WQ0000957_Monitoring - 07-2020_20200817

Nor
August 10, 2020
VALLEY PROTEINS, INC.
L
001
4L
C
LL
DeLj—
partment of Environment &Natural Resources
Division of Water Resources — Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Valley Proteins, Inc. — Wadesboro Division,
Permit #WQ0000957
Enclosed please find the Quarterly Monitoring Wells Report for our Wadesboro, North
Carolina Division.
If you require any additional information or wish to discuss the information in this report,
please feel free to call me at [phone].
Sincerely,
Matt Ha
General Manager �
66 Little Duncan Road
W'adeAvro, NC 28170
O 540.8-72590
Making a Sustainable Difference. as 704.694.6145
�-1-ul leyprotein5.com

SUBMIT FORM ON YELLOW PAPER ONLY
119�,
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617Phone: [phone]i
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge WQ0000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
0 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #9
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permd
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#1
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Well Depth: 33 ft.
Well Diameter: 2 in.
pH 7 units Temp. 18 eC
DRY at
Depth to Water Level: 14.64 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 1656 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
9.0 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample ailaiyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
13.7 mg/I
Zn - Zinc mg/1
Coliform: MF Total /100ml
Phosphorus: Total as P
.092 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 974 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7.1 units
Ba - Barium
mg/I
TOC 1.8 mg/I
Ca - Calcium
mg/I
Chloride 346 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 30.5 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Agent) Name and Title - Please print or type
Authorized Agent)
(Date)
GW-59 Rev. 1/2007

aceAnalytical
www.pacolabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92488133
Sample: MW-1
Lab ID: 92488133001 Collected: 07/28/20 10:15
Received: 07/28/20 15:35 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/BMS
1
07/28/20 10:15
Collected Date
07/28/20
1
07/28/20 10:15
Collected Time
10:15
1
07/28/20 10:15
pH
7.0 Std. Units
1
07/28/20 10:15
Temperature
18.0 deg C
1
07/28/20 10:15
Static Water Level
14.64 feet
1
07/28/20 10:15
Specific Conductance
1656 umhos/cm
1
07/28/20 10:15
Total Well Depth
33.19 feet
1
07/28/20 10:15
Odor
None
1
07/28/20 10:15
Appearance
Clear
1
07/28/20 10:15
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Chai lotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/28/20 16:53 07/29/20 15:56
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
974 mg/L 50.0
1
07/30/20 18:02
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.1 Std. Units 0.10
1
08/02/20 15:31
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
30.5 mg/L 1.0
1
07/29/20 22:21
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
08/04/20 11:23
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
13.7 mg/L 0.80
20
07/28/20 23:44
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.092 mg/L 0.050
1
07/29/20 20:36 07/30/20 19:25
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
346 mg/L 20.0
20
07/30/20 22:54
16887-00-6
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 45

aceAnalytical
www.pecolabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-1 Lab ID: 92488133001 Collected: 07/28/20 10:15 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310E TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon 1.8 mg/L 1.0 1 08/01/20 11:07 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 45

Document Name: Field data Sheet
Date Issued: March 8, 2019
ace.tfj�ff�al'
Page: 1 of
Document Number: F•CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality
Office .
Name and Affiliation (Inspector):
Well Information
Well ID: vvkw — I
Well Diameter: all
Total Well Depth: '93 1, ft
Static Water Level: g, (,g
i
Height of Water Column:—mAx5 ft
Vyell Locked:
d-Project #: ST4"+ i TejC1
i
Date: 7• A -do
NO / Flushmount )
Construction: (I Steel/Stainless Steel)
Multi Factor": a � ('(Radius/12)2 x 3.14 x 7.48]
Casing Volume: 1,0 gallons
Cal, 3 Volumes: q .0 gallons
Pump Intake:. __ ' —ft
Purge Information
Date Purged:// �p Start: j�Finish:11 oq� Purge Rate:
Purging Method: `%c, .1(/ Total Volume Purged: 9.0 go:n)smls/L)
Samnliniz Infozmation
Date Collected: Q1— /2-Sj 2Q ` Time Collected: 016. r 5 /pm)
? Sampling Equipment Used: ?,at l4r" Instrument ID:__ Y �+��44'
Bottle Type Preservation Analysis Required
3 -gomA W A
'Y;1 c
tf 1) I&rph0-5
r- 1
- w.k NtiNF. ,t-t�5 �f1YIWSjkty f�►yir+AL
Field Measurements/Observations
Sample Temp (°C): 0 Time: O ] S Turbidity (ntu): Time:
Diss Oxy (mg/L): Time: Fe 2+ mg/L: Time:
Specific Cond. (uS): I Co F(o Time: 1 D ; (5.- Res. Cl (mg/L)/(ug/L):=Time:. r--
Sample pH (s.u.): Time: ( 0 ; I `� Odor: Nb AT Time: / O 1 6
ReDox (mV): "'�' Time: Appearance: _ (Ji-A - Time: 1015
ReDox (EH value):YSI ProPlus +200mV Other: Time:
General/Weather Observations:. JA !�_ f .
Sampler Signature
Stabilization Test
M
surlycloudy/rain Temp.2Q_(°F) Wind Sfb t D (mph)
Time
Purged
Temp.
(oC)
Digs Oxy.
(mg/L)
Spec,
(us)
pH (s.u.}
ReDox
(mV)
Turbidity
(ntu)
Volume
r oved
allo MIS/
Water
level (ft)
Other
a
Page 38 of 45

SUBMIT FORM ON YELLOW PAPER ONLY
IMF.DEPARTMENT
OF ENVIRONMENT &'NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��16117
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
❑K Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #4
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#2
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 6.9 units Temp. 19 °C
DRY at
Depth to Water Level: 10.25 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 1925 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling: 11.25 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /loom[
Nitrate (NO3) as N
11 mg/I
Zn - Zinc mg/I
Coliform: MF Total /loom[
Phosphorus: Total as P
.079 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 1040 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7 units
Ba - Barium
mg/I
TOC 1 mg/I
Ca - Calcium
mg/I
Chloride 423 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 7.6 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/[
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
Authorized Aqent)
Sl1e'
GW-59 Rev. 1/2007

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-2 Lab ID: 92488133002 Collected: 07/28/20 09:45 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/BMS
1
07/28/20 09:45
Collected Date
07/28/20
1
07/28/20 09:45
Collected Time
09:45
1
07/28/20 09:45
pH
6.9 Std. Units
1
07/28/20 09:45
Temperature
19.0 deg C
1
07/28/20 09:45
Static Water Level
10.25 feet
1
07/28/20 09:45
Specific Conductance
1925 umhos/cm
1
07/28/20 09:45
Total Well Depth
33.16 feet
1
07/28/20 09:45
Odor
None
1
07/28/20 09:45
Appearance
Clear
1
07/28/20 09:45
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms,
ND CFU/100 mL 1.0
1
07/28/20 16:53 07/29/20 15:56
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
1040 mg/L 50.0
1
07/30/20 18:02
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.0 Std. Units 0.10
1
08/02/20 15:20
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
7.6 mg/L 1.0
1
07/29/20 22:36
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
08/04/20 11:25
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
11.0 mg/L 0.20
5
07/28/20 23:45
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.079 mg/L 0.050
1
07/29/20 20:36 07/30/20 19:27
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
423 mg/L 20.0
20
07/30/20 22:34
16887-00-6
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
WPA9
H3
Page 7 of 45

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-2 Lab ID: 92488133002 Collected: 07/28/20 09:45 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310E TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 08/01/20 11:43 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 45

Document Name: Field data Sheet
Date Issued: March 812019
Page: 1 of t
,. aGeAwlj,tkafL
Issuing Authority: Pace untersville Quality,
Document Number: F•CAR-FLD-001-cev.03
Office
Name and Affiliation (Inspector):
Well Information
Well ID: Y%w D-
Well Diameter: a li
Total Well Depth: ft
Static Water Level:,t C7 `J✓ - ft
Height of Water Column:1--ft
4zi -
Date: 7-a9-do
Well Locked: ((REV NO / Flushmount )
Construction: (IC�Steel/StainlessSteel)
Multi Factor*: o. t 3 (*(Radius/ 12)2 x 3.14 x 7.48)
Casing Volume: 3_ gallons.
Cal. 3 VoIumes: gallons
Pump Intake: ft
Purge Information
Date Purged:07/�/,A-j-_ Start : I D '' ► 5 Finish: J 0 Z� Purge Rate:
Welk
By: W.
Purging Method: R1 t e vl Total Volume Purged:
Sampling Information , r
Date Collected: // Time Collected: `t �' a pm)
Instrument ID:
Sampling Equipment Used: �i;t ,�-V' •
Bottle Type Preservation
1-aspA P1u5 J Q
N o of —
Field Measurements/Ob�serva"t�ions
Sample Temp (°C): _ i q • 0 Time: Uq 145 Turbidity (ntu):
Analysis Required
.rr�l-� � TPhoS
�T�S (cklor►r,�a,, s� ��vr ���y,�h.,
-"" Time:
Dins Oxy (mg/L): Time: Fe 2+ mg/L: Time:
Specific Cond. (uS):Time: 0 iy 5� Res. Cl (mg/L)/(µg/L): Time:.
Sample pH (s.u-): Time: 09 4 Odor: &0n Time: 0`7Lt 5
ReDox (mV): Time: 0'745 Appearance: C 1 e4y- Time: 0,745
ReDox (F.H value):YSI ProPlus +200rriV` Other: Time:
General/Weather Observations:
sunn /cloudy/ralny) Temp--Za °F) Wind 2f l) (mph)
Sampler Signature
Stahilization Test
Time
Purged
Temp.
(°C)
Diss Oxy.
(mg/L)
Spec.
(S)
pH (a.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
r oved
/mis/
Ll
Water
level (ft)
Other
Zolo
✓�
5J
,
-_-
Page 39 of 45

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OFENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
[VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 ` Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number:
Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957
NPDES
UIC
Other
Permit Name (if different):
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION
❑ Lagoon
BEING MONITORED
❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
© Spray Field
❑ Remediation:
contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor
❑ Land Application of Sludge
Nell Location/Site Name: Behind Field #1
No. of wells to be sampled: 8
❑ Water Source Heat Pump
❑ Other:
fram Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#3
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Nell Depth: 29.2 ft.
Well Diameter: 4 in.
pH 7.1 units
Temp. 18.9 °C
DRY at
Depth to Water Level: 15.32 ft. below measuring point Screened Interval: ft. to
ft. Spec. Cond.
1923 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor None
check
Volume of water pumped/bailed before sampling:
12.0 gallons
Appearance Clear
here: El
for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
sample analyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
,AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
N/D /100ml
Nitrate (NO3) as N
6.2 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
N/D mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
1110 mg/I
Al - Aluminum
mg/I
pH (when analyzed)
7.1 units
Ba - Barium
mg/I
TOC
1.2 mg/I
Ca - Calcium
mg/I
Chloride
388 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
171 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia
ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N; Ammonia Nitrogen,
Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory ana.ytical data was produced using approved methods of analysis by a
_-.__.__.___-____ _. __--g--ffic--t
.._ ..____:_ _ ._.._ _ _ .------ ----- ---_ --- - - ---V-ng
__.. ..__-_
DWQ certiFied laborato I am aware that there are si_ ncant haloes for submttih false..informaton; including the possibility f^.as- and rmpn- ;onment for knowing violations._
Permittee (or Authorized Aqent) Name and Title - Please print or tVpe
ii �e (or Authorized Aqent) D

aceAnapica l
www.pacolabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92488133
Sample: MW-3 Lab ID: 92488133003 Collected: 07/28/20 11:00 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/BMS
1
07/28/20 11:00
Collected Date
07/28/20
1
07/28/20 11:00
Collected Time
11:00
1
07/28/20 11:00
pH
7.1 Std. Units
1
07/28/20 11:00
Temperature
18.9 deg C
1
07/28/20 11:00
Static Water Level
15.32 feet
1
07/28/20 11:00
Specific Conductance
1923 umhos/cm
1
07/28/20 11:00
Total Well Depth
27.31 feet
1
07/28/20 11:00
Odor
None
1
07/28/20 11:00
Appearance
Clear
1
07/28/20 11:00
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/28/20 16:53 07/29/20 15:56
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
1110 mg/L 50.0
1
07/30/20 18:03
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.1 Std. Units 0.10
1
08/02/20 15:37
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
171 mg/L 3.0
3
07/30/20 03:33
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
08/04/20 11:29
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate
6.2 mg/L 0.12
3
07/28/20 23:46
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050
1
07/29/20 20:36 07/30/20 19:28
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
388 mg/L 20.0
20
07/30/20 22:34
16887-00-6
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
Page 9 of 45

117;a'ce Analytical
www.pacelabs.com
f
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-3 Lab ID: 92488133003 Collected: 07/28/20 11:00 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon 1.2 mg/L 1.0 1 08/01/20 12:19 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 45

Cer{lic9F}rfiedl4
�
Document Name: Field data Sheet
Date Issued: Marche 8, 2019
Page: 1 of 1
.Document Number: F-CAR-FLD•001-rev.03
Issuing Authority: Pace Huntersville Quality
Office
Name and Affiliation (Inspector): . N 1 I,
Well Information
Wel1ID: M\ —3
Well Diameter: I yx
Total Well Depth: a 7.3 ft
Static Water Level: 1 `✓ 3 ';k ft
Height of Water Column:_ "q ft
Well Locked:
Construction:
#: S Qnu,l W 0 e I I.s
Date: 7- -C�a By: BRG'
i NO / Flushmount )
Steel/Stainless Steel)
Multi Factor": 0 •(OJ 3 r(Radius/12)2 x 3.14 x 7.48).
Casing Volume: gallons.
Cal. 3 VoIumes; gallons
?
Pump Intake: ft
Purge Information
Date Purged: 0 0 Start: I i I Finish: �l -s'� Purge Rate:
Purging Method: '�n.�� for Total Volume'Purged: 2 0 &/nds/L)
41
Sampling Information pr�
Date Collected:C)T/a!f aV Time Collected: 00 a pm)
Sampling equipment Used: Ve V_ Instrument ID:_ 6 i 414
Bottle Type
Preservation
tn� . /J0')4�
Field Measurements/Observations
Sample Temp (°C): 1$ 9 Time: aD Turbidity (ntu):
Analysis Required
— Time; 1n
Diss Oxy (mg/L): , . Time: '--\ Fe 2+ mg/L: Timer
Specific Cond. (uS): _ Time: ,_ Res. Cl (mg/LY(µg/L): Time:.
Sample pH (s.u.): Time: (1 : 9;ID Odor: Nod Time: W 00
ReDox (mV): '� Time: Appearance: GR Pair Time: _ i : V 0
ReDox (EH value):YSI ProPlus +200mV Other: "'-----' Time:
General/Weather Observations:_ "�l wt_ 3
Sampler Signature
Stabilization Test
su cloudy/rainy) Temp.70_(°F) Wind Elk (mph)
v
Time
Purged
Temp.
(°C)
Diss Oxy,
(mg/L)
LCond.
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
( 0 /mis/
Water
level (ft)
Other
-.�
Z(Z3
Du
42
3
Page 40 of 45

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT&' NATURALRESOURCES
GROUNDWATER QUALITY MONITORING:
1=1617
IVISION of WATER QUALITYaNFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC`27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
1 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Pond #1
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#5
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Well Depth: 29.2 ft.
Well Diameter: 2 in.
pH 6.6 units Temp. 18.5 °C
DRY at
Depth to Water Level: 9.71 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 2345 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation.
ft.
Odor None
check
Volume of water pumped/bailed before sampling: 9•75 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: El YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
N/D mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.089 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 1340 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.7 units
Ba - Barium
mg/I
TOC 2.0 mg/I
Ca - Calcium
mg/I
Chloride 392 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 32.4 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Agent) Name and Title - Please print or type
Aqent)
GW-59 Rev.1/2007

Pace Analytical Services, LLC
aceAnalytical 2225 Riverside
Asheville, NC 2880404
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Sample: MW-5 Lab ID: 92488133004 Collected: 07/28/20 09:00 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/BMS
1
07/28/20 09:00
Collected Date
07/28/20
1
07/28/20 09:00
Collected Time
09:00
1
07/28/20 09:00
pH
6.6 Std. Units
1
07/28/20 09:00
Temperature
18.5 deg C
1
07/28/20 09:00
Static Water Level
9.71 feet
1
07/28/20 09:00
Specific Conductance
2345 umhos/cm
1
07/28/20 09:00
Total Well Depth
29.63 feet
1
07/28/20 09:00
Odor
None
1
07/28/20 09:00
Appearance
Clear
1
07/28/20 09:00
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method: SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/28/20 16:53 07/29/20 15:56
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
1340 mg/L 125
1
07/30/20 18:03
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+6-2011
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.7 Std. Units 0.10
1
08/02/20 15:14
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
32.4 mg/L 1.0
1
07/29/20 23:36
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
08/04/20 11:31
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
07/28/20 23:15
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.089 mg/L 0.050
1
07/29/20 20:36 07/30/20 19:29
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
392 mg/L 20.0
20
07/30/20 22:35
16887-00-6
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 45

aceAnalytical
www.pacelabsxam
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92488133
Sample: MW-5 Lab ID: 92488133004 Collected: 07/28/20 09:00 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon 2.0 mg/L 1.0 1 08/01/20 12:43 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 45

Document Name: Field data Sheet
Date Issued: March 8, 2014
aceAtv441cal'
Pap: 1 of
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality
f
Office
Client: K Lo
- -rTr:
Name and Affiliation (Inspector); .
Well Information
Well ID: m �Sr
Well Diameter: a 1
Total Well Depth: °• b 3 ft
Static Water Level: 7' 1 ft
Height of Water Column:_P Iq U
Well Locked:
Date: '7-ag-ab
NO / Flushmount )
Construction: 9t1/Stee1/Stain1ess Steel)
Multi Factor*: [ (Radius/12)2 x 3.14 x 7.48]
i
Casing Vo)ume: gallons.
Cal. 3 Volumes: qJ5 gallons
Pump Intake: PJA ft
By: 4-ACT
'Purge Information
Date Pu rged:07—/ c- x /0 Start: Finish: G PurgeRate:_ i_q.
Purging Method: .\� Total Volume Purged:_ allon /mis/L)
Sampling Information
Date Collected:.' // Time Collected: 07 pm)
Sampling Equipment Used: �,rtill�✓ Instrument ID: Y514-1-t4
t,.1,e, l I
Bottle Type Preservation Analysis Required
T65 AC-
4-Ca a.,A ti-isa-J% N 4 5 03 C1 (z
L/II�rPbQ:� a-��sh.m 1i A)#4l
4Y {, j c kto�-46 IFn s /Nr �Qe s s�N� �-�-��
!Nt-sao,,p s�� k TD v�
Field Measurements/Observations
Sample Temp (oC): Time: 0 % 0 a Turbidity (ntu): Time:
Digs Oxy (rng/L): Time: Fe 2+ mg/L: Time:
Specific Cond. (uS): a3 5 Time: O . ©0 Res. Cl (mg/L)/(µg/L): Time:.
Sample pH (s.u.): Time: Odor: Aic Y1,P Time: a a
ReDox(m.V): Time: Appearance:. rIeav Time: 0g0f7
ReDox (EH value):YSI ProPlus +2001i1V Other: Time:
General/WeatherObservations: MY I—q_
cloudy/rainy) Temp.-'Q_(°F)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(°C)
Diss Oxy,
(mg/L)
Spec.
Cus)
pH (s u)
ReDox
(mV)
Turbidity
(ntu)
Volume
removed
�mis/
L
Water
level (ft)
Other
o4,3©
.--
.--
a
—
r-
Deco.�
_._
Page 41 of 45

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISI IN OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC27699-1617 ;Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge WQ0000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Wadesboro NC 28170 County Anson
❑ Lagoon ❑ Remediation: Infiltration Gallery
0 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #20
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#6
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Well Depth: 45 ft.
Well Diameter: 2 in.
pH 6.5 units Temp. 19.6 °C
DRY at
Depth to Water Level: 7.73 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 160.2 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling: 12.50 gallons
Appearance Clear
here: ElSamples
for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
N/D mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.22 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 127 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.3 units
Ba - Barium
mg/I
TOC 1.0 mg/I
Ca - Calcium
mg/I
Chloride 14.5 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 4.7 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/1
method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permihee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev. 1/2007
Aqent)

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfeld Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-6 Lab lD: 92488133005 Collected: 07/28/20 13:30 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/BMS
1
07/28/20 13:30
Collected Date
07/28/20
1
07/28/20 13:30
Collected Time
13:30
1
07/28/20 13:30
pH
6.5 Std. Units
1
07/28/20 13:30
Temperature
19.6 deg C
1
07/28/20 13:30
Static Water Level
7.73 feet
1
07/28/20 13:30
Specific Conductance
160.2 umhos/cm
1
07/28/20 13:30
Total Well Depth
45.04 feet
1
07/28/20 13:30
Odor
None
1
07/28/20 13:30
Appearance
Clear
1
07/28/20 13:30
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/28/20 17:15 07/29/20 15:58
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
127 mg/L 25.0
1
07/30/20 18:03
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.3 Std. Units 0.10
1
08/02/20 16:12
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
4.7 mg/L 1.0
1
07/29/20 23:51
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
08/04/20 11:32
7664-41-7
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
07/28/20 23:17
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.22 mg/L 0.050
1
07/29/20 20:36 07/30/20 19:29
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
14.5 mg/L 1.0
1
07/30/20 22:36
16887-00-6
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
Page 13 of 45

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92488133
Sample: MW-6 Lab ID: 92488133005 Collected: 07/28/20 13:30 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 08/01/20 13:19 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 45

Document Name: Field data Sheet
Date Issued: March 8, 2019
CeMnlyflcal `
Page: 1 of A
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality
Office .
l5
Name and Affiliation (Inspector): W k
Date: 7�a9-� By: ��'�'
Well Information
Well ID: V� lei.
Well Locked: YE / NO / Hushmount }
u
Well Diameter:
Construction: PV Steel/Stainless Steel)
/a
Total Well Depth: 7 C% ft
Multi Factor: P3 ('(Rad1us/12)1 z 3.14 x 7.48j
Static Water Level: ft
Casing Volume: _ �v 1 gallons n
Height of Water Column, 37.31 ft
Cal. 3 Volumes: 3 gallons
Pump Intake: ft
Purge Information
Date Purged: Start :_ l 56�o Finish:15:1.5 Purge Rate
Purging Method:
Total Volume Purged:
1,54 gallon /mis/L)
Sampling Information
Date Collected:. Q9 /A/ (Z Time Collected: r330
(am In
Sampling Equipment Used:
1
Ct N Instrument ID:
�)-}4 4
Bottle Type
Preservation
Analysis Required
3- q O rn L V-0 A
- PhDS R c.i �_
/�.0G
:Q coo
a - IDS
t (aSBzl
/1i%���/ T PlIZSS
=►Gb!42 ia9t„ L
AJO V ~ 'J
� �h �n ri c. So 14L &Jriyill
Field Measurements/Observations
P 4
Sample Temp (°C): IVP
Time: 13 3 Turbidity (ntu):
Time:
Digs Oxy (mg/L):
--,Time; "` Fe 2+ mg/L:
Time:
Specific Cond. (uS): [ 60 ,
Time:�3_Res. CI (mg/L)/(µg/L): —' Time:.
Sample pH (s.u.):
Time: 13 10. Odor: Amn0
Time: _ !
ReDox I—V}:
Time' A earance•
e.1Q4✓ TimeT3:wt�
PP
ReDox (EH value):YSI ProPlus +200riiV Other:
General/Weather Observations:. Yh W — (6
Sampler Signature
Stabilization Test
Time:
cloudy/rainy) Temp. Vn (°F) Wind 6hlr) (mph)
Time
Purged
Temp.
(C)
Digs Oxy,
(mg/L)
Spec.
C(US)
PH (s.u.)
ReDox
(mV)
Turbidity
(ntu)
Volume —
removed
allonS mis/
Water
level (ft)
Other
7 7
rSDun
Page 42 of 45

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT &NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��,
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
X❑ Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #19
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#7
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Well Depth: 52 ft.
Well Diameter: 2 in.
pH 7.2 units Temp. 19.6 °C
DRY at
Depth to Water Level: 19.43 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 557 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
12.0 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
.17 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
N/D mg/I
(NoteUse MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 333 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7.1 units
Ba - Barium
mg/I
TOC N/D mg/I
Ca - Calcium
mg/I
Chloride 33.6 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 20.4 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, N1­13as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Agent) Name and Title -Please print or type atu of a (or Authorized Agent)
GW-59 Rev. 1/2007

aceAnalytical
www.pacelob3.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92488133
Sample: MW-7 Lab ID: 92488133006 Collected: 07/28/20 13:00 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services -Charlotte
Collected By
JJQ/BMS
1
07/28/20 13:00
Collected Date
07/28/20
1
07/28/20 13:00
Collected Time
13:00
1
07/28/20 13:00
pH
7.2 Std. Units
1
07/28/20 13:00
Temperature
19.6 deg C
1
07/28/20 13:00
Static Water Level
19.43 feet
1
07/28/20 13:00
Specific Conductance
557 umhos/cm
1
07/28/20 13:00
Total Well Depth
53.43 feet
1
07/28/20 13:00
Odor
None
1
07/28/20 13:00
Appearance
Clear
1
07/28/20 13:00
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method: SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/28/20 17:15 07/29/20 15:58
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
333 mg/L 25.0
1
07/30/20 18:03
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
pH at 25 Degrees C
7.1 Std. Units 0.10
1
08/02/20 16:06
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
20.4 mg/L 1.0
1
07/30/20 00:36
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
08/04/2011:34
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.17 mg/L 0.040
1
07/28/20 23:18
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050
1
07/29/20 20:36 07/30/20 19:30
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
33.6 mg/L 1.0
1
07/30/20 22:37
16887-00-6
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 45

(�IaceAnalytical
www.paceiab3.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-7 Lab ID: 92488133006 Collected: 07/28/20 13:00 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 08/03/20 19:55 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 45

% Ce Document Name: Field data Sheet
96 bo £b 96ed rf QDocument Number
Client: g Field Data Sheet
Lccation., A
Name and AffiliationSaar Ier s
{ p () us`1'lj 8 fY1 ��P aye Field
Name and Affiliation (Inspector):
���Well Informatio
Well ID: W-
Well Diameter: of }(
Total Well Depth: �,j 7
ft
Static Water Level: ( 4 ft
Height of Water Colum23 n Q
Date Issued: March 8, 26i9
Pa e: 7 of
unters,,We Qua]
Office .
—Project #:
Data Sheet Review:
Date: 7'rg -ao
NO / Flushmount )
Construction: O'Vq/Steel/Stainless Steel)
Multi Factor*:_D r(Rad1us/12)2 x 3.14 x 7.481.
Casing Volume:
gallons.
Cal. 3 Volumes ;.
gallons
Well Locked:
By: BRCS
Pur a Irtformatl'o Pump Intake:
fr
Date Purged: C_1L /_.;,L7_/
�_ Start: Y-
Ap
PurgingPurge Rate:—r
Method: � � �
Total Volume Purged: 1a. 0
Sam Iin Informs ion J)rJga110 /mis/L)
Date Collected:
Time collect ed:h {arr
Sampling Equipment Used:
Instrument ID: Bottle Type
Preservatibn Analysis Required
CID
1 � U, �
Ph 0
Field Measurement Observations
Sample Temp (°C ; � 1' � � A-O
) �"Y``Time:— �-�� Turbidi n� �--
DW Oxy (mg/L): — tY { )' ---�_ Time:: _
--- �__ Time: Fe 2+ mg/L:
Sam
Specific Cond. (uS):�� Timec.��
Time:—LIC.Q— Res. Cl (m /L )'g )/(µg/>r
ple pH (s.u.): -F.)_ Time: — =Ttme:��
ReDox (mV): ®O Odor: ]Vk" Time: Time: 1 fib
"
ReDox (Ffl value):YSI ProPlus +200mV Appearance: —e ✓ Time:�i30,Q
General/Weather Observations: t Id-�" Other, Time:
-----
Sampler Signature:
sunny cloudy/y)
ram Temp._ ] (�F) Wind_rJ,, D(n#)
Stabilization Test
Date:
Time Temp, Diss Oxy,
Purged (°C) (mg/L)
Spec•
Cond.
o ume
pH (s•u.) ReDox Turbidity removed Water
�
(US)
(mV) (ntu) do /MIS/ level (ft) Other
a'1 �
ba
3 - —

SUBMIT FORM ON YELLOW PAPER ONLY
,
DEPARTMENT OF ENVIRONMENT&'NATURALRESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��1617
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 =Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
X1 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #16
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#8
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 6.8 units Temp. 19.1 °C
DRY at
Depth to Water Level: 4.54 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 717 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling: 12.75 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
N/D mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.092 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 447 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.9 units
Ba - Barium
mg/I
TOC N/D mg/I
Ca - Calcium
mg/I
Chloride 124 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 9.8 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/1
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007
Aqent)
`e

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-8 Lab ID: 92488133007 Collected: 07/28/20 12:40 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/BMS
1
07/28/20 12:40
Collected Date
07/28/20
1
07/28/20 12:40
Collected Time
12:40
1
07/28/20 12:40
pH
6.8 Std. Units
1
07/28/20 12:40
Temperature
19.1 deg C
1
07/28/20 12:40
Static Water Level
4.54 feet
1
07/28/20 12:40
Specific Conductance
717 umhos/cm
1
07/28/20 12:40
Total Well Depth
29.74 feet
1
07/28/20 12:40
Odor
None
1
07/28/20 12:40
Appearance
Clear
1
07/28/20 12:40
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/28/20 17:15 07/29/20 15:58
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
447 mg/L 25.0
1
07/30/20 18:03
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.9 Std. Units 0.10
1
08/02/20 15:55
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
9.8 mg/L 1.0
1
07/30/20 00:51
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
08/04/20 11:35
7664-41-7
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
07/28/20 23:19
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.092 mg/L 0.050
1
07/29/20 20:36 07/30/20 19:31
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
124 mg/L 10.0
10
07/30/20 22:39
16887-00-6
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
Page 17 of 45

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-8 Lab ID: 92488133007 Collected: 07/28/20 12:40 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon ND mg/L 1.0 1 08/03/20 20:45 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 45

i+�,Bk?lyf�esl1
Name: Field data Sheet
Date Issued: March 8, 2019
Page -Document
of
Document Number: F-CAR-FLD-001-rev.03
issuing Authority: Pace Huntersville Quality
Office
cation:
Name and Affiliation (Inspector): iti /�_
Well Information
Well ID: & w = Well Locked:
Well Diameter: 9-1 k
Total Well Depth: Z , 4q ft
Static Water Level: Y , Sy ft
Height of Water Column: -21%-� €t
N C Proiect #:
Date: -7- a9-ao
NO /
Construction:teel/Stainless Steel)
Multi Factor*: a.1/d3 [•(Radius/12)2 x 3.14 x 7.481
Casing Volume: `�� gallons
Cal. 3 Volumes:'_:gallons
Pump Intake: ft
By: QF'&
Purge Information
Date Purged;/ / _.:? Start : La2_!� Finish: Purge Rater
Purging Method: QA��-{.✓ Total Volume Purged: i �)-45- CaUon)smis/L)
Y py-
Sampling Information
Date Collected:._/A/ aU Time Collected:__ 0-40 (amo;jg,
Sampling Equipment Used: •N:_2�n 11 el✓ Instrument ID: —
Bottle Type Preservatia Analysis Required
N4as
1 a-S� 1-Fy�OU
I- i-wb�,x Pon4
Field Measurements/Observations
Sample Temp (IC): . Vt t Time: (D410 Turbidity (ntu):
. G
co qw
Time:
Dins Oxy (mg/L): Time: �'Fe 2+ mg/L: Time:
Specific Cond. uS : ( g/ }/(µg/)
p ( ) },._Time: b Res. CI m L L : —'"Time:.
Sample pH (s.u.): Ist Time: I)-q O Odor: NCNf- Time: 1-141)`
ReDox (mV): Time: Appearance:. C4Pflr Time: �4
ReDox (EH value):YSI ProPlus +200mV Other: Time:
GeneraVWeather Observations_ UV1 Wg
(st u yjcloudy/rainy) Temp._(°F) Wind SIoID (mph)
Sampler Signature
Stabilization Test
x
Time
Purged
Temp.
(°C)
Diss Oxy,
(mg/L)
Spec. Cond.ReDox
(US)
p H (s'u ')
(mV)
Turbidity
(ntu)
o ume
removed
(g o /mis/
Water
level (ft)
Other
1
�z.ZA�--
--
�•�
�—
.._
+ Lj
4
!
-^
I z
6�t
-•—
�-
Page 44 of 45

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
[VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
INNIM617
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please PnntClearlyorType
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
NPDES Other
Permit Name (if different):
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
❑>c Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #14
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#9
Date sample collected: 7/28/20
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 6.7 units Temp. 18.2 °C
DRY at
Depth to Water Level: 4.54 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 1778 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
9•75 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/28/20 - 08/04/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
.69 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100m1
Phosphorus: Total as P
.076 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 914 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.9 units
Ba - Barium
mg/I
TOC N/D mg/I
Ca - Calcium
mg/I
Chloride 418 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 26.5 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen. NH,as N: Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev. 1/2007
(or Authorized Aqent)

aceAnalytical
www.pacelabs.com
I
Project: Sprayfietd Wells
Pace Project No.: 92488133
Sample: MW-9
Parameters
Monitoring Well Data
Collected By
Collected Date
Collected Time
pH
Temperature
Static Water Level
Specific Conductance
Total Well Depth
Odor
Appearance
MBIO 9222D Fecal Coliform CHT
Fecal Coliforms
2540C Total Dissolved Solids
Total Dissolved Solids
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
365.1 Phosphorus, Total
Phosphorus
4500 Chloride
Chloride
Date: 08/05/2020 04:25 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92488133008 Collected: 07/28/20 12:00 Received: 07/28/20 15:35 Matrix: Water
Results Units Report Limit
DF
Prepared Analyzed
CAS No.
Analytical Method:
Pace Analytical Services - Charlotte
JJQ/BMS
1
07/28/20 12:00
07/28/20
1
07/28/20 12:00
12:00
1
07/28/20 12:00
6.7 Std. Units
1
07/28/20 12:00
18.2 deg C
1
07/28/20 12:00
10.50 feet
1
07/28/20 12:00
1778 umhos/cm
1
07/28/20 12:00
29.37 feet
1
07/28/20 12:00
None
1
07/28/20 12:00
Clear
1
07/28/20 12:00
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
ND CFU/100 mL 1.0
1
07/28/20 17:15 07/29/20 15:58
Analytical Method: SM 254OC-2011
Pace Analytical Services - Asheville
914 mg/L 50.0
1
07/30/2018:03
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
6.9 Std. Units 0.10
1
08/02/20 15:49
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
26.5 mg/L 1.0
1
07/30/20 01:05
14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.10
1
08/04/2011:37
7664-41-7
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
0.69 mg/L 0.040
1
07/28/20 23:20
14797-55-8
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
0.076 mg/L 0.050
1
07/29/20 20:36 07/30/20 19:32
7723-14-0
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
418 mg/L 20.0
20
07/30/20 22:40
16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qual
MW
H3
Page 19 of 45

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92488133
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-9 Lab ID: 92488133008 Collected: 07/28/20 12:00 Received: 07/28/20 15:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon ND mg/L 1.0 1 08/03/20 21:07 7440-44-0
Date: 08/05/2020 04:25 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 45

aceAnalylieal"
Document Name: Field data Sheet
Date Issued: March 8, 2019
Page: 1 of
Document Number: F-CAR-FLD-001-rev.03
Issuing Authority: Pace Huntersville Quality
Office .
;-
P
Name and Affiliation (Inspector):
'V 1A,
Well Information
Date:?"o? q �O
Well ID: -'_
Well Locked: Y / NO / Flushmount )
Well Diameter: !"`�
Construction:V /SteeI/Stainless Steel)
. (P
Total Well Depth: 62,31: ft
Multi Factor*: 0•1103 r(Radius/12)2x3.14x7.481
Static Water Level: �.0 SC�O�
Casing Volume: 3 ' gallons
eft
Height of Water Column:
Cal. 3 Volumes: '-5_ gallons
Pump Intake: `" It
W -2 l
By: BP G
Purge Information
Date Purged 07- / � / a'� Start:
l� Finish: 160b Purge Rate:
Purging Method: 1��'�
Total Volume Purged: �•� gallon /mis/L)
Sampling Information
Date Collected:�/aqj �Lp
Time Collected:._ f _ROD (am m
.--�
Sampling Equipment Used: dJ� t��� Instrument ID;_ � ''� 1744
Bottle Type
Preservation Analysis Required
C,
;�-5Utnti0
AI«�Q ccc colt 2m
a ' i
4+:2 $04 iJ (� ' 'rjt�1YI OS
I~ Or..Q. 1-35U �fi►,Sl
#—
N-0AlE `�) Cc,�[ori14 Sk,f,-,tL11f11iYalR
Field Measurements/Observations
p i{ L&i3
Sample Temp (°C): Time:
)�© Turbidity (ntu): Time:
Dins Oxy (mg/L): Time:
—' Fe 2+ mg/L: Time:
Specific Cond. (uS): t Time:
lADO Res. Cl (mg/L)/(µg/L). Time:.
Sample pH (s. u.): (0,1- Time:
( a 00 Odor: Time; 1200
ReDox (m.V): Time:
Appearance: Time:�(Z
ReDox (EH value):YSI ProPlus +200mV
Other: ^'^ Time: *--+
General/Weather Observations: M W -
(sunnt /cloudy/rainy) Temp._?jZ(°F) Wind -1m) (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(°C)
Diss Oxy.
(mg/L)
Spec.
(US)Cond
(US)
pH (s.u.)
ReDox
(mv)
Turbidity
(ntn)
Volume
removed
o/R►ls/
Water
level (ft)
Other
.-.,
Page 45 of 45

r rw.ncruu.C"
I
Section
Section B
Required
Clent Monnation: Required Project Wormatfon•
Company
Valley Proteins
Report To: Jarres Hodges
Address:
656 Lrr,le, Duncan Road
Copy To:
Wadesba
o, NC 28170
Email:
j iodges@valleyproteins.00m
Purchase Order#:
Phone.
704-7184912 Fax
Protect Name: SprayWd Wefls
Requeste
I Due Date
project C.
WIMIX CO(
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COL
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CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately
Section C
Invoice Information:
Pf
Attention:
Company Name:
Address:
Pace Quote:-
Pace Project Manager tyriek.hook [e-mail].
k
Pace Profile #: 5703b
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END
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IPRINT Name of SAMPLER: i� III I Pfr
DATE Signed:
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1— cmaY BUY in � �'

GW-59A COMPLIANCE REPORT FORM Permit #
(Submit one each monitoring period wth GW_59 forms.)
W00000957
1
Enter date monitoring results were due. ( 8/30/2020 ) Will this monitoring report (GW-59 and GW-59A)
YES
®O
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
O
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc. 7f the answer is "YES", contact to Regional Office for guidance
4
Are any monitoring constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES'list the affected wells individually with constituents(s) and concentration(s)
exceeding standards in the space provided below:
MW# 1, 2, 3, 5, and 9 exceed ground water standards for Total Dissolved Solids.
MW# 1, 2, 3, 5, and 9 exceed for chlorides.
MW#1 and 2 exceeds for nitrate.
5
For the same constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituents s in the same wells s in the last two ears?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES"Dist in the space provided below, each well with constituent(s) exceeding
standards, concentrations) reported, and sample collection date for each occurrence (for the last two years).
See Report enclosed.
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occuring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO'Icontact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permitteee to a Notice of Violation
fines, and/or penalties.
Piezometers were placed in the irrigation fields to determine water quality .
Total Dissolved Solids and Chlorides are naturally high In this area.
Sprinkler heads were purposely capped off near monitoring well #1 as instructed by Jim Barber (Regional Engineer)
to see if the nitrate level will change in the well.
8
The Person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the Information submitted In this
report (Compliance Report GW-69A) is true and complete to the best of my knowledge.
C
re of ittee (or Authorized Agent) 4ate
G W-59 12/8/2003