WQ0009949_2016 Opp Report_20170217

2016 ANNUAL OPERATING REPORT
RECEIVEDINCDEQIDWR
FEB 17 2017
Site: Water Quality Regional
Operations Section
GEIGY CHEMICAL CORPORATION CERCLA SITE
ABERDEEN, MOORE COUNTY, NORTH CAROLINA
COMMITTEE CORRESPONDENCE
Submitted To:
MR. JON BORNHOLM
USEPA REGION IV
61 FORSYTH STREET, SW
MAIL CODE: 9T25
ATLANTA, GA 30303.8960
Prepared By:
ENVIROTRAC LTD.
7343 WEST FRIENDLY AVENUE, SUITE J
GREENSBORO, NC 27410
[phone]
FEBRUARY 2017
A Full Service Environmental Consulting
and Contracting Firm

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enviroiFa�Z
Environmental Services
February 13, 2017
Mr. Jon Bornholm
Remedial Project Manager
USEPA Region IV
61 Forsyth Street, SW
Mail Code: 9T25
Atlanta, Georgia 30303-8960
RE: 2016 Annual Operating Report
Groundwater Remediation Permit No. W00009949
Geigy Chemical Corporation CERCLA Site
Aberdeen, North Carolina
Dear Mr. Bornholm:
RECEIVEDNCHOIDWR
FEB 1.7 2017
Water Quality Regional
Operations Section
On behalf of Olin Corporation and Syngenta Crop Protection (the Companies), the purpose of
this letter is to transmit the analytical results for the 2016 annual sampling event for the Geigy
Chemical Corporation CERCLA Site groundwater extraction, treatment, and discharge system.
Information provided in this report includes:
• Monitoring requirements summary table (Attachment 1);
• Site extraction and treatment system layout (Attachment 2);
• Monitoring event analytical summary tables (Attachment 3);
• BHC isomer trend graphs for site indicator wells and figures (Attachment 4);
• Completed copies of NCDEQ GW-59 Forms and laboratory reports with chain -of -
custody documents (Attachment 5); and
• Monthly windshield survey for new construction (Attachment 6).
The system performed as designed during 2016 and experienced minimal down -time. Over 8.3
million gallons of water was extracted and treated between December 30, 2015 and December
21, 2016, at an effective treatment efficiency of nearly 100 percent. The system is routinely
shutdown for brief periods to conduct operation and maintenance activities such as replacing
carbon drums, fittings, and bag filters. Well pumps, flow meters, and electrical relays were
replaced without shutting down the system. Five 55-gallon drums of granular activated carbon
were transported to Siemens for recycling/re-activation. Pumping of the Upper Black Creek
Aquifer extraction wells (PW-1 D, PW-2D, and PW-31D) continues to fulfill the closed -loop
requirement of the Site Groundwater Remediation Permit. Due to the inconsistency in quality
7434 West Friendly Avenue, Suite J, Greensboro, North Carolina 27410 1 Office [phone] 1 Fax [phone]
www.envirotrac.com

EvirT
Environmental Services
control and results attributed to laboratory error, a different laboratory will be utilized during the
2017 sampling events.
BHC isomer concentration trend graphs are provided in Attachment 4. The graphs include data
from the initial sampling event through the October 2016 sampling event to facilitate review of
the groundwater quality monitoring data. Alpha-BHC, beta-BHC, delta-BHC, and gamma-BHC
concentrations are provided on the graphs as these constituents typically represent the highest
concentrations and detection frequencies among the pesticides included in the sample
analyses. In reviewing the graphs, please note that monitoring wells MW-16S, MW-17S, and
MW-18S are screened in the surficial aquifer to monitor the infiltration gallery. Monitoring wells
MW-16D and MW-17D are screened in the Upper Black Creek aquifer and are located
hydraulically upgradient of the site. The graphs generally indicate steady or decreasing trends in
BHC isomer concentrations from historical levels.
Information provided in Attachment 5 of this submittal is intended to fulfill the annual reporting
requirements described in Section IV, Paragraph 4 of the Site Groundwater Remediation
Permit. Accordingly, one copy of this report has been sent to the North Carolina Department of
Environmental Quality (NCDEQ) Division of Water Resources (DWR).
Monthly windshield surveys of properties within the BHC plume have been summarized on the
Table included in Attachment 6. New construction was observed on Campbell Street between
High Street and Bethesda Avenue during the October 2016 site reconnaissance and is
documented on the form.
Should you have questions regarding the report, please contact Chris Hay at [phone].
Sincerely,
ENVIROTRAc LTD.
Gail G. Hay, P.E.
Senior Engineer
Christopher W. Hay, E.I.
Principal
Enclosure
Cc: Doug Rumford, NCDEQ Superfund Section, w/enc.
Michael Rogers, NCDEQ DWR, w/enc.
Garland Hilliard, Olin Corporation, w/enc.
George Crouse, Syngenta, w/enc.
i'
F
7434 West Friendly Avenue, Suite J, Greensboro, North Carolina 27410 1 Office [phone] 1 Fax [phone]
www.envirotrac.com

0 I LEGEND
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> NOTES:
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FIGURE 1
EXTRACTION AND TREATMENT SYSTEM SITE LAYOUT
Geigy Chemical Corporation
Aberdeen, North Carolina
DATE: 11/04/2015 APPROVED BY:
SCALE: AS SHOWN
CWH
DRAWN BY: AB PROJECT NO: 11.990010.DO

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FIGURE 3
UPPER sUUx CREEK AQUIFER MONITORING RESULTS
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ATTACHMENT I
MONITORING REQUIREMENTS
SUMMARY TABLE

TABLE 1: GROUNDWATER EXTRACTION AND TREATMENT SYSTEM MONITORING SCHEDULE
SAMPLE
PARAMETERS
FREQUENCY
TCL PESTICIDES I TCE
QUARTERLY
ANNUALLY
LOCATION
M W-4S
✓
M W-5S
`�
✓
M W-6S
✓
MW-10S
✓
✓
MW-16S
`�
✓
✓
MW-17S
✓
MW-18S
✓
✓
M W-11 D
`�
✓
MW-16D
✓
✓
MW-17D
✓
✓
MW-18D
✓
✓
M W-20 D
✓
MW-22D
I ✓
M W-23D
✓
M W-26 D
`/
✓
M W-30D
v
'�
✓
M W-22 L
`�
✓
MW-25L
v
✓
M W-27L
v
✓
M W-31 L
`�
✓
M W-32 L
v
✓
M W-36 L
✓
✓
M W-37 L
✓
✓
MW-38L
✓
✓
MW-39L
✓
M W-40 L
`/
✓
PZ-2
`�
✓
PZ-3
✓
PZ-5
`�
✓
Influent
`�
✓
✓
Effluent
`�
✓
✓
Carbon Train A
✓
`�
Carbon Train B
✓
✓
✓
11.990010.00
© 2017 EnviroTrac January 2017

TABLE 2: UPPER BLACK CREEK AQUIFER GROUNDWATER MONITORING SUMMARY
PARAMETER
ANALYTICAL DATA
PERFORMANCE
STANDARD
SAMPLE LOCATION
MW-11D
MW-18D
MW-20D
MW-22D
MW-23D
MW-26D
MW-30D
DATE COLLECTED
10/04/16
10/05/16
10/04/16
10/04/16
10/04/16
10/04/16
10/0.
Aldrin
0.058 U
0.049 U
0.049 U
0.050 U
0.049 U
0.049 U
0.049 U
0.05
alpha-BHC
beta-BHC
0.022 J
1.1
0.050
0.58
0.049 U
0.033 J
0.016 J p
0.16
0.040 J
0.044 J
0.014 J
0.049 U
0.12
4.5
0.05
0.05
delta-BHC
0.072
0.11
0.049 U
0.067
0.049 U
0.049 U
0.50
0.05
gamma-BHC (Lindane
alpha -Chlordane
gamma -Chlordane
0.019 J
0.027 J
0.019 J
0.062
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.019 J
0.050 U
0.0098 J
0.030 J
0.049 U
0.049 U
0.030 J
0.019 J p
0.014 J
0.11
0.11
0.066
0.2
NE
NE
Dieldrin
0.089 p
0.10
0.049 U
0.050 U
0.049 U
0.049 U
0.50
0.1
4,4'-DDD
4,4'-DDE
4,4'-DDT
Endosulfan 1
0.058 U
0.058 U
0.058 U
0.058 U
0.049 U
0.011 JP
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.050 U
0.050 U
0.050 U
0.050 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
NE
NE
NE
NE
Endosulfan II
0.058 U
0.049 U
0.049 U
0.050 U
0.049 U
0.049 U
0.049 U
NE
Endosulfan sulfate
0.017 J
0.049 U
0.049 U
0.050 U
0.049 U
0.049 U
0.049 U
NE
Endrin
0.058 U
0.049 U
0.049 U
0.050 U
0.049 U
0.049 U
0.049 U
NE
Endrin aldehyde
0.058 U
0.049 U
0.049 U
0.050 U
0.049 U
0.049 U
0.049 U
NE
Endrin ketone
0.091
0.076
0.049 U
0.050 U
0.049 U
0.049 U
0.39
0.1
Heptachlor
0.058 U
0.049 U
0.049 U
0.050 U
0.049 U
0.049 U
0.049 U
NE
Heptachlor epoxide
0.030 J
0.013 Jp
0.049 U
0.050 U
0.049 U
0.015 J
0.092
NE
Methoxychlor
0.058 U
0.049 U
0.049 U
0.050 U
0.049 U
0.049 U
0.049 U
NE
Toxaphene
2.1 J
3.2 J
4.9 U
5.0 U
4.9 U
4.9 U
8.1
1
Trichloroethene
1.0 U
1.1
NA
NA
NA
NA
1.3
NOTES
Results are presented in micrograms per liter NE = No standard established
J = Estimated value less than the reporting limit but greater than the method detection limit NA = Not analyzed for this compound
= LCS and LCSD exceeds the control limits NS = Not sampled
* = Trichloroethene is not a COC for the Geigy site. U = Indicates the analyte was not detected
p = The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
Bold = Concentration exceeds performance standard or method detection limits if no standard is established
11.990010.00
© 2017 EnviroTrac January 2017

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O o
0 0
0 Q
0 0
0 0
0 0
0 o
0 0
0 0 0
O
a
^
m O
LL 00
0 0
0 C
O O
0 0
C O
C O
O o
0 CO
p
E
w
- -
❑Zma
Z
o o
Z
W
J C
o 0
0 0
0 0
0 0
0 0
0 0
N
166
o
O o
o O
a a
o O
o O
o 0
0 0
o O
o
m
Z
LL, a
d
m n
d W
m m
d d
a m
d d
N m
M Q
m m
d d
m m
d d
m m
d
d
N
m m m
d d Q
a
a
m
ti
J
LL 0
w o
w
0 0
0 0
0 0�
0 0
0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0 0
0 0 0
m
_
-
m
O
Z 7-�
W m
N n
N N
Q M
m m
d d
h m
M V
m m
V d
m m
d d
m m
d Q
m M
d N
m 1[! m
d Y1 Q
e'f
r
O
d
d
zoo
O
O O
O
C 0
0 0
0 0
0
.-0
Ljmmmrnma,rnrn�m�{{rnmrnsrns}�ma�rnma,rnamamo
O
O
0 0
0 0
0 0
O O
O O
O
O
b o o
d
^
m y
n
LL
ly O
W
O O
O O
0,
O O
0 0
0 0
O O
O
O O O
.
O
mE�
C
O
Z
(r
v
W mm
m
N
� ti
m m
mm
m m
m m
mm
O
m
C
N m m
m t'i
n
j
(
O
Z o
O
e
� O
0
0
0 0
0' O
0
O O
0 0
O O
C. 0
0 0
d
O �
o e
0
O
a
a �
-
p
N
Z p
p❑
Z) p❑
7
7
7 7
p p
p
7 7 7❑
7
= CY
"'mmmwrnmowmmmrnmmornm
d
d d
d Q
d d
Q a
d Q
g
0
d d
o?o
�o `f
j li
LL p
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0 0
O
O
O G
O 0
0 0
0 0
0 0
0 C
b 0
0
0 0 0
0
w
u
LL
o,
000
oo
o o oo1P'o
LL 0
Z
p
oo0
O O
O O
O O
om
0 0
0 0
0 0
0
non
z
S
z
w
p
c
Z
U
c
a
H
v
o
c
UU
c
c
c
g
c m
a�
a
m 2
m
U
s c O
y
c
L
`_°may
o
g o
.Lj4
a
c :om�
EL
Ebo❑o
E
0
0 0cc
me
n
=_
C ❑
a
V)
N;zA-M
-6
E n
v
aoddQwwwwwwi
v v
a �
c c�
c
c v'
m
o .53
a
m
0

TABLE 5: ON SITE GROI
INDWATER MUNI
IURINUi Uffl l
-
MW-6s
10/05/16
MW-10S
10/05/16
0.055 U
0.055 U
0.31
0.055 U
0.055 U
0.055 U
0.055 U
0.037 J
D.055 U
0.055 U
0.021 J p
0.055 U
0.055 U
0.055 U
0.055 U
0.055 U
0.061
0.055 U
0.055 U
0.055 U
0.52Jp
1.0U
MW-116
10/04/16
0.058 U
0.022 J
1.1
0.072
0.019 J
0.027 J
0.019 J
0.089 P
O.D58 U
0.058 U
0.055 U
0.058 U
0.058 U
0.017 J
- -18 U
0.058 U
0.091
0.058 U
0.030 J
0.058 U
2.1J
loll
MW-16S
10/04116
0.053 U
0.D53 U
0.053 U
0.053 U
MHEN01,11,
0.053 U
0.053 U
0.053 U
0.053 U
0053 U
0.053 U
0.053 U
0.053 U
5.3U
1.OU
MW-16D
10/04/16
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NAWO4
NA
NA
NANA
NA
NANA
NA
NA
59
MW-17S
10104M 6
0.049 U
0.049 U
0.020 J
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
0.049 U
Q.049 U
0.049 U
O.tM9 U
0.049 U
4.9U
1.OU
MW-17D
10/D4/16
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
160
MW-18S
10/04/18
0.055 U
0.055 U
0.063
0.055 U
0.055 U
0.055 U
0.055 U
0.031 J
0.055 U
0.D55 U
0.055 U0.049
0.055 U
0.055 U
0.055 U
0.055 U
0.055 U
0021 J
0.055 U
0.055 U
0.055 U
0.24Jp
1.OU
MW-18D
10/05116 1
0.049 U
0.050
0.58
0.11
0.062
0.049 U
0,049 U
D.10
D.049 U
0.011 J
U
0.049 U
0.049 U
0.049 U
0.049 U
MW-3DD
1 D/04116
0.049 U
0.12
4.5
0.50
0.11
0.11
0.066
0.60
0.049 UNE
0.049 U
PERFORMANCE
STANDARD
005
0.05
0.05
005
0.2
NE
NEO.p50
ANALYTICAL DATA
MW-4S
MW-5s
10/05/18
1 D/05116
0.050 U
0.096
O.D11 J
HE
0.14
48
0.40
0.077
0.050 U
U
6.2
U
0.050 U
0.050 U
O.D50 U
D.O50 U
0 05D U
1.6
0.050 U
6.4
D.050 U
0.52
005D U
24
24p
O.D26 J
2.5
p23
0.058
0.22
0.15
0.87
D.058 U
0.058 U
0.058 U
0.058 U
0.058 U
O.OSA U
0.058 U
0 058U
0,29
0.058 U
0.059 U
0.058 U
17
J
2.8
D.24
D_051 U
O.D51 U
0.051U
0.22
0.051 U
0.051 U
0051 U
0.051 U
0.051 U
0.051 U
O.D51 U
0.051 U
0.18
O.tM1 U
p.032 J p
0.051U
4.2J
NA
0.1
N0.050
NE
0.049 U
NF
0 049 U
NE
O.D49 U
NE
0.049 U
NE
0,049 U
NE
0.049 U
0.049 U
NE
0.078
0.049 U
0.39
0.049 U
0.1
NE
0.p13 J
0.092
NE
0.049 U
3.2J
1.1
0.049 U
1.3
NF
NA
Results are presented in micrograms per liter
J = Estimated vahra less than the reporting limit but greater than the method detection limit
'• = Trichloroethene is not a CDC for the Geigy site.
p = The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.
Bold = Concentration exceeds performance standard or method detection limits if no standard is established
NE = No standard established
NA = Not analyzed for this compound
U = Indicates the analyte was not detected
11.990010.00 January 2017
© 2017 EnviroTrac

TABLE 6! GROUNDWAT EK I:X1
Kwc uvN AMU I MEM I r 1- ­
� �,., .....•..•.^•-•
ATION
fAl.E
1S
-2S -
PW 35 -- -
PW-3D -- -
12/30/15 01/27/16
5208,763 5,224,913
61,603,778 62,151,975
1,433,548 1448,740
17.784,743 17,851,900
1,761,752 1,789,383
15,098,339 15,190,393
21,539,792 21,663883
124,B08,715 125,321,107
02/18118
5,238,925
03130116
5248,937
62,799,3DO
1,489,090
18,036,403
1,888,177
16,379,319
21,892,699
126,712,925
04/28/16 05/17/16 06/24/16
5,260,949 5,315,%5 5,389,508_
63,127.268 83,310,481 63,5B2,674
1,508,759 1,521,071 1,534,733
18,135,426 18,198,085 18,292,463
1,898,88o 1.932,954 � 1,987,214 3
15.491,650 15,553,572 15.645.840
22,014,538 22,089,076 22.201,959
127,437,18D 127,920,794 128.614.389
07/12116
6,444.649
0B103f18 09/13MBr135
5,497,625 5,590,483
tt117l18 12! 1!
5,601,640 5,888,097
64,994,811 85284,971 °
379
1,639,636 8.90 ,723-2D
78,830,50T 18,904,723
2,097,147 2,129,584
16,155,994 18,219,565
22.84 ,,876 22,920173
134383,811 133,008.472
140,790,259 141,398,9
8,426,448 6,390,460_
6.0% 5.9%
82,426174
1,461,833
17,924.972
1 815,958
15.267,088
21.782.731
125,895,681
63,7T0,362
1,549,081
18.358,082
1,977,096
15,710.541
22275,963
129,095,754
137138,955
8,053,101
84,024,704
1,�2.714
18,443,471
1,990,180
15,796.869
22.384675
129,700,238
137,781,637
8,081,399
- -
5.9%
64,498,994
1,592,9T7
18,599,433
2,015,664
15,942,912
22580.281
130.820,738
138,958,886
8,136,158
5.9%
16,2,
22678.719
131,397.221
139,557,837
8,160,616 -
5.8%
PW-4S
Extraction Weis
-
Treahnent Building
132,466,791
7,856,078
5.9%
--52
-
133,213,702
7,892,515
---
5,9%
133,798,492
7,902,811
5.9%
134,778,887
8,065,962
--
6.0%
135,492,555
8,055,375
- --
5.9°/
135,961,742
B,D40,948
5.9%
136,646.738
8,032,349 -
5.9%
Difference
%Difference
-
5.9%
LOCATION
11104/15
12l30I15
56
6,735
12/30l15
01127/16
28
6,763
Dil27/16
02/18/15
22
6,786
02/18/16
03/30/16
41
6,826
03/30116
04128116
29
6,855
04/28l18
(15117116
19
j 6,874
05/17/16
D8l24l16
38
1 6,912
OB@4116
07l12118
16
6,930
07/1?116
D8/03/16
22
6,952
06/03/16
09/13I16
41
6,993
09l13/16
10/04/i6
21
7,014
10104l16
11/17/16
44
7,058
11117(16
12121/16
34
7,D92
TIME PERIOD
DAYS IN PERIOD
TOTAL DAYS OF OPERATION
Average Daily Volume allons)
546
12,464
595
3,321
1,208
3,488
293
9,101
886
2,693
1,274
414
11,309
878
3,449
1,052
2,874
9,843
548
3,298
1,803
1,948
7163
360
2,484
902
3,064
10,427
797
3,644
549
2,408
11,501
620
3,882
595
2,285
11,588
738
3,804
822
2,154
11,078
878
3,076
809
3,707 _
4,688
27,452
3,776
6,741
741
3402
1,581
3,073
2.537
6,540
634
2,183
963
1.870
2,244
1 18,961
PWAS
470
10586
423
2,125
829
64B
12,438
543
3,113
987
PWAD
PW-2S
PW-2D
PEA/-3S
3,562
Pt/µ 3D
PW 4S
Extraction Wells
2,986
3,268
2,737
3,870
3,264
2,428
3.595
3.924
4.941
27,931
_
4,771
27,329
3,754
21,968
4493
26 113
3,170
19,933
4,201
24,974
3901
25.483
2971
18,253
4,111
26,187
3,401
20,81e
4432
25,445
Average Flow Rate (gall r minute
PW-1S 0.33
PW-1D 7.35
Pin/-2S 0.29
PW-2D 1.48
PW-3S 0.44
PW-3D 2.07
PW-4S 238
Extraction Wefts 14.32
SYSTEM TO DATE 13.66
0.20
5.32
OA6
1.87
0.88
1.90
2,20
13.84
13.71
--
-
---
-
1.67
8.03
0.51
2.64
DA3
2.47
3.31
18.98
13.80
150
8.15
0.47
289
OA2
2.57
3.26
119.06
13.82
- -
282
3.93
0.51
1.08
1.08
2.13
2.81
15.26
13.85
-
1.76
5.93
0.44
52
1.86
O.BB
1.30
1.56
13.17
13.85
0.45
8.64
0.38
2.16
089
2.28
3.08
17.67
13.68
OSB
@AS
CAI
2.31
0.84
2.42
3.12
18.13
13.69
0.29
7AS
OA7
2AD
0.73
2.80
2.92
17.34
73,79
2.00
6.70
0.45
229
1.25
2.27
2.72
17.68 7
13 (4
1.39
4.97
0.25
1.72
0.63
1.69
2.06
12.68
13.73
2.13
7,24
0.55
2.38
0.38
2.60
2.86
18.19
13.74
1.67
8A3
0 43
2J0
0A1
2.73
3.43
19.40
13.76
NOTES
Estimated gallons, based on average Row during the last three years. Flow meter replaced 4128/16.
Y Groundwater pump in PW-3S failed and was replaced 5119116.
3 Estimated gallons, based on average Row during the last three years. Flow meter replaced 711811B.
" Estimated gallons, based on average flow during the last three years. Flow meter replaced 12/21116.
11.990010.00
© 2017 EnviroTrac
January 2017

ATTACHMENT 4
BHC ISOMER TREND GRAPHS AND FIGURES
LAM

MW-11 D
--+--alpha-BHC —'-!--beta-BHC -.delta-BHC ---gamma-BHC (Lindane)
18
16
14
12
6
4
2
mx+ 0
JAN-90 JAN-92 JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

MW-18D
--m—alpha-BHC .beta-BHC —delta-BHC gamma-BHC (Lindane)
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12
TIME
10
8
6 n
O
z
0
m
z
D
O
z
4
2
0
JAN-14 JAN-16

MW-20D
t-alpha-BHC —t—beta-BHC —«—delta-BHC --+.—gamma-BHC (lindane)
10
8
6 np
z
0
m
9
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN
TIME

MW-22D
---alpha-BHC 11 •«beta-BHC delta-BHC - 4--°gamma-BHC(Lindane)
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06
TIME
JAN-08 JAN-10 JAN-12
10
S
6 O
O
z
O
m
z
D
O
z
t
4
2
0
JAN-14 JAN-16

L
MW-23D
-, --alpha-BHC - beta-BHC delta-BHC --+ gamma-BHC (Lindane)
10
6 n
O
z
O
m
z
0
z
t
4
2
0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME
- — r

JAN-94
MW-26D
-3—alpha-BHC beta-BHCdetta-BHC -+r--gamma-BHC (Lindane)
10
a
2
0
JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

JAN-94 JAN-96 JAN-98
MW-3OD
—m—alpha-BHC tbeta-BHC —µ—delta-BHC —o+—gamma-BHC (Lindane)
10
8
2
IPF 0
JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

MW-22L
-•-alpha-BHC beta-BHC —►--delta-BHC - gamma-BHC (Lindane)
12
10
1
8
n
O
z
C
m
z
6 D
O
z
4
2
0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

JAN-94
MW-25L
•alpha-BHC beta-BHC - delta-BHC gamma-BHC (Lindane)
JAN-96 JAN-98 JAN-00 JAM-02 JAN-04 JAN-06
TIME
12
10
8
4
2
0
JAN-08 JAN-10 JAN-12 JAN-14 JAN-16

MW-27L
— alpha-BHC —*—beta-BHC --N-delta-BHC -- gamma-BHC (Lindane)
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02
JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14
TIME
12
10
8
n
O
z
0
m
z
4
6 D
O
z
L
r
4
2
0
JAN-16

MW-31 L
alpha-BHC beta-BHC --- delta-BIiC gamma-BHC (Undane)
12
10
8
0
O
z
C)
m
z
6
O
z
L
4
3
0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

MW-32L
"a •alpha-BHC beta-BHC --o --delta-BHC gamma-BHC (Lindane)
12
10
0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

i
MW-36L
7--•alpha-BHC -beta-BHC —delta-BHC •—io--gamma-BHC(Lindane)
12
6
4
2
0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

MW-37L
talpha-BHC -beta-BHC —+•--delta-BHC - gamma-BHC (Lindane)
12
10
B
4
OA
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

MW-38L
—m—alpha-BHC beta-BHC — delta-BHC --gamma-BHC (Lindane)
12
10
8
4
2
i
0 a
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

JAN-94 JAN-96
MW-39L
--alpha-BHC beta-BHC -delta-BHC gamma-BHC (Lindane)
1
I
I
JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME
10
8
4
2

MW-40L
—t—alpha-BHC —+—beta-BHC --m.—delta-BHC—gamml-BWC Nnditfs)
0
0
z
0
m
z
6
0
z
z
m
4
2
lAr--K —,U a 0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

h
PZ-2
• alpha-BHC beta-BHC — delta-BHC - -gamma-BHC (Lindane)
12
10
8
n
O
z
0
m
z
s n
0
z
L
r
4
3
- 3- _ _ - ---lw— — — _ _ — _ 0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME

PZ-3
—t—alpha-BHC —r--beta-BHC ---+*—delta-BHC —m-gamma-BHC (Lindane)
12
10
8
C>
O
z
n
m
6
O
z
t
m
4
2
06
0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14
TIME

PZ-5
--alpha-BHC -beta-BHC —+«—delta-BHC gamma-BHC (Lindane)
12
10
8
4
2
0
JAN-94 JAN-96 JAN-98 JAN-00 JAN-02 JAN-04 JAN-06 JAN-08 JAN-10 JAN-12 JAN-14 JAN-16
TIME
w

ATTACHMENT 2
SITE EXTRACTION AND TREATMENT
SYSTEM LAYOUT

Figure 2
Treatment System Process Layout
Geigy Chemical Corporation Site
Transfer
Pump P-6
Influent0. Equalization
Tank
Transfer
Pump P-7
Carbon Carbon Carbon
Unit 3A Unit 2A Unit 1A
Sample Sample Sample
Effluent
Port V-49 Port V-48 Port V-47
Sample
Port V-54
Carbon Carbon Carbon
Unit 3B Unit 2B Unit 1 B
Sample Sample Sample
Port V-52 Port V-51 Port V-50

.ne,..�wawe�,vaa:m»w_�_�ax:�rv+v �. •r,ra� cMxo.rcr`.��.k�'n•.��aas.t.av .h-•�k:�
. r
ATTACHMENT 5
GW-59 FORMS
AND
LABORATORY REPORTS AND CHAIN -OF -CUSTODY

— r nur PAPER ONLY
�uorvu � rvnm vr. LLI • •• �,
0001101WEPARTMENT
GROUNDWATER QUALITY MONITORING:
��16117 OMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Ctearty or Type
Facility Name: Geigy Chemical Corporation Site
Permit Name (if different).
Facility Address: Domino Drive
Aberdeen NC County Moore
Contact Person: Garland Hilliard Telephone#: [phone]
Well Location/Site Name: No. of wells to be sampled:
from Permit)
OF ENVIRONMENT & NATURAL RESOURCES
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number: Expiration Date: 05/31 /18
Non -Discharge W00009949 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field 5d Remediation: Groundwater
❑ Rotary Distributor ❑ Land Application of Sludge
ElWater Source Heat Pump ElOther:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): Influent
Date sample collected: 1/27/16
FIELD ANALYSES:
°C
WAS
DRY at
Well Depth: ft.
Well Diameter: in.
pH units Temp .
ItMhos
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft,
Spec. Cond.
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
here:
Plume of water pumped/bailed before sampling:
gallons
Appearance
❑
Samples for metals were collected unfiltered: OYES
❑ NO and field acidified: ❑ YES ❑ NO
IABORATORYINFORMATION
Date sample analyzed: 2/1116 TICE, 2/2116 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/1
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform. MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(NoteUse MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/1
Al - Aluminum
mg/I
TICE 0.93J alpha-BHC 0.055, beta-BHC 2.8,
pH (when analyzed) units
Ba - Barium
mg/I
delta-BHC 0.44 gamma-BHC 0.037Jp,
TOC mg/I
Ca - Calcium
mg/I
Dieldrin 0.32 Endrin ketone 0.28, Toxaphene
Chloride mg/1
Cd - Cadmium
mg/l
5.7 (all ug/L)
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls _ method # 8081 B/8082A
(Ammcma Nitrogen, NH3ss N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
�n nn•t ._rur inn
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00093J mg/L Effluent Total VUCa: mgrc vv%, nennrvar.a -
Garland Hilliard - Director, Environmental Remediation
Perri (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007
Signature of Permittee (or Authorized Agent) ;Date)

2016 MONTHLY WINDSHIELD SURVEY

SUBMIT FORM ON YELLOW PAPER ONLY
IME.IMEPARTMENTOF
ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
SION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION PleasePnotClearly orType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different)
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon CI Remediation: Infiltration Gallery
Aberdeen """' NC County Moore
F Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:_
No. of wells to be sampled:
morn Permit
❑ Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Influent
Date sample collected: 1/27/16
FIELD ANALYSES:
WAS
Well Depth ft.
Well Diameter in.
pH units Temp. `C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. } rMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: r- l
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
u
LABORATORY INFORMATION
Date sample analyzed: 2/1/16 TCE, 2/2/16 PEST
Laboratory Name: Test America
Certification No,
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use VPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units)
Dissolved Solids: Total mg/I
AI - Aluminum
mg/l
TICE 0.93J, alpha-BHC 0.055, beta-BHC 2.8,
pH (when analyzed) units
Ba - Barium
mg/I
delta-BHC 0.44, gamma-BHC 0.037Jp,
TOC mg/I
Ca - Calcium
mg/I
Dieldrin 0.32, Endrin ketone 0.28, Toxaphene
Chloride ni
Cd - Cadmium
mg/I
5.7 (all ug/L)
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu- Capper
mg/I
ORGANICS: (by GC, GC/MS. HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/1
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia ni
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B/8082A
(Ammonia Nitrogen: NH3as N: Ammonia Nitrogen. Total)
Mn -Manganese
mg/I
.method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00093J mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
GW-59 Rev.112007

1
1
Reconnaissance for New Construction within Area of Plume
Project: Geigy Superfund Site Date: January to December 2016
Location: Aberdeen, NC Data Collected by: CWH
Project No.: 11.990010.00
Date
Address
Property Description
01/27/16
No observed change
02/18/16
No observed change
03/30/16
No observed change
04/28/16
No observed change
05/17/16
No observed change
06/14/16
No observed change
06/24/16
No observed change
07/12/16
No observed change
08/03/16
No observed change
09/13/16
No observed change
10/04/16
Campbell
New homes on Campbell between High and Bethesda
11/17/16
No observed change
12/21/16
No observed change

CI IRRAIT Pn PhA nM VFI 1 r11A1 PAPFR r1Nl V
EPART TENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearfy or Type
PERMIT Number: Expiration Date. 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge 1N00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen NC County Moore
s` e'
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled:
irnm Pe-mii
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Influent
Date sample collected: 2/19/16
FIELD ANALYSES:
WAS
Well Depth: ft_
Well Diameter: in.
pH units Temp. °C
DRY at
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. }Mhos
time of sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: f'.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑YES (� NO
LABORATORY INFORMATION
Date sample analyzed: 3/1116 TCE, 2/26116 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/l
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/1
Zn -Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P ___mg/l
(Note Use MPN method for highly tumid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al -Aluminum
mg/I
TCE 0.77J. alpha-BHC 0.053, beta-BHC 2.6,
pH (when analyzed) units
Ba - Barium
mg/I
delta-BHC 0.37, gamma-BHC 0.037Jp,
TOC mg/I
Ca - Calcium
mg/I
Dieldrin 0.33, Endrin ketone 0.35, Heptachlor
Chloride mg/I
Cd - Cadmium
mg/l
epoxide 0.086, Toxaphene 6.3 (all ug/L)
Arsenic mg/1
Chromium: Total
mg/1
Grease and Oils mg/I
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
mg/I
Report Attached? [td Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mgll
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B/8082A
(Ammonia Nitrogen: NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00077J mg/L , Effluent Total VOCs: <0.001 mg/L VOC Removal°/, 100
GW-59 Rev.1/2007

SURMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
EM16117
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Pnnt
Clearly orType
PERMIT Number: Expiration Date. 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen '"`°" NC County Moore
is" '
❑ Spray Field 5d Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
hom Permlr
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Influent
Date sample collected: 4/28/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in,
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. (Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 5/9/16 TCE, 5/3/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg,rl
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO,) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus. Total as P
mg/I
(Note Use MPNmethod for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg,rl
AI - Aluminum
mg/I
alpha-BHC 0.042J, beta-BHC 2.3, delta-BHC
pH (when analyzed) units
Ba - Barium
mg/I
0.45, gamma-BHC 0.032Jp, Dieldrin 0.33B,
TOC mg/I
Ca - Calcium
mg/I
Endrin ketone 0.23, Heptachlor epoxide
Chloride mg/I
Cd - Cadmium
mg/I
0.055pB, Toxaphene 7.3 (all ug/L)
Arsenic mg/1
Chromium: Total
mg/I
Grease and Oils mg/1
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS. HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT,)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? Ik Yes (1) n No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B/8082A
(Ammonia Nitrogen: NH,as N: Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: <0.001 mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007

CI IR6AIT PnPU ON VFI I OW PAPFR ONI Y
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
�1617
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address. Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
''
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Influent
Date sample collected: 5/17/16
FIELD ANALYSES:
WAS
ell Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. i tMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: —]YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 5/25/16 TCE, 5/24116 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/l
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO,) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mgil
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TICE 0.73J ug/L
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe - Iron __mgll
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
mg/I
Report Attached? ❑X Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B/8082A
(Ammonia Nitrogen, NH3 as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/1
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00073J mg/L Effluent Total VOCs: <U.UU1 mg/L VOC Removal% 1UU
GW-59 Rev. 1/2007

e
cI IRMIT FORM ON YFI I OW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
�'
I'IS!ON OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ RemediationInfiltration Gallery
Aberdeen NC County Moore
I1 Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor n Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): Influent
Date sample collected: 6/24/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. C
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. µMhos
time P g,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed 6/29/16 TCE, 7/8/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units)
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I
Aldrin 0.0479 alpha-BHC 0.0385, beta-BHC
pH (when analyzed) units
Ba - Barium
mg/1
1.94 delta-BHC 0.301 gamma-BHC 0.0498,
TOC mg/I
Ca - Calcium
mg/I
4,4'-DDE 0.0885, Dieldrin 0.284, Endosulfan II
Chloride mg/I
Cd - Cadmium
mg/I
0.178 Endrin ketone 0.186 (all ug/L)
Arsenic mg/I
Chromium. Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? Fk Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B/8082A
(Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For RemediationSystemsOnly (Attach Lab Reports): Influent Total VOCs: <0.001 mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
GW-59 Rev.112007

SUBMIT FORM ON YEI I OW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
E116117
ON OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field Remediation: Groundwater
Contact Person. Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor Ll Land Application of Sludge
Well Location/Site Name:
No, of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
Ram Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Influent
Date sample collected: 7112/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
Depth to Water Level: ft, below measuring point
Screened Interval ft. to
_ft.
Spec. Cond. iiMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: F_IYES
[__) NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed 7/15116 TCE, 7/20116 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (Ni as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/l
(Note Use MPNmethod for highly turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I
TICE 0.66J, beta-BHC 2.1, delta-BHC 0.37,
pH (when analyzed) units
Ba - Barium
mg/I
4,4'-DDE 0.069J, Dieldrin 0.24p, Endrin ketone
TOC mg/I
Ca - Calcium
mg/I
0.16 (all ug/L)
Chloride mg/l
Cd - Cadmium
mg/l
Arsenic mg/l
Chromium Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? M Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B18082A
(Ammonia Nitrogen: NH3as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/1
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00066J mg/L Effluent Total VOCs: <0.00020 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007
or Authorized Aqent)
3,

SIIRMIT FORM ONYFLLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
�Glllr COMPLIANCE REPORT FORM MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site Non -Discharge WQ0009949 UIC
Permit Name (if different): NPDES Other
Facility Address: Domino Drive TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC County Moore ❑ Lagoon 1.1 Remediation Infiltration Gallery
❑ Spray Field ® Remediation: Groundwater
Contact Person. Garland Hilliard Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other:
from Permit)
- --- — - If WELL
=LL ID NUMBER (from Permit): Influent
;II Depth: ft.
pth to Water Level: ft. below measuring point
tasuring Point is ft. above land surface
lume of water pumped/bailed before sampling:
moles for metals were collected unfiltered: EYES
_ Date sample collected: 10/4/16
Well Diameter: in.
Screened Interval: ft.
Relative M.P. Elevation:
_gallons
❑ NO and field acidified: ❑ YES
FIELD ANALYSES:
pH units
to ft. Spec. Cond.
ft. Odor
Appearance
❑ NO
Temp. °C DRY at
µMhos time of
sampling,
:e sample analyzed: 10/13/16 TCE 10/12/16 PEST
Laboratory Name: Test America
Certification No.
RAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (Nos) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units)
Dissolved Solids: Total
mgil
Al -Aluminum
mg/I
TCE 0.53J Aldrin 0.018Jp, alpha-BHC 0.072.
pH (when analyzed)
units
Ba - Barium
mg/l
beta-BHC 3.2 delta-BHC 0.46, gamma-BHC
TOC
mg/I
Ca - Calcium
mg/l
0.083 alpha -Chlordane 0.094, Dieldrin 0.36,
Chloride
mg/I
Cd - Cadmium
mg/1
Endrin ketone 0.22, Heptachlor epoxide
Arsenic
mgil
Chromium: Total
mg/I
0.054p. Toxaphene 6.7 (all ug/L)
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC , method # 8260
Total Ammonia
mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B/8082A
(Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/l
. method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00053J mg/L Effluent Total VOCs: <U.UU1 mg/L VOC Removal% I Uu
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
MMM2Dr=PARTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
iml17
]VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please PrrntClearly orType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation. Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field M Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Effluent
Date sample collected: 1/27/16
FIELD ANALYSES:
WAS
ell Depth: ft.
Well Diameter: in.
pH units Temp. "C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. µ Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: 1
Samples for metals were collected unfiltered: ❑ YES
L_] NO and field acidified: ❑ YES ❑ NO
u
LABORATORY INFORMATION
Date sample analyzed: 2/1/16 TICE, 212/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /loom[
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /loom[
Phosphorus: Total as P
mg/I
(Note Use AAPV method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/l
Al - Aluminum
mg/l
beta-BHC 0.059 ug/L
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/l
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mgil
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mgil
Report Attached? bd Yes (i) L .i No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH3as N. Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/l
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00093J mg/L Effl�ent Total VOCs: <0.001 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007
iqnature
-- - .. :t..a.« , . - .

SUBMIT FORA ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
•
VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
Ll Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: 423.336,4479
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
Ll Water Source Heat Pump Ll Other:
rom Per t)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Effluent
Date sample collected: 2/19/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. uMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: DYES
NO and field acidified: El YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/1/16 TICE, 2/26/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /loom[
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/1
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Nore Use MPN method to, highly turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/l
TCE. PEST - all BOL
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/1
Ca - Calcium
mg/l
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS. HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH3as N; Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/1
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00077J mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
GW-59 Rev.1/2007

SI IRMIT FORM ON YELLOW PAPER ONLY
fflIMEPARTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
11617
=
[VISION OFWATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date. 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge VV00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field W Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
Yrom Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Effluent
Date sample collected: 4/28/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. ()Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
INFORMATION
LABORATORY
Date sample analyzed: 5/9/16 TCE, 5/3/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: ME Fecal it 00ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/1
Coliform: ME Total /100ml
Phosphorus: Total as P
mgil
(Note Use MPN method for h',ghiy turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I
beta-BHC 0.057, Dieldrin 0.032JB, Endrin ketone
pH (when analyzed) units
Ba - Barium
mg/I
0.024J (all ug/L)
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/1
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH3 as N; Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: <0.001 mg/L Effluent Total VOCs _<0.001 mg/L VOC Removal°% 100
GW-59 Rev. 1/2007

SIIRMIT FORM ON YELLOW_ PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or type
PERMIT Number: Expiration Date. 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field M Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Effluent
Date sample collected: 5/17/16
FIELD ANALYSES:
WAS
Well Depth. ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. F rMhas
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered n YES
NO and field acidified �� YES (__] NO
LABORATORY INFORMATION
Date sample analyzed: 5/25/16 TICE. 5/24116 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /10oml
Nitrate (NO3) as N
mi
Zn - Zinc mg/I
Coliform: MF Total /loom[
Phosphorus: Total as P
mg/I
(Note use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
beta-BHC 0.12 delta-BHC 0.017J, gamma -
pH (when analyzed) units
Ba - Barium
mg/l
Chlordane 0.0059 Jp, Dieldrin 0.076, Endrin
TOC mg/I
Ca - Calcium
mg/I
ketone 0.043J, Toxaphene 1.1 J (all ug/L)
Chloride mg/l
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? k Yes (1) ❑ No (0)
Specific Conductance [.Mhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH,as N. Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00073J mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007
re of

SUBMIT FORM ON YELLOW PAPER ONLY
ARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• ,
SION OF WATER QUALITY -INFORMATION PROCESSING UNIT
76w,
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: (919) 73JJ221
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
U Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
LJ Rotary Distributor LJ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
/rnm Permit
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Effluent
Date sample collected: 6/24/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft, below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. µMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: r
Samples for metals were collected unfiltered OYES
Ll NO and field acidified: ❑ YES n NO
u
LABORATORY INFORMATION
Date sample analyzed: 6/29/16 TCE, 7/11/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/1
Coliform: MF Total /100ml
Phosphorus: Total as P
mall
(Note Use MPNmethod for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I
beta-BHC 0.0849, Dieldrin 0.0303p, Endrin
pH (when analyzed) units
Ba - Barium
mg/I
ketone 0.0226
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/l
Report Attached? bd Yes (1) L No (0)
Specific Conductance uMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH,as N: Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only(Attach Lab Reports): Influent Total VOCs: <0.001 mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Narne and Title - Please print or type
GW-59 Rev. 112007
of

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
E1516117
IvISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: (919) 733J221
FACILITY INFORMATION Please Pnnt CleaHy or type
PERMIT Number: Expiration Date: 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
"�'
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from P-0
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Effluent
Date sample collected: 7/12/16
FIELD ANALYSES:
WAS
ell Depth. ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. } Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: YES El NO
LABORATORY INFORMATION
Date sample analyzed: 7/15/16 TCE, 7/20116 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NOS) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mgll
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Notes Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/l
TCE. PEST - all BQL
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mg/I
Cu - Copper
mgll
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mgll
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen: NH,as N; Ammonia Nitrogen Total)
Mn - Manganese
mg/l
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00066J mg/L EffWent Total VOCs: 1. <0.00020 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Atdhorized Agent) Name and Title - Please print or type
GVNJ-59 Rev. 1/2001
(or Kuthorized Agent)

St1RMIT FORM ON YELLOW_ PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
RM11617
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC. 27699A617 Phone: [phone]
FACILITY INFORMATION Pease Print Cleady or Type
PERMIT Number: Expiration Date 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different).
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
from Permit
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Effluent
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. eC
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. I iMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/baled before sampling:
gallons
Appearance
here:
Samples for metals were collected unfiltered: DYES
n NO and field acidified: ❑YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/13/16 TCE, 10/12/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
beta-BHC 0.20 delta-BHC 0.017Jp, alpha -
pH (when analyzed) units
Ba - Barium
mg/I
Chlordane 0.014J, gamma -Chlordane 0.013J,
TOC mg/I
Ca - Calcium
mg/I
Dieldrin 0.074, Endrin ketone 0.051,
Chloride mg/i
Cd - Cadmium
mg/I
Toxaphene 1.1 J (all ug/L)
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance IiMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Blphenyls method # 8081 B 18082A
(Ammonia Nitrogen, N1­13as N: Ammonia Nitrogen. Total(
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00053J mg/L Effluent TotalVOCs: <0.001 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation \_1
e
Permittee (or Authorized Agent) Name and Title - Please print or type gnature of Permittee for Authorized Agent)
GW-59 Rev.1/2007

CI IRKAIT FnpM 0WYF1 I OW PAPFR ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
NOW1617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-t6f7 Phone: [phone]
FACILITY INFORMATION Please Pnnt
Clearly or lype
PERMIT Number: Expiration Date: 05/31/18
Facility Name Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
"'"
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon A-1
Date sample collected: 1/27/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cord. µMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling
gallons
Appearance
here: r�
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑YES ❑ NO
u
LABORATORY INFORMATION
Date sample analyzed: 2/1/16 TICE, 2/2/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /loom[
Nitrate (NO3) as N
mg/I
Zn -Zinc mg/I
Coliform: MF Total /loom[
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TICE, PEST - all BQL
pH (when analyzed) units
Ba - Barium
mg/l
TOC mg/l
Ca - Calcium
mg/l
Chloride mg/l
Cd - Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS. HPLC)
Phenol mg/I
Fe - Iron
mgil
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
mg/I
Report Attached? R Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
ni
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH, as N, Ammonia Nitrogen. Total)
Mn - Manganese
mg/l
method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only • '-••rts): Influent Total VOCs:-1 100 •/L EffLvnt Total VOC&
'I cerhPi that, to the best of my kno Medge and belief. the information submitted in this report is true. accurate. and comoiete.. and that the tdborarcry am!ytr;at data
DWO-certified laboratory. 1 am aware that there are si nrficant penaffies for submdtiM false information. inchtdmg the possibility of ,oes and irr,• ison'� lent f,.
Garland Hilliard - Director, Environmental Remediation AI'M 0--ARM
<0.001 mg/L VOC Removal% 1 UU
Permittee (or Authorized Agent) Name and Title - Please print or type -'Signature of Pe`rmibee (or AutforizedAgen-fr— ;Date)
GW-59 Rev.112007

Q1 IQhAIT Gr)Pt,A r)Kl VFI I nlAf PGPFR OU Y
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
�1617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print ClearfyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different)
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
Ll Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
;'x
❑ Spray Field ® Remediation: Groundwater
Contact Person Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon A-2
Date sample collected: 2/19/16
FIELD ANALYSES:
WAS
Well Depth ft.
Well Diameter: in.
pH units Temp. C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. f Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified ❑ YES ❑ NO
LABORATOBY. INFORMATION
Date sample analyzed: 3/1/16 TCE 2/26/16 PEST
Laboratory Name Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/1
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn -Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note use MPN method for higrly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCE, PEST - all BQL
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mgil
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/1
Grease and 011s mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mgll
Fe - Iron
mg/1
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen: NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/l
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00077J mg/L Effluept Total VOCs: <0.001 mg/L VOC Removal% 100
GW-59 Rev. 1/2007
2
i�
t

Sl IRMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date. 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone# [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
tram Permit
SAMPLING INFORMATION
If WELL
ELL ID NUMBER (from Permit): Carbon A-1
Date sample collected: 4/28/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
p LMhos
Sec. Cond. i
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: []YES
❑ NO and field acidified: ❑ YES ❑ NO
INFORMATION
LABORATORY
Date sample analyzed: 5/9/16 TCE 5/3/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/l
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: use MPN method for highly turbid Samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al -Aluminum
mg/I
TCE, PEST - all BQL
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS. HPLC)
Phenol mg/1
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? (2d Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH,as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT a NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
�1617
[VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: 423.336,4479
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump n Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon A-2
Date sample collected: 5/17/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft,
Spec. Cond. [ tMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: L] YES L) NO
INFORMATION
LABORATORY
Date sample analyzed: 5/25/16 TCE, 5/24116 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO3) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mgll
Zn - Zinc mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/l
(Note: Use VPNmethodfor highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
beta-BHC 0.025J, Dieldrin 0.0083J, Endrin
pH (when analyzed) units
Ba - Barium
mg/l
ketone 0.0075J (all ug/L)
TOG mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/1
Hg - Mercury
mg/l
Report Attached? M Yes (1) Ll No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mgll
Pest & Biphenyls method # 8081 B ► 8082A
(Ammonia Nitrogen: NH.as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00073J mg/L Effluent Total VOCs_ <0.001 mg/L VOC Removal% i UU
GW-59 Rev.1/2007

si IRNAIT Fnpu nN YFI I OW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
�1617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27639-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or 1 ype
PERMIT Number: Expiration Date: 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
Permit Name (if different)-
NPDES Other
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC County Moore
❑ Lagoon L] Remediation: Infiltration Gallery
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
rmm Permit
If WELL
ELL ID NUMBER (from Permit). Carbon A-2
ell Depth. ft.
�!pth to Water Level: ft. below measuring point
easuring Point is ft. above land surface
)fume of water pumpedibailed before sampling:
amoles for metals were collected unfiltered: ❑YES
_ Date sample collected: 6/24/16
Well Diameter: in.
Screened Interval: ft. to _ft
Relative M.P. Elevation: ft.
_gallons
❑ NO and field acidified: ❑ YES ❑ NO
FIELD ANALYSES:
pH units
Spec. Cond.
Odor
Appearance
Temp. °C
uMhos
Date sample analyzed: 6/29/16 TCE, 7/7/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect
dissolved and
colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NOa) as N
mg/1
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note use VPN method for highly turbid samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
mg/I
Al -Aluminum
mg/I
TICE, PEST - all BQL
pH (when analyzed)
units
Ba - Barium
mg/l
TOC
mg/1
Ca - Calcium
mg/l
Chloride
mg/l
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mgll
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? bid Yes (1) ❑ No (0)
Specific Conductance
tMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia
mg/1
Mg - Magnesium
mg/l
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Totall
Mn - Manganese
mg/I
method #
TKN as N
mg/I
Ni - Nickel
mg/1
method #
RY at
ne of
)mpling,
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: <0.001 mg/L Effluent Total VOCs: <U.UU1 mg/L VOC Removal% i uu
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007
Agent)

SUBMIT FORM ON YELLOW PAPER ONLY
.
PART TENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
tVIStON OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print
ClearfyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge VV00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
if-om Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon A-1
Date sample collected: 7/12/16
FIELD ANALYSES:
WAS
Well Depth. ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. µ Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: C YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORYINFORMATION
Date sample analyzed: 7/15/16 TCE, 7/19/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/1
Zn - Zinc mg/I
Coliform: MF Total 1100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TICE, PEST - all BQL
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/1
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/1
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? R Yes (1) ❑ No (0)
Specific Conductance ItMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & BlphenylS method # 8081 B 18082A
(Ammonia Nitrogen: NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese
mg/l
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00066J mg/L Effluent Total VOCs: <0.00020 mg/L VOC Removal% 100
f errnittee (or AUthorize(l Agent) Name artl I Itle - Please print or type
GVV-59 Rev. 112001

SUt1Nll 1 t-UNM UN T ty1 L!vv r-MrCrt UrvL t
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
1=1617
[VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGN, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
Permit Name (if different):
NPDES Other
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC County Moore
LJ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard Telephone#: [phone]
Rotary Distributor -� Land Application of Sludge
Well Location/Site Name: No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
cram Permit
WELL ID NUMBER (from Permit): Carbon A-1 Date sample collected: 10/4/16
Well Depth: ft. Well Diameter: in.
Depth to Water Level: ft. below measuring point Screened Interval: ft. to ft
Measuring Point is ft. above land surface Relative M.P. Elevation: ft.
Volume of water pumped/bailed before sampling gallons
Samoles for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO
sample analyzed: 10/13/16 TICE, 10/12/16 PEST Laboratory Name: Test America
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
mg/I
Coliform: ME Fecal
/loom]
Nitrate (NO3) as N
mg/I
Coliform: ME Total
/100ml
Phosphorus: Total as P
mg/I
(NoteUse MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
mg/I
Al - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOG
mg/I
Ca - Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mg/l
Arsenic
mg/I
Chromium: Total
mg/l
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/l
Hg - Mercury
mg/I
Specific Conductance
ltMhos
K - Potassium
mg/I
Total Ammonia
mg/I
Mg - Magnesium
mg/I
(Ammonia Nitrogen', NH,as N: Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
TKN as N
mg/I
Ni - Nickel
mgll
FIELD ANALYSES:
911H3
pH units Temp. °C
DRY at
t
Spec. Cord. iMhos
time of sampling,
Odor
check
Appearance
here: ❑
Certification No.
Pb - Lead mg/I
Zn - Zinc mg/l
Other (Specify Compounds and Concentration Units).
beta-BHC 0.076, Dieldrin 0.018J, Endrin
ketone 0.010Jp (all ug/L)
ORGANICS: (by GC, GC/MS. HPLC)
(Specify test and method #. ATTACH LAB REPORT,)
Report Attached? ® Yes (1 } ❑ No (0)
VOC , method # 8260
Pest & Biphenyls , method # 8081 B 18082A
method #
method #
• _ • • • '-•. • • I III • rent Total•Cs: <111111 9111• T• ■•
certify that. to the best of my knowledge and belief. the information submitted in this report is true. accurate. and complete: and that'..e labor.i, cy analytical f'ata wAk rf—" using approved methods of analysis by a
OWO-certified laboratory. I am aware that there are si nifrcanl nalbes for submien false information, lnclud n the possibilit, a li,io; an.impr:> .of'cr > ,rve no violations.
Garland Hilliard - Director, Environmental Remediation — //��-�/
lermllee (or Authorized Agent) Narne and Title - Please print Dr type �Siqnature of Permittee (or AuthorIzed Acient) D
GW-59 Rev. ..

Pr
SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
7MI617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field !� Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING.] NFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon B-2
Date sample collected: 1/27/16
FIELD ANALYSES:
WAS
Well Depth ft.
Well Diameter: in.
pH units Temp. °C
DRY at
time of
Depth to Water Level. ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. µ Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 2/1/16 TCE, 2/2/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/l
Pb - Lead mg/l
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
mg/1
Zn - Zinc mg/I
Coliform: MF Total /1ooml
Phosphorus: Total as P
mg/1
(Note use MPN method ror highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/l
TCE, PEST - all BQL
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/l
Cd - Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mg/l
Grease and Oils mg/l
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? k Yes (1) LJ No (C)
Specific Conductance µMhos
K - Potassium
mg/l
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/l
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NHeas N, Ammonia Nitrogen. Total)
Mn - Manganese
mg/l
. method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCS: 0.00093J mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 1 UU
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007
Agent)
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
PARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
WiF611117COMPLIANCE
ISIoN OF WATER QUALITY -INFORMATION PROCESSING UNIT
REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen NC
County Moore
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ® Remediation Groundwater
Contact Person. Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name-
No. of wells to be sampled.
❑ Water Source Heat Pump ❑ Other.
from Pernitl
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon B-3
Date sample collected: 2/19/16
FIELD ANALYSES:
WAS
Well DepthIt.
Well Diameter: in.
pH units Temp. °C
DRY at
Depth to Water Level. ft. below measuring point
Screened Interval: ft. to
_
ft. Spec. Cond. uMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here. f
Samples for metals were collected unfiltered: LJYES
L NO and field acidified: ❑YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/1/16 TICE, 2/26/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/l
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /loom]
Nitrate (NO3) as N
mg/I
Zn -Zinc mg/I
Coliform: IMF Total /100ml
Phosphorus Total as P
mg/I
(Note Use MPNTethod for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units) .
Dissolved Solids: Total mg/1
At - Aluminum
mg/I
beta-BHC 0.085, delta-BHC 0.015J (all in ug/L)
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/l
Cd - Cadmium
mg/l
Arsenic mg/I
Chromium. Total
mg/l
Grease and Oils mg/I
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ?k Yes (1) �71 No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/l
Mg - Magnesium
mg/I
Pest & BiphenylS method # 80818 1 8082A
(Ammonia Nitrogen: NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/1
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00077J mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permiltee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007
(Date)

SUBMIT P:ORM r1NYFI I nw PAPFR ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
•'
•
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print C!earty or Type
PERMIT Number: Expiration Date. 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Perrnif
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon B-2
Date sample collected: 4/28/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. oC
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. f Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: �(
LJ
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed 5/9/16 TCE, 5/3/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO;) as N
mg/1
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mall
Al -Aluminum
mg/I
beta-BHC 0.085, delta-BHC 0.011J, Dieldrin
pH (when analyzed) units
Ba - Barium
mg/I
0.06213, Endrin ketone 0.043J, Heptachlor
TOC mg/I
Ca - Calcium
mg/I
epoxide 0.0055JpB Toxaphene 0.92J (all
Chloride mg/l
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mall
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mgll
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/l
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitragen. NH3 as N, Ammonia Nitrogen. Total)
Mn -Manganese
mg/l
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: <0.001 mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal % I uU
GW-59 Rev. 112007

SURMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
� •'
'
IWSION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date: 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different).
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): Carbon B-3
Date sample collected: 5/17/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter in.
pH units Temp. C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_
ft. Spec. Cond. µ Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling
gallons
Appearance
here:
Samples for metals were collected unfiltered: DYES
l _7 NO and field acidified: ❑ YES ❑ NO
INFORMATION
LABORATORY
Date sample analyzed: 5/25/16 TICE, 5/24/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NOA as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN meumd for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/1
Al -Aluminum
mg/I
alpha-BHC 0.062, beta-BHC 2.9, delta-BHC
pH (when analyzed) units
Ba - Barium
mg/I
0.56, gamma-BHC 0.043Jp. Dieldrin 0.48,
TOC mg/I
Ca - Calcium
mg/I
Endrin ketone 0.29, Toxaphene 9.9 (all ug/L)
Chloride mg/I
Cd - Cadmium
mg/1
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/l
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen: NH,as N, Ammonia Nitrogen, Totalj
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00073J mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type '-9iq ature or Permittee (or Authorized Agent) ;Date)
GW-59 Rev.112007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
EM1617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Cleany or Type
PERMIT Number: Expiration Date. 05/31/18
Facility Name Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
Tram Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon B-3
Date sample collected: 6/24/16
FIELD ANALYSES:
WAS
ell Depth: ft.
Well Diameter: in.
pH units Temp. "C
DRY at
time of
Depth to Water Level: ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. } Mhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here: ❑
Samples for metals were collected unfiltered ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6129116 TCE, 7/7/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
mg/1
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mgil
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I
TCE, PEST - all BQL
pH (when analyzed) units
Ba - Barium
mgil
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? R Yes (1) ❑ No (0)
Specific Conductance ttMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen: NH3as N, Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
method #
TKN as N mgil
Ni - Nickel
mg/I
method #
or Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: <0,00 1 mgh
i cerfFj that. to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and the
DWQ-certified laboratory, I am aware that there are sign ficant penalties for s bmittinq false information, including the possibility or
Garland Hilliard - Director,• -• •
Permittee (or Authorized Agent) Name and Title - Please print or type '�reture of F
GW-59 Rev. •0
Effluent Total VOCs: . <0.001_ _ mg/L VOC Removal% 100
Date)

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 276SS-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field 5d Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Pennit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon B-2
Date sample collected: 7/12/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. °C
DRY at
Depth to Water Level ft. below measuring point
Screened Interval: ft. to
_ft.
Spec. Cond. (iMhos
time of
sampling,
Measuring Point is fL above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling
gallons
Appearance
here:
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 7/15/16 TICE. 7/20/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/l
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total 1100ml
Phosphorus: Total as P
mg/I
(Note Use MFN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I
TICE 0.42J, beta-BHC 1.1, delta-BHC 0.18,
pH (when analyzed) units
Ba - Barium
mg/I
Dieldrin 0.12p, Endrin ketone 0.083J (all ug/L)
TOC mg/I
Ca - Calcium
mg/l
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance F,Mhos
K - Potassium
mg/l
VOC method # 8260
Total Ammonia mg/l
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen. Total)
Mn -Manganese
mg/1
,method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00066J mg/L El5wnt Total VOCS: <0.00020 mg/L VOC Removal°/ 100
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007
ermittee (or
(Date)
%3,

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
15M,7
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print IXearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different)
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other.
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): Carbon B-2
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH units Temp. `C
DRY at
Depth to Water Level: ft. below measuring point
Screened Interval ft. to
_ft.
Spec. Cond. } ) Mhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/13/16 TCE, 10/12/16 PEST
Laboratory Name: Test America
Certification No.
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations_
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/1
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note use VPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total ma/I
At - Aluminum
mg/I
Aldrin 0.0084Jp, alpha-BHC 0.046J, alpha -
pH (when analyzed) units
Ba - Barium
mg/1
Chlordane 0.049, beta-BHC 1.8, delta-BHC
TOC mg/I
Ca - Calcium
mg/I
0.30, Dieldrin 0.23, Endrin ketone 0.16,
Chloride mg/l
Cd - Cadmium
mg/I
gamma-BHC 0,048, Heptachlor epoxide
Arsenic mg/I
Chromium: Total
mg/I
0.033J. Toxaphene 3.9J (all ug/L)
Grease and Oils mg/I
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance -Mhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B 18082A
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: 0.00053J mg/L Effluent Total VOCs: <0.001 mg/L VOC Removal% 100
GW-59 Rev. 112007
k

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
E15617
IVI5lON OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION PfeasePrint CleadyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
cy:
❑ Spray Field Remediation: Groundwater
Contact Person. Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
lfram Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4S
Date sample collected: 10/5/16
FIELD ANALYSES:
WAS
Well Depth: 41.97 ft.
Well Diameter: 2 in.
pH 4.68 units Temp. 17.89 °C
DRY at
Depth to Water Level 3 4.9 5 ft. below measuring point
Screened Interval: 31.9 ft. to 41.9
ft. Spec. Cond. 97 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 473.49 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
0.5 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORYINFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Noce Use MPN mathod for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al -Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/l
Report Attached? W Yes (1) ❑ No (0)
Specific Conductance trMhcs
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8085A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N ma/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Narre and Title - Please print or type
GW-59 Rev.1/2007

SUBMIT FORM ON YFFI I OW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
15M1617
IVISfON OF WATER QUALITY-] NFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27639-1617 Phone: [phone]
FACILITY INFORMATION Pfease Print Clearty or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
5_w
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Perron)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-5S
Date sample collected: 10/5/16
FIELD ANALYSES:
WAS
Well Depth: 47.44 ft.
Well Diameter: 2 in.
pH 4.22 units Temp. 17.68 °C
DRY at
Depth to Water Level: 38.89 ft. below measuring point
Screened Interval: 37.4 ft. to
47.4 ft. Spec. Cond. 48 µMhos
time of
sampling.
Measuring Point is ft. above land surface
Relative M.P. Elevation: 471.36 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
0.5 gallons
Appearance Clear
here ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/1
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
;Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/1
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOG mg/I
Ca - Calcium
mg/I
Chloride mg/1
Cd - Cadmium
mg/1
Arsenic mg/1
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? W Yes (1) 11 No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B /8082A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ann'°nia Nitrogen, N"'as N, Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
method #
TKN as N mg/i
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev. 112007

SUBMIT FORM ONYELL=PAPER ONLY
W I
-
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• •
,
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different).
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field 9 Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
!Torn Perms
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6S
Date sample collected: 10/5/16
FIELD ANALYSES:
WAS
ell Depth: 47.01 ft.
Well Diameter: 2 in.
pH 3.88 units Temp. 18.80 °C
DRY at
time of
Depth to Water Level: 41.15 ft, below measuring point
Screened Interval: 37. ft. to 47.0 ft. Spec. Cond. 145 µMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 464.73 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 0.75 gallons
Appearance Slightly Cloudy
here r t
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES LINO
LABORATORYINFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/1
Pb - Lead mg/I
Coliform: ME Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: ME Total /100ml
Phosphorus: Total as P
mg/l
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOG mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium- Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Soecific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenlys method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/1
method #
(Ammonia Nitrogen, NH,as Nl Ammonia Nitrogen. Total)
Mn - Manganese
mg/l
method #
TKN as N mg/l
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/t_ VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type Slgna re of Permittee (or AuthorizedAqent) (Date)
GW-59 Rev.1/200/

SUBMIT FORM ON YEl I OW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearty or Type
PERMIT Number: Expiration Date. 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen " "' NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled.
from Permfl
❑ Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-10S
Date sample collected: 10/5/16
FIELD ANALYSES:
WAS
Well Depth 41.36 ft.
Well Diameter: 2 in.
pH 4.64 units Temp. 17.44 °C
DRY at
Depth to Water Level: 25.53 ft. below measuring point
Screened Interval: 31.3 ft. to 41_3
ft. Spec. Cond. 29 IMhos
time of sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 461.50 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 10.5 gallons
Appearance Slightly Cloudy
here: r— 1
Samples for metals were collected unfiltered El YES
❑' NO and field acidified' ❑ YES ❑ NO
u
LABORATORY INFORMATION
Date sample analyzed: 10/12/16 PEST, 10/13/16 TCE
Laboratory Name: Test America
Certification No, 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/1
Coliform: MF Fecal /loom)
Nitrate (NO3) as N
mg/l
Zn - Zinc mgll
Coliform: MF Total /10oml
Phosphorus: Total as P
mg/1
(Ncte Use MPN method for highly turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TCE - Results attached
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? Ik Yes (1) 1 1 No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenlys method # 8081 B / 8082A
(Ammonia Nitrogen: NH3as N, Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev. 1/2007

Sl IRMIT FORM ON YELLOW PAPER ONLY
EMMMEPARTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IMM1617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION PfeasePrint GeanyorType
PERMIT Number. Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
imm Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-16S
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth: 68,04 ft.
Well Diameter: 2 in.
pH 4.31 units Temp. 17.50 °C
DRY at
time of
Depth to Water Level: 46.02 ft. below measuring point
Screened Interval: 58. ft. to
68. ft. Spec. Cond. 63 µMhos
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 484.58 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
5.0 gallons
Appearance Clear
here.
Samples for metals were collected unfilteredLJYES
❑ NO and field acidified: ❑ YES ❑ NO
u
LABORATORY INFORMATION
Date sample analyzed: 10/12/16 PEST, 10/13/16 TCE
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: ME Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: ME Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
rngll
TCE - Results attached
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/1
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mgll
ORGANICS: (by GC. GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/l
Hg - Mercury
mgll
Report Attached? M Yes (1) n No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenlys method # 8081B / 8082B
(Ammoria Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn -Manganese
mgll
,method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee or Authorized Aqent)
GW-59 Rev.1/2007

SUBMI r FORM ON YELLOW PAPER ONLY
PARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
11W617
ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field W Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permrc
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-17S
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
ell Depth: 59.42 ft.
Well Diameter: 2 in.
pH 4.46 units Temp. 17.61 °C
DRY at
Depth to Water Level. 46.37 ft. below measuring point
Screened Interval: 49.4 ft. to 59.4 ft. Spec. Cond. 66 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 48022 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 5.25
gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES ❑
NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16 PEST, 10/13/16 TCE
Laboratory Name Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mgll
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Noce_ use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al -Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TCE - Results attached
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenlys method # 8081 B / 8082A
(Ammonia Nitrogen; NH,as N, Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mgll
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
PARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
4111ISION
71me"
OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person. Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
ifrGm re,ma
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-18S
Date sample collected: 10/4116
FIELD ANALYSES:
WAS
Well Depth: 4 9.7 5 ft.
Well Diameter: 2 in.
pH 4.03 units Temp. 20.21 °C
DRY at
Depth to Water Level 4 7.6 3 ft. below measuring point
Screened Interval: 39.7 ft. to
49.7
ft. Spec. Cond. 94 FtMhos
time of sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 467.83 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 0.4
gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered. ❑YES ❑ NO and field acidified. ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16 PEST, 10/13/16 TCE
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: ME Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mgll
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TICE - Results attached
TOC mg/l
Ca - Calcium
mg/l
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GCIMS, HPLC)
Phenol mg/I
Fe - Iron
ma/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/l
Pest & Biphenlys method # 8081 B / 8082A
(Ammonia Nitrogen. N113as N. Ammonia Nitrogen, Total)
Mn -Manganese
mgll
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs: mg/L VOC Removal%
Permittee (or Authorized Agent) Name and I dte - Please print or type
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
PARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
EW61\17
ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Prnt Clearly or Iype
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.
No. of wells to be sampled:
❑ Water Source Heat Pump LJ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-11 D
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth: 75.39 ft.
Well Diameter: 2 in.
pH 3.98 units Temp. 17.35 °C
DRY at
Depth to Water Level 69.31 ft. below measuring point
Screened Interval: 65 ft. to
75
ft. Spec. Cond. 16 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 463.41 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 2.5
gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES ❑
NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16 PEST, 10/13/16 TCE
Laboratory Name Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /loom]
Nitrate (NO3) as N
mg/l
Zn - Zinc mg/I
Coliform: MF Total /10oml
Phosphorus: Total as P
mg/l
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
A] - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TCE - Results attached
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC. GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mgil
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? I] Yes (1) ® No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC . method # 8260
Total Ammonia mg/l
Mg - Magnesium
mg/I
Pest & Biphenlys method # 8081 B / 8082A
(Ammonia Nitrogen: NH,as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/l
.method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007
of
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NG 27699-1617 Phone: [phone]
FACILITY INFORMATION PleasePrint ClearlyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ RemediationInfiltration Gallery
Aberdeen NC 28315 County Moore
'-
❑ Spray Field lk Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump n Other:
from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-16D
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Vell Depth 123.57 ft.
Well Diameter: 2 in.
pH 4.24 units Temp. 18.52 "C
DRY at
Depth to Water Level: 92.82 ft. below measuring point
Screened Interval: 113 ft. to
123 ft. Spec. Cond. 38 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 487.55 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance Clear
here.
El
Samples for metals were collected unfiltered: EYES ❑ NO and field acidified: ❑YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/13/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (i as N
mgfl
Pb - Lead mg/I
Coliform: MF Fecal /loom[
Nitrate (NO,) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /loom]
Phosphorus: Total as P
mg/I
(Note use MPN method for highly turbid samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg.I
Al - Aluminum
mg/I
TCE - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/l
Ca - Calcium
mg/1
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
ni
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen. N1­13as N: Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal°/
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007

SURMIT FORM ONYELI.OVV PAPER ONLY
EPAR7MENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
o "SIQN OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Pnnt Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different).
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ RemediationInfiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
from Permii
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
ELL ID NUMBER (from Permit): MW-17D
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth 123.17 ft.
Well Diameter: 2 in.
pH 4.39 units Temp. 17.65 °C
DRY at
time of
Depth to Water Level: 94.65 ft- below measuring point
Screened Interval: 113 ft. to
123
ft. Spec. Cond. 27 tiMhos
sampling,
Measuring Point is ft- above land surface
Relative M.P. Elevation: 489.60 ft.
Odor None
check
Volume of water pumped/bailed before sampling
4 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/14/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCE - Results attached
pH (when analyzed) units
Ba - Barium
mg/l
TOC mg/l
Ca - Calcium
mg/I
Chloride mg/l
Cd - Cadmium
mg/I
Arsenic mg/1
Chromium: Total
mg/I
Grease and Oils mg/1
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS. HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/l
VOC method # 8260
Total Ammonia mg/l
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/1
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.11200]

SUBMIT FORM ON YELLOW PAPER ONLY
MIMMEPARTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field 5d Remediation: Groundwater
Contact Person Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
from Permil
El Water Source Heat Pump El Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-18D
Date sample collected: 10/5/16
FIELD ANALYSES:
WAS
Well Depth: 72.36 ft.
Well Diameter. 2 in.
pH 4.09 units Temp. 16.93 °C
DRY at
Depth to Water Level: 56.20 ft. below measuring point
Screened Interval: 62.6 ft. to
72.3
ft. Spec, Cond. 73 µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 447.41 ft,
Odor None
check
Volume of water pumped/bailed before sampling:
3 gallons
Appearance Clear
here. f ,
Sam les for metals were collected unfiltered: ❑ YES
U NO and field acidified: ❑ YES ❑ NO
u
LABORATORY INFORMATION
Date sample analyzed: 10/12/16 PEST, 10/13/16 TCE
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/1
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/1
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/1
Al -Aluminum
mg/I
TCE - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TCL Pesticides - Results Attached
TOC mg/I
Ca - Calcium
mg/1
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mgll
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenlys method # 8081 B 18082 A
(Ammonia Nitrogen: NH,as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/1
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007
Agent)
:Date)

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
EMIT1117
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Pnnt Clearly or Type
PERMIT Number: Expiration Date: 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field IXl Remediation Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
ram Perms
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-20D
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth: 47.44 ft.
Well Diameter: 2 in.
pH 4.23 units Temp. 17.79 °C
DRY at
Depth to Water Level 37.29 ft. below measuring point
Screened Interval 37.4 ft. to 47.4
ft. Spec. Cond. 31 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 421.24 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
2 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered ❑YES
n NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/1
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phcsphorus: Total as P
mg/I
(Note Use MPNmethod for highly turbid Samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/1
AT - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/l
TOC mg/1
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mg/1
Grease and Oils mg/l
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/1
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mgll
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ® No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest R Biphenyls method # 8081 B / 8082A
Total Ammonia mg/l
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen; NH,as N; Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
. method #
TKN as N mg/1
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mglL Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.112007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
.
a
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
0
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please PnntClearly crType
PERMIT Number: Expiration Date 05/31/18
Facility Name. Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
Permit Name (if different):
NPDES Other
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-22D
Date sample collected: 10/4116
FIELD ANALYSES:
WAS
Well Depth: 85.73 ft.
Well Diameter: 2 in.
pH 4.29 units Temp. 17.83 °C
DRY at
Depth to Water Level: 66.47 ft. below measuring point
Screened Interval 75.7 ft. to
85.7
ft. Spec. Cond. 31 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 449.23 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
4.5 gallons
Appearance Clear
here ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ElYES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/l
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/l
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/1
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1
Fe - Iron
mgil
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/1
method #
(Ammonia Nitrogen', NH3as N', Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
. method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev. 112007

SUBMIT FORM ON YELLOIdLPAPER ONLY
EPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
NMI
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM17
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print ClearfyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen NC 28315 County Moore
il_+ej
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
(from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-23D
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth: 87.96 ft.
Well Diameter: 2 in.
pH 4.41 units Temp. 17.24 eC
DRY at
Depth to Water Level: 66.95 ft. below measuring point
Screened Interval 77.9 ft. to 87.9 ft. Spec. Cond. 26 µMhos
-
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 455.22 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
4.5 gallons
Appearance Clear
here: �l
Samples for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES Li NO
U
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO,) as N
mg/I
Zn -Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid sampies)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units)
Dissolved Solids: Total mg/I
AI - Aluminum
mg/1
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/1
TOG mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total --mg/1
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance E,Mhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen. NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total Vi ni VOC Removal%
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print CteadyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Gelgy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ RemediationInfiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field IR Remediation: Groundwater
Contact Person. Garland Hilliard
Telephone#: 423,336.4479
❑ Rotary Distributor ❑ Land Application of Sludge
Well LocationiSite Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ElOther:
--
0— Puma
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MVV-26D
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth. 27•35 ft.
Well Diameter: 2 in.
pH 4.35 units Temp. 17.69 °C
DRY at
Depth to Water Level: 6.66 ft. below measuring point
Screened Interval: 17.3 ft. to 27.3
ft. Spec. Cond. 46 FtMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 378.95 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
4 gallons
Appearance Clear
here:
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note use MPNmelhodfor hlghlyturbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/l
TOC mg/I
Ca - Calcium
mall
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/1
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? W Yes (1) ❑ No (0)
Specific Conductance uMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH, as N: Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: _Cz mg/L VOC Removal%
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
ImtvisioN
OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
Permit Name (if different):
NPDES Other
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
1 1 Spray Field M Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name
No. of wells to be sampled:
n Water Source Heat Pump ❑ Other:
rmm Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-30D
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth. 75.38 ft.
Well Diameter: 2 in.
pH 3.53 units Temp. 16.92 °C
DRY at
Depth to Water Level 58.45 ft. below measuring point
Screened Interval 65.3 ft. to
75.3
ft. Spec. Cond. 76 µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 451.25 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
3.5 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: PEST 10112/16. TICE 10/13/16
Laboratory Name. Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/1
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPNmethodfor highly turbid sample%)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units)
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
m9/1
TCE - Results attached
TOC mg/I
Ca - CalCium
mg/I
Chloride mg/I
Cd - Cadmium
mg/l
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/l
Report Attached? M Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # 8260
Total Ammonia mg/I
Mg - Magnesium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
(Ammonia Nitrogen, NH3as N: Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
.method #
TKN as N mg/i
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.112007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IMM1617
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print CleartyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon J RemediationInfiltration Gallery
Aberdeen NC 28315 County Moore
zs '
❑ Spray Field Remediation Groundwater
Contact Person. Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor Land Application of Sludge
ell Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump n Other.
o-om Pe,r,a
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-22L
Date sample collected: 10/4/16
FIELD ANALYSES:
WAS
Well Depth: 145.20 ft_
Well Diameter: 2 in.
pH 3.89 units Temp. 19.54 °C
DRY at
Depth to Water Level: 68.34 ft. below measuring point
Screened Interval: 135 ft. to
145
ft. Spec. Cond. 49 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 449.51 ft.
Odor None
check
Volume of water pumped/bailed before sampling: 12.5
gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES ❑
NO and field acidified: OYES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: ME Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid Samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/l
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) LJ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH�as N, Ammonia Nitrogen. Total)
Mn -Manganese
mg/l
,method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg/L VOC Removal%
GW-59 Rev. 1/2007

Cl IPKAIT Pr)PM nKl VPI I n%A1 PAPi nNl V
W -
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:0.
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearfy or Type
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Tele hone#: 423-336.4479
p
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name.
No. of wells to be sampled:
from Permit
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-25L
Date sample collected: 10/5116
FIELD ANALYSES:
WAS
Well Depth: 74.60 ft.
Well Diameter: 2 in.
pH 4.59 units Temp. 17.54 Its
DRY at
Depth to Water Level: 25.00 ft. below measuring point
Screened Interval: 64.6 ft. to 74.6
ft. Spec. Cond 26 uMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 384.63 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
6 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered. ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100m]
Nitrate (NOA as N
mg/I
Zn - Zinc mgll
Coliform: MF Total /loom]
Phosphorus: Total as P
mg11
(Note use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/1
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? bild Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenlys method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen; NH3as N, Ammonia Nitrogen Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
i Rev.112007
of Permittim-(a7"AuthtSrized Aqent)
Z �3
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
U.MPEPARTMENT
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
1=1617
IVISIO.N OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
o---n Per a
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-27L
Date sample collected: 10/19/16
FIELD ANALYSES:
WAS
Well Depth: 86.54 ft.
Well Diameter: 2 in.
pH 3.09 units Temp. 17.06 °C
DRY at
Depth to Water Level 31.60 ft. below measuring
p g point
Screened Interval: 76.5 ft. to
86.5
ft. Spec. Cond. 75 µ Mhos
time of
sampling,
Measuring Point is tt. above land surface
Relative M.P. Elevation: 397.13 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
9 gallons
Appearance Clear
here.l l
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES NO
u
LABORATORY INFORMATION
Date sample analyzed: 10/26/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO,) as N
mg/1
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
Note Use MPN method for highly h,rbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units)
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/l
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) 1-1 No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen: NH3as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: ni Effluent Total VOCs. ---�� mg/L VOC Removal%
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
imml(lii7
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699A617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen "' "" NC 28315 County Moore
❑ Spray Field 5a Remediation. Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-31 L
Date sample collected: 10/19/16
FIELD ANALYSES:
WAS
Well Depth: 22.0 ft.
Well Diameter: 2 in.
pH 3.44 units Temp. 23.91 °C
DRY at
Depth to Water Level: 1.74 ft. below measuring point
Screened Interval: 12.0 ft. to
22.
_
ft. Spec. Cond. 65 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 332.68 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
4 gallons
Appearance Clear
here. ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified. ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/26/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mgil
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: ME Fecal /100ml
Nitrate (NOA as N
mg/I
Zn - Zinc mg/I
Coliform: ME Total /100ml
Phosphorus: Total as P
mg/I
(Note Use rv1PNmPtnnefor highly turbid Samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al -Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/1
Chromium: Total
mg/I
Grease and Oils mg/1
Cu - Copper
mgil
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mgil
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007

SI IRMIT FORM nN YFI_LOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date. 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person. Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location!Site Name.
No. of wells to be sampled.
❑ Water Source Heat Pump ❑ Other:
Rnm Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-32L
Date sample collected: 10/19/16
FIELD ANALYSES:
WAS
Well Depth: 26.99 ft.
Well Diameter: 2 in.
pH 3.82 units Temp. 19.53 °C
DRY at
Depth to Water Level: 3.97 ft. below measuring point
Screened lnterval: 16.9 ft. to 26.9 ft. Spec. Cond. 32 uMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 322.45 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
4.5 gallons
Appearance Clear
here:
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/26/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I Pb - Lead mg/I
Coliform: MF Fecal /loom[
Nitrate (NO3) as N
mg/I Zn - Zinc mg/I
Coliform: MF Total /10oml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/1 Other (Specify Compounds and Concentration Units)'
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/1
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg!I
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I ORGANICS: (by GC GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I (Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/1 Pest & Biphenyls , method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/I method #
(Ammonia Nitrogen: NH,as IN: Ammonia Nitrogen, Total)
Mn - Manganese
mg/I method #
TKN as N mg/I
Ni - Nickel
mgA method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: ___ mg/L Efflyent Total VOCs /—'' mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007
Authorized Aqent)

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
MOINPDES
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-36L
Date sample collected: 10/4116
FIELD ANALYSES:
WAS
Well Depth 106.0 ft.
Well Diameter: 2 in.
pH 4.40 units Temp. 17.06 °C
DRY at
Depth to Water LeveL 36.40 ft. below measuring point
Screened Interval 96.0 ft. to
106
—
ft. Spec. Cond.1 g µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation. 414.18 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
10 gallons
Appearance Clear
here.
Samples for metals were collected unfiltered: EYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: ME Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al - Aluminum
mg/l
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOG mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mgil
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
moll
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/1
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls , method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen. NH3 as N: Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
.method #
TKN as N mg/I
Ni - Nickel
mg/1
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007
.-
ind that the laboratory anr!yitcal ,-?'d
ilit • of fir and Snr, iscnrrs +1 : it i.nr!,n!
mg/L VOC Removal%

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING;
j
Jj11
VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date, 05/31 /18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled
❑ Water Source Heat Pump ❑ Other:
from Permu
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-37L
Date sample collected: 10/5/16
FIELD ANALYSES:
WAS
Well Depth: 46.18 ft.
Well Diameter: 2 in.
pH 4.39 units Temp. 16.89 °C
DRY at
Depth to Water Level: 11.00 ft, below measuring point
Screened Interval: 36.1 ft. to 46.1
ft. Spec. Cond. 32 uMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 354.86 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
6 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO.) as N
mg/I
Ph - Lead mg/I
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
mg/l
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/l
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/1
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? bd Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/1
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/l
Mg- Magnesium
mg/I
method #
(Ammonia Nitrogen: NH,as N: Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/1
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type - ignature of Permittee (or Authorized Agent)
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
ISM116117
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print
DearfyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ® Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
from Permit
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-38L
Date sample collected: 10/19/16
FIELD ANALYSES:
WAS
Well Depth: 28.14 ft.
Well Diameter: 2 in.
pH 4.25 units Temp. 20.05 °C
DRY at
Depth to Water Level 9.58 ft. below measuring point
Screened Interval: 18.1 ft. to 28.1
ft. Spec. Cond. 51 tiMhos
time of
sampling,check
Measuring Point is ft. above land surface
Relative M.P. Elevation: 327.30 ft.
Odor None
Volume of water pumped/bailed before sampling:
4 gallons
Appearance Clear
here: L7
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: LL YES Ll NO
LABORATORY INFORMATION
Date sample analyzed: 10/26/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/1
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO,) as N
mg/1
Zn - Zinc mg/I
Coliform. MF Total /100ml
Phosphorus: Total as P
mg/1
(Note use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
AI - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC. GC/MS. HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? M Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081B / 8081A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NHias N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs mg/L VOC Removal%
GW-59 Rev.112007

CI IAKAIT FnRAA ON VFI I OVU PAPFR r1Nt Y
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
WIMID617
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen NC 28315 County Moore
❑ Spray Field ❑X RemediationGroundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
fwrPernut
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-39L
Date sample collected: 10/19/16
FIELD ANALYSES:
WAS
Well Depth: 20.29 ft.
Well Diameter: 2 in.
pH 3.99 units Temp. 23.16 °C
DRY at
Depth to Water Level. 3.97 ft. below measuring point
Screened Interval: 10.2 ft. to 20.2 ft. Spec. Cond. 62 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 389.86 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
3 gallons
Appearance Clear
here. ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/26/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO,) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units)
Dissolved Solids: Total mg/I
Al -Aluminum
mg/l
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mgll
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mgll
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mg/l
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? k Yes (1) ( 1 No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/l
Mg - Magnesium
mg/I
method #
(.Ammonia Nitrogen, NH,as N: Ammonia Nitrogen. Totals
Mn -Manganese
mg/1
,method #
TKN as N mg/I
Ni - Nickel
mg!I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007
of Pe? ittee (a Autrorized Agent)
'Date)

SUBMIT FORM ON YELLOW PAPER ONLY
_
q
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
0 a
0
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print CiearfyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ RemediationInfiltration Gallery
Aberdeen NC 28315 County Moore
'-
❑ Spray Field M Remediation: Groundwater
Contact Person. Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
—, Pe—M
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-40L
Date sample collected: 10/19/16
FIELD ANALYSES:
WAS
Well Depth: 27.76 ft.
Well Diameter: 2 in.
pH 3.41 units Temp. 18.72 °C
DRY at
Depth to Water Level: 1.75 ft. below measuring point
Screened Interval: 17.7 ft. to
27.7
ft. Spec. Cond. 38 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P, Elevation: 334.45 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
12.5 gallons
Appearance Cloudy
here
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: [:]YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/26/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/l
Nitrite (NO.) as N
mg/l
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/l
Arsenic mg/1
Chromium: Total
mg/I
Grease and Oils mg/1
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate -mg/l
Hg - Mercury
mg1I
Report Attached? M Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/1
Mg - Magnesium
mg/I
method #
(Ammonia Nit`oge NH,- N, Amm°nia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
PARTMENT OF ENVIRONMENT & NATURAL RESOURCES
ROUNDWATER QUALITY MONITORING:
lime,
VISION OF WATER QUALITY -IN FORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM17
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Pont Clearly or Type
PERMIT Number: Expiration Date. 05/31/18
Facility Name Geigy Chemical Corporation Site
Non -Discharge W00009949 UIC
NPDES Other
Permit Name (if different):
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen "'' NC 28315 County Moore
❑ Spray Field R Remediation: Groundwater
Contact Person: Garland Hilliard
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
from Permit,
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): PZ-2
Date sample collected, 10/5/16
FIELD ANALYSES:
WAS
Well Depth: 36.18 ft.
Well Diameter: 2 in.
pH 4.50 units Temp. 18.81 °C
DRY at
Depth to Water Level: 5.15 ft. below measuring point
Screened Interval: 26.1 ft. to
36.1
-
ft. Spec. Cond. 30 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 343.79 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
5.5 gallons
Appearance Clear
here -
Samples for metals were collected unfiltered: [-]YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name: Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
Al - Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
Chloride mg/I
Cd - Cadmium
mg/l
Arsenic mg/I
Chromium. Total
mg/I
_
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/l
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen. N113as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mgll
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs mg/L VOC Removal%
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev 112007

SUBMIT FORM ON Y II I OW PAPER ONLY
ARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
SION OF WATER QUALITY -INFORMATION PROCESSING UNIT
761V117,
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print ClearfyorType
PERMIT Number: Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949 UIC
NPDES Other
Permit Name (if different)
Facility Address: Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Aberdeen NC 28315 County Moore
Spray Field k Remediation Groundwater
Contact Person: Garland Hilliard
Tele hone#: 423.336.4479
p
❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name:
No. of wells to be sampled:
Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): PZ-3
Date sample collected: 10/5/16
FIELD ANALYSES:
WAS
Well Depth: 61.54 ft.
Well Diameter: 2 in.
pH 4.40 units Temp. 16.90 °C
DRY at
Depth to Water Level 3 5.6 9 ft. below measuring point
Screened Interval: 51.5 ft. to
61.5
-
ft. Spec. Cond. 20 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: 381.02 ft.
Odor None
check
Volume of water pumped/bailed before sampling:
4 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑ YES
C NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 10/12/16
Laboratory Name. Test America
Certification No. 269
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/l
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/1
Al - Aluminum
mg/l
TCL Pesticides - Results attached
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/l
Chloride mg/ I
Cd - Cadmium
mg/l
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached? ❑X Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/l
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia mg/l
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen: NH,as N. Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/l
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L EfflVM Total VOCs: mg/L VOC Removal%
Garland Hilliard - Director, Environmental Remediation
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: Imi,
VISION OF WATER QUALITY4NFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
17 MAIL SERVICE CENTER, RALEIGH,
NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Pnnt Clearly or Type
PERMIT Number:
Expiration Date: 05/31/18
Facility Name: Geigy Chemical Corporation Site
Non -Discharge WQ0009949
UIC
Permit Name (if different):
NPDES
Other
Facility Address. Domino Drive
TYPE OF PERMITTED OPERATION BEING MONITORED
Aberdeen " ' NC 28315 County Moore
❑ Lagoon
❑ Remediation: Infiltration Gallery
n Spray Field
nX Remediation: Groundwater
Contact Person. Garland Hilliard Telephone#: [phone]
❑ Rotary Distributor
❑ Land Application of Sludge
Well Location/Site Name: No. of wells to be sampled:
n Water Source Heat Pump
❑ Other:
from Fermit
CAMP[ IMr. IMPr)PRil rIN
If WELL
ILL ID NUMBER (from Permit): PZ-5
II Depth: 30.12 ft.
)th to Water Level: 4.62 ft. below measuring point
asuring Point is ft. above land surface
ume of water pumped/bailed 'before sampling:
voles for metals were collected unfiltered: EYES
Date sample collected: 10/19/16
Well Diameter: 2 in.
Screened Interval: 20.1 ft. to 30.1 ft
Relative M.P. Elevation: 335.98 ft_
5 gallons
❑ NO and field acidified: U YES U NO
FIELD ANALYSES:
pH 3.19 units
Spec. Cond.
Odor None
Appearance Clear
Temp. 21.60 °C
RR uMhos
sample analyzed: 10/27/16
Laboratory Name: Test America
Certification No. 269
:AMETERS NOTE: Values should reflect
dissolved and
colloidal concentrations.
COD
mg/I
Nitrite (NO,_) as N
mg/1
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total
/loom]
Phosphorus: Total as P
mall
(Note use MPN method for highly turbid sampled
Orthophosphate —mull
Other (Specify Compounds and Concentration Units).
Dissolved Solids: Total
mg/I
Al -Aluminum
mg/I
TCL Pesticides - Results attached
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
mg/I
Ca - Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? n Yes (1) n No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
Pest & Biphenyls method # 8081 B / 8082A
Total Ammonia
mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev. 1/2007
DRY at
time of
sampling,
here:1
-11

enviroirac
Environmental Services
May 9, 2017
Mr. Jon Bornholm
Remedial Project Manager
USEPA Region IV
61 Forsyth Street, SW
Mail Code: 9T25
Atlanta, Georgia 30303-8960
RE: 2016 Annual Operating Report Comments Response
Groundwater Remediation Permit No. W00009949
Geigy Chemical Corporation CERCLA Site
Aberdeen, North Carolina
Dear Mr. Bornholm
In response to your letter dated March 8, 2017 requesting additional information please see the
responses to your questions below.
1. First page, last paragraph: Please provide the month/year when these activated carbon
drums were exchanged.
The activated carbon drums were exchanged on August 3, 2016.
2. Second page, last paragraph: This paragraph discusses the construction of new
residential dwellings on Campbell Street. Please confirm that no potable wells were
installed with this new construction.
Based on a telephone conversation with Harold Watts, Aberdeen Public Works, no
potable wells have been installed at the new residences.
3. Table 4: Please provide the rationale as to why resampling occurred in the first and
second quarters.
In the first quarter sampling event conducted in January 2016, beta-BHC was reported in
the laboratory results of the effluent sample. However, laboratory analysis of samples
collected from both Carbon A and Carbon B lines reported all analytes below detection
limits. Therefore, a resampling event was completed in February 2016, and all analytes
were reported below detection limits in the effluent sample.
During the second quarter, beta-BHC was reported again in the effluent sample
collected in April 2016. As a result, the carbon drums were exchanged and a resampling
event was conducted in May. Unfortunately the May laboratory results were suspect due
to probable inadvertent laboratory switching of samples at sample log -in. Quarterly
sampling was thus conducted again in June. Laboratory results for the June sampling
were inconsistent as the laboratory experienced several QC issues which increased
laboratory error. We worked with the laboratory extensively to eliminate the QC issues
and results from the third quarter sampling in July were consistent with historical values.
These inconsistencies in quality control and results attributed to laboratory error were
7434 West Friendly Avenue: Suite J. Greensboro, North Carolina 27410 ( Office [phone] 1 Fax [phone]
www.envirotrac.com

tvirT
Environmental Services
reviewed in detail with our laboratory in order to ensure more consistency during the
2017 sampling events. To date, the first and second quarter 2017 results have been
consistent with historical values and the expected laboratory quality control has been
achieved.
4. Attachment 4 — BHC isomer Trend Graphs and Figures: FYI — the color schemes used
to represent each contaminant were consistent in all the graphs except for the graph for
MW-1ID.
The graph for MW-11 D has been updated.
Should you have questions regarding the report, please contact Chris Hay at [phone].
Sincerely,
ENVIROTRAc LTD.
Gail G. Hay, P.E.
Senior Engineer
ChristopherW. Hay, E.I.
Principal
Enclosure
Cc: Doug Rumford, NCDEQ Superfund Section
Michael Rogers, NCDEQ DWR
Garland Hilliard, Olin Corporation
George Crouse, Syngenta
7434 West Friendly Avenue, Suite J, Greensboro, North Carolina 274101 Office (336) 763-60251 Fax [phone]
www.envirotrac.com

•
Rogers, Michael
From: Christopher Hay, El, RSM <[e-mail]>
Sent: Tuesday, May 09, 2017 2:44 PM
To: [e-mail]- Rumford, Doug; Rogers, Michael
Cc: Garland E. Hilliard ([e-mail]); George Crouse ([e-mail])
Subject: Geigy Chemical Corporation CERCLA Site - Aberdeen, NC - 2016 Annual Operating Report
Comments Response
Attachments: EPA—Response—Geigy-2016 Operating Report.pdf
Gentlemen,
Please find the attached letter in response to EPA's comments in their letter dated March 8, 2017 requesting additional
information for the Geigy Chemical Corporation CERCLA Site 2016 Annual Operating Report.
Christopher Hay, El, RSM I Regional Operations Manager I EnviroTrac Ltd. 17343 West Friendly Ave Suite J, Greensboro NC 27410
336.763.6025 (Office) 1336.763.6034 (Fax) 1 336.602.0977 (Cell) I [e-mail]
Solutions in Action -.hftp://www.envirotrac.com
i.rtt l "—raw racy
Think before you point

enviroirac
Environmental Services
May 9, 2017
Mr. Jon Bornholm
Remedial Project Manager
USEPA Region IV
61 Forsyth Street, SW
Mail Code: 9T25
Atlanta, Georgia 30303-8960
RE: 2016 Annual Operating Report Comments Response
Groundwater Remediation Permit No. WQ0009949
Geigy Chemical Corporation CERCLA Site
Aberdeen, North Carolina
Dear Mr. Bornholm:
In response to your letter dated March 8, 2017 requesting additional information please see the
responses to your questions below.
1. First page, last paragraph: Please provide the month/year when these activated carbon
drums were exchanged.
The activated carbon drums were exchanged on August 3, 2016.
2. Second page, last paragraph: This paragraph discusses the construction of new
residential dwellings on Campbell Street. Please confirm that no potable wells were
installed with this new construction.
Based on a telephone conversation with Harold Watts, Aberdeen Public Works, no
potable wells have been installed at the new residences.
3. Table 4: Please provide the rationale as to why resampling occurred in the first and
second quarters.
In the first quarter sampling event conducted in January 2016, beta-BHC was reported in
the laboratory results of the effluent sample. However, laboratory analysis of samples
collected from both Carbon A and Carbon B lines reported all analytes below detection
limits. Therefore, a resampling event was completed in February 2016, and all analytes
were reported below detection limits in the effluent sample.
During the second quarter, beta-BHC was reported again in the effluent sample
collected in April 2016. As a result, the carbon drums were exchanged and a resampling
event was conducted in May. Unfortunately the May laboratory results were suspect due
to probable inadvertent laboratory switching of samples at sample log -in. Quarterly
sampling was thus conducted again in June. Laboratory results for the June sampling
were inconsistent as the laboratory experienced several QC issues which increased
laboratory error. We worked with the laboratory extensively to eliminate the QC issues
and results from the third quarter sampling in July were consistent with historical values.
These inconsistencies in quality control and results attributed to laboratory error were
7434 West Friendly Avenue, Suite J, Greensboro, North Carolina 27410 1 Office [phone] 1 Fax [phone]
www.envirotrac.com

Ift
env roi Qom.
Environmental Services
reviewed in detail with our laboratory in order to ensure more consistency during the
2017 sampling events. To date, the first and second quarter 2017 results have been
consistent with historical values and the expected laboratory quality control has been
achieved.
4. Attachment 4 — BHC isomer Trend Graphs and Figures: FYI — the color schemes used
to represent each contaminant were consistent in all the graphs except for the graph for
MW-1ID.
The graph for MW-11 D has been updated.
Should you have questions regarding the report, please contact Chris Hay at [phone].
Sincerely,
ENVIROTRAc LTD.
luuA w
Gail G. Hay, P.E.
Senior Engineer
5o +�04'
Christopher W. Hay, E.I.
Principal
Enclosure
Cc: Doug Rumford, NCDEQ Superfund Section
Michael Rogers, NCDEQ DWR
Garland Hilliard, Olin Corporation
George Crouse, Syngenta
7434 West Friendly Avenue, Suite J, Greensboro, North Carolina 27410 1 Office [phone] 1 Fax [phone]
www.envirotrac.com