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HomeMy WebLinkAboutNCG120064_DMR_20200924� a A August 28, 2020 Chambers Development of NC, Inc. and Waste Connections of the Carolinas, Inc. Anson Waste Management Facility 375 Dozer Road Polkton, NC 28135 Attention: Mr. Tyler Fitzgerald Reference: Monthly Stormwater Monitoring Anson Waste Management Facility NCG120064 Polkton, North Carolina S&ME Project No. 4140-15-007 Dear Mr. Fitzgerald: l69 `3 DEVAYETTEVILLE REGIONAL OFFICE S&ME, Inc. (S&ME) is pleased to submit this report detailing the results of the August 2020 stormwater monitoring activities conducted at the Anson Waste Management Facility (AWMF) in Polkton, North Carolina. This work was completed in accordance with our Master Services Agreement dated January 2, 2017, and in accordance with Task 2 in S&ME Proposal No. 41-1600394 (Rev. 1) dated August 8, 2016. This letter summarizes results of sampling efforts conducted by facility personnel. ® Background Stormwater sampling is required on a semi-annual basis, as defined by the National Pollutant Discharge Elimination System (NPDES) General Permit for Landfills (Permit No. NCG120000) for the facility outfalls. The following outfalls are identified at the facility: Outfall 1, Outfall 2, Outfall 3, Outfall 4, Borrow Area North Outfall, and Borrow Area West Outfall. Outfall 2 was eliminated in August 2018 by the expansion of Sediment Basin 3 and, therefore, is no longer sampled. Monthly sampling was initiated following December 2019 results at Outfall 3 and Outfall 4, in response to Tier 2 and Tier 3 response actions at the facility. Parameters for quantitative analysis include chemical oxygen demand (COD) per Standard Method (SM) 2540D, fecal coliform per SM 9222D, and total suspended solids (TSS) utilizing SM 2540D. In addition to the previously listed parameters, Outfall 1 and Outfall 3 are also sampled for chemical parameters associated with vehicle maintenance which include total petroleum hydrocarbons (TPH) per Environmental Protection Agency (EPA) Method 1664B and pH utilizing SM 4500. Stormwater Sampling and Quantitative Analyses AWMF personnel collected the August stormwater samples at two (2) designated outfall locations on August 18, 2020. The total rainfall for the August 18, 2020 storm event was reported as approximately 0.83 inches in 24 hours. Sampling was performed during that storm event. S&ME, Inc. 1 644 Eastern Star Road l Kingsport, TN 37663 1 p 423.349.2800 1 www.smeinc.com X 9 a Monthly Stormwater Monitoring Anson Waste Management Facility S&ME Project No. 4140-15-007 Quantitative chemical laboratory results for the monitoring event are compared to benchmark values established by the facility NPDES permit on the attached Discharge Monitoring Report (DMR). Parameter exceedances of benchmark values, if any were documented through field and laboratory analyses, are summarized in bold type below. Benchmark 120: 100 . 1000 15 6 - 9 Outfall3 Sed Basin 3 <25.0 54.7 450 <7.6 6.63 Outfall 4 Sed Basin 4 31.7 11.4 3500 ANR 6.81 ANR = Analyte not requested and not required by the NPDES Permit mg/l= milligrams per liter CFU/ml= colony -forming units per milliliter The DMR is included with this letter as Attachment I for signature and submittal to the North Carolina Department of Environmental Quality (NCDEQ), Division of Water Quality. The Laboratory Data Report for this sampling event is included as Attachment II. ® Closure S&ME appreciates this opportunity to be of service to Waste Connections and trust this information is responsive to your current needs. If you have any questions, please contact us at your convenience. Sincerely, S&ME, Inc. rdAOrris Project Manager Attachments: Discharge Monitoring Report Laboratory Data Report Site SWPPP Map Victor M. Augspurger Senior Reviewer cc: Mike Lawyer, Fayetteville Regional Office Lana Brown, Waste Connections Nelson Breeden, Waste Connections of the Carolinas, Inc. Page 2 Attachments Attachment I — Discharge Monitoring Report F.I. O O O O N (7 u z O z a m AY' W N GJ U i O H cu M C f0 m L C ui v- O c O M 0 C u s O z 4- M ia e� Z� a El ❑� N C. 7 CL OL = O Elf�6 3 3Ll y 3 = ❑ p oEl 3 3� L d o s N N �,pri0 ❑❑❑ Q } f100 00 g z p ❑❑■ uj O O O p a Z U a a Q 2 N Q to Q lA ,I - co I o of N Uco O c Z :3 LUU LL O > N O uQ LL W 0 LU a z¢ zz U LQ1. U W U 3 Ma 4 C m N m p `o c W O ,U '2 c Q d Z U E b N m UJ a J } c p to 0 Uo4, z a: m E CL u T C n O 0 _ '6 M q Oo CL ,m 6 t0 (O (O O m y M 0 c. o L M r- v - bA ° o O .- v3i (A E c u Y ei E -•� wCL LO LO CA A m M m u c LPL O u c d OG O L OD N M r u E G04 M E C (D L V w C •i 3 G1 N CO m CC) y O u p E C ttoo O O ,c m — N N N •i L C) cm N Ln d 0000 ar c o m u E 07 07 z c 00 U M -Adh a L. Cc Ca � p E _ a 0 o m a° c co v E d cu o :�i 3 5 O 6 I v E v .v V) LA 7 Q a) OL t N dA -Y p �. M t `' E m " E v v t O o c a — 00 o N� v f0 c 3 z .0 a) w oq E Y O U N N = > N N a, � N CL > x �. a, ° 3 v v o Ln E o O a, a U += `M L 3 Z s v vCL v 4° v � += e o v o a E a O M 'G E ED : v L J £ a) tm u to aj 4 m X pa M v Qi m t E o L a°1i c U O E 3 �, J m 3 O v E. c o E=L. N� Y v O +, O N. E Lm u U L C � N v o m 3 :p X -0 !A �1v..r Y _ m L N B E 6 3 o L v o��i = c w n E C M OU = to •� L G y O w p u}1 0 +_+ A O N +,,, L. a = o Ln > ax E 3 4 E m `o v 3 C O O u N LL -0>. C W M a 4 4 U Ln L COL a) -A C M 'O a)L C r i=.. EA•- M E c .c +� "" Q) O Ln O M a-+ M c v v 4' p k c Ua"O c E v E c, O C _ N E 0 v � 4 (Ao a, 0 -o + v N O } a H O 00 C O aO+ N L �' to -- 'O ++ .0 a 00 to .O coo ++ Q v O o \ 0. CL a U d E M c°ai Q M 4-o m - E 4- a, M 0 (D cu °J _U O at 'L- o C O L N N . 41 a)U y, E LL H N O M a)O •1.+ 4J .� N m a Z C •D Z G. 0 v 4 a Co ,� G O •O 3 C O CIO LA Ln A bA C •m m N .m L C O ai m O _u 3 C i 0 J O ;lk-Z, Z `O r `0 O 3 d z O O L M h C Op aoo OLn O uLO !n � r O F- 0) 0 rNI L m 0 V O a e 0 Z c 0 E m m C u N Im L C - d O 7 O itt Q N M a a O � N uoc d ' N \ z Q 0 E E 00 n 00 am-• m co v Z Y L W O — m o a° m a s 0 Q M m 0 mH a t m CL O N O c O 0 LL Z z z ■ _o t z W to I- w �. W a f- J J LL W M. =) w 0 w z 00 Z } W Z �a WLIJ Q c w w CO N Q K 0 W d cc W w W C N L N — o W cr Q -j d .J_I LLLLZ w =w ao Z w El LU y) 2 NN LU W x X w Z H w u Ll Y LL L Q CC LL W w Q 0 cr W u Z ui 2 z o CC m C7 at LU a � N Q w w M N 0 0 Q w x w x LLI u LL a0�F� M z a Z a LuaWoz U O O ,= Z Q Q > o x 0 = 2 w u w U z LLI LL wL&j LL m w w >' o Q N P: Q z ■ O t9 w w n r-I v 41 0 0 Y 1Q u (A O c 1 C E Qw 41 o tW T C u ,0 m E m b'D o 3 3 Y o u C Y C O •- i i 4- L N -fl Y O CL o c r o m E C C O C C O w O O CL CL G1 v C a, o E N Y Y 'O O > m L. - v O '> O C C Q y �- O C O 0 .0 N E-+ AO Y O O N � '� Q O m ' C 44,10 Y o v E C L :3 o c a C m c O E O 3 Y L Y m o m +n E c C p N O U C _vOi M Y o m `—° 1 Eo c m � m L E a`, c 4- u N N v ul T M m a`) 0 Q C Y Q Q Y m o v o +' CL _O m @ O c Q v�L Q T m v Q_ t m 4' O 1 41 C s 0 Y +- Q m v 3 m m - 0 t E C m 4-1m 00 0 N N Attachment II - Laboratory Data Report aceAnalytical www.pacelabs.com August 24, 2020 Lindsey Harris SWE, Inc. 644 Eastern Star Road Kingsport, TN 37663 RE: Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 Dear Lindsey Harris: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on August 18, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, " cwc Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures - AS,'RBO- 2- qe� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 P { aceAnalytical www.pacelabs.com CERTIFICATIONS Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92491267001 Outfall 3 EPA 1664B HH 1 PASI-C SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 RED 1 PASI-A SM 5220D-2011 NAL 1 PASI-A 92491267002 Outfall 4 SM 9222D-2006 KDF 1 PASI-C SM 2540D-2011 RED 1 PASI-A SM 5220D-2011 NAL 1 PASI-A 92491267003 Outfall 1 EPA 1664B HH 1 PASI-C PASI-A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 aceAnalytical www.pecalabs.com SUMMARY OF DETECTION Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92491267001 Outfall 3 SM 9222D-2006 Fecal Coliforms 450 CFU/100 mL 1.0 08/19/20 13:40 SM 254OD-2011 Total Suspended Solids 54.7 mg/L 6.3 08/20/20 18:33 92491267002 Outfall 4 SM 9222D-2006 Fecal Coliforms 3500 CFU/100 mL SM 2540D-2011 Total Suspended Solids 11.4 mg/L SM 5220D-2011 Chemical Oxygen Demand 31.7 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 1.0 08/19/2013:40 3.3 08/20/2018:34 26.0 08/24/2014:48 Page 4 of 14 y 'r aceAnalytical www.pacolabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 Sample: Outfall 3 Lab ID: 92491267001 Collected: 08/18/20 08:29 Received: 08/18/20 11:39 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 7.6 1 08/24/20 10:51 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 460 CFU/100 mL 1.0 1 08/18/20 14:24 08/19/20 13:40 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 64.7 mg/L 6.3 1 08/20/20 18:33 6220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand ND mg/L 25.0 1 08/23/20 16:21 08/24/20 14:48 Sample: Outfall 4 Lab ID: 92491267002 Collected: 08/18/20 08:01 Received: 08/18/20 11:39 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 3500 CFU/100 mL 1.0 1 08/18/20 14:24 08/19/20 13:40 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 11.4 mg/L 3.3 1 08/20/20 18:34 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services - Asheville Chemical Oxygen Demand 31.7 mg/L 25.0 1 08/23/20 16:21 08/24/20 14:48 Sampler Outfall 1 Lab ID: 92491267003 Collected: 08/18/20 08:14 Received: 08/18/20 11:39 Matrix: Water Parameters 1664 SGT-HEM, TPH Total Petroleum Hydrocarbons Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 1664E Pace Analytical Services - Charlotte ND mg/L 7.5 1 08/24/2010:51 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2020 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 Y Y Pace Analytical Services, LLC te 100 aceAnalytical ® 9800Hunte svlle, NCKincey Ave. 128078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 QC Batch: 561898 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92491267001, 92491267003 METHOD BLANK: 2980095 Matrix: Water Associated Lab Samples: 92491267001, 92491267003 Blank Reporting Parameter Units . Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 08/24/20 10:43 LABORATORY CONTROL SAMPLE: 2980096 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 18.6 93 64-132 MATRIX SPIKE SAMPLE: 2980097 92491329001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 15.3 74 64-132 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2020 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 aceAnaljdical www.pacelabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater- Monthly Pace Project No.: 92491267 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 560742 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92491267001, 92491267002 METHOD BLANK: 2974810 Matrix: Water Associated Lab Samples: 92491267001, 92491267002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 08/19/20 13:40 SAMPLE DUPLICATE: 2974811 92491267001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 450' 460 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2020 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 r aceAnalytical www.picelabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 561370 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92491267001, 92491267002 METHOD BLANK: 2977740 Matrix: Water Associated Lab Samples: 92491267001, 92491267002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/20/20 18:20 LABORATORY CONTROL SAMPLE: 2977742 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 97 90-110 SAMPLE DUPLICATE: 2978122 92491381001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 230 232 1 SAMPLE DUPLICATE: 2978123 92491263001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 111 98.7 11 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2020 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 (�IaceAnaljdical" www.pacelabs.com Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 QC Batch: 561812 QC Batch Method: SM 5220D-2011 Associated Lab Samples: 92491267001, 92491267002 QUALITY CONTROL DATA Analysis Method: Analysis Description: Laboratory: SM 5220D-2011 5220D COD Pace Analytical Services -Asheville METHOD BLANK: 2979829 Matrix: Water Associated Lab Samples: 92491267001, 92491267002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 08/24/20 14:41 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2979830 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 751 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2979831 2979832 MS MSD 92490400002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 1660 100 100 1730 1730 69 69 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2979833 2979834 MS MSD 92490474001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[ Chemical Oxygen Demand mg/L 68.7 100 100 175 175 106 106 90-110 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2020 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 1� aceAnaljftal www.pacelabs.com QUALIFIERS Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2020 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 AnalXical(�Iac www.pacelabo.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater - Monthly Pace Project No.: 92491267 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92491267001 Outfall 3 EPA 1664B 561898 92491267003 Outfall 1 EPA 1664B 561898 92491267001 A Outfall 3 SM 9222D-2006 560742 SM 9222D-2006 560743 92491267002 Outfall 4 SM 9222D-2006 560742 SM 9222D-2006 560743 92491267001 Outfall 3 SM 2540D-2011 561370 92491267002 Outfall 4 SM 2540D-2011 561370 92491267001 Outfall 3 SM 5220D-2011 561812 SM 5220D-2011 561992 92491267002 Outfall 4 SM 5220D-2011 561812 SM 5220D-2011 561992 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/24/2020 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14 aCBAnalyficaI Document Name: Sample Condition Upon Recei t(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville� Raleigh❑ Mechanicsville[] ConditionSamplo Client Name: Upon Receipt r ^ Project t: WII O(I'# II I. I�9LI2II 49l l'1I� 267 C❑ Commercial �Cll�entourier: ❑FedEx�U�P�SEDIUSPS f4paceezaeizs F-6.A., cnal Prntnnf? Mvac IWNn Seals Intact? I IYes ONO Date/InitlalsPerson Examining Packing Material: ❑Bubble Wrap �Bubble Bags ❑None ❑ Other Biological Tlss Frozen? /J p1 �� Thermom: 92FTO61 Type of Ice; b4wet []Blue []None None []Yes❑NoV/A R Gun ID; Cooler Temp (•C): Correction Factor: Add/Subtract (•C) 0.0 Temp should be above freezing to 6•C Cooler Temp Corrected (•C):_ ❑Samples out of temp criteria, Samples on ice, cooling process has begun USDA Regulated Soil (tQI/A, water sample) Old samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ram.. rt_. .,.6�.n.,•u�u��i� ..A Du 'tn A1r 171- 1vat r 1Nn Comments/Discrepancy: Chain of Custody Present? Yes EJN0 N/A 1. Samples Arrived within Hold Time? Yes No N/A 2. Short Hold Time Analysis 02 hr.)? Yes Pbo N/A 3. Rush Turn Around Time Requested? Yes No E1NtA 4. Sufficient Volume? MYes QNo ❑N/A - 5. Correct Containers Used? -Pace Containers Used? es Yes [:]No[ oft --]N/A N/A 6. Containers Intact? MYes [:]No N A 7. Dissolved analysis: Samples Field Filtered? ❑Yes INNO N n 8. Sample Labels Match COC? (FlYes ❑No ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix; Heads ace in VOA Vials >5-6mm ? C3Yes C3No /A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes []Yes ❑No QN0 N/A /A 11. COMMENTS/SAMPLE DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATIONIRESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? Oyes ❑No Page 12 of 14 a ". aCeAnaliftal Document Name: Sample Condition Upon Recel t(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: Issuing Authority: /- F-CAR•CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box If pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coiiform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project ri r WQ## : 92491267 PM: AMB Due Date: 08/25/20 CLIENT: 92-SAME TN n D a J E m 9 n a a. .J c 3 m 9 a a .J E ro 3i �r= +3 6. Y 3 m N = u a J E on N Z T y a '.., of z 6 m 2 0 C Z a J E N m N , x0 z u �/ E u mY, c n M 3 '�, E v Z a a E Q n V x E Q °: ,y 1 d c = ¢ J o N �q�' �J _ d E Q ti :.i ry V S .. a EE d. J E i+i J N Mf Z _ t� a O D J o rM z O J c�qE N Z a a a OR .I o Or z r�Z s m a d E Q o � s= "W a A s U] CL t: " a A _y � ,n Ln a d r d E o y 2 °� E Q a c dE E Q B oc .a a { �I E > n j E E J c�E z l � 3 r V 4 S 6 7 8 9 10 11 N \N 12 L- pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N Note: wnenevertnere is a oiscrepancy aneccing rvvnn %.drmum w,,,P„u„Lc aumP,ca, o ..vpr I� �••�� ••+^^ ^ • ••�+•••• •" •••- ••"• •••--•-••••- __...... __. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 13 of 14 of fl oq� a4 ITEM # r U 0 0 0 Co z 0 . C) > m P P 0 Z ;a M C E5 1-1 (,V Ib X- b C Lq m*o w 9¢S - 0 CL MATRIXCODE (see valid codes to lefl) SAMPLE TYPE (G=GRAB CzCOMP) In 0 m -0 a<Jl m Z 0 z m r Fn =Wj $AMP LE TE M P AT COLLECTION OF CONTAINERS -V -0 9 D 0 Fi, Unpreserved X.. C) - 0 R 1 QP H2804 50 HNO3 HCI ip m ro NsOH WS203 CD Methanol 9 > ,;m Other Pp Me q0, Yft- �J X >4 COD X >4 Fecal Coli (8 Hr Hold) In X X TPH Oil and Grease by 166, x X TSS to ILAJ O V TEMP in C z Residual Chlorine (YIN) Received on Ice (YIN) g, CS � T—usroTy— Sealed Cooler JJ (YIN) Samples Intact (YIN) j 0 Page 14 of 14 ;, , Attachment III — Site SWPPP Map LL_ IAJ z 0 6 z En ir 0 y z w W 2 OW L" < Ir _. _j z 0:: ( < w w z FW-_Ld -j Z< — > �< Lod Z z z Qv) 0 i� �le !q:- - LQLl Lei. - Lei.LOJ Z) :5 Fx m li rn _j WE 0 (D En (MV) (D WO 'a<- 0 wo H "k E z AY owtvelw1vol4w - O*W - Owtvam M I"