J 0.012 J . 0.05 U 0.0066 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U , 0.01 J 0.05 U 0.015 J _ 0.016 J 2.0 U NA 10/14/05 0.05 U 0.02 J 0.029 J 0.019 J 0.046 J 0.027 J 0.05 U 0.0093 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.01 J 0.05 U 0.015 J 0.009 J 2.0 U NA 10/23/06 0.05 U 0.017 J 0.031 J 0.011 J 0.038 J 0.005 J _ 0.1 U 0.1 U 0.1 U 0.1 U 0.0093 J 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.013 J 0.5 U 2.0 U NA 10/16/07 0.055 U 0.014 J 0.021 J 0.0085 J 0.032 J 0.055 U 0.055 U 0.11 U 0.11 U 0.11 U 0.11 U 0.055 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.055 U 0.025 J 0.55 U 2.2 U NA 10/15/08 0.055 U 1.4 3.0 4.4 0.34 0.047 U 0.047 U 0.098 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.26 0.047 U 0.047 U 0.47 U 4.7 U NA 10/20/09 0.05 U 0.05 U 0.05 U 0.05 U 0.015 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5.0 U NA 10/13/10 0.049 U 0.010 J 0.0089 Jp 0.0084 Jp 0.027 J 0.016 J 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.097 U 4.9 U NA 10/12/11 0.051 U 0.014J 0.013Jp 0.051 U 0.029J . 0.051 U 0.051 U 0.10 U 0.10 U 0.10 U 0.10 U 0.051 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.051 U 0.051 U 0.10 U 5.1 U NA 10/25/12 0.047 U 0.0082 J 0.0093 Jp 0.047 U 0.021 J 0.014 Jp 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 4.7 U NA 10/17/13 0.048 U 0.013 J 0.048 U 0.0088 Jp . 0.022 J 0.021 J 0.0081 Jp 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U , 0.048 U 0.02 J 0.048 U 4.8 U NA 10/23/14 0.049 U 0.0085 J 0.01 J 0.0094 J 0.021 J 0.022 J 0.0092 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U* 0.049 U 0.049 U 0.049 U 0.026 J 0.049 U 4.9 U NA 10/21/15 0.049 U 0.049 U 0.049 U 0.049 U 0.019 J 0.016 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.016 J 0.049 U 4.9 U NA MW-30D 04/21/98 I 0.5 U 1.1 I 4.8 I 1.0 I 0.73 0.5 U I 0.5 U 0.51 J I 1.0 U I 1.0 U 1.0 U I 0.5 U I 1.0 U 1.0 U I 1.0 U I 1.0 U I 0.81 J 0.5 U I 0.5 U I 5.0 U I 10 U NA 1998 3rd Quarter not sampled 10/29/98 I 1.0 U I 2.30 I 9.8 I 2.0 I 0.75 J I 1.0 U I 1.0 U 0.5 J I 2.0 U I 2.0 U I 2.0 U I 1.0 U I 2.0 U I 2.0 U J 2.0 U I 2.0 U I_ 2.0 U I 1.0 U I 1.0 U j 10 U I 20 U I NA 1999 1st Quarter not Sampled 11.990010.00 Page 9 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) 0 0 _ - m c U U m c >, c o 0 0 0 m 'v c c w F- ca c L o 0 0 o o c w c i I o m •c 0 0 0 4- a? c a� a) t s a o a> PARAMETER .c m m m s E v -0 Q 4 4 . `o - '� a x X a o Q L m Ev U EL b v v �t .o o p w 0 a QQ t x o m a -o W _c �U v v v c c -o c 2 2 0 a> I o rn as w w c w g H PERFORMANCE - STANDARD 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** 04/15/99 0.25 U 0.78 2.5 Q _ 0.52 0.42 0.25 U 0.25 U 0.15 J 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.28 J 0.25 U 0.25 U 2.5 U 10 U NA 08/13/99 0.25 U 0.46 _ 4.4 0.61 0.3 0.25U 0.25U 0.29J 0.46J _ 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.61 0.25 U 0.25 U 2.5 U 10 U NA 10/14/99 0.25 U 0.25 2.5 0.3 0.18 JD 0.25 U 0.25 U 0.14 J 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.34 J 0.25 U 0.25 U 2.5 U 10 U NA 02/04/00 0.25 U 0.29 _ 2.2 0.26 0.19 J 0.25 U 0.25 U 0.5 U 0.5 U 0.48 J 0.5 U 0.25 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.25 U 0.25 U 2.5 U 10 U NA 04/12/00 0.25U,Q 0.3 1.9 0.29 0.19J 0.25U 0.25U 0.19J 0.5U _ 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.22J 0.25U 0.25U 2.5U 10U NA 07/24/00 0.25 U,Q 0.67 3.5 0.55 0.35 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.4 J 0.25 U 0.25 U 2.5 U 10 U NA 10/15/00 0.25 U,Q 0.52 _ 2.8 0.31 J 0.27 J 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5U 1.0 U 1.0 U 1.0 U 1.0 U 0.26 J 0.5 U 0.5U 5.0 U 20 U NA 01/12/01 0.25 U 0.31 2.4 0.3 0.19 J 0.25 U 0.25 U 0.13 J 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.26 J 0.25 U 0.25 U 2.5 U 10 U NA 10/12/01 0.25 U 0.47 4.0 0.36 0.26 0.25 U 0.25 U 0.38 J 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.45 J 0.25 U 0.25 U 2.5 U 10 U NA 2002 Second Quarter not Sampled 10/22/02 0.05 U 0.069 0.38 0.13 0.049 0.05 U 0.05 U 0.022 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.036 J 0.05 U 0.05 U 0.5 U 2.0 U NA 10/08/03 0.25 U 0.22 J 1.2 0.41 0.19 J 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U _ 0.5 U 0.5 U 0.5 U 0.15 J 0.25 U 0.25 U 2.5 U 10 U NA 10/18/04 0.25 U 0.28 2.4 0.45 0.17 J 0.25 U 0.25 U 0.21 J 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.042 J 0.5 U 0.24 J 0.25 U 0.25 U 2.5 U 3.1 J NA 10/11/05 0.25 U 0.15 J 2.4 0.23 J - 0.095 J 0.25 U 0.25 U 0.24 J 0.5 U 0.041 J 0.5 U 0.25 U 0.5 U 0.5 U 0.042 J 0.062 J 0.33 J 0.25 U 0.009 J 2.5 U 10 U NA 10/25/06 0.5 U 0.34 J 4.9 0.535 0.2 J , 0.5 U 0.5 U 0.35 J 1 U 1 U 1 U 0.5 U 1 U 1 U 1 U 1 U 0.53 J 0.5U 0.17 J,PG 5U 20U NA 10/16/07 0.096 U 0.28 4.9 0.53 0.13 0.096 U 0.096 U 0.36 0.19 U 0.19 U 0.19 U 0.096 U 0.19 U 0.19 U 0.19 U 0.19 U 0.5 0.096 U 0.0061 J,PG 0.96 U 3.8 U NA 10/16/08 0.047 U 0.16 2.1 0.22 0.095 0.047 U 0.047 U 0.21 0.094 U 0.022 J 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.35 0.047 U 0.047 U 0.47 U 4.7 0.78 10/20/09 0.05 U 0.084 2.8 E 0.3 0.079 0.05 U 0.05 U 0.36 0.1 U 0.1 U 0.077 J 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.31 0.05 U 0.022 J 0.1 U 5 U 28 10/12/10 0.048 U 0.24 JD 5.1 D 0.41 JD 0.20 JD 0.048 U 0.048 U 0.36 JD 0.095 U 0.095 U 0.095 U 0.048 U 0.095 U 0.095 U* 0.095 U 0.095 U 0.62 JD 0.48 U 0.48 U 0.095 U 48 U 7.8 10/11/11 0.048 U 0.10 3.3 D 0.44 0.087 0.048 U 0.048 U 0.29 0.096 U �0.096 U 0.096 U 0.048 U 0.096 U 0.096 U 0.096 U 0.096 U 0.43 0.048 U 0.048 U 0.096 U 4.3 Jp 2.9 10/23/12 0.48 U 0.17 JD 6.3 D 2.2 D 0.14 JD 0.48 U 0.48 U _ 0.48 D 0.48 U 0.48 U 0.48 U 0.48 U 0.48 U 0.48 U 0.48 U 0.48 U 0.48 U 0.48U _ 0.48 U 0.48 U 11 JD 6.7 10/16/13 0.049 U 0.12 2.4 Ep 1.1 Ep 0.068 p 0.049 U 0.065 p 0.21 p 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.24 0.049 U 0.049 U 0.049 U 3.7 Jp 0.21 J 10/21/14 0.048 U 0.15 3.3 0.73 0.16 0.048 U 0.047 Jp 0.51 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.32 0.048 U 0.048 U 0.048 U 5.3 p 1.3 10/21/15 _ 0.05 U 0.081 1.7 0.27 0.067 0.05 U 0.05 U 0.17 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.017 Jp 0.05 U 0.05 U 0.17 0.05 U 0.019 Jp 0.05 U 2.6 J 1.0 U MW-22L 05/05/98 0.5U 3.40 1.8 2.7 3.0 0.5U 0.5U 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 1.OU 0.5U j 0.5U 5.OU 10U NA 07/23/98 0.5U 4.4 2.5 3.9 3.9 0.5U 0.5U . 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 1.OU 0.5U 0.5U 5.OU 10U NA 10/27/98 2.6 U 3.7 _ 2.3 J 3.1 3.3 2.6 U 2.6 U 5.1 U 5.1 U 5.1 U 5.1 U 2.6 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 0.26 U 0.26 U 2.6 U 51 U NA 01/13/99 0.5 U,O 4.0 2.1 3.4 3.5 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 04/13/99 1 U 4 Q 2.2 3.5 3.6 1.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 40 U NA 08/12/99 0.26 U 4.0 2.2 3.6 3.6 0.26 U 0.26 U 0.12 J 0.081 J 0.53 U 0.53 U 0.26 U 0.53 U 0.53 U 0.53 U 0.53 U 0.53 U 0.26 U _ 0.26 U 2.6 U 11 U NA 10/14/99 0.5 U 3.2 1.8 2.8 2.8 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 02/04/00 0.25 U 3.3 Q 1.8 2.9 3.0 0.25 U 0.25 U 0.074 J 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.095 J 0.25 U _ 0.25 U 2.5 U 10 U NA 04/11/00 0.25U,Q 2.4 1.5 2.3 2.2 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 07/21/00 0.25U,Q 2.5 1.5 2.4 2.3 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 10/11/00 0.25U,Q 2.7 1.6 2.5 2.4 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 01/10/01 0.5 U 2.7 Q 1.8 Q 2.5 Q 2.5 Q 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/10/01 0.5 U 2.1 1.8 2.1 1.8 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 04/09/02 0.5G 1.1 1.2 1.8 0.61 0.25 U 0.25U , 0.2J 0.5U 0.5U 1.OG 0.25U 1.OG 0.5U 0.5U 0.5U 0.18J 0.25U 0.5G 2.5U 10U NA 10/23/02 0.5 U 1.2 1.5 2.1 0.56 0.5 U 0.5 U 1.0 U 1.0 U , 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U _ 5.0 U 2 U NA 10/07/03 0.25U 1.2 1.4 2.2 0.68 0.25U 0.25U 0.079J 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.13J 0.25U 0.25U 2.5U 10U NA 10/21/04 0.5 U 1 1.5 1.7 0.66 0.5 U 0.5 U 0.2 J,PG 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 0.11 J 0.2 J 0.5 U 0.5 U 5.0 U 6.4 J NA 10/11/05 0.5U 0.91 1.2 1.5 0.75 0.5U 0.5U 0.075J 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 1.OU 0.5U 0.5U 5.OU 20U NA 10/23/06 0.5 U 1.1 1.4 1.7 0.95 0.5U 0.5 U 0.1 J,PG 1.OU 1.0 U 1.OU 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/15/07 0.25U 0.99 1.1 1.4 0.81 0.25U 0.25U 0.035J 0.5U 0.5U 0.027J 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 10/14/08 0.049 U 0.66 0.76 0.97 0.44 0.049 U 0.049 U 0.046 J 0.097 U 0.097 U , 0.097 U 0.049 U 0.097 U , 0.097 U 0.097 U 0.097 U 0.035 J 0.049 U 0.049 U 0.49 U 4.9 U NA 10/20/09 0.05 U 0.22 0.32 0.38 0.2 0.05 U 0.05 U 0.014 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5.0 U NA 11.990010.00 Page 10 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a> a) 0 C = a a) c = U U 2 a p W I- C C cCo t o 0 o s c c o m m m m m E cis mc S 0 @ :> o _� a) >, s a> PARAMETER o @ t6 a r 2 -a 9 9 9 = . a " as m X X n 2 L _� E C U E O a) O m O > C N C .-. .. O Q c4 C Q a N N J (6 CD C)L b ;:r k a , W C •` X Ts _o a t6 .0 U '� vt C C W a C I I I- U C) 0 W W LC W F- PERFORMANCE STANDARD 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** 10/13/10 0.05 U 0.34 0.52 p 0.6 0.3 0.05 U 0.05 U 0.033 J 0.1 U 0.1 U 0.1 U 0.05 U 0.021 J 0.1 U 0.1 U 0.1 U 0.033 J 0.05 U 0.05 U 0.49 U 5.0 U NA 10/12/11 0.049 U 0.27 0.52 p 0.51 0.24 0.049 U 0.049 U 0.059 J 0.097 U 0.097 U 0.097 U 0.49 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U " 0.049 U 0.049 U 0.097 U 4.9 U NA 10/24/12 0.049 U 0.23 0.66 0.48 _ 0.2 0.049 U 0.049 U 0.072 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.047 J 0.049 U 0.049 U 0.049 U 4.9 U NA _ 10/16/13 0.05 U 0.2 0.82 E* 0.53 0.18 0.05 U 0.05 U 0.094 0.05 U 0.05 U 0.05 U _ 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.064 0.05 U 0.05 U 0.05 U 1.1 Jp NA 10/22/14 0.048 U 0.19 0.71 0.47 0.16 0.048 U 0.048 U 0.091 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U* 0.048 U 0.078 0.048 U 0.048 U 0.048 U 1.2 J NA 10/20/15 0.049 U 0.17 0.71 0.44 0.12 _ 0.049 U 0.049 U 0.071 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.072 0.049 U 0.049 U 0.049 U 1.9 J NA MW-25L 05/05/98 0.5 U 3.1 0.53 1.2 2.5 0.5 U 0.5 U 1 U 1 U 1 U 1 U 0.5 U 1 U 1 U 1 U 1 U 1 U 0.5 U 0.5 U 5U 10U NA 07/23/98 0.25 U 3.1 0.53 0.96 2.5 _ 0.25 U 0.25 U 1 U 1 U 1 U 1 U 0.25 U 1 U 1 U 1 U 1 U 1 U 0.25 U 0.25 U 2.5 U 5 U NA 10/29/98 2.5 U 2.9 0.57 J 0.89 J 2.4 J _ 2.5 U 2.5 U 5.1 U 5.1 U 5.1 U 5.1 U 2.5 U 5.1 U 5.1 U 5.1 U 5.1 U 5.1 U 2.5 U 2.5 U 25 U 51 U NA 01/14/99 0.5 U,O 3.7 0.63 1.2 3.1 0.5 U 0.5 U 1 U 1 U 1 U 1 U 0.5 U 1 U 1 U 1 U 1 U 1 U 0.5 U 0.5 U 5U 20 U NA 04/14/99 0.5 U,Q 3.7 0.63 1.2 3.1 0.5 U 0.5 U _ 1 U 1 U 1 U 1 U 0.5 U 1 U 1 U 1 U 1 U 1 U 0.5 U 0.5 U 5U 20 U NA 08/12/99 0.27 U 3.7 0.62 1.2 3.1 0.27 U 0.27 U 0.54 U 0.54 U 0.54 U 0.54 U 0.27 U 0.54 U 0.54 U 0.54 U 0.54 U 0.54 U 0.27 U 0.27 U 2.7 U 11 U NA 10/12/99 0.5 U 3.2 0.57 1.1 2.7 0.5 U 0.5 U 1 U 1 U 1 U 1 U 0.5 U 1 U 1 U 1 U 1 U 1 U 0.5 U 0.5 U 5U 20 U NA 02/03/00 0.25 U 3.5 0.55 1.2 _ 2.9 0.25 U 0.25 U 1U 1U 1U 1U 0.25 U 1U 1U 1U 1U 1U 0.25 U 0.25 U 2.5 U 10 U NA 04/12/00 0.5 U 2.4 1.5 2.3 2.2 0.5 U 0.5 U 1 U 1 U 1 U 1 U 0.5 U 1 U 1 U 1 U 1 U 1 U 0.5 U 0.5 U 5U 20 U NA 07/23/00 0.25 U,Q 3.4 0.56 1.2 2.9 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U _ 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 10/12/00 0.25 U,Q 3.2 0.54 1 2.6 0.25 U 0.25 U 0.5 U 0.5 U _ 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10U NA 01/10/01 0.5 J4 3.7 Q,J4 0.72 Q,J4 1.3 Q,J4 3.2 Q,J4 0.5 J4 0.5 J4 1 1 J4 1 J4 1 J4 0.5 J4 1 J4 1 J4 1 J4 1 J4 1 J4 0.5 J4 0.5 J4 5 J4 20 J4 NA 10/11/01 0.25 U 1.7 0.35 0.68 1.2 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 04/10/02 0.5 U 2.5 0.57 1.1 1.8 0.5 U 0.5 U 1 U 1 U 1 U 1 U 0.5 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 5U 20 U NA 10/24/02 0.25 U 2.3 0.58 1.1 1.5 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 2.0 U NA 10/08/03 NR 1.6 0.59 0.97 0.99 _ 0.5U 0.5U 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 1.OU 0.5U 0.5U 5.OU 20U NA 10/20/04 0.25 U 1.4 0.56 0.89 0.73 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.02 J 0.5 U 0.5 U 0.059 J 0.25 U 0.25 U 0.079 J 10 U NA 10/14/05 0.5 U 1.5 0.6 0.93 0.7 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5U 0.5 U 5.0 U 20 U NA 10/23/06 1.OU 1.4 0.79J 1.3 0.65J 1.OU 1.OU 2.OU 2.OU 2.OU 2.OU 1.OU 2.OU 2.OU 2.OU 2.OU 2.OU 1.OU 1.OU 10U 40U NA 10/15/07 0.47 U 1.5 0.63 1.1 0.54 0.47 U 0.47 U 0.95 U 0.95 U 0.95 U 0.95 U 0.47 U 0.95 U 0.95 U 0.95 U 0.95 U 0.95 U 0.47 U 0.47 U 4.7 U 19 U NA 10/15/08 0.049 U 1.2 0.53 1.2 0.47 0.049 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.49 U 4.9 U NA 10/20/09 0.05 U 0.62 0.43 0.84 E 0.069 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5.0 U NA 10/13/10 0.048 U 1.0 E 0.49 p 1.3 E 0.13 0.048 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U _ 0.095 U 0.095 U 0.095 U 0.095 U 0.025 J 0.048 U 0.048 U _ 0.095 U 4.8 U NA 10/12/11 0.050 U 0.87 D 0.54 p _ 1.1 D 0.15 0.050 U 0.050 U 0.099 U 0.099 U 0.099 U 0.099 U 0.050 U 0.099 U 0.099 U 0.099 U 0.099 U 0.099 U 0.050 U 0.050 U 0.099 U 5.0 U NA 10/24/12 0.20 U 0.88 D 0.56 D 0.97 D 0.1 JD 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 0.20 U 20 U NA 10/16/13 0.051 U 0.93 E 0.64 1.4 E 0.13 0.051 U 0.051 U 0.028 J 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.033 J 0.051 U 0.051 U 0.051 U 5.1 U NA 10/23/14 0.049 U 0.77 0.56 0.98 0.11 0.049 U 0.049 U 0.025 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U* 0.049 U 0.031 J 0.049 U 0.049 U 0.049 U 4.9 U NA 10/21/15 0.05 U 0.7 0.56 0.97 0.1 0.05 U 0.05 U _ 0.015 J 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.027 J 0.05 U 0.05 U 0.05 U 5.0 U NA MW-27L 05/05/98 0.5U 9.9 2.5 4.7 7.9 0.5U 0.5U 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 0.15J 0.5U 0.5U 5.OU 10U NA 07/23/98 2U 10 3.0 4.6 8.4 2.0 U 2.0 U 4.0 U 4.0 U 4.0 U 4.0 U 2.0 U 4.0 U 4.0 U 4.0 U 4.0 U 4.0 U 2.0 U 2.0 U 20 U 40 U NA 11/04/98 2.6 U 11 0 3.0 5.6 9.4 2.6 U 2.6 U 5.3 U 5.3 U 5.3 U 5.3 U 2.6 U 5.3 U 5.3 U 5.3 U 5.3 U 5.3 U 2.6 U 2.6 U 26 U 53 U NA 01/14/99 2.5 U,O 12 3.6 5.8 10 2.5 U 2.5 U 5.0 U 5.0 U 5.0 U 5.0 U 2.5 U 5.0 U 5.0 U 5.0 U 5.0 U 5.0 U 2.5 U 2.5 U 25 U 1000 NA 04/15/99 1.0 U 12 Q 3.0 5.7 9.9 1.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 40 U NA 08/13/99 1.0 U 11 3.0 5.3 9.5 1.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 40 U NA 10/13/99 1.0 U 11 3.2 5.8 9.5 1.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 40 U NA 02/03/00 1.OU 12Q 3.0 5.3 9.7 1.OU 1.OU 2.OU 2.OU 2.OU 2.OU 1.OU 2.OU 2.OU 2.OU 2.OU 2.OU 1.OU 1.OU 10U 40U NA 04/13/00 1 U,Q 10 3.0 5.2 8.6 1.OU 1.OU 2.OU 2.OU 2.OU 2.OU 1.OU 2.OU 2.OU _ 2.OU 2.OU 2.OU 1.OU 1.OU 10U 40U NA 07/21/00 1.1 Q,V 11 3.4 5.6 9.5 1.1 U 1.1 U 2.3U 2.3U 2.3U 2.3U 1.1 U 2.3U 2.3U 2.3U 2.3U 2.3U 1.1 U 1.1 U 11 U 46U NA 10/14/00 2.5 U,Q 9.8 2.9 4.5 8.3 2.5 U 2.5 U 5.0 U 5.0 U 5.0 U 5.0 U 2.5 U 5 U 5.0 U 5.0 U 5.0 U 5.0 U 2.5 U 2.5 U 25 U 100 U NA 11.990010.00 Page 11 of 18 0 2016 EnviroTrac January 2016 i TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) U o - = -a a) Z5 c c = _ = m N o @ c 0 W H c a, r o 0 0 s c _c PARAMETER _•c mcis m f s coo L E -o 9 0 Q . ° a Y @ m 'x X n 2 Q a_ a� Ev U mL v v v v ° p w c a na_c �U c c c a> m mm w w c w = _ 2 H H PERFORMANCE - 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** STANDARD 01/11/01 0.5 U : 8.9 3.0 4.7 8.1 0.5 U : 0.5 U 1.0 U 1.0 U _ 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/10/01 0.5 U _ 3.7 1.5 2.4 2.3 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 2.5G 1.0 U 1.0 U 1.0 U 0.5U 0.5 U 5.0 U 20 U NA 04/09/02 0.5 U 3.9 3.0 4.9 1.9 0.5 U 0.5 U 0.35 J 1.0 U _ 2.0 G 1.0 U 0.5U 1.0 U 1.0 U 1.0 U 1.0 U 0.39 J 0.5 U 1.0 G 5.0 U 20 U NA 10/25/02 , 1.2U , 1.9 2.7 3.8 0.54J 1.2U 1.2U 2.5U 2.5U _ 2.5U 2.5U 1.2U 2.5U 2.5U 2.5U 2.5U 2.5U _ 1.2U 1.2U 12U 120U NA 10/08/03 1.0 U _ 1.4 2.9 4.0 1.0 U 1.0 U 1.0 U 2.0 U 2.0 U _ 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 40 U NA 10/20/04 1.OU _ 1.3 2.6 3.5 0.18J 1.OU 1.OU 0.17J 0.25J 0.081J 0.21J 0.063J 2.OU 0.28J 2U 0.34J 0.56J 1.OU 1.OU 1.5J 40U NA 10/13/05 1.0 U 1.3 2.7 3.0 0.18 J 1.0 U 1.0 U 0.16 J 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 40 U NA 10/24/06 0.5G 1.6 2.9 4.1 0.25J 0.5U 0.5U 0.11 JD 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 0.38J,PG 0.5U 0.5U 5.OU 20U NA 10/16/07 2U 1.7 3.1 3.9 0.27 J 0.98 U 0.98 U 2.0 U 2.0 U 2.0 U 2.0 U 0.98 U 2.0 U 2.0 U 2.0 U 2.0 U 2U 0.98 U 0.98 U 9.8 U 39 U NA 10/15/08 0.047 U 0.047 U 0.047 U 0.047 U 0.034 J 0.017 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.019 U 0.47 U 4.7 U NA 10/21/09 0.05 U _ 0.21 0.84 E 0.89 E 0.053 0.05 U 0.05 U 0.055 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.086 J 0.05 U 0.05 U 0.1 U 5.0 U NA 10/14/10 0.049 U 3.0 2.3 Ep 2.6 Ep 0.23 p 0.049 U 0.049 U 0.097 p 0.097 U 0.024 Jp 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.3 0.049 U 0.049 U 0.097 U 4.9 U NA 10/12/11 0.050U 1.OD 2.2D 2.7D 0.22 0.050U � 0.050U 0.11 0.10U 0.024Jp 0.10U 0.050U 0.10U 0.10U 0.10U 0.10U 0.22 0.050U 0.050U 0.10U 5.OU NA 10/24/12 0.19 U 1.1 D 2.1 D 2.4 D 0.14 JD 0.19 U 0.19 U 0.11 JD 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.16 JD 0.19 U 0.19 U 0.19 U 19 U NA 10/17/13 0.018 Jp 1.3 E 2.4 E* _ 2.4 Ep 0.21 0.047 U 0.047 U 0.17 0.047 U _ 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.23 0.047 U 0.047 U 0.047 U 2.1 Jp NA 10/22/14 0.049 U 1.3 2.5 2.9 0.25 0.049 U 0.049 U 0.18 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U* 0.049 U 0.25 0.049 U 0.049 U 0.049 U 2 Jp NA 10/21/15 0.05 U 0.92 2.0 2.1 0.17 0.05 U 0.05 U 0.1 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U _ 0.05 U 0.18 0.05 U 0.05 U 0.05 U 0.89 Jp NA MW-31L 05/04/98 0.5 U 2 0 0.49 J 0.95 1.8 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 10 U NA 07/23/98 0.2U 30 0.65 1.2 2.5 0.2U 0.2U 0.4U 0.4U 0.4U 0.4U 0.2U 0.4U 0.4U 0.4U 0.4U 0.4U 0.2U _ 0.2U 2.OU 4.OU NA 10/28/98 0.51 U 2.7 0.64 0.99 2.3 0.51 U 0.51 U 1.0U 1.0 U 1.0 U 1.0 U 0.51 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.51 U 0.51 U 5.1 U 10 U NA 01/12/99 0.5 U,O 2.2 0.6 0.81 1.8 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 04/13/99 0.5 U , 3.5 Q 0.9 1.4 2.8 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 08/11/99 0.28 U 3.4 0.8 1.3 2.8 0.28 U 0.28 U 0.56 U 0.56 U 0.56 U 0.56 U 0.28 U 0.56 U 0.56 U 0.56 U 0.56 U 0.56 U 0.28 U 0.28 U 2.8 U 11 U NA 10/13/99 0.25 U 3.1 0.8 1.4 2.6 0.25 U 0.25 U 0.5 U _ 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 02/03/00 0.25 U 3.6 0.79 1.5 2.9 0.25 U 0.25 U 0.5 U 0.5 U _ 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 04/13/00 0.25 U 3.5 0.82 1.5 2.9 0.25 U _ 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 07/21/00 0.5 U,Q 2.7 0.82 1.5 1.7 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/12/00 0.25U 2.3Q 0.85 1.5 1.0 0.25U 0.25U 0.029J 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 01/11/01 0.25U 2.1Q 0.92Q 1.6Q 0.97Q 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 10/12/01 0.25 U 2.2 0.62 1.1 1.2 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 04/10/02 0.5 U 2.3 0.47 J 0.86 1.8 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U _ 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/22/02 0.25U 1.2 0.61 0.74 0.62 0.25U 0.25U 0.5U 0.5U_ 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 2U NA 10/07/03 0.5 U 1.9 0.92 1.4 0.87 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/21/04 0.5 U 2.4 1.2 1.4 1.5 0.5 U 0.5 U 0.039 J 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.1 J,PG 0.5U 0.5U 5.0 U 20 U NA 10/13/05 0.5 U _ 2.1 0.8 1.0 1.3 0.5 U 0.5 U . 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/23/06 1 U 2.0 1.2 1.8 0.89J 1.OU 1.OU 2.OPG 2.OU 2.OU 2.OU 1.OU 2.OU 2.OU 2.OU 2.OU 2.OU 1.OU 1.OU 10U 40U NA 10/16/07 0.048 U 1.9 1.0 1.4 0.63 0.48 U 0.48 U 0.95 U 0.95 U 0.95 U 0.95 U 0.48 U 0.95 U 0.95 U 0.95 U 0.95 U 0.95 U 0.48 U 0.48 U 4.8 U 19 U NA 10/14/08 0.047 U 1.2 0.72 1.1 _ 0.25 0.047 U _ 0.047 U 0.02 J 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.036 J 0.047 U 0.047 U 0.47 U 4.7 U NA 10/21/09 0.05 U 0.58 0.52 0.76 0.099 0.05 U 0.05 U 0.018 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.035 J 0.05 U 0.05 U 0.1 U 5.0 U NA 10/14/10 0.20 U 1.0 D 1.1 D 1.4 D 0.18 JD 0.20 U 0.20 U 0.41 U 0.41 U 0.41 U 0.41 U 0.20 U 0.41 U 0.41 U 0.41 U 0.41 U 0.41 U 0.20 U 0.20 U 0.41 U 20 U NA 10/12/11 0.054 U 0.59 0.65 0.69 _ 0.16 0.054 U 0.054 U 0.11 U 0.11 U 0.11 U 0.11 U 0.054 U 0.11 U 0.11 U 0.11 U 0.11 U 0.021 Jp 0.054 U 0.054 U 0.11 U 5.4 U NA 10/24/12 0.048 U 0.47 0.47 0.53 0.14 0.048 U 0.048 U 0.020 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.028 J 0.048 U 0.048 U 0.048 U 4.8 U NA 10/17/13 0.053 U 0.57 0.75 1.0 E 0.095 0.015 J 0.053 U 0.032 J 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.056 0.053 U 0.021 J 0.053 U 5.3 U NA 10/23/14 0.049 U 0.58 0.77 1.1 _ 0.11 0.049 U 0.009 J _ 0.035 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U* 0.049 U 0.063 0.049 U 0.012 Jp 0.049 U 4.9 U NA 10/21/15 0.048 U 0.4 0.62 0.86 0.084 0.048 U 0.048 U 0.028 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.049 0.048 U 0.048 U 0.048 U 0.22 Jp NA 11.990010.00 Page 12 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS 0 _ = C a) a� m UI I m a as c c 0 0 @ w a) c a�i _Z s v o aci PARAMETER . co 6 m E 2 as U E o m ft ft co P a c 2 2 F- v a) a w w c w M H To w PERFORMANCE STANDARD 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** MW-32L 04/30/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U _ 0.1 U 0.05 U 0.05 U 0.5 U _ 1 U NA 07/23/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1 U NA 10/28/98 0.055 U 0.055 U 0.055 U 0.055 U 0.055 U 0.055 U 0.055 U 0.11 U 0.11 U 0.11 U 0.11 U 0.055 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.055 U 0.055 U 0.55 U 1.1 U NA 01/19/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 08/11/99 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.11 U 0.11 U 0.11 U 0.11 U 0.05U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.05U 0.05U 0.53U 2.1 U NA 10/13/99 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U _ 10 U NA 02/03/00 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.1 U ' 0.1 U 0.1 U 0.1 U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.05U 0.5U 2.OU NA 04/13/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 07/23/00 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 10/13/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U _ 2.0 U NA 01/11/01 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/12/01 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/10/02 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U _ 2.0 U NA 10/22/02 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U _ 2.0 U NA 10/07/03 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/21/04 0.15U 0.15U 0.15U 0.15U 0.15U 0.15U 0.15U 0.3U 0.3U 0.3U 0.3U 0.15U 0.3U 0.3U 0.3U 0.3U 0.3U 0.15U 0.15U 0.018J . 2.OU NA 10/13/05 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 10/24/06 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/16/07 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.047 U 0.47 U 1.9 U NA 10/14/08 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.047 U 0.47 U _ 4.7 U NA 10/21/09 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U _ 5 U NA 10/14/10 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.1 U 0.1 U 0.1 U 0.1 U 0.051 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.051 U 0.051 U 0.1 U 5.0 U NA 10/12/11 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.10 U 0.10 U 0.10 U 0.10 U 0.052 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.052 U 0.052 U 0.10 U 5.2 U NA 10/25/12 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U _ 5.1 U NA 10/17/13 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 5.1 U NA 10/23/14 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 4.9 U NA 10/22/15 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U* 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 5.3 U NA MW-36L 05/05/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U _ 0.5 U 1.0 U NA 07/22/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 1.0 U NA 11/04/98 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.1 U 0.1 U 0.1 U 0.1 U 0.052 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.052 U 0.052 U 0.52 U 1.0 U NA 01/14/99 0.05 U 0.05 U 0.013 J 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/14/99 0.05 U 0.05 U 0.013 J 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 08/13/99 0.05 U 0.05 U 0.013 J 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/12/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 2.0 U 2.0 U NA 02/03/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 04/11/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 07/22/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/13/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 01/11/01 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005U 0.05U 0.5U 2.OU NA 10/11/01 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 04/10/02 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U _ 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/24/02 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U _ 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/07/03 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U _ 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/21/04 0.05 U 0.05 U 0.05 U 0.007 J 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.008 J 2.0 U NA 11.990010.00 Page 13 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS U_ U N _ = a a) 8 c U U 2 m c c o W H c c m o `o `o t c °� .L m m m C o @ as 0 0 0 ,@ c a) N L : a U a) ) PARAMETER a @cis co a s E -o v 0 9 9 , u'i w a '� cvo m .X X n o Q n E2 U cEo ° v_ a o P a `_a a m t �U v ,a' cc a c 2 2 a> rn o w w lL W 2 (- PERFORMANCE 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** STANDARD 10/14/05 0.05 U 0.05 U 0.05 U 0.012 J 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/23/06 0.05 U 0.05 U 0.05 U 0.012 J 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U , 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.005 U 0.05 U 0.5 U 2.0 U NA 10/15/07 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.1 U 0.1 U 0.1 U 0.1 U 0.052 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.052 U 0.052 U 0.52 U 2.1 U NA 10/16/08 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.047 U 0.47 U 4.7 U NA 10/20/09 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5 U NA 10/13/10 0.048 U 0.010 J 0.048 U 0.014 Jp 0.048 U 0.048 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U 0.048 U 0.095 U 5.0 U NA 10/12/11 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.097 U 0.097 U 0.097 U 0.097 U 0.048 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.048 U 0.048 U 0.097 U 4.8 U NA 10/24/12 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 5.0 U NA 10/16/13 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 4.9 U NA 10/22/14 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U* 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 4.9 U NA 10/21/15 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 4.9 U NA MW-37L 05/05/98 0.05 U 0.79 0.15 0.33 0.87 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1.0 U NA 07/23/98 0.2U 1.20 0.18J 0.38 0.96 0.2U 0.2U 0.4U 0.4U 0.4U 0.4U 0.2U 0.4U 0.4U 0.4U 0.4U 0.4U 0.2U 0.2U 2.OU 4.OU NA 10/27/98 0.51 U 1.5 0.51 U 0.51 U 1.2 0.51 U 0.51 U 1.0 U 1.0 U 1.0 U 1.0 U 0.51 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.51 U 0.51 U 5.1 U 10 U NA 01/13/99 0.5 U,O 1.6 0.24 J 0.57 1.3 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 04/14/99 0.5 U,Q 1.7 0.24 J 0.55 1.3 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 08/12/99 0.28 U 2.3 0.32 0.78 1.8 0.28 U 0.28 U 0.56 U 0.56 U 0.56 U 0.56 U 0.28 U 0.56 U 0.56 U 0.56 U 0.56 U 0.56 U 0.28 U 0.28 U 2.8 U 11 U NA 10/12/99 0.25 U 1.8 0.27 0.62 1.4 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 02/04/00 0.25 U 2.0 0.29 0.66 1.6 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 04/12/00 0.25 U,Q 2.2 0.32 0.8 1.7 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 07/22/00 0.25 U,Q 2.6 0.36 0.94 2.1 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 10/12/00 0.25 U 2.3 Q 0.34 0.84 1.9 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 01/11/01 0.5 U 2.4 0.41 J 0.84 1.9 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/11/01 0.25 U 2.5 0.37 0.91 2.0 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 04/09/02 0.5 U 2.5 0.52 1.0 1.9 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.26 J 0.5 U 0.5 U 5.0 U 20 U NA 10/24/02 1.0 U 3.1 0.65 J 1.3 2.3 1.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 2.0 U NA 10/08/03 0.5 U 2.9 0.61 J 1.2 2.4 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/20/04 0.25 U 2.3 0.67 1.2 1.7 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.013 J 0.5 U 0.5 U 0.068 J 0.25 U 0.25 U 0.049 J 10 U NA 10/13/05 0.5 U 2.6 0.66 J 1.2 1.8 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5 U 20 U NA 10/23/06 1.0 U 2.4 0.74 1.5 1.6 1.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 2.0 U 2.0 U 2.0 U 2.0 U 2.0 U 1.0 U 1.0 U 10 U 40 U NA 10/15/07 0.24 U 3.1 2.4 U 1.8 J 2 J 2.4 U 2.4 U 4.8 U 4.8 U 4.8 U 4.8 U 2.4 U 4.8 U 4.8 U 4.8 U 4.8 U 4.8 U 2.4 U 2.4 U 24 U 95 U NA 10/14/08 0.047 U 2.2 0.72 U 1.8 1.3 0.047 U 0.047 U 0.019 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.027 J 0.047 U 0.047 U 0.47 U 4.7 U NA 10/20/09 0.05 U 0.77 0.43 1.0E 0.11 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.026 J 0.05 U 0.05 U 0.1 U 5.0 U NA 10/13/10 0.49 U 3.4 D 1.1 D 3.4 D 1.2 D 0.49 U 0.49 U 0.97 U 0.97 U 0.97 U 0.97 U 0.49 U 0.97 U 0.97 U 0.97 U 0.97 U 0.97 U 0.49 U 0.97 U 0.49 U 49 U NA 10/12/11 0.050U 0.92D 0.59 1.4D 0.23 0.050U 0.050U 0.10U 0.10U 0.10U 0.10U 0.050U 0.10U 0.10U 0.10U 0.10U 0.018Jp 0.050U 0.050U 0.10U 5.OU NA 10/24/12 0.19 U 0.76 D 0.66 D 1.2 D 0.16 JD 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 19 U NA 10/16/13 0.048 U 1.0 E 0.77 1.6 E 0.23 _ 0.048 U 0.048 U 0.021 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.049 0.048 U 0.048 U 0.048 U 4.8 U NA 10/23/14 0.048 U 0.61 0.5 1.0 0.18 0.048 U 0.048 U_ 0.016 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.036 J 0.048 U 0.048 U 0.048 U 4.8 U NA 10/21/15 0.049 U 0.88 0.68 1.5 0.18 0.049 U 0.049 U 0.018 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.046 J 0.049 U 0.049 U 0.049 U 0.75 J NA MW-38L 05/05/98 0.05 U 0.05 U _ 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.066 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1.0 U NA 07/23/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.059 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1 U NA 10/28/98 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.043 J 0.11 U 0.11 U 0.11 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.053 U 0.53 U 1.1 U NA 01/19/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U _ 0.05 U 0.056 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA _ 04/13/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U _ 0.05 U 0.05 U _ 0.054 J 0.1 U , 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 08/11/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.041 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 11.990010.00 Page 14 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS U as = -a a) 8 m C = I I m "d (6 C C 0 W al N w L O O O L C L PARAMETER m @ o s a QTD cn w -o " m x x n o o as fl N E J N cn b Ni-- v v -o a C w .` o N N N w xp m rn n lL W w c W = = g ~ H m w PERFORMANCE STANDARD 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** 10/13/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.043 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.O U NA 02/03/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.037 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 07/23/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U _ 0.5 U 2.0 U NA 10/12/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U , 0.05 U _ 0.05 U 0.035 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U _ 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 01/11/01 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.05U 0.033J 0.1 U 0.1 U 0.1 U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.05U 0.5U 2.OU NA 10/10/01 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.021 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U _ 0.05 U 0.5 U 2.0 U NA 04/10/02 0.12 J 0.05 U 0.05 U 0.16 J 0.05 U 0.05 U 0.05 U 0.038 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U , 0.05 U 0.05 U 0.5 U 2.O U NA 10/22/02 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U , 0.05 U _ 0.05 U . 0.021 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/08/03 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.03 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/21/04 0.001 J,PG 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.04 J 0.012 J,PG 0.0059 J 0.015 J,PG 0.05 U 0.1 U 0.015 J 0.1 U 0.016 J 0.016 J 0.05 U 0.005 J 0.078 J 2.0 U NA 10/13/05 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.028 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/23/06 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.02 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/15/07 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.028 J 0.098 U 0.098 U 0.098 U 0..049 U 0.098 U 0.098 U 0.098 U 0.098 U 0.098 U 0.049 U 0.049 U 0.49 U 2.0 U NA 10/14/08 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.098 U 0.098 U 0.098 U 0.098 U 0.049 U 0.098 U 0.098 U 0.098 U 0.098 U 0.098 U 0.049 U 0.049 U 0.49 U 4.9 U NA 10/21/09 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5 U NA 10/14/10 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.016 J 0.095 U 0.095 U 0.095 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U 0.048 U 0.095 U 4.8 U NA 10/13/11 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.050 U 0.10 U 0.10 U 0.10 U 0.10 U 0.050 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.050 U 0.050 U 0.10 U 5.O U NA 10/24/12 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U NA 10/17/13 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 5.1 U NA 10/23/14 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.0041 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U NA 10/22/15 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U* 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 5.3 U NA MW-39L 05/05/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 1.0 U NA 07/23/98 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 1.0 U NA 10/28/98 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.1 U 0.1 U 0.1 U 0.1 U 0.51 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.051 U 0.051 U 0.51 U 1.0 U NA 01/19/99 0.05 U 0.05 U , 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 1.0 U NA 04/14/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 08/12/99 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.1U 0.5U 2.OU NA 10/13/99 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 02/03/00 0.05 U 0.05 U 0.05 U . 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.O U NA 04/13/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 07/23/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U , 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 10/12/00 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 01/11/01 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 10/10/01 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 04/10/02 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 10/22/02 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 10/07/03 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.5 U 2.0 U NA 10/21/04 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.0044 J 0.0032 J 0.0036 J 0.006 J 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.0009 J 0.32 J 2.0 U NA 10/13/05 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1.OU 4.OU NA 10/24/06 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 0.5 U 2.0 U NA 10/15/07 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.094 U 0.094 U 0.094 U 0.094 U 0.094 U 0.047 U 0.047 U 0.47 U 1.9 U NA 10/14/08 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U - 0.047 U 0.047 U 0.047 U 0.047 U 4.7 U NA 10/20/09 0.05 U 0.05 U _ 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5.0 U NA 10/14/10 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.097 U 4.9 U NA 10/13/11 0.048 U 0.048 U 0.048 U _ 0.048 U 0.048 U 0.048 U 0.048 U 0.097 U 0.097 U 0.097 U 0.097 U 0.048 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.048 U_ 0.048 U 0.097 U 4.8 U NA 11.990010.00 Page 15 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) a) U 0 m = c �. c O a) a) c = _ = m 0 C c W F- @ �.0- L o O o 0 t c .c • CD i •c 0 w w .0. N L L -0 U a) PARAMETER a °�cis f° a r E a o Q Q C)) w a m '� 'x X a o Q Q v U m � Q tt '�t P W Lu = _ 2 ~ .c PERFORMANCE 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** STANDARD 10/24/12 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 4.7 U NA 10/17/13 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U NA 10/23/14 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U NA 10/21/15 0.051 U 0.051 U 1 0.051 U _ 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 5.1 U NA MW-40L 04/30/98 0.05U I 0.79 0.1 0.2 0.69 0.05U I 0.05U I 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.1 U I 0.1 U I 0.1 U 0.1 U 0.012J 0.05U I 0.05U 0.5U I 1.OU I NA 07/23/98 0.25 U 2.40 0.28 0.66 2.0 0.25 U 0.25 U 0.5 U 0.5 U , 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 5U NA 11/04/98 0.51 U 3.2 0.4J 0.9 2.6 0.51 U 0.51 U 1.OU 1.OU 1.OU 1.OU 0.51 U 1.OU 1.OU 1.OU 1.OU 1.OU 0.51 U 0.51 U 5.1 U 10U NA 01/19/99 0.5U 2.1 0.33J 0.63 1.8 0.5U 0.5U 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 1.OU 0.5U 0.5U 5.OU 20U NA 04/14/99 0.5U,Q 2.0 0.26J 0.52 1.6 0.5U 0.5U 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 1.OU 0.5U 0.5U 5.OU 20U NA 08/11/99 0.27 U 3.3 0.44 1.0 2.6 0.27 U 0.27 U 0.54 U 0.54 U 0.54 U 0.54 U 0.27 U 0.54 U 0.54 U 0.54 U 0.54 U 0.54 U 0.27 U 0.27 U 2.7 U 11 U NA 10/13/99 0.25 U 2 0.32 0.73 1.5 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 02/03/00 0.1 U 1.5 0.2 0.46 1.1 0.1 U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1.OU 4U NA 04/13/00 0.25 U,Q 1.7 l 0.41 0.81 0.93 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 07/22/00 0.25 U,Q 2.0 0.45 1.1 0.85 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 10/13/00 0.25 U,Q 1.8 0.47 1.0 0.67 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 01/11/01 0.25U 1.9Q 0.57Q 1.3Q 0.89Q 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 10/11/01 0.25U 1.2 0.45 0.76 0.18J 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 04/10/02 0.3 U 0.97 0.3 0.64 0.32 0.3 U 0.3 U 6.0 U 6.0 U 6.0 U 6.0 U 0.3 U 6.0 U 6.0 U 6.0 U 6.0 U 6.0 U 0.3 U 0.3 U 3.0 U 12 U NA 10/24/02 0.25 U 1.1 0.49 0.97 0.17 J 0.25 U 0.25 U - 0.5 U 0.5 U , 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U _ 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 10/07/03 0.05 U 0.81 0.29 0.72 0.084 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U _ 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2 U NA 10/21/04 0.25 U 1.2 0.54 1.0 0.26 0.25 U 0.25 U 0.021 J,PG 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.055 J 0.25 U 0.25 U 2.5 U 10 U NA 10/13/05 0.25 U 0.46 0.31 0.54 0.066 J 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25U 0.25 U 2.5 U 10U NA 10/23/06 0.25 U 0.7 0.56 1.1 0.13J 0.5 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 0.5 U 5.0 U 20 U NA 10/15/07 0.95U 0.86J 1.0 1.9 0.12J 0.95U 0.95U 1.9U 1.9U 1.9U 1.9U 0.95U 1.9U 1.9U 1.9U 1.9U 1.9U 0.95U 0.95U 9.5U 38U NA 10/15/08 0.049 U 0.4 0.43 0.91 0.057 0.049 U , 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.49 U 4.9 U NA 10/21/09 0.05 U 0.51 0.73 1.5 E 0.082 0.05 U 0.05 U 0.018 J 0.1 U 0.1 U 0.1 U 0.05 U _ 0.1 U 0.1 U 0.1 U 0.1 U 0.043 J 0.05 U 0.05 U 0.1 U 5 U NA 10/13/10 0.049 U 0.84 E 1.3 E 2.5 E 0.15 0.049 U 0.049 U 0.023 J 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.070 J 0.049 U 0.049 U 0.097 U 4.9 U NA 10/13/11 0.048 U 0.54 1.1 D 2.1 D 0.084 0.048 U 0.048 U 0.019 Jp 0.095 U 0.095 U 0.095 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.062 Jp 0.048 U 0.048 U 0.095 U 4.8 U NA 10/24/12 0.19 U 0.56 D 1.2 D 2.0 D 0.064 JD 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U . 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 19 U NA 10/17/13 0.049 U 0.049 U 0.042 Jp 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 4.9 U NA 10/23/14 0.048 U 0.048 U 0.048 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U NA 10/22/15 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 10.048 U* 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 4.8 U NA PZ-2 04/30/98 0.05 U 0.67 0.17 0.27 0.59 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.012 J 0.05 U 0.05 U 0.5 U 1.0 U NA 07/23/98 0.2U 0.90 0.23 0.38 0.78 0.2U 0.2U 0.4U 0.4U 0.4U 0.4U , 0.2U 0.4U 0.4U 0.4U 0.4U 0.4U 0.2U 0.2U 2U 4U NA 10/28/98 0.053 U 0.98 R 0.24 0.43 0.83 0.053 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.053 U 0.53 U 1.1 U NA 01/19/99 0.05 U 1 0.25 0.45 0.87 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/15/99 0.2 U 0.91 Q 0.25 0.38 0.8 0.2 U 0.2 U 0.4 U 0.4 U 0.4 U 0.4 U 0.2 U 0.4 U 0.4 U 0.4 U 0.4 U 0.4 U 0.2 U 0.2 U 2U 8U NA 08/11/99 0.053 U 0.91 0.22 0.38 0.79 0.053 U 0.0553 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.11 U _ 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.053 U 0.53 U 2.1 U NA 10/14/99 0.25 U 0.83 0.22 J 0.34 0.71 0.25 U 0.25 U 0.5U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 02/04/00 0.05 U 0.59 0.21 0.39 0.78 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U . 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/00 0.05 U 0.79 0.21 0.35 0.7 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 07/23/00 0.1 U,Q 0.92 0.24 0.4 0.82 0.1 U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1.OU 4U NA 10/12/00 . 0.05 U 0.79 0.2 0.33 0.69 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U , 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 01/11/01 0.25U 0.87Q 0.27Q 0.4Q 0.81 Q 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 10/09/01 0.25 U 0.62 0.17 J 0.25 0.56 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.25 U 2.5 U 10 U NA 11.990010.00 Page 16 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) a) a) U c - o a) c c > c O c = 2 2 o=O c co c c ❑ W H m 6 ra L o E 0 0 s c [� o to c ❑ ❑ ❑ 9= :? c a) a) t r o i iv PARAMETER -a 6 cis m E -a U E o a) o - u) y p m m ca 0 o soca z U ❑ v v v c c W c c = 2 CD xo 0 a) I. W W W W 2 ~ H PERFORMANCE STANDARD 0.05 0.05 0.05 0.05 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** 04/10/02 0.05 U 0.56 0.17 0.28 0.5 0.05 U 0.05 U 0.034 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.032 J 0.05 U 0.05 U 0.5 U 2.0 NA 10/22/02 0.05 U 0.72 0.2 0.33 0.62 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/07/03 0.05 U 0.5 _ 0.16 0.25 0.46 0.05 U 0.05 U 0.0062 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/21/04 0.05 U 0.56 0.28 J 0.37 0.48 0.5 U 0.8 U 1.0 U 1.0 U 1.0 U 1.0 U 0.5 U 1.0 U 1.0 U 1.0 U 1.0 U 0.19 J 0.5 U 0.41 J 5U 20 U NA 10/13/05 0.0072 J 0.59 0.21 J 0.31 0.43 0.05 U 0.05 U 0.012 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/23/06 0.1 U 0.6 0.25 _ 0.36 0.46 0.1 U 0.1 U 0.015J,PG 0.2U 0.2U 0.2U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1.OU 4.OU NA 10/16/07 0.094 U 0.78 0.27 0.43 0.58 0.094 U 0.094 U 0.012 J 0.19 U 0.19 U 0.19 U 0.094 U 0.19 U 0.19 U 0.19 U 0.19 U 0.19 U 0.094 U 0.094 U 0.94 U 3.8 U NA 10/14/08 0.049 U 0.59 0.25 0.39 0.39 0.049 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.49 U 4.9 U NA 10/21/09 0.05 U 0.34 0.17 0.27 0.22 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.11 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5.0 U NA 10/13/10 0.049 U 0.45 0.22 p 0.36 0.24 0.049 U 0.049 U 0.013 J 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.097 U 4.9 U NA 10/13/11 0.050 U 0.43 0.25 0.34 _ 0.28 0.050 U 0.050 U 0.10 U 0.10 U 0.10 U 0.10 U 0.050 U 0.10 U 0.10 U 0.10 U 0.10 U 0.10 U 0.050 U 0.050 U 0.10 U 5.O U NA 10/24/12 0.051 U 0.38 0.18 0.24 0.27 0.051 U 0.051 U 0.014 J 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 5.1 U NA 10/17/13 0.049 U 0.31 - 0.19 0.22 0.2 0.049 U 0.049 U 0.015 J 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.049 U 0.013 J 0.049 U 0.049 U 0.049 U 4.9 U NA 10/22/14 0.048 U 0.36 0.18 0.25 0.26 0.048 U 0.048 U 0.014 J 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U 0.048 U* 0.048 U 0.013 Jp 0.048 U 0.048 U 0.048 U 4.8 U NA 10/21/15 0.053 U 0.31 0.17 0.23 0.2 0.053 U 0.053 U 0.011 J 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 0.053 U 5.3 U NA PZ-3 04/30/98 0.05 U 0.33 0.08 0.1 0.29 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.0096 J 0.05 U 0.05 U 0.5 U 1.0 U NA 07/23/98 0.05 U 0.42 0.091 0.14 0.36 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1.0 U NA 10/28/98 0.053 U 0.42 R 0.097 0.14 0.37 0.053 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.053 U 0.053 U 0.53 U 1.1 U NA 01/19/99 0.05 U 0.44 0.1 0.15 0.38 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/15/99 0.05 U 0.43 0.091 0.15 0.38 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 08/11/99 0.05 U 0.46 0.11 0.16 0.41 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.O U NA 10/13/99 0.05 U 0.48 0.11 0.17 0.42 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 02/04/00 0.05 U 0.46 0.089 0.16 0.4 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/00 0.05 U 0.48 0.1 0.17 0.42 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 07/22/00 0.05 U 0.46 0.1 0.16 0.41 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/12/00 0.05 U 0.45 0.1 0.16 0.4 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 01/11/01 0.1 U 0.48Q 0.12Q 0.18Q 0.45Q 0.1 U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1.OU 4.OU NA 10/09/01 0.05 U 0.49 0.11 0.17 0.42 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/10/02 0.05 U 0.46 _ 0.12 0.19 0.37 0.05 U 0.05 U 0.034 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.03 J 0.05 U 0.011 J 0.5 U 2.0 U NA 10/22/02 0.05 U 0.45 0.11 0.18 0.33 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/07/03 0.05 U 0.44 0.13 0.21 0.33 0.05 U 0.05 U 0.0081 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/07/04 01 U 0.41 0.14 0.2 0.31 0.1 U 0.1 U 0.015 J 0.2 U 0.2 U 0.2 U 0.1 U 0.2 U 0.011 J 0.2 U 0.2 U 0.2 U 0.1 U 0.1 U 0.023 J 4.0 U NA 10/13/05 0.05 U 0.41 _ 0.1 _ 0.18 0.29 0.05 U 0.05 U 0.012 J 0.1 U 0.1 U 0.011 J _ 0.05 U 0.1 U 0.1 U 0.014 J 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.O U NA 10/23/06 0.05 U 0.45 0.14 0.23 0.3 0.05 U 0.05 U 0.015 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/16/07 0.05 U 0.56 0.15 0.262 0.38 0.05 U 0.05 U 0.01 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 J 0.1 U 0.1 U 0.05 U 0.0027 J,PG 0.5 U 2.0 U NA 10/14/08 0.049 U 0.39 0.1 0.23 0.21 0.049 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.49 U _ 4.9 U NA 10/30/09 0.049 U 0.31 0.13 0.20 0.23 0.049 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.097 U 4.9 U NA 10/13/10 0.048 U 0.39 0.10 p 0.21 0.27 0.048 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U 0.095 U 0.095 U 0.095 U 0.095 U 0.095 U 0.048 U 0.048 U 0.095 U 4.8 U NA 10/13/11 0.049 U 0.29 0.11 p 0.19 0.20 0.049 U 0.049 U 0.98 U 0.98 U 0.98 U 0.98 U 0.049 U 0.098 U 0.98 U 0.98 U 0.98 U 0.98 U 0.049 U 0.049 U 0.098 U 4.9 U NA 10/24/12 0.047 U 0.3 0.15 0.17 0.19 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 0.047 U 4.7 U NA 10/17/13 0.051 U 0.24 - 0.093 0.14 0.17 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 5.1 U NA 10/22/14 0.05 U 0.27 0.1 0.17 0.19 0.05 U 0.05 U 0.0081 J 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U* 0.05 U 0.0078 J 0.05 U 0.05 U 0.05 U 5.0 U NA 10/21/15 0.052 U 0.25 0.088 0.15 0.17 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 0.052 U 5.2 U NA 11.990010.00 Page 17 of 18 ©2016 EnviroTrac January 2016 TABLE 4: HISTORICAL SUMMARY OF GROUNDWATER SAMPLE RESULTS a) 0 c - = a m c = U V = N as ' C C 0 w i--' C v°c t o o O O L c oo. c m = m m e o o a) .c 0 0 0 w ? t s a a) PARAMETER `o m COai L E 73 Q w -0 m . 0 ccoo .X x n o Q _c to v U 03 O �r "v_ k o o °0 W c a. O. o. s co O 0. N m L 0 a a C y •0 13 a) a) a) o L W fa a m c U er LL Lc W C Lc 2 = i- fo W H PERFORMANCE STANDARD' 0.05 0.05 0.05 i 0.05 i 0.2 NE NE 0.1 NE NE NE NE NE NE NE NE 0.1 NE NE NE 1 ** PZ-5 05/05/98 0.05 U 0.05 U 0.015 J 0.05 U 0.015 J 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 1.0 NA 07/23/98 0.05U 0.05U 0.019J 0.05U 0.018J 0.05U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.05U 0.5U 1.0 NA 10/28/98 0.056 U,R 0.056 U 0.028 J 0.056 U 0.035 J 0.056 U 0.056 U 0.11 U 0.11 U _ 0.11 U 0.11 U 0.056 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.056 U 0.056 U 0.56 U 1.1 U NA 01/19/99 0.05 U 0.02 J 0.039 J 0.05 U 0.07 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U _ 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/15/99 0.05 U 0.048 J 0.046 J 0.05 U 0.12 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 08/11/99 0.054 U 0.087 0.066 0.0094 J 0.18 0.054 U 0.054 U 0.11 U 0.11 U 0.11 U 0.11 U 0.054 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U 0.054 U 0.054 U 0.54 U 2.2 U NA 10/14/99 0.05 U 0.073 0.055 0.0064 J 0.16 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U _ 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 02/03/00 0.05 U 0.083 0.06 0.066 J 0.18 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/13/00 0.05 U 0.1 0.064 0.0095 0.19 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 07/22/00 0.05 U 0.12 _ 0.074 0.05 0.23 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 10/13/00 0.05 U 0.11 0.069 0.0087 J 0.21 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 01/11/01 0.05U 0.14 0.084 0.015J 0.25 0.05U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05U 0.05U 0.5U 2.OU NA 10/10/01 0.05 U 0.18 0.069 0.021 J 0.26 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.5 U 2.0 U NA 04/11/02 0.05 U 0.27 0.11 0.059 0.37 0.05 U 0.05 U 0.03 J 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.03 J 0.05 U 0.05 U 0.5 U 2.0 U NA 10/23/02 0.05 U 0.32 0.11 0.051 0.41 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U _ 0.05 U 0.5 U 2.0 U NA 10/08/03 0.1 U 0.64 0.2 0.13 0.79 0.1 U 0.1 U 0.2U 0.2U 0.2U 0.2U 0.1U 0.2U 0.2U 0.2U 0.2U 0.2U 0.1 U 0.1 U 1.OU 4.OU NA 10/21/04 0.25 U 0.66 0.31 0.21 0.78 . 0.25 U 0.25 U 0.5 U 0.5 U 0.5 U 0.5 U 0.25 U 0.5 U 0.5 U 0.5 U 0.061 J 0.082 J,PG 0.25 U 0.015 J 2.5 U 10 U NA 10/13/05 0.25U 0.47 _ 0.13J 0.11J 0.51 0.25U 0.25U 0.5U 0.5U 0.5U 0.5U 0.25U 0.5U 0.5U 0.5U 0.5U 0.5U 0.25U 0.25U 2.5U 10U NA 10/23/06 0.5U 1.0 0.29J 0.37J 1.1 0.5U 0.5U 1.OU 1.OU 1.OU 1.OU 0.5U 1.OU 1.OU 1.OU 1.OU 1.OU 0.5U 0.5U 5.OU 20U NA 10/15/07 0.024 U 1.4 0.29 0.34 1.3 0.24 U 0.24 U 0.48 U 0.48 U 0.48 U 0.48 U 0.24 U 0.48 U 0.48 U 0.48 U 0.48 U 0.48 U 0.24 U 0.24 U 2.4 U 9.5 U NA 10/14/08 0.049 U 0.89 0.37 0.44 0.85 0.049 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U_0.097 U 0.097 U 0.049 U 0.049 U 0.49 U 4.9 U NA 10/21/09 0.05 U 0.96 E 0.28 0.31 0.92 E 0.05 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.05 U 0.05 U 0.1 U 5.0 U NA 10/14/10 0.049 U 1.6 E 0.27 p 0.46 1.5 E 0.049 U 0.049 U 0.097 U 0.097 U _0.097 U _ 0.097 U 0.049 U 0.097 U 0.097 U 0.097 U 0.097 U 0.097 U 0.049 U 0.049 U 0.097 U 4.9 U NA 10/12/11 0.050 U 0.93 D 0.28* 0.43 0.89 D 0.050 U 0.050 U 0.099 U 0.099 U 0.099 U _ 0.099 U 0.050 U 0.099 U 0.099 U 0.099 U 0.099 U 0.018 J 0.050 U 0.050 U 0.099 U 5.0 U NA 10/24/12 0.21 U 1.7 D 0.34D 0.42 D 1.5 D 0.21 U _ 0.21 U 0.21 U , 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 0.21 U 21 U NA 10/17/13 0.05 U 2 E 0.48 0.55 1.7 E 0.05 U 0.05 U 0.05 U 0.05 U _0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.05 U 0.021 J 0.05 U 0.05 U 0.05 U 5.0 U NA 10/23/14 0.051 U 1.5 0.35 0.61 1.1 0.051 U 0.051 U 0.0078 J 0.051 U 0.051 U_ 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U* 0.051 U 0.022 J 0.051 U 0.051 U 0.051 U 5.1 U NA 10/21/15 0.051 U 1.0 0.31 0.48 0.36 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U 0.051 U* 0.051 U 0.031 J 0.051 U 0.051 U 0.051 U 5.1 U NA NOTES: Results are presented in micrograms per liter J= Estimated value less than the reporting limit but greater than the method detection limit U=Indicates the analyte was not detected p=The%RPD between the primary and confirmation column/detector is>40%. The lower value has been reported E= Results exceeded calibration range D=Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis;also compounds analyzed at a dilution may be flagged with a D PG =The percent difference between the original and confirmation analysis is greater than 40% O= Reporting limit(s)raised due to high level of analyte present in sample NE= No standard established R=Reporting limit(s) raised due to sample volume limitations Q= Elevated reporting limit V=Reporting limit is elevated due to limited sample volume *= LCS or LCSD exceeds the control limits. **=Trichloroethene is not a COC for the Geigy site 4=Sample preparation difficulties NA= Not analyzed for this compound Bold =Concentration exceeds performance standard or method detection limits if no standard is established NS= Not sampled 11.990010.00 Page 18 of 18 ©2016 EnviroTrac January 2016 ATTACHMENT 2 MONITORING LOCATIONS AND DETECTED CONSTITUENTS OCTOBER 2015 MONITORING EVENT � II ----_ /........sel 7____*0 A , ../ Z ........,..--.._...—01-N.......„..\:N....„„\\_:_,4 N °,c o \ ' . _______ • '"�.lti '°cam\ r - \ S \ 1-1/2" gp PVC ``\t.�E HIGHWAY MT- \.... ------.'t...-------- s----. , WP-3D "...%,„„ MW-5S \\+ 4 \ v ko FAVN•12S -� 0+1N-2S� ��� v A \ �,��_ PW-2S qS \ '%--,34 MW-300 WP-38 \ ' , str+-----"--..„..,..*„..........). .,4 ,.., 3 ig, -.",r MW-1OS J 4 ' v Vr.....-- �� 'S r ` " i•-• isi? , MW-14D i u)I \ + \ LEGEND / l.r4,`` -1� 11r `' ,/ t r N Cr/ I. 'q c 4 (46 s �b'l I N MW-5S$ EXISTING MONITORING WELL 0' t 1-//2-.SGH 80 PVC i\s-- S /1 o N.‹PW-1S♦ EXISTING EXTRACTION WELL �\ •• ` 04 AMsuLDING.1. ' WP-1S♦ EXISTING WELL POINT PIEZOMETER ikk• MW-161 c FENCE ' - Q Ln EXTRACTION WELL FORCE MAIN v& 'S TREATED GROUNDWATER N a) DISCHARGE LINE NOTES: MW-17S ,�'a UFILTRATION GALLERIES _m N TOPO MAPPING BY WOOLPERT CONSULTANTS BASED ON MW-16S AERIAL PHOTOGRAPHY FLOWN MARCH 26,1989 WITH +MW-17D 5 GROUND CONTROL TIED TO THE STATE PLANE --- 6C PROPERTY COORDINATE SYSTEM. UNE BUFFER ..A0 p PLANIMETRIC FEATURES WERE FIELD IDENTIFIED ON MAY O 18,1989 BY WOOLPERT CONSULTANTS. O 0 ORIGINAL DRAWING PRODUCED BY RUST ENVIRONMENT AND INFRUSTRUCTURE. • FIGURE 1 LOCATION OF ACCESS ROAD SHOWN ON THIS DRAWING IS EXTRACTION AND TREATMENT SYSTEM SITE LAYOUT y a0i APPROXIMATE. Eii 'iro rac Geigy Chemical Corporation Aberdeen, North Carolina 0 50 100 200 300 a; I Environmental Services LL SCALE IN FEET DATE: 11/04/2015 APPROVED BY: J 7343 W.FRIENDLY AVENUE,SUITE J SCALE: AS SHOWN Q GREENSBORO,NORTH CAROLINA CWH J DRAWN BY:AB PROJECT NO:11.990010.00 • -;, E LIVES • I, •, `' CREEK Z RAfr ( MILL Ln \ / ...._`.4 z 4k-- IT'_� �� Q"� qp I I I I I 4 QO ` 4e It 0 7- _ I. FAV ErrFV�LL f T G`FN0gI �o ,p� F II*C.' Cr q� z #1111441001144 FRS � 41 11)46 � TB CREEL . ...a C z y z �q�R �� �O tiiGy a U k. ViF� �_ • ,�� Mq `� 'ET HESDA �2 J O Q q� =ate ��vv �•• g N my w Op v0 MW-22D J y/GH alpha-BHC 0.028 J 1\ lirVr dbeta-BHCC 0.18 6G„9 XJ�S , �O gamma)BHC 0.0221 -s, MW-18D /� Rj alpha-BHC 0.098 SOOTy delta-BHC 0.39 Q gamma-BHC 0.1 o, c,Q'`' RG>-�! ....I MAIN 0c Dieldrin 0.26 1— Endrin ketone 0.16 ;OSELAND \ IMO SO(7TH FINLEY �� u �- Toxaphene 4.51 I ___ • -. _we& Trichlorothene 1.9 s Mc-F .. •_ `� P. NC J Q 0 211 vS1 o �O��F C4N�- /t �Q I CHAPEL GREENS / • 4411P,N1 / B NCy7 • --- MW-30D PARKWAY _- MW-26D MW-20D alphabeta BHC BHC0.0811.7 I* NI NOT SAMPLED • gamma BHC 0.019 J LLJ delta-BHC 0.27 MW-11D Z alpha-chlordane 0.016 J Q gamma BHC 0.067 NOT SAM LED Q Heptachlor epoxide 0.016 J 44.1 Dieldrin 0.17 0 m a MW-23D• Endosulfan sulfate 0.017 Jp c Lu alpha-BHC 0.0211 Endrin ketone 0.17I HARRIS •F`- beta-BHC 0.0221 Toxaphene 2.6 J gamma-BHC 0.0151 Heptachlor epoxide 0.019 Jp o - - • S'c` • o NOTES: LEGEND FIGURE 2 • MONITORING WELLS SAMPLED IN OCTOBER 2015 UPPER BLACK CREEK AQUIFER MONITORING RESULTS MW-23D• MONITORING WELL LOCATION P ESTIMATED CONCENTRATION nviro rac Geigy p alpha-BHC 0.0211 LABORATORY RESULTS INCLUDE ONLY o beta-BHC 0.022 J LABORATORY RESULTS(ug/L) THE%RPD BETWEEN THE PRIMARY AND CONFIRMATION CONTAMINANTS REPORTED Chemical Corporation gamma-BHC 0.015 J [BOLD EXCEEDS PERFORMANCE STANDARD] ABOVE THE METHOD DETECTION LIMITS. Aberdeen, North Carolina COLUMN/DETECTOR IS>40%. THE LOWER VALUE HAS BEEN REPORTED. Environmental Services _._/ STREAM BACKGROUND MAP FROM MOORE COUNTY GIS. Er_LAPPROVED BY: 7343 W.FRIENDLY AVENUE,SUITE 1 SCALE: AS SHOWN -� DATE: 11 04 2015 0 150 300 450 600 GREENSBORO,NORTH CAROLINA CWH PHONE: 336-763-6025 DRAWN BY:AB PROJECT NO:11.990010.00 SCALE IN FEET I , ��., ,MW 39L 7ELIVEs • .' NO ANALYTES DET E� •4 •. E - RAYS CREEK S PZ-2 alpha-BHC 0.31 U h� beta-BHC 0.17 Z l delta BHC 0.23 • �- gamma-BHC 0.2 m ,I S ..� Dieldrin 0.011 J PZ-3 =1 Q '1,0 • alpha-BHC 0.25 Q �F ,d,aaggpoll beta-BHC 0.088 MW-32L 4 O�Z •: F delta-BHC 0.15 GAF NO ANALYTES DETECTED �0o \ A�`I /EV/L \ gamma-BHC 0.17 T N�q e Qy l " <t• Iq,L z FRS 49 I a ,, zTB CREEL ,S, z c��4044, �� y/Gy MW-36L q/R / V� 4tri: MW-37L NO ANALYTES DETECTED �e� . = v ‹il � Mq �' beta BHC 0 68ha-BHC 8 'ETHESDA TOA No . 41i / / J ? Q- ,, , O� 4<i/ / ° N Qj" delta-BHC 1.5 w O00 `O� �' �I gamma-BHC 0.18 (7 �� p "4 k`r it Dieldrin 0.018J MW-27L \c7 Q Q �j Endrin ketone 0.046 J Qj�` alpha-BHC 0.92 VToxaphene 0.75 J y/GH beta-BHC 2.0 �il Q delta-BHC 2.1 .� 5� St•,- � gamma-BHC 0.17 G'f'J ��J� �O Dieldrin 0.1 Q�� R/ Endrin ketone 0.18 O ANALYTES DETE TE8D2 q spry Toxaphene 0.89 Jp 3 •Cl RGy�I MAIN I-- .g ROSELA 211 z ND MW-40L SOVTN r FINLEY u MW-2 • _ beta BHC 0.043 J • al ha BHC 0.17 �� McF 2.. Q beta-BHC 0.71 N 1 PZ 5 . lr ? �� delta-BHC 0.44 C?j2 �S C,r 40. /. Q C gamma-BHC 0.12 alpha-BHC 1.0 ZS` i v Q HApE beta-BHC 0.31 0, Fkp el vNE � Q MW-25L L GREENS Dieldrin 0.071 4444 ESN \ 9 I Endrin ketone 0.072 delta BHC 0.48 6 NCy alpha-BHC 0.7 ----PARKWAY Toxa hene 1.9 J gamma-BHC 0.36 beta-BHC 0 / Toxaphene Endrin ketone 0.031 J MW 31L•s delta-BHC 0.97 \ IN alpha-BHC 0.4 `roe, gamma-BHC 0.1 beta-BHC 0.62 Dieldrin 0.015 JLi delta-BHC 0.86 Z Endrin ketone 0.027 J Q gamma-BHC 0.084 z \ 4.1 0 Dieldrin 0.028 J co Q. Lu Endrin ketone 0.049 Q Toxaphene 0.22 Jp ¢ / HARRIS Fi_ \ o - - / s� n 0 LEGEND NOTES: FIGURE 3 Pz-s MONITORING WELLS SAMPLED IN OCTOBER 2015 • LOWER BLACK CREEK AQUIFER MONITORING RESULTS , alpha-BHC 1.0 MONITORING WELL LOCATION \/ STREAM aLABORATORY RESULTS(ug/L) LABORATORY RESULTS INCLUDE ONLY nviro rac o beta-BHC 0.31 J ESTIMATED CONCENTRATION CONTAMINANTS REPORTED Geigy Chemical Corporation delta-BHC 0.48 [BOLD EXCEEDS PERFORMANCE STANDARD] p gamma-BHC 0.36 ABOVE THE METHOD DETECTION LIMITS. Aberdeen, North Carolina 11 Endrin ketone 0.031 J p THE%RPD BETWEEN THE PRIMARY AND CONFIRMATION BACKGROUND MAP FROM MOORE COUNTY GIS. Environmental Services COLUMN/DETECTOR IS>40%. THE LOWER VALUE HAS W APPROVED BY: � BEEN REPORTED. 7343 W.FRIENDLY AVENUE,SUITE J DATE: 11/04/2015 0 150 300 450 600 GREENSBORO,NORTH CAROLINA CWH TOA No 2. TOWN OF ABERDEEN SUPPLY WATER WELL SCALE: AS SHOWN SCALE IN FEET DRAWN BY:AB PROJECT NO:11.990010.00 1 • t LIVES II `' CREEK \ i RAY'S MILL 7 SW 08 ,n ) beta-BHC 0.0131p U _ / � / At SW-09 NO ANALYTES DETECTED Lf)T 4 Q F It SW-07 p� �1. FAVf�fVi<<F T GCF'110 alpha-BHC 0.00861 rr �� F beta BHC 0.016 Jp to __ ,tQ , �'�+i�,'+ G(; JNO Q� • - Sly Q��� y�'P ��k, Q. II 9,1, a FRS �� TB CREEL **, C` z q/ ti 4- # /F/ SW-06 CJ < 444 : QQ i!q <v iFTNESD NO ANALYTES DETECTED ��v� O� ��,� ��� (;� ��N �� A ��O O� Q A. LU T� i (.9 O Ov ,c ,`<- •� v a \ �� Q' �• cu `� L `NIGH SW-11-2 ; , �G \T NO ANALYTES DETECTED r S / 0 SOU Skl4 MAIN oac GSELAND \ 211 Z So, r FINLEY u ilj _ M o-� 44, S1 beta-BHCSW-05 �� 'Lio l/ cF''r q �_ (,) 0 NC211 0.013 Jp 6% ��F , N1j�,,` QvQ Q SNAP / l� SW-03 (I) '61"°NE �4N EL GREENS/ , alpha-BHC 0.0 1 i Cy PARKWAY beta-BHC 0.0 •J \ SW-04 s delta-BHCO.s 9J SW-02 NO ANALYTES DETECTED ' beta-BHC 0.0171 1.1., W z a Q ; m SW-01 a p beta-BHC 0.0181 HARRIS <F`_ s X • LEGEND NOTES: FIGURE 4 sw-ol 0 SURFACE WATER LOCATION J ESTIMATED CONCENTRATION MONITORING WELLS SAMPLED IN OCTOBER 2015 • SURFACE WATER MONITORING RESULTS beta-BHC 0.0181 LABORATORY RESULTS(ug/L) LABORATORY RESULTS INCLUDE ONLY nviro rac [BOLD EXCEEDS PERFORMANCE STANDARD] p THE%RPD BETWEEN THE PRIMARY AND CONFIRMATION CONTAMINANTS REPORTED Geigy Chemical Corporation COLUMN/DETECTOR IS>40%. THE LOWER VALUE HAS ABOVE THE METHOD DETECTION LIMITS. Aberdeen, North Carolina STREAM BEEN REPORTED. Environmental Services v BACKGROUND MAP FROM MOORE COUNTY GIS. DATE: 11 04 2015 SCALE: AS SHOWN W 7343 W.FRIENDLY AVENUE,SUITE J / APPROVED BY: 0 150 300 450 600 GREENSBORO,NORTH CAROLINA CWH SCALE IN FEET PHONE: 336-763-6025 DRAWN BY:AB PROJECT NO:11.990010.00 ATTACHMENT 3 ANALYTICAL LABORATORY REPORTS OCTOBER 2015 MONITORING EVENT lestAmerica THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 TestAmerica Job ID: 680-118203-1 1111P.P."w Client Project/Site: Geigy Chemical Corp. For: EnviroTrac, Ltd. 7343 W. Friendly Avenue __ Suite J Greensboro, North Carolina 27410 Attn: Chris Hay Authorized for release by: 11/3/2015 12:02:09 PM Michele Kersey, Project Manager (912)354-7858 michele.kersey@testamericainc.com LINKS Review your project results through Total Access Have a Question? Ask treThe The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters,exceptions are noted in this report. This report may not be reproduced except in full, Ex art and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. *Visit us at: Results relate only to the items tested and the sample(s)as received by the laboratory. www.testamericainc.com Case Narrative Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Job ID: 680-118203-1 Laboratory: TestAmerica Savannah Narrative CASE NARRATIVE Client: EnviroTrac, Ltd. Project: Geigy Chemical Corp. Report Number: 680-118203-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits,with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples,the reporting limits are adjusted relative to the dilution required. RECEIPT The samples were received on 10/23/2015 9:44 AM;the samples arrived in good condition, properly preserved and,where required, on ice. The temperatures of the 5 coolers at receipt time were 1.8°C, 1.8°C, 2.2°C,2.4°C and 4.2°C. VOLATILE ORGANIC COMPOUNDS (GC-MS) Samples Influent(680-118203-12), Effluent(680-1 1 8203-1 3), Carbon Train A-1 (680-118203-14), Carbon Train B-2 (680-118203-15), MW-30D (680-1 1 8203-1 7), MW-18D (680-118203-22), Duplicate 2(680-118203-25), Duplicate 1 (680-118203-27), MW-10S (680-118203-29), MW-18S (680-118203-31), MW-16S (680-118203-34), MW-17S (680-118203-35), MW-16D (680-118203-36)and MW-17D (680-118203-37)were analyzed for Volatile Organic Compounds(GC-MS) in accordance with EPA SW-846 Method 8260B. The samples were analyzed on 10/27/2015. No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. PESTICIDES AND PCBS Samples SW-01 (680-118203-1), SW-02(680-118203-2), SW-03(680-118203-3), SW-04(680-118203-4), SW-05(680-118203-5), SW-11-2(680-118203-6), SW-06(680-118203-7), SW-07(680-118203-8), SW-08(680-118203-9), SW-09(680-118203-10), SW Duplicate (680-118203-11), Influent(680-118203-12), Effluent(680-118203-13), Carbon Train A-1 (680-118203-14), Carbon Train B-2 (680-118203-15), MW-30D(680-118203-17), PZ-2 (680-118203-18), PZ-3(680-118203-19), MW-27L(680-118203-20), MW-36L (680-118203-21), MW-18D(680-118203-22), MW-39L(680-118203-23), MW-31 L(680-118203-24), Duplicate 2 (680-118203-25), MW-65 (680-118203-26), Duplicate 1 (680-118203-27), MW-4S(680-118203-28), MW-10S (680-118203-29), MW-5S(680-118203-30), MW-18S (680-118203-31), MW-22D(680-118203-32), MW-22L(680-118203-33), MW-16S (680-118203-34), MW-17S(680-118203-35), MW-26D (680-118203-38), MW-25L(680-118203-39), MW-37L(680-118203-40), PZ-5 (680-118203-41), MW-23D(680-118203-42), MW-38L (680-118203-43), MW-40L(680-118203-44), MW-32L(680-118203-45)and Duplicate 3 (680-118203-46)were analyzed for Pesticides and PCBs in accordance with EPA SW-846 Method 80816_8082A.The samples were prepared on 10/26/2015, 10/27/2015 and 10/28/2015 and analyzed on 10/29/2015 and 10/30/2015. Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate(MS/MSD/DUP)associated with prep batch 407400. Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate(MS/MSD/DUP)associated with prep batch 407580. Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate(MS/MSD/DUP)associated with prep batch 407762. The following analyte(s) recovered outside control limits for the LCS associated with preparation batch 680-407762 and analytical batch 680-408178: Endrin. This is not indicative of a systematic control problem because these were random marginal exceedances. Qualified TestAmerica Savannah Page 2 of 81 Case Narrative Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Job ID: 680-118203-1 (Continued) Laboratory:TestAmerica Savannah (Continued) results have been reported. This method incorporates 2nd column confirmation. Corrective action is not taken for surrogate/spike compounds unless results from both columns are unacceptable. Results outside criteria are qualified. Samples Influent(680-118203-12)[5X], MW-30D(680-118203-17)[10X], MW-27L(680-118203-20)[4X], MW-18D(680-118203-22)[10X], MW-31 L(680-118203-24)[4X], Duplicate 2(680-118203-25)[4X], MW-6S(680-118203-26)[10X], MW-6S(680-118203-26)[25X], MW-10S (680-118203-29)(4X], MW-5S(680-118203-30)[4X], MW-25L(680-118203-39)[4X], MW-37L(680-118203-40)[4X]and PZ-5 (680-118203-41)[4X]required dilution prior to analysis. The reporting limits have been adjusted accordingly. No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. TOTAL SUSPENDED SOLIDS Samples SW-01 (680-118203-1), SW-02(680-118203-2),SW-03(680-118203-3), SW-04(680-118203-4), SW-05(680-118203-5), SW-11-2(680-118203-6), SW-06(680-118203-7), SW-07(680-118203-8), SW-08(680-118203-9), SW-09(680-118203-10)and SW Duplicate(680-118203-11)were analyzed for total suspended solids in accordance with EPA Method 160.2.The samples were analyzed on 10/26/2015 and 10/27/2015. No analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page. TestAmerica Savannah Page 3 of 81 Sample Summary 1. Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. II Lab Sample ID Client Sample ID Matrix Collected Received 1 680-118203-1 SW-01 Water 10/21/15 09:36 10/23/15 09:44 680-118203-2 SW-02 Water 10/21/15 10:07 10/23/15 09:44 680-118203-3 SW-03 Water 10/21/15 10:32 10/23/15 09:44 680-118203-4 SW-04 Water 10/21/15 11:04 10/23/15 09:44 680-118203-5 SW-05 Water 10/21/15 11:17 10/23/15 09:44 680-118203-6 SW-11-2 Water 10/21/15 11:38 10/23/15 09:44 680-118203-7 SW-06 Water 10/21/15 12:05 10/23/15 09:44 680-118203-8 SW-07 Water 10/21/15 13:19 10/23/15 09:44 680-118203-9 SW-08 Water 10/21/15 13:39 10/23/15 09:44 680-118203-10 SW-09 Water 10/21/15 13:52 10/23/15 09:44 680-118203-11 SW Duplicate Water 10/21/15 13:26 10/23/15 09:44 680-118203-12 Influent Water 10/21/15 14:32 10/23/15 09:44 680-118203-13 Effluent Water 10/21/15 14:38 10/23/15 09:44 680-118203-14 Carbon Train A-1 Water 10/21/15 14:47 10/23/15 09:44 680-118203-15 Carbon Train B-2 Water 10/21/15 15:03 10/23/15 09:44 680-118203-17 MW-30D Water 10/21/15 10:50 10/23/15 09:44 680-118203-18 PZ-2 Water 10/21/15 13:30 10/23/15 09:44 680-118203-19 PZ-3 Water 10/21/15 12:50 10/23/15 09:44 680-118203-20 MW-27L Water 10/21/15 12:00 10/23/15 09:44 680-118203-21 MW-36L Water 10/21/15 10:59 10/23/15 09:44 680-118203-22 MW-18D Water 10/21/15 11:49 10/23/15 09:44 680-118203-23 MW-39L Water 10/21/15 14:12 10/23/15 09:44 680-118203-24 MW-31 L Water 10/21/15 14:16 10/23/15 09:44 680-118203-25 Duplicate 2 Water 10/21/15 10:50 10/23/15 09:44 680-118203-26 MW-6S Water 10/20/15 14:19 10/23/15 09:44 680-118203-27 Duplicate 1 Water 10/20/15 15:04 10/23/15 09:44 680-118203-28 MW-4S Water 10/20/15 13:28 10/23/15 09:44 680-118203-29 MW-10S Water 10/20/15 11:14 10/23/15 09:44 680-118203-30 MW-5S Water 10/20/15 12:02 10/23/15 09:44 680-118203-31 MW-18S Water 10/20/15 15:04 10/23/15 09:44 680-118203-32 MW-22D Water 10/20/15 15:47 10/23/15 09:44 680-118203-33 MW-22L Water 10/20/15 15:21 10/23/15 09:44 680-118203-34 MW-16S Water 10/20/15 13:23 10/23/15 09:44 680-118203-35 MW-17S Water 10/20/15 14:09 10/23/15 09:44 680-118203-36 MW-16D Water 10/20/15 11:38 10/23/15 09:44 680-118203-37 MW-17D Water 10/20/15 12:23 10/23/15 09:44 680-118203-38 MW-260 Water 10/21/15 17:06 10/23/15 09:44 680-118203-39 MW-25L Water 10/21/15 15:17 10/23/15 09:44 680-118203-40 MW-37L Water 10/21/15 16:02 10/23/15 09:44 680-118203-41 PZ-5 Water 10/21/15 15:55 10/23/15 09:44 680-118203-42 MW-23D Water 10/22/15 13:40 10/23/15 09:44 680-118203-43 MW-38L Water 10/22/15 12:31 10/23/15 09:44 680-118203-44 MW-40L Water 10/22/15 13:03 10/23/15 09:44 680-118203-45 MW-32L Water 10/22/15 11:44 10/23/15 09:44 680-118203-46 Duplicate 3 Water 10/22/15 12:37 10/23/15 09:44 TestAmerica Savannah Page 4 of 81 Method Summary Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds(GC/MS) SW846 TAL SAV 8081 B/8082A Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography SW846 TAL SAV 160.2 Solids,Total Suspended(TSS) MCAWW TAL SAV Protocol References: MCAWW="Methods For Chemical Analysis Of Water And Wastes",EPA-600/4-79-020,March 1983 And Subsequent Revisions. SW846="Test Methods For Evaluating Solid Waste,Physical/Chemical Methods",Third Edition,November 1986 And Its Updates. Laboratory References: TAL SAV=TestAmerica Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL(912)354-7858 TestAmerica Savannah Page 5 of 81 Definitions/Glossary Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Qualifiers GC/MS VOA Qualifier Qualifier Description U Indicates the analyte was analyzed for but not detected. GC Semi VOA Qualifier Qualifier Description U Indicates the analyte was analyzed for but not detected. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. p The%RPD between the primary and confirmation column/detector is>40%.The lower value has been reported. * LCS or LCSD is outside acceptance limits. General Chemistry Qualifier Qualifier Description U Indicates the analyte was analyzed for but not detected. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. Listed under the"D"column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio(normalized absolute difference) Dil Fac Dilution Factor DL,RA,RE,IN Indicates a Dilution,Re-analysis,Re-extraction,or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level(Dioxin) NC Not Calculated ND Not detected at the reporting limit(or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit(Radiochemistry) RPD Relative Percent Difference,a measure of the relative difference between two points TEF Toxicity Equivalent Factor(Dioxin) TEQ Toxicity Equivalent Quotient(Dioxin) TestAmerica Savannah Page 6 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-01 Lab Sample ID: 680-118203-1 Date Collected: 10/21/15 09:36 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/26/15 16:51 10/29/15 05:23 1 alpha-BHC 0.050 U 0.050 0.0078 ug/L 10/26/15 16:51 10/29/15 05:23 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/26/15 16:51 10/29/15 05:23 1 beta-BHC 0.018 J 0.050 0.012 ug/L 10/26/15 16:51 10/29/15 05:23 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/26/15 16:51 10/29/15 05:23 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/26/15 16:51 10/29/15 05:23 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:23 1 delta-BHC 0.050 U 0.050 0.013 ug/L 10/26/15 16:51 10/29/15 05:23 1 Dieldrin 0.050 U 0.050 0.0086 ug/L 10/26/15 16:51 10/29/15 05:23 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/26/15 16:51 10/29/15 05:23 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:23 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 05:23 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/26/15 16:51 10/29/15 05:23 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/26/15 16:51 10/29/15 05:23 1 Endrin ketone 0.050 U 0.050 0.0089 ug/L 10/26/15 16:51 10/29/15 05:23 1 gamma-BHC(Lindane) 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 05:23 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:23 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/26/15 16:51 10/29/15 05:23 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/26/15 16:51 10/29/15 05:23 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/26/15 16:51 10/29/15 05:23 1 Toxaphene 5.0 U 5.0 0.19 ug/L 10/26/15 16:51 10/29/15 05:23 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 53 10-130 1026/15 16:51 10/29/15 05:23 1 Tetrachloro-m-xylene 63 39-130 1026/15 16:51 10/29/15 05:23 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.0 U 2.0 2.0 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 7 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-02 Lab Sample ID: 680-118203-2 Date Collected: 10/21/15 10:07 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/26/15 16:51 10/29/15 05:37 1 alpha-BHC 0.050 U 0.050 0.0078 ug/L 10/26/15 16:51 10/29/15 05:37 1 L alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/26/15 16:51 10/29/15 05:37 1 beta-BHC 0.017 J 0.050 0.012 ug/L 10/26/15 16:51 10/29/15 05:37 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/26/15 16:51 10/29/15 05:37 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/26/15 16:51 10/29/15 05:37 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:37 1 delta-BHC 0.050 U 0.050 0.013 ug/L 10/26/15 16:51 10/29/15 05:37 1 Dieldrin 0.050 U 0.050 0.0086 ug/L 10/26/15 16:51 10/29/15 05:37 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/26/15 16:51 10/29/15 05:37 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:37 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 05:37 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/26/15 16:51 10/29/15 05:37 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/26/15 16:51 10/29/15 05:37 1 Endrin ketone 0.050 U 0.050 0.0089 ug/L 10/26/15 16:51 10/29/15 05:37 1 gamma-BHC(Lindane) 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 05:37 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:37 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/26/15 16:51 10/29/15 05:37 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/26/15 16:51 10/29/15 05:37 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/26/15 16:51 10/29/15 05:37 1 Toxaphene 5.0 U 5.0 0.19 ug/L 10/26/15 16:51 10/29/15 05:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 50 10-130 1026/15 16:51 10/29/15 05:37 1 Tetrachloro-m xylene 72 39-130 10/26/15 16:51 10/29/15 05:37 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.0 U 2.0 2.0 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 8 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-03 Lab Sample ID: 680-118203-3 Date Collected: 10/21/15 10:32 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/26/15 16:51 10/29/15 05:52 1 alpha-BHC 0.010 J 0.050 0.0078 ug/L 10/26/15 16:51 10/29/15 05:52 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/26/15 16:51 10/29/15 05:52 1 beta-BHC 0.029 J 0.050 0.012 ug/L 10/26/15 16:51 10/29/15 05:52 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/26/15 16:51 10/29/15 05:52 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/26/15 16:51 10/29/15 05:52 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:52 1 delta-BHC 0.029 J 0.050 0.013 ug/L 10/26/15 16:51 10/29/15 05:52 1 --- Dieldrin 0.050 U 0.050 0.0086 ug/L 10/26/15 16:51 10/29/15 05:52 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/26/15 16:51 10/29/15 05:52 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:52 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 05:52 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/26/15 16:51 10/29/15 05:52 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/26/15 16:51 10/29/15 05:52 1 Endrin ketone 0.050 U 0.050 0.0089 ug/L 10/26/15 16:51 10/29/15 05:52 1 gamma-BHC(Lindane) 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 05:52 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 05:52 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/26/15 16:51 10/29/15 05:52 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/26/15 16:51 10/29/15 05:52 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/26/15 16:51 10/29/15 05:52 1 Toxaphene 5.0 U 5.0 0.19 ug/L 10/26/15 16:51 10/29/15 05:52 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 49 10-130 1026/15 16:51 1029/15 05:52 1 Tetrachloro-m-xylene 56 39-130 1026/15 16:51 10/29/15 05:52 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.0 U 2.0 2.0 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 9 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-04 Lab Sample ID: 680-118203-4 Date Collected: 10/21/15 11:04 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/26/15 16:51 10/29/15 06:06 1 alpha-BHC 0.050 U 0.050 0.0078 ug/L 10/26/15 16:51 10/29/15 06:06 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/26/15 16:51 10/29/15 06:06 1 beta-BHC 0.050 U 0.050 0.012 ug/L 10/26/15 16:51 10/29/15 06:06 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/26/15 16:51 10/29/15 06:06 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/26/15 16:51 10/29/15 06:06 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 06:06 1 delta-BHC 0.050 U 0.050 0.013 ug/L 10/26/15 16:51 10/29/15 06:06 1 Dieldrin 0.050 U 0.050 0.0086 ug/L 10/26/15 16:51 10/29/15 06:06 1 -- Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/26/15 16:51 10/29/15 06:06 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 06:06 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 06:06 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/26/15 16:51 10/29/15 06:06 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/26/15 16:51 10/29/15 06:06 1 Endrin ketone 0.050 U 0.050 0.0089 ug/L 10/26/15 16:51 10/29/15 06:06 1 gamma-BHC(Lindane) 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 06:06 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 06:06 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/26/15 16:51 10/29/15 06:06 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/26/15 16:51 10/29/15 06:06 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/26/15 16:51 10/29/15 06:06 1 Toxaphene 5.0 U 5.0 0.19 ug/L 10/26/15 16:51 10/29/15 06:06 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 46 10-130 10/26/15 16:51 10/29/15 06:06 1 Tetrachloro-m xylene 67 39-130 1026/15 16:51 10/29/15 06:06 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 8.0 4.0 4.0 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 10 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-05 Lab Sample ID: 680-118203-5 Date Collected: 10/21/15 11:17 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0074 ug/L 10/26/15 16:51 10/29/15 06:21 1 alpha-BHC 0.051 U 0.051 0.0080 ug/L 10/26/15 16:51 10/29/15 06:21 1 alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/26/15 16:51 10/29/15 06:21 1 beta-BHC 0.013 J p 0.051 0.012 ug/L 10/26/15 16:51 10/29/15 06:21 1 4,4'-DDD 0.051 U 0.051 0.0079 ug/L 10/26/15 16:51 10/29/15 06:21 1 4,4'-DDE 0.051 U 0.051 0.0075 ug/L 10/26/15 16:51 10/29/15 06:21 1 4,4'-DDT 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 06:21 1 delta-BHC 0.051 U 0.051 0.013 ug/L 10/26/15 16:51 10/29/15 06:21 1 Dieldrin 0.051 U 0.051 0.0088 ug/L 10/26/15 16:51 10/29/15 06:21 1 Endosulfan I 0.051 U 0.051 0.0084 ug/L 10/26/15 16:51 10/29/15 06:21 1 Endosulfan II 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 06:21 1 Endosulfan sulfate 0.051 U 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 06:21 1 Endrin 0.051 U 0.051 0.0090 ug/L 10/26/15 16:51 10/29/15 06:21 1 Endrin aldehyde 0.051 U 0.051 0.017 ug/L 10/26/15 16:51 10/29/15 06:21 1 Endrin ketone 0.051 U 0.051 0.0091 ug/L 10/26/15 16:51 10/29/15 06:21 1 gamma-BHC(Lindane) 0.051 U 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 06:21 1 gamma-Chlordane 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 06:21 1 Heptachlor 0.051 U 0.051 0.0081 ug/L 10/26/15 16:51 10/29/15 06:21 1 Heptachlor epoxide 0.051 U 0.051 0.0083 ug/L 10/26/15 16:51 10/29/15 06:21 1 Methoxychlor 0.051 U 0.051 0.0095 ug/L 10/26/15 16:51 10/29/15 06:21 1 Toxaphene 5.1 U 5.1 0.19 ug/L 10/26/15 16:51 10/29/15 06:21 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 48 10-130 10/26/15 16:51 10/29/15 06:21 1 Tetrachloro-m xylene 66 39-130 10/26/15 16:51 10/29/15 06:21 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 14 1.9 1.9 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 11 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-11-2 Lab Sample ID: 680-118203-6 Date Collected: 10/21/15 11:38 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0075 ug/L 10/26/15 16:51 10/29/15 06:36 1 alpha-BHC 0.051 U 0.051 0.0080 ug/L 10/26/15 16:51 10/29/15 06:36 1 alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/26/15 16:51 10/29/15 06:36 1 beta-BHC 0.051 U 0.051 0.012 ug/L 10/26/15 16:51 10/29/15 06:36 1 4,4'-DDD 0.051 U 0.051 0.0079 ug/L 10/26/15 16:51 10/29/15 06:36 1 4,4'-DDE 0.051 U 0.051 0.0076 ug/L 10/26/15 16:51 10/29/15 06:36 1 4,4'-DDT 0.051 U 0.051 0.0088 ug/L 10/26/15 16:51 10/29/15 06:36 1 delta-BHC 0.051 U 0.051 0.013 ug/L 10/26/15 16:51 10/29/15 06:36 1 Dieldrin 0.051 U 0.051 0.0089 ug/L 10/26/15 16:51 10/29/15 06:36 1 Endosulfan I 0.051 U 0.051 0.0084 ug/L 10/26/15 16:51 10/29/15 06:36 1 Endosulfan II 0.051 U 0.051 0.0088 ug/L 10/26/15 16:51 10/29/15 06:36 1 Endosulfan sulfate 0.051 U 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 06:36 1 Endrin 0.051 U 0.051 0.0091 ug/L 10/26/15 16:51 10/29/15 06:36 1 Endrin aldehyde 0.051 U 0.051 0.018 ug/L 10/26/15 16:51 10/29/15 06:36 1 Endrin ketone 0.051 U 0.051 0.0092 ug/L 10/26/15 16:51 10/29/15 06:36 1 gamma-BHC(Lindane) 0.051 U 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 06:36 1 gamma-Chlordane 0.051 U 0.051 0.0088 ug/L 10/26/15 16:51 10/29/15 06:36 1 Heptachlor 0.051 U 0.051 0.0081 ug/L 10/26/15 16:51 10/29/15 06:36 1 Heptachlor epoxide 0.051 U 0.051 0.0083 ug/L 10/26/15 16:51 10/29/15 06:36 1 Methoxychlor 0.051 U 0.051 0.0096 ug/L 10/26/15 16:51 10/29/15 06:36 1 Toxaphene 5.1 U 5.1 0.20 ug/L 10/26/15 16:51 10/29/15 06:36 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 45 10-130 10/26/15 16:51 10/29/15 06:36 1 Tetrachloro-m-xylene 60 39-130 10/26/15 16:51 10/29/15 06:36 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.1 U 2.1 2.1 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 12 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-06 Lab Sample ID: 680-118203-7 Date Collected: 10/21/15 12:05 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0074 ug/L 10/26/15 16:51 10/29/15 06:50 1 alpha-BHC 0.051 U 0.051 0.0079 ug/L 10/26/15 16:51 10/29/15 06:50 1 alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/26/15 16:51 10/29/15 06:50 1 beta-BHC 0.051 U 0.051 0.012 ug/L 10/26/15 16:51 10/29/15 06:50 1 4,4'-DDD 0.051 U 0.051 0.0078 ug/L 10/26/15 16:51 10/29/15 06:50 1 4,4'-DDE 0.051 U 0.051 0.0075 ug/L 10/26/15 16:51 10/29/15 06:50 1 4,4'-DDT 0.051 U 0.051 0.0086 ug/L 10/26/15 16:51 10/29/15 06:50 1 delta-BHC 0.051 U 0.051 0.013 ug/L 10/26/15 16:51 10/29/15 06:50 1 Dieldrin 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 06:50 1 Endosulfan I 0.051 U 0.051 0.0083 ug/L 10/26/15 16:51 10/29/15 06:50 1 Endosulfan II 0.051 U 0.051 0.0086 ug/L 10/26/15 16:51 10/29/15 06:50 1 Endosulfan sulfate 0.051 U 0.051 0.0084 ug/L 10/26/15 16:51 10/29/15 06:50 1 Endrin 0.051 U 0.051 0.0089 ug/L 10/26/15 16:51 10/29/15 06:50 1 Endrin aldehyde 0.051 U 0.051 0.017 ug/L 10/26/15 16:51 10/29/15 06:50 1 Endrin ketone 0.051 U 0.051 0.0090 ug/L 10/26/15 16:51 10/29/15 06:50 1 gamma-BHC(Lindane) 0.051 U 0.051 0.0084 ug/L 10/26/15 16:51 10/29/15 06:50 1 gamma-Chlordane 0.051 U 0.051 0.0086 ug/L 10/26/15 16:51 10/29/15 06:50 1 Heptachlor 0.051 U 0.051 0.0080 ug/L 10/26/15 16:51 10/29/15 06:50 1 Heptachlor epoxide 0.051 U 0.051 0.0082 ug/L 10/26/15 16:51 10/29/15 06:50 1 Methoxychlor 0.051 U 0.051 0.0094 ug/L 10/26/15 16:51 10/29/15 06:50 1 Toxaphene 5.1 U 5.1 0.19 ug/L 10/26/15 16:51 10/29/15 06:50 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 48 10-130 10/26/15 16:51 10/29/15 06:50 1 Tetrachloro-m-xylene 67 39-130 10/26/15 16:51 10/29/15 06:50 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.2 U 2.2 2.2 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 13 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-07 Lab Sample ID: 680-118203-8 Date Collected: 10/21/15 13:19 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.054 U 0.054 0.0078 ug/L 10/27/15 16:05 10/29/15 12:47 1 alpha-BHC 0.0086 J 0.054 0.0084 ug/L 10/27/15 16:05 10/29/15 12:47 1 alpha-Chlordane 0.054 U 0.054 0.011 ug/L 10/27/15 16:05 10/29/15 12:47 1 beta-BHC 0.016 J p 0.054 0.013 ug/L 10/27/15 16:05 10/29/15 12:47 1 4,4'-DDD 0.054 U 0.054 0.0083 ug/L 10/27/15 16:05 10/29/15 12:47 1 4,4'-DDE 0.054 U 0.054 0.0080 ug/L 10/27/15 16:05 10/29/15 12:47 1 4,4'-DDT 0.054 U 0.054 0.0091 ug/L 10/27/15 16:05 10/29/15 12:47 1 delta-BHC 0.054 U 0.054 0.014 ug/L 10/27/15 16:05 10/29/15 12:47 1 Dieldrin 0.054 U 0.054 0.0092 ug/L 10/27/15 16:05 10/29/15 12:47 1 Endosulfan I 0.054 U 0.054 0.0088 ug/L 10/27/15 16:05 10/29/15 12:47 1 Endosulfan II 0.054 U 0.054 0.0091 ug/L 10/27/15 16:05 10/29/15 12:47 1 Endosulfan sulfate 0.054 U 0.054 0.0089 ug/L 10/27/15 16:05 10/29/15 12:47 1 Endrin 0.054 U 0.054 0.0095 ug/L 10/27/15 16:05 10/29/15 12:47 1 Endrin aldehyde 0.054 U 0.054 0.018 ug/L 10/27/15 16:05 10/29/15 12:47 1 Endrin ketone 0.054 U 0.054 0.0096 ug/L 10/27/15 16:05 10/29/15 12:47 1 gamma-BHC(Lindane) 0.054 U 0.054 0.0089 ug/L 10/27/15 16:05 10/29/15 12:47 1 gamma-Chlordane 0.054 U 0.054 0.0091 ug/L 10/27/15 16:05 10/29/15 12:47 1 Heptachlor 0.054 U 0.054 0.0085 ug/L 10/27/15 16:05 10/29/15 12:47 1 Heptachlor epoxide 0.054 U 0.054 0.0087 ug/L 10/27/15 16:05 10/29/15 12:47 1 Methoxychlor 0.054 U 0.054 0.010 ug/L 10/27/15 16:05 10/29/15 12:47 1 Toxaphene 5.4 U 5.4 0.20 ug/L 10/27/15 16:05 10/29/15 12:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 36 10-130 10/27/15 16:05 10/29/15 12:47 1 Tetrachloro-m-xylene 62 39-130 10/27/15 16:05 10/29/15 12:47 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.0 U 2.0 2.0 mg/L 10/26/15 15:13 1 TestAmerica Savannah Page 14 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-08 Lab Sample ID: 680-118203-9 Date Collected: 10/21/15 13:39 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A -Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 13:01 1 alpha-BHC 0.049 U 0.049 0.0077 ug/L 10/27/15 16:05 10/29/15 13:01 1 alpha-Chlordane 0.049 U 0.049 0.0099 ug/L 10/27/15 16:05 10/29/15 13:01 1 beta-BHC 0.013 J p 0.049 0.012 ug/L 10/27/15 16:05 10/29/15 13:01 1 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 13:01 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/27/15 16:05 10/29/15 13:01 1 4,4'-DDT 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 13:01 1 delta-BHC 0.049 U 0.049 0.013 ug/L 10/27/15 16:05 10/29/15 13:01 1 Dieldrin 0.049 U 0.049 0.0085 ug/L 10/27/15 16:05 10/29/15 13:01 1 Endosulfan I 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 13:01 1 Endosulfan II 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 13:01 1 Endosulfan sulfate 0.049 U 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 13:01 1 Endrin 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 13:01 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 13:01 1 Endrin ketone 0.049 U 0.049 0.0088 ug/L 10/27/15 16:05 10/29/15 13:01 1 gamma-BHC(Lindane) 0.049 U 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 13:01 1 gamma-Chlordane 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 13:01 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/27/15 16:05 10/29/15 13:01 1 Heptachlor epoxide 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 13:01 1 Methoxychlor 0.049 U 0.049 0.0092 ug/L 10/27/15 16:05 10/29/15 13:01 1 Toxaphene 4.9 U 4.9 0.19 ug/L 10/27/15 16:05 10/29/15 13:01 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 38 10-130 10/27/15 16:05 10/29/15 13:01 1 Tetrachloro-m-xylene 62 39-130 10/27/15 16:05 10/29/15 13:01 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.9 1.0 1.0 mg/L 10/27/15 11:02 1 TestAmerica Savannah Page 15 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-09 Lab Sample ID: 680-118203-10 Date Collected: 10/21/15 13:52 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A -Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1 Aldrin 0.049 U 0.049 0.0071 ug/L 10/27/15 16:05 10/29/15 13:16 1 alpha-BHC 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 13:16 1 alpha-Chlordane 0.049 U 0.049 0.0097 ug/L 10/27/15 16:05 10/29/15 13:16 1 beta-BHC 0.049 U 0.049 0.012 ug/L 10/27/15 16:05 10/29/15 13:16 1 4,4'-DDD 0.049 U 0.049 0.0075 ug/L 10/27/15 16:05 10/29/15 13:16 1 4,4'-DDE 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 13:16 1 4,4'-DDT 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 13:16 1 I delta-BHC 0.049 U 0.049 0.013 ug/L 10/27/15 16:05 10/29/15 13:16 1 Dieldrin 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 13:16 1 Endosulfan I 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 13:16 1 Endosulfan II 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 13:16 1 Endosulfan sulfate 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 13:16 1 Endrin 0.049 U 0.049 0.0086 ug/L 10/27/15 16:05 10/29/15 13:16 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 13:16 1 Endrin ketone 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 13:16 1 gamma-BHC(Lindane) 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 13:16 1 gamma-Chlordane 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 13:16 1 Heptachlor 0.049 U 0.049 0.0077 ug/L 10/27/15 16:05 10/29/15 13:16 1 Heptachlor epoxide 0.049 U 0.049 0.0079 ug/L 10/27/15 16:05 10/29/15 13:16 1 Methoxychlor 0.049 U 0.049 0.0091 ug/L 10/27/15 16:05 10/29/15 13:16 1 Toxaphene 4.9 U 4.9 0.19 ug/L 10/27/15 16:05 10/29/15 13:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 38 10-130 10/27/15 16:05 10/29/15 13:16 1 Tetrachloro-m-xylene 63 39-130 10/27/15 16:05 10/29/15 13:16 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 1.7 1.0 1.0 mg/L 10/27/15 11:02 1 TestAmerica Savannah Page 16 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW Duplicate Lab Sample ID: 680-118203-11 Date Collected: 10/21/15 13:26 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.055 U 0.055 0.0080 ug/L 10/27/15 16:05 10/29/15 13:30 1 alpha-BHC 0.055 U 0.055 0.0086 ug/L 10/27/15 16:05 10/29/15 13:30 1 alpha-Chlordane 0.055 U 0.055 0.011 ug/L 10/27/15 16:05 10/29/15 13:30 1 beta-BHC 0.055 U 0.055 0.013 ug/L 10/27/15 16:05 10/29/15 13:30 1 4,4'-DDD 0.055 U 0.055 0.0085 ug/L 10/27/15 16:05 10/29/15 13:30 1 4,4'-DDE 0.055 U 0.055 0.0081 ug/L 10/27/15 16:05 10/29/15 13:30 1 4,4'-DDT 0.055 U 0.055 0.0093 ug/L 10/27/15 16:05 10/29/15 13:30 1 delta-BHC 0.055 U 0.055 0.014 ug/L 10/27/15 16:05 10/29/15 13:30 1 Dieldrin 0.055 U 0.055 0.0094 ug/L 10/27/15 16:05 10/29/15 13:30 1 Endosulfan I 0.055 U 0.055 0.0090 ug/L 10/27/15 16:05 10/29/15 13:30 1 Endosulfan II 0.055 U 0.055 0.0093 ug/L 10/27/15 16:05 10/29/15 13:30 1 Endosulfan sulfate 0.055 U 0.055 0.0091 ug/L 10/27/15 16:05 10/29/15 13:30 1 Endrin 0.055 U 0.055 0.0097 ug/L 10/27/15 16:05 10/29/15 13:30 1 Endrin aldehyde 0.055 U 0.055 0.019 ug/L 10/27/15 16:05 10/29/15 13:30 1 Endrin ketone 0.055 U 0.055 0.0098 ug/L 10/27/15 16:05 10/29/15 13:30 1 gamma-BHC(Lindane) 0.055 U 0.055 0.0091 ug/L 10/27/15 16:05 10/29/15 13:30 1 gamma-Chlordane 0.055 U 0.055 0.0093 ug/L 10/27/15 16:05 10/29/15 13:30 1 Heptachlor 0.055 U 0.055 0.0087 ug/L 10/27/15 16:05 10/29/15 13:30 1 Heptachlor epoxide 0.055 U 0.055 0.0089 ug/L 10/27/15 16:05 10/29/15 13:30 1 Methoxychlor 0.055 U 0.055 0.010 ug/L 10/27/15 16:05 10/29/15 13:30 1 Toxaphene 5.5 U 5.5 0.21 ug/L 10/27/15 16:05 10/29/15 13:30 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 35 10-130 10/27/15 16:05 10/29/15 13:30 1 Tetrachloro-m-xylene 63 39-130 10/27/15 16:05 10/29/15 13:30 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 2.1 2.1 2.1 mg/L 10/27/15 11:02 1 TestAmerica Savannah Page 17 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Influent Lab Sample ID: 680-118203-12 Date Collected: 10/21/15 14:32 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260E-Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.1 1.0 0.48 ug/L 10/27/15 13:18 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac ill Toluene-d8(Sun) 103 70-130 10/27/15 13:18 1 1,2-Dichloroethane-d4(Surr) 107 70-130 10/27/15 13:18 1 Dibromofluoromethane(Surr) 110 70-130 10/27/15 13:18 1 4-Bromofluorobenzene(Surr) 101 70-130 10/27/15 13:18 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 21:51 1 alpha-BHC 0.077 0.049 0.0077 ug/L 10/27/15 16:05 10/29/15 21:51 1 alpha-Chlordane 0.049 U 0.049 0.0098 ug/L 10/27/15 16:05 10/29/15 21:51 1 beta-BHC 3.2 0.25 0.059 ug/L 10/27/15 16:05 10/29/15 22:06 5 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 21:51 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/27/15 16:05 10/29/15 21:51 1 4,4'-DDT 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 21:51 1 delta-BHC 0.63 0.049 0.013 ug/L 10/27/15 16:05 10/29/15 21:51 1 Dieldrin 0.24 0.049 0.0085 ug/L 10/27/15 16:05 10/29/15 21:51 1 Endosulfan I 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 21:51 1 Endosulfan II 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 21:51 1 Endosulfan sulfate 0.025 J p 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 21:51 1 Endrin 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 21:51 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 21:51 1 Endrin ketone 0.19 0.049 0.0088 ug/L 10/27/15 16:05 10/29/15 21:51 1 gamma-BHC(Lindane) 0.056 p 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 21:51 1 gamma-Chlordane 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 21:51 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/27/15 16:05 10/29/15 21:51 1 Heptachlor epoxide 0.031 J p 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 21:51 1 Methoxychlor 0.049 U 0.049 0.0092 ug/L 10/27/15 16:05 10/29/15 21:51 1 Toxaphene 5.0 4.9 0.19 ug/L 10/27/15 16:05 10/29/15 21:51 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobipheny! 59 10-130 10/27/15 16:05 10/29/15 21:51 1 Tetrachloro-m-xylene 56 39-130 10/27/15 16:05 10/29/15 21:51 1 TestAmerica Savannah Page 18 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Effluent Lab Sample ID: 680-118203-13 Date Collected: 10/21/15 14:38 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260E-Volatile Organic Compounds(GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 13:40 1 i Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac il Toluene-d8(Surr) 101 70-130 10/27/15 13:40 1 1,2-Dichloroethane-d4(Sun-) 107 70-130 10/27/15 13:40 1 Dibromofluoromethane(Sun-) 110 70-130 10/27/15 13:40 1 4-Bromofluorobenzene(Surr) 99 70-130 10/27/15 13:40 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 13:45 1 alpha-BHC 0.049 U 0.049 0.0077 ug/L 10/27/15 16:05 10/29/15 13:45 1 alpha-Chlordane 0.049 U 0.049 0.0099 ug/L 10/27/15 16:05 10/29/15 13:45 1 beta-BHC 0.017 J 0.049 0.012 ug/L 10/27/15 16:05 10/29/15 13:45 1 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 13:45 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/27/15 16:05 10/29/15 13:45 1 4,4'-DDT 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 13:45 1 delta-BHC 0.049 U 0.049 0.013 ug/L 10/27/15 16:05 10/29/15 13:45 1 Dieldrin 0.049 U 0.049 0.0085 ug/L 10/27/15 16:05 10/29/15 13:45 1 Endosulfan I 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 13:45 1 Endosulfan II 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 13:45 1 Endosulfan sulfate 0.049 U 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 13:45 1 Endrin 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 13:45 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 13:45 1 Endrin ketone 0.049 U 0.049 0.0088 ug/L 10/27/15 16:05 10/29/15 13:45 1 gamma-BHC(Lindane) 0.049 U 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 13:45 1 gamma-Chlordane 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 13:45 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/27/15 16:05 10/29/15 13:45 1 Heptachlor epoxide 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 13:45 1 Methoxychlor 0.049 U 0.049 0.0092 ug/L 10/27/15 16:05 10/29/15 13:45 1 Toxaphene 4.9 U 4.9 0.19 ug/L 10/27/15 16:05 10/29/15 13:45 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 59 10-130 10/27/15 16:05 10/29/15 13:45 1 Tetrachloro-m-xylene 53 39-130 10/27/15 16:05 10/29/15 13:45 1 TestAmerica Savannah Page 19 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Carbon Train A-1 Lab Sample ID: 680-118203-14 Date Collected: 10/21/15 14:47 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B -Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 14:01 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac IIII Toluene-d8(Surr) 103 70-130 10/27/15 14:01 1 1,2-Dichloroethane-d4(Surr) 107 70-130 10/27/15 14:01 1 Dibromofluoromethane(Surr) 109 70-130 10/27/15 14:01 1 4-Bromofluorobenzene(Surr) 98 70-130 10/27/15 14:01 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.048 U 0.048 0.0071 ug/L 10/27/15 16:05 10/29/15 13:59 1 alpha-BHC 0.048 U 0.048 0.0075 ug/L 10/27/15 16:05 10/29/15 13:59 1 alpha-Chlordane 0.048 U 0.048 0.0097 ug/L 10/27/15 16:05 10/29/15 13:59 1 beta-BHC 0.048 U 0.048 0.012 ug/L 10/27/15 16:05 10/29/15 13:59 1 4,4'-DDD 0.048 U 0.048 0.0074 ug/L 10/27/15 16:05 10/29/15 13:59 1 4,4'-DDE 0.048 U 0.048 0.0072 ug/L 10/27/15 16:05 10/29/15 13:59 1 4,4'-DDT 0.048 U 0.048 0.0082 ug/L 10/27/15 16:05 10/29/15 13:59 1 delta-BHC 0.048 U 0.048 0.013 ug/L 10/27/15 16:05 10/29/15 13:59 1 Dieldrin 0.048 U 0.048 0.0083 ug/L 10/27/15 16:05 10/29/15 13:59 1 Endosulfan I 0.048 U 0.048 0.0079 ug/L 10/27/15 16:05 10/29/15 13:59 1 Endosulfan II 0.048 U 0.048 0.0082 ug/L 10/27/15 16:05 10/29/15 13:59 1 Endosulfan sulfate 0.048 U 0.048 0.0080 ug/L 10/27/15 16:05 10/29/15 13:59 1 Endrin 0.048 U 0.048 0.0085 ug/L 10/27/15 16:05 10/29/15 13:59 1 Endrin aldehyde 0.048 U 0.048 0.016 ug/L 10/27/15 16:05 10/29/15 13:59 1 Endrin ketone 0.048 U 0.048 0.0086 ug/L 10/27/15 16:05 10/29/15 13:59 1 gamma-BHC(Lindane) 0.048 U 0.048 0.0080 ug/L 10/27/15 16:05 10/29/15 13:59 1 gamma-Chlordane 0.048 U 0.048 0.0082 ug/L 10/27/15 16:05 10/29/15 13:59 1 Heptachlor 0.048 U 0.048 0.0076 ug/L 10/27/15 16:05 10/29/15 13:59 1 Heptachlor epoxide 0.048 U 0.048 0.0078 ug/L 10/27/15 16:05 10/29/15 13:59 1 Methoxychlor 0.048 U 0.048 0.0090 ug/L 10/27/15 16:05 10/29/15 13:59 1 Toxaphene 4.8 U 4.8 0.18 ug/L 10/27/15 16:05 10/29/15 13:59 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 50 10-130 10/27/15 16:05 10/29/15 13:59 1 Tetrachloro-m-xylene 60 39-130 10/27/15 16:05 10/29/15 13:59 1 TestAmerica Savannah Page 20 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Carbon Train B-2 Lab Sample ID: 680-118203-15 Date Collected: 10/21/15 15:03 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B-Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 14:23 1 i Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac la Toluene-d8(Surr) 103 70-130 1027/15 14:23 1 1,2-Dichloroethane-d4(Surr) 107 70-130 1027/15 14:23 1 Dibromofluoromethane(Surr) 109 70-130 1027/15 14:23 1 4-Bromofluorobenzene(Surr) 101 70-130 1027/15 14:23 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 14:14 1 alpha-BHC 0.049 U 0.049 0.0077 ug/L 10/27/15 16:05 10/29/15 14:14 1 alpha-Chlordane 0.049 U 0.049 0.0098 ug/L 10/27/15 16:05 10/29/15 14:14 1 beta-BHC 0.049 U 0.049 0.012 ug/L 10/27/15 16:05 10/29/15 14:14 1 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 14:14 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/27/15 16:05 10/29/15 14:14 1 4,4'-DDT 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 14:14 1 delta-BHC 0.049 U 0.049 0.013 ug/L 10/27/15 16:05 10/29/15 14:14 1 Dieldrin 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 14:14 1 Endosulfan I 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 14:14 1 Endosulfan II 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 14:14 1 Endosulfan sulfate 0.049 U 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 14:14 1 Endrin 0.049 U 0.049 0.0086 ug/L 10/27/15 16:05 10/29/15 14:14 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 14:14 1 Endrin ketone 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 14:14 1 gamma-BHC(Lindane) 0.049 U 0.049 0.0082 ug/L 10/27/15 16:05 10/29/15 14:14 1 gamma-Chlordane 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 14:14 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/27/15 16:05 10/29/15 14:14 1 Heptachlor epoxide 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 14:14 1 Methoxychlor 0.049 U 0.049 0.0091 ug/L 10/27/15 16:05 10/29/15 14:14 1 Toxaphene 4.9 U 4.9 0.19 ug/L 10/27/15 16:05 10/29/15 14:14 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 58 10-130 1027/15 16:05 1029/15 14:14 1 Tetrachloro-m-xylene 70 39-130 1027/15 16:05 1029/15 14:14 1 TestAmerica Savannah Page 21 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-30D Lab Sample ID: 680-118203-17 Date Collected: 10/21/15 10:50 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260E -Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 14:44 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 111 Toluene-d8(Sun-) 100 70-130 1027/15 14:44 1 1,2-Dichloroethane-d4(Surr) 107 70-130 1027/15 14:44 1 Dibromofluoromethane(Sun) 111 70-130 1027/15 14:44 1 4-Bromofluorobenzene(Sun) 101 70-130 1027/15 14:44 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0072 ug/L 10/27/15 16:05 10/29/15 22:20 1 alpha-BHC 0.081 0.050 0.0077 ug/L 10/27/15 16:05 10/29/15 22:20 1 alpha-Chlordane 0.050 U 0.050 0.0099 ug/L 10/27/15 16:05 10/29/15 22:20 1 beta-BHC 1.7 0.50 0.12 ug/L 10/27/15 16:05 10/29/15 22:35 10 4,4'-DDD 0.050 U 0.050 0.0076 ug/L 10/27/15 16:05 10/29/15 22:20 1 4,4'-DDE 0.050 U 0.050 0.0073 ug/L 10/27/15 16:05 10/29/15 22:20 1 4,4'-DDT 0.050 U 0.050 0.0084 ug/L 10/27/15 16:05 10/29/15 22:20 1 delta-BHC 0.27 0.050 0.013 ug/L 10/27/15 16:05 10/29/15 22:20 1 Dieldrin 0.17 0.050 0.0085 ug/L 10/27/15 16:05 10/29/15 22:20 1 Endosulfan I 0.050 U 0.050 0.0081 ug/L 10/27/15 16:05 10/29/15 22:20 1 Endosulfan II 0.050 U 0.050 0.0084 ug/L 10/27/15 16:05 10/29/15 22:20 1 Endosulfan sulfate 0.017 J p 0.050 0.0082 ug/L 10/27/15 16:05 10/29/15 22:20 1 Endrin 0.050 U 0.050 0.0087 ug/L 10/27/15 16:05 10/29/15 22:20 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/27/15 16:05 10/29/15 22:20 1 Endrin ketone 0.17 0.050 0.0088 ug/L 10/27/15 16:05 10/29/15 22:20 1 gamma-BHC(Lindane) 0.067 0.050 0.0082 ug/L 10/27/15 16:05 10/29/15 22:20 1 gamma-Chlordane 0.050 U 0.050 0.0084 ug/L 10/27/15 16:05 10/29/15 22:20 1 Heptachlor 0.050 U 0.050 0.0078 ug/L 10/27/15 16:05 10/29/15 22:20 1 Heptachlor epoxide 0.019 J p 0.050 0.0080 ug/L 10/27/15 16:05 10/29/15 22:20 1 Methoxychlor 0.050 U 0.050 0.0092 ug/L 10/27/15 16:05 10/29/15 22:20 1 Toxaphene 2.6 J 5.0 0.19 ug/L 10/27/15 16:05 10/29/15 22:20 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 62 10-130 1027/15 16:05 1029/15 22:20 1 Tetrachloro-m-xylene 57 39-130 1027/15 16:05 1029/15 22:20 1 TestAmerica Savannah Page 22 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: PZ-2 Lab Sample ID: 680-118203-18 Date Collected: 10/21/15 13:30 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.053 U 0.053 0.0077 ug/L 10/27/15 16:05 10/29/15 14:28 1 alpha-BHC 0.31 0.053 0.0082 ug/L 10/27/15 16:05 10/29/15 14:28 1 alpha-Chlordane 0.053 U 0.053 0.011 ug/L 10/27/15 16:05 10/29/15 14:28 1 beta-BHC 0.17 0.053 0.013 ug/L 10/27/15 16:05 10/29/15 14:28 1 4,4'-DDD 0.053 U 0.053 0.0081 ug/L 10/27/15 16:05 10/29/15 14:28 1 4,4'-DDE 0.053 U 0.053 0.0078 ug/L 10/27/15 16:05 10/29/15 14:28 1 4,4'-DDT 0.053 U 0.053 0.0090 ug/L 10/27/15 16:05 10/29/15 14:28 1 delta-BHC 0.23 0.053 0.014 ug/L 10/27/15 16:05 10/29/15 14:28 1 Dieldrin 0.011 J 0.053 0.0091 ug/L 10/27/15 16:05 10/29/15 14:28 1 Endosulfan I 0.053 U 0.053 0.0087 ug/L 10/27/15 16:05 10/29/15 14:28 1 Endosulfan II 0.053 U 0.053 0.0090 ug/L 10/27/15 16:05 10/29/15 14:28 1 Endosulfan sulfate 0.053 U 0.053 0.0088 ug/L 10/27/15 16:05 10/29/15 14:28 1 Endrin 0.053 U 0.053 0.0093 ug/L 10/27/15 16:05 10/29/15 14:28 1 Endrin aldehyde 0.053 U 0.053 0.018 ug/L 10/27/15 16:05 10/29/15 14:28 1 Endrin ketone 0.053 U 0.053 0.0094 ug/L 10/27/15 16:05 10/29/15 14:28 1 gamma-BHC(Lindane) 0.20 0.053 0.0088 ug/L 10/27/15 16:05 10/29/15 14:28 1 gamma-Chlordane 0.053 U 0.053 0.0090 ug/L 10/27/15 16:05 10/29/15 14:28 1 Heptachlor 0.053 U 0.053 0.0083 ug/L 10/27/15 16:05 10/29/15 14:28 1 Heptachlor epoxide 0.053 U 0.053 0.0086 ug/L 10/27/15 16:05 10/29/15 14:28 1 Methoxychlor 0.053 U 0.053 0.0098 ug/L 10/27/15 16:05 10/29/15 14:28 1 Toxaphene 5.3 U 5.3 0.20 ug/L 10/27/15 16:05 10/29/15 14:28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 57 10-130 10/27/15 16:05 10/29/15 14:28 1 Tetrachloro-m-xy/ene 67 39-130 10/27/15 16:05 10/29/15 14:28 1 TestAmerica Savannah Page 23 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: PZ-3 Lab Sample ID: 680-118203-19 Date Collected: 10/21/15 12:50 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.052 U 0.052 0.0076 ug/L 10/27/15 16:05 10/29/15 19:55 1 alpha-BHC 0.25 0.052 0.0081 ug/L 10/27/15 16:05 10/29/15 19:55 1 alpha-Chlordane 0.052 U 0.052 0.010 ug/L 10/27/15 16:05 10/29/15 19:55 1 beta-BHC 0.088 0.052 0.013 ug/L 10/27/15 16:05 10/29/15 19:55 1 4,4'-DDD 0.052 U 0.052 0.0080 ug/L 10/27/15 16:05 10/29/15 19:55 1 4,4'-DDE 0.052 U 0.052 0.0077 ug/L 10/27/15 16:05 10/29/15 19:55 1 4,4'-DDT 0.052 U 0.052 0.0089 ug/L 10/27/15 16:05 10/29/15 19:55 1 delta-BHC 0.15 0.052 0.014 ug/L 10/27/15 16:05 10/29/15 19:55 1 Dieldrin 0.052 U 0.052 0.0090 ug/L 10/27/15 16:05 10/29/15 19:55 1 Endosulfan I 0.052 U 0.052 0.0085 ug/L 10/27/15 16:05 10/29/15 19:55 1 Endosulfan II 0.052 U 0.052 0.0089 ug/L 10/27/15 16:05 10/29/15 19:55 1 Endosulfan sulfate 0.052 U 0.052 0.0086 ug/L 10/27/15 16:05 10/29/15 19:55 1 Endrin 0.052 U 0.052 0.0092 ug/L 10/27/15 16:05 10/29/15 19:55 1 Endrin aldehyde 0.052 U 0.052 0.018 ug/L 10/27/15 16:05 10/29/15 19:55 1 Endrin ketone 0.052 U 0.052 0.0093 ug/L 10/27/15 16:05 10/29/15 19:55 1 gamma-BHC(Lindane) 0.17 0.052 0.0086 ug/L 10/27/15 16:05 10/29/15 19:55 1 gamma-Chlordane 0.052 U 0.052 0.0089 ug/L 10/27/15 16:05 10/29/15 19:55 1 Heptachlor 0.052 U 0.052 0.0082 ug/L 10/27/15 16:05 10/29/15 19:55 1 Heptachlor epoxide 0.052 U 0.052 0.0084 ug/L 10/27/15 16:05 10/29/15 19:55 1 Methoxychlor 0.052 U 0.052 0.0097 ug/L 10/27/15 16:05 10/29/15 19:55 1 Toxaphene 5.2 U 5.2 0.20 ug/L 10/27/15 16:05 10/29/15 19:55 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 46 10-130 10/27/15 16:05 1029/15 19:55 1 Tetrachloro-m-xylene 67 39-130 1027/15 16:05 10/29/15 19:55 1 TestAmerica Savannah Page 24 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-27L Lab Sample ID: 680-118203-20 Date Collected: 10/21/15 12:00 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Di!Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/27/15 16:05 10/30/15 10:42 1 alpha-BHC 0.92 0.20 0.031 ug/L 10/27/15 16:05 10/30/15 10:56 4111 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/27/15 16:05 10/30/15 10:42 1 beta-BHC 2.0 0.20 0.048 ug/L 10/27/15 16:05 10/30/15 10:56 4 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/27/15 16:05 10/30/15 10:42 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/27/15 16:05 10/30/15 10:42 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/30/15 10:42 1 delta-BHC 2.1 0.20 0.052 ug/L 10/27/15 16:05 10/30/15 10:56 4 Dieldrin 0.10 0.050 0.0086 ug/L 10/27/15 16:05 10/30/15 10:42 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/27/15 16:05 10/30/15 10:42 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/30/15 10:42 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/27/15 16:05 10/30/15 10:42 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/27/15 16:05 10/30/15 10:42 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/27/15 16:05 10/30/15 10:42 1 Endrin ketone 0.18 0.050 0.0089 uglL 10/27/15 16:05 10/30/15 10:42 1 gamma-BHC(Lindane) 0.17 0.050 0.0083 ug/L 10/27/15 16:05 10/30/15 10:42 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/30/15 10:42 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/27/15 16:05 10/30/15 10:42 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/27/15 16:05 10/30/15 10:42 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/27/15 16:05 10/30/15 10:42 1 Toxaphene 0.89 J p 5.0 0.19 ug/L 10/27/15 16:05 10/30/15 10:42 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 63 10-130 1027/15 16:05 10/30/15 10:42 1 Tetrachloro-m-xylene 68 39-130 1027/15 16:05 10/30/15 10:42 1 TestAmerica Savannah Page 25 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-36L Lab Sample ID: 680-118203-21 Date Collected: 10/21/15 10:59 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0071 ug/L 10/27/15 16:05 10/29/15 20:10 1 alpha-BHC 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 20:10 1 alpha-Chlordane 0.049 U 0.049 0.0097 ug/L 10/27/15 16:05 10/29/15 20:10 1 beta-BHC 0.049 U 0.049 0.012 ug/L 10/27/15 16:05 10/29/15 20:10 1 4,4'-DDD 0.049 U 0.049 0.0075 ug/L 10/27/15 16:05 10/29/15 20:10 1 4,4'-DDE 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 20:10 1 4,4'-DDT 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 20:10 1 delta-BHC 0.049 U 0.049 0.013 ug/L 10/27/15 16:05 10/29/15 20:10 1 Dieldrin 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 20:10 1 Endosulfan I 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 20:10 1 Endosulfan II 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 20:10 1 Endosulfan sulfate 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 20:10 1 Endrin 0.049 U 0.049 0.0086 ug/L 10/27/15 16:05 10/29/15 20:10 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 20:10 1 Endrin ketone 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 20:10 1 gamma-BHC(Lindane) 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 20:10 1 gamma-Chlordane 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 20:10 1 Heptachlor 0.049 U 0.049 0.0077 ug/L 10/27/15 16:05 10/29/15 20:10 1 Heptachlor epoxide 0.049 U 0.049 0.0079 ug/L 10/27/15 16:05 10/29/15 20:10 1 Methoxychlor 0.049 U 0.049 0.0090 ug/L 10/27/15 16:05 10/29/15 20:10 1 Toxaphene 4.9 U 4.9 0.18 ug/L 10/27/15 16:05 10/29/15 20:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 64 10-130 10/27/15 16:05 10/29/15 20:10 1 Tetrachloro-m-xylene 67 39-130 10/27/15 16:05 10/29/15 20:10 1 TestAmerica Savannah Page 26 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-18D Lab Sample ID: 680-118203-22 Date Collected: 10/21/15 11:49 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B -Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.9 1.0 0.48 ug/L 10/27/15 15:06 1 1 mil Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Sun-) 104 70-130 10/27/15 15:06 1 1,2-Dichloroethane-d4(Sun) 107 70-130 10/27/15 15:06 1 Dibromofluoromethane(Sun) 111 70-130 10/27/15 15:06 1 4-8romofluorobenzene(Sun) 100 70-130 10/27/15 15:06 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/27/15 16:05 10/30/15 14:47 1 alpha-BHC 0.098 0.050 0.0078 ug/L 10/27/15 16:05 10/30/15 14:47 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/27/15 16:05 10/30/15 14:47 1 beta-BHC 1.5 0.50 0.12 ug/L 10/27/15 16:05 10/30/15 15:02 10 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/27/15 16:05 10/30/15 14:47 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/27/15 16:05 10/30/15 14:47 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/30/15 14:47 1 delta-BHC 0.39 0.050 0.013 ug/L 10/27/15 16:05 10/30/15 14:47 1 Dieldrin 0.26 0.050 0.0086 ug/L 10/27/15 16:05 10/30/15 14:47 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/27/15 16:05 10/30/15 14:47 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/30/15 14:47 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/27/15 16:05 10/30/15 14:47 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/27/15 16:05 10/30/15 14:47 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/27/15 16:05 10/30/15 14:47 1 Endrin ketone 0.16 0.050 0.0089 ug/L 10/27/15 16:05 10/30/15 14:47 1 gamma-BHC(Lindane) 0.10 0.050 0.0083 ug/L 10/27/15 16:05 10/30/15 14:47 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/30/15 14:47 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/27/15 16:05 10/30/15 14:47 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/27/15 16:05 10/30/15 14:47 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/27/15 16:05 10/30/15 14:47 1 Toxaphene 4.5 J 5.0 0.19 ug/L 10/27/15 16:05 10/30/15 14:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 66 10-130 10/27/15 16:05 10/30/15 14:47 1 Tetrachloro-m-xylene 64 39-130 10/27/15 16:05 10/30/15 14:47 1 TestAmerica Savannah Page 27 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-39L Lab Sample ID: 680-118203-23 Date Collected: 10/21/15 14:12 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0075 ug/L 10/27/15 16:05 10/29/15 20:24 1 alpha-BHC 0.051 U 0.051 0.0080 ug/L 10/27/15 16:05 10/29/15 20:24 1II alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/27/15 16:05 10/29/15 20:24 1 beta-BHC 0.051 U 0.051 0.012 ug/L 10/27/15 16:05 10/29/15 20:24 1 4,4'-DDD 0.051 U 0.051 0.0079 ug/L 10/27/15 16:05 10/29/15 20:24 1 4,4'-DDE 0.051 U 0.051 0.0076 ug/L 10/27/15 16:05 10/29/15 20:24 1 4,4'-DDT 0.051 U 0.051 0.0087 ug/L 10/27/15 16:05 10/29/15 20:24 1 delta-BHC 0.051 U 0.051 0.013 ug/L 10/27/15 16:05 10/29/15 20:24 1 Dieldrin 0.051 U 0.051 0.0088 ug/L 10/27/15 16:05 10/29/15 20:24 1 Endosulfan I 0.051 U 0.051 0.0084 ug/L 10/27/15 16:05 10/29/15 20:24 1 Endosulfan II 0.051 U 0.051 0.0087 ug/L 10/27/15 16:05 10/29/15 20:24 1 Endosulfan sulfate 0.051 U 0.051 0.0085 ug/L 10/27/15 16:05 10/29/15 20:24 1 Endrin 0.051 U 0.051 0.0090 ug/L 10/27/15 16:05 10/29/15 20:24 1 Endrin aldehyde 0.051 U 0.051 0.017 ug/L 10/27/15 16:05 10/29/15 20:24 1 Endrin ketone 0.051 U 0.051 0.0091 ug/L 10/27/15 16:05 10/29/15 20:24 1 gamma-BHC(Lindane) 0.051 U 0.051 0.0085 ug/L 10/27/15 16:05 10/29/15 20:24 1 gamma-Chlordane 0.051 U 0.051 0.0087 ug/L 10/27/15 16:05 10/29/15 20:24 1 Heptachlor 0.051 U 0.051 0.0081 ug/L 10/27/15 16:05 10/29/15 20:24 1 Heptachlor epoxide 0.051 U 0.051 0.0083 ug/L 10/27/15 16:05 10/29/15 20:24 1 Methoxychlor 0.051 U 0.051 0.0096 ug/L 10/27/15 16:05 10/29/15 20:24 1 Toxaphene 5.1 U 5.1 0.20 ug/L 10/27/15 16:05 10/29/15 20:24 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decach/orobiphenyl 67 10-130 10/27/15 16:05 10/29/15 20:24 1 Tetrachloro-m-xylene 61 39-130 10/27/15 16:05 10/29/15 20:24 1 TestAmerica Savannah Page 28 of 81 Client Sample Results 1 Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 I Project/Site: Geigy Chemical Corp. Client Sample ID: MW-31L Lab Sample ID: 680-118203-24 Date Collected: 10/21/15 14:16 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.048 U 0.048 0.0071 ug/L 10/27/15 16:05 10/30/15 15:18 1 1 alpha-BHC 0.40 0.048 0.0075 ug/L 10/27/15 16:05 10/30/15 15:18 1 INI alpha-Chlordane 0.048 U 0.048 0.0097 ug/L 10/27/15 16:05 10/30/15 15:18 1 beta-BHC 0.62 0.048 0.012 ug/L 10/27/15 16:05 10/30/15 15:18 1 4,4'-DDD 0.048 U 0.048 0.0075 ug/L 10/27/15 16:05 10/30/15 15:18 1 4,4'-DDE 0.048 U 0.048 0.0072 ug/L 10/27/15 16:05 10/30/15 15:18 1 4,4'-DDT 0.048 U 0.048 0.0082 ug/L 10/27/15 16:05 10/30/15 15:18 1 delta-BHC 0.86 0.19 0.050 ug/L 10/27/15 16:05 10/30/15 15:33 4 Dieldrin 0.028 J 0.048 0.0083 ug/L 10/27/15 16:05 10/30/15 15:18 1 Endosulfan I 0.048 U 0.048 0.0079 ug/L 10/27/15 16:05 10/30/15 15:18 1 Endosulfan II 0.048 U 0.048 0.0082 ug/L 10/27/15 16:05 10/30/15 15:18 1 Endosulfan sulfate 0.048 U 0.048 0.0080 ug/L 10/27/15 16:05 10/30/15 15:18 1 Endrin 0.048 U 0.048 0.0085 ug/L 10/27/15 16:05 10/30/15 15:18 1 Endrin aldehyde 0.048 U 0.048 0.016 ug/L 10/27/15 16:05 10/30/15 15:18 1 Endrin ketone 0.049 0.048 0.0086 ug/L 10/27/15 16:05 10/30/15 15:18 1 gamma-BHC(Lindane) 0.084 0.048 0.0080 ug/L 10/27/15 16:05 10/30/15 15:18 1 gamma-Chlordane 0.048 U 0.048 0.0082 ug/L 10/27/15 16:05 10/30/15 15:18 1 Heptachlor 0.048 U 0.048 0.0076 ug/L 10/27/15 16:05 10/30/15 15:18 1 Heptachlor epoxide 0.048 U 0.048 0.0078 ug/L 10/27/15 16:05 10/30/15 15:18 1 Methoxychlor 0.048 U 0.048 0.0090 ug/L 10/27/15 16:05 10/30/15 15:18 1 Toxaphene 0.22 J p 4.8 0.18 ug/L 10/27/15 16:05 10/30/15 15:18 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 65 10-130 10/27/15 16:05 10/30/15 15:18 1 Tetrachloro-m-xylene 68 39-130 10/27/15 16:05 10/30/15 15:18 1 TestAmerica Savannah Page 29 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Duplicate 2 Lab Sample ID: 680-118203-25 Date Collected: 10/21/15 10:50 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260E-Volatile Organic Compounds(GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 15:27 1 g Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac II Toluene-d8(Surr) 103 70-130 10/27/15 15:27 1 1,2-Dichloroethane-d4(Sun) 108 70-130 10/27/15 15:27 1 Dibromofluoromethane(Sun) 111 70-130 10/27/15 15:27 1 4-Bromofluorobenzene(Sun) 103 70-130 10/27/15 15:27 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/30/15 15:48 1 alpha-BHC 0.073 0.049 0.0077 ug/L 10/27/15 16:05 10/30/15 15:48 1 alpha-Chlordane 0.049 U 0.049 0.0099 ug/L 10/27/15 16:05 10/30/15 15:48 1 beta-BHC 1.7 0.20 0.047 ug/L 10/27/15 16:05 10/30/15 16:04 4 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/30/15 15:48 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/27/15 16:05 10/30/15 15:48 1 4,4'-DDT 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/30/15 15:48 1 delta-BHC 0.25 0.049 0.013 ug/L 10/27/15 16:05 10/30/15 15:48 1 Dieldrin 0.20 0.049 0.0085 ug/L 10/27/15 16:05 10/30/15 15:48 1 Endosulfan I 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/30/15 15:48 1 Endosulfan II 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/30/15 15:48 1 Endosulfan sulfate 0.049 U 0.049 0.0082 ug/L 10/27/15 16:05 10/30/15 15:48 1 Endrin 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/30/15 15:48 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/30/15 15:48 1 Endrin ketone 0.14 0.049 0.0088 ug/L 10/27/15 16:05 10/30/15 15:48 1 gamma-BHC(Lindane) 0.061 0.049 0.0082 ug/L 10/27/15 16:05 10/30/15 15:48 1 gamma-Chlordane 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/30/15 15:48 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/27/15 16:05 10/30/15 15:48 1 Heptachlor epoxide 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/30/15 15:48 1 Methoxychlor 0.049 U 0.049 0.0092 ug/L 10/27/15 16:05 10/30/15 15:48 1 Toxaphene 2.3 J 4.9 0.19 ug/L 10/27/15 16:05 10/30/15 15:48 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 65 10-130 10/27/15 16:05 10/30/15 15:48 1 Tetrachloro-m-xylene 63 39-130 10/27/15 16:05 10/30/15 15:48 1 TestAmerica Savannah Page 30 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-6S Lab Sample ID: 680-118203-26 Date Collected: 10/20/15 14:19 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A -Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/26/15 16:51 10/29/15 10:36 1 alpha-BHC 0.11 0.050 0.0078 ug/L 10/26/15 16:51 10/29/15 10:36 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/26/15 16:51 10/29/15 10:36 1 beta-BHC 7.3 1.3 0.30 ug/L 10/26/15 16:51 10/29/15 17:59 25 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/26/15 16:51 10/29/15 10:36 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/26/15 16:51 10/29/15 10:36 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 10:36 1 delta-BHC 1.7 0.50 0.13 ug/L 10/26/15 16:51 10/29/15 10:50 10 Dieldrin 0.43 0.050 0.0086 ug/L 10/26/15 16:51 10/29/15 10:36 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/26/15 16:51 10/29/15 10:36 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 10:36 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 10:36 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/26/15 16:51 10/29/15 10:36 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/26/15 16:51 10/29/15 10:36 1 Endrin ketone 0.39 0.050 0.0089 ug/L 10/26/15 16:51 10/29/15 10:36 1 gamma-BHC(Lindane) 0.30 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 10:36 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 10:36 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/26/15 16:51 10/29/15 10:36 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/26/15 16:51 10/29/15 10:36 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/26/15 16:51 10/29/15 10:36 1 Toxaphene 7.6 p 5.0 0.19 ug/L 10/26/15 16:51 10/29/15 10:36 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 60 10-130 10/26/15 16:51 10/29/15 10:36 1 Tetrachloro-m-xylene 69 39-130 10/26/15 16:51 10/29/15 10:36 1 TestAmerica Savannah Page 31 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Duplicate 1 Lab Sample ID: 680-118203-27 Date Collected: 10/20/15 15:04 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260E -Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 15:49 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac III Toluene-d8(Sun-) 102 70-130 10/27/15 15:49 1 1,2-Dichloroethane-d4(Surr) 109 70-130 10/27/15 15:49 1 Dibromofluoromethane(Surr) 110 70-130 10/27/15 15:49 1 4-Bromofluorobenzene(Surr) 99 70-130 10/27/15 15:49 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.048 U 0.048 0.0071 ug/L 10/26/15 16:51 10/29/15 11:05 1 alpha-BHC 0.048 U 0.048 0.0075 ug/L 10/26/15 16:51 10/29/15 11:05 1 alpha-Chlordane 0.048 U 0.048 0.0097 ug/L 10/26/15 16:51 10/29/15 11:05 1 beta-BHC 0.048 U 0.048 0.012 ug/L 10/26/15 16:51 10/29/15 11:05 1 4,4'-DDD 0.048 U 0.048 0.0074 ug/L 10/26/15 16:51 10/29/15 11:05 1 4,4'-DDE 0.048 U 0.048 0.0072 ug/L 10/26/15 16:51 10/29/15 11:05 1 4,4'-DDT 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 11:05 1 delta-BHC 0.048 U 0.048 0.013 ug/L 10/26/15 16:51 10/29/15 11:05 1 Dieldrin 0.048 U 0.048 0.0083 ug/L 10/26/15 16:51 10/29/15 11:05 1 Endosulfan I 0.048 U 0.048 0.0079 ug/L 10/26/15 16:51 10/29/15 11:05 1 Endosulfan II 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 11:05 1 Endosulfan sulfate 0.048 U 0.048 0.0080 ug/L 10/26/15 16:51 10/29/15 11:05 1 Endrin 0.048 U 0.048 0.0085 ug/L 10/26/15 16:51 10/29/15 11:05 1 Endrin aldehyde 0.048 U 0.048 0.016 ug/L 10/26/15 16:51 10/29/15 11:05 1 Endrin ketone 0.048 U 0.048 0.0086 ug/L 10/26/15 16:51 10/29/15 11:05 1 gamma-BHC(Lindane) 0.048 U 0.048 0.0080 ug/L 10/26/15 16:51 10/29/15 11:05 1 gamma-Chlordane 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 11:05 1 Heptachlor 0.048 U 0.048 0.0076 ug/L 10/26/15 16:51 10/29/15 11:05 1 Heptachlor epoxide 0.048 U 0.048 0.0078 ug/L 10/26/15 16:51 10/29/15 11:05 1 Methoxychlor 0.048 U 0.048 0.0090 ug/L 10/26/15 16:51 10/29/15 11:05 1 Toxaphene 4.8 U 4.8 0.18 ug/L 10/26/15 16:51 10/29/15 11:05 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 59 10-130 10/26/15 16:51 10/29/15 11:05 1 Tetrachloro-m-xylene 63 39-130 1026/15 16:51 10/29/15 11:05 1 TestAmerica Savannah Page 32 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-4S Lab Sample ID: 680-118203-28 Date Collected: 10/20/15 13:28 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A -Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/26/15 16:51 10/29/15 07:05 1 alpha-BHC 0.049 U 0.049 0.0077 ug/L 10/26/15 16:51 10/29/15 07:05 1 alpha-Chlordane 0.049 U 0.049 0.0099 ug/L 10/26/15 16:51 10/29/15 07:05 1 beta-BHC 0.75 0.049 0.012 ug/L 10/26/15 16:51 10/29/15 07:05 1 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/26/15 16:51 10/29/15 07:05 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/26/15 16:51 10/29/15 07:05 1 4,4'-DDT 0.049 U 0.049 0.0084 ug/L 10/26/15 16:51 10/29/15 07:05 1 delta-BHC 0.31 0.049 0.013 ug/L 10/26/15 16:51 10/29/15 07:05 1 Dieldrin 0.25 0.049 0.0085 ug/L 10/26/15 16:51 10/29/15 07:05 1 Endosulfan I 0.049 U 0.049 0.0081 ug/L 10/26/15 16:51 10/29/15 07:05 1 Endosulfan II 0.049 U 0.049 0.0084 ug/L 10/26/15 16:51 10/29/15 07:05 1 Endosulfan sulfate 0.049 U 0.049 0.0082 ug/L 10/26/15 16:51 10/29/15 07:05 1 Endrin 0.049 U 0.049 0.0087 ug/L 10/26/15 16:51 10/29/15 07:05 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/26/15 16:51 10/29/15 07:05 1 Endrin ketone 0.073 0.049 0.0088 ug/L 10/26/15 16:51 10/29/15 07:05 1 gamma-BHC(Lindane) 0.049 U 0.049 0.0082 ug/L 10/26/15 16:51 10/29/15 07:05 1 gamma-Chlordane 0.010 J p 0.049 0.0084 ug/L 10/26/15 16:51 10/29/15 07:05 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/26/15 16:51 10/29/15 07:05 1 Heptachlor epoxide 0.026 J p 0.049 0.0080 ug/L 10/26/15 16:51 10/29/15 07:05 1 Methoxychlor 0.049 U 0.049 0.0092 ug/L 10/26/15 16:51 10/29/15 07:05 1 Toxaphene 2.7 J 4.9 0.19 ug/L 10/26/15 16:51 10/29/15 07:05 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobipheny/ 69 10-130 1026/15 16:51 10/29/15 07:05 1 Tetrachloro-m-xylene 71 39-130 10/26/15 16:51 1029/15 07:05 1 TestAmerica Savannah Page 33 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-10S Lab Sample ID: 680-118203-29 Date Collected: 10/20/15 11:14 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B -Volatile Organic Compounds(GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 16:10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac II Toluene-d8(Surr) 103 70-130 10/27/15 16:10 1 1,2-Dichloroethane-d4(Surr) 108 70-130 10/27/15 16:10 1 Dibromofluoromethane(Surr) 111 70-130 10/27/15 16:10 1 4-Bromofluorobenzene(Surr) 99 70-130 10/27/15 16:10 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.048 U 0.048 0.0071 ug/L 10/26/15 16:51 10/29/15 07:19 1 alpha-BHC 0.048 U 0.048 0.0075 ug/L 10/26/15 16:51 10/29/15 07:19 1 alpha-Chlordane 0.048 U 0.048 0.0097 ug/L 10/26/15 16:51 10/29/15 07:19 1 beta-BHC 0.88 0.19 0.046 ug/L 10/26/15 16:51 10/29/15 18:13 4 4,4'-DDD 0.048 U 0.048 0.0074 ug/L 10/26/15 16:51 10/29/15 07:19 1 4,4'-DDE 0.048 U 0.048 0.0072 ug/L 10/26/15 16:51 10/29/15 07:19 1 4,4'-DDT 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 07:19 1 delta-BHC 0.020 J 0.048 0.013 ug/L 10/26/15 16:51 10/29/15 07:19 1 Dieldrin 0.12 0.048 0.0083 ug/L 10/26/15 16:51 10/29/15 07:19 1 Endosulfan I 0.048 U 0.048 0.0079 ug/L 10/26/15 16:51 10/29/15 07:19 1 Endosulfan II 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 07:19 1 Endosulfan sulfate 0.048 U 0.048 0.0080 ug/L 10/26/15 16:51 10/29/15 07:19 1 Endrin 0.048 U 0.048 0.0085 ug/L 10/26/15 16:51 10/29/15 07:19 1 Endrin aldehyde 0.048 U 0.048 0.016 ug/L 10/26/15 16:51 10/29/15 07:19 1 Endrin ketone 0.17 0.048 0.0086 ug/L 10/26/15 16:51 10/29/15 07:19 1 gamma-BHC(Lindane) 0.015 J 0.048 0.0080 ug/L 10/26/15 16:51 10/29/15 07:19 1 gamma-Chlordane 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 07:19 1 Heptachlor 0.048 U 0.048 0.0076 ug/L 10/26/15 16:51 10/29/15 07:19 1 Heptachlor epoxide 0.012 J p 0.048 0.0078 ug/L 10/26/15 16:51 10/29/15 07:19 1 Methoxychlor 0.048 U 0.048 0.0090 ug/L 10/26/15 16:51 10/29/15 07:19 1 Toxaphene 0.97 J 4.8 0.18 ug/L 10/26/15 16:51 10/29/15 07:19 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 64 10-130 10/26/15 16:51 10/29/15 07:19 1 Tetrachloro-m-xylene 71 39-130 10/26/15 16:51 10/29/15 07:19 1 TestAmerica Savannah Page 34 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-5S Lab Sample ID: 680-118203-30 Date Collected: 10/20/15 12:02 Matrix:Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0074 ug/L 10/26/15 16:51 10/29/15 11:34 1 alpha-BHC 0.018 J 0.051 0.0079 ug/L 10/26/15 16:51 10/29/15 11:34 1 alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/26/15 16:51 10/29/15 11:34 1 beta-BHC 2.8 0.20 0.049 ug/L 10/26/15 16:51 10/29/15 11:49 4 4,4'-DDD 0.051 U 0.051 0.0078 ug/L 10/26/15 16:51 10/29/15 11:34 1 4,4'-DDE 0.051 U 0.051 0.0075 ug/L 10/26/15 16:51 10/29/15 11:34 1 4,4'-DDT 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 11:34 1 delta-BHC 0.28 0.051 0.013 ug/L 10/26/15 16:51 10/29/15 11:34 1 Dieldrin 0.54 0.051 0.0088 ug/L 10/26/15 16:51 10/29/15 11:34 1 Endosulfan I 0.051 U 0.051 0.0084 ug/L 10/26/15 16:51 10/29/15 11:34 1 Endosulfan II 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 11:34 1 Endosulfan sulfate 0.051 U 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 11:34 1 Endrin 0.051 U 0.051 0.0090 ug/L 10/26/15 16:51 10/29/15 11:34 1 Endrin aldehyde 0.051 U 0.051 0.017 ug/L 10/26/15 16:51 10/29/15 11:34 1 Endrin ketone 0.30 0.051 0.0091 ug/L 10/26/15 16:51 10/29/15 11:34 1 gamma-BHC(Lindane) 0.028 J p 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 11:34 1 gamma-Chlordane 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 11:34 1 Heptachlor 0.051 U 0.051 0.0080 ug/L 10/26/15 16:51 10/29/15 11:34 1 Heptachlor epoxide 0.051 U 0.051 0.0082 ug/L 10/26/15 16:51 10/29/15 11:34 1 Methoxychlor 0.051 U 0.051 0.0095 ug/L 10/26/15 16:51 10/29/15 11:34 1 Toxaphene 9.6 5.1 0.19 ug/L 10/26/15 16:51 10/29/15 11:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 71 10-130 10/26/15 16:51 10/29/15 11:34 1 DCB Decachlorobiphenyl 73 10-130 10/26/15 16:51 10/29/15 11:49 4 Tetrachloro-m-xylene 68 39-130 10/26/15 16:51 10/29/15 11:34 1 Tetrachloro-m-xylene 68 39-130 10/26/15 16:51 10/29/15 11:49 4 TestAmerica Savannah Page 35 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-18S Lab Sample ID: 680-118203-31 Date Collected: 10/20/15 15:04 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B -Volatile Organic Compounds(GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 16:32 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Surr) 102 70-130 10/27/15 16:32 1 1,2-Dichloroethane-d4(Sun-) 109 70-130 10/27/15 16:32 1 Dibromofluoromethane(Sun-) 112 70-130 10/27/15 16:32 1 4-Bromofluorobenzene(Surr) 100 70-130 10/27/15 16:32 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.048 U 0.048 0.0070 ug/L 10/26/15 16:51 10/29/15 07:34 1 alpha-BHC 0.048 U 0.048 0.0075 ug/L 10/26/15 16:51 10/29/15 07:34 1 alpha-Chlordane 0.048 U 0.048 0.0096 ug/L 10/26/15 16:51 10/29/15 07:34 1 beta-BHC 0.048 U 0.048 0.012 ug/L 10/26/15 16:51 10/29/15 07:34 1 4,4'-DDD 0.048 U 0.048 0.0074 ug/L 10/26/15 16:51 10/29/15 07:34 1 4,4'-DDE 0.048 U 0.048 0.0071 ug/L 10/26/15 16:51 10/29/15 07:34 1 4,4'-DDT 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 07:34 1 delta-BHC 0.048 U 0.048 0.013 ug/L 10/26/15 16:51 10/29/15 07:34 1 Dieldrin 0.048 U 0.048 0.0083 ug/L 10/26/15 16:51 10/29/15 07:34 1 Endosulfan I 0.048 U 0.048 0.0079 ug/L 10/26/15 16:51 10/29/15 07:34 1 Endosulfan II 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 07:34 1 Endosulfan sulfate 0.048 U 0.048 0.0080 ug/L 10/26/15 16:51 10/29/15 07:34 1 Endrin 0.048 U 0.048 0.0085 ug/L 10/26/15 16:51 10/29/15 07:34 1 Endrin aldehyde 0.048 U 0.048 0.016 ug/L 10/26/15 16:51 10/29/15 07:34 1 Endrin ketone 0.048 U 0.048 0.0086 ug/L 10/26/15 16:51 10/29/15 07:34 1 gamma-BHC(Lindane) 0.048 U 0.048 0.0080 ug/L 10/26/15 16:51 10/29/15 07:34 1 gamma-Chlordane 0.048 U 0.048 0.0082 ug/L 10/26/15 16:51 10/29/15 07:34 1 Heptachlor 0.048 U 0.048 0.0076 ug/L 10/26/15 16:51 10/29/15 07:34 1 Heptachlor epoxide 0.048 U 0.048 0.0078 ug/L 10/26/15 16:51 10/29/15 07:34 1 Methoxychlor 0.048 U 0.048 0.0089 ug/L 10/26/15 16:51 10/29/15 07:34 1 Toxaphene 4.8 U 4.8 0.18 ug/L 10/26/15 16:51 10/29/15 07:34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 67 10-130 10/26/15 16:51 10/29/15 07:34 1 Tetrachloro-m xylene 64 39-130 10/26/15 16:51 10/29/15 07:34 1 TestAmerica Savannah Page 36 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-22D Lab Sample ID: 680-118203-32 Date Collected: 10/20/15 15:47 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0075 ug/L 10/26/15 16:51 10/29/15 07:48 1 alpha-BHC 0.028 J 0.051 0.0080 ug/L 10/26/15 16:51 10/29/15 07:48 1 alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/26/15 16:51 10/29/15 07:48 1 beta-BHC 0.18 0.051 0.012 ug/L 10/26/15 16:51 10/29/15 07:48 1 4,4'-DDD 0.051 U 0.051 0.0079 ug/L 10/26/15 16:51 10/29/15 07:48 1 4,4'-DDE 0.051 U 0.051 0.0076 ug/L 10/26/15 16:51 10/29/15 07:48 1 4,4'-DDT 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 07:48 1 delta-BHC 0.11 0.051 0.013 ug/L 10/26/15 16:51 10/29/15 07:48 1 Dieldrin 0.051 U 0.051 0.0088 ug/L 10/26/15 16:51 10/29/15 07:48 1 Endosulfan I 0.051 U 0.051 0.0084 ug/L 10/26/15 16:51 10/29/15 07:48 1 Endosulfan II 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 07:48 1 Endosulfan sulfate 0.051 U 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 07:48 1 Endrin 0.051 U 0.051 0.0090 ug/L 10/26/15 16:51 10/29/15 07:48 1 Endrin aldehyde 0.051 U 0.051 0.017 ug/L 10/26/15 16:51 10/29/15 07:48 1 Endrin ketone 0.051 U 0.051 0.0091 ug/L 10/26/15 16:51 10/29/15 07:48 1 gamma-BHC(Lindane) 0.022 J 0.051 0.0085 ug/L 10/26/15 16:51 10/29/15 07:48 1 gamma-Chlordane 0.051 U 0.051 0.0087 ug/L 10/26/15 16:51 10/29/15 07:48 1 Heptachlor 0.051 U 0.051 0.0081 ug/L 10/26/15 16:51 10/29/15 07:48 1 Heptachlor epoxide 0.051 U 0.051 0.0083 ug/L 10/26/15 16:51 10/29/15 07:48 1 Methoxychlor 0.051 U 0.051 0.0095 ug/L 10/26/15 16:51 10/29/15 07:48 1 Toxaphene 5.1 U 5.1 0.19 ug/L 10/26/15 16:51 10/29/15 07:48 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 60 10-130 10/26/15 16:51 10/29/15 07:48 1 Tetrachloro-m-xylene 64 39-130 10/26/15 16:51 10/29/15 07:48 1 TestAmerica Savannah Page 37 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-22L Lab Sample ID: 680-118203-33 Date Collected: 10/20/15 15:21 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/26/15 16:51 10/29/15 12:18 1 alpha-BHC 0.17 0.049 0.0077 ug/L 10/26/15 16:51 10/29/15 12:18 1 alpha-Chlordane 0.049 U 0.049 0.0099 ug/L 10/26/15 16:51 10/29/15 12:18 1 beta-BHC 0.71 0.049 0.012 ug/L 10/26/15 16:51 10/29/15 12:18 1 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/26/15 16:51 10/29/15 12:18 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/26/15 16:51 10/29/15 12:18 1 4,4'-DDT 0.049 U 0.049 0.0084 ug/L 10/26/15 16:51 10/29/15 12:18 1 delta-BHC 0.44 0.049 0.013 ug/L 10/26/15 16:51 10/29/15 12:18 1 Dieldrin 0.071 0.049 0.0085 ug/L 10/26/15 16:51 10/29/15 12:18 1 Endosulfan I 0.049 U 0.049 0.0081 ug/L 10/26/15 16:51 10/29/15 12:18 1 Endosulfan II 0.049 U 0.049 0.0084 ug/L 10/26/15 16:51 10/29/15 12:18 1 Endosulfan sulfate 0.049 U 0.049 0.0082 ug/L 10/26/15 16:51 10/29/15 12:18 1 Endrin 0.049 U 0.049 0.0087 ug/L 10/26/15 16:51 10/29/15 12:18 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/26/15 16:51 10/29/15 12:18 1 Endrin ketone 0.072 0.049 0.0088 ug/L 10/26/15 16:51 10/29/15 12:18 1 gamma-BHC(Lindane) 0.12 0.049 0.0082 ug/L 10/26/15 16:51 10/29/15 12:18 1 gamma-Chlordane 0.049 U 0.049 0.0084 ug/L 10/26/15 16:51 10/29/15 12:18 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/26/15 16:51 10/29/15 12:18 1 Heptachlor epoxide 0.049 U 0.049 0.0080 ug/L 10/26/15 16:51 10/29/15 12:18 1 Methoxychlor 0.049 U 0.049 0.0092 ug/L 10/26/15 16:51 10/29/15 12:18 1 Toxaphene 1.9 J 4.9 0.19 ug/L 10/26/15 16:51 10/29/15 12:18 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 67 10-130 10/26/15 16:51 10/29/15 12:18 1 Tetrachloro-m-xylene 66 39-130 10/26/15 16:51 10/29/15 12:18 1 TestAmerica Savannah Page 38 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-16S Lab Sample ID: 680-118203-34 Date Collected: 10/20/15 13:23 Matrix:Water Date Received: 10/23/15 09:44 Method: 8260B -Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 16:53 1 i Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Surr) 102 70-130 10/27/15 16:53 1 1,2-Dichloroethane-d4(Surr) 108 70-130 10/27/15 16:53 1 Dibromofluoromethane(Surr) 112 70-130 10/27/15 16:53 1 4-Bromofluorobenzene(Surr) 100 70-130 10/27/15 16:53 1 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.054 U 0.054 0.0078 ug/L 10/26/15 16:51 10/29/15 08:03 1 alpha-BHC 0.054 U 0.054 0.0084 ug/L 10/26/15 16:51 10/29/15 08:03 1 alpha-Chlordane 0.054 U 0.054 0.011 ug/L 10/26/15 16:51 10/29/15 08:03 1 beta-BHC 0.054 U 0.054 0.013 ug/L 10/26/15 16:51 10/29/15 08:03 1 4,4'-DDD 0.054 U 0.054 0.0083 ug/L 10/26/15 16:51 10/29/15 08:03 1 4,4'-DDE 0.054 U 0.054 0.0079 ug/L 10/26/15 16:51 10/29/15 08:03 1 4,4'-DDT 0.054 U 0.054 0.0091 ug/L 10/26/15 16:51 10/29/15 08:03 1 delta-BHC 0.054 U 0.054 0.014 ug/L 10/26/15 16:51 10/29/15 08:03 1 Dieldrin 0.054 U 0.054 0.0092 ug/L 10/26/15 16:51 10/29/15 08:03 1 Endosulfan I 0.054 U 0.054 0.0088 ug/L 10/26/15 16:51 10/29/15 08:03 1 Endosulfan II 0.054 U 0.054 0.0091 ug/L 10/26/15 16:51 10/29/15 08:03 1 Endosulfan sulfate 0.054 U 0.054 0.0089 ug/L 10/26/15 16:51 10/29/15 08:03 1 Endrin 0.054 U 0.054 0.0094 ug/L 10/26/15 16:51 10/29/15 08:03 1 Endrin aldehyde 0.054 U 0.054 0.018 ug/L 10/26/15 16:51 10/29/15 08:03 1 Endrin ketone 0.054 U 0.054 0.0095 ug/L 10/26/15 16:51 10/29/15 08:03 1 gamma-BHC(Lindane) 0.054 U 0.054 0.0089 ug/L 10/26/15 16:51 10/29/15 08:03 1 gamma-Chlordane 0.054 U 0.054 0.0091 ug/L 10/26/15 16:51 10/29/15 08:03 1 Heptachlor 0.054 U 0.054 0.0085 ug/L 10/26/15 16:51 10/29/15 08:03 1 Heptachlor epoxide 0.054 U 0.054 0.0087 ug/L 10/26/15 16:51 10/29/15 08:03 1 Methoxychlor 0.054 U 0.054 0.010 ug/L 10/26/15 16:51 10/29/15 08:03 1 Toxaphene 5.4 U 5.4 0.20 ug/L 10/26/15 16:51 10/29/15 08:03 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 74 10-130 1026/15 16:51 1029/15 08:03 1 Tetrachloro-m-xylene 72 39-130 10/26/15 16:51 1029/15 08:03 1 TestAmerica Savannah Page 39 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-17S Lab Sample ID: 680-118203-35 Date Collected: 10/20/15 14:09 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260E -Volatile Organic Compounds(GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 14:07 1 L Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Surr) 98 70-130 1027/15 14:07 1 1,2-Dichloroethane-d4(Sun-) 77 70-130 1027/15 14:07 1 Dibromofluoromethane(Surr) 87 70-130 1027/15 14:07 1 4-Bromofluorobenzene(Surr) 94 70-130 1027/15 14:07 1 Method: 8081 B/8082A -Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.053 U 0.053 0.0077 ug/L 10/26/15 16:51 10/29/15 08:18 1 alpha-BHC 0.053 U 0.053 0.0082 ug/L 10/26/15 16:51 10/29/15 08:18 1 alpha-Chlordane 0.053 U 0.053 0.011 ug/L 10/26/15 16:51 10/29/15 08:18 1 beta-BHC 0.053 U 0.053 0.013 ug/L 10/26/15 16:51 10/29/15 08:18 1 4,4'-DDD 0.053 U 0.053 0.0081 ug/L 10/26/15 16:51 10/29/15 08:18 1 4,4'-DDE 0.053 U 0.053 0.0078 ug/L 10/26/15 16:51 10/29/15 08:18 1 4,4'-DDT 0.053 U 0.053 0.0090 ug/L 10/26/15 16:51 10/29/15 08:18 1 delta-BHC 0.053 U 0.053 0.014 ug/L 10/26/15 16:51 10/29/15 08:18 1 Dieldrin 0.053 U 0.053 0.0091 ug/L 10/26/15 16:51 10/29/15 08:18 1 1 Endosulfan I 0.053 U 0.053 0.0086 ug/L 10/26/15 16:51 10/29/15 08:18 1 Endosulfan II 0.053 U 0.053 0.0090 ug/L 10/26/15 16:51 10/29/15 08:18 1 Endosulfan sulfate 0.053 U 0.053 0.0088 ug/L 10/26/15 16:51 10/29/15 08:18 1 Endrin 0.053 U 0.053 0.0093 ug/L 10/26/15 16:51 10/29/15 08:18 1 Endrin aldehyde 0.053 U 0.053 0.018 ug/L 10/26/15 16:51 10/29/15 08:18 1 Endrin ketone 0.053 U 0.053 0.0094 ug/L 10/26/15 16:51 10/29/15 08:18 1 gamma-BHC(Lindane) 0.053 U 0.053 0.0088 ug/L 10/26/15 16:51 10/29/15 08:18 1 gamma-Chlordane 0.053 U 0.053 0.0090 ug/L 10/26/15 16:51 10/29/15 08:18 1 Heptachlor 0.053 U 0.053 0.0083 ug/L 10/26/15 16:51 10/29/15 08:18 1 Heptachlor epoxide 0.053 U 0.053 0.0085 ug/L 10/26/15 16:51 10/29/15 08:18 1 Methoxychlor 0.053 U 0.053 0.0098 ug/L 10/26/15 16:51 10/29/15 08:18 1 Toxaphene 5.3 U 5.3 0.20 ug/L 10/26/15 16:51 10/29/15 08:18 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 65 10-130 1026/15 16:51 1029/15 08:18 1 Tetrachloro-m-xylene 71 39-130 1026/15 16:51 1029/15 08:18 1 TestAmerica Savannah Page 40 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-16D Lab Sample ID: 680-118203-36 Date Collected: 10/20/15 11:38 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B -Volatile Organic Compounds(GC/MS) Analyte •Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 56 1.0 0.48 ug/L 10/27/15 13:45 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Surr) 99 70-130 10/27/15 13:45 1 1,2-Dichloroethane-d4(Surr) 77 70-130 10/27/15 13:45 1 Dibromofluoromethane(Surr) 87 70-130 10/27/15 13:45 1 4-Bromofluorobenzene(Surr) 93 70-130 10/27/15 13:45 1 TestAmerica Savannah Page 41 of 81 Client Sample Results • Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-17D Lab Sample ID: 680-118203-37 Date Collected: 10/20/15 12:23 Matrix: Water Date Received: 10/23/15 09:44 Method: 8260B -Volatile Organic Compounds(GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 190 1.0 0.48 ug/L 10/27/15 14:30 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac In Toluene-d8(Sun-) 96 70-130 10/27/15 14:30 1 1,2-Dichloroethane-d4(Sun) 81 70-130 10/27/15 14:30 1 Dibromofluoromethane(Sun-) 87 70-130 10/27/15 14:30 1 4-Bromofluorobenzene(Surr) 90 70-130 10/27/15 14:30 1 TestAmerica Savannah Page 42 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-26D Lab Sample ID: 680-118203-38 Date Collected: 10/21/15 17:06 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0071 ug/L 10/27/15 16:05 10/29/15 20:39 1 alpha-BHC 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 20:39 1 alpha-Chlordane 0.016 J 0.049 0.0097 ug/L 10/27/15 16:05 10/29/15 20:39 1 beta-BHC 0.049 U 0.049 0.012 ug/L 10/27/15 16:05 10/29/15 20:39 1 4,4'-DDD 0.049 U 0.049 0.0075 ug/L 10/27/15 16:05 10/29/15 20:39 1 4,4'-DDE 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 20:39 1 4,4'-DDT 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 20:39 1 delta-BHC 0.049 U 0.049 0.013 ug/L 10/27/15 16:05 10/29/15 20:39 1 Dieldrin 0.049 U 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 20:39 1 Endosulfan I 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 20:39 1 Endosulfan II 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 20:39 1 Endosulfan sulfate 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 20:39 1 Endrin 0.049 U 0.049 0.0086 ug/L 10/27/15 16:05 10/29/15 20:39 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 20:39 1 Endrin ketone 0.049 U 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 20:39 1 gamma-BHC(Lindane) 0.019 J 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 20:39 1 gamma-Chlordane 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 20:39 1 Heptachlor 0.049 U 0.049 0.0077 ug/L 10/27/15 16:05 10/29/15 20:39 1 Heptachlor epoxide 0.016 J 0.049 0.0079 ug/L 10/27/15 16:05 10/29/15 20:39 1 Methoxychlor 0.049 U 0.049 0.0090 ug/L 10/27/15 16:05 10/29/15 20:39 1 Toxaphene 4.9 U 4.9 0.18 ug/L 10/27/15 16:05 10/29/15 20:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 71 10-130 1027/15 16:05 10/29/15 20:39 1 Tetrachloro-m-xylene 67 39-130 1027/15 16:05 1029/15 20:39 1 TestAmerica Savannah Page 43 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-25L Lab Sample ID: 680-118203-39 Date Collected: 10/21/15 15:17 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/27/15 16:05 10/29/15 20:53 1 alpha-BHC 0.70 0.050 0.0078 ug/L 10/27/15 16:05 10/29/15 20:53 1 alpha-Chlordane 0.050 U 0.050 0.0099 ug/L 10/27/15 16:05 10/29/15 20:53 1 beta-BHC 0.56 0.050 0.012 ug/L 10/27/15 16:05 10/29/15 20:53 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/27/15 16:05 10/29/15 20:53 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/27/15 16:05 10/29/15 20:53 1 4,4'-DDT 0.050 U 0.050 0.0084 ug/L 10/27/15 16:05 10/29/15 20:53 1 delta-BHC 0.97 0.20 0.052 ug/L 10/27/15 16:05 10/29/15 21:08 4 Dieldrin 0.015 J 0.050 0.0085 ug/L 10/27/15 16:05 10/29/15 20:53 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/27/15 16:05 10/29/15 20:53 1 Endosulfan II 0.050 U 0.050 0.0084 ug/L 10/27/15 16:05 10/29/15 20:53 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/27/15 16:05 10/29/15 20:53 1 Endrin 0.050 U 0.050 0.0087 ug/L 10/27/15 16:05 10/29/15 20:53 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/27/15 16:05 10/29/15 20:53 1 Endrin ketone 0.027 J 0.050 0.0088 ug/L 10/27/15 16:05 10/29/15 20:53 1 gamma-BHC(Lindane) 0.10 0.050 0.0083 ug/L 10/27/15 16:05 10/29/15 20:53 1 gamma-Chlordane 0.050 U 0.050 0.0084 ug/L 10/27/15 16:05 10/29/15 20:53 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/27/15 16:05 10/29/15 20:53 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/27/15 16:05 10/29/15 20:53 1 Methoxychlor 0.050 U 0.050 0.0092 ug/L 10/27/15 16:05 10/29/15 20:53 1 Toxaphene 5.0 U 5.0 0.19 ug/L 10/27/15 16:05 10/29/15 20:53 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 67 10-130 1027/15 16:05 10/29/15 20:53 1 Tetrachloro-m-xylene 70 39-130 10/27/15 16:05 1029/15 20:53 1 TestAmerica Savannah Page 44 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-37L Lab Sample ID: 680-118203-40 Date Collected: 10/21/15 16:02 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.049 U 0.049 0.0072 ug/L 10/27/15 16:05 10/29/15 21:22 1 alpha-BHC 0.88 0.20 0.031 ug/L 10/27/15 16:05 10/29/15 21:37 4 alpha-Chlordane 0.049 U 0.049 0.0098 ug/L 10/27/15 16:05 10/29/15 21:22 1 beta-BHC 0.68 0.049 0.012 ug/L 10/27/15 16:05 10/29/15 21:22 1 4,4'-DDD 0.049 U 0.049 0.0076 ug/L 10/27/15 16:05 10/29/15 21:22 1 4,4'-DDE 0.049 U 0.049 0.0073 ug/L 10/27/15 16:05 10/29/15 21:22 1 4,4'-DDT 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 21:22 1 delta-BHC 1.5 0.20 0.051 ug/L 10/27/15 16:05 10/29/15 21:37 4 Dieldrin 0.018 J 0.049 0.0084 ug/L 10/27/15 16:05 10/29/15 21:22 1 Endosulfan I 0.049 U 0.049 0.0080 ug/L 10/27/15 16:05 10/29/15 21:22 1 Endosulfan II 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 21:22 1 Endosulfan sulfate 0.049 U 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 21:22 1 Endrin 0.049 U 0.049 0.0086 ug/L 10/27/15 16:05 10/29/15 21:22 1 1 Endrin aldehyde 0.049 U 0.049 0.017 ug/L 10/27/15 16:05 10/29/15 21:22 1 Endrin ketone 0.046 J 0.049 0.0087 ug/L 10/27/15 16:05 10/29/15 21:22 1 gamma-BHC(Lindane) 0.18 0.049 0.0081 ug/L 10/27/15 16:05 10/29/15 21:22 1 gamma-Chlordane 0.049 U 0.049 0.0083 ug/L 10/27/15 16:05 10/29/15 21:22 1 Heptachlor 0.049 U 0.049 0.0078 ug/L 10/27/15 16:05 10/29/15 21:22 1 Heptachlor epoxide 0.049 U 0.049 0.0079 ug/L 10/27/15 16:05 10/29/15 21:22 1 Methoxychlor 0.049 U 0.049 0.0091 ug/L 10/27/15 16:05 10/29/15 21:22 1 Toxaphene 0.75 J 4.9 0.19 ug/L 10/27/15 16:05 10/29/15 21:22 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 65 10-130 1027/15 16:05 10/29/15 21:22 1 Tetrachloro-m-xylene 64 39-130 1027/15 16:05 1029/15 21:22 1 I 1 TestAmerica Savannah Page 45 of 81 I Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: PZ-5 Lab Sample ID: 680-118203-41 Date Collected: 10/21/15 15:55 Matrix:Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0074 ug/L 10/28/15 15:40 10/30/15 17:50 1 alpha-BHC 1.0 0.20 0.032 ug/L 10/28/15 15:40 10/30/15 18:05 4 alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/28/15 15:40 10/30/15 17:50 1 beta-BHC 0.31 0.051 0.012 ug/L 10/28/15 15:40 10/30/15 17:50 1 4,4'-DDD 0.051 U 0.051 0.0078 ug/L 10/28/15 15:40 10/30/15 17:50 1 4,4'-DDE 0.051 U 0.051 0.0075 ug/L 10/28/15 15:40 10/30/15 17:50 1 4,4'-DDT 0.051 U 0.051 0.0086 ug/L 10/28/15 15:40 10/30/15 17:50 1 delta-BHC 0.48 0.051 0.013 ug/L 10/28/15 15:40 10/30/15 17:50 1 Dieldrin 0.051 U 0.051 0.0087 ug/L 10/28/15 15:40 10/30/15 17:50 1 Endosulfan I 0.051 U 0.051 0.0083 ug/L 10/28/15 15:40 10/30/15 17:50 1 Endosulfan II 0.051 U 0.051 0.0086 ug/L 10/28/15 15:40 10/30/15 17:50 1 Endosulfan sulfate 0.051 U 0.051 0.0084 ug/L 10/28/15 15:40 10/30/15 17:50 1 Endrin 0.051 U* 0.051 0.0089 ug/L 10/28/15 15:40 10/30/15 17:50 1 Endrin aldehyde 0.051 U 0.051 0.017 ug/L 10/28/15 15:40 10/30/15 17:50 1 Endrin ketone 0.031 J 0.051 0.0090 ug/L 10/28/15 15:40 10/30/15 17:50 1 gamma-BHC(Lindane) 0.36 0.051 0.0084 ug/L 10/28/15 15:40 10/30/15 17:50 1 gamma-Chlordane 0.051 U 0.051 0.0086 ug/L 10/28/15 15:40 10/30/15 17:50 1 Heptachlor 0.051 U 0.051 0.0080 ug/L 10/28/15 15:40 10/30/15 17:50 1 Heptachlor epoxide 0.051 U 0.051 0.0082 ug/L 10/28/15 15:40 10/30/15 17:50 1 Methoxychlor 0.051 U 0.051 0.0094 ug/L 10/28/15 15:40 10/30/15 17:50 1 Toxaphene 5.1 U 5.1 0.19 ug/L 10/28/15 15:40 10/30/15 17:50 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 73 10-130 10/28/15 15:40 10/30/15 17:50 1 Tetrachloro-m-xylene 67 39-130 10/28/15 15:40 10/30/15 17:50 1 TestAmerica Savannah Page 46 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-23D Lab Sample ID: 680-118203-42 Date Collected: 10/22/15 13:40 Matrix:Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.048 U 0.048 0.0071 ug/L 10/28/15 15:40 10/30/15 07:47 1 alpha-BHC 0.021 J 0.048 0.0076 ug/L 10/28/15 15:40 10/30/15 07:47 1 alpha-Chlordane 0.048 U 0.048 0.0097 ug/L 10/28/15 15:40 10/30/15 07:47 1 beta-BHC 0.022 J 0.048 0.012 ug/L 10/28/15 15:40 10/30/15 07:47 1 4,4'-DDD 0.048 U 0.048 0.0075 ug/L 10/28/15 15:40 10/30/15 07:47 1 4,4'-DDE 0.048 U 0.048 0.0072 ug/L 10/28/15 15:40 10/30/15 07:47 1 4,4'-DDT 0.048 U 0.048 0.0082 ug/L 10/28/15 15:40 10/30/15 07:47 1 delta-BHC 0.048 U 0.048 0.013 ug/L 10/28/15 15:40 10/30/15 07:47 1 Dieldrin 0.048 U 0.048 0.0083 ug/L 10/28/15 15:40 10/30/15 07:47 1 Endosulfan I 0.048 U 0.048 0.0079 ug/L 10/28/15 15:40 10/30/15 07:47 1 Endosulfan II 0.048 U 0.048 0.0082 ug/L 10/28/15 15:40 10/30/15 07:47 1 Endosulfan sulfate 0.048 U 0.048 0.0080 ug/L 10/28/15 15:40 10/30/15 07:47 1 Endrin 0.048 U* 0.048 0.0085 ug/L 10/28/15 15:40 10/30/15 07:47 1 . Endrin aldehyde 0.048 U 0.048 0.016 ug/L 10/28/15 15:40 10/30/15 07:47 1 Endrin ketone 0.048 U 0.048 0.0086 ug/L 10/28/15 15:40 10/30/15 07:47 1 gamma-BHC(Lindane) 0.015 J 0.048 0.0080 ug/L 10/28/15 15:40 10/30/15 07:47 1 gamma-Chlordane 0.048 U 0.048 0.0082 ug/L 10/28/15 15:40 10/30/15 07:47 1 Heptachlor 0.048 U 0.048 0.0077 ug/L 10/28/15 15:40 10/30/15 07:47 1 Heptachlor epoxide 0.048 U 0.048 0.0078 ug/L 10/28/15 15:40 10/30/15 07:47 1 Methoxychlor 0.048 U 0.048 0.0090 ug/L 10/28/15 15:40 10/30/15 07:47 1 Toxaphene 4.8 U 4.8 0.18 ug/L 10/28/15 15:40 10/30/15 07:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 59 10-130 10/28/15 15:40 10/30/15 07:47 1 Tetrachloro-m-xylene 68 39-130 10/28/15 15:40 10/30/15 07:47 1 I TestAmerica Savannah Page 47 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-38L Lab Sample ID: 680-118203-43 Date Collected: 10/22/15 12:31 Matrix:Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.053 U 0.053 0.0077 ug/L 10/28/15 15:40 10/30/15 08:01 1 alpha-BHC 0.053 U 0.053 0.0082 ug/L 10/28/15 15:40 10/30/15 08:01 1 alpha-Chlordane 0.053 U 0.053 0.011 ug/L 10/28/15 15:40 10/30/15 08:01 1 beta-BHC 0.053 U 0.053 0.013 ug/L 10/28/15 15:40 10/30/15 08:01 1 4,4'-DDD 0.053 U 0.053 0.0081 ug/L 10/28/15 15:40 10/30/15 08:01 1 4,4'-DDE 0.053 U 0.053 0.0078 ug/L 10/28/15 15:40 10/30/15 08:01 1 4,4'-DDT 0.053 U 0.053 0.0089 ug/L 10/28/15 15:40 10/30/15 08:01 1 delta-BHC 0.053 U 0.053 0.014 ug/L 10/28/15 15:40 10/30/15 08:01 1 Dieldrin 0.053 U 0.053 0.0091 ug/L 10/28/15 15:40 10/30/15 08:01 1 Endosulfan I 0.053 U 0.053 0.0086 ug/L 10/28/15 15:40 10/30/15 08:01 1 Endosulfan II 0.053 U 0.053 0.0089 ug/L 10/28/15 15:40 10/30/15 08:01 1 Endosulfan sulfate 0.053 U 0.053 0.0087 ug/L 10/28/15 15:40 10/30/15 08:01 1 Endrin 0.053 U* 0.053 0.0093 ug/L 10/28/15 15:40 10/30/15 08:01 1 Endrin aldehyde 0.053 U 0.053 0.018 ug/L 10/28/15 15:40 10/30/15 08:01 1 Endrin ketone 0.053 U 0.053 0.0094 ug/L 10/28/15 15:40 10/30/15 08:01 1 gamma-BHC(Lindane) 0.053 U 0.053 0.0087 ug/L 10/28/15 15:40 10/30/15 08:01 1 gamma-Chlordane 0.053 U 0.053 0.0089 ug/L 10/28/15 15:40 10/30/15 08:01 1 Heptachlor 0.053 U 0.053 0.0083 ug/L 10/28/15 15:40 10/30/15 08:01 1 Heptachlor epoxide 0.053 U 0.053 0.0085 ug/L 10/28/15 15:40 10/30/15 08:01 1 Methoxychlor 0.053 U 0.053 0.0098 ug/L 10/28/15 15:40 10/30/15 08:01 1 Toxaphene 5.3 U 5.3 0.20 ug/L 10/28/15 15:40 10/30/15 08:01 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 43 10-130 10/28/15 15:40 10/30/15 08:01 1 Tetrachloro-m-xylene 61 39-130 10/28/15 15:40 10/30/15 08:01 1 TestAmerica Savannah Page 48 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-40L Lab Sample ID: 680-118203-44 Date Collected: 10/22/15 13:03 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.048 U 0.048 0.0071 ug/L 10/28/15 15:40 10/30/15 08:16 1 alpha-BHC 0.048 U 0.048 0.0076 ug/L 10/28/15 15:40 10/30/15 08:16 1 alpha-Chlordane 0.048 U 0.048 0.0097 ug/L 10/28/15 15:40 10/30/15 08:16 1 beta-BHC 0.043 J 0.048 0.012 ug/L 10/28/15 15:40 10/30/15 08:16 1 4,4'-DDD 0.048 U 0.048 0.0075 ug/L 10/28/15 15:40 10/30/15 08:16 1 4,4'-DDE 0.048 U 0.048 0.0072 ug/L 10/28/15 15:40 10/30/15 08:16 1 4,4'-DDT 0.048 U 0.048 0.0082 ug/L 10/28/15 15:40 10/30/15 08:16 1 delta-BHC 0.048 U 0.048 0.013 ug/L 10/28/15 15:40 10/30/15 08:16 1 Dieldrin 0.048 U 0.048 0.0083 ug/L 10/28/15 15:40 10/30/15 08:16 1 Endosulfan I 0.048 U 0.048 0.0080 ug/L 10/28/15 15:40 10/30/15 08:16 1 Endosulfan II 0.048 U 0.048 0.0082 ug/L 10/28/15 15:40 10/30/15 08:16 1 Endosulfan sulfate 0.048 U 0.048 0.0080 ug/L 10/28/15 15:40 10/30/15 08:16 1 Endrin 0.048 U* 0.048 0.0085 ug/L 10/28/15 15:40 10/30/15 08:16 1 Endrin aldehyde 0.048 U 0.048 0.016 ug/L 10/28/15 15:40 10/30/15 08:16 1 Endrin ketone 0.048 U 0.048 0.0086 ug/L 10/28/15 15:40 10/30/15 08:16 1 gamma-BHC(Lindane) 0.048 U 0.048 0.0080 ug/L 10/28/15 15:40 10/30/15 08:16 1 gamma-Chlordane 0.048 U 0.048 0.0082 ug/L 10/28/15 15:40 10/30/15 08:16 1 Heptachlor 0.048 U 0.048 0.0077 ug/L 10/28/15 15:40 10/30/15 08:16 1 Heptachlor epoxide 0.048 U 0.048 0.0079 ug/L 10/28/15 15:40 10/30/15 08:16 1 Methoxychlor 0.048 U 0.048 0.0090 ug/L 10/28/15 15:40 10/30/15 08:16 1 Toxaphene 4.8 U 4.8 0.18 ug/L 10/28/15 15:40 10/30/15 08:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 47 10-130 10/28/15 15:40 10/30/15 08:16 1 Tetrachloro-m-xy/ene 59 39-130 10/28/15 15:40 10/30/15 08:16 1 TestAmerica Savannah Page 49 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-32L Lab Sample ID: 680-118203-45 Date Collected: 10/22/15 11:44 Matrix: Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.053 U 0.053 0.0077 ug/L 10/28/15 15:40 10/30/15 08:31 1 alpha-BHC 0.053 U 0.053 0.0083 ug/L 10/28/15 15:40 10/30/15 08:31 1 alpha-Chlordane 0.053 U 0.053 0.011 ug/L 10/28/15 15:40 10/30/15 08:31 1 beta-BHC 0.053 U 0.053 0.013 ug/L 10/28/15 15:40 10/30/15 08:31 1 4,4'-DDD 0.053 U 0.053 0.0082 ug/L 10/28/15 15:40 10/30/15 08:31 1 4,4'-DDE 0.053 U 0.053 0.0078 ug/L 10/28/15 15:40 10/30/15 08:31 1 4,4'-DDT 0.053 U 0.053 0.0090 ug/L 10/28/15 15:40 10/30/15 08:31 1 delta-BHC 0.053 U 0.053 0.014 ug/L 10/28/15 15:40 10/30/15 08:31 1 Dieldrin 0.053 U 0.053 0.0091 ug/L 10/28/15 15:40 10/30/15 08:31 1 Endosulfan I 0.053 U 0.053 0.0087 ug/L 10/28/15 15:40 10/30/15 08:31 1 Endosulfan II 0.053 U 0.053 0.0090 ug/L 10/28/15 15:40 10/30/15 08:31 1 Endosulfan sulfate 0.053 U 0.053 0.0088 ug/L 10/28/15 15:40 10/30/15 08:31 1 Endrin 0.053 U* 0.053 0.0093 ug/L 10/28/15 15:40 10/30/15 08:31 1 Endrin aldehyde 0.053 U 0.053 0.018 ug/L 10/28/15 15:40 10/30/15 08:31 1 Endrin ketone 0.053 U 0.053 0.0094 ug/L 10/28/15 15:40 10/30/15 08:31 1 gamma-BHC(Lindane) 0.053 U 0.053 0.0088 ug/L 10/28/15 15:40 10/30/15 08:31 1 gamma-Chlordane 0.053 U 0.053 0.0090 ug/L 10/28/15 15:40 10/30/15 08:31 1 Heptachlor 0.053 U 0.053 0.0084 ug/L 10/28/15 15:40 10/30/15 08:31 1 Heptachlor epoxide 0.053 U 0.053 0.0086 ug/L 10/28/15 15:40 10/30/15 08:31 1 Methoxychlor 0.053 U 0.053 0.0098 ug/L 10/28/15 15:40 10/30/15 08:31 1 Toxaphene 5.3 U 5.3 0.20 ug/L 10/28/15 15:40 10/30/15 08:31 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 56 10-130 10/28/15 15:40 10/30/15 08:31 1 Tetrachloro-m-xylene 70 39-130 10/28/15 15:40 10/30/15 08:31 1 TestAmerica Savannah Page 50 of 81 Client Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Duplicate 3 Lab Sample ID: 680-118203-46 Date Collected: 10/22/15 12:37 Matrix:Water Date Received: 10/23/15 09:44 Method: 8081 B/8082A-Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.051 U 0.051 0.0075 ug/L 10/28/15 15:40 10/30/15 08:45 1 alpha-BHC 0.051 U 0.051 0.0080 ug/L 10/28/15 15:40 10/30/15 08:45 1 alpha-Chlordane 0.051 U 0.051 0.010 ug/L 10/28/15 15:40 10/30/15 08:45 1 beta-BHC 0.051 U 0.051 0.012 ug/L 10/28/15 15:40 10/30/15 08:45 1 4,4'-DDD 0.051 U 0.051 0.0079 ug/L 10/28/15 15:40 10/30/15 08:45 1 4,4'-DDE 0.051 U 0.051 0.0076 ug/L 10/28/15 15:40 10/30/15 08:45 1 4,4'-DDT 0.051 U 0.051 0.0087 ug/L 10/28/15 15:40 10/30/15 08:45 1 delta-BHC 0.051 U 0.051 0.013 ug/L 10/28/15 15:40 10/30/15 08:45 1 Dieldrin 0.051 U 0.051 0.0088 ug/L 10/28/15 15:40 10/30/15 08:45 1 Endosulfan I 0.051 U 0.051 0.0084 ug/L 10/28/15 15:40 10/30/15 08:45 1 Endosulfan II 0.051 U 0.051 0.0087 ug/L 10/28/15 15:40 10/30/15 08:45 1 Endosulfan sulfate 0.051 U 0.051 0.0085 ug/L 10/28/15 15:40 10/30/15 08:45 1 Endrin 0.051 U* 0.051 0.0090 ug/L 10/28/15 15:40 10/30/15 08:45 1 Endrin aldehyde 0.051 U 0.051 0.017 ug/L 10/28/15 15:40 10/30/15 08:45 1 Endrin ketone 0.051 U 0.051 0.0091 ug/L 10/28/15 15:40 10/30/15 08:45 1 gamma-BHC(Lindane) 0.051 U 0.051 0.0085 ug/L 10/28/15 15:40 10/30/15 08:45 1 gamma-Chlordane 0.051 U 0.051 0.0087 ug/L 10/28/15 15:40 10/30/15 08:45 1 Heptachlor 0.051 U 0.051 0.0081 ug/L 10/28/15 15:40 10/30/15 08:45 1 Heptachlor epoxide 0.051 U 0.051 0.0083 ug/L 10/28/15 15:40 10/30/15 08:45 1 Methoxychlor 0.051 U 0.051 0.0095 ug/L 10/28/15 15:40 10/30/15 08:45 1 Toxaphene 5.1 U 5.1 0.19 ug/L 10/28/15 15:40 10/30/15 08:45 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 43 10-130 10/28/15 15:40 10/30/15 08:45 1 Tetrachloro-m-xylene 59 39-130 10/28/15 15:40 10/30/15 08:45 1 it TestAmerica Savannah Page 51 of 81 7 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8260B -Volatile Organic Compounds (GC/MS ) Lab Sample ID: MB 680-407542/9 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407542 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 09:58 1 MB MB III Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Surr) 103 70-130 1027/15 09:58 1 1,2-Dichloroethane-d4(Surr) 108 70-130 1027/15 09:58 1 Dibromofluoromethane(Surr) 111 70-130 1027/15 09:58 1 4-Bromofluorobenzene(Surr) 98 70-130 1027/15 09:58 1 Lab Sample ID: LCS 680-407542/4 Client Sample ID: Lab Control Sample Matrix:Water Prep Type: Total/NA Analysis Batch: 407542 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Trichloroethene 50.0 52.0 ug/L 104 80-123 LCS LCS Surrogate %Recovery Qualifier Limits Toluene-d8(Surr) 98 70-130 1,2-Dichloroethane-d4(Surr) 101 70-130 Dibromofluoromethane(Surr) 105 70-130 4-Bromofluorobenzene(Surr) 97 70-130 Lab Sample ID: LCSD 680-407542/5 Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type: Total/NA Analysis Batch: 407542 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Trichloroethene 50.0 53.6 ug/L 107 80-123 3 20 LCSD LCSD Surrogate %Recovery Qualifier Limits Toluene-d8(Surr) 98 70-130 1,2-Dichloroethane-d4(Surr) 115 70-130 Dibromofluoromethane(Surr) 116 70-130 4-Bromofluorobenzene(Surr) 100 70-130 Lab Sample ID: MB 680-407549/9 Client Sample ID: Method Blank Matrix:Water Prep Type: Total/NA Analysis Batch: 407549 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Trichloroethene 1.0 U 1.0 0.48 ug/L 10/27/15 10:48 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Toluene-d8(Sun-) 99 70-130 1027/15 10:48 1 1,2-Dichloroethane-d4(Surr) 77 70-130 1027/15 10:48 1 Dibromofluoromethane(Sun-) 88 70-130 1027/15 10:48 1 4-Bromofluorobenzene(Surr) 96 70-130 1027/15 10:48 1 TestAmerica Savannah Page 52 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 680-407549/4 Client Sample ID: Lab Control Sample Matrix:Water Prep Type: Total/NA Analysis Batch: 407549 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Trichloroethene 50.0 46.0 ug/L 92 80-123 LCS LCS Surrogate %Recovery Qualifier Limits Toluene-d8(Surr) 92 70-130 1,2-Dichloroethane-d4(Surr) 89 70-130 Dibromofluoromethane(Surr) 93 70-130 4-Bromofluorobenzene(Surr) 83 70-130 rLab Sample ID: LCSD 680-407549/5 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 407549 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Trichloroethene 50.0 49.3 ug/L 99 80-123 7 20 LCSD LCSD Surrogate %Recovery Qualifier Limits Toluene-d8(Sun-) 99 70-130 1,2-Dichloroethane-d4(Sun-) 86 70-130 Dibromofluoromethane(Sun-) 94 70-130 4-Bromofluorobenzene(Surr) 87 70-130 Method: 8081 B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Lab Sample ID: MB 680-407400/21-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407953 Prep Batch: 407400 i MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/26/15 16:51 10/29/15 03:41 1 alpha-BHC 0.050 U 0.050 0.0078 ug/L 10/26/15 16:51 10/29/15 03:41 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/26/15 16:51 10/29/15 03:41 1 beta-BHC 0.050 U 0.050 0.012 ug/L 10/26/15 16:51 10/29/15 03:41 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/26/15 16:51 10/29/15 03:41 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/26/15 16:51 10/29/15 03:41 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 03:41 1 delta-BHC 0.050 U 0.050 0.013 ug/L 10/26/15 16:51 10/29/15 03:41 1 Dieldrin 0.050 U 0.050 0.0086 ug/L 10/26/15 16:51 10/29/15 03:41 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/26/15 16:51 10/29/15 03:41 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 03:41 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 03:41 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/26/15 16:51 10/29/15 03:41 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/26/15 16:51 10/29/15 03:41 1 Endrin ketone 0.050 U 0.050 0.0089 ug/L 10/26/15 16:51 10/29/15 03:41 1 gamma-BHC(Lindane) 0.050 U 0.050 0.0083 ug/L 10/26/15 16:51 10/29/15 03:41 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/26/15 16:51 10/29/15 03:41 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/26/15 16:51 10/29/15 03:41 1 TestAmerica Savannah Page 53 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8081 B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued) Lab Sample ID: MB 680-407400/21-A Client Sample ID: Method Blank Matrix:Water Prep Type: Total/NA Analysis Batch: 407953 Prep Batch: 407400 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/26/15 16:51 10/29/15 03:41 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/26/15 16:51 10/29/15 03:41 1 Toxaphene 5.0 U 5.0 0.19 ug/L 10/26/15 16:51 10/29/15 03:41 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 67 10-130 10/26/15 16:51 10/29/15 03:41 1 Tetrachloro-m-xylene 75 39-130 10/26/15 16:51 1029/15 03:41 1 Lab Sample ID: LCS 680-407400/22-A Client Sample ID: Lab Control Sample Matrix:Water Prep Type: Total/NA Analysis Batch: 407953 Prep Batch: 407400 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Aldrin 0.100 0.0796 ug/L 80 48-130 alpha-BHC 0.100 0.0923 ug/L 92 45-130 alpha-Chlordane 0.100 0.0868 ug/L 87 60-130 beta-BHC 0.100 0.0863 ug/L 86 50-130 4,4'-DDD 0.100 0.0818 ug/L 82 52-130 4,4'-DDE 0.100 0.0765 ug/L 77 48-130 4,4'-DDT 0.100 0.0725 ug/L 72 59-130 delta-BHC 0.100 0.0875 ug/L 87 47-140 Dieldrin 0.100 0.0848 ug/L 85 55-130 Endosulfan I 0.100 0.0843 ug/L 84 27-130 Endosulfan II 0.100 0.0842 ug/L 84 39-130 Endosulfan sulfate 0.100 0.0794 ug/L 79 57-130 Endrin 0.100 0.0807 ug/L 81 62-131 Endrin aldehyde 0.100 0.0789 ug/L 79 39-177 Endrin ketone 0.100 0.0846 ug/L 85 47-130 gamma-BHC(Lindane) 0.100 0.0861 ug/L 86 47-130 gamma-Chlordane 0.100 0.0855 ug/L 85 50-145 Heptachlor 0.100 0.0802 ug/L 80 49-130 Heptachlor epoxide 0.100 0.0865 ug/L 87 54-130 Methoxychlor 0.100 0.0702 ug/L 70 53-130 LCS LCS Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl 61 10-130 Tetrachloro-m-xylene 75 39-130 Lab Sample ID: LCSD 680-407400/23-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 407953 Prep Batch: 407400 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Aldrin 0.100 0.0834 ug/L 83 48-130 5 40 alpha-BHC 0.100 0.0962 ug/L 96 45-130 4 30 alpha-Chlordane 0.100 0.0915 ug/L 92 60-130 5 50 TestAmerica Savannah Page 54 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8081 B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued) Lab Sample ID: LCSD 680-407400/23-A Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type: Total/NA Analysis Batch: 407953 Prep Batch: 407400 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit beta-BHC 0.100 0.0917 ug/L 92 50-130 6 40 I 4,4'-DDD 0.100 0.0837 ug/L 84 52-130 2 40 4,4'-DDE 0.100 0.0827 ug/L 83 48-130 8 30 4,4'-DDT 0.100 0.0776 ug/L 78 59-130 7 40 delta-BHC 0.100 0.0926 ug/L 93 47-140 6 30 Dieldrin 0.100 0.0890 ug/L 89 55-130 5 30 Endosulfan I 0.100 0.0898 ug/L 90 27-130 6 30 Endosulfan II 0.100 0.0873 ug/L 87 39-130 4 30 Endosulfan sulfate 0.100 0.0814 ug/L 81 57-130 2 40 Endrin 0.100 0.0798 ug/L 80 62-131 1 30 Endrin aldehyde 0.100 0.0754 ug/L 75 39-177 4 40 Endrin ketone 0.100 0.0914 ug/L 91 47-130 8 40 gamma-BHC(Lindane) 0.100 0.0910 ug/L 91 47-130 6 30 gamma-Chlordane 0.100 0.0898 ug/L 90 50-145 5 50 Heptachlor 0.100 0.0822 ug/L 82 49-130 2 30 Heptachlor epoxide 0.100 0.0906 ug/L 91 54-130 5 40 Methoxychlor 0.100 0.0751 ug/L 75 53-130 7 40 LCSD LCSD Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl 65 10-130 Tetrachloro-m-xylene 76 39-130 Lab Sample ID: MB 680-407580/21-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 408014 Prep Batch: 407580 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/27/15 16:05 10/29/15 09:52 1 alpha-BHC 0.050 U 0.050 0.0078 ug/L 10/27/15 16:05 10/29/15 09:52 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/27/15 16:05 10/29/15 09:52 1 beta-BHC 0.050 U 0.050 0.012 ug/L 10/27/15 16:05 10/29/15 09:52 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/27/15 16:05 10/29/15 09:52 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/27/15 16:05 10/29/15 09:52 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/29/15 09:52 1 delta-BHC 0.050 U 0.050 0.013 ug/L 10/27/15 16:05 10/29/15 09:52 1 Dieldrin 0.050 U 0.050 0.0086 ug/L 10/27/15 16:05 10/29/15 09:52 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/27/15 16:05 10/29/15 09:52 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/29/15 09:52 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/27/15 16:05 10/29/15 09:52 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/27/15 16:05 10/29/15 09:52 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/27/15 16:05 10/29/15 09:52 1 Endrin ketone 0.050 U 0.050 0.0089 ug/L 10/27/15 16:05 10/29/15 09:52 1 gamma-BHC(Lindane) 0.050 U 0.050 0.0083 ug/L 10/27/15 16:05 10/29/15 09:52 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/27/15 16:05 10/29/15 09:52 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/27/15 16:05 10/29/15 09:52 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/27/15 16:05 10/29/15 09:52 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/27/15 16:05 10/29/15 09:52 1 TestAmerica Savannah Page 55 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8081 B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued) Lab Sample ID: MB 680-407580/21-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 408014 Prep Batch: 407580 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Toxaphene 5.0 U 5.0 0.19 ug/L 10/27/15 16:05 10/29/15 09:52 1 r MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 65 10-130 10/27/15 16:05 10/29/15 09:52 1 Tetrachloro-m-xylene 80 39-130 10/27/15 16:05 10/29/15 09:52 1 Lab Sample ID: LCS 680-407580/22-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 408014 Prep Batch:407580 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Aldrin 0.100 0.0948 ug/L 95 48-130 alpha-BHC 0.100 0.0948 ug/L 95 45-130 alpha-Chlordane 0.100 0.0917 ug/L 92 60-130 beta-BHC 0.100 0.0908 ug/L 91 50-130 4,4'-DDD 0.100 0.0851 ug/L 85 52-130 4,4'-DDE 0.100 0.0853 ug/L 85 48-130 4,4'-DDT 0.100 0.0768 ug/L 77 59-130 delta-BHC 0.100 0.0924 ug/L 92 47-140 Dieldrin 0.100 0.0890 ug/L 89 55-130 Endosulfan I 0.100 0.0879 ug/L 88 27-130 Endosulfan II 0.100 0.0866 ug/L 87 39-130 Endosulfan sulfate 0.100 0.0825 ug/L 82 57-130 Endrin 0.100 0.0836 ug/L 84 62-131 Endrin aldehyde 0.100 0.0779 ug/L 78 39-177 Endrin ketone 0.100 0.0877 ug/L 88 47-130 gamma-BHC(Lindane) 0.100 0.0889 ug/L 89 47-130 gamma-Chlordane 0.100 0.0905 ug/L 90 50-145 Heptachlor 0.100 0.0875 ug/L 88 49-130 Heptachlor epoxide 0.100 0.0901 ug/L 90 54-130 Methoxychlor 0.100 0.0749 ug/L 75 53-130 LCS LCS Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl 70 10-130 Tetrachloro-m-xylene 73 39-130 Lab Sample ID: LCSD 680-407580/23-A Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type: Total/NA Analysis Batch: 408014 Prep Batch:407580 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Aldrin 0.100 0.0805 ug/L 81 48-130 16 40 alpha-BHC 0.100 0.0808 ug/L 81 45-130 16 30 alpha-Chlordane 0.100 0.0797 ug/L 80 60-130 14 50 beta-BHC 0.100 0.0801 ug/L 80 50-130 13 40 4,4'-DDD 0.100 0.0760 ug/L 76 52-130 11 40 TestAmerica Savannah Page 56 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8081 B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued) Lab Sample ID: LCSD 680-407580/23-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 408014 Prep Batch: 407580 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit 4,4'-DDE 0.100 0.0756 ug/L 76 48-130 12 30 I 4,4'-DDT 0.100 0.0685 ug/L 68 59-130 11 40 delta-BHC 0.100 0.0818 ug/L 82 47-140 12 30 Dieldrin 0.100 0.0759 ug/L 76 55-130 16 30 Endosulfan I 0.100 0.0765 ug/L 76 27-130 14 30 Endosulfan II 0.100 0.0759 ug/L 76 39-130 13 30 Endosulfan sulfate 0.100 0.0717 ug/L 72 57-130 14 40 Endrin 0.100 0.0742 ug/L 74 62-131 12 30 Endrin aldehyde 0.100 0.0742 ug/L 74 39-177 5 40 Endrin ketone 0.100 0.0782 ug/L 78 47-130 11 40 gamma-BHC(Lindane) 0.100 0.0762 ug/L 76 47-130 15 30 gamma-Chlordane 0.100 0.0787 ug/L 79 50-145 14 50 Heptachlor 0.100 0.0764 ug/L 76 49-130 14 30 Heptachlor epoxide 0.100 0.0769 ug/L 77 54-130 16 40 Methoxychlor 0.100 0.0688 ug/L 69 53-130 9 40 LCSD LCSD Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl 53 10-130 Tetrachloro-m-xylene 67 39-130 Lab Sample ID: MB 680-407762/13-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 408178 Prep Batch: 407762 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin 0.050 U 0.050 0.0073 ug/L 10/28/15 15:40 10/30/15 06:34 1 alpha-BHC 0.050 U 0.050 0.0078 ug/L 10/28/15 15:40 10/30/15 06:34 1 alpha-Chlordane 0.050 U 0.050 0.010 ug/L 10/28/15 15:40 10/30/15 06:34 1 beta-BHC 0.050 U 0.050 0.012 ug/L 10/28/15 15:40 10/30/15 06:34 1 4,4'-DDD 0.050 U 0.050 0.0077 ug/L 10/28/15 15:40 10/30/15 06:34 1 4,4'-DDE 0.050 U 0.050 0.0074 ug/L 10/28/15 15:40 10/30/15 06:34 1 4,4'-DDT 0.050 U 0.050 0.0085 ug/L 10/28/15 15:40 10/30/15 06:34 1 delta-BHC 0.050 U 0.050 0.013 ug/L 10/28/15 15:40 10/30/15 06:34 1 Dieldrin 0.050 U 0.050 0.0086 ug/L 10/28/15 15:40 10/30/15 06:34 1 Endosulfan I 0.050 U 0.050 0.0082 ug/L 10/28/15 15:40 10/30/15 06:34 1 Endosulfan II 0.050 U 0.050 0.0085 ug/L 10/28/15 15:40 10/30/15 06:34 1 Endosulfan sulfate 0.050 U 0.050 0.0083 ug/L 10/28/15 15:40 10/30/15 06:34 1 Endrin 0.050 U 0.050 0.0088 ug/L 10/28/15 15:40 10/30/15 06:34 1 Endrin aldehyde 0.050 U 0.050 0.017 ug/L 10/28/15 15:40 10/30/15 06:34 1 Endrin ketone 0.050 U 0.050 0.0089 ug/L 10/28/15 15:40 10/30/15 06:34 1 gamma-BHC(Lindane) 0.050 U 0.050 0.0083 ug/L 10/28/15 15:40 10/30/15 06:34 1 gamma-Chlordane 0.050 U 0.050 0.0085 ug/L 10/28/15 15:40 10/30/15 06:34 1 Heptachlor 0.050 U 0.050 0.0079 ug/L 10/28/15 15:40 10/30/15 06:34 1 Heptachlor epoxide 0.050 U 0.050 0.0081 ug/L 10/28/15 15:40 10/30/15 06:34 1 Methoxychlor 0.050 U 0.050 0.0093 ug/L 10/28/15 15:40 10/30/15 06:34 1 Toxaphene 5.0 U 5.0 0.19 ug/L 10/28/15 15:40 10/30/15 06:34 1 TestAmerica Savannah Page 57 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8081 B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued) Lab Sample ID: MB 680-407762/13-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 408178 Prep Batch: 407762 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac DCB Decachlorobiphenyl 57 10-130 10/28/15 15:40 10/30/15 06:34 1 Tetrachloro-m-xylene 74 39-130 10/28/15 15:40 10/30/15 06:34 1 Lab Sample ID: LCS 680-407762/14-A Client Sample ID: Lab Control Sample Matrix:Water Prep Type: Total/NA Analysis Batch: 408178 Prep Batch: 407762 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Aldrin 0.100 0.0661 ug/L 66 48-130 alpha-BHC 0.100 0.0674 ug/L 67 45-130 alpha-Chlordane 0.100 0.0673 ug/L 67 60-130 beta-BHC 0.100 0.0677 ug/L 68 50-130 4,4'-DDD 0.100 0.0627 ug/L 63 52-130 4,4'-DDE 0.100 0.0609 ug/L 61 48-130 4,4'-DDT 0.100 0.0593 ug/L 59 59-130 delta-BHC 0.100 0.0635 ug/L 64 47-140 Dieldrin 0.100 0.0666 ug/L 67 55-130 Endosulfan I 0.100 0.0620 ug/L 62 27-130 Endosulfan II 0.100 0.0644 ug/L 64 39-130 Endosulfan sulfate 0.100 0.0650 ug/L 65 57-130 Endrin 0.100 0.0552 * ug/L 55 62-131 Endrin aldehyde 0.100 0.0601 ug/L 60 39-177 Endrin ketone 0.100 0.0632 p ug/L 63 47-130 gamma-BHC(Lindane) 0.100 0.0641 ug/L 64 47-130 gamma-Chlordane 0.100 0.0662 ug/L 66 50-145 Heptachlor 0.100 0.0629 ug/L 63 49-130 Heptachlor epoxide 0.100 0.0659 ug/L 66 54-130 Methoxychlor 0.100 0.0626 ug/L 63 53-130 LCS LCS Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl 41 10-130 Tetrachloro-m-xylene 60 39-130 Lab Sample ID: LCSD 680-407762/15-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 408178 Prep Batch: 407762 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Aldrin 0.100 0.0836 ug/L 84 48-130 23 40 alpha-BHC 0.100 0.0819 ug/L 82 45-130 19 30 alpha-Chlordane 0.100 0.0790 ug/L 79 60-130 16 50 beta-BHC 0.100 0.0786 ug/L 79 50-130 15 40 4,4'-DDD 0.100 0.0730 ug/L 73 52-130 15 40 4,4'-DDE 0.100 0.0696 ug/L 70 48-130 13 30 4,4'-DDT 0.100 0.0725 ug/L 73 59-130 20 40 delta-BHC 0.100 0.0804 ug/L 80 47-140 23 30 TestAmerica Savannah Page 58 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 8081B/8082A - Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography (Continued) Lab Sample ID: LCSD 680-407762/15-A Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 408178 Prep Batch: 407762 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Dieldrin 0.100 0.0791 ug/L 79 55-130 17 30 I Endosulfan I 0.100 0.0768 ug/L 77 27-130 21 30 Endosulfan II 0.100 0.0788 ug/L 79 39-130 20 30 Endosulfan sulfate 0.100 0.0792 ug/L 79 57.130 20 40 Endrin 0.100 0.0699 ug/L 70 62-131 24 30 Endrin aldehyde 0.100 0.0774 ug/L 77 39-177 25 40 Endrin ketone 0.100 0.0844 ug/L 84 47-130 29 40 gamma-BHC(Lindane) 0.100 0.0756 ug/L 76 47.130 16 30 gamma-Chlordane 0.100 0.0779 ug/L 78 50-145 16 50 Heptachlor 0.100 0.0732 ug/L 73 49-130 15 30 Heptachlor epoxide 0.100 0.0780 ug/L 78 54-130 17 40 Methoxychlor 0.100 0.0781 ug/L 78 53-130 22 40 LCSD LCSD Surrogate %Recovery Qualifier Limits DCB Decachlorobiphenyl 54 10-130 Tetrachloro-m-xylene 62 39-130 Method: 160.2 -Solids, Total Suspended (TSS) Lab Sample ID: MB 680-407486/1 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 407486 MB MB Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 1.0 U 1.0 1.0 mg/L 10/26/15 15:13 1 Lab Sample ID: LCS 680-407486/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 407486 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 20.0 20.5 mg/L 103 80-120 Lab Sample ID: LCSD 680-407486/3 Client Sample ID: Lab Control Sample Dup Matrix: Water Prep Type: Total/NA Analysis Batch: 407486 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 20.0 21.0 mg/L 105 80.120 2 25 Lab Sample ID: 680-118203-4 DU Client Sample ID: SW-04 Matrix: Water Prep Type: Total/NA Analysis Batch: 407486 Sample Sample DU DU RPD Analyte Result Qualifier Result Qualifier Unit D RPD Limit LTotal Suspended Solids 8.0 7.60 mg/L 5 5 TestAmerica Savannah Page 59 of 81 QC Sample Results Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Method: 160.2 - Solids, Total Suspended (TSS) (Continued) Lab Sample ID: MB 680-407601/1 Client Sample ID: Method Blank Matrix:Water Prep Type: Total/NA Analysis Batch: 407601 MB MB Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Total Suspended Solids 1.0 U 1.0 1.0 mg/L 10/27/15 11:02 1 Lab Sample ID: LCS 680-407601/2 Client Sample ID: Lab Control Sample T Matrix:Water Prep Type: Total/NA Analysis Batch: 407601 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 20.0 23.0 mg/L 115 80-120 Lab Sample ID: LCSD 680-407601/3 Client Sample ID: Lab Control Sample Dup Matrix:Water Prep Type: Total/NA Analysis Batch: 407601 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 20.0 22.0 mg/L 110 80-120 4 25 TestAmerica Savannah Page 60 of 81 QC Association Summary Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. GC/MS VOA Analysis Batch: 407542 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-12 Influent Total/NA Water 8260B 680-118203-13 Effluent Total/NA Water 8260B 680-118203-14 Carbon Train A-1 Total/NA Water 8260B 680-118203-15 Carbon Train B-2 Total/NA Water 8260E 680-118203-17 MW-30D Total/NA Water 8260E 680-118203-22 MW-18D Total/NA Water 8260E 680-118203-25 Duplicate 2 Total/NA Water 8260E 680-118203-27 Duplicate 1 Total/NA Water 8260E 680-118203-29 MW-10S Total/NA Water 8260E 680-118203-31 MW-18S Total/NA Water 8260E 680-118203-34 MW-16S Total/NA Water 8260B LCS 680-407542/4 Lab Control Sample Total/NA Water 8260E LCSD 680-407542/5 Lab Control Sample Dup Total/NA Water 8260E MB 680-407542/9 Method Blank Total/NA Water 8260E Analysis Batch: 407549 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-35 MW-17S Total/NA Water 8260B 680-118203-36 MW-16D Total/NA Water 8260B 680-118203-37 MW-17D Total/NA Water 8260B LCS 680-407549/4 Lab Control Sample Total/NA Water 8260B LCSD 680-407549/5 Lab Control Sample Dup Total/NA Water 8260B MB 680-407549/9 Method Blank Total/NA Water 8260B GC Semi VOA Prep Batch: 407400 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-1 SW-01 Total/NA Water 3520C 680-118203-2 SW-02 Total/NA Water 3520C 680-118203-3 SW-03 Total/NA Water 3520C 680-118203-4 SW-04 Total/NA Water 3520C 680-118203-5 SW-05 Total/NA Water 3520C 680-118203-6 SW-11-2 Total/NA Water 3520C 680-118203-7 SW-06 Total/NA Water 3520C 680-118203-26 MW-6S Total/NA Water 3520C 680-118203-27 Duplicate 1 Total/NA Water 3520C 680-118203-28 MW-4S Total/NA Water 3520C 680-118203-29 MW-10S Total/NA Water 3520C 680-118203-30 MW-5S Total/NA Water 3520C 680-118203-31 MW-18S Total/NA Water 3520C 680-118203-32 MW-22D Total/NA Water 3520C 680-118203-33 MW-22L Total/NA Water 3520C 680-118203-34 MW-16S Total/NA Water 3520C 680-118203-35 MW-17S Total/NA Water 3520C LCS 680-407400/22-A Lab Control Sample Total/NA Water 3520C LCSD 680-407400/23-A Lab Control Sample Dup Total/NA Water 3520C MB 680-407400/21-A Method Blank Total/NA Water 3520C TestAmerica Savannah Page 61 of 81 QC Association Summary Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. GC Semi VOA (Continued) Prep Batch: 407580 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-8 SW-07 Total/NA Water 3520C 680-118203-9 SW-08 Total/NA Water 3520C 680-118203-10 SW-09 Total/NA Water 3520C 680-118203-11 SW Duplicate Total/NA Water 3520C 680-118203-12 Influent Total/NA Water 3520C 680-118203-13 Effluent Total/NA Water 3520C 680-118203-14 Carbon Train A-1 Total/NA Water 3520C k 680-118203-15 Carbon Train B-2 Total/NA Water 3520C 680-118203-17 MW-30D Total/NA Water 3520C 680-118203-18 PZ-2 Total/NA Water 3520C 680-118203-19 PZ-3 Total/NA Water 3520C 680-118203-20 MW-27L Total/NA Water 3520C 680-118203-21 MW-36L Total/NA Water 3520C 680-118203-22 MW-18D TotaUNA Water 3520C 680-118203-23 MW-39L Total/NA Water 3520C 680-118203-24 MW-31 L Total/NA Water 3520C 680-118203-25 Duplicate 2 Total/NA Water 3520C 680-118203-38 MW-26D Total/NA Water 3520C 680-118203-39 MW-25L Total/NA Water 3520C 680-118203-40 MW-37L Total/NA Water 3520C LCS 680-407580/22-A Lab Control Sample Total/NA Water 3520C LCSD 680-407580/23-A Lab Control Sample Dup Total/NA Water 3520C MB 680-407580/21-A Method Blank Total/NA Water 3520C Prep Batch: 407762 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-41 PZ-5 Total/NA Water 3520C 680-118203-42 MW-23D Total/NA Water 3520C 680-118203-43 MW-38L Total/NA Water 3520C 680-118203-44 MW-40L Total/NA Water 3520C 680-118203-45 MW-32L Total/NA Water 3520C 680-118203-46 Duplicate 3 Total/NA Water 3520C LCS 680-407762/14-A Lab Control Sample Total/NA Water 3520C LCSD 680-407762/15-A Lab Control Sample Dup Total/NA Water 3520C MB 680-407762/13-A Method Blank Total/NA Water 3520C Analysis Batch: 407953 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-1 SW-01 Tota/NA Water 8081B/8082A 407400 680-118203-2 SW-02 Total/NA Water 8081B/8082A 407400 680-118203-3 SW-03 Total/NA Water 8081B/8082A 407400 680-118203-4 SW-04 Total/NA Water 8081 B/8082A 407400 680-118203-5 SW-05 Total/NA Water 8081 B/8082A 407400 680-118203-6 SW-11-2 Total/NA Water 8081B/8082A 407400 680-118203-7 SW-06 Total/NA Water 8081 B/8082A 407400 680-118203-28 MW-4S Total/NA Water 8081B/8082A 407400 680-118203-29 MW-10S Total/NA Water 8081B/8082A 407400 680-118203-31 MW-18S Total/NA Water 8081B/8082A 407400 680-118203-32 MW-22D Total/NA Water 8081B/8082A 407400 680-118203-34 MW-16S Total/NA Water 8081B/8082A 407400 680-118203-35 MW-17S Total/NA Water 8081 B/8082A 407400 TestAmerica Savannah Page 62 of 81 QC Association Summary Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. GC Semi VOA (Continued) Analysis Batch: 407953 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCS 680-407400/22-A Lab Control Sample Total/NA Water 8081 B/8082A 407400 LCSD 680-407400/23-A Lab Control Sample Dup Total/NA Water 8081 B/8082A 407400 MB 680-407400/21-A Method Blank Total/NA Water 8081B/8082A 407400 Analysis Batch: 408014 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-8 SW-07 Total/NA Water 8081B/8082A 407580 I 680-118203-9 SW-08 Total/NA Water 8081 B/8082A 407580 680-118203-10 SW-09 Total/NA Water 8081B/8082A 407580 680-118203-11 SW Duplicate Total/NA Water 8081B/8082A 407580 680-118203-13 Effluent Total/NA Water 8081B/8082A 407580 680-118203-14 Carbon Train A-1 Total/NA Water 8081B/8082A 407580 680-118203-15 Carbon Train B-2 Total/NA Water 8081 B/8082A 407580 680-118203-18 PZ-2 Total/NA Water 8081 B/8082A 407580 680-118203-26 MW-6S Total/NA Water 8081 B/8082A 407400 680-118203-26 MW-6S Total/NA Water 8081B/8082A 407400 680-118203-27 Duplicate 1 Total/NA Water 8081B/8082A 407400 680-118203-30 MW-5S Total/NA Water 8081 B/8082A 407400 680-118203-30 MW-5S Total/NA Water 8081B/8082A 407400 680-118203-33 MW-22L Total/NA Water 8081B/8082A 407400 LCS 680-407580/22-A Lab Control Sample Total/NA Water 8081 B/8082A 407580 LCSD 680-407580/23-A Lab Control Sample Dup Total/NA Water 8081 B/8082A 407580 MB 680-407580/21-A Method Blank Total/NA Water 8081B/8082A 407580 Analysis Batch: 408124 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-12 Influent Total/NA Water 8081B/8082A 407580 680-118203-12 Influent Total/NA Water 8081 B/8082A 407580 680-118203-17 MW-30D Total/NA Water 8081 B/8082A 407580 680-118203-17 MW-30D Total/NA Water 8081 B/8082A 407580 680-118203-19 PZ-3 Total/NA Water 8081B/8082A 407580 680-118203-21 MW-36L Total/NA Water 8081B/8082A 407580 680-118203-23 MW-39L Total/NA Water 8081B/8082A 407580 680-118203-26 MW-6S Total/NA Water 8081B/8082A 407400 680-118203-29 MW-10S Total/NA Water 8081B/8082A 407400 680-118203-38 MW-26D Total/NA Water 8081 B/8082A 407580 680-118203-39 MW-25L Total/NA Water 8081 B/8082A 407580 680-118203-39 MW-25L Total/NA Water 8081 B/8082A 407580 680-118203-40 MW-37L Total/NA Water 8081 B/8082A 407580 680-118203-40 MW-37L Total/NA Water 8081 B/8082A 407580 Analysis Batch: 408178 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-20 MW-27L Total/NA Water 8081B/8082A 407580 680-118203-20 MW-27L Total/NA Water 8081 B/8082A 407580 680-118203-42 MW-23D Total/NA Water 8081 B/8082A 407762 680-118203-43 MW-38L Total/NA Water 8081 B/8082A 407762 680-118203-44 MW-40L Total/NA Water 8081B/8082A 407762 680-118203-45 MW-32L Total/NA Water 8081B/8082A 407762 680-118203-46 Duplicate 3 Total/NA Water 8081B/8082A 407762 LCS 680-407762/14-A Lab Control Sample Total/NA Water 8081B/8082A 407762 TestAmerica Savannah Page 63 of 81 QC Association Summary Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. GC Semi VOA (Continued) Analysis Batch: 408178 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch LCSD 680-407762/15-A Lab Control Sample Dup Total/NA Water 8081B/8082A 407762 MB 680-407762/13-A Method Blank Total/NA Water 8081B/8082A 407762 Analysis Batch: 408260 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-22 MW-18D Total/NA Water 8081 B/8082A 407580 680-118203-22 MW-18D Total/NA Water 8081B/8082A 407580 6 680-118203-24 MW-31 L Total/NA Water 8081 B/8082A 407580 680-118203-24 MW-31 L Total/NA Water 8081 B/8082A 407580 680-118203-25 Duplicate 2 Total/NA Water 8081B/8082A 407580 680-118203-25 Duplicate 2 Total/NA Water 8081B/8082A 407580 680-118203-41 PZ-5 Total/NA Water 8081B/8082A 407762 680-118203-41 PZ-5 Total/NA Water 8081 B/8082A 407762 General Chemistry Analysis Batch: 407486 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-1 SW-01 Total/NA Water 160.2 680-118203-2 SW-02 Total/NA Water 160.2 680-118203-3 SW-03 Total/NA Water 160.2 680-118203-4 SW-04 Total/NA Water 160.2 680-118203-4 DU SW-04 Total/NA Water 160.2 680-118203-5 SW-05 Total/NA Water 160.2 680-118203-6 SW-11-2 Total/NA Water 160.2 680-118203-7 SW-06 Total/NA Water 160.2 680-118203-8 SW-07 Total/NA Water 160.2 LCS 680-407486/2 Lab Control Sample Total/NA Water 160.2 LCSD 680-407486/3 Lab Control Sample Dup Total/NA Water 160.2 MB 680-407486/1 Method Blank Total/NA Water 160.2 Analysis Batch: 407601 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-118203-9 SW-08 Total/NA Water 160.2 680-118203-10 SW-09 Total/NA Water 160.2 680-118203-11 SW Duplicate Total/NA Water 160.2 LCS 680-407601/2 Lab Control Sample Total/NA Water 160.2 LCSD 680-407601/3 Lab Control Sample Dup Total/NA Water 160.2 MB 680-407601/1 Method Blank Total/NA Water 160.2 TestAmerica Savannah Page 64 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-01 Lab Sample ID: 680-118203-1 Date Collected: 10/21/15 09:36 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotalNA Analysis 8081B/8082A 1 407953 10/29/15 05:23 JCK TAL SAV TotaUNA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV Client Sample ID: SW-02 Lab Sample ID: 680-118203-2 Date Collected: 10/21/15 10:07 Matrix: Water 1 Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 407953 10/29/15 05:37 JCK TAL SAV Total/NA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV Client Sample ID: SW-03 Lab Sample ID: 680-118203-3 Date Collected: 10/21/15 10:32 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 407953 10/29/15 05:52 JCK TAL SAV TotaUNA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV Client Sample ID: SW-04 Lab Sample ID: 680-118203-4 Date Collected: 10/21/15 11:04 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 407953 10/29/15 06:06 JCK TAL SAV TotaUNA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV Client Sample ID: SW-05 Lab Sample ID: 680-118203-5 Date Collected: 10/21/15 11:17 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 407953 10/29/15 06:21 JCK TAL SAV TotaUNA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV TestAmerica Savannah Page 65 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW-11-2 Lab Sample ID: 680-118203-6 Date Collected: 10/21/15 11:38 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaVNA Analysis 8081B/8082A 1 407953 10/29/15 06:36 JCK TAL SAV Total/NA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV Client Sample ID: SW-06 Lab Sample ID: 680-118203-7 Date Collected: 10/21/15 12:05 Matrix:Water l Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaVNA Analysis 8081 B/8082A 1 407953 10/29/15 06:50 JCK TAL SAV TotaVNA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV Client Sample ID: SW-07 Lab Sample ID: 680-118203-8 Date Collected: 10/21/15 13:19 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081 B/8082A 1 408014 10/29/15 12:47 JCK TAL SAV TotaVNA Analysis 160.2 1 407486 10/26/15 15:13 KLD TAL SAV Client Sample ID: SW-08 Lab Sample ID: 680-118203-9 Date Collected: 10/21/15 13:39 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081B/8082A 1 408014 10/29/15 13:01 JCK TAL SAV TotaVNA Analysis 160.2 1 407601 10/27/15 11:02 KLD TAL SAV Client Sample ID: SW-09 Lab Sample ID: 680-118203-10 Date Collected: 10/21/15 13:52 Matrix:Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081B/8082A 1 408014 10/29/15 13:16 JCK TAL SAV TotaVNA Analysis 160.2 1 407601 10/27/15 11:02 KLD TAL SAV TestAmerica Savannah Page 66 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: SW Duplicate Lab Sample ID: 680-118203-11 Date Collected: 10/21/15 13:26 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081B/8082A 1 408014 10/29/15 13:30 JCK TAL SAV TotaVNA Analysis 160.2 1 407601 10/27/15 11:02 KLD TAL SAV Client Sample ID: Influent Lab Sample ID: 680-118203-12 Date Collected: 10/21/15 14:32 Matrix: Water • Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Analysis 8260B 1 407542 10/27/15 13:18 CEJ TAL SAV TotaVNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081B/8082A 1 408124 10/29/15 21:51 JCK TAL SAV TotaVNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081 B/8082A 5 408124 10/29/15 22:06 JCK TAL SAV Client Sample ID: Effluent Lab Sample ID: 680-118203-13 Date Collected: 10/21/15 14:38 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260E 1 407542 10/27/15 13:40 CEJ TAL SAV Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081B/8082A 1 408014 10/29/15 13:45 JCK TAL SAV Client Sample ID: Carbon Train A-1 Lab Sample ID: 680-118203-14 Date Collected: 10/21/15 14:47 Matrix:Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Analysis 8260B 1 407542 10/27/15 14:01 CEJ TAL SAV TotaVNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 408014 10/29/15 13:59 JCK TAL SAV Client Sample ID: Carbon Train B-2 Lab Sample ID: 680-118203-15 Date Collected: 10/21/15 15:03 Matrix:Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Analysis 8260E 1 407542 10/27/15 14:23 CEJ TAL SAV TotaVNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaVNA Analysis 8081B/8082A 1 408014 10/29/15 14:14 JCK TAL SAV TestAmerica Savannah Page 67 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-30D Lab Sample ID: 680-118203-17 Date Collected: 10/21/15 10:50 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407542 10/27/15 14:44 CEJ TAL SAV Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081B/8082A 1 408124 10/29/15 22:20 JCK TAL SAV Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081 B/8082A 10 408124 10/29/15 22:35 JCK TAL SAV Client Sample ID: PZ-2 Lab Sample ID: 680-118203-18 I Date Collected: 10/21/15 13:30 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081 B/8082A 1 408014 10/29/15 14:28 JCK TAL SAV Client Sample ID: PZ-3 Lab Sample ID: 680-118203-19 ' Date Collected: 10/21/15 12:50 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081B/8082A 1 408124 10/29/15 19:55 JCK TAL SAV Client Sample ID: MW-27L Lab Sample ID: 680-118203-20 Date Collected: 10/21/15 12:00 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 408178 10/30/15 10:42 JCK TAL SAV Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081B/8082A 4 408178 10/30/15 10:56 JCK TAL SAV Client Sample ID: MW-36L Lab Sample ID: 680-118203-21 Date Collected: 10/21/15 10:59 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 408124 10/29/15 20:10 JCK TAL SAV TestAmerica Savannah Page 68 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-18D Lab Sample ID: 680-118203-22 Date Collected: 10/21/15 11:49 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Analysis 8260B 1 407542 10/27/15 15:06 CEJ TAL SAV TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 408260 10/30/15 14:47 JCK TAL SAV TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 10 408260 10/30/15 15:02 JCK TAL SAV Client Sample ID: MW-39L Lab Sample ID: 680-118203-23 I Date Collected: 10/21/15 14:12 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081B/8082A 1 408124 10/29/15 20:24 JCK TAL SAV Client Sample ID: MW-31L Lab Sample ID: 680-118203-24 Date Collected: 10/21/15 14:16 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081B/8082A 1 408260 10/30/15 15:18 JCK TAL SAV TotalNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 4 408260 10/30/15 15:33 JCK TAL SAV Client Sample ID: Duplicate 2 Lab Sample ID: 680-118203-25 Date Collected: 10/21/15 10:50 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Analysis 8260E 1 407542 10/27/15 15:27 CEJ TAL SAV Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 408260 10/30/15 15:48 JCK TAL SAV TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081 B/8082A 4 408260 10/30/15 16:04 JCK TAL SAV Client Sample ID: MW-6S Lab Sample ID: 680-118203-26 Date Collected: 10/20/15 14:19 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotalNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 408014 10/29/15 10:36 JCK TAL SAV Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TestAmerica Savannah Page 69 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-6S Lab Sample ID: 680-118203-26 Date Collected: 10/20/15 14:19 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab 1 TotaUNA Analysis 8081B/8082A 10 408014 10/29/15 10:50 JCK TAL SAV TotaUNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaUNA Analysis 8081B/8082A 25 408124 10/29/15 17:59 JCK TAL SAV Client Sample ID: Duplicate 1 Lab Sample ID: 680-118203-27 Date Collected: 10/20/15 15:04 Matrix: Water Date Received: 10/23/15 09:44 I. Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Analysis 8260E 1 407542 10/27/15 15:49 CEJ TAL SAV Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotalNA Analysis 8081B/8082A 1 408014 10/29/15 11:05 JCK TAL SAV Client Sample ID: MW-4S Lab Sample ID: 680-118203-28 Date Collected: 10/20/15 13:28 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 407953 10/29/15 07:05 JCK TAL SAV Client Sample ID: MW-10S Lab Sample ID: 680-118203-29 Date Collected: 10/20/15 11:14 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Analysis 8260B 1 407542 10/27/15 16:10 CEJ TAL SAV Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081B/8082A 1 407953 10/29/15 07:19 JCK TAL SAV TotalNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081 B/8082A 4 408124 10/29/15 18:13 JCK TAL SAV Client Sample ID: MW-5S Lab Sample ID: 680-118203-30 Date Collected: 10/20/15 12:02 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 408014 10/29/15 11:34 JCK TAL SAV Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081B/8082A 4 408014 10/29/15 11:49 JCK TAL SAV TestAmerica Savannah Page 70 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-18S Lab Sample ID: 680-118203-31 Date Collected: 10/20/15 15:04 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Analysis 8260B 1 407542 10/27/15 16:32 CEJ TAL SAV Total/NA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 407953 10/29/15 07:34 JCK TAL SAV Client Sample ID: MW-22D Lab Sample ID: 680-118203-32 Date Collected: 10/20/15 15:47 Matrix:Water • Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaVNA Analysis 8081 B/8082A 1 407953 10/29/15 07:48 JCK TAL SAV Client Sample ID: MW-22L Lab Sample ID: 680-118203-33 Date Collected: 10/20/15 15:21 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaVNA Analysis 8081 B/8082A 1 408014 10/29/15 12:18 JCK TAL SAV Client Sample ID: MW-16S Lab Sample ID: 680-118203-34 Date Collected: 10/20/15 13:23 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaVNA Analysis 8260B 1 407542 10/27/15 16:53 CEJ TAL SAV TotaVNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaVNA Analysis 8081 B/8082A 1 407953 10/29/15 08:03 JCK TAL SAV Client Sample ID: MW-17S Lab Sample ID: 680-118203-35 Date Collected: 10/20/15 14:09 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407549 10/27/15 14:07 CEJ TAL SAV TotaVNA Prep 3520C 407400 10/26/15 16:51 RBS TAL SAV TotaVNA Analysis 8081 B/8082A 1 407953 10/29/15 08:18 JCK TAL SAV TestAmerica Savannah Page 71 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: MW-16D Lab Sample ID: 680-118203-36 Date Collected: 10/20/15 11:38 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407549 10/27/15 13:45 CEJ TAL SAV L Client Sample ID: MW-17D Lab Sample ID: 680-118203-37 Date Collected: 10/20/15 12:23 Matrix:Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared I Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 407549 10/27/15 14:30 CEJ TAL SAV Client Sample ID: MW-26D Lab Sample ID: 680-118203-38 Date Collected: 10/21/15 17:06 Matrix:Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 408124 10/29/15 20:39 JCK TAL SAV Client Sample ID: MW-25L Lab Sample ID: 680-118203-39 Date Collected: 10/21/15 15:17 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 1 408124 10/29/15 20:53 JCK TAL SAV TotaUNA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081B/8082A 4 408124 10/29/15 21:08 JCK TAL SAV Client Sample ID: MW-37L Lab Sample ID: 680-118203-40 Date Collected: 10/21/15 16:02 Matrix:Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV Total/NA Analysis 8081B/8082A 1 408124 10/29/15 21:22 JCK TAL SAV Total/NA Prep 3520C 407580 10/27/15 16:05 RBS TAL SAV TotaUNA Analysis 8081B/8082A 4 408124 10/29/15 21:37 JCK TAL SAV TestAmerica Savannah Page 72 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: PZ-5 Lab Sample ID: 680-118203-41 Date Collected: 10/21/15 15:55 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotalNA Prep 3520C 407762 10/28/15 15:40 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 408260 10/30/15 17:50 JCK TAL SAV TotaUNA Prep 3520C 407762 10/28/15 15:40 RBS TAL SAV Total/NA Analysis 8081 B/8082A 4 408260 10/30/15 18:05 JCK TAL SAV Client Sample ID: MW-23D Lab Sample ID: 680-118203-42 Date Collected: 10/22/15 13:40 Matrix: Water I Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407762 10/28/15 15:40 RBS TAL SAV TotaUNA Analysis 8081 B/8082A 1 408178 10/30/15 07:47 JCK TAL SAV Client Sample ID: MW-38L Lab Sample ID: 680-118203-43 Date Collected: 10/22/15 12:31 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407762 10/28/15 15:40 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 408178 10/30/15 08:01 JCK TAL SAV Client Sample ID: MW-40L Lab Sample ID: 680-118203-44 Date Collected: 10/22/15 13:03 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407762 10/28/15 15:40 RBS TAL SAV Total/NA Analysis 8081 B/8082A 1 408178 10/30/15 08:16 JCK TAL SAV Client Sample ID: MW-32L Lab Sample ID: 680-118203-45 Date Collected: 10/22/15 11:44 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407762 10/28/15 15:40 RBS TAL SAV TotaUNA Analysis 8081 B/8082A 1 408178 10/30/15 08:31 JCK TAL SAV Client Sample ID: Duplicate 3 Lab Sample ID: 680-118203-46 Date Collected: 10/22/15 12:37 Matrix: Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab TotaUNA Prep 3520C 407762 10/28/15 15:40 RBS TAL SAV TestAmerica Savannah Page 73 of 81 Lab Chronicle Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Client Sample ID: Duplicate 3 Lab Sample ID: 680-118203-46 Date Collected: 10/22/15 12:37 Matrix:Water Date Received: 10/23/15 09:44 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8081 B/8082A 1 408178 10/30/15 08:45 JCK TAL SAV Laboratory References: TAL SAV=TestAmerica Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL(912)354-7858 I TestAmerica Savannah Page 74 of 81 Certification Summary Client: EnviroTrac, Ltd. TestAmerica Job ID: 680-118203-1 Project/Site: Geigy Chemical Corp. Laboratory: TestAmerica Savannah All certifications held by this laboratory are listed. Not all certifications are applicable to this report. Authority Program EPA Region Certification ID Expiration Date AFCEE SAVLAB A2LA DoD ELAP 399.01 02-28-17 A2LA ISO/IEC 17025 399.01 02-28-17 Alabama State Program 4 41450 06-30-16 Arkansas DEQ State Program 6 88-0692 01-31-16 California State Program 9 2939 07-31-16 Colorado State Program 8 N/A 12-31-15 Connecticut State Program 1 PH-0161 03-31-17 Florida NELAP 4 E87052 06-30-16 GA Dept.of Agriculture State Program 4 N/A 06-12-17 Georgia State Program 4 803 06-30-16 Guam State Program 9 14-004r 04-16-16 Hawaii State Program 9 N/A 06-30-16 Illinois NELAP 5 200022 11-30-15* Indiana State Program 5 N/A 06-30-16 Iowa State Program 7 353 06-30-17 Kentucky(DW) State Program 4 90084 12-31-15 Kentucky(UST) State Program 4 18 06-30-16 Kentucky(WW) State Program 4 90084 12-31-15 Louisiana NELAP 6 30690 06-30-16 Louisiana(DW) NELAP 6 LA150014 12-31-15 Maine State Program 1 GA00006 09-24-16 Maryland State Program 3 250 12-31-15 Massachusetts State Program 1 M-GA006 06-30-16 Michigan State Program 5 9925 03-05-16 Mississippi State Program 4 N/A 06-30-15* Montana State Program 8 CERT0081 12-31-15 Nebraska State Program 7 TestAmerica-Savannah 06-30-16 New Jersey NELAP 2 GA769 10-30-16* New Mexico State Program 6 N/A 06-30-16 New York NELAP 2 10842 03-31-16 North Carolina(DW) State Program 4 13701 07-31-16 North Carolina(\ /SW) State Program 4 269 12-31-15 Oklahoma State Program 6 9984 08-31-16 Pennsylvania NELAP 3 68-00474 06-30-16 Puerto Rico State Program 2 GA00006 12-31-15 South Carolina State Program 4 98001 06-30-15* Tennessee State Program 4 TN02961 06-30-16 Texas NELAP 6 T104704185-14-7 11-30-15* USDA Federal SAV 3-04 06-11-17 Virginia NELAP 3 460161 06-14-16 Washington State Program 10 C805 06-10-16 West Virginia(DW) State Program 3 9950C 12-31-15 West Virginia DEP State Program 3 094 06-30-16 Wisconsin State Program 5 999819810 08-31-16 Wyoming State Program 8 8TMS-L 06-30-16 Certification renewal pending-certification considered valid. TestAmerica Savannah Page 75 of 81 Serial Number 99645 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD INF TestAmerica Savannah Website:www.testamericainc.com 5102 LaRoche Avenue Phone:(912)354-7858 1est1 r'ri erica Savannah,GA 31404 Fax:(912)352-0165 CD Alternate Laboratory Name/Location Phone: THE LEADER IN ENVIRONMENTAL TESTING CjAc. Fax: PROJEC REFERENCE G "�� PROJECT NO PROJECT LOCATION MATRIX PAGE OF �,AVi G$S t� e � rp, � Z'5 (STATE) NG TYPE REQUIRED ANALYSIS TAL(LA TOJED' ANAGER FAO.NUMBERP CONTRACT NO. _ STANDARD REPORT ( 4C I�y��a� �` 6® ti 3 DELIVERY 4110 CLIENT(SITE)PM i CLIENT PHONE CLIENT FAX v z LU -Tames i " A L�Z.� �I( -Lioz_ E3 J 0 t.L DATE DUE CLIENT NAME Cup. CLIENT E-MAIL ee EXPEDITED REPORT VJ, C "' i cA C ,9 .vti+�r'k ¢ o ¢� � (SDELIVERY(SURCHARGE) 4 a o gJ (SURCHARGE) CLIENT ADDRESS o ¢ o D .' g u� 13 DATE DUE E.-) COMPANY CONTRACTING THIS WO K if applicable) w G "' -3 ' ,o,y.74, . OZ4, `' i,'f•. ?;°-g"zL;1,4 •-1'�« NUMBER OF COOLERS SUBMITTED /�COM C PP ) 'y �f'��,�,ILI (n o `»'a?;���;,-p. :4a.-2'114��!':'"'t: f-.��.6+ qb c• `i.�:., PER SHIPMENT. Y'i 1A1� C 15� 1�`i� �. N.y� �m"^"'ems'p p O v,. le. 1,r„'t.uz:t'I �'6 'w< ;`o�.t �a.' �a 1 SAMPLE d 7 ° "' SAM LE IDENTIFICATION o s o lx o NUMBER OF CONTAINERS SUBMITTED REMARKS DATE ' TIME c� ¢ cn ¢ moo' 13 to 4 7 aiS(k --d -G1 'c )( ,X X /Q 7z2- -C3 1 x X s., ) T #$ 6� c `�&t X �c ntit _ I i113b -lilt-2- 2 ? _ I l?ems 5- p - I i3 s.w-4) X X. p k 3 �— )( 680-i 18203 Chain of Custody i 1NQUISHED Y:(SIGNATURE) `DATE TIME/ RELINQUISHED )BY�:�(SIGNATURE) DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME 15 EIVED BY_(SIGNATU ) DATE ! TIME RECEIVED BY.(SIGNATURE) DATE TIME RECEIVED BY:(SIGNATURE) DATE TIME LABORATORY USE ONLY RECEIVED FOR LABORATORY BY• DATE TIME CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REMARKS C 6 oq(CelT7A- :.<Th.......__-"\\ OS OQ S L(N C1 , z3i+� 1 C(//? /3-0/.1 (cr. ‘, i . 'a_�.ii_ i !!fj !a 1 ,.�L 49680(1008) — ..._ - - - .-- --- • Serial Number 9 9 6 4 6 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD ® TestAmerica Savannah Website:www.testamericainc.com 5102 LaRoche Avenue Phone:(912)354-7858 1est, ri' eri ca Savannah,GA31404 Fax:(912)352-0165 CD Alternate Laboratory Name/Location Phone. THE LEADER IN ENVIRONMENTAL TESTING Fax: PROJECT R FERENCE PROJECT NO. PROJECT LOCATION MATRIX REQUIRED ANALYSIS PAGE OF (STATE) TYPE 6 011 f-� wA 4 goo(0� 1 � TAL([AB P OJEC N ER P.O.NUMBER CONTRACT NO STANDARD REPORT /y1 �� 5 ¢y€tr W DELIVERY '� ti U I . y- CLIENT(SJ ,P, �cl �D s CLIENT FAX z 0 S' DATE DUE �L��l 1 O CLIENT NAME CLIENT E-MAIL 6 Co gb 0 EXPEDITED REPORT �` a O — Cyl DELIVERY idl Cif ^V1 0� N "'1 ;) (SURCHARGE) CLIENT ADDRESS cc — �J O r a - DATE DUE__ COMPANY CONTRACTING THIS ORK if a livable u., LLI -P 3"`)f'i i".'`:'..'.'4 �.a F',4 %;, '`',.',F'' a('' NUMBER OF COOLERS SUBMITTED _ ( P �$ ) ,9�.• c O •.� „4',.sz.:. ..?a e°( "r i:,',i. ::c c PER SHIPMENT: SAMPLE SAMPLE IDENTIFICATION o u o x o NUMBER OF CONTAINERS SUBMITTED REMARKS DATE TIME cQ -Sw < z iC Izi 1 IS-1 Z- - iteof 4 sg X , J © i, ---r C, ram-,-1 G X )4 X a tSc3 C. Q1 rut Z ~=L q S X I R lUAliSHED,13 •(SIGNATURE) DATE TIME RELINQUISHED BY• (SIGNATURE) DATE TIME RELINQUISHED BY. (SIGNATURE) DATE TIME -.), 10-2-415 1\52 7,---L--,,e-ID. ...,-?<- R IVED BY:(SIGNATU ) DATE TIME RECEIVED BY:(SIGNATURE) DATE TIME RECEIVED BY•(SIGNATURE) DATE TIME LABORATORY USE ONLY RECEIVED FOR LABORATORY BY: DATE TIMEf CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REARKS /� � (SI ) p)..........,_ / 2 /$ V ��NO SEAL /i /' /i. / o/ /i4 l ��1 3 11 %a� 7 -q/d ],� j, C(TAIS�240-680(1008) Serial Number 9 9 6 5 6 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD igfp TestAmerica Savannah Website:www.testamericainc.com 858 Test7rr'ierica Sa)2 LaRoche h,GA31Avenue Phone: )(912) -01 5 Savannah,GA 31404 Fax:(912)352-0165 CD Alternate Laboratory Name/Location MMENSIM Phone: THE LEADER IN ENVIRONMENTAL TESTING LA.6 Fax: PROJECT REFERENCE PROJECT NO. PROJECT LOCH €ON MATRIX PAGE I OF 6 CI Ca\ c c (40.1C,CZ ` (STATE) �� TYPE REQUIRED ANALYSIS TAL(LA8)pPROJCC�MjANAGER 1 P.O.NUMBER CONTRACT NO. STANDARD REPORT to C:i 1 1� t� il1 t�}S ®OE Z ti 1y DELIVERY 40 CLIENT(SITE)PM J CLIENT HONE CLIENT FAX z f C �{ DATE DUE CLIENT NAME CLIENT E-MAIL a C` 1 p 6.1 I EXPEDITED REPORT ` co 0 0lti� C - 1 V`�1 COIAN 11Z,N 0k.1V\ . `1 o o (SURCHARGE) CLIENT ADDRESS cc o ,`; a DATE DUE U ¢ z CD — w 8 s� , Si,\ /;.-g,�2 ,yA,�0 NUMBER OF COOLERS SUBMITTED COMPANY CONTRACTING THIS WO K(if applicable) LI-I§ v, o �`,��,��'';;,c�„ ��� � � t` � �, < _ E w el;wr."v.x it a &' ? < � PER SHIPMENT. SAMPLE {l SAMPLE IDENTIFICATION o 0 o g z NUMBER OF CONTAINERS SUBMITTED REMARKS DATE TIME o a cn a a o Cr cn l C550 i.--Z. Grx X t25o PZ3 C-y X CJ jZop Aw — 21L GcX ?G 169 _ >"-- r)L x N 12__- Mvw 3`1 L ), �0 ��z z X ,x RELINQUISHED BY:( NATURE) DATE TIME RELINQUISHED BY: (SIGNATURE) DATE TIME RELINQUISHED BY: {SIGNATURE) DATE TIME PIECE! BY:(SIGNATURE) DA"f'E TIME RECEIVED BY-(SIGNATURE) DATE TIME RECEIVED BY:(SIGNATURE) DATE TIME ti/ LABORATORY USE ONLY RECEIVED OR BORATORY BY DATE TIME CUSTODY INTACT CUSTODY SAVANNAH LABORATORY g MARKS (SIG u - L� : NOS O EAI r � ,� 1" au/� ��! � ✓) jo 1 o ,?.J,2-ei J e.4_ ,2/ v' TAL8240-680(1008) Serial Number 9 9 6 5 5 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD ozw TestAmerica Savannah Website:www.testamericainc.com 5102 LaRoche Avenue Phone:(912)354-7858 Test, rrieri ca Savannah,GA31404 Fax:(912)352-0165 cp Alternate Laboratory Name/Location INNOMMIMMIIMNI Phone: THE LEADER IN ENVIRONMENTAL TESTING Fax: PROJECT PIEFERENCE PROJECT NO. PROJECT LOCATION MATRIX PAGE OF C�VOA L^Rs'MOit5AlYl.tC�,Ccr 6 U(c-.SI (STATE) i�C TYPE REQUIRED ANALYSIS TAL(LAB)\PROJEC ` NAGECR�n P.O.NUMBER CONTRACT NO. STANDARD REPORT l�1Y 1X \q,c9z- RE 55 Q)ce.7. Lt., DELIVERY CLIENT(SITE)PM CLIENT PHONE CLIENT FAX o w S,1 DATE DUE 06Q.S CAS\A� N1 c�ZS)3 5(,-`'jo)2, p �� z t C, CLIENT NAME CLIENT E-MAIL �? 2 € L. s EXPEDITED REPORT ,� �q� m o DELIVERY CD (*NV-) Copt?` j w1 C S\iN `C:j'L® ©A\V CON 'N� 1 o a ict -9N (SURCHARGE) CLIENT ADDRESS J J j p ci Z ` DATE DUE co c? co w �;.-.�...� a•zQ _�, z.• w: NUMBER OF COOLERS SUBMITTED COMPANY CONTRACTING THIS RK(if applicable} w w O I 3 P. R i [� r k f?".. `' c', /' r t. ;f PER SHIPMENT. Erin �c�c Cvc i rtNri,t k'� �� ,Ce;0 0 0 0 Z 77 a :I;" ..r t �:° , .--r-. : C: �: i i awo SAMPLE SAMPLE IDENTIFICATION o 0 0 a o NUMBER OF CONTAINERS SUBMITTED REMARKS DATE TIME v ¢ u0 ¢ z TII ) 061-k D k)016rAl- \ 4:21 )( . \\(Lk Am-1-tag x x x 12�2 Ar\ -'c �x i - 1�et /VA -i 5 X ir I 15 _ ng -2Zt) C X. _ i�s21 r� -�1�-- fix, I HA i -06 6/ Y > _ 1 0 ‘6 0 NW\1 --1p .67 - K _ -1/4 teZ23 NINE --Al c X RELIN SHED BY: ( NATURE) DATE TIME RELINQUISHED BY:(SioNATu8E) DATE TIME RELINQUISHED BY:(SIGNATURE) DATE TIME LAM 142/'' RECEIVED BY:(SIGNATUR DlrE TIME RECEIVED BY:(SIGNATURE) DATE TIME RECEIVED BY.(SIGNATURE) DATE TIME ��VJJ I LABORATORY USE ONLY , 1 �j; RECEIVED FO BORATORY BY: DATE TIME CUSTODY INTACT CUSTODY SAVANNAH LABORATORY REMA) 'q r S�//2 ,)/3 �I I U"— /f`, (slaty �V{ C/ t / -.- pail � YES O SE � L9� , 45 �. f i r 1 ' 6 7 % I ✓ • TAL6240-680(100e) Serial Number 9 9 6 57 ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD TestAmerica Savannah Website:www.testamericainc.com 5102 LaRoche Avenue Phone:(912)354-7858 1est7ór'r eri ca Savannah,GA 31404 Fax:(912)352-0165 CD Alternate Laboratory Name/Location Phone. THE LEADER IN ENVIRONMENTAL TESTING ( Fax: PROJECT/R�EFERENCE� PROJECT NO. PROJECT LOCATION MATRIX REQUIRED ANALYSIS PAGE OP © >G) +`iC G'Vu A:�,C 4 C cp-a57 (STATE) TYPE TAL(LAB)PRO C`tTMANAGER PER CONTRACT NO. I STANDARD REPORT IIl'�,)GQa i Pc>£� ti r 0.9 DELIVERY At CLIENT(SITE)PM CLIENT•PHONE CLIENT FAX Q e DATE DUE sA�v e5 G s11��.� c44 JR?--44 G(z- z CLIENT NAME CLIENT E-MAIL a 2)Q-I,,. EXPEDITED REPORT 1 CO .- ( DELIVERY CD �}��s1 CT Sr✓1. 4- a_cAl ►hl ____E o o e, •I� (SURCHARGE) CLIENT ADDRESS O w $ c� DATE DUE Cfj J U Q 0 COMPANY CONTRACTING THIS WORI (if applicable) ���_ (�` �w ,. uwi =o ;�°'^. :•('- =; °" y ' °•:'d':•' 7 NUMBER OF COOLERS SUBMITTED wz4—.67i g,a,�S 1I � & 1��00�vg.`�'°" '� Cr) p LU Z � I wYr 3ti kai4cif�'�e�l.iax.1 V; PER SHIPMENT: I 0_ Lu Lu0 `� SAMPLE SAMPLE IDENTIFICATION 0 Q o Cr 0 NUMBER OF CONTAINERS SUBMITTED REMARKS ¢ z DATE TIME c� a coU cp 1 1'7;11 NW —`2-5 (-- ?C' 1 i4 �6-2 AA it- X x (2:3 l AA., .--- iL x -;c _ t303 MW —9:0tr. G.N. )C "'IL-kg Arm - 32L qK >C 1237T\-k cAsksz 3 x RE UISHED :(SIGNATURE) DATE TIME RELINQUISHED BY. (SIGNATURE) DATE TIME RELINQUISHED BY. (SIGNATURE) DATE TIME t. RECEIVgBY•(sisnAT DATE • TIME RECEIVED BY:(SIGNATURE) DATE TIME RECEIVED BY:(SIGNATURE) DATE TIME f LABORATORY USE ONLY _o �` � -� RECEIVED FOR ATORY BY. DATE TIME CUSTODY INTACT CUSTODY SAVANNAH LABOR TOY 71/),R1S-4 /:: (SIGNATURE) •' YES SE O i r( 1 0 i NO [ (/�' _( 1 TAL8240-680(1008) Login Sample Receipt Checklist Client: EnviroTrac, Ltd. Job Number:680-118203-1 Login Number: 118203 List Source:TestAmerica Savannah List Number: 1 Creator: Banda,Christy S Question Answer Comment Radioactivity wasn't checked or is</= background as measured by a N/A survey meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present,are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? N/A There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol.for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm(1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A TestAmerica Savannah Page 81 of 81