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HomeMy WebLinkAboutWQ0031314_Application_20200910tWoInslon-Salern / Forsyth County tl l hies Water • Wastewater • Solid Waste Administration, P.O. Box 2511, Winston-Salem, NC 27102 O: 336-727-8000, F: 336-727-8432, cityofws.or [i es July 24, 2020 Mr. Nathaniel Thornburg �� ��� North Carolina Department of Environmental Quality 17 Aquifer Protection Unit — Land Application Unit 1617 Mail Service Center 0111-tDischar9 Raleigh, NC 27699-1617 Pennitting Unit Dear Mr. Thornburg, The City of Winston-Salem owns and operates three water treatment facilities in Forsyth County; the P.W. Swann, R.W. Neilson and R.A. Thomas Water Treatment Plants. The Swann Plant currently has a Class A Distribution Permit (WQ0031314) for the residuals produced. In 2012, the city added the Neilson and Thomas WTP's as additional generating facilities under the Swann WTP's permit. We are requesting a renewal of permit WQ0031314 with one exception of a major modification increasing the R.W. Neilson's generating limit to 2,500 dry tons. This request is due to NOD-2020-PC-3075 where the Neilson WTP exceeded its current limit of 1,499 dry tons per year (see attached letter from Lon T. Snider dated July 7, 2020 and Bill Brewer's response dated July 13, 2020). By increasing the permitted dry tonnage for Neilson, we should eliminate future exceedances if we are unable to haul of-e year due to rainfall or other issues. Below is a summary of the documents included in this renewal application package. P.W. Swann Water Treatment Plant • Application Fee in the amount of $395.00 for a Major Modification being requested increasing the quantity of the R.W. Neilson's generating limit to 2,500 dry tons per year • Completed form DCAR 08-11 indicating this request as a renewal of our existing distribution permit WQ0031314 which includes the following: ✓ A copy of documentation of NOD-2020-PC-0375 as justification for our Major Permit Modification Request for the Neilson WTP generating facility ✓ A copy of the P.W. Swann's current distribution permit WQ0031314 ✓ Scope of work from our bid documents showing how our contracts for residuals land application are structured. Material from all plants are hauled in bulk Completed form RSC 11-13 which includes the following: ✓ Completed Form RSC 11-13 ✓ Map of plant site and adjacent fields proposed for application when available ✓ Process diagram (waste facilities highlighted in green) ✓ Black & Veatch's design criteria estimated residuals quantitative production rates ✓ P.W. Swann's Solids Handling Plan ✓ TCLP and corrosivity sample results dated April 8, 2016 ✓ Nutrient metal results from our most recent sampling events from samples collected September 17, 2019 and November 25, 2019 City Council: Mayor Allen Joines; Denise D. Adams, Mayor Pro Tempore, North Ward; Dan Besse, Southwest Ward; Robert C. Clark, West Ward; John C. Larson, South Ward; Jeff Macintosh, Northwest Ward; Morticia'Tee-Tee" Parmon, Northeast Ward; Annette Scippio, East Ward; James Taylor, Jr., Southeast Ward; City Manager: Lee D. Garrity County Commissioners: David R. Plyler, Chair; Don Martin, Vice Chair; Fleming El -Amin; Ted Kaplan; Richard V. Linville; Tonya McDaniel; Gloria D. Whisenhunt; Call 311 or 336-727-8000 County Manager: Dudley Watts,Jr. Winston-salem/Forsyth County Utility Commission: Randall S. Tuttle, Chair; L. Wesley Curtis, Jr., Vice Chair; Harold E. Day; Tom Griffin; Yvonne H. Hines; citylink@cityofws.org Duane Long; Hugh W. Jernigan; Chris Parker; Donald R. Stewart; Allan Younger ✓ Fecal coliform data dated April 8, 2016 The P.W. Swann WTP has acreage adjacent to the residuals lagoons available for land application. In addition to this area, the City of Winston-Salem has been working with local area farmers to place residuals on pastureland as the need arises. W. Neilson Water Treatment Plant Completed form RSC 11-13 which includes the following: ✓ Form RSC 11-13 ✓ Map of plant site (field for land application varies based on contractor) ✓ Process diagram (waste facilities highlighted in green) ✓ Black & Veatch's design criteria estimated residuals quantitative production rates ✓ R.W. Neilson's Solids Handling Plan ✓ TCLP and corrosivity sample results dated March 1, 2016 ✓ Nutrient metal results from our most recent sampling events from samples collected April 25, 2019 and September 11, 2019 ✓ Fecal coliform data dated March 1, 2016 The R.W. Neilson WTP's land application sites vary based on the current contractor. Contracts are awarded to the lowest responsive responsible bidder. Our contracts are structured that each contractor is responsible for finding additional land to apply the material as per our permit conditions. R.A. Thomas Water Treatment Plant • Completed form RSC 11-13 which includes the following: ✓ Form RSC 11-13 ✓ Map of plant site ✓ Process diagram (waste facilities highlighted in green) ✓ Black & Veatch's design criteria estimated residuals quantitative production rates ✓ R.A. Thomas's Solids Handling Plan ✓ TCLP and corrosivity sample results dated April 26, 2016 ✓ Nutrient metal results from our most recent land application samples collected August 30, 2017 ✓ Fecal coliform data dated April 26, 2016 In 2018, residuals generated at the R.A. Thomas WTP were hauled to the Hanes Mill Road Landfill. located at 325 W. Hanes Mill Road, Winston-Salem 27105 and plans are to continue this practice until further notice. Once reviewed, should you have any questions regarding this application, please contact Bill Brewer at (336) 397-7727. Sincerely, Courtne L. river, P.E. Utilities Director ROY COOPER Governor MICHAEL S. REGAN Secretary S. DANIEL SMITH Director NORTH CAROLINA Environmental Quality July 7, 2020 Mr. Bill Brewer Winston-Salem/Forsyth County Utilities Commission Post Office Box 2511 Winston-Salem, North Carolina 27102 SUBJECT: Notice of Deficiency (NOD-2020-PC-0375) 2019 Annual Report Review Swann WTP, Neilson WTP, and Thomas WTP Distribution of Class A Water Treatment Plant Residuals Permit No. WQ0031314 Forsyth County Dear Mr. Brewer: The Division of Water Resources (DWR) acknowledges receipt of your 2019 Annual Report for the subject permit. A review of this report was conducted by DWR staff person Jim Gonsiewski. The following deficiency was noted from the review: Attachment A of the Permit states that the yearly maximum dry tons to be distributed annually from the Neilson WTP is 1,499 dry tons. A total of 2,334.69 dry tons from the Neilson WTP were distributed in 2019. This is an exceedance of 835.69 dry tons for the year. Please provide a response to this letter within 30 days of receipt by your office indicating the corrective actions taken to address this deficiency. If you anticipate this condition occurring again, this office recommends that you apply for a permit modification to increase the permit limit. If this exceedance occurs again without a permit modification, a Notice of Violation may be issued. If you or your staff have any questions concerning this letter, please contact me or Jim Gonsiewski at (336) 776-9800 or via email at jim.,-,onsiewski_�i_ncdenr.gov. Sincerely, ED—Signed by: LoriT.T*Alier Regional Supervisor Water Quality Regional Operations Section Division of Water Resources, NCDEQ — WSRO cc: Forsyth County Environmental Health (Electronic Copy) Courtney Driver — City of Winston-Salem (Electronic Copy) WSRO Electronic Files Laserfiche Files North Carolina Department of Environmental Quality Division of Water Resources Winston-Salem Regional Office V 450 West Hanes Mill Road. Suite 3001 Winston-Salem, North Carolina 27105 "� 336.776.9800 .Winston-Salem / Forsyth County ! J : ti f It1e5 Water • Wastewater • Solid Waste P.W. Swann Water Treatment Plant, 2800 River Ridge Road, Pfafftown, NC 27040 0: 336-727-8000, F: 336-946-2574, wsfcutilities.org July 13, 2020 Mr. Lon T. Snider —Regional Supervisor NC DEQ- Water Quality regional Operations Section 450 West Hanes Mill Road Suite 350 Winston-Salem, NC 27105 Subject: Notice of Deficiency (NOD-2020-PC-3075) 2019 Annual Permit Review Swann WTP, Neilson WTP and Thomas WTP Distribution of Class A Water Treatment Plant Residuals Permit No. WQ0031314 Forsyth County Dear Mr. Snider, This letter is in response to your Notice of Deficiency (NOD-2020-PC-3075) letter dated July 7, 2020 regarding an exceeciance of the Neilson WTP's permit distribution limit of 1,499 dry tons of residuals. This hauling event represents residuals generated over a 34-month period for an average annual production rate of 824 dry tons per year ([2,334.69 DT's _ 34 months] X 12 Months). Lagoon #2 was in service from January 2016 until April 2017 and lagoon #3 was in service from April 2017 until October 2018. Under normal circumstances at the Neilson Plant, one lagoon is clean and ready for service, one lagoon is drying and one lagoon is in service. During the 2015 and 2017 calendar years, the Neilson WTP did not distribute any residuals, which created a "backlog" that was caught up in 2019 by hauling more than one lagoon. The residuals hauled in calendar year 2019 eliminated any backlog and we have returned to our normal schedule. In addition we will be applying for a major modification to our permit for the Neilson WTP requesting a generating limit of 2,500 dry tons to eliminate this from being an issue should we be presented with the same situation in the future. Our existing permit expires in February 2021 and I am currently preparing the renewal application. If you have any questions regarding this matter, please contact me at 336-397-7727. Sincerely, William C. Brewer Water Treatment Superintendent City Council: Mayor Allen Joines; Den Ise D. Adams, Mayor Pro Tempore, North Ward; Dan Besse, Southwest Ward; Robert C. Clark, West Ward; John C. Larson, South Ward; Jeff Maclntosh, Northwest Ward; Morticia "Tee -Tee" Parmon, Northeast Ward; Annette Scippio, East Ward; James Taylor, Jr., Southeast Ward; City Manager: Lee D. Garrity County Commissioners: David R. Plyler, Chair; Don Martin, Vice Chair; Fleming El -Amin; Ted Kaplan; Richard V. Linville; Tonya McDaniel; Gloria D. Whisenhunt; Call 311 or 336-727-8000 County Manager: Dudley Watts, Jr. Winston-Salem/Forsyth County Utility Commission: Randall S. Tuttle, Chair; L. Wesley Curtis, Jr., Vice Chair; Harold E. Day; Tom Griffin; Yvonne H. Hines; citylink@cityofws.org Duane Long; Hugh W. Jernigan; Chris Parker; James Ruffin; Donald R. Stewart; Allan Younger State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Ai)vlicant shall submit one original and two conies of the application and sunportino_ documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permittin Unit website General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ❑ Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ The project name should be consistent on the plans, specifications, etc. ❑ The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106( h i. An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). [✓]/If this project is for a modification of an existing permit, submit one copy of the existing permit. [✓Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification I Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395 Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245 1 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ❑ List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Pagel of 3 D. Pro ram Information (All Application Packages) Provide a narrative explaining the following: 9w the materials will be handled and transported from where the residuals were produced to where it will be treated. w the residuals will be processed/treated (attach process flow diagram). 9 [W ow leachate collection will be handled. Where the residuals will be stored until processed. Vthe final product will be distributed (packaging, bulk, etc.) t nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. 2 ach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. Prttovide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following info ation: [me and address of the person who prepared the residual that is sold or given away. L'7 A statement that application of the residuals to the land shall be in accordance with the instructions on the label or Wi formation sheet. rstatement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored 3911duals into any surface waters. VA ormation on all applicable setbacks in accordance with 15A NCAC 02T .1�b.. tatement that the residuals shall be applied at agronomic or recommended rates for intended uses. - v�:esrr_sre:�srr - - .. - - ., - ' - - .. • - _ •IL :1i7 - .. vac�w INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Op e ation and Maintenance Plan (New and Renewal Application Packages) For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. FZK,qS,ubmit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: 511"Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. �aintenance schedules; may include equipments calibration, maintenance of signs, etc. [/Safety measures; may include safety training program, manuals, signs, etc. pill response plan; including control, containment, remediation, emergency contact information, etc. [Inspection plan including the following information; /[]Fames and titles of personnel responsible for conducting the inspections. requency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected [cation(s) and inspection frequency are representative of the residuals management program. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event hat noncompliance is observed. ampling and monitoring plan including the following information; ames and titles of personnel responsible for conducting the sampling and monitoring. Vj�)etailed description of monitoring procedures including parameters to be monitored. frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 1. APPLICANT INFORMATION: 1. Applicant's name: Winston-Salem/Forsyth County Utilities Commission Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership Privately -Owned Public Utility ❑ Federal 0 State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Courtney L. Driver Title: Utilities Director Applicant's mailing address: 101 N. Main Street City: Winston-Salem State: NC Zip: 27101- Telephone number: (336) 727-8000 Email Address: courtneyd(&cityofws.org 2. Consultant's name: Jeff Coggins License Number (for P.E.): NC - 20626 Affiliation: N On Staff ® Retained (Firm: Black & Veatch -Charlotte Office) Consultant's mailing address: 10715 David Taylor Drive, Suite 240 City: Charlotte State: NC Zip: 28262- Telephone number: (704) 510-8415 Email Address: cogginsjdkbv.com 3. Fee submitted: $0.00 — None required for Permit Renewal (See Instruction B) IL PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ® modified, 0 renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00031314 Date of most -recently issued permit: March 1, 2016 Date of most -recently certified Attachment A (if different than the permit): March 28, 2016 III. FACILITY INFORMATION: 1. Name of residuals processing facility: P.W. Swann Water Treatment Plant City: Pfafftown State: NC Zip: 27040-U Coordinates: Latitude: N36° 8' 51.5" Longitude: W80° 25' 14" Datum: DMS Level of accuracy: 100% Method of measurement: Survey County where facility is located: Fors h 2. Facility contact (person familiar with residuals preparation): Name: Bill Brewer Title: Water Treatment Superintendent Mailing address: 2800 River Ridge Road City: Pfafftown State: NC Telephone number: (336) 397-7727 Zip: 27040-8435 E-mail address: billbacityofws.org FORM: DCAR 06-16 Page 1 of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: Until distributed. Please refer to Operation and Maintenance Plan for Swann, Neilson and Thomas WTP's for information on how residuals will be processed at each facility. days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); Please refer to Operation and Maintenance Plans submitted with this application for how residuals will be distributed or managed b, each water treatment facility. Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added er 1.0 dry ton of residuals ton) Not a licable Not applicable 3. Approximate amounts of the residuals received and processed at the facility: Swann WTP — 750, Neilson -1.499 and Thomas — 750 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 2,999 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Please refer to the Operation and Maintenance Plans submitted for how each facility will store and handle residuals produced. 6. Does the facility have a stormwater management plan? ❑ Yes; ❑ No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: When necessan: silt fence and/or earthen berms will be used to prevent storm water runoff from entering surface waters as per the Operation and Maintenance Plans. V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. -- i RSC 06-16.doc FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Cer-tifleation! (Appheation invelying New or- Changes to Treatment or- Storage Units) Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes ❑ No, Explain; I, ,Courtney L. Driver Winston-Salem/Forsylh Counly Utilities Director (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for WO031314 P.W. P.W. Swann WTP. R.W. Neilson WTP and R.A. Thomas WTP (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. 0I Signature: Date: &4, FORM: DCAR 06-16 Page 3 of 3 Water Resources ENVIRONMENTAL QUALITY PAT MCCRORY {iamneir DONALD R. VAN DER VAART Secrem y S. 'JAY ZIMMERMAN Direciar February 9, 2016 ROT] I.IARGRovE — DIRECTOR or. UTILITIES WINsTON-SALEWFORsyni COUNTY UTILiTMS COMMISSION POST OFFICE Box 2511 WINsTON-SALEM, NORTIi CAROLINA 27102 Dear Mr. Hargrove: Subject: Permit No. WQ0031314 P. W. Swann WTP Distribution of Class A Water Treatment Plant Residuals Forsyth County In accordance with your permit renewal request received December 2, 2015, we are forwarding herewith Permit No. WQ00313I4 dated February 9, 2016, to Winston-Salem/Forsyth County Utilities Commission for the continued operation of the subject residuals management program. Please'note that this renewed permit shall become effective on March 1, 2016 (i.e. the day after the expiration date of the existing permit). This permit shall be effective from March 1, 2016, until February 28, 2021, shall void Permit No. WQ0031314 issued November 30, 2012, and shall be subjeetto the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachment A for they may differ from the previous pexmit issuance. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. Please note the following permit conditions are new since the last permit issuance dated November 30, 2012: ➢ Condition 111.9. — There are new provisions for the utilization agreement compared to Old Condition I1I.9., e.g., can be dissolved at request of those receiving residuals or sale of land; the length of agreement is up to parties concerned, Read carefully. D Condition II1.13. — Similar to Old Condition III.13., but now if the Permittee knows that those receiving residuals are over -applying, the Permittee shall report this to the Winston-Salem Regional Office. There was a request to remove Condition III.B.h, from the Perinit, i.e., the soil pH requirement. The laboratory results showed that the pH of the residuals to be applied was less than 6.5. Because the pH is this low, Condition 111.81, remains in the permit even though it is water treatment plant residual being applied. State ofNortli Carolina lEnvkomaontal Quality Wator Resoorces i water Quality Permitting l ] Ion-DIScharge Aennitting 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919 807 54& Mr. Ron Hargrove February 9, 2016 Page 2 of 2 If any pants, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes; and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need additional information concerning this permit, please contact Troy Doby at (919) 807- 6336 or troy.doby@ncdenr.gov Sincerely, / �Jay Zimmerman, P. G., Direct O Division of Water Resources cc, Forsyth County Health Department (Electronic Copy) Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy) Beth Buffington -- Protection and Enforcement Branch (Electronic Copy) Digital Permit Archive (Electronic Copy) Central Piles NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENTAL QUALITY RALEIGH DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Winston-Salem/Forsyth County Utilities Commission Forsyth County FOR THE continued operation of a residuals management program for Whiston-Salem/Forsyth County Utilities Commission and consisting of distribution of CIass A Water Treatment Plant residuals generated by the approved facilities listed in Attachment A with no discharge of wastes to suuface waters, pursuant to the application received December 2, 2015, and in conformity with other supporting data subsequently tiled and approved by the Department of Environmental Quality and considered a past of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Pail 257. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from March 1, 2016, until February 28, 2021, shall void Permit No, WQ0031314 issued November 30, 2012, and shall be subject to the following specified conditions and limitations: 1. ti CHEDULES 1. No later than six months prior to the expiration of this permit, the Pennittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. [15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109) H. PERFORMANCE STANDARDS 1. The subject residuals management program shall be effectivelymaintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease distribution of residuals, contact the Winston-Salem Regional Office supervisor, and take any immediate corrective actions. [G.S. 143-215.11 WQ0031314 Version 2.0 Shell Version 151201 Pagel of I I 2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [15A NCAC 02B .0200, 02L -.0100] 3. only residuals generated by the facilities listed in Attachment A are approved for distribution in accordance with this permit. [G.S. 143-215.11 4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis): Parameter Ceiling Concentration (ndiligrams per kilogram) Monthly Average Concentration (ni ligrams per kilogram) - Arsenic _l 75 - - - —41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 n/a - Nickel 420 420 Selenium 100 100 i Zinc 7,500 2,800 [15A NCAC 02T .11051 5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [I 5A NCAC 02T .1106] 6. Setbacks for treatment and storage facilities shall be as follows: Setback Description Setback _ (feet_ Habitable residence or place of public assembly under separate ownership or not 100 to be maintained as part of the project site Property lines 50 Private or public water supply 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and 50 wetlands) Wells with exception to monitoring wells 100 All treatment and storage facilities were originally permitted prior to September 1, 2006 [15A NCAC 02T .1108] WQ0031314 Version 2.0 Shell Version 151201 Page 2 of 11 7. Setbacks for Class Aland applied built residuals shall be as follows: Setback by residual type Setback Description (feet) Liquid Cake* Private or public water supply 100 100 Surface waters (streams — intermittent and perennial, 100 25 perennial waterbodies and wetlands)_ Surface water diversions (ephemeral streams, 0 waterways, ditches)25 Groundwater lowering ditches (where the bottom of 25 0 the ditch intersects the SRWT) Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15% solids by weight and can be stacked without flowing, as well as can be handled, transported and spread as a solid (e.g., using a backhoe, front end loader, clinger spreader, broadcast spreader or other equipment designed for handling solid materials) without leaving any significant liquid fraction behind, [15A NCAC 02T ,1108] 8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (http-//nutrients.soil.nesu.edu/yields/index.Ilip). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.6. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 (htt3�://www.ncggr.aov/SWC/tech/documents/9tb Guidance Doc 100109.>.4f). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards (Ltl; i.,-fe.so.errov.usda.-Lov/NH:.)/i.)ractice-standards/standards/590.p a.. d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action, [I SA NCAC 02T .1109(b)(1)(k)] WQ0031314 Version 2.0 Shell Version 151201 Page 3 of 11 The Permittee shall not distribute Class A Water Treatment Plant residuals that have a sodium adsorption ratio (SAR) of I0 or higher without prior written Division approval. The Permittee may seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high SAR content; has agreed on proper residual application rates; and has agreed to- operational considerations to ensure that the high SAR content will not adversely impact the receiving sites. Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site integrity and conditions conducive to crop growth, ran be obtained from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist. [ISANCAC 02T .0108(b)(1)] III. OPERATION AND MAINTENANCE RE, QU REMENTS 1. The residuals management program shall be properly maintained and operated at all times. The program shall be effectively mauitained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. [ 15A NCAC 02T .1110] 2. The Permittee shall maintain. an approved Operation and Maintenance Plan (O&M Plan) Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a. Operational functions; b. Maintenance schedules; e. Safety measures; d. Spill response plan; e. Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f. Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; I Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The safnpling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling fiequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). [15A NCAC 02T A 1001 WQ0031314 Version 2.0 Shell Version 151201 Page 4 of i l 3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification ofthe facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 080. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition III. 2), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Protection and Enforcement ' Branch at (919) 707-9105. [15A NCAC 02T .0117] 4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. [15A NCAC 02T .0108(b)(1)] 5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained In all residuals transport and application vehicles. [15A NCAC 02T .1110] 6, When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. [G.S. 143-215.1] 7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. [15A NCAC 02T .1109(b)(1)] 8. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulkresiduals or the application causes the contravention of surface water or groundwater standards; d. Ifthe land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur, e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than IS% for injected or incorporated bulk liquid residuals; It. If the soil pH is not maintained at 6.0 or greater, unless Sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist'provides information indicating that the pH ofthe soil, residuals and Tune mixture is suitable for the specified crop, Any approved variations to the acceptable soil pH (6.0) will be noted in this permit; i. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a tJSDA no -till program shall be exempted from meeting this vegetative cover requirement; j. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; k. If the vertical separation of bedrock and the depth of residuals application is less than one foot, WQ0031314 Version 2.0 Shell Version 151201 Page 5 of 11 1. Application exceeds agronomic rates. [15A NCAC 02T ,11091 9, A Utilization Agreement between the Permittee, his subcontractor distributing and applying the residuals, and the entity agreeing to accept Class A bulk residuals shall be in place prior to distribution of the bulk residuals. The agreement shall specify the subcontractors and the agreeing entity's responsibilities. The Permittee, the subcontractor, and the entity accepting the Class A bulk residuals shall sign the Utilization Agreement, The Utilization Agreement shall have a clause allowing the recipient of the residuals to end the Utilization Agreement at any time by notifying the Permittee in writing. If the recipient of the residuals sells the property, the Utilization Agreement shall automatically terminate. If the permit is rescinded, the Utilization Agreement shall automatically terminate. The duration of the Utilization Agreement shall be one to which the Permittee, the subcontractor, and the recipient of the residuals agree. Any changes in the agreement that are necessitated by changes in the permit shall be mailed to the subcontractor and the recipient of the residuals by certified mail with return receipt. The Permittee shall keep these records on file for inspection by the Division for each Utilization Agreement while that Utilization Agreement is in force. 115A NCAC 02T .0108(b)(1), 02T .1104j 10. At a minimum, the Utilization Agreement shall stipulate the following; a. By agreeing to accept the bulk Class A residuals, it is recognized that the application of these residuals is allowed under the conditions of this agreement including the prohibitions contained in Condition 111.8. Land application of Class A residuals is considered the beneficial reuse of a waste under 15A NCAC 02T .1100, and has been deemed permitted under 15A NCAC 02T .1103(4) provided the conditions of this agreement are met. Any action resulting in damages to surface water or groundwater, caused by failure to follow the conditions of this agreement, is subject to Division enforcement action; b, Application of Class A residuals shall meet the following application requirements: i. Residuals shall not be stockpiled for more than 60 days (after the delivery of the last load) unless the permittee notifies the Winston-Salem Regional Office and receives approval to exceed the 60 day limit. At a minimum, the information provided shall be, the location, the date that the last load was delivered, the quantity of residuals stockpiled, the percent solids of the residuals stockpiled, measures taken to prevent stockpile runoff (e.g. placement, perimeter berms, etc.) and the anticipated date the residuals will be spread. ii. Application of bulk residuals shall not occur within 100 feet of a public or private water supply source; iii. Application of bulk residuals shall not occur within 100 feet of any well, with the exception of Division approved monitoring wells; iv. Application of bulk residuals shall not occur within 25 feet of surface waters. c. The generator of the Class A bulk residuals shall provide information on the proper use of the residuals, including information on the recommended application rates. d. The applicator or party accepting bulk residuals from the Permittee shall supply all third parties receiving bulk residuals with documentation specifying that application shall occur consistent with the utilization agreement, e. Instructions, including contact information for key personnel, shall be provided to the applicator or party receiving bulk residuals in the event that any requirements specified in the utilization agreement are not met. f, A copy of the Utilization Agreement shall be maintained at the land application sites when bulk residuals are being applied. [15A NCAC 02T .0108(b)(1), 02T .11041 WQ0031314 Version 2.0 Shell Version I51201 Page 6 of 11 I I . All residuals shall be adequately stored to prevent untreated leaohate runoff. The finished product may be placed on a concrete pad, placed under shelter or physically covered until it is distributed to the buyer. If an alternate storage site is used, approval must be obtained from the Division. [15A NCAC 02T .0108(b)(1)] 12. A label shall be affixed to the bag or other container in which residuals are sold or given away for land application, or an information sheet shall be provided to the person who receives Class A residuals. At a minimum, the label or information sheet shall contain the following: a, The name and address of the person who prepared the residuals; b, A statement that residual land application is prohibited except in accordance with the instructions on the label or information sheet, c. A statement identifying that this material shall be prevented from entering any public or private water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.); d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its intended use. [I5ANCAC 02T .I 109(a)] 13. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement. The Permittee shall report to the Winston-Salem Regional Office as per repotting conditions under Condition IV.8. any person or entity known to be applying residuals contrary to the condition of the signed Utilization Agreement. [I5A NCAC 02T .1103(a)] WQ0031314 Version 2.0 Shell Version 151201 Page 7 of 11 IV. MONITORING AND REPORTING RC UMMENTS 1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)] 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be used or disposed under this permit. The analyses [eorrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Diehlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Diehloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Tetrachloroethylene (0.7) Chlordane (0.03) Chlorobenzene (100.0) Hexachlorobenzene (0.13) Heptachlor (and its hydroxide) OA08 Toxaphene (0.5) Triohloroethylene (0.5) Chloroform (6.0) Chromium (5.0) IIexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) 2,4,5-Trichlorophanol (400.0) m-Cresol (200.0) o-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2) p-Cresol (200.0) Mercury (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200A) [15A NCAC 13A A 102(b), 02T .1101, 02T .11051 3. An analysis shall be conducted on residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Molybdenum Potassium Ammonia -Nitrogen Selenium Sodium Arsenic Nickel Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) _ Percent Total Solids pH TKN Calcium Copper Zinc Lead Phosphorus Plant Available Nitrogen Magnesium (by calculation) WQ0031314 Version 2.0 Shell Version 151201 Page 8 of 11 [ 15A NCAC 02T .1101 ] 4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .1111(c)] 5. Laboratory parameter analyses shall be petforined on the residuals as they are distributed, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .0505] 6. The Permittee shall maintain records tracking all bulk residual distribution or land application events performed by the Permittee. At a minimum, these records shall include the following: a. Source of residuals; b. Date of distribution/land application; c. Name and address of recipient of residuals; , d. Volume of residuals distributed to each recipient; e,. Intended use of residuals; f. If land application events performed by the Permittee -Nitrogen Application Rate based on RYES (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years). [15A NCAC 02T .0109(a)] 7. Three copies of an annual report shall be submitted on or before March 11t. The annual report shall meet the requirements described in the Instructions for Residuals AV lication AnnualRtorting Forms. Instructions for reporting and - annual report forms are available at http;l/portal.ncdenr.oralweb/wy/atas/lau/reporting, or can be obtained by contacting the Land Application Unit directly. The annual report shall be submitted to the following address; Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 (15ANCAC 02T .1111(a)) WQ0031314 Version 2.0 Shell Version 151201 Page 9 of 11 8. Noncompliance Notification The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (3 36) 776-9800, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Distribution of residuals abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to surface waters. c. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number(800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)] V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)] 2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals processing and storage facilities to identify malfunctions, facility deterioration and operator errors that could result in discharges to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)] 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. [G.S.143-215.3(a)(2)] VL GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to 143-215.6C. [G.S.143-215.6A to 143-215.6C] 2. This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. [ 15A NCAC 02T .0110] 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. [G.S. 143-215.11 WQ0031314 Version 2.0 Shell Version 151201 Page 10 of 11 The issuance of this permit does not exempt the Permittee from complying with any and all statutes, miles, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCG010000; any requirements pertaining to wetlands under 15A NCAC 02B ,0200 and 0211.0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. [I 5A NCAC 02T .0105(c)(6)] S. In the event the residuals program changes ownership or the Permittee changes his name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible :For maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. [15A NCAC 02T .0104] 6. This permit is subject to revocation or unilateral modification upon 60 days notice fioin the Division Director, in whole or part for the requirements listed in 15A NCAC 02T .0110, [15A NCAC 02T .0110] 7, Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in I SA NCAC 02T .0120(b), [I 5A NCAC 02T .0120] S. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T .0105(e)(3)] Permit issued this the 9 h day of February 2016 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION S. Jay Zimmerman, P.G., Director Division of Water. Resources By Authority of the Environmental Management Commission Permit Number WQ00311314 WQ0031314 Version 2.0 Shell Version 151201 Page 11 of 11 THIS PAGE BLANK Water Resources ENVIRONMENTAL OUALITY PAT MCCRORY Gulvraar DONALD R_ VAN DER VAART Secretary S. JAY ZIMMERMAN Director March 28, 2016 RON HARGROV}s — DIRECTOR OF UTILITIES WINSTON—SALEMMORSYTH COUNTY UTILITIES COMMISSION POST OFFICE BOX 2511 WINSTON—SALEM, NORTH CAROLINA 27102 Dear Mr. Hargrove: Subject: Permit No. WQ0031314 Correction P. W. Swann WTP Distribution of Class A Water Treatment Plant Residuals Forsyth County In accordance with an oral request received March 28, 2016 fiom you, we are forwarding herewith corrected Attachment A of Permit No. WQ0031314 issued February 9, 2016. The correction to the subject permit is as follows: 1. The residuals quantities for Thomas WTP and Nielsen WTP were reversed. Please replace Attachment A of Permit No. WQ0031314 issued February 9, 2016 with the enclosed corrected Attachment A. If you need additional information concerning this permit correction, please contact Troy Doby at (919) 807-6336 or troy.doby@ncdenr.gov. Sincerely, S. Jay Zimmerman, P.G., Direct Division of Water Resources Enclosure cc: Forsyth County Health Department (Electronic Copy) Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy) Beth Buffington, Public Water Supply Section — Protection and Enforcement Branch Digital Permit Archive WQ0031314 (Electronic Copy) Central Files State of North Carolina I Environmental Quality I WaterResourcea ( Water Quality Permitting I Non -Discharge Permitting 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919 807 6464 - r--z- This Page Blank ATTACHMENT A - Approved Residual Sources Certification Date: February 9, 2016 - Winston-Salem/Forsyth County Utilities Commission Permit Number: WQ0031314 Version: 2.0- Class A Water Treatment Plant Residuals Product Generated for Distribution Owner Winston-Salem/Forsyth County Utilities Commission Winston-Salem/Forsyth County Utilities Commission Winston-Salem/Forsyth County Utilities Commission Total Facility Name County permit Number Swann WTP Neilson WTP Forsyth i NCO079821 Forsyth I NCO086011 Biological Monitoring Maximum Frequency for Monitoring Frequency for Monitoring Frequency for Approved Residuals Dry D Tons per Years Non -hazardous Metals and Pathogen & Mineralization Characteristics I Nutrients 3•11 See Table Below Vector Attraction Reductions° e None state No 750 Once per permit cvele No 1,499 Once per r permit See Table Below `None Thomas WTP I Forsyth I NCO086762 I No 750 Once per cycle See Table Below None 2,999 1. Maximum Dry Tons per Year is the amount of residuals approved for distribution from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV,2. 3. Testing of metals and nutrients as stipulated under permit Condition 1V.3. 4. Analyses of pathogen reductions as stipulated under pen -nit Condition IV_4. S. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Distributed short tons l2er ear Monitoring Frequency Established in 40 Cr, R 503 and 1SA NCAC 02T .1111 <319 i/Year ==-319 - c1,650 11 Quarter (4 times per ear) - 1,650 - <-16,500 1/60 Days 6 times er ear) —16500 lhnonth I times wear) 6. Water Treatment Plant residuals are exempt from meeting the pathogen & vector attraction reduction requirements in Condition IVA, provided they are not mixed with residuals that have been generated during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The Water Treatment Plant residuals must be treated and processed in a manner as to not meet the definition of "Biological Residuals" as defined in 15A NCAC 02T .I 102(6). If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shalI include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification. WQ0031314 Version 2.0 Attachment A Page 1 of 1 SCOPE OF WORK SWANK LAGOON CLEANOUT Furnish all labor, materials, equipment, supervision, insurance and abide by all local, state and federal codes applicable to perform the alum residuals removal and land application from the P.W. Swann Water Treatment Plant lagoon #2 as per the city's current Land Application Permit #WQ0031314. The Contractor will provide the following services: 1. Removal of residuals from lagoon #2 and haul it to an approved land application site provided by the Contractor. • The Contractor is responsible for coordinating and acquiring suitable land for application of the residuals and maintaining records of quantities of residuals applied to each parcel in accordance with agronomic rates as defined in Permit WQ0031314. • The Contractor shall be responsible for collecting and testing a representative set of soil pH's for each parcel of land residuals are to be applied to. Should the pH of these samples be below 6.0 on average the Contractor shall be responsible for calculating the amount of lime required to bring the soil above 6.0 as required by our residuals permit. The Contractor shall provide a unit cost for lime per ton with their bid which shall include purchasing the lime, transportation to the parcel's and application of a sufficient quantity to satisfy the requirements of our land application permit. • Special attention is required as not to disturb the Bentonite clay liner at the bottom of lagoon #2. 2. The Contractor will be required to show certified volumes of tankers used to haul residuals. The Contractor will have the responsibility of keeping the roads at and along the haul route and Swann WTP clean at all times. If it is necessary to have any roads scraped due to debris it will be done at the expense of the Contractor. The Swann Plant lagoon area and site roads must be returned to their original condition at the end of the work. This includes replacing gravel on the gravel road at/around the lagoons if deemed necessary by the Plant Supervisor. 4. The Contractor will be required to provide maps of the application sites with drawn boundaries and documentation of the amount of residuals applied on each field per acre. The Contractor will be required to provide the Plant Supervisor with soil testing results and maps detailing the approximate locations of soil tests and land application sites with drawn boundaries delineating where residuals were applied and documentation regarding the quantity of residuals applied on each field (per acre). 5. The Contractor shall provide restroom facilities for their employees. Page 19 of 23 SPECIFICATIONS Safety The Contractor is responsible for complying with all applicable OSHA standards during the entire project duration. General Site Conditions Each bidder will be responsible for having knowledge of the site conditions and submitting bids based on the conditions that exist at the site. A site inspection may be arranged by contacting the Swann Water Plant Supervisor, Bill Goss, at (336) 945-1179. Work Hours Work hours for this project are limited to 7:00 a.m. to 5:00 p.m., Monday through Friday. . Schedulin-- The Contractor will be expected to begin work within thirty (30) days after receiving a Notice to Proceed. Work shall progress continuously with sufficient personnel to complete the work within sixty (60) days. Time extensions may be granted for unusually inclement weather but no change in price will be allowed. Equipment The Contractor will be responsible for furnishing and operating all necessary equipment. The equipment used will be left to the Contractor's discretion. The Contractor will be required to show certified volumes of tankers used to haul residuals. Residuals Removal The Contractor will be responsible for removing the residuals from the lagoon, hauling to the deposition site and applying the residuals to the site as per the city's Land Application Permit WQ031314. The removal of the residuals will be completed without disturbing the bentonite clay bottom of the lagoon. The Contractor will be responsible for any damage to the clay bottom, or any other facility that is caused by his work. Sediment Consistence The Owner will coordinate with the Contractor on adding water to get the residuals to the desired consistency for removal. The Contractor is responsible for all equipment necessary to properly mix, pump, haul and land apply the residuals. Sediment Volume and PaN-ment It is estimated there is an average of 3 to 7 feet of residuals present in the lagoon depending on conditions. The low bidder will be determined by the lowest unit price per gallon. It will be the Contractor's responsibility to do any surveying or other calculation to determine approximate volume. Contractors will be provided as builts of lagoon #2 to assist in estimating volumes of residuals. The Contractor will be paid for based on the calculation (Gallons Removed X Price/Gallon) as per the Contractor's bid. No adjustments in price or quantities will be made for items such as mobilization, ramp construction or removal, sediment fluffing during loading, fuel surcharges, etc. All costs are to be covered in the unit price per gallon. Page 20 of 23 Transporting The Contractor shall furnish all necessary vehicles to transport the materials from the lagoon to the designated deposition site. The City is requiring that all transport vehicles be of a type that is watertight to prevent any leakage or spillage along the haul route. In order to prevent excess damage to the plant grounds and facilities, the haul route across the plant property must be approved by the Swann Plant Supervisor or his duly appointed representative. Upon completion of the project, the Contractor will restore the haul route to its original condition. All travel on state maintained roads shall be in accordance with all local, state and federal transportation rules and regulations. Deposition The material removed from the lagoon shall be applied at a location approved for land application of alum residuals which is to be coordinated and provided by the Contractor. The Contractor shall maintain a log documenting the number of gallons removed from lagoon and quantity of gallons applied to each field each day. This log should be available for inspection by Plant Supervision as needed. The Contractor shall calculate and adhere to agronomic rates as outlined in Permit WQ0031314 Dust Control and Road Cleaning The Contractor shall control dust throughout the entire contract period within project areas and at all other areas affected by the project. This includes, but is not limited to, paved and unpaved roads, haul roads, access roads, disposal sites, and material and equipment storage sites. Dust control measures may include, but are not limited to, wetting down disturbed earth surfaces or eliminating traffic across them, removing accumulations of dirt from paved areas by hand or mechanical means, and washing roads at the end of each work day. Roads utilized by the Contractor during the execution of the work related to this project shall be inspected by the Contractor frequently on each day that work is being conducted. Any material spilled onto the roads along the haul route or material tracked onto the road at the lagoon entrance or at the deposition site during the day shall be removed and the road scraped or washed by a company normally involved in this type of work at the end of each work day at the expense of the Contractor. All roads shall be left clear and free of mud, dust, dirt, debris, etc. prior to the Contractor leaving the project site at the end of each work day. The Commission reserves the right to require that roads be cleaned more frequently than once a day if it determines that it is necessary to do so. Additional road cleanings will be at no additional expense to the Commission. Site Clean Up The Contractor shall keep the project areas at the lagoon and the disposal site free at all times from accumulations of waste materials, rubbish, and debris. All wastes shall be removed from the project areas and disposed of in a manner complying with local ordinances and antipollution laws. Contractor Field Superintendent The Contractor shall provide a Project Field Superintendent to supervise this Contract throughout its duration. The Field Superintendent's responsibilities shall include, but not be limited to, the following: The Project Field Superintendent shall be full-time on site during all project activities, including those of any subcontractor, and shall be the main point of contact for the Project Page 21 of 23 Manager and Swann Plant staff. - Be available for contact after working hours should it become necessary - Coordinate all work and work schedules - Supervise all field work - Coordinate with property owners and the public - Ensure that all work meets all Contract requirements. - Maintain logs of gallons removed, hauled and applied to each site on a daily basis. Residuals Testing. Sample Collection and Annual Reyorting The Contractor shall have on site at all times a foreman responsible for overseeing the work being performed. The foreman shall coordinate with the Swann WTP Plant Supervisor/ORC regarding the work performed. The Contractor shall be responsible for the following: Soil SamNin�� • Collection and analysis of representative soil samples from all parcels residuals are applied to prior to residuals application. • Actual application quantities per acre for lime applied to each parcel. • Soil reports for each parcel residuals are applied to. Residuals Sampling and Reporting Deliverables • The Contractor shall maintain logs for each application site detailing the rate of application per site (PAN), maps with boundaries drawn showing disposal area for each site and sodium absorption rate (SAR)/exchangeable sodium percentage (ESP) for the residuals applied. • Collection and analysis of residuals to demonstrate that residuals are non -hazardous (i.e. TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. NOTE: These samples are required once per permit cycle and were collected during residuals removal in April 2016, therefore, they are not due again until 2021. • Collection, analysis and delivery of final report to owner of required metals and nutrient samples as stipulated under permit Condition IV.3 by a NC certified laboratory. • Adherence to monitoring frequencies based on dry tons as outlined in Condition 5. of permit Attachment A for metals and nutrients. • Obtaining signed Land Use Agreements by land owners/entities receiving residuals, City of Winston-Salem ORC, and representative from company land applying residuals for each parcel of land residuals are applied to. • Completion of the following reports necessary for annual reporting which must be delivered to the ORC no later than February 1 following the year in which residuals were applied to allow the ORC ample time to review and submit the annual report to the State of North Carolina. - DENR Form DMSDF — Class A Annual Distribution and Marketing/Surface Disposal Certification and Summary Form signed by preparer. - DENR Form DMSDF — Supplemental Form - Class A Annual Distribution and Marketing/Surface Disposal Certification and Summary Form — Supplemental information signed by preparer. - DENR Form RSSF — Annual Residual Sampling Summary Form signed by preparer. Page 22 of 23 - DENR Form RSSF — B Annual Residual Sampling Summary Form signed by preparer. - All sample analysis final reports, laboratory data sheets and chain of custodies supporting above forms. - Maps of each residuals distribution site with boundaries of residuals application clearly delineated. - Soil reports for each parcel residuals applied to. - Contractor logs for each application site detailing the rate of application per site (PAN). - Contractor logs detailing sodium absorption rate (SAR)/exchangeable sodium percentage (ESP) for the residuals applied for each parcel. Page 23 of 23 DETAILED SPECIFICATIONS RESIDUALS REMOVAL AT THOMAS WTP Scope Of Work Furnish all labor, materials, equipment, insurance and supervision and abide by all local, state and federal codes applicable to haul alum residuals from the R.A. Thomas Water Treatment Plants to the WSFU Utilities Hanes Mill Road Landfill located at 325 W. Hanes Mill Road, Winston-Salem NC 27105. There are two lagoons on the plant site. These lagoons are cleaned out on an approximately 1-year rotation and each lagoon averages approximately 800 cubic yards of material (this number is an approximation based on historical quantities and can differ, the city cannot guarantee volumes as they are subject to change based on many factors). Only one lagoon is cleaned each year. The contractor will provide the following services: a. Removal of residuals from each lagoon and haul it to WSFC Utilities landfill located at 325 W. Hanes Mill Road, Winston-Salem NC 27105. b. The Contractor shall provide one price per cubic yard to remove and haul material. c. WSFC Utilities will pay all tipping fees at Hanes Mill Road Landfill. d. The residuals may be dry to wet and may have the consistency of cake batter. e. Residuals will be removed down to the solid bottom of the lagoon being careful not to remove material from the perimeter of the lagoon and side slopes. 2. The contractor will have the responsibility of keeping the Thomas Water Plant and the road frontage along Martin Luther King, Jr. Drive clean at all times. If it is necessary to have any roads washed due to debris on the road, or from complaints by any resident along the route of transport due to spilled material it will be the financial responsibility of the contractor. The Thomas Plant must be returned to its original condition at the end of each cleaning. This includes replacing gravel on the gravel road at/around the lagoons if deemed necessary by the Plant Supervisor. 3. The Contractor shall provide restroom facilities for their employees. Safety The Contractor is responsible for complying with all applicable OSHA standards during the entire project duration. General Site Conditions Each bidder will be responsible for having knowledge of the site conditions and submitting bids based on the conditions that exist at the site. A site inspection can be coordinated by contacting the Thomas Water Plant Supervisor, Donna Lankford, at (336) 788-0152. Work Hours Work hours for this project are limited to 7:00 a.m. to 4:00 p.m., Monday through Friday. Schedulin The work may commence upon Notice to proceed. The contractor will be expected to begin work within 30 days after receiving a Notice to Proceed. Work shall progress continuously with sufficient personnel to complete the work within 30 days of the start of residuals removal. Time extensions may be granted for unusually inclement weather but no change in price will be allowed. Equipment The Contractor will be responsible for furnishing and operating all necessary equipment. The equipment used will be left to the Contractor's discretion. The, contractor will be responsible for any damage to the gravel, underdrain system, or any other facility or structure that is the result of their work. Residuals Removal The Contractor will be responsible for removing the residuals from the lagoon and hauling them to WSFC Utilities Hanes Mill Road Landfill. When all residuals removal is complete the lagoon reservoir floor and sides are to be graded smooth. IF2082 Residuals Removal at Thomas WTP Page 23 of 32 Residuals Consistency It is anticipated the material should have a percent solids of approximately 20% or more. However, the owner cannot guarantee this condition. Sediment Volume and Payment It is estimated there is an average of 3.0 feet of sediment present totaling approximately 800 cubic yards in each lagoon. The low bidder will be determined by the lowest unit price per cubic yard. A contracted licensed surveying company, hired by the City of Winston-Salem, will perform a grid topographical survey of the material prior to the Contractor beginning work and after the contractor has completed his work. The contractor will be paid the product of their submitted unit price in cubic yards multiplied by the volume as determined by the contracted licensed surveying company's measurements. Therefore, actual quantities may be higher or lower than estimated. The City of Winston-Salem shall hire a licensed survey company to perform this work and will be the sole basis for compensation under this contract. No adjustments in price or quantities will be made for items such as mobilization, ramp construction or removal, sediment fluffing during loading, fuel surcharges, etc. All costs are to be covered in the unit price per cubic yard. Transportinn The Contractor shall furnish all necessary vehicles to transport the materials from the lagoon to the designated deposition site. The City is requiring that all transport vehicles be of a type that is watertight to prevent any leakage or spillage along the haul route. In order to prevent excess damage to the plant grounds and facilities, the haul route across the plant property must be approved by the Thomas Plant Supervisor or his/her duly appointed representative. Upon completion of the project, the Contractor will restore the haul route to its original condition which may include reseeding, deposition of stone or other methods to repair worn surfaces of travel. All travel on state maintained roads shall be in accordance with all local, state and federal transportation rules and regulations. Dust Control and Road Cleaning The Contractor shall control dust throughout the entire contract period within project areas and at all other areas affected by the project. This includes, but is not limited to, paved and unpaved roads, haul roads, access roads, disposal sites, and material and equipment storage sites. Dust control measures may include, but are not limited to, wetting down disturbed earth surfaces or eliminating traffic across them, removing accumulations of dirt from paved areas by hand or mechanical means, and washing roads at the end of each work day. Roads utilized by the Contractor during the execution of the work related to this project shall be inspected by the Contractor frequently on each day that work is being conducted. Any material spilled onto the roads along the haul route or material tracked onto the road at the lagoon entrance or at the disposal site entrance during the day shall be removed and the road washed at the end of each work day. All roads shall be left clear and free of mud, dust, dirt, debris, etc. prior to the Contractor leaving the project site at the end of each work day. The Commission reserves the right to require that roads be cleaned more frequently than once a day if it determines that it is necessary to do so. Additional road cleanings will be at no additional expense to the Commission. The awarded Contractor must have an approved Spill and Control Plan that satisfies the North Carolina's Department of Environmental Quality Aquifer Protection Section's requirements for the material being hauled. This plan must be submitted for review by the Plant Supervisor prior to residuals being hauled. Site Clean Up The Contractor shall keep the project areas at the lagoon and the disposal site free at all times from accumulations of waste materials, rubbish, and debris. All wastes shall be removed from the proj ect areas and disposed of in a manner complying with local ordinances and antipollution laws. Contractor Field Superintendent The Contractor shall provide a Project Field Superintendent to supervise this Contract throughout its duration. The Project Field Superintendent shall make routine visits to the plant to monitor his crew's activities and to ensure smooth operation. Residuals Samnlin, and Reportine Deliverables Collection and analysis of one percent (1%) total solids to be used to determine the total dry tons of material hauled. It is the contractor's responsibility to collect the sample and have it analyzed by NC certified laboratory for wastewater analysis for percent total solids. IF2082 Residuals Removal at Thomas WTP Page 24 of 32 SPECIFICATIONS Safe The Contractor is responsible for complying with all applicable OSHA standards during the entire project duration. General Site Conditions Each bidder will be responsible for having knowledge of the site conditions and submitting bids based on the conditions that exist at the site. A site inspection may be arranged by contacting the Neilson Water Plant Supervisor, Gabe Sparks, at (336) 766-9885. Work Hours Work. hours for this project are limited to 7:00 a.m. to 4:00 p.m., Monday through Friday. Scheduling It is anticipated that work could begin in early 2018. The contractor will be expected to begin work within 30 days after receiving a Notice to Proceed, if necessary. Work shall progress continuously with sufficient personnel to complete the work within 120 days of the start of residuals removal. Time extensions may be granted for unusually inclement weather but no change in price will be allowed. Equipment The Contractor will be responsible for furnishing and operating all necessary equipment. The equipment used will be left to the Contractor's discretion. The contractor will be responsible for any damage to the gravel, underdrain system, or any other facility or structure that is caused by their work. Residuals Removal The Contractor will be responsible for removing the residuals from the lagoon, hauling them to the application site and land applying as per the City of Winston-Salem's Land Application Permit #WQ0031314. The Contractor shall be responsible for removing and disposing of any vegetation that may have grown on top of the residuals in the lagoons prior to hauling. The residuals will be removed down to the top of the clay bottom being careful not to remove clay from the perimeter of the lagoon, bottom and side slopes. When all residuals removal is complete the lagoon reservoir floor and sides are to be graded smooth. Residuals Consistency It is anticipated the material should have a percent solids of approximately 20% or more. However, the owner cannot guarantee this condition. Sediment Volume and Pavment It is estimated there is an average of 3.0 feet of sediment present totaling approximately 3,500-4,000 cubic yards in each lagoon. The low bidder will be determined by the lowest unit price per cubic yard for residuals land applied. A contracted licensed surveying company, hired by the City of Winston- Salem, will perform a grid topographical survey of the material prior to the Contractor beginning work and after the contractor has completed his work. The contractor will be paid the product of their submitted unit price in cubic yards multiplied by the volume as determined by the contracted licensed surveying company's measurements. Therefore, actual quantities may be higher or lower than estimated. The City of Winston-Salem shall hire a licensed survey company to perform this work and will be the sole basis for compensation under this contract. IF18145 Residuals Removal From Lagoons at R.W. Neilson WTP Page 24 of 30 No adjustments in price or quantities will be made for items such as mobilization, ramp construction or removal, sediment fluffing during loading, fuel surcharges, etc. All costs are to be covered in the unit price per cubic yard. Transoortin� The Contractor shall furnish all necessary vehicles to transport the materials from the lagoon to the designated deposition site. The City is requiring that all transport vehicles be of a type that is watertight to prevent any leakage or spillage along the haul route. In order to prevent excess damage to the plant grounds and facilities, the haul route across the plant property must be approved by the Neilson Plant Supervisor or his duly appointed representative. Upon completion of the project, the Contractor will restore the haul route to its original condition which may include reseeding, deposition of stone or other methods to repair worn surfaces of travel. All travel on state maintained roads shall be in accordance with all local, state and federal transportation rules and regulations. Deposition The material excavated from the lagoons shall be deposited as per the city's land application permit. The contractor is solely responsible for locating suitable land in sufficient acreage for the application of the material. Dust Control and Road Clean The Contractor shall control dust throughout the entire contract period within project areas and at all other areas affected by the project. This includes, but is not limited to, paved and unpaved roads, haul roads, access roads, disposal sites, and material and equipment storage sites. Dust control measures may include, but are not limited to, wetting down disturbed earth surfaces or eliminating traffic across them, removing accumulations of dirt from paved areas by hand or mechanical means, and washing roads at the end of each work day. Roads utilized by the Contractor during the execution of the work related to this project shall be inspected by the Contractor frequently on each day that work is being conducted. Any material spilled onto the roads along the haul route or material tracked onto the road at the lagoon entrance or at the disposal site entrance during the day shall be removed and the road washed at the end of each work day. All roads shall be left clear and free of mud, dust, dirt, debris, etc. prior to the Contractor leaving the project site at the end of each work day. The Commission reserves the right to require that roads be cleaned more frequently than once a day if it determines that it is necessary to do so. Additional road cleanings will be at no additional expense to the Commission. The Contractor must have an approved Spill and Control Plan that satisfies the North Carolina's Department of Environmental Quality Aquifer Protection Section's requirements for the material being hauled. This plan must be submitted for review by the Plant Supervisor prior to residuals being hauled. Site Clean Uv The Contractor shall keep the project areas at the lagoon and the disposal site free at all times from accumulations of waste materials, rubbish, and debris. All wastes shall be removed from the project areas and disposed of in a manner complying with local ordinances and antipollution laws. Contractor Field Superintendent The Contractor shall provide a Project Field Superintendent to supervise this Contract throughout its duration. The Field Superintendent's responsibilities shall include, but not be limited to, the following: - The Project Field Superintendent shall be full-time on site during all project activities, including IF18145 Residuals Removal From Lagoons at R.W. Neilson WTP Page 25 of 30 those of any subcontractor, and shall be the main point of contact for the Project Manager and Neilson Plant staff. - Be available for contact after working hours should it become necessary - Coordinate all work and work schedules - Supervise all field work - Coordinate with property owners and the public - Ensure that all work meets all Contract requirements. - Maintain logs of residuals removed, hauled and land applied to each site on a daily basis. Residuals Sampling and Renortim-, Deliverables • The Contractor shall maintain logs for each application site detailing the rate of application per site (PANT), maps with boundaries drawn showing disposal area for each site and sodium absorption rate (SAR)/exchangeable sodium percentage (ESP) for the residuals applied. • Collection and analysis of residuals to demonstrate that residuals are non -hazardous (i.e. TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. NOTE: These samples are required once per permit cycle and were collected during residuals removal in March 2016, therefore they are not due again until 2021. • Collection, analysis and delivery of final report to owner of required metals and nutrient samples as stipulated under permit Condition IV.3 by a NC certified laboratory. • Collection and analysis of representative soil samples and application of lime when/as required by Land Application Permit #WQ0031314. • Adherence to monitoring frequencies based on dry tons as outlined in Condition 5. of permit Attachment A for metals and nutrients. • Obtaining signed Land Use Agreements by land owners/entities receiving residuals, City of Winston-Salem ORC, and representative from company land applying residuals for each parcel of land residuals are applied to. • Completion of the following reports necessary for annual reporting which must be delivered to the ORC no later than February 1 following the year in which residuals were applied to allow the ORC ample time to review and submit the annual report to the State of North Carolina. IF18145 Residuals Removal From Lagoons at R.W. Neilson WTP Page 26 of 30 DWR, State of North Carolina Department of Environmental Quality Division of Water Resources Divislon of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and supporting, documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Res' uals Source Certification (FORM: RSC 11-15): [Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. VO r new or renewed permits, submit a separate certification for each source facility. Vr modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. omplete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Res' duals Source -Generating Facility Information: Res Vach source facility, attach the following: icinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Ike siduals Land A lication Permits"'. Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals e to be generated, treated, processed, and stored at the facility. Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during _Jdocessing. Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Re ' uals Quality Information: [��oteac Fh source facility, attach the following: [aboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector action reduction requirements. For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Winston-Salem/Forsyih County Utilities Commission (P.W. Swann Water Treatment :Plant) Status Code a Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R Swann WTP Swann WTP Forsyth WQ0031314 750 750 R Swann WTP Neilson WTP Forsyth WQ0031314 2,500 1,499 R Swann WTP Thomas WTP Forsyth WQ0031314 750 750 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 State of North Carolina nWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: P.W. Swann Water Treatment Plant 2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Bill Brewer — Water Treatment Superintendent Complete mailing address: 2800 River Ridge Road City: Pfafftown State: NC Zip: 27040-8435 Telephone number: (336) 397-7727 E-mail address: billb@cjtyofws.org 4. Facility physical address: 2800 River Ridge Road City: Pfafftown State: NC Zip: 27040-8435 Coordinates: Latitude: N36° 8' 51.5" Longitude: W80° 25' 14" Datum: DMS Level of accuracy: 100% Method of measurement: Survey 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ® treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ❑ Yes ® No 7. Facility permitted/design flow: 25.0 MGD and facility average daily flow: 12.4 MGD 8. Average amount of residuals being generated at this facility 750 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: The treatment facilities for wash water consists of one 1 equalization basin with a capacity of 0.489 MG's and two 2) residuals lagoons for settling and duving solids with an effective storage volume of 3.2 MG's each. Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 021.110Z O as: d Biological Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Research & Analytical Laboratories, Inc, and Date of analysis: 4/8/2016 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >212 OF (> 140°F) Passed reactivity test: ®yes ❑no. HCN: <250 mg/kg (<250) & H2S: <500 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 0.192 Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene Trichloroethylene 2,4,5-Trichlorophenol 0.5 0.5 400.0 ND ND ND 1,2-Dichloroethane 0.5 ND 1, 1 -Dichloroethylene 0.7 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105, a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: WaN 1�oint Analytical Virginia Inc. and Date of analysis: 11/25/2019 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Result Concentration Limits (Class A Only) (mg1kg) (mglkg) 41 <27.8 39 <5.56 Arsenic 75 Cadmium 85 Copper 4,300 1,500 70.6 Lead 840 300 25.4 Mercury 57 17 <0.811 Molybdenum 75 n/a <13.9 Nickel 420 420 23.8 Selenium 100 100 <27.8 Zinc 7,500 2,800 503 b. For Surface Disposal Unit llandfllj: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Research & Analytical Laboratories Inc. and Date of analysis: 4/8/2016 Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic Chromium (mg/kg) (mg/kg) Nickel (mg/kg) 210 > 0 but < 25 ❑ > 25 but < 50 30 200 34 220 240 ::[![] > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) <27.8 36.7 23.8 FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 14.2 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical Vir .inia Inc. and Date of analysis: 11/25/2019 Parameter Result (mg/kg) Aluminum 160,000 Ammonia -Nitrogen 11,400 Calcium 4,520 Magnesium 2,400 Nitrate -Nitrite Nitrogen <262 pH (Standard Unit) 6.3 Phosphorus 4,920 Potassium 2,120 Sodium <1,390 Total Kjeldahl Nitrogen 25,700 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.61 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0.4 or 40 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Accepted formula for water plant residuals. e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: I Application Method Surface Injection/Incorporation First (111) Year PAN (mg/kg) 11,682 N/A Five -Year Maximum Adjusted PAN (mg/kg) 15,187 N/A 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N/A -water plant residuals FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land A lication o -Class A or Er uivalent: 10 A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. B ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)( )] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, [] heat drying, ❑heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land A lication o Class B: ❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction WAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)1 - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. Page 5 of 5 FORM: RSC 06-16 ce 04- i� r A A ; I P.W. Swann Water Treatment Plant Water System Facility ID = TP3 Production Capacity = 25.0 MGD City of Winston-Salem Yadkin River NPDES# = NCG590003 - - 50 MG Raw Water Off Stream Storage Basin #1 100 MG Raw Water Off Stream Storage Basin #2 The Northwest WTP has two treatment trains that are Mix 12.5 MGD each for a total Flash plant capacity of 25.0 MGD. Flocculation Sedimentation Basins 25 MGD Chlorine Alum 10 Filters 1-6 Caustic So( Chlorine Fluoride Ortho-Phc Alum 25 MGD T Chlorine KMn04 Caustic Soda Alum Residual Lagoon Residual Lagoon (4.3 MG)� (4.3 MG) A —0.5 MGD 25 MGD 30 MGD Entry Point-EP3 Chlorine 5.0 MG Clearwell �I 0.489 MG Equalization Basin Distribution System BLACK & VEATCH LLP CIVIL DESIGN MEMORANDUM 1lP S«� ?Alt- Winston-Salem/Forsyth County Utility Commission B&V Project 37604 Winston-Salem, North Carolina First Issue: July 31, 1998 Northwest Water Treatment Plant Latest Revision: October 30, 1998 3. Flow Measurement. Initial Ultimate Type Magnetic Magnetic Number of meters 1 2 Size, each, inches 30 30 Flow measurement range, mgd 10-37.5 10-37.5 Control: Flow signal will be transmitted to the plant control room and local indication will be provided in the pumping station. F. WASH WATER AND RESIDUALS HANDLING 1. General. a. Initial Wash Water and Residuals Handlin 7 . Spent wash water and filter -to -waste will discharge by gravity to a wash water equalization basin. The collected water will gravity discharge from the equalization basin to the residuals storage lagoons. Gravity flow rates from the equalization basin will be controlled by a rate control valve. The wash water drainage system upstream of the equalization basin will be designed to allow six filters (two treatment trains) to be simultaneously wasted at the design filtration rate. This drainage capacity is provided for an emergency condition when water quality dictates the basins be wasted until necessary treatment adjustments are made. Because this is an emergency condition and not part of the normal plant operation, the facilities downstream of the equalization basin will not be designed to accommodate this increased emergency flow. Flows in excess of the equalization basin drainage capacity will overflow to the plant overflow drain. Unthickened residuals from the sedimentation basins will discharge by gravity through the viewing pit to the residuals storage lagoons. I-19 BLACK & VEATCH LLP CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 37604 Winston-Salem, North Carolina First Issue: July 31, 1998 Northwest Water Treatment Plant Latest Revision: October 30, 1998 Decant/overflow from the residuals lagoons will discharge to the creek in accordance with the NPDES permit. The initial wash water equalization basin will be designed to be readily converted to a future clarifier by installation of circular clarifier equipment. Piping provisions will be made to allow the residuals to drain to future residuals thickeners when the basin is converted to a clarifier. b. Future Wash Water and Residuals Handlin•,. Provisions will be made to allow the future addition of a dedicated filter -to -waste drain to a future equalization basin for filter -to -waste recycle. The future filter -to -waste equalization basin will be equipped with pumps for recycling to the plant raw water influent piping. The existing equalization basin will be dedicated to handling filter backwash water. Provisions will be made to allow the addition of a second equalization basin dedicated to filter backwash water handling. The future wash water equalization basin will be equipped with pumps to pump wash water to the existing equalization basin which will be converted to a clarifier for wash water treatment. Wash water and residuals handling and treatment facilities will be designed to allow a possible future addition of the following. • Equalization basins. • Wash water clarifiers. • Residuals thickeners. • Residuals dewatering facilities. I-20 BLACK & VEATCH LLP CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 37604 Winston-Salem, North Carolina First Issue: July 31, 1998 Northwest Water Treatment Plant Latest Revision: October 30, 1998 2. Wash Water and Residuals Flows and Solids Production. Initial Ultimate Filter Backwash Water Per filter(l), gal 164,000 164,000 Avg�Z�, gpd 492,000 984,000 Max(3), gpd 984,000 1,968,000 Filter -to -Waste Per filter(4), gal 58,300 58,300 Avg�2��4�, gpd 174,900 349,800 Max�3��4�, gpd 349,800 699,600 Total Residuals Production Avg�6�, lb/day 3,600 7,200 Max('), lb/day 7,500 15,000 Unthickened Residuals Flow to LaL oons Avg�6��8�, gpd 216,000 432,000 Max�'��8�, gpd 450,000 900,000 Thickened Residuals Production Avg�6��9�, gpd 21,600 43,200 Max�'��9�, gpd 45,000 90,000 Free Liquid from Residuals(io) Avg, gpd 194,400 388,800 Max, gpd 405,000 810,000 Overflow from LaL,00ns�5� Avg, mgd 0.95 1.89 Max, mgd 1.91 3.83 (1) Flow rate of 22.5 gpm/sf for 10 minutes. (2) Half of the filters backwashed in one day. I-21 BLACK & VEATCH LLP CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 37604 Winston-Salem, North Carolina First Issue: July 31, 1998 Northwest Water Treatment Plant Latest Revision: October 30, 1998 (3) All filters backwashed in one day. (4) Flow rate of 4 gpm/sf for 20 minutes. (5) Backwash water, plus filter -to -waste, plus free liquid from residuals, plus 10 percent (miscellaneous plant flows). (6) Two hundred forty pounds per million gallons, using average flow rate (Initial flow 15 mgd, ultimate flow 30 mgd). (7) Three hundred pounds per million gallons, using maximum flow rate (Initial flow 25 mgd, ultimate flow 50 mgd). (8) 0.2 percent solids. (9) 2.0 percent solids. (10) Unthickened residuals flow minus thickened residuals flow. 3. Wash Water EQualization Basin. Number of basins Design criteria, each Volume, each, gal Basin type B asin shape Dimensions, ft Inside diameter Sidewall water depth Bottom slope to center hopper Water depth at top of hopper Initial Ultimate 1 2 Storage volume of two filter wash cycles plus 10 percent 489,000 Reinforced concrete Circular 85 12 12:1 15.25 Controls: A ball valve will be provided on the -equalization basin drain line in a vault to control flow rates from the equalization basin to the residuals storage lagoons. The valve will be controlled manually from the control room or locally from the valve vault. A level sensor will be provided in the equalization basin. Basin level will be transmitted to each filter console and to the plant control room. At basin overflow level, an overflow alarm will be transmitted to the control room. I-22 BLACK & VEATCH LLP CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 37604 Winston-Salem, North Carolina First Issue: July 31, 1998 Northwest Water Treatment Plant Latest Revision: October 30, 1998 4. Residuals Storage LaLoons. The residuals storage lagoons will receive all plant residuals and wash water for treatment and storage. Initial Ultimate Number of lagoons 2 3 Lagoon type Earthen lagoon with concrete slope protection and underdrain Dimensions, each, ft Length 350 350 Width 235 235 Max residuals depth 8 8 Max water depth 10 10 Freeboard 2 2 Perimeter slope 3:1 3:1 Liquid volume, each, mg 4.3 4.3 Storage volume, each, mg 3.2 3.2 Effective storage, each lagoon, days 365 183 Access Ramp Width, ft 12 12 Slope, percent 12 12 Decant Discharge to creek Sludge removal method Air drying, excavate with front-end loader or clam bucket Cleaning duration, years 1 1 G. OPERATIONS BUILDING An operations building will be provided for administrative facilities, chemical feed and storage, and maintenance and control facilities. Figures I-13 and I-14 showing the floor plans for the basement and operating floor and Figure I-15 showing the building elevations are attached. I-23 P.W. Swann Water Treatment Plant Solids Handling Plan The Swann Water Treatment Plant is a 25.0 MGD water treatment facility. Solids are generated by sludge removal from two sedimentation basins, backwashing six filters, and filter -to -waste after filter backwashes are completed. Solids produced from filter backwashes and filter -to -waste are routed to a flow equalization basin before entering one of two residual lagoons. Solids removed from the sedimentation basins are routed directly to one of two residual lagoons. The equalization basin volume is 0.489 MG, and each of the two residual lagoons has a volume of 3.2 MG. Permits and Classifications: 1. The discharge from the residuals lagoons is authorized by NPDES Permit NCG590003. The classification for the discharge is Grade 1 Physical/Chemical. 2. The distribution of the residuals removed from the lagoons is authorized by permit WQ0031314. The residuals are classified as Class A. Operation: 1. The system consists of a 0.489 MG equalization basin (EQ basin) and two (2) residuals lagoons with a capacity of 4.3 MG's each. 2. Routine inspections of equipment will be conducted Senior Utility Plant Supervisor to ensure proper operation of equipment. Any equipment not functioning properly are reported through the water division's asset management program, MAXIMO, to the appropriate support group for repair/replacement. 3. Each lagoon consists of an oval concrete apron, a clay bottom, and an access ramp used for residuals removal. The solids stream enters on one end of the lagoon and there is an adjustable weir on the opposing end allowing decant to flow to the discharge. 4. Backwash and filter -to -waste water from the plant process flow by gravity to the EQ basin. The backwash and filter -to -waste water then flows by gravity into the lagoon in service. A regulating valve prevents flow spike from entering the residuals lagoons. 5. A flow meter measures flow leaving the EQ basin and 38% Sodium bisulfite is applied to the EQ basin discharge for dechlorination of effluent being sent out discharge NCG590003. 6. All sedimentation basin residuals flow by gravity directly to the residuals lagoon in service. P.W. Swann Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 7. Each lagoon has the capacity to accept and store the solids produced by the plant for approximately 18 months. This allows one lagoon to accept the daily waste stream of solids while the other is out of service. 8. Residuals are removed from the lagoons in liquid form and hauled to land application sites by a private contractor. Monitoring and Reporting Requirements: 1. Residuals generated by each source -generating facility must be analyzed to demonstrate that they are non -hazardous based on the most current permit requirements (Attachment A). Sampling will be conducted under supervision of the Senior Water Treatment Plant Supervisor by WSFC Utilities current contractor as described below in compliance with permit requirements. 2. Analysis will be performed by a NC Certified Laboratory. 3. Analyses made according to monitoring and reporting requirements must be certified for the required parameter(s). 4. Corrosivity, ignitability, reactivity, and a Toxicity Characteristics Procedure analysis are required once each permit cycle. The TCLP analysis includes the following parameters (i.e., note the regulatory level in milligrams per liter in parentheses): Arsenic (5.0) Barium (100.0) Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) m-Cresol (200.0) o-Cresol (200.0) p-Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene(7.5) 1,2-Dichloroethane (0.5) 1, 1 -Dichloroethylene (0.7) 2,4-Dinintrotolulene (0.13) Endrin (0.02) Hexachlorobenzene (0. 13) Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lead (5.0) Lindane (0.4) Mercury (0.2) Methoxychlor(10.0) Methyl ethyl ketone (200.0) Nitrobenzene (2.0) Pentachlorophenol (100.0) Pyridine (5.0) Selenium (1.0) Silver (5.0) Tetrachloroethylene (0.7) Toxaphene (0.5) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2) 5. Analyses of the following parameters are also required with each application event: Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Phosphorous Potassium P.W. Swann Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 pH Plant Available Nitrogen (by calculation) Selenium Sodium % Total Solids TKN Zinc 2 6. Data to verify pathogen reduction and vector attraction reduction of the residuals is maintained on file for five years. The required data is specific to the stabilization process utilized, and is also sufficient to demonstrate clear compliance with the Class A pathogen requirements and restrictions noted in 15A NCAC 02T .1106 (a) and (b) and vector attraction reduction requirements in 15A NCAC 02T .1107 (a). 7. Proper records are maintained tracking all residuals activities. These records include the source, volume, analysis, and recipient of the residuals. 8. Three copies, per application event, of all required monitoring and reporting requirements are submitted annually before March 1, to NC DEQ-DWQ. Performance Standards: 1. The pollutant concentrations in any residuals that are land applied to any land application site shall not exceed the following Ceiling and Monthly Average Concentrations (i.e. dry weight basis): Parameter Monthly Average Concentration (milligrams per kilogram) Ceiling Concentration (milligrams per kilogram) Arsenic 41 75 Cadmium 39 85 Copper 1,500 4,300 Lead 300 840 Mercury 17 57 Molybdenum n/a 75 Nickel 420 420 Selenium 100 100 Zinc 2,800 7,500 2. If residuals are sold or given away, one of the Class A pathogen requirements in 15A NCAC 02T .I 106(b) must be met. Application Requirements: 1. Bulk residuals are not applied under the following conditions: i. If the residuals are likely to adversely affect a threatened or endangered species. ii. If the application causes prolonged nuisance conditions. iii. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards. P.W. Swann Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 3 iv. If the land is flooded, frozen, or snow-covered or is otherwise in a condition such that runoff of the residuals would occur. v. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following the residuals application event. vi. During a precipitation event or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. vii. If the slope of the land is greater than 10 percent when the bulk residuals are surface applied, and if the slope of the land is greater than 18 percent when bulk residuals are injected or incorporated. viii. If pH maintained in the soil and residuals mixture is greater than 6.0. ix. If the land does not have an established vegetative cover. x. If the vertical separation of the seasonal high water table and the depth of the residuals application is less than one foot. xi. If the vertical separation of the depth to bedrock and the depth of residuals application is less than one foot. xii. Application exceeds agronomic rates. xiii. For residuals treatment and storage facilities, the following minimum setbacks shall be adhered to: Minimum Setback Description of Setback (feet) Habitable residence or place of public assembly under separate ownership or not to be maintained as part of the project site 100 Property lines 50 Private or public water supply 100 Surface waters (streams, -intermittent and perennial, perennial waterbodies, and wetlands) 50 Wells with exception to monitoring wells 100 2. When land applying bulk residuals to any land application site, the following minimum setbacks are maintained at all times: Setback By TY a of Residual feet Description of Setback Liquid Cake Private or public water supply 100 100 Surface waters (streams -intermittent and perennial, perennial waterbodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where bottom of The ditch intersects SHWT) 25 0 Subsurface groundwater lowering system Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 3. Specific bulk residuals land application area boundaries are clearly marked on each land application site prior to and during a residuals land application event. P.W. Swann Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 4 4. Bulk residuals and other sources of PAN (Plant Available Nitrogen) are applied to all land application sites at or below agronomic rates. Appropriate agronomic rates are calculated using expected nitrogen requirements based on the Realistic Yield Expectations (RYE) field cover for each approved land application site. Spills and Noncompliance Notification: 1. The Winston-Salem Regional Office, telephone number (336) 771-5000, will be notified within 24 hours or the next working day following the occurrence or first knowledge of the occurrence of any of the following: i. Any occurrence with the distribution program, which results in the land application of significant amounts of wastes, which are abnormal in quantity or characteristic. ii. Any failure of the distribution program resulting in a release of materials to receiving waters. iii. Any time that self -monitoring information indicates that, the facility has gone out of compliance with the conditions and limitations of the permit or the parameters on which the system was designed. iv. Any process unit failure, due to known or unknown reasons, that renders the facility incapable of adequate residual treatment. v. Any spillage or discharge from a vehicle or piping system during transportation of residuals. 2. Persons reporting such occurrences by telephone shall also file a written report in letter form within (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. 3. Emergency Contacts: Swann Water Treatment Plant (336) 945-1179 (Main) Billy Goss, Plant Supervisor (336) 397-7728 (0) (336) 399-3264 (M) Bill Brewer (336) 397-7727 (0) Water Plants Superintendent (336) 745-5277 (M) Winston-Salem/Forsyth County (336) 727-8418 Utility Administration DEHNR Regional Office (336) 771-5000 General Emergency 911 HazMat P.W. Swann Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 Ifs 1EsEARCh ANA1yTiCAi LAboRAT®R1F-5r INC. . : z. Analytical/Process Consultations �.% Q.r Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Lagoon 1 (A City of Winston-Salem Swann WTP Prai ect, collected 08 April 2016) Lagoon I EPA HW Quantitation Results Characteristic Number Contaminant Limit(me1L) (melt) Level(me/L) EPA Method 1 TCLP METALS D-004 Arsenic 0.010 BQL 5.00 6010C D-005 Barium 0.040 0.192 100 6010C D-006 Cadmium 0.005 BQL 1.00 6010C D-077 Chromium 0,010 BQL 5.00 6010C D-008 Lead 0-005 BQL 5.00 6010C D-009 Mercury 0.0020 BQL 0.200 7470A D-010 Selenium 0.100 BQL 1.00 6010C D-011 Silver 0.010 BQL 5.00 6010C II . TCLP VOLATILES 0,050 BQL 0.500 8260B D-018 Benzene D-019 Carbon Tetrachloride 0.050 BQL 0.500 8260E D-021 Chlorobenzene 0.050 BQL 100 8260B D-QT? Chloroform 0.500 BQL 6.00 8260E D-028 12-D-rchlorocthane 0-050 BQL 0.500 8260B D-D29 1.1-Dichloroethylene 0-050 BQL 0.700 8260E 0-035 Methyl Ethyl Ketone 0.500 BQL 200 8260E D-039 Tetrachloroe1hylene 0.050 BQL 0.700 8260B D-040 Trichloroethylcne 0.050 SQL 0.500 8360E D-043 Vinyl Chloride 0.050 BQL 0.200 8260E III. TCLP SEMI-VOLATILES 20.0 BQL 200 8270D D-023 O-Creosol D-024 M-Creosol 20-0 BQL 200 8270D D-025 p-Creosol 2010 BQL 200 8270D D-026 Creosol 20.0 BQL 200 8270D D-027 1,4-Dichlorobenzene 0.750 BQL 730 8270D D-030 2,4-Dinitrotolucne 0.050 BQL 0.130 8270D D-032 Hexachlorobenzene 0.050 BQL 0.130 8270D D-033 Hexachlorobutadiene 0.050 BQL 0.500 8270D D-034 Hexachloroethane 0.300 BQL 3.00 8270D D-036 Nitrobenzene 0.200 BQL 2.00 8270D D-037 Pentachlorophenol 10.0 BQL 100 9270D D-038 Pyridine 0,500 BQL 5.00 82700 D-041 2,4,5-Trichlorophenol 40.0 BQL 400 8270D D-042 2,4,6-Trichlorophenol 0.200 SQL 2.00 8270D IV, TCLP PESTICIDESlHERBICIDES 0.003 BQL 0.030 8081 B D-020 Chlordane D-016 2,4-D 1.000 BQL 10.0 8151 A D-012 Endrin 0.002 BQL 0.020 8081 B D-031 Heptachlor 0.0008 BQL 0.008 8081 B D-013 Lindane 0.040 BQL 0.400 8081 B D-014 Methoxychlor I.ODO BQL BQL 10.0 0.500 8081 B 8081 B D-015 Toxaphene D-017 2.4.5-TP(Silvex) 01050 0.100 BQL 1.00 8151 A V. REACTIVITY 2.0 BQL 9010 D-003 Cyanide D-003 Sulfide 10.0 BQL 9030 VI. CORROSIVITY Std. Units 5.40 9045 D 00R pH Vli. TCLP,VIISCELLANEOUS Paint Filter rest NFL VIII, IGNITABILITY NVNI 1010 D-001 Ittnitability Sample Number 17319-01 Sample Date 04/08/16 Sample Time (hrs) 0745 Sample Matrix Solid BOL = Below Ouantitation Limits mgfL -milligrams per Liter = pamper million (ppm) NFL = No Free Liquids a ,¢ r t ICAL Y X z ✓r Way nt PA . 9/2712019 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-262-0017 Project Description: Winston WTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalydcaf.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) an 9/19/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 16 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated_ This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 (2) 7621 Whitepine Road, Richmond, VA 23237 Waypoint, Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 19-262-0017 Client Project Description: Winston WTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 SM-4500-NH3C WTN 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 9045D WTN 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 4500NO3F-2011 WTN 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 6010D WTN 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 SW-7471B WTN 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 SM-4500-NH3C-TKN WTN 68269 Winston WTP Solids 09/17/2019 14:00 09/19/2019 SM-254OG WIN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia Page 2 of 6 Report Number: 19-262-0017 .rs�rr C i 4ny gip', fir`: �- po Account Number: 46622 7621 Whitepine Road, Richmond, VA 23237 )int..Main $04-743-9401 ° fax BD4-271-6446 ANALY www.waypo inta nalydca I -corn Send To: Synagro Central LLC/ Technical Project, Winston WTP Mary Brewer 284 Boger Road Mocksville , NC 27028 REPORT OF ANALYSIS Date Sampled: 9/17/2019 14:00:00 Lab Number. 68259 Date Received: 09/19/2019 00:00 Sample Id : Winston WTP Date Reported: 09/27/2019 • METHOD . D Total Solids " 3.42 ADM 09/20/2019 16:38 SM-254OG Moisture * 96.60 ADM 09120/2019 16:38 SM-2540G Total ICeldahl Nitrogen 2.09 20900 250 JPJ 09/26/2019 13:00 SM-4500-NH3C-TKN Phosphorus 0.29 2870 50.0 BKN 09/24/2019 21:47 60100 Potassium 0.11 1120 50.0 BKN 09/24/2019 21:47 6010D Sulfur 0.41 4110 50.0 BKN 09124/2019 21:47 6010D Calcium 0.53 5290 250 BKN 09/24/2019 21:47 6010D Magnesium 0.17 1670 50.0 BKN 09/24/2019 21:47 6010D Sodium 0.03 302 250 BKN 09/24/2019 21:47 6010D Iron 24200 50.0 BKN 09/24/2019 21:47 6010D Aluminum 120000 500 BKN 09125/201913.37 6010D Manganese 1120 5.00 BKN 09/24/2019 21:47 6010D Copper 49.3 2.50 BKN 09/24/2019 21:47 6010D Zinc 442 12.5 BKN 09/24/2019 21:47 6010❑ Ammonia Nitrogen 0.62 6180 100 JPJ 09/26/2019 13:00 SM-4500-NH3C Organic N 1.47 14720 250 09/2612019 13:00 CALCULATION Nitrate+Nitrite-N <4.90 4.90 ZBD 09/241201915:33 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time t it: #1C 101' Y Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary to the work, the results, or the company in any advertising, news release, or other, public announcements without obtaining our prior written authorization. Agronomist Page 3 of 6 Report Number. 19-262-0017 Account Number: 46622 Send To: Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksviile , NC 27028 Lab Number: 66269 Sample Id : Winston WTP Cadmium Chromium Nickel Lead Arsenic Mercury Selenium pH * Molybdenum Comments: Waypoint.(D ANALYTICAL Project: Winston WTP REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 'Fox 804-271-6446 www.waypointanalytical.com Date Sampled: 9/17/2019 14:00:00 Date Received: 09/19/2019 00:00 Date Reported: 09/27/2019 <1.00 1.00 BKN 09/24/2019 21:47 601 OD 48.9 2.50 BKN 09/24/2019 21:47 6010D 22.9 2.50 BKN 09/24/2019 21:47 601 OD 12.6 3.00 BKN 09/24/2019 21:47 6010D 8.73 5.00 BKN 09/24/2019 21:47 601 OD 0,0332 0.0155 TJS 09/24/2019 13:43 SW-7471 B <5.00 5.00 BKN 09/24/2019 21:47 6010D 6.7 JSL 09/24/2019 06:50 9045D <2.50 2.50 BKN 09/24/2019 21:47 6010D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond holding time Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced In whole or part, nor may any reference be made to the worn, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Page 4 of 6 s: aN FAIr 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 1 Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46622 Customer Name: Synagro Central LLCI Technical Report Number: 19-262-0017 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other, ` is UPS 0 Client 0 Courier Thermometer ID: Shipping container/cooler uncompromised? ISYes 0 No Number of coolers received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No ® Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? ® Yes 0 No All samples received within holding time? ® Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved 0 Yes 0 No NIA Water - VOA vials free of headspace 0 Yes 0 No * NIA Trip Blanks received with VOAs 0 Yes 0 No 0 NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 49 N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) F- High concentration pre -weighed (methanol -14 d) F- Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes No Comments Signature: Brandi Watson Date & Time: 09119/2019 13:42.28 Page 5 of 6 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WiP 9/17/2019 91112019-1213112019 0.1709 LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (302 x 3.4200) + 100 = 10.3294 Ca mgll = (Ca mg/kg x °/a Solids) + 100 = (5290 x 3,4200) 100=180.918 Mg mg1I = (mg mg/kg x % Solids) + 100 = (1670 x 3.4200) + 100 = 57.114 Na meq = Na mg/I + Molec.Wgt.Na = 10.3284 + 23 = 0.449061 Ca meq = Ca mg/I + Molec.Wgt.Ca = 180.918 + 20 = 9.0459 Mg meq = Mg mgll+Molec.Wgt.Mg = 57.114 + 12 = 4.7595 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0,449061 + SgrRool[0.5(9.0459+4.7595)] = 0.170921 Printed: 1/22/2020 17:02 Page 1 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointa nalytica Isom 12/5/2019 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref; Analytical Testing Report Number: 19-330-0005 Project Description: Winston 2nd Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 11/2612019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, P&A iff �r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. 6 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 19-330-0005 Client Project Description: Winston 2nd Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 69698 Winston 2nd Solids 11/25/2019 13:45 11/26/2019 69698 Winston 2nd Solids 11/25/2019 13:45 11/26/2019 SM-4500-NH3C WTN 69698 Winston 2nd Solids 11/25/2019 13:45 11/26/2019 9045D WTN 69698 Winston 2nd Solids 11/25/2019 13:45 11/26/2019 4500NO3F-2011 WTN 69698 Winston 2nd Solids 11/25/2019 13:45 11/26/2019 6010D WTN 69698 Winston 2nd Solids 11/25/2019 13:45 11/26/2019 SW-74718 WTN 69698 Winston 2nd Solids 11/25/2019 13AS 11/2612019 SM-4500-NH3C-TKN WTN 69698 Winston 2nd Solids 11/25/2019 13:45 11/26/2019 SM-2540G WTN WTN: Waypoint Analytical - TN, Memphis, TN PaaP 2 of 6 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointa nalytical.com Mary Brewer Project Winston 2nd 284 Boger Road Information Mocksville , NC 27028 Report Number:19-330-0005 Lab No: 69698 Sample ID: Winston 2nd Test Moisture Test Ammonia Nitrogen Nitrate+Nitrite-N Organic N PH Total Solids Total Kjeldahl Nitrogen Phosphorus Aluminum Arsenic Calcium Cadmium Chromium Copper Iron Lead Magnesium Manganese REPORT OFANAL YSIS Results Units MQL 98.2 % 0.010 Results Units MQL 10800 mg/Kg - dry 5560 <273 mg/Kg - dry 273 23600 mg/Kg - dry 13900 6.3 S.U. 1.84 % 0.010 34400 mg/Kg dry 13900 4440 mg/Kg - dry 278 160000 mg/Kg - dry 278 <27.8 mg/Kg - dry 27.8 3670 mg/Kg - dry 1390 <5.56 mg/Kg - dry 5.56 34.2 mg/Kg - dry 13.9 65.6 mg/Kg - dry 13.9 35800 mg/Kg - dry 278 25.4 mg/Kg - dry 16.7 2110 mg/Kg - dry 278 1130 mg/Kg - dry 27.8 Qualifiers/ DF Dilution Factor Definitions MQL Method Quandtation Limit Report Date : 12/05/2019 Received : 11/26/2019 Pauric McGroary Agronomist Matrix: Solids Sampled: 11/ 25/ 2019 13:45 DF Date / Time By Analytical Analyzed Method 1 12/02/1918:43 ADM SM-2540G DF Date I Time By Analytical Analyzed Method 1 12/05/19 08:30 JPJ SM-4500-NH3C 1 12/05/19 12:05 ZBD 4500NO3F-2011 1 12/04/19 09:00 CALCULATION 1 12/03/19 07:06 JSL 9045D 1 12/02/1-918:43 ADM SM-2540G 1 12/04/19 09:00 3PJ iM-4500-NH3C-TKP 1 12/03/19 19:27 BKN 6010D 1 12103/1919:27 KKM 60100 1 12/03/19 19,27 BKN 6010D 1 12/03/19 19:27 KKM 6010D 1 12/03/19 19:27 BKN 6010D 1 12/0311919:27 BKN 6010D 1 12/03/19 19:27 BKN 6010D 1 12/03/19 19:27 KKM 6010D 1 12/03/19 19:27 BKN 6010D 1 12/03/19 19:27 KKM 6010D 1 12/03/19 19:27 BKN 6010D L Limit Exceeded ---- , -4 C h 7621 Whitepine Road, Richmond, VA 23237 Waypoit Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www,waypolntanalytical.com 46622 Synagro Central LLC/ Technical Report Date : 12/05/2019 Mary Brewer Project Winston 2nd Received, 11/26/2019 284 Boger Road Information : Mocksville , NC 27028 �Vw"' zG X 60wr Pauric McGroary Report Number :19-330-0005 REPORT OFANAL YSIS Agronomist Matrix: Solids Lab No : 69698 Sampled: 11/25/2019 13:45 Sample ID : Winston 2nd Test Results Units MQL DF Date I Time By Analytical Analyzed Method Mercury <0.850 mg/Kg - dry 0.850 1 12/04/19 15:23 KKM SW-7471B Molybdenum <13.9 mg/Kg - dry 13.9 1 12/03/19 19:27 BKN 6010D Nickel 22.3 mg/Kg - dry 13.9 1 12/03/19 19:27 BKN 6010D Potassium 2110 mg/Kg - dry 278 1 12/03/19 19:27 KKM 6010D Selenium <27.8 mg/Kg - dry 27.8 1 12/03/19 19:27 BKN 6010D Sodium <1390 mg/Kg - dry 1390 1 12/03/19 19:27 BKN 6010D Zinc 387 mg/Kg - dry 69.4 1 12/03/19 19:27 BKN 6010D Sulfur 6110 mg/Kg - dry 278 1 12/03/19 19:27 BKN 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quandtation Limit L Limit Exceeded Para 4 of 6 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 46622 Customer Name: Synagro Central LLCI Technical Report Number: 19-330-0005 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other - UPS 0 Client 0 Courier Thermometer ID: Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received I ' Custody seals intact on shipping container/cooler? n Yes 0 No 0 Not Present Custody seals intact on sample Mottles? 0 Yes 0 No 19 Not Present Chain of Custody (COC) present? Yes 0 No COG agrees with sample label(s)? 0 Yes 0 No COG properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved 0 Yes 0 No 0 NIA Water - VOA vials free of headspace 0 Yes 0 No 0 NIA Trip Blanks received with VOAs 0 Yes 0 No • N/A Soil VOA method 5035 -- compliance criteria met 0 Yes 0 No ID NIA F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes No Comments: Signature: Bran& Watson Date & Time: ,11126/2019 13:37:11 n- S _f G to w 0 M rn v� j 0 �(n 0 n: �fn r4 R a. co cn G v c w � �. CD C � Z (A Q COCD 10 (D C C O(mil a •a C 7 O ^e � 6 G 7 O D_a o �• N C (p 3 3 P D (a Al 7 (D ur (D m n I� m 33 N C: �' o l O N N M 7 9n CD Q cu ID j .n U7 V] a � n a 15 L< cr W u CD -W 1► m 3 3~3 0 (D CD CD (7 ((D C] a 0- @ C- (D SL1 N O ou �r 0 d 9z -n Ili m N 0 m r �z no m _ g m �i 0a S 0 o 0 co c r u -u O r D z t O m G) r CD L) M LNf `� o(� 0 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 1112512019 ! ! - 1 1 0.6116 LIQUID Na mg1I = (Na mg/kg x % Solids) � 100 = (1390 x 1.8400) 100 = 25.676 Ca mgll = (Ca mg/kg x % Solids) + 100 = (3670 x 1.8400) + 100 = 67.528 Mg mg/I = (mg mg/kg x % Solids) + 100 = (2110 x 1.8400) + 100 = 38.824 Na meq = Na mgll + Molec.Wgt.Na = 25.576 = 23 = 1.112 Ca meq = Ca mgll + Molec.Wgt.Ca = 67.528 = 20 = 3.3764 Mg meq = Mg mgA + Molec.Wgt.Mg = 38.824 - 12 = 3,23533 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.112 + SgrRoot[0.5(3.3764+3.23533)] = 0.611592 Printed: 1/2812020 13:25 Page i Waypointo ANALYTICAL 12/5/2019 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-330-0006 Project Description: Winston 3rd 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www,waypofntanalocal.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, ?W,. W r77� Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Pars I of 9 0 7621 Whitepine Road, Richmond, UA 23237 Waypoint Main 804-743-9401 ° Fox 804-271-6446 ANALYTICAL www.waypointanalytical.corn Sample Summary Table Report Number: 19-330-0006 Client Project Description: Winston 3rd Laic No Client Sample ID Matrix Date Collected Date Received Method — Lab ID 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 SM-4500-NH3C WTN 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 9045D WTN 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 4SOONO3F-2011 WTN 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 6010D WTN 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 SW-7471B WTN 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 SM-4500-NH3C-TKN WTN 69699 Winston 3rd Solids 11/25/2019 13:45 11/26/2019 SM-254OG WTN WTN: Waypoint Analytical - TN, Memphis, TN Pane 2 of 6 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointa n alvbcal.corn Mary Brewer Project Winston 3rd 284 Boger Road Information Mocksvilie . NC 27028 Report Number :19-330-0006 Lab No : 69699 Sample ID : Winston 3rd Test Moisture Test Ammonia Nitrogen Nitrate+ N itrite-N Organic N pH Total Solids Total Kjeldahl Nitrogen Phosphorus Aluminum Arsenic Calcium Cadmium Chromium Copper Iron Lead Magnesium Manganese REPORT OFANAL YSl'S Results Units Report Date ; 12/05/2019 Received : 11/26/2019 Pauric McGroary Agronomist Matrix: Solids Sampled: 11/ 25/ 2019 13:45 MQL DF Date I Time By Analytical Analyzed Method 97.8 % 0.010 1 12/0211918:43 ADM SM-254OG Results Units MQL DF Date lTime By Analytical Analyzed Method B270 mg/Kg - dry 4550 1 12/05/19 08:30 JPJ SM-4500-NH3C <225 mg/Kg - dry 225 1 12/05/19 12:06 ZBD 45DONO3F-2011 20500 mg/Kg - dry 11400 1 12/04/19 09:00 CALCULATION 6.3 S.U. 1 12/03/19 07:06 JSL 9045D 2.19 % 0.010 1 12/02/1918:43 ADM SM-2540G 26700 mg/Kg - dry 11400 1 12/04/19 09:00 JPJ ;M-4500-NH3C-TKO 3610 mg/Kg - dry 227 1 12/03/19 19:43 BKN 60101) 127000 mg/Kg - dry 227 1 12/03/19 19:43 KKM 6010D <22.7 mg/Kg - dry 22.7 1 12/03/19 19:43 BKN 6010D 2840 mg/Kg - dry 1140 1 12/03/19 19:43 KKM 6010D <4.55 mg/Kg - dry 4.55 1 12/03/19 19:43 BKN 6010D 27.5 mg/Kg - dry 11A 1 12/03/19 19:43 BKN 601OD 54.5 mg/Kg - dry 11.4 1 12/03/19 19:43 BKN 6010D 29100 mg/Kg - dry 227 1 12/03/19 19:43 KKM 6010D 19.1 mg/Kg - dry 13.6 1 12/03/19 19:43 BKN 6010D 1800 mg/Kg - dry 227 1 12/03/19 19:43 KKM 6010D 836 mg/Kg - dry 22,7 1 12/03/19 19:43 BKN 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Pava 3 of 6 7621 Whitepine Road, Richmond, VA 23237 WaypoiMain �t 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalyticai.eom 46622 Synagro Central LLC/ Technical Mary Brewer Project Winston 3rd Report Date : 12/05/2019 284 Boger Road Information : Received : 11/26/2019 Mocksville , NC 27028 10 �(JO7--- Pauric McGroary Report Number :19-330-0006 R,6PORT OFANALYSls Agronomist Lab No : 69699 Matrix: Solids Sample ID : Winston 3rd Sampled: 11/255/2019 13:45 Test Results Units MQt- DF Date I Time By Analytical Analyzed Method Mercury <0.686 mg/Kg - dry 0.686 1 12/04/19 15:24 KKM SW-74718 Molybdenum <11.4 mg/Kg - dry 11.4 1 12/03/19 19:43 BKN 6010D Nickel 18.0 mg/Kg - dry 11.4 1 12/03/19 19:43 BKN 6010D Potassium 1730 mg/Kg - dry 227 1 12/03/19 19:43 KKM 6010D Selenium <22.7 mg/Kg - dry 22.7 1 12/03/19 19:43 BKN 6010D Sodium <1140 mg/Kg - dry 1140 1 12/03/19 19:43 BKN 6010D Zinc 260 mg/Kg - dry 56.8 1 12/03119 19:43 BKN 6010D Sulfur 5000 mg/Kg -dry 227 1 12/03/19 19:43 BKN 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L. Limit Exceeded to4 W-a 0 ypoin i 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 *Fax 804-271-W6 www.waypointanalytical.com Shipment Receipt Form Customer Number: 46622 Customer Name: Synagro Central LLC/ Technical Report Number 19-330-0006 0 Fed Ex 0 US Postal ® UPS 0 Client Shipping Method 0 Lab 0 Other. 0 Courier Thermometer ID: Shipping container/cooler uncompromised? Yes Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes Custody seals intact on sample bottles? 0 Yes Chain of Custody (COC) present? COC agrees with sample label(s)? 10 Yes 0 Yes 1�1M 0 No i Not Present 0 No 19 Not Present 0 No 0 No COC properly completed 40 Yes 0 No Samples in proper containers? 0 Yes n Na Sample containers intact? • Yes 0 No Sufficient sample volume for indicated test(s)? ti Yes 0 No All samples received within holding time? • Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. • Yes 0 No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved 0 Yes 0 No _ Water - VOA vials free of headspace 0 Yes 0 No Trip Blanks received with VOAs 0 Yes 0 No 0 N/A 0 N/A 41 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A High concentration container (48 hr) F Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes No Comments: - �- Signature: I.Brandi Watson Date & Time: ,11/26/2019 13:38:171 n­ 9 _4, r_ SAMPLING LOG # Z A 8s L Er 'aRS. INC. j, 7621 W' (CHABN OF (CUSTODY CUSTOMER: suer® m Ri°gym° IlI�lllt111111111111�1r1llllllll�llllllll� C ANALYsus RECORD 1 r �' ao41��� earo �nlfal LLC/ Technical l��ll>fi1!l111l1� uv`nslan �s.zsz.00v 4S62z 09 PROJECT MANAGER: I ;ILK k _ .� wTp Tg za,s npling procedures "7 at these Samples. Phone: ( 33 W 7�3 �o`b � - — J - SAMPLER -- ---- A & L CUSTOMER SAMPLING SAMPLE LAB # I.D. LOCATION TYPE # OF SAMPLING CONTAINERS DATE METHOD METHOD _SAMPLE _ TIME PRESERVED SHIPPED nu,lnquisneo oy Sampler: Relinquished by: Relinquished by: SPECIAL INSTRUCTIONS: ba e Time � j Date Time Date Time 11 I /1 - d by: REMARKS: Recleved by: WWI For monitoring purposes. p0#: �3TATE) SAMPLE ANALYSIS REQUEST I.D. Organic SL8 SL2 NH4 N NO3-N N Cd Cr Ni Pb As Hg $e PH CaCO3 Volatile Mo CI NO -N equiv. Solids z SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc Page 6 of 6 SAIMP! NG LOG I; _ �.�-S' INC. _ ? CUSTOMER: SYNAG ; Svnaaro Central LLCTechnical Q 5 RECORD 13:37:50 Winston 3rd PROJECT MANAGER: _-.--_.— /L-?'� — i'as Thal the proper herd samplirrg;orocedures a used d''__ urig� t j collection of these samples. I ?1z � I :•. L L C.US' OMER SAMPLING SAMPLE OF SAMPLING MIETHOD MET110D I B SAMPLE I.D. LOC TIOrd TYPE" CONTAINERS DATE TIME PRESERVED SHIPPED J . Relinquished by Sampler r J — — J — -- Daie Time Recieved by: _ REMARKS: Rc?I6 �gLIlSiled by: - ---•-- - uS� tllllr"? Recieved by: Relinqui,";hed by: Date Tinier Recieved by � -- i j a SPECIAL INSTRUCTIONS: — purposes. S� MIPLE ANALYSIS REQUEST I.0 SL9 S-L2 Organic s N { Cd Cr } Ni I b i As lig Sc! PH i 'aCO3 VGtatile Me Cl I NO N r I equiv. Solids , I xocv �l✓ � �` �I� 77�� 7/r p I ' f a i r ✓4 i i SLI: Total Solids (Moisture), Total l<jr-idafil'N4rogen, Phlosphorus, and Potassiulll SL2: Basic irst SI_ i plus Sulfur, Calcium, MagneSlUrn, Sodium, Iron, Alurninurn. Ma"ganese, Copper and Zir-Ic Page 6 cf 6 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sam pie Date Report Range Ratio 2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 11/25/2019 ! 1 - ! 1 0.6070 LIQUID Na mg/I = (Na mglkg x % Solids) + 100 = (1140 x 2.1900) + 100 = 24.966 Ca mgll = (Ca mglkg x % Solids) + 100 = (2840 x 2.1900) + 100 = 62.196 Mg mgli = (mg mglkg x % Solids) + 100 = (1800 x 2.1900) + 100 = 39.42 Na meq = Na mg/I + Mofec.Wgt, Na = 24.966 + 23 = 1.08548 Ca meq = Ca mgll + Molec.Wgt.Ca = 62.196 20 = 3.1098 Mg meq = Mg mgll + Molec.Wgt.Mg = 39.42 4 12 = 3.285 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.08648 SgrRoo1[0.5(3.1098+3.285)] = 0,607047 Printed: 1/28/2020 13:32 Page 1 Waypointo ANALYTICAL 12/5/2019 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 19-330-0007 Project Description: Winston 4th 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 904-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 138 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certaln parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 16 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, P'_« P'a-/- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Pace 1 of 6 0 7fi21 Whitepine Road, Richmond, VA 23237 Waypoint,Main 804-743-9401 ° Fax 8o4-271-6446 ANALYTICAL www.waypointanalytical.coni Sample Summary Table Report Number: 19-330-0007 Client Project Description: Winston 4th Lab No Client Sample ID Matrix Date Collected Date Received Method — Lab ID 69700 Winston 4th Solids 11/25/2019 13:45 11/26/2019 69700 Winston 4th Solids 11/25/2019 13:45 11/26/2019 SM-4500-NH3C WTN 69700 Winston 4th Solids 11/25/2019 13:45 11/26/2019 9045D WTN 69700 Winston 4th Solids 11/25/2019 13:45 11/26/2019 450oNO3F-2011 WTN 69700 Winston 4th Solids 11/25/2019 13AS 11/26/2019 6010D WTN 69700 Winston 4th Solids 11/25/2019 13:45 11/26/2019 SW-7471B WTN 69700 Winston 4th Solids 11/25/2019 13:45 11/26/2019 SM-4500-NH3C-TKN WTN 69700 Winston 4th Solids 11/25/2019 13:45 11/26/2019 SM-2540G WTN WrN: Waypoint Analytical - TN, Memphis, TN Dana i of 9 7621 Whitep€ne Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypoi n tanalyti ca I.com Mary Brewer Project Winston 4th 284 Boger Road Information Moci<svllle , NC 27028 Report Number:19-330-0007 REPORT OFANALYSIS Lab No : 69700 Sample ID: Winston 4th Test Results Units Report Date : 12/05/2019 Received /: 11/26/2019 pwyj Pauric McGroary Agronomist Matrix: Solids Sampled: 11 / 25 / 2019 13:45 MQL DF Date ITime By Analytical Analyzed Method Moisture 98.2 % 0.010 1 12/02/1918:43 ADM SM-254OG Test Results Units MQL DF Date ITime By Analytical Analyzed Method Ammonia Nitrogen 11.400 mg/Kg - dry 5560 1 12/05/19 08:30 JPJ SM-4500-NH3C Nitrate+Nitrite-N <262 mg/Kg - dry 262 1 12/05/19 12:06 ZBD 4500NO3F-2011 Organic N 14300 mg/Kg - dry 13900 1 12/04/19 09:00 CALCULATION pH 6.3 S.U. 1 12/03/19 07:06 JSL 9045D Total Solids 1.78 % 0.010 1 12/02/19 18:43 ADM SM-254OG Total Kjeldahi Nitrogen 25700 mg/Kg - dry 13900 1 12/04/19 09:00 JPJ ;M-4500-NH3C-TKP Phosphorus 4920 mg/Kg - dry 278 1 12/03/19 19:48 BKN 6010D Aluminum 160000 mg/Kg - dry 278 1 12/03/19 19:48 KKM 6010D Arsenic <27.8 mg/Kg - dry 27.8 1 12/03/19 19:48 BKN 6010D Calcium 4520 mg/Kg - dry 1390 1 12/03/19 19:48 KKM 6010D Cadmium <5.56 mg/Kg - dry 5.56 1 12/03/19 19:48 BKN 6010D Chromium 36.7 mg/Kg - dry 13.9 1 12/03/19 19:48 BKN 6010D Copper 70.6 mg/Kg - dry 13.9 1 12/03/19 19:48 BKN 6010D Iron 36i00 mg/Kg - dry 278 1 12/03/19 19:48 KKM 6010D Lead 25.4 mg/Kg - dry 16.7 1 12/03/19 19:48 BKN 6010D Magnesium 2400 mg/Kg - dry 278 1 12/03/19 19:48 KKM 6010D Manganese 1360 mg/K9 - dry 27.8 1 12/03/19 19:48 BKN 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quandtation Limit Paqe 3 of 6 m 7621 Whitepine Road, Richmond, VA 23237 Waypoint, Main 804-743-94010 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.corn 46622 Synagro Central LLC/ Technical Report Date : 12/05/2019 Mary Brewer Project Winston 4th Received : 11/26/2019 284 Boger Road Information : Mocksville , NC 27028 ��lcc IV 6gorr� Pauric McGroary Report Number .19-330-0007 REPORT OFAIVALYSIS Agronomist Matrix: Solids Lab No: 69700 Sampled: 11/25/2019 13:45 Sample ID : Winston 4th Test Results Units MQL. DF Date/Time By Analytical Analyzed Method Mercury <0.811 mg/Kg - dry 0.811 1 12/04/19 15:25 KKM SW-7471B Molybdenum <13.9 mg/Kg - dry 13.9 1 12/03/19 19:48 BKN 6010D Nickel 23.8 mg/Kg - dry 13.9 1 12/03/19 19:48 BKN 6010D Potassium 2120 mg/Kg - dry 278 1 12/03/19 19:48 KKM 6010D Selenium <27.8 mglKg - dry 27.8 1 12/03/19 19:48 BKN 6010D Sodium <1390 mg/Kg - dry 1390 1 12/03/19 19:48 BKN 6010D Zinc 503 n)g/Kg - dry 69.4 1 12/03/19 19:48 BKN 6010D Sulfur 5720 mg/Kg - dry 278 1 12/03/19 19:48 BKN 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Para 4 of 6 Waypointe ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-Z71-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 46622 Customer Name: Synagro Central LLC/ Technical Report Number: 19-330-0007 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other . 1 41 UPS 0 Client 0 Courier Thermometer ID: �.vA Shipping container/cooler uncompromised? rp Yes 0 No Number of coolers/boxes receivedL� Custody seals intact on shipping container/cooler? 0 Yes 0 No Not present Custody seals intact on sample bottles? 0 Yes 0 No , Not Present Chain of Custody (COC) present? Yes 0 No CDC agrees with sample label(s)? Yes 0 No COC properly completed Yes 0 No Samples in proper containers? * Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? i Yes 0 No Cooler/Samples arrived at the laboratory on ice. s Yes 0 No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved 0 Yes 0 No I* N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No s N/A Soil VOA method 5035 -- compliance criteria met High concentration container (48 hr) High concentration pre -weighed (methanol -14 d Special precautions or instructions included? Comments: Signature: Brandi Watson 0 Yes 0 No 0 N/A (— Low concentration EnCore samplers (48 hr) F_ Low cone pre -weighed vials (Sod Bis -14 d) 0 Yes * No Date & Time: ,11/2612019 13:40:02 SAMPLING LOG # A & L EASTERN AGRICI-11 T o F^ 76?rt u�"°' CHAIN OF r2m�DS�f'O®�'T CUSTOMER: SYV�AGRO Ftolllllllllilll�llllllll � z ' RECORD ��® RECORD �v�°� lalllllllllllllllllllllll 8156 PROJECT '� Illlllll�lltlll 1TJ _� . _. •operfield sampling procedures MANAGER:..___. 7'. C. _ / Svnaur6C£PtralLLCITech���ai Winston Atli section of these samples. --��++77 Phone:-�._J 7>.� ` 7d 6 (� i _ - A (f �_Z— _ SA A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED Relinquished by Sampler: !"^ D to Time Recieved by: Relinquished by: — - Relinquished by: SPECIAL INSTRUCTIONS: For V�nonitoring purposes. Date Time Recieved by: ate Time Recieved by: a REMARKS: _4 cr v SAMPLE ANALYSIS REQUEST I.D. SLi 5L2 NHq N NO.-N Organic Cd Cr Ni Pb As HS Se FPH CaCO3 equi v. Volatile Solids Mo Cl NO SL1: Total Solids (Moisture), Total Kjoldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SL'1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc Page 6 of 6 Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2065-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 11/25/2019 1 1 - 1 1 0.5526 LIQUID Na mg/I = (Na mg/kg x % Solids) � 100 = (1390 x 1.7800) + 100 = 24.742 Ca mg1I = (Ca mg/kg x % Solids) = 100 = (4520 x 1.7600) = 100 = 80.456 Mg mg/I = (mg mg/kg x % Solids) + 100 = (2400 x 1.7800) + 100 = 42.72 Na meq = Na mg/l ; Molec.Wgt.Na = 24.742 _ 23 = 1.07574 Ca meq = Ca mg/l Molec.Wgt.Ca = 80.456 + 20 = 4.0228 Mg meq = Mg mg/I _ Molec,Wgt.Mg = 42.72 =12 = 3.66 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.07574 _ SgrRoot[0.5(4.0228+3.56)] = 0.552468 Printed: 1 /28/2020 Page 1 13:37 ESEARCN ANALYTiCA1 LA ORATORIES, INC. Analytical/Process Consultations May S, 2016 City of Winston-Salem Swann WTP 2800 River Ridge Road Pfafftown, NC 27040 Attention: Bill Brewer Chemical Analysis for Selected Parameters and Sampling Location Identified as Lagoon 1 (A City of Winston-Salem Swann WTI' Project, collected 08 April 201.E I. Miscellaneous 1 2 3 4 5 Parameters Unit Results Results Results Results Results Fecal Coliform MPN/g TS <2 <2 <2 <2 <2 Sample Numben 17319-02 17319-03 17319-04 17319-05 17319-06 Sample Collected Date: 04/08/16 04/08/16 04/08/16 04/08/16 04/08/16 Sample Collected Time: __ -_-- MPN/g TS = Most Probable Number per gram Total Solids Norm } rm RESEARCh & A,NA1yTICA[ TAbORATORIES, INC. CHAIN OF CUSTODY RECORD Analytical / process Consultations Phone 1336) 696-pRdj DWR Division of Water Resources State of North Carolina tal Quality io Resources 1DUANCffl"fff-RVTIFICA ION TRUCTIONS FOR FORM: RSC 6-16 Please use the following instructions as a checklist in order to ensure all requirep items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker revie time anN#ffDidQhA&Vvt of addi ional information requested. Failure to submit all of the required items will lead to a ditional���i� view time f r the permit application. Unless otherwise noted. the Applicant shall submit one Spliqtio and sunoortina documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Reoduals Source Certification (FORM: RSC 11-15): Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the /application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. [/ For new or renewed permits, submit a separate certification for each source facility. or modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. [/Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Res uals Source -Generating Facility Information: [For each source facility, attach the following: Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Matz Guidance for esiduals Land Application Permits". Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals ,afe to be generated, treated, processed, and stored at the facility. Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during rocessing. Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: M Pordach source facility, attach the following: aboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector action reduction requirements. Lid For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Winston-Salem/Forsyth County Utilities Commission (R.W. Neilson Water Treatment Plant) Status Code a Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R Swann WTP Swann WTP Forsyth WQ0031314 750 750 R Swann WTP Neilson WTP Forsyth WQ0031314 2,500 1,499 R Swann WTP Thomas WTP Forsyth WQ0031314 750 750 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: R.W. Neilson Water Treatment Plant 2. Facility permit holder is: ❑ Federal, ❑ State, 0 Local Government, or ❑ Private. Facility permit issued by: Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Bill Brewer — Water Treatment Superintendent Complete mailing address: 2800 River Ridge Road City: Pfafftown State: NC Zip: 27040-8435 Telephone number: 336) 397-7727 E-mail address: billb@cityofws.org 4. Facility physical address: 5725 Frye Bridoe Road City: Clemmons State: NC Zip: 27012 Coordinates: Latitude: N35° 59' 40.7" Longitude: W80° 21' 4" Datum: DMS Level of accuracy: 100% Method of measurement: Survey 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ❑ Yes ® No 7. Facility permitted/design flow: 48.0 MGD and facility average daily flow: 21.0 MGD 8. Average amount of residuals being generated at this facility 1,499 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: The Neilson WTP has a residuals pump station that recycles filter backwash water directly to the head of the plant. This pump station has three (3) 6.48 MGD pumps. The treatment facilities for basin residuals (heavy solids) consists of three (3) residuals lagoons for settling and drying of solids. Each lagoon has an effective storage volume of 2.1 MG's each. Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257, 2. Specify if residuals are defined under 15A NCAC 02T.1102(6} as: ❑ Biological ® Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ED no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Research & Analytical Laboratories, Inc. and Date of analysis: 3/1/2016 Passed corrosivity test: [D yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >212 OF (> 140°F) Passed reactivity test: ® yes ❑no. HCN: <250 mg/kg (<250) & H2S: <500 mg/kg (<500) TCLP Parameter Limit (Mg/1) Result (Mg/1) TCLP Parameter Limit Result (Mg/1) (mg/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 0.376 Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 0.011 Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 0.020 Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1, 1 -Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical Laboratories, Inc. and Date of analysis: 9/11/2019 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 6.54 Cadmium 85 39 0.353 Copper 4,300 1,500 44.9 Lead 840 300 27.1 Mercury 57 17 0.0846 Molybdenum 75 n/a <0.625 Nickel 420 420 22.5 Selenium 100 100 <2.36 Zinc 7,500 2,800 137 b. For Surface Disposal Unit Randfll): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical Laboratories, and Date of analysis: 9/11/2019 Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ® > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) 6.54 48.1 22.5 FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 20.8 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analvtical Laboratories. Inc. and Date of analysis: 9/11/2019 Parameter Result (mg/kg) Aluminum 112,000 Ammonia -Nitrogen 480 Calcium 1,080 Magnesium 2,440 Nitrate -Nitrite Nitrogen <21.1 pH (Standard Unit) 6.2 Phosphorus 2,500 Potassium 2,150 Sodium 1,010 Total Kjeldahl Nitrogen 1,150 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.64 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0.40 or 40 % %. This rate is a (check one): 10 default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Accepted formula for water plant residuals. e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (J.") Year PAN Five -Year Maximum Adjusted PAN (mg�kg) (m9/k9) 824 Surface 634 Injection/Incorporation N/A N/A 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N/A -Water plant residuals FORM: RSC 06-16 Page 4 of 5 7 Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Eq uivalent: ® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Applicationot Class B: ❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Colifonn Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Dis ?osal. ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item I1. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [ 15A NCAC 02T.I 106(a)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction ( VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 cc Ar lit] 1 1 mit ml, lilt t 71 d6IALL' I I 4V 36 4k .06 R.W Neilson Water Treatment Plant Water System Facility ID = TP2 Production Capacity = 48.0 MGD City of Winston-Salem NPDES # = NCO086011 Yadkin River 100.0 MGD Idol's Raw Water Pump Station Raw Water Reservoir Raw Water Reservoir Outfall 001 15.0 MG 15.0 MG ! (Currently Inactive) J 48.0 MGD 20.0 MGD Chlorine Caustic Soda/Lime 48.0 MGD ■ Alum Coagulation j Waste Pump Station V (3) 4,500 GPM Pumps Flocculation 1.15 MGD 2.0 MGD Lagoon � Residuals Lagoons Decant Sedimentation Basins ( ) (3) 2.1 MG25 Each � ~ 400 GPM Chlorine i Pumps Filtration Filter Backwash Filter to Waste Caustic Soda/Lime 48.0 MGD Fluoride 48.0 MGD Chlorine 10 Ortho-phosphate ■ 1.0 MG Clearwell 1.0 MG Clearwell ' 1.0 MG Clearwell 1.0 MG Clearwell Entry Point-EP2 Distribution System jeA) 4,el-P Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM 2.7 WASH WATER AND RESIDUALS HANDLING �ua.►� �w�� JliS� c�iati.. S,-L eu,�.� A -as ZJJ Wash Water and Residuals Handling The existing wash water and residuals generated at the WTP consist of four main flow streams: Spent wash water, Filter -to -waste, Sedimentation basin residuals, and Miscellaneous drains. The existing facilities available to process the wash water and residuals include three residuals lagoons, a lagoon decant pumping station, and a waste pumping station. The plant currently recycles the plant wash water and residuals decant to the head of the plant. In this project, the wash water and residuals handling system will change in the following ways: Abandon the practice of recycling plant wash water and residuals decant, Demolish the existing lagoon decant pumping station, Remove all existing pumps and electrical equipment from the waste pumping station. Abandon the waste pumping station in place. Cap all lines that provide flow to the existing waste pumping station, Construct new wash water equalization basin and wash water clarifier, Demolish existing inlet and decant structures in residual storage lagoons, Install new inlet structures in residual storage lagoons to receive residuals from new hoseless vacuum system and wash water clarifier, Construct new decant structures in residual storage lagoons and tie discharge decant in new wash water equalization basin, The proposed wash water and residuals handling system will consist of a new wash water equalization basin and wash water clarifier, while retaining the use of the existing residual storage lagoons. For the proposed wash water handling system, spent wash water, filter -to -waste, sedimentation basin drain, basin overflow, and miscellaneous drain flows for Neilson and East will be combined in an existing manhole upstream of the waste pumping station and discharged to the new wash water equalization basin. Each residual storage lagoon will have a new decant structure installed which will collect and convey the decant by gravity to the new wash water equalization basin. Submersible pumps in the wash water equalization basin will pump the collected wash water flows to the new wash water clarifier. The wash water equalization basin effluent will be dechlorinated in the force main before discharging to the wash water clarifier. The wash water clarifier effluent and equalization basin overflow will discharge to the creek in accordance with the existing NPDES permit. The wash water drainage system upstream of the wash water equalization basin will be designed to allow one filter to be wasted while one filter is backwashing at the design filtration rate. In addition, continuous flows from the miscellaneous drains will be discharged to the wash water equalization basin. BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2_26 Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM Residuals collected from the track vacuums and wash water clarifier will discharge by gravity to the existing storage lagoons in new inlet structures. Operations of the lagoons will not change in this project to maintain existing redundancy in the residuals storage lagoons. The existing system consists of three lagoons that are rotated for storage on an annual basis. Throughout the year, one lagoon receives residuals from the plant while the previous year's residuals air dry in the other lagoon. The third lagoon is offline and acts as a standby available for emergencies. In the lagoon that is operating, residuals are thickened throughout the year, and decant and overflow are discharged to the existing equalization basin. When a lagoon has reached its storage capacity at the end of the year, it is taken off-line for approximately one year and allowed to dry through evaporation. After one year of drying, the residuals are removed with a front-end loader and transported off -site for disposal. The remaining lagoon is off-line and remains as a standby in case of emergencies. BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-27 Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM 2.7.2 Wash Water and Residuals Flows and Solids Production Table 2-24 Wash Water and Residuals Flows Production Filter Backwash Water Per filter', gal 63,000 Avg2, gpd 378,000 Maxi, gpd 1,008,000 Filter -to -Waste Per filter4, gal 24,996 Avg2,4, gpd 149,976 Max3.4, gpd 399,936 Total Residuals Production Avgs, lb/day 8,551 Max6, lb/day 44,295 Unthickened Residuals Production (track vac+clarifier effluent to lagoons) Avg5.7, gpd 580,875 Max6.$, gpd 601,231 Thickened Residuals Production (dewatered cake) Avgs•9, gpd 7,313 Max6,9, gpd 37,846 Free Liquid from Residuals10 (lagoon decant flow to EQ) Avg, gpd 573,562 Max, gpd 563,385 Clarifier Effluent (to creek) Avg", gpd 1,229,143 Max12, gpd 2,078,570 1. Flow rate of 20 gpm/sf for six minutes and 5 gpm/sf for one minute. 2. Six filters backwashed in one day. 3. All filters backwashed in one day. 4. Flow rate of 4.13 gpm/sf for 12 minutes. 5. 267 lb/MG, using average flow rate of 32 mgd and 50th percentile turbidity. 6. 9231b/MG, using max flow rate of 48 mgd and 90th percentile turbidity. 7. 0.17 percent solids (from track vacs to EQ basin). 8. 0.88 percent solids (from track vacs to EQ basin). 9. 14.0 percent solids. 10. Unthickened residuals flow minus thickened residuals flow. 11. Pumped flowrate from wash water equalization basin to wash water clarifier under average daily conditions of six filter washes per day. 12. Pumped flowrate from wash water equalization basin to wash water clarifier under maximum daily conditions of sixteeen filter washes per day. BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-28 Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM 2.7.3 Wash Water Equalization Basin A wash water equalization basin will be provided for flow equalization of wash water prior to treatment in the wash water clarifier. Depending on the daily flow to the equalization basin, one or up to three pumps will be required to pump the contents of the basin to the wash water clarifier. An additional fourth pump will be provided as a standby. Under average daily conditions of six filter wash cycles per day, one pump is required with three standby pumps available. Under maximum daily conditions of sixteen filter wash cycles per day, two pumps are required with two standby pumps available. In the event of a sedimentation basin drain, all three pumps are required with one standby pump available. Submersible mixers will not be provided. Operations staff will be required to wash down settled solids on an as needed basis. Table 2-25 Wash Water Equalization Basin Design Parameters Number of basins Design criteria Equalization volume, gal. Basin type Basin shape Basin Dimensions Inside diameter, ft Average sidewall water depth, It Average sidewall depth, ft Slope to sump Water depth at top of sump, ft Pumps Number of pumps Rated capacity, each, gpm Rated head, ft Operating head range, ft Motor brake horsepower, bhp Flow Meter Number of units Type Size, inches Flow measurement range, mgd 1 Storage volume of 6 average filter wash cycles plus 10% 595,000 Reinforced concrete Circular 75 18 20 1:75 18.5 4 920 35 34-43 15 1 Magnetic 12 1-5 BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-29 Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM Controls Level sensors will be provided in the equalization basin for level monitoring and control of the wash water equalization pumps. Basin level will be transmitted to the PCs. At basin overflow levels in the basin, an overflow alarm will be transmitted to the PCs. Chemical Feed Point The wash water equalization basin pumps will be automatically alternated and started and stopped based on level in the wash water equalization basin. Provisions will be made to start/stop the pumps locally and from the PCs. Pump status and alarm conditions will be indicated locally and transmitted to the PCs. The signal from the flowmeter will be used by the chemical feed system for pacing of the calcium thiosulfate. The signal will be transmitted to the PCs for indication. Calcium thiosulfate will be fed at the wash water equalization basin valve vault in the clarifier influent force main. Table 2-26 Wash Water Equalization Basin Flow Conditions Average daily flow Six filter wash cycles and misc. drains Pumps required Maximum daily flow Pumps required Maximum daily flow with sedimentation basin drain Pumps required 2.7.4 Wash Water Clarifier 1 active (3 standby) Sixteen filter wash cycles and misc. drains 2 active (2 standby) Sixteen filter wash cycles, misc. drains, and sedimentation basin drain 3 active (1 standby) A new wash water clarifier will be constructed to accept wash water equalization basin effluent and treat the wash water prior to discharge in the creek. Prior to entering the plant discharge line, the wash water clarifier effluent flow will be measured in a metering manhole. These measurements will be compiled in a monthly report and sent to NCDEQ to comply with the existing NPDES permit. The residuals drain in the wash water clarifier will be exercised twice per day to send accumulated residuals to the storage lagoons. BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-30 Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM Table 2-27 Wash Water Clarifier Design Parameters COMPONENT Number of basins 1 Basin type Reinforced concrete Proposedgoo Inside wall diameter, ft 80 Inside weir diameter, ft 73.67 Sidewall water depth, ft 12 Total sidewall depth, ft 14 Water depth at center pier, ft 15.1 Floor radial slope to center loadingHydraulic 1:12 Average daily Max daily Max daily with sedimentation basin drain Detention time, hr Average daily Max daily Max daily with sedimentation basin drain Weir type Weir loading rate, gpm/ft Average daily Max daily Max daily with sedimentation basin drain Controls 0.18 0.37 0.55 8.81 4.40 2.94 Perimeter; sharp -crested, V-notch 11.54 23.08 34.61 Clarifier drive status and alarm conditions will be indicated locally and transmitted to the PCS. The clarifier residual drain valve will be opened and closed automatically either (1) based on an operator selectable cycle time set point for number of hours of plant operation or (2) a total accumulated wash water clarifier flow volume between blow -downs. In "time" mode, the PCS will open the valve for an operator -entered duration and close the valve for the remainder of the cycle. In "flow" mode, the valve open duration will be the same as the "time" mode "open duration set point". The basis for automatic control ("time" or "flow"), the cycle time set point, and the flow volume set point is entered at the PCS workstation computers. Provisions will be made to open and close the residuals drain valve locally and from the PCS. BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-31 Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM 2.7.5 Residuals Storage Lagoons and Decant Structures Each existing storage lagoon can hold all of the solids produced in one year, assuming that the design thickened residual concentration is 14% and the plant is consistently receiving median raw water turbidity based on the existing monthly operating reports. According to plant data, the existing average flowrate is 19.2 mgd. In the future, it is anticipated that the average flowrate of the plant will increase up to 32 mgd. The existing and anticipated residuals production is detailed in the table below. Table 2-28 Residuals Solids Production Filtered Flow, mgd 19.2 32 Turbidity, NTU 16.0 16.0 Coagulant, mg/L 16.8 20 Carbon (PAC), mg/L 0.17 0.84 Solids Production, ppd 4,802 8,551 Solids Production, lbs/yr 1,752,789 3,121,016 Solids Production, lb/MG 250 267 In the future, to maintain annual turnover of the storage lagoons with increased solids production, the lagoons will need to be enlarged. For lagoons 1 and 2, two additional feet will be excavated and the length of the lagoons will be extended to the north for future growth. For lagoon 3, two feet will be excavated.and the width and length will remain unchanged. The expansion and excavation of the lagoons will not be completed in this project, but the future elevations will be used for the proposed decant structure design and construction. Table 2-29 Residuals Storage Lagoons Dimensions Bottom surface area, ft2 22,498 22,617 29,506 Top surface area, ft2 36,949 36,983 43,107 Residuals depth, ft 7 7 7 Freeboard,ft 1 1 1 Available lagoon volume, gal 1,556,322 1,560,328 1,901,008 Solids storage, lbs/yr 1,817,162 1,821,839 2,219,617 BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-32 Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM 11 11 11 Bottom surface area, ft2 36,021 36,021 24,868 Top surface area, ftz 58,068 58,068 43,107 Residuals depth, ft 9 9 9 Freeboard,ft 1 1 1 Available lagoon volume, gal 3,167,036 3,167,036 3,050,718 Solids storage, ibs/yr 3,697,831 3,697,831 3,562,018 The proposed changes to the residuals handling system will require the existing residuals lines to be cut, capped, and abandoned in place. The existing inlet and decant structures will be demolished and replaced. The proposed hoseless track vacuum system will have new residuals headers installed from the sedimentation basins to the residuals storage lagoons. In the proposed inlet structure, the clarifier drain lines will discharge to the lagoons. The residuals and effluent drain lines will be isolated from each other despite sharing the same inlet structure. The proposed lagoon decant structures will include weirs and manual slide gates that can be adjusted throughout the collection year. The decant structures for the three lagoons will tie together with manholes and discharge by gravity to the wash water equalization basin. Table 2-30 Residuals Storage Lagoons Number of lagoons 3 Lagoon type Earthen lagoon with existing bentonite liner Perimeter Slope 2:1 (future) Effective storage, each lagoon, days 365 Influent 8" residuals line from track vacs and 8" clarifier drain Decant Discharge to equalization basin 2.8 CHEMICAL FEED AND STORAGE BUILDING The following chemicals are used in the existing treatment processes: sodium hypochlorite, aluminum sulfate, hydrofluosilicic acid, zinc orthophosphate, and sodium hydroxide. These chemicals, with the exception of the sodium hypochlorite holding tanks, are stored in and pumped out of the chemical storage building. Sodium hypochlorite is stored outside in an outdoor containment structure with a canopy cover. The existing floor drains located in each chemical storage room drain to the lagoons. In this project, the existing storage tanks and chemical metering pumps will be removed and replaced. A more detailed description of the Chemical Building modifications can be found in section 3.0 - Chemical Feed Design Memorandum. BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-33 R.W. Neilson Water Treatment Plant Solids Handling Plan The Neilson Water Treatment Plant is a 48 MGD water treatment facility. Solids are generated by manual sludge removal from sedimentation basins, backwashing filters, and filter -to -waste after filter backwashes are completed. Solids produced from filter backwashes and filter -to -waste is routed to a waste pump station and is then pumped to the head of the water treatment process. Solids removed from the sedimentation basins are routed directly to one of three residual lagoons. Permits and Classifications: 1. The discharge from the residuals lagoons is authorized by NPDES Permit NCO086011. The classification for the discharge is Grade 1 Physical/Chemical. 2. The distribution of the residuals removed from the lagoons is authorized by permit WQ0031314. The residuals are classified as Class A. Operation: 1. The system consists of a waste station with (3) Fairbanks Morse single stage pumps rated at 6.48 MGD each, (2) Fairbanks Morse basin sludge pumps rated at 1.0 MGD each, (2) lagoon pumps rated at 0.65 MGD each and (3) residuals lagoons (3 lagoons at —2.0 MG). Each residuals lagoon consists of an oval earthen lagoon with clay bottom. 2. Routine inspections of equipment will be conducted Senior Utility Plant Supervisor to ensure proper operation of equipment. Any equipment not functioning properly will be reported through the water division's asset management program, MAXIMO, to the appropriate support group for repair/replacement. 3. Backwash and filter -to -waste water from the plant process flows to the waste station and then is pumped by the waste station pumps to raw water reservoirs at the head of the plant treatment process. 4. All sedimentation basin and hopper blow downs are pumped by the basin sludge pumps directly to one of three residuals lagoons. The solids stream enters on one end of each lagoon and decant is pumped from the opposite end by the lagoon pumps to the waste station where it is returned to the head of the treatment process. 6. Residuals lagoons are rotated with one cleaned and ready for use, one in service and one drying at all times. R.W. Neilson Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 7. Residuals are removed from the lagoons and hauled to the application site by a private contractor. Monitoring and Reporting Requirements: 1. Residuals generated by each source -generating facility must be analyzed to demonstrate that they are non -hazardous based on the most current permit requirements (Attachment A). Sampling will be conducted under supervision of the Senior Water Treatment Plant Supervisor by WSFC Utilities current contractor as described below in compliance with permit requirements. 2. Analysis will be performed by a NC Certified Laboratory. 3. Analyses made according to monitoring and reporting requirements must be certified for the required parameter(s). 4. Corrosivity, ignitability, reactivity, and a Toxicity Characteristics Procedure analysis are required once each permit cycle. The TCLP analysis includes the following parameters (i.e., note the regulatory level in milligrams per liter in parentheses): Arsenic (5.0) Barium (100.0) Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) m-Cresol (200.0) o-Cresol(200.0) p-Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene(7.5) 1,2-Dichloroethane (0.5) 1, 1 -Dichloroethylene (0.7) 2,4-Dinintrotolulene (0.13) Endrin (0.02) Hexachlorobenzene(0.13) Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lead (5.0) Lindane (0.4) Mercury (0.2) Methoxychlor (10.0) Methyl ethyl ketone (200.0) Nitrobenzene (2.0) Pentachlorophenol (100.0) Pyridine (5.0) Selenium (1.0) Silver (5.0) Tetrachloro ethylene (0.7) Toxaphene (0.5) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2) 5. Analyses of the following parameters are also required with each application event: Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Phosphorous Potassium pH Plant Available Nitrogen (by calculation) Selenium Sodium % Total Solids TKN Zinc 6. Data to verify pathogen reduction and vector attraction reduction of the residuals is maintained on file for five years. The required data is specific to the stabilization process utilized, and is also sufficient to demonstrate clear compliance with the Class A pathogen R.W. Neilson Water Treatment Plant Solids Handling Plan -Permit 4WQ031314 Revised 07/14/2020 2 requirements and restrictions noted in 15A NCAC 02T .1106 (a) and (b) and vector attraction reduction requirements in 15A NCAC 02T .1107 (a). 7. Proper records are maintained tracking all residuals activities. These records include the source, volume, analysis, and recipient of the residuals. 8. Three copies, per application event, of all required monitoring and reporting requirements are submitted annually before March 1, to NC DEQ-DWQ. Performance Standards: The pollutant concentrations in any residuals that are land applied to any land application site shall not exceed the following Ceiling and Monthly Average Concentrations (i.e. dry weight basis): Parameter Monthly Average Concentration milligrams per kilo,i am)(milligrams Ceiling Concentration per kilogram) Arsenic 41 75 Cadmium 39 85 Copper 1,500 4,300 Lead 300 840 Mercury 17 57 Molybdenum n/a 75 Nickel 420 420 Selenium 100 100 Zinc 2,800 7,500 2. If residuals are sold or given away, one of the Class A pathogen requirements in 15A NCAC 02T .I 106(b) must be met. Application Requirements: 1. Bulk residuals are not applied under the following conditions: i. If the residuals are likely to adversely affect a threatened or endangered species. ii. If the application causes prolonged nuisance conditions. iii. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards. iv. If the land is flooded, frozen, or snow-covered or is otherwise in a condition such that runoff of the residuals would occur. v. During a precipitation event or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. vi. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following the residuals application event. R.W. Neilson Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 vii. During a precipitation event or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. viii. If the slope of the land is greater than 10 percent when the bulk residuals are surface applied, and if the slope of the land is greater than 18 percent when bulk residuals are injected or incorporated. ix. If pH maintained in the soil and residuals mixture is greater than 6.0. x. If the land does not have an established vegetative cover. xi. If the vertical separation of the seasonal high water table and the depth of the residuals application is less than one foot. xii. If the vertical separation of the depth to bedrock and the depth of residuals application is less than one foot. xiii. Application exceeds agronomic rates. xiv. For residuals treatment and storage facilities, the following minimum setbacks shall be adhered to: Minimum Setback Description of Setback (feet) Habitable residence or place of public assembly under separate ownership or not to be maintained as part of the project site 100 Property lines 50 Private or public water supply 100 Surface waters (streams, -intermittent and perennial, perennial water bodies, and wetlands) 50 Wells with exception to monitoring wells 100 2. When land applying bulk residuals to application site, the following minimum setbacks are maintained at all times: Setback By Type of Residual feet Description of Setback Liquid Cake Private or public water supply 100 100 Surface waters (streams -intermittent and perennial, perennial water bodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where bottom of The ditch intersects SHWT) 25 0 Subsurface groundwater lowering astern Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 3. Specific bulk residuals land application area boundaries are clearly marked on each land application site prior to and during a residuals land application event. 4. Bulk residuals and other sources of PAN (Plant Available Nitrogen) are applied to all land application sites at or below agronomic rates. Appropriate agronomic rates are calculated R.W. Neilson Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 4 using expected nitrogen requirements based on the Realistic Yield Expectations (RYE) field cover for each approved land application site. Spills and Noncompliance Notification: 1. The Winston-Salem Regional Office, telephone number (336) 771-5000, will be notified within 24 hours or the next working day following the occurrence or first knowledge of the occurrence of any of the following: i. Any occurrence with the distribution program which results in the land application of significant amounts of wastes which are abnormal in quantity or characteristic. ii. Any failure of the distribution program resulting in a release of materials to receiving waters. iii. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. 2. Persons reporting such occurrences by telephone shall also file a written report in letter form within (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. 3. Emergency Contacts: Neilson Water Treatment Plant (336) 766-9885 (Main) Gabriel Sparks, Plant Supervisor (336) 747-7471 (0) (336) 944-1222 (M) Bill Brewer (336) 397-7727 (0) Water Treatment Superintendent (336) 745-5277 (M) Winston-Salem/Forsyth County (336) 727-8418 Utility Administration DEQ Regional Office (336) 771-5000 General Emergency 911 HazMat R.W. Neilson Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 5 RESEARCh & lANAlyT7CAI LAboRAToFtks, INC. AnaWloal/Process Consultations Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Neilson WTP _(A City of Winston-Salern Neilson WTP Project collected 011VIarch 2016 Nelson WTP EPA HW Quantitating Results Characteristic Number Contaminant Lita(t(msrll.) {melt.) LavellmWL) EPA Method i. TCLP METALS 1:1.004 Aronle 0.0I0 BQL S.00 6010C 1) Barium 0.040 0.376 100 6010C 1)•006 Cadmium 0.005 BQL 1.00 6010C D-077 Chromium 0.010 0.020 5.00 6010C D-008 Lead 0.60S 06011 5.00 601DC 13-009 Mercury 0.0020 BQL 0,200 7470A D•010 selenlum 0.100 BQL 1.00 6010C D-01I Silver 01010 BQL 5,00 6010C IL TCLP VOLATILES D-018 Benzene 0.050 BQL 0.500 8260B D-019 Carbon Tetrachloride 0.050 BQL 0.500 82609 D-021 Chlorobenzene 0.030 BQL too 8250B D-022 Chloroform 0.500 BQL 6.00 8260B D-028 1,2-Dichlomthnne 0.050 BQL 0,500 8260E D-029 1,i-Dichloroethytene 0.050 BQL 0.700 8260E D-035 Methyl Ethyl Ketone 0.5u0 BQL 200 8260E D-039 Tetmehlomethylene 0.050 BQL 0.700 8260B D•040 Trichlemethylene 0.050 BQL 0.500 8z6OB D-043 Vinyl Chlodde 0.050 BQL 0.200 9260B I[I� TCLF SEMI-VULATILES D-023 (I -Creosol 20.0 BQL 200 8270D D-024 M-Creosol 2010 BQL 200 82701) D-025 p-Crcosol 2010 BQL 200 817013 D-026 Creosol 20.0 BQL 20D 8270D D-027 1,4-Dichlorobenzene 0.750 BQL 7.50 8270D D-030 2,40nitrotoluene 0.050 BQL 0.130 8270D D-032 Hexachlorobenzene 0.050 BQL 0.Do 8270D D-035 Hexaehlorobutadiene 050 BQL 0.500 8270D D•034 Hexachloroethane 0.300 BQL 3.OD 8270D 1)•036 Nitrobemzeno 0.200 BQL 2.0D MOD D-037 Pentachlarophenol 10.0 BQL too 9270D D-038 Pyridine 0.500 BQL 5.00 8270D D-041 2,4,5-Trichloruphenol 40.0 BQL 400 8270D D-042 2,4,6-Trich1orophenol 0.200 BQL 2.00 8270D iv. TCLP PLSTICIDESl01il111CIDES 0.003 BQL 0.030 BOB] B D-020 D-016 Chlordane 2,4-D 1.000 BQL 10.0 B15I A D-012 Endrin 0.002 SQL 0.020 8091 B D-031 Heptachlor 0.0008 BQL 0.008 8031 B D-013 Lindane 0.040 BQL 0.400 8081 B D-014 Medwxyahlor 1-000 BQL 1010 8081 B D-015 Toxaphene 0.050 BQL 0.500 8081 B D-017 2A5-TP(Silvex) 0.100 BQL 1.00 8151 A V. REACTIVITY 0-003 Cyanide 2.0 BQL 9010 D-003 Sulfido 10.0 BQL 9030 VL CORROSIVITY D-002 pH Std. Units i.30 9045 VII. TCLPMiscELLANEOUS Paint Filter Test NFL VIILIGNITABILITY D-001 Ipnitability WNI 1010 Sample Number 15606-08 Sample Date 03/01/16 Sample Time (hrs) 0800 Sample Matrix Solid BQL = BelowQuentitationLimiu rnWL cmiltigcamaper Liter =parts per million (ppm) NFL No Fret Liquids Waypoint,o ANALYTICAL 5f7/2019 EMA Resources Inc Brent Collins 755 Yadkinviile Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 19-116-0282 Client Project Description: Neilson WTP 2790 Whitten Road, Memphis, TN 38133 Main 901.213,24001 Fax 901.213.2440 www.waypointa nalytical. com Dear Brent Collins: Waypoint Analytical, LLC. received sample(s) on 4/26/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be heldiare available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulflte...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysls(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability In any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Alabama #40750 Louisiana #04015 mississippi California #2904 Kentucky #90047 Tennessee #TN02027 •=�>"1 FP s e VA NELAP 4460181 NC #415 EPA #TN00012 Texas #TI04704180 Arkansas #88-0650 Oklahoma #9311 5C #84002 Kentucky UST #80215 PA DEP #68-03195 Page 1 of 13 d .a- Waypoinx- ANALYTICAL Client: EMA Resources Inc Project: Neilson WTP Lab Report Number: 19-116-0282 Date: 5/7/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400" Fax 901.213.2440 www.waypointanalytica Isom CASE NARRATIVE Metals Analysis Method 601 OD Analyte: Aluminum QC Batch No: L434240 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Calcium QC Batch No: L434067 MS/MSD Recovery failed, DT confirmed matrix interference Analyte: Iron QC Batch No: L434240 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Potassium QC Batch No: L434240 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Magnesium QC Batch No: L434067 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was not within the method limits. Matrix interference is suspected. Analyte: Manganese QC Batch No: L434067 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was not within the method limits. Matrix Interference is suspected. Analyte: Molybdenum QC Batch No: L434067 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Analyte: Lead QC Batch No: L434067 Page 2 of 13 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901,213.2400 0 Fax 901.213.2440 www.waypointanalytical.com The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was performed and the recovery was not within the method limits. Matrix interference is suspected. Analyte: Selenium QC Batch No: L434067 The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was performed and the recovery was within the method limits. No matrix interference is suspected. Page 3 of 13 P WlJFpainry 2790 Whitten Road, Memphis, TN 38133 ® a Main 901.213.2400 0 Fax 901.213.7440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Brent Collins Project Neilson WTP Report Date: 05/07/2019 755 Yadkinville Rd Information : Received : 04/26/2019 Macksville , NC 27028 Report Number :19-116-0282 REPORTOFANALYSIS Danyale Love Project Manager Lab No : 92234 Sample ID: Neilson WTP #'1 Matrix: Solids Sampled: 4/25/2019 8:30 Test Results Units MDL MOL DF Date I Time By Analytical Analyzed Method % Moisture 78.4 % 0,010 1 04/26/19 16:25 ADM SW-DRYWT Ammonia Nitrogen 284 mg/Kg - dry 116 1 05/06/19 15:00 JPJ 4500NH3C-2011 Nitrate+ N itrite-N 75.9 mg/Kg - dry 21.5 21.5 1 05/03/19 12:45 ZBD 4500NO3F-2011 Organic N 5050 mg/Kg - dry 323 1 05/06/19 15:00 CALCULATION pH 7.1 s.u. 1 05/06/19 07:11 JSL 9045D Total Solids 21.6 % 0.010 0.010 1 04/26/19 16:25 ADM 2540G-2011 Total Volatile Solids 25.1 % 0.010 0.010 1 04/26/19 16:25 ADM 254OG-2011 Total Kjeldahl Nitrogen 5320 mg/Kg - dry 323 1 05/07/19 14.22 CLP 4500NORGD-2011 Phosphorus 2990 mg/Kg - dry 11.9 23.1 1 05/01/19 22:34 BKN 6010D Aluminum 117000 mg/Kg - dry 94.0 231 10 05/02/19 13:57 BKN 6010D Arsenic 6.67 mg/Kg - dry 1.94 2.31 1 05/01/19 22:34 BKN 6010D Cadmium <0.229 mg/Kg - dry 0.229 0.463 1 05/01/19 22:34 BKN 6010D Calcium 861 mg/Kg - dry 77.8 116 1 05/01/19 22:34 BKN 6010D Chromium 35.0 mg/Kg - dry 0.879 1.16 1 05/01/19 22:34 BKN 6010D Copper 34.6 mg/Kg - dry 0.671 1.16 1 05/01/19 22:34 BKN 6010D Iron 3280D mg/Kg - dry 1916 23.1 1 05/01/19 22:34 BKN 6010D Lead 23.1 mg/Kg - dry 0.689 1,39 1 05/O1/19 22:34 BKN 6010D Magnesium 1500 mg/Kg - dry 10.3 23.1 1 05/01/19 22:34 8KN 6010D Manganese 359 mg/Kg - dry 0.847 2.31 1 05/01/19 22:34 BKN 60101) Mercury 0.0912 mg/Kg - dry 0,0150 0.0681 1 05/02/19 11:25 KKM 7471A Molybdenum 0.787J mg/Kg - dry 0,601 1.16 1 05/01/19 22:34 BKN 6010D Nickel 16.2 mg/Kg - dry 0.763 1.16 1 05/O1/19 22:34 BKN 6010D Potassium 1440 mg/Kg - dry 13.8 23A 1 05/01/19 22:34 BKN 6010D Qualifiers/ B Analyte detected in blank DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit Page 4 of 13 O W point, ay ANALYTICAL 46245 EMA Resources Inc Brent Collins 755 yadkinville Rd Mocksville , NC 27028 Report Number :19-116-0282 Lab No: 92234 Sample ID : Neilson WTP #1 Test Selenium Sodium Zinc Sulfur Sodium Absorption Ratio Qualifiers/ B Definitions I 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waygointanalytical.com Project Neilson WTP Information : REPORT OFANALYSIS Results Units MOL Report Date : 05/07/2019 Received : 04/26/2019 0C"'6&s� Q�-a Danyale Love Project Manager Matrix: Solids Sampled: 4/25/2019 8:30 MQL DF Date I Time By Analytical Analyzed Method <2.27 mg/Kg - dry 2.27 2.31 1 05/O1/19 22:34 BKN 6010D <357 mg/Kg - dry 357 1160 10 05/02/19 13:57 BKN 6010D 96.3 mg/Kg - dry 5.00 5.79 1 05/01/19 22:34 BKN 6010D 2780 mg/K9 - dry 22.6 23.1 1 05/01/19 22:34 BKN 6010D <5.00 Ratio 5.00 1 05/01/19 22:34 CALCULATION Analyte detected in blank Estimated value OF Dilution Factor MQL Method Quantitation Urnit Page 5 of 13 0 2790 Whitten Road, Memphis, TN 38133 Waypoint.Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Brent Collins Project Neilson WTP Report Date : 05/07/2019 755 Yadkinville Rd Information: Received: 04/26/2019 Mocksville , NC 27028 Report Number: 19-116-0282 Lab No : 92235 Sample ID : Neilson WTP #2 REPORTOFANALYSlS a Love Proect Manager Project Matrix: Solids Sampled: 4/25/201.9 8:30 Test Results Units MDL MOL DF Date/Time By Analytical Analyzed Method % Moisture 78.7 % 0.010 1 04/26/19 16:25 ADM SW-DRYWT Ammonia Nitrogen 445 mg/Kg - dry 117 1 05/06/19 15:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 54.0 mg/Kg - dry 22.9 22.9 1 05/03/19 12:45 ZBD 4500NO3F-2011 Organic N 5120 mg/Kg - dry 245 1 05/06/19 15:00 CALCULATION - pH 6.6 S.U. 1 05/06/19 07:11 JSL 9045D Total Solids 23.8 % 0.010 0.010 1 04/26/19 16:25 ADM 254OG-2011 Total Volatile Solids 24.9 % 0.010 0.010 1 04/26/19 16:25 ADM 254OG-2011 Total Kjeldahl Nitrogen 5540 mg/Kg - dry 245 1 05/07/19 14:23 CLP 4500NORGD-2011 Phosphorus 2590 mg/Kg - dry 12.1 23.5 1 05/01/19 22:39 BKN 6010D Aluminum 140000 mg/Kg - dry 95.3 235 10 05/02/19 14:02 BKN 6016D Arsenic 7.46 mg/Kg - dry 1.97 2.35 1 05/01/19 22:39 BKN 6010D Cadmium 0.3713 mg/Kg - dry 0.232 0.469 1 05/01/19 22:39 BKN 6010D Calcium 869 mg/Kg - dry 78.9 117 1 05/01/19 22:39 BKN 6010D Chromium 60.6 mg/Kg - dry 0.892 1.17 1 05/01/19 22:39 SKN 6010D Copper 50.7 mg/Kg - dry 0.681 1.17 1 05/01/19 22:39 BKN 6010D Iron 6060D mg/Kg - dry 199 235 10 05/02/19 14:02 BKN 6010D Lead 37.2 mg/Kg - dry 0.699 1.41 1 05/01/19 22:39 BKN 6010D Magnesium 2330 mg/Kg - dry 10.4 23.5 1 05/01/19 22:39 BKN 6010D Manganese 402 mg/Kg - dry 0.859 2.35 1 05/01/19 22:39 BKN 6010D Mercury 0.0859 mg/Kg - dry 0.0160 0.0723 1 05/02/19 11:27 KKM 7471A Molybdenum 1.27 mg/Kg - dry 0.610 1.17 1 05/01/19 22:39 BKN 6010D Nickel 26.9 mg1Kg - dry 0.774 1.17 1 05/01/19 22:39 BKN 6010D Potassium 2310 mg/Kg - dry 14.0 23.5 1 05/01/19 22:39 BKN 6010D Qualifiers/ B Analyte detected in blank Definitions J Estimated value DF Dilution Factor MQL Method Quantitation Limit Page 6of13 e 2790 Whitten Road, Memphis, TN 38133 Waypoint. Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Project Neilson VdTP Report Date : 05/07/2019 Brent Collins Received : 04/Z6/2019 755 Yadkinvilie Rd Information : Mocksville , NC 27028 Danyale Love Report Number :19-116-0282 REPORT OFANAL YSIS project Manager Matrix: Solids Lab No: 92235 Sampled; 4/25/2019 8:30 Sample ID: Neilson WTP #2 Test Results Units MQL MQL DF Date I Time By Analytical Analyzed Method Selenium <2.30 mg/Kg - dry 2.30 2.35 1 05/01/19 22:39 BKN 6010D Sodium <362 mg/Kg - dry 362 1170 10 05/02/19 14:02 BKN 6010D 144 mg/Kg -dry 5.07 5.87 1 05/01/19 22:39 BKN 6010D Zinc Sulfur 3030 mg/Kg - dry 23.0 23.5 1 05/O1/19 22:39 8KN 60100 Sodium Absorption Ratio <5.00 Ratio 5.00 1 05/01/19 22:39 CALCULATION Qualifiers/ B Anaiyte detected in blank Definitions 3 Estimated value DF Dilution Factor MQL Method Quantitation Limit Page 7 of 13 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number :19-116-0282 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 w w w.wa y p o i n t a n a lyti ca I -co m Project Neilson WTP Information : REPORT OFANALYSiS Report Date: 05/07/2019 Received : 04/26/2019 00,'6acb Q�.a Danyale Lave Project Manager Lab No : 92236 Matrix: Solids Sample ID :!Neilson WTP #3 Sampled: 4/25/2019 8:30 Test Results Units MDL MQL DF Date lTime By Analytical Analyzed Method %Moisture 70.4 °/a 0.010 1 04126/1916:25 ADM SW-DRYWT Ammonia Nitrogen 358 mg/Kg - dry 84.5 1 05/06/19 15:00 IP] 4500NH3C-2011 Nltrate+Nltrite-N 47.3 mg/Kg - dry 15.7 15.7 1 05/03/19 12:46 ZBD 4500NO3F-2011 Organic N 3990 mg/Kg - dry 281 1 05/06/19 15:00 CALCULATION pH 6.4 SM. 1 05/06/19 07:11 JSL 9045D Total Solids 29.6 % 0.010 0.010 1 04/26/19 16:25 ADM 254OG-2011 Total Volatile Solids 22.5 % 0.010 0.010 1 04/26/19 16:25 ADM 2540G-2011 Total Kjeldahl Nitrogen 4360 mg/Kg - dry 281 1 05/07/19 14:24 CLP 4500NORGD-2011 Phosphorus 2070 mg/Kg - dry 8.68 16.9 1 05/01/19 22:44 BKN 6010D Aluminum 1.16000 mg/Kg - dry 68.6 169 10 05/02/19 14:07 BKN 6010D Arsenic 7.26 mg/Kg - dry 1.42 1.69 1 05/01/19 22:44 BKN 6010D Cadmium 0.378 mg/Kg - dry 0.167 0.338 1 05/01/19 22:44 BKN 6010D Calcium 652 mg/Kg - dry 56.8 84.5 1 05/01/19 22:44 BKN 6010D Chromium 44.3 mg/Kg - dry 0.641 0.844 1 05/01/19 22:44 BKN 6010D Copper 37.8 mg/Kg - dry 0.490 0,845 1 05/01/19 22:44 BKN 6010D iron 49300 mglKg - dry 143 169 10 05/02/19 14:07 BKN 6010D Lead 28.7 mg/Kg - dry 0.503 1.01 1 05/01/19 22:44 BKN 6010D Magnesium 2040 mg/Kg - dry 7.50 16.9 1 05/01/19 22:44 BKN 6010D Manganese 588 mg/Kg - dry 0.618 1.69 1 05/01/19 22:44 BKN 6010D Mercury 0.0912 mg/Kg - dry 0.0114 0.0514 1 05/02/19 11:28 KKM 7471A Molybdenum 1.05 mg/Kg - dry 0.439 0.844 1 05/01/19 22:44 BKN 6010D Nickel 19.7 mg/Kg - drY 0.557 0.844 1 05/01/19 22:44 BKN 6010D Potassium 1950 mg/Kg - dry 10.1 16.9 1 05/01/19 22:44 BKN 6010D Qualifiers/ 8 Analyte detected in blank DF Dilution Factor Definitions J Estimated value MQL Method Quantitation Limit Page 8 of 13 46245 EMA Resources Inc Brent Collins 755 yadkinville Rd Mocksville , NC 27028 Report Number :19-116-0282 Lab No: 92236 Sample ID : Neilson WTP #3 Test Selenium Sodium Zinc Sulfur Sodium Absorption Ratio ww" 2790 Whitten Road, Memphis, TN 38133 Main 901,213.2400 0 Fax 901.213.244D www.waypointa nalyti cal.com Project Neilson WTP Report Date : 05/07/2019 Information : Received ; 04/2612019 Q'" Danyale Love REpORTOFANALY.SIS project Manager Matrix: Solids sampled: 4/25/2019 8,30 Results units MDL MQL DF Date 1 Time By Method l Analyzed <1.66 mg/Kg - dry 1.66 1.69 1 05/01/19 22:44 BKN 6010D <261 mg/Kg - dry 261 845 16 05/02/19 14:07 BKN 6010D 106 mg/Kg - dry 3.65 4.22 1 05/01/19 22:44 BKN 6010D 2470 mg/Kg - dry 16.5 16.9 1 05/01/19 22:44 BKN 6010D <5.00 Ratio 5.00 1 05/01/19 22:44 CALCULATION DF Dilution Factor Qualifiers/ B Analyze detected in blank MQL Method Quantization L"smit Definitions 7 Estimated value Page 9 of 13 0 Waypoinic- 2790 Whitten Road, Memphis, TN 38133 Main 901,213.2400 1 Fax 901.213.2440 ANALYTICAL. www.waypointanalytical.com 46245 EMA Resources Inc Brent Coffins Project Neilson WTP Report Date: 05/07/2019 755 Yadkinville Rd Information: Received : 04/26/2019 Mocksville , NC 27028 Report Number :19-116-0282 Lab No : 92237 Sample ID : Neilson WTP #4 Test RrPORTOFANALYSIS Danyale Love Project Manager Matrix: Solids Sampled: 4/25/2019 8:30 Results Units MDL MQL DF Date i Time By Analytical Analyzed Method % Moisture 71.7 % 0.010 1 04/26/19 16:25 ADM SW-DRYWF Ammonia Nitrogen 392 mg/Kg - dry 88.3 1 05/06/19 15:00 JPJ 4500NH3C-2011 Nitrate+Nftrite-N 32.0 mg/Kg - dry 17.7 17.7 1 05/03/19 12:47 ZBD 4500NO3F-2011 Organic N 4060 mg/Kg - dry 248 1 05/06/19 15:00 CALCULATION - pH 5.9 s.u. 1 05/06/19 07:11 ISL 9045D Total Solids 28.3 % 0.010 0.010 1 04/26/19 16:25 ADM 254OG-2011 Total Volatile Solids 23.3 % 0.010 0.010 1 04/26/19 16:25 ADM 254OG-2011 Total Kjefdahl Nitrogen 4450 mg/Kg - dry 248 1 05/07/19 14.25 CLP 4500NORGD-2011 Phosphorus 2210 mg/Kg - dry 9.08 17.7 1 05/01/19 22:50 BKN 6010D Aluminum 118000 mg/Kg - dry 71.7 177 10 05/02/19 14:12 BKN 6010D Arsenic 7.81 mg/Kg - dry 1.48 1.77 1 05/01/19 22:50 BKN 6010D Cadmium 0.382 mg/Kg - dry 0.175 0.353 1 05/01/19 22:50 BKN 6010D Calcium 809 mg/Kg - dry 59.4 88.3 1 05/01/19 22:50 BKN 6010D Chromium 43.5 mg/Kg - dry 0,671 0.883 1 05/01/19 22:50 BKN 6010D Copper 37.8 mg/Kg - dry 0.512 0.883 1 05/01/19 22:50 BKN 6010D Iron 47700 mg/Kg - dry 150 177 10 05/02/19 14:12 BKN 6010D Lead 29.1 mg/Kg - dry 0.526 1.06 1 05/01/19 22:50 BKN 6010D Magnesium 1880 mg/Kg - dry 7.84 17.7 1 05/01/19 22:50 BKN 6010D Manganese 537 mg/Kg - dry 0.646 1.77 1 05/01/19 22:50 BKN 6010D Mercury 0.0746 Ong/Kg - dry 0.0123 0.0555 1 05/02/19 11:29 KKM 7471A Molybdenum 0.985 mg/Kg - dry 0.459 0.883 1 0S/01/19 22:50 BKN 6010D Nickel 19.5 mg/Kg - dry 0.583 0.883 1 05/01/19 22:50 BKN 6010D Potassium 1780 mg/Kg - dry 10.5 17.7 1 05/01/19 22:50 BKN 6010D Qualifiers/ B Analyte detected in blank DeFnitions J Estimated value DF Dilution Factor MQL Method Quantitation Limit Page 10of13 �4�,�Y,�7. v Waypoint`-- ANALYTICAL 46245 EMA Resources Inc Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number :19-116-0282 Lab No : 92237 Sample ID : Neilson WTP #4 Test 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointa nalyti cal. com Project Neilson UUTP Information : REPORT OFANALYSIS Results Units MDL Report Date : 05/07/2019 Received -�((: 0,�,4�/.2}612019 Q� `,R7�ti Danyale Love Project Manager Matrix: Solids Sampled: 4/25/2019 8:30 MOIL OF Date / Time By Analytical Analyzed Method <1.73 mg/Kg - dry 1.73 1.77 1 05/01/19 22:50 BKN 6010D Selenium <273 mg/Kg - dry 273 863 10 05/02/19 14:12 BKN 6010D Sodium 1.08 mg/Kg - dry 3.82 4.42 1 05/01/19 22:50 BKN 6010D Zinc 2590 mg/Kg - dry 17.3 17.7 1 05/01/19 22:50 BKN 6010D Sulfur Ratio 5.00 1 05/01/19 22:50 CALCULATION Sodium Absorption Ratio <5.00 Qualifiers/ B Analyte detected in blank Definitions DF Dilution Factor Page 11 of 13 Wayo ', ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.7-400 1 Fax 901.713.2440 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 19-116-0282 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other: 0 UPS 0 Client 0 Courier Thermometer ID: Fi5 Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Required Custody seals intact on sample bottles? 0 Yes 0 No Not Required Chain of Custody (COC) present? COC agrees with sample label(s)? COC properly completed 0 Yes • Yes is Yes 0 No 0 No 0 No Samples in proper containers? it Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved Water - VOA vials free of headspace Trip Blanks received with VOAs Soil VOA method 5035 — compliance criteria met 0 Yes 0 Yes 0 Yes 0 Yes 0 No 0 No 0 No 0 No 0 NIA * N/A N/A �* N/A F High concentration container (48 hr) F Low concentration EnCore samplers (48 hr) F— High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes No Comments: Signature: oryPhillips _ Date & Time: 4/26/2019 13:35:27 Page 12of13 ME Client Name/Address Client Project Manager/Contact Sitting Information For laboratory Use Only EMA Resources Inc Brent Collins Account #46245 755 YadkinAlle Rd Mocksville, NC27028 Mf 1l['�I I 111` 1`j'�V�` j�j�� Il Project Description Project/site location (City/State) RUSH —Additional charges apply Special Detection Unilt(s) L k �lilll[ I+ iter 1�l11 1 1��� 11111111 11��� Date Results Needed I" l_ 111H ul `u ��Z6620192 I —Oil Eh1AResources Ine 13:32:42 Pu. Neilson WTP Project Number Project Manager Phone 0 Project Manager Email 336-399-3646 brent.callins@emaresources.com A Coal a 10C Na2S203 (Mlao Only) ��as /�a aypoInt_ m _CD a 0 Q C G Cool a=GC G H7SOaPHGi 1P ANALYTICAL A c Y $ a E [7 O E t0 D D None Required E NaOH pHa10 2790 Whitten Road Unless noted, all carttainers •S u to m ¢ z 43 ca T \ F HNO3pH.2 G HCLpHeI Memphis, TN 38133 V a is — H (9U1) 213-2400 per Table II of 40 CFR Part Z l� lr� U cad c_6C NAZS203 136. 3 z m 4` Time Sample Identification Required Analysis / Prese•rva9wo Comments/Notes Ne;1-4 �lC }(Metals:AI,As,Ca,Cd,Cr,Cu,Fe,Pb 912;5 t!z C }C Mn,M9,Mo,H9,Ni,Se,Na,P,S,K,Zn 3 1 y%25 A cl I G is X X X For Laboratory Use Only Sam Lb;V7INa e—Print) 21ii Client Remarks/Comments Sludge SamplesReport Dry Weight Ice CSeals LahGomments �y�Seals N X R TU E) Date Time Received by. {SIGNATURE) Date rime V Y t Rel aq shed by. (SIGNATURE) , J thank% oolerTe ti Date Time Recelved : (SI NATURE) i Date Time 5 Ret}nquished by- (SIGNATURE) Data Time Rece' : (SIG TURF) Da Time ' Lr 0 0 Cl'' CrD Waypointo ANALYTICAL 9/24/2019 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 19-255-0023 Client Project Description: Winston- Salem, NC 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 9/12/2019 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '-'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Danyale Love Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Alabama #40750 Louisiana #04015 VAN ELAP #460181 Texas #T104704180 Arkansas #88-0650 Mississippi California #2904 NC 4415 Oklahoma #9311 SC #84002 Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST #90215 PA DEP 468.03195 .c_c.a. Page 1 of 13 d Way PA A A Client: EMA Resources Inc Project: Winston- Salem, NC Lab Report Number: 19-255-0023 Cate: 9/24/2019 2790 Whitten Road, Memphis, TN 38133 Main 901.213.7-400 0 Fax 901.213.2440 www.waypointa nalytical.corn CASE NARRATIVE Metals Analysis Method 601 OD Sample 92694 (Neilson WTP #1) Analyte: Aluminum QC Batch No: L454349IL453670 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: 1-454349/1-453670 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: 1-454188/1-453670 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 92596 (Neilson WTP #3) Analyte: Aluminum QC Batch No: L4543231L453733 The matrix spike and/or the matrix spike duplicate was outside qualify control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Iron QC Batch No: L454323IL453733 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L4543231L453733 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Manganese QC Batch No: L454101IL453733 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Phosphorus QC Batch No: L454101/1-453733 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Page 2 of 13 WayPANAE.YTlCAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com Analyte: Sulfur QC Batch No: L4541011L453733 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix Interference is suspected. Sample 92697 (Neilson WTP #4) Analyte: Aluminum QC Batch No: 1-454323/1-453811 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Iron QC Batch No: 1-454323/1-453811 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix Interference is suspected. Analyte: Potassium QC Batch No: L454323/L453811 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Manganese QC Batch No: L454137/1-453811 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Analyte: Mercury QC Batch No: 1-454339/1-454229 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges, A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 3 of 13 • =poina ANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksvilie , NC 27028 Report Number :19-255-0023 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901,213.2440 www.waypoin tana lytical.com Project Winston- Salem, NC Information : REPORT OPANALWS Report Date : 09/24/2019 Received : 09/ 1212019 0on`.6&sb- W-Q Danyale Love Project Manager Matrix: Solids Lab No: 92694 Sampled: 9111/2019 9:00 Sample ID : Neilson WTP *1 Test Results Units MDL MQL DF Date 1 Time Analyzed By Analytical Method 76.6 % 0.010 1 09/16/19 16:43 ADM SW-DRYWT °k Moisture 1290 mg/Kg - dry 107 1 09/23/19 15:00 JPJ 4500NH3C-2011 Ammonia Nitrogen <21.4 mgJKg - dry 21.4 21.4 1 09/23/19 14:16 ZBD 4500NO3F-2011 Nitrate+Nitrite-N mg/Kg - dry 214 1 09/23/19 15:00 CALCULATION - Organic N 2680 6.1 S.U. 1 09/23/19 07:03 JSL 9045D pH 23.4 % 0.010 0.010 1 09/16/19 16:43 ADM 254OG-2011 Total Solids mg/Kg - dry 214 1 09/24/19 14:40 CLP 4500NORGD-2011 Total Kjeldahl Nitrogen 3970 Phosphorus 2300 mg/Kg - dry 11.0 21.4 1 09/13/19 22:08 JTR 6010D Aluminum 104000 mg/Kg - dry 86.8 214 10 09/17/1914:20 BKN 6010D 8.25 mg/Kg - dry 1.79 2.14 1 09/13/19 22:08 JTR 6010D Arsenic <0.212 mg/Kg - dry 0.212 0.427 1 09/13/19 22:08 JTR 6010D Cadmium 974 mg/Kg - dry 71.8 107 1 09/13/19 27:08 JTR 6010D Calcium 44.0 mg/Kg - dry 0.811 1.07 1 09/13/19 22:08 ITR 6010D Chromium 45.3 mg/Kg - dry 0.620 1.07 1 09/13/19 22:08 JTR 6010D Copper 45300 mg/Kg - dry 181 214 10 09/17/19 14:20 BKN 6010D Iron 24.9 mg/Kg - dry 0.636 1.28 1 09/13/19 22:08 JTR 6010D Lead 2260 mg/Kg - dry 9.49 21.4 1 09/13/19 22:08 JTR 6010D Magnesium 551 mg/Kg - dry 0.782 2.14 1 09/13/19 22:08 JTR 60101) Manganese 0.0739 mg/Kg - dry 0.0150 0.0679 1 09/17/19 14:07 TJS 7471A Mercury 1.50 mg/Kg - dry 0.555 1.07 1 09/13/19 22:08 JTR 6010D Molybdenum 22.0 mg/Kg - dry 0.705 1.07 1 09/13/19 22:08 JTR 6010D Nickel 1920 mg/Kg - dry 12.7 21.4 1 09/13/19 22:08 JTR 6010D Potassium <2.09 mg/Kg - dry 2.09 2.14 1 09/13/19 22:08 JTR 6010D Selenium J Estimated value Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions L Limit Exceeded Page 4 of 13 l 2790 Whitten Road, Memphis, TN 38133 point, 901.213.24.00 ° Fax 901.213.2440 .VIMain ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Mr. Brent Collins Project Winston- Salem, NC Report Date : 09/24/2019 755 Yadkinville Rd Information : Received : 09/12/2019 Mocksville , NC 27028Danya a Love Report Number: 19-255-0023 REPORT OPANALYSi'S Proect Manager Project Lab No: 92694 Matrix: Solids Sample ID : Neilson WTP #1 Sampled: 9/11/2019 9:00 Test Results Units MDL MOL DF Date ITime By Analytical Analyzed Method Sodium 79.53 mg/Kg - dry 33.0 107 1 09/13/19 22:08 JTR 6010D Zinc 123 mg/Kg - dry 4.62 5.34 1 09/13/19 22:08 JTR 6010D Sulfur 2220 mg/Kg - dry 20.9 21.4 1 09/13/19 22:08 IT'R 6010D Sodium Absorption Ratio <5.00 Ratio 5.00 1 09/13/19 22:08 CALCULATION Qualifiers/ DF Dilution Factor Definitions L Limit Exceeded Estimated value MQL Method Quandtation Limit Page 5 of 13 �r b Waypoint. ANALYTICAL 46245 CMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number :19-255-0023 Lab No: 92695 Sample ID : Neilson WTP #2 Test 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901,213.2440 www.wayp ointanalytical. corn Project Winston- Salem, NC Information : Results REPORT OFANAL YSIS Units Report Date : 09/24/2019 Received : 09/12/2019 Danyale Love Project Manager Matrix: Solids Sampled: 9/11/2019 9:15 MDL MOL DF Date ITime By Analyzed Analytical Method 76.8 % 0.010 1 09/16/19 16:59 ADM SW-DRYWT 0/6 Moisture 741 rng/Kg - dry 108 1 09/23/19 15,00 JPJ 4500NH3C-2011 Ammonia Nitrogen <21,6 mg/Kg - dry 21.6 21.6 1 09/23/19 14:17 ZBD 4500NO3F-2011 Nitrate+Nitrite-N mg/Kg - dry 216 1 09123/19 15:00 CALCULATION - Organic N 845 1 09/23/19 07:03 JSL 9045D PH H 5.9 SM. 23.2 % 0.010 0.010 1 09/16/19 16:59 ADM 2540G-2011 Total Solids mg/Kg - dry 216 1 09/24/19 14:41 CLP 4500NORGD-2011 Total Kjeldahl Nitrogen 1590 mg/Kg - dry 11.1 21.6 1 09/13/19 18:55 JTR 6010D Phosphorus 2470 109000 mg/Kg - dry 43.5 108 5 09/16/19 19:02 BKN 6010D Aluminum 6.51 mg/Kg - dry 1.81 2.16 1 09/1311918:55 JTR 6010D Arsenic 0.3441 mg/Kg - dry 0.213 0.431 1 09/13/19 18:55 JTR 6010D Cadmium 1030 mg/Kg - dry 72.4 108 1 09/13/19 18:55 JTR 6010D Calcium 49.1 mg/Kg - dry 0,818 1.08 1 09/13/19 18:55 JTR 6010D Chromium 46.6 mg/Kg - dry 0,625 1.08 1 09/13/19 18:55 JTR 6010D Copper 50000 mg/Kg - dry 91.4 108 5 09/16/19 19:02 BKN 6010D Iron 28.0 mg/Kg - dry 0.642 1.29 1 09/13/19 18:55 JTR 6010D Lead 2450 mg/Kg - dry 9.57 21.6 1 09/13/19 18:55 JTR 6010D Magnesium 582 mg/Kg - dry 0.788 2.16 1 09/13/19 18:55 JTR 6010D Manganese 0.0780 mg/Kg - dry 0.0140 0.0634 1 09/17/19 14:18 TJS 7471A Mercury 0.7713 mg/Kg - dry 0.560 1.08 1 09/13/19 18:55 JTR 6010D Molybdenum 22.1 mg/Kg - dry 0.711 1.08 1 09/13/19 18:55 JTR 6010D Nickel 2130 mg/Kg - dry 64.2 108 5 09/16/19 19:02 BKN 6010D Potassium <2.11 mg/Kg - dry 2.11 2.16 1 09/13/19 18:55 JTR 6010D Selenium J Estimated value Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions L Limit Exceeded Page 6 of 13 a Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 'Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Mr. Brent Collins Project Winston- Salem, NC Report Date : 09/24/2019 755 Yadidnville Rd information : Received : 09/12/2019 Mocksville , NC 27028 Danyale Love Report Number :19-255-0023 REPORTOFANALYSIS Project Manager Lab No ; 92695 Matrix; Solids Sample ID: Neilson WTP #2 Sampled: 9/11/2019 9:15 Test Results Units MDL MQL DF Date ITime By Analytical Analyzed Method Sodium 1023 mg/Kg - dry 33.3 108 1 09/13/19 18:55 JTR 6010D Zinc 130 mg/Kg - dry 4.66 5.39 1 09/13/19 18:55 JTR 6010D Sulfur 2420 mg/Kg - dry 21A 21.6 1 09/13/19 18:55 JTR 6010D Sodium Absorption Ratio <5.00 Ratio 5.00 1 09/13/19 18:55 CALCULATION Qualifiers/ DF Dilution Factor Definitions L Limit Exceeded J Estimated value MQL Method Quantitation Limit Page 7 of 13 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number :l9-255-0023 Lab No: 92696 Sample ID : Neilson WTP #3 Test 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 vvww.way poin to nal yticat.com Project Winston- Salem, NC Information : REPORT OFANAL YSIS Report Date : 09/24/2019 Received : 09/12/2019 Danyale Love Project Manager Matrix: Solids Sampled: 9/11/2019 9:30 Results Units MDL MQL DF Date I Time By Analytical Analyzed Method 0/0 0.010 1 09/1611916:59 ADM SW-DRYWT 0/6 Moisture 71.6 mg/Kg - dry 88.0 1 09/23/19 15:00 JPJ 4500NH3C-2011 Ammonia Nitrogen 683 mg/Kg - dry 17.6 17.6 1 09/23/19 14:18 ZBD 4500NO3F-2011 Nitrate+Nitrite-N <17.6 mg/Kg - dry 176 1 09/23/19 15:00 CALCULATION - Organic N 489 1 09/23/19 07:03 JSL 9045D PH 5.6 S.U. % 0,010 0.010 1 09/16/19 16:59 ADM 2540E-2011 Total Solids 28.4 mg/Kg - dry 176 1 09/24/19 14:42 CLP 4500NORGD-2011 Total Kjeidahl Nitrogen 1170 mg/Kg - dry 9.05 0.6 1 09/13/19 19:01 JTR 60100 Phosphorus 2510 107000 mg/Kg - dry 35.6 88.0 5 09/16/19 19:07 BKN 6010D Aluminum 5.39 mg/Kg - dry 1.48 1.76 1 09/13/19 19:01 JTR 6010D Arsenic 0.359 mg/Kg - dry 0.174 0.352 1 09/13/19 19:01 JTR 6010D Cadmium $38 mg/Kg - dry 59.2 88.0 1 09/13/19 19:01 JTR 6010D Calcium 43.0 mg/Kg - dry 0,669 0.880 1 09/13/19 19:01 JTR 60101) Chromium 4M8 mg/Kg - dry 0.511 0.880 1 09/13/19 19:01 JTR 6010D Copper 44000 mg/Kg - dry 74.6 88.0 5 09/16/19 19:07 BKN 6010D Iron 25.3 mg/Kg - dry 0,524 1.06 1 09/13/19 19:01 JTR 6010D Lead 2140 mg/Kg - dry 7.82 17.6 1 09/13/19 19:01 JTR 6010D Magnesium 521 mg/Kg - dry O.644 1.76 1 09/13/19 19:01 JTR 6010D Manganese 0.0856 mg/Kg - dry 0.0119 0.0539 1 09/17/19 14:22 TJS 7471A Mercury 0.6023 mg/Kg - dry 0.457 0.880 1 09/13/19 19:01 JTR 6010D Molybdenum 19.4 mg/Kg - dry 0.580 0.880 1 09/13/19 19:01 JTR 6010D Nickel 1680 mg/Kg - dry 52.5 Salo 5 09/16/19 19:07 BKN 6010D Potassium <1.73 mg/Kg-dry 1.73 1.76 1 09/13/19 19:01 JTR 6010D Selenium 3 Estimated value Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions L Limit Exceeded Page 8 of 13 waypoint."'."- ANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadldnville Rd Mocksville , NC 27028 Report Number : 19-255-0023 Lab No ; 92696 Sample ID : Neilson WTP #3 Test 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901,213.2440 www.waypoln tanalytical.com Project Winston- Salem, NC Information : REPORT OF'ANALYSIS Results Units MDL Report Date : 09/24/2019 Received : 09/12/2019 Qc"'6& WD- Danyale Love Project Manager Matrix: Solids Sampled: 9/1112O19 9:30 MQL DF Date I Time By Analytical Analyzed Method Sodium 60.93 mg/Kg - dry 27.2 88.0 1 09/13/19 19:01 JTR 6010D Zinc 115 mg/Kg - dry 3.80 4.40 1 09/13/19 19:01 JTR 6010D Sulfur 2450 mg/Kg - dry 17.2 17.6 1 09/13/19 19:01 JTR 6010D Sodium Absorption Ratio <5.00 Ratio 5.00 1 09/13/19 19:01 CALCULATION Qualifiers/ DF Dilution Factor Definitions L Limit Exceeded J Estimated value MQL Method Quantitation Limit Page 9 of 13 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Report Number:19-255-0023 Lab No: 92697 Sample ID; Neilson WTP #4 Test 2790 Whitten Road, Memphis, TN 38133 Main 901,213.2400 0 Fax 901.213.2440 www.way pain to nalyticaLcom Project Winston- Salem, NC Information : REPORrOPANALYSIS Report Date : 09/24/2019 Received ,_,(�:09/ 12/2019 Q0 6&� w-,D- Danyale Love Project Manager Matrix: Solids Sampled: 9/11/2019 9,45 Results Units MDL MQL DF Date ITime By Analytical Analyzed Method Moisture 79.2 0/0 0.010 1 09/26/1916:59 ADM SW-DRYvrr Ammonia Nitrogen 480 mg/Kg - dry 120 1 09/23/19 15:00 3P3 4500NH3C-2011 Nitrate+Nitrite-N <21.1 mg/Kg - dry 21.1 21.1 1 09/23/19 14:18 ZBD 4500NO3F-2011 Organic N 673 mg/Kg - dry 240 1 09/23/19 15:00 CALCULATION - pH 6.2 s.u. 1 09/23/19 07:03 JSL 9045D Total Solids 20.8 % 0.010 0.010 1 09/16/19 16:59 ADM 2540G-2011 Total Kjeldahl Nitrogen 1150 mg/Kg - dry 240 1 09/24/19 14:43 CLP 4500NORGD-2011 Phosphorus 2500 mg/Kg - dry 12.4 24.0 1 09/13/19 17:35 JTR 6010D Aluminum 112000 mg/Kg - dry 97.6 240 10 09/16/19 18:13 BKN 6010D Arsenic 6.54 mg/Kg - dry 2.01 2.40 1 09/13/19 17:35 JTR 6010D Cadmium 0.3533 mg/Kg - dry 0.238 0.481 1 09/13/19 17:35 JTR 6010D Calcium 1080 mg/Kg - dry 80.8 120 1 09/13/19 17:35 3TR 6010D Chromium 48.1 mg/Kg - dry 0.913 1.20 1 09/13/19 17:35 JTR 6010D Copper 44.9 mg/Kg - dry 0.697 1.20 1 09/13/19 17:35 JTR 6010D Iron 48600 mg/Kg - dry 204 240 10 09/16/19 18:13 BKN 6010D Lead 27.1 mg/Kg - dry 0.716 1.44 1 09/13/19 17:35 JTR 6010D Magnesium 2440 m9/Kg - dry 10.7 24.0 1 09/13/19 17:35 JTR 6010D Manganese 625 mg/Kg - dry 0.879 2.40 1 09/13/19 17:35 JTR 6010D Mercury 0,0846 mg/Kg - dry 0.0151 0.0688 1 09/17/19 14:23 TIS 7471A Molybdenum <0.625 mg/Kg - dry 0.625 1.2D 1 09/13/19 17:35 JTR 6010D Nickel 22.5 mg/Kg - dry 0.793 1.20 1 09/13/19 17:35 JTR 6010D Potassium 2150 mg/Kg - dry 143 240 10 09/16/19 18:13 BKN 6010D Selenium <2.36 mg/Kg - dry 2.36 2.40 1 09/13/19 17:35 JTR 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions L Limit Exceeded MQL Method Quantitation Limit Page 10 of 13 C Wavpoint2790 Whitten Road, Memphis, TN 32133 AF Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 46245 EMA Resources Inc Mr. Brent Collins Project Winston- Salem, NC Report Date ; 09/24/2019 755 Yadkinville Rd Information : Received : 09/12/2019 Mocksville , NC 27028 Report Number :19-Z55-OD23 REPORTOFANALY5t5 Danyale LoveProject Manager Lab No: 92697 Matrix: Solids Sample ID : Neilson WTP 44 Sampled: 9/11/2019 9:45 Test Results units MDL MQL DF Date ITime By Analytical Analyzed Method Sodium 1017 m9/Kg - dry 37.1 120 1 09/13/19 17:35 TFR 6010D Zinc 137 mg/Kg - dry 5.19 6.01 1 09/13/19 17:35 7TR 6010D Sulfur 2450 mg/Kg - dry 23.5 24.0 1 09/13/19 1735 ]TR 6010D Sodium Absorption Ratio <5.00 Ratio 5.00 1 09/13/19 17:35 CALCULA71ON Qualifiers/ DF Dilution Factor Definitions L Limit Exceeded J Estimated value MQL Method Quantitation Limit Page 11 of 13 nt+Ir" r :: ANALYTICAL Customer Number: 46245 Customer Name: EMA Resources inc Report Number: 19-255-0023 • Fed Ex Q US Postal Q UPS Q Client 2790 Whitten Road, Memphis, TN 38133 Main 901.2112400 0 Fax 901.213.2440 www.waypointa nalyticai.co m Cooler Receipt Form Shipping Method Q Lab Q Other. r—�---� Q Courier Thermometer ID: l 4't 5 Shipping container/cooler nuncompromised?-; NI.—iharof rnlers received 1 ' Yes Q No Custody seals intact on shipping container/cooler? Q Yes (�} No Q No � Not rcegwrea®Not Required Custody seals intact on sample bottles? Q Yes Chain of Custody (COC) present? 0 Yes Q No COC agrees with sample label(s)? 0 Yes Q No COC properly completed 0Yes QNo Samples in proper containers? ® Yes No Sample containers Intact? 0 Yes Q No. Sufficient sample volume for indicated test(s)? Yes Q No _ All samples received within holding time? Yes Q No Cooler temperature in compliance? ® Yes Q No Cooler/Samples arrived at the laboratory on ice. i Yes Q No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved Q Yes Q No 4& N/A Water -VOA vials free of headspace Q Yes Q No Q Na � N/A � - NIA Trip Blanks received with VOAs Q Yes Soil VOA method 5035 — compliance criteria met Q Yes Q No i N/A r— High concentration container (48 hr) [— Low concentration EnCore samplers (48 hr) F— High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Q Yes No — f Comments: Signature: arleen Qualls Date &Time: L12/2019 08:36:46 Page 12 of 13 ClientName/Address Client Project Manager/Contact Billing Information For Laboratory Use Only EMA Resources Inc Brent Collins Account #46245 755 Yadkinville Rd Mocksville, NC 27028 Project Description Project/Site Location (city/State] RUSH - Additional charges apply Special Detection Limit(s) Me of Shipment Matrix Key � ���57a,,1-�FlrtA?L/A OateResultsNeeded PQUSPS WW - Wastewater GW - Groundwater ❑ Fed Ex HUCI(esnt CourieroropCS DW-Drinking Water S-Sail/Solid O-Oil /C, P- Product M - Misc I V Other Project Number Project Manager Phone IJ Project Manager Email Purchase Order Number Site/Facility iD P 336-399-3646 brent_coilins@emaresources.Gom C ^ to z f ) ;: O C U A Cool s 10C NRM03 (Mi. Only) e Codc-6C WalpoinIk. ANALYTICAL c e w r O c - E O � u [ xo4 pxa O Nenexegeired E NaO3 279a Whimn (load $ ° ° a f0 W V J PHa10 Memphis, TN 3sw Unless noted, all contalners o t0 � w M T G xCLp (901) 213-2400 per Table fl of 40 CPR Part 136. s5 (D Y ;E Q L° �"' + � x H3PG4 p<g CL • s m z Z 1 Cool a 6C MUS203 Date I Time Sam IeIdentification R tilted nalyais/ PfeserwatIve Comments/Notes JA) j Metals:AI,AS,Ca,Cd,Cr,Cu,Fe,Pb I(t 1ST G LSa #, a Gr Mn,M9,M0,H9,Ni,Se,Na,P,S,K,Zn W:3,, �v�z� 0" �3 1 �`'` F�L M 1(1 GJ � G� W 4.11 1f��CIfClIlIIiCII�I�CCIIIIC�(IIIIIiC<� �;� 193 EmA Resources Inc 08.35:46 Winston- Salem. NC For Laboratory Use Only Sampled by (Name - Print) Client Remarks/Comments Ice C�lsy Lab Comments C i Y `ki7�?JJ `� Sludge Samples - Report Dry Weight Y N y Sell she b (E A( RE Da a Time�/ Received by: (SIGNATURE) Date Time / !' k oe err P Refinquished by (SIGNATURE] a Time Received by: (SIGNATURE) Date Time %� , ^{Sian` i / �►\v{1xN.�'XI Relinquished by. (SIGNATURE) Date Time a : (SIGNATU Date Time ,� errs+„ream ESEARC NA TiCAI �4`aaawuy� - Ubo Tor$6Esr INC. €� 0 NOW of _ Anclytical/Process Consultations March 24, 2016 i City of Winston-Salem Neilson WTP 5725 l?rye Bridge Road CIemmons, NC 27012 Attention: Rodney Darr Chemical Analysis for Selected Parameters and Sampling Locations Identified as Neilson WTP j (A City of Winston-Salem Neilson WTP Project, collected 01 March 2016) i 1. Miscellaneous 1 2 3 4 5 6 7 Parameters unit Results Results Results Results Results Results Results Fecal Coliform NTN/g`I`S 4 <2 <2 <2 <2 <2 Sample Number: I5606-61 15606-02 15606-03 15606-04 15606-05 I5606-06 I5606-07 SampleCollededDate: 0.3/01116 03/01/16 03/01/16 03/01/16 03/01/16 03/01/16 03101/16 Sample Collected Time: 0730 0732 0735 0740 0744 0746 07$0 MPNIg TS = Most Probable Numberper gram Total Solids uxx....avawnm�.u�r+ ...,.� �....... � ���;�.�ar;��smn�r+x+ .. •�, .. ... a��-w�v�a+nmwx�a,mienor+.ca�u�e...�.xaamwmyanw. . ro.awr..,.wane.rR.�vm«�w�.r..wawww,..�...... North Carolina nIA/D C44Quality Mar r r lML NCDEd?bWW' of Wat r Resources Division of Water Resources RURCE CE TIFICATION j� FOR FO M: RSC 06-16 Please use the following instructions as a checklist in order to ensure ill require�I em�a�Afited. Ad rence to these instructions and checking the provided boxes will help produce a quieter revi&81Mkt#nVJJBJte amou t of additional information requested. Failure to submit all of the required items will lead o a i Bona w time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Res uals Source Certification (FORM: RSC 11-15): Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. or new or renewed permits, submit a separate certification for each source facility. [C[]� or modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. omplete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Res'duals Source -Generating Facility Information: [?For each source facility, attach the following: [Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for ,Residuals Land Application Permits Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals e to be generated, treated, processed, and stored at the facility. We justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during _41rocessing. Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Rgoilluals Quality Information: Fo each source facility, attach the following: [Tf aboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector action reduction requirements. For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Winston-Salem/Fors\ th County Utilities Commission (R.A. Thomas Water Treatment Plant i. Status Code Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed R Swann WTP Swann WTP Forsyth WQ0031314 750 750 R Swann WTP Neilson WTP Forsyth WQ0031314 2,500 1,499 R Swann WTP Thomas WTP Forsyth WQ0031314 750 750 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: R.A. Thomas Water Treatment Plant 2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Bill Brewer — Water Treatment Su erintendent Complete mailing address: 2800 River Ridge Road City: Pfafftown State: NC Zip: 27040-8435 Telephone number: 336) 945-1179 E-mail address: billb@cityofws.org 4. Facility physical address: ,1201 S. Martin Luther King, Jr. Drive City: Winston-Salem State: NC Zip: 27107-8435 Coordinates: Latitude: N36° 5' 11.7" Longitude: W80° 13' 8" Datum: DMS Level of accuracy: 100% Method of measurement: Survey 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, Z treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: �^ % industrial and % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ❑ Yes ® No 7. Facility permitted/design flow: 18.0 MGD and facility average daily flow: 5_7 MGD 8. Average amount of residuals being generated at this facility 750 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: The treatment facilities for wash water consists of one (1) equalization basin with a capacity of 0.545 MG's and one (U circular clarifier with a maximum daily hydraulic loading rate of 0.36 & m/sf. In addition. the Thomas Plant has a residuals pumps station for pumping thickened solids to one of two (2) residuals lagoons for settling and drying of solids. Each lagoon has an effective storage volume of 2.1 MG's each. Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or Z. 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6] as: Biological E Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Research & Analytical Laboratories. Inc. and Date of analysis: 4/26/2016 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: 212 °F (> 140°F) Passed reactivity test: ®yes ❑no. HCN: <250 mg/kg (<250) & H2S: <500 mg/kg (<500) TCLP Parameter Limit (mglo Result TCLP Parameter (mgfl) Limit (mg/V Result (mg/1) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 0.454 Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 N D Lindane 0.4 ND Chlordane 0.03 N D Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1, 1 -Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land jM ication: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Research & Analytical Laboratories. Inc. and Date of analysis: 8/30/2017 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) 3.51 <0.278 33.6 Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 13.1 Mercury 57 17 0.124 <2.78 Molybdenum 75 420 100 n/a Nickel 420 18.9 Selenium 100 <2.78 Zinc 7,500 2,800 173 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Research & Analytical Laboratories, Inc. and Date of analysis: 8/30/2017 Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ® > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) 3.51 ND 18.9 FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Research & Analytical Laboratories. Inc. and Date of analysis: 8/30/2017 Parameter Result (mg/kg) Aluminum 109,000 Ammonia -Nitrogen 1,380 Calcium 4,100 Magnesium 1,660 Nitrate -Nitrite Nitrogen 26.1 pH (Standard Unit) 6.54 Phosphorus 1,260 Potassium 1,510 Sodium 239 Total Kjeldahl Nitrogen 7,170 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40% or 0.40 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: Accepted formula for water plant residuals. e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (13t) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 3,010 3,913 Injection/Incorporation N/A N/A 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N/A -Water plant residuals FORM: RSC 06-16 Page 4 of 5 7. PathoQen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of 'Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (1'AR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T. 1 107(a)(6)] -Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 R.A. Thomas Water Treatment Plant Water System Facility ID = TP1 Production Capacity = 18.0 MGD City of Winston-Salem NPDES ID# = NCO079821 Potassium Permanganate 1 Salem Lake —1.0 Billion � Gallon Raw Water Reservoir Alum Caustic Chlorine Chlorine Filter Aid Polymer Chlorine Fluoride Ortho-Phosphate Caustic Entry Point-EP1 10.0 MGD i--*[— Common Header • a v► ■ • Coagulatior. 9 Flocculation Residuals Sedimentation Basins ■j r Yadkin River via Neilson WTP Raw Water Reserviors (2) 1.76 MG Residuals Lagoons ■ Residuals Pump Station (3) 200 GPM Pumps r m au Polymer Filtration Backwash and Washwater - Filter to Waste ■ EQ Basin OP 0.55 MG Ok (4) - 1.12 MGD Pump= _ r— - Max Flow = 4.5 MGD —� 1.5 MG Clearwell 1.5 MG Clearwell Distribution System 24.0 MGD r Washwater + Clarifier 4.5 MGD Discharge Outfall 001 I?t4 -/-A WI-1 BLACK & VEATCH INTERNATIONAL COMPANY ,SGe' ILit, 1 - 69 CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 Control: The pumps will be controlled manually from the plant control system or locally at the finished water pumping station. A low level sensor will be provided in each finished water storage reservoir to stop the pumps on low water level. Pump status and alarm conditions, pump discharge valve position, and finished water storage reservoir levels will be indicated locally and transmitted to the plant control system. 3. Flow Measurement. Type Magnetic Number of meters 1 Size, each, inches 24 Flow measurement range, mgd 4-26 Control: Flow signal will be transmitted to the plant control system and local indication will be provided in the pumping station. G. WASH WATER AND RESIDUALS HANDLING 1. Wash Water and Residuals Handling. Currently, a common drainage system exists for sedimentation basin overflow, for basin drainage and residuals drawdown, for filter backwash and filter -to -waste drainage, and for storm water. These flow streams drain to the wash water and residuals pumping station where they are pumped to one of two residuals storage lagoons. This practice will be abandoned and the clear water and residuals flow streams will be separated and treated. Spent wash water and filter -to -waste will discharge by gravity to a new wash water equalization basin. The collected water will be pumped from the equalization basin to a new wash water clarifier. Wash water clarifier effluent will discharge to the creek in accordance with the NPDES permit. The wash water drainage system upstream of the equalization basin will be designed to allow all four filters to be simultaneously wasted at the design filtration rate prior to the addition of ozone, and three filters to be wasted at I-18 BLACK & VEATCH INTERNATIONAL COMPANY CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 the design filtration rate after the addition of ozone (filter hydraulic grade line is reduced). This drainage capacity assumes a maximum headloss of 5 feet through a filter's media and underdrain during the wasting period. This drainage capacity is provided for an emergency condition when water quality dictates the basins be wasted until necessary treatment adjustments are made. Because this is an emergency condition and not part of the normal plant operation, flows in excess of the equalization basin pumping capacity will overflow to the plant overflow drain. Unthickened residuals from the sedimentation basins will discharge by gravity through the viewing pit to the residuals pumping station. Residuals from the wash water clarifier will also discharge by gravity to the residuals pumping station. The combined residuals will be pumped to the residuals storage lagoons. Decant/overflow from the residuals storage lagoons will flow by gravity back to the wash water equalization basin. 2. Wash Water and Residuals Flows and Solids Production. Filter Backwash Water Initial Per filter"', gal 179,775 Avg (2), gpd 359,550 Max(3), gpd 719,100 Filter -to -Waste Per filter"), gal 63,920 in Avg (2)(4), gpd 127,840 Max(3)(4), gpd 255,680 Total Residuals Production Avg('), lb/day 2,290 Max('), lb/day 4,122 Unthickened Residuals Flow to La ,00ns Avg(S)(7) gpd W 137,290 Max(6)(7), gpd 247,122 I- l 9 BLACK & VEATCH INTERNATIONAL COMPANY CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 Thickened Residuals Production Avg (5)(8), gpd 5,492 Max (6)(8), gpd 9,885 Free Liquid from Residuals(9) Avg, gpd 131,798 Max, gpd 237,237 Effluent _Clarifier Avg( 10), mgd 1.13 Max (11), mgd 2.25 (1) Flow rate of 22.5 gpm/sf for 10 minutes. (2) Half of the filters backwashed in one day. (3) All filters backwashed in one day. (4) Flow rate of 4 gpm/sf for 20 minutes. (5) Two hundred twenty-nine pounds per million gallons, using average flow rate of 10 mgd. (6) Two hundred twenty-nine pounds per million gallons, using design flow rate of 18 mgd. (7) 0.2 percent solids. (8) 5.0 percent solids. (9) Unthickened residuals flow minus thickened residuals flow. (10) Pumped flowrate from wash water equalization basin to wash water clarifier under average daily conditions of two filter washes per day. (11) Pumped flowrate from wash water equalization basin to wash water clarifier under maximum daily conditions of four filter washes per day. 3. Wash Water E ualization Basin. A wash water equalization basin will be provided for flow equalization of wash water prior to treatment in the wash water clarifier. Depending on the daily flow to the equalization basin, as few as one or up to four pumps will be required to pump the contents of the basin to the wash water clarifier. Under average daily conditions of two filter wash cycles per day, one pump is required with three standby pumps available. Under maximum daily conditions of four filter wash cycles per day, two pumps are required with two standby pumps available. In the event of a sedimentation basin drain, all four pumps are required with no standby pump available. I-20 BLACK & VEATCH INTERNATIONAL COMPANY CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 Submersible mixers will not be provided. Operations staff will be required to wash down settled solids on an as needed basis. Number of basins Design criteria, each Volume, each, gal Basin type Basin shape Dimensions, ft Inside diameter, ft Average sidewall water depth, ft Average sidewall depth, ft Bottom slope to sump Water depth at top of sump, ft Pumps Number of pumps Rated capacity, each, gpm Rated head, ft Operating head range, ft Motor brake horsepower, bhp Storage volume of two filter wash cycles plus 10 percent 545,000 Reinforced concrete Circular 75 16.5 18.5 1:75 17.0 4 780 18 12-33 10 Controls: Level sensors will be provided in the equalization basin for level monitoring and control of the wash water equalization pumps and mixers. Basin level will be transmitted to the plant control system. At basin overflow level, an overflow alarm will be transmitted to the plant control system. The wash water equalization basin pumps will be automatically alternated and started and stopped based on level in the wash water equalization basin. Provisions will be made to start/stop the pumps locally and from the plant control system. Pump I-21 BLACK & VEATCH INTERNATIONAL COMPANY CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 status and alarm conditions will be indicated locally and transmitted to the plant control system. 4. Wash Water Clarifier. Number I Basin Type Reinforced Concrete Basin Dimensions Inside wall diameter, ft 75 Inside weir diameter, ft 68.67 Sidewall water depth, ft 12 Total sidewall depth, ft 14 Water depth at center pier, ft 15.1 Floor radial slope to center 1:12 Hydraulic loading rate, gpm/sf Average daily 0.18 Max daily 0.36 Sedimentation Basin Drain 0.72 Detention time, hr Average daily 8.5 Minimum daily 4.2 Sedimentation Basin Drain 2.1 Weir type Perimeter; sharp crested, V-notch Weir loading rate, gpm/ft Average 3.62 Maximum daily 7.24 Sedimentation Basin Drain 14.48 Control: Clarifier drive status and alarm conditions will be indicated locally and transmitted to the plant control system. The clarifier residual drain valve will be opened and closed automatically either (1) based on an operator selectable cycle I-22 BLACK & VEATCH INTERNATIONAL COMPANY CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 time set point for number of hours of plant operation or (2) a total accumulated wash water clarifier flow volume between blow -downs. The plant control system will open the valve for an operator -entered duration and close the valve for the remainder of the cycle. In Flow mode, the valve open duration will be the same as the Time mode "open duration setpoint". The basis for automatic control ("timed" or "flow"), the cycle time set point, and the flow volume set point is entered at the plant control system workstation computers. Provision will be made to open and close the residuals drain valve locally and from the plant control system. 5. Residuals Pum in•� Station. The existing residuals pumping station will remain. The contents of the station will be demolished and completely renovated. The following new facilities will be provided: • Residuals pumps and associated pump controls • Piping and valves • Plumbing • HVAC • Doors • Handrail and guardrail • Protective coatings • Electrical • Instrumentation and control system Under maximum residuals drainage conditions from the sedimentation basins and wash water clarifier, two pumps are required with one standby pump available. In the event the wash water clarifier is taken offline for maintenance, the wash water equalization basin flow will be drained into the pumping station wetwell, and three pumps will be required with no standby pumps available. During this wash water clarifier maintenance period, the I-23 BLACK & VEATCH INTERNATIONAL COMPANY CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 equalization basin level must be limited to approximately half full to limit the flow rate into the residuals pumping station wetwell. Residuals Pumps Type of pump Horizontal end suction centrifugal Number of pumps 3 Rated capacity, each, gpm 200 Rated head, ft 46 Operating head range, ft 24-46 Motor brake horsepower, each, bhp 10 Controls: The residuals pumps will be automatically alternated and started and stopped based on level in the residuals pumping station wet well. Provisions will be made to start/stop the pumps locally and from the plant control system. Pump status and alarm conditions will be indicated locally and transmitted to the plant control system. 6. Residuals Storage Lagoons. The existing residuals storage lagoons will be expanded and modified to receive all plant residuals for storage. The design criteria provided herein is based upon a design thickened residual concentration of 5%. Number of lagoons Lagoon type Dimensions, each, ft Length Width Max residuals depth Max water depth Freeboard I-24 2 Earthen lagoon with concrete slope protection and underdrain 311 157 8 10 2 BLACK & VEATCH INTERNATIONAL COMPANY CIVIL DESIGN MEMORANDUM Winston-Salem/Forsyth County Utility Commission B&V Project 145730 Winston-Salem, North Carolina First Issue: December 15, 2006 R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007 Perimeter slope Liquid volume, each, mg Storage volume, each, mg Effective storage, each lagoon, days Access Ramp Width, ft Slope, percent Decant Sludge removal method Cleaning duration, years H. OPERATIONS BUELDING 2:1 2.8 2.1 365 12 10 Discharge to wash water equalization basin Air drying, excavate with front-end loader or clam bucket 1 The existing control building will be demolished and a new operations building will be provided for administrative facilities, chemical feed and storage, and maintenance and control facilities. Figures I-16 and 1-17 showing the floor plans for the basement and operating floor and Figure I-18 showing the building elevations are attached. The following facilities will be provided: Basement Floor Bulk Liquid Chemical Storage Room Coagulant (Alum) Storage Area Zinc Orthophosphate Storage Area Future Storage Areas Sodium Hypochlorite Storage Room Fluoride Storage Room Sodium Hydroxide Storage Room General Storage Room Electrical Room I-25 R.A. Thomas Water Treatment Plant Solids Handling Plan The Thomas Water Treatment Plant is an 18.0 MGD water treatment facility. Solids are generated by automatic sludge removal from sedimentation basins, backwashing filters, and filter -to -waste after filter backwashes are completed. Solids produced from filter backwashes and filter -to -waste is routed to an equalization basin (0.545 MG), is treated with polymer, and then pumped to a clarifier. Solids settled in the clarifier flow to the plants waste station and are then pumped to one of two residuals lagoons (1.76 MG each) using one of three 0.288 MGD pumps. One lagoon is kept in service while the second is dried and cleaned. Clarified water from the clarifier is discharged to an unnamed tributary of Salem Creek through the permitted NPDES discharge NC0079821. Permits and Classifications: 1. The discharge from the clarifier is authorized by NPDES Permit NC0079821. The classification for the discharge is Grade 1 Physical/Chemical. 2. The distribution of the residuals removed from the lagoons is authorized by permit WQ0031314. The residuals are classified as Class A. Operation: 1. The system consists of a 0.545 MG equalization basin (EQ basin), (4) equalization basin discharge pumps rated at 1.0 MGD each, a residuals clarifier rated at maximum weir loading rate of 7.24 gpm/ft, a residuals pump station with (3) residuals pumps rated at 0.29 MGD each for transferring residuals to (2) residuals lagoons rated at 1.76 MG each. 2. Routine inspections of equipment will be conducted the Senior Utility Plant Supervisor to ensure proper operation of equipment. Any equipment not functioning properly are reported through the water division's asset management program, MAXIMO, to the appropriate support group for repair/replacement. 3. Backwash and filter -to -waste water from the plant process flow by gravity to the EQ basin and are pumped by the EQ basin pumps to the wash water clarifier. 4. 38% Sodium bisulfite is fed atone of two locations (influent or effluent to clarifier) for dechlorination of effluent being sent out discharge NCO079821. 5. All sedimentation basin residuals and residuals from the wash water clarifier flow to the residuals pump station and are then pumped directly to one of the two residuals lagoons. R.A. Thomas Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 6. Clarified water from the washwater clarifier is discharged to an unnamed tributary of Salem Creek through the permitted NPDES discharge NC0079821. 7. Residuals are dried then removed from the lagoons and hauled to the application site by a private contractor. Monitoring and Reporting Requirements: 1. Residuals generated by each source -generating facility must be analyzed to demonstrate that they are non -hazardous based on the most current permit requirements (Attachment A). Sampling will be conducted under supervision of the Senior Water Treatment Plant Supervisor by WSFC Utilities current contractor as described below in compliance with permit requirements. 2. Analysis will be performed by a NC Certified Laboratory. 3. Analyses made according to monitoring and reporting requirements must be certified for the required parameter(s). 4. Corrosivity, ignitability, reactivity, and a Toxicity Characteristics Procedure analysis are required once each permit cycle. The TCLP analysis includes the following parameters (i.e., note the regulatory level in milligrams per liter in parentheses): Arsenic (5.0) Barium (100.0) Benzene (0.5) Cadmium (1.0) Carbon tetrachloride (0.5) Chlordane (0.03) Chlorobenzene (100.0) Chloroform (6.0) Chromium (5.0) m-Cresol (200.0) o-Cresol (200.0) p-Cresol (200.0) Cresol (200.0) 2,4-D (10.0) 1,4-Dichlorobenzene (7.5) 1,2-Dichloroethane (0.5) 1, 1 -Dichloroethylene (0.7) 2,4-Dinintrotolulene (0.13) Endrin (0.02) Hexachlorobenzene (0. 13) Heptachlor (and its hydroxide) (0.008) Hexachloro-1,3-butadiene (0.5) Hexachloroethane (3.0) Lead (5.0) Lindane(0.4) Mercury (0.2) Methoxychlor (10.0) Methyl ethyl ketone (200.0) Nitrobenzene (2.0) Pentachlorophenol (100.0) Pyridine (5.0) Selenium (1.0) Silver (5.0) Tetrachloroethylene (0.7) Toxaphene (0.5) Trichloroethylene (0.5) 2,4,5-Trichlorophenol (400.0) 2,4,6-Trichlorophenol (2.0) 2,4,5-TP (Silvex) (1.0) Vinyl chloride (0.2) 5. Analyses of the following parameters are also required with each application event: Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Phosphorous Potassium R.A. Thomas Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 pH Plant Available Nitrogen (by calculation) Selenium Sodium % Total Solids TKN Zinc FA 6. Data to verify pathogen reduction and vector attraction reduction of the residuals is maintained on file for five years. The required data is specific to the stabilization process utilized, and is also sufficient to demonstrate clear compliance with the Class A pathogen requirements and restrictions noted in 15A NCAC 02T .1106 (a) and (b) and vector attraction reduction requirements in 15A NCAC 02T .1107 (a). 7. Proper records are maintained tracking all residuals activities. These records include the source, volume, analysis, and recipient of the residuals. 8. Three copies, per application event, of all required monitoring and reporting requirements are submitted annually before March 1, to NC DEQ-DWQ. Performance Standards: 1. The pollutant concentrations in any residuals that are land applied to any land application site shall not exceed the following Ceiling and Monthly Average Concentrations (i.e. dry weight basis): Parameter Monthly Average Concentration milli rams per kilogram) Ceiling Concentration (milligrams per kilogram) Arsenic 41 75 Cadmium 39 85 Copper 1,500 4,300 Lead 300 840 Mercury 17 57 Molybdenum n/a 75 Nickel 420 420 Selenium 100 100 Zinc 2,800 7,500 2. If residuals are sold or given away, one of the Class A pathogen requirements in 15A NCAC 02T .I 106(b) must be met. Application Requirements: 1. Bulk residuals are not applied under the following conditions: i. If the residuals are likely to adversely affect a threatened or endangered species. ii. If the application causes prolonged nuisance conditions. iii. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards. iv. If the land is flooded, frozen, or snow-covered or is otherwise in a condition such that runoff of the residuals would occur. R.A. Thomas Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 v. During a precipitation event or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period. vi. For residuals treatment and storage facilities, the following minimum setbacks shall be adhered to: Description of Setback Minimum Setback feet Habitable residence or place of public assembly under separate ownership or not to be maintained as part of the project site 100 Property lines 50 Private or public water supply 100 Surface waters (streams, -intermittent and perennial, perennial water bodies, and wetlands) 50 Wells with exception to monitoring wells 100 2. When land applying bulk residuals to application site, the following minimum setbacks are maintained at all times: Setback By Type of Residual (feet) Description of Setback Liquid Cake Private or public water supply 100 100 Surface waters (streams -intermittent and perennial, perennial water bodies, and wetlands) 100 25 Surface water diversions (ephemeral streams, waterways, ditches) 25 0 Groundwater lowering ditches (where bottom of The ditch intersects SHWT) 25 0 Subsurface groundwater lowering system Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 3. Specific bulk residuals land application area boundaries are clearly marked on each land application site prior to and during a residuals land application event. Spills and Noncompliance Notification: 1. The Winston-Salem Regional Office, telephone number (336) 771-5000 will be notified within 24 hours or the next working day following the occurrence or first knowledge of the occurrence of any of the following: i. Any occurrence with the distribution program, which results in the land application of significant amounts of wastes, which are abnormal in quantity or characteristic. ii. Any failure of the distribution program resulting in a release of materials to receiving waters. iii. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate residual treatment. R.A. Thomas Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 4 2. Persons reporting such occurrences by telephone shall also file a written report in letter form within (5) days following first knowledge of the occurrence. This report must outline the actions taken or proposed to be taken to ensure that the problem does not recur. 3. Emergency Contacts: Thomas Water Treatment Plant (336) 788-0152 (Main) Donna Lankford, Plant Supervisor (336) 734-1577 (0) (336) 655-9616 (M) Bill Brewer (336) 397-7727 (0) Water Treatment Superintendent (336) 745-5277 (M) Winston-Salem/Forsyth County (336) 727-8418 Utility Administration DEHNR Regional Office (336) 771-5000 General Emergency 911 HazMat R.A. Thomas Water Treatment Plant Solids Handling Plan -Permit #WQ031314 Revised 07/14/2020 R ESEARCh & ANAtyTiCAL LAbORATORIESi INC. Analyflcal/Process Consultaflons August 17, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford NO Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis (A City of Winston-Salem Thomas WTP Project, collected 26 July 2017) I. Miscellaneous Thomas Lagoon #1 Parameters Unit Results Aluminum, Total mg/kg 86,400 Ammonia -Nitrogen (NH-3-N) mg/kg 488 Arsenic,Total mg/kg 3.48 Calcium, Total mg/kg 744 Cadmium, Total mg/kg <0.325 Copper, Total mg/kg 28.2 Lead, Total mg/kg 8.41 Magnesium, Total mg/kg 1,300 Mercury, Total mg/kg <0.105 Molybdenum, Total rng/kg <3.25 Nickel, Total mg/kg 15.5 NO2+NO3 mg/kg 3.82 Phosphorus, Total mg/kg 4,240 Potassium, Total mg/kg 954 Selenium, Total mg/kg <3.25 Sodium, Total mg/kg 209 Total Kjeldahl Nitrogen (TKN) mg/kg 3,960 Total Solids % 31.4 Zinc, Total mg/kg 132 PH Std. Units 6.31 Fecal Conform mpn/g TS <2 Sample Number: 37718-01 Sample Collected Date: 07/26/17 Sample Collected Time: 0845 mg/kg = milligrams per kilogram = parts per million % = Percent Std. Units = Standard Units RESEARCh . ANALY1FiCAt LA ORATORiIES� INC. Analyt€col/Process Consultations August 17, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis (A Cites Winston-Salem Thomas WTP Project, collected 26 July 2017) 1. Miscellaneous Parameters PAN = [MRx(TKN-NH3-N)] + (0.5x(NH-3-N))+ (NO3+NO2) = 0.4x(3,960-488) + (0.5x(488)+3.82 =1,650 mg/kg Sample Number: Sample Collected Date: Sample Collected Time: 37718-01 07/26/17 0845 PAN = Plant Available Nitrogen mg/kg = milligrams per kilogram = parts per million LA�®RAToRIES� INC. Analyticai/Process consultations August 17, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford i�'�2wtJC /13q zi 3»,� r '•.�,�,n�Fa�aNP�.,• Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis (A City of Winston-Salem Thomas WTP Project collected 26 July 2017) I. Miscellaneous Parameters SAR = Na Ca+ Ma 7_ 9.09 F2337.2+108 = 1.07 Sample Number: Sample Collected Date: Sample Collected Time: 37718-01 07/26/17 0845 SAR = Sodium Absorption Rate maJkg = milligrams per kilogram = parts per million RESEARCH & ANAtyTiCAt UboiimoR[ESi INC. Analytical/Process Consultations September 21, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis A City of Winston-Salem Thomas WTP Pro.'ect, collected 30 August 2017 I. Miscellaneous Thomas Lagoon #1 Thomas Lagoon #1 Thomas Lagoon #1 Sample A Sample B Sample C Parameters Unit Results Results Results Aluminum, Total mg/kg 109,000 94,000 106,000 Ammonia -Nitrogen (NH-3-N) mg/kg 772 1,380 735 Arsenic,Total mg/kg 2.74 3.51 2.64 Calcium, Total mg/kg 909 4,100 1,070 Cadmium, Total mg/kg <0.255 <0.278 <0.257 Copper, Total mg/kg 25.9 33.6 29.0 Lead, Total mg/kg 299 13.0 13.1 Magnesium, Total n1cr CY 1,040 1,510 1,660 Mercury, Total mg/kg 0.088 0.117 0.124 Molybdenum, Total mg/kg <2.55 <2.78 <2.57 Nickel, Total mg/kg 10.9 18.9 13.8 NO2+1903 mg/kg 26.1 3.57 3.66 Phosphorus, Total mg/kg 788 1,260 1,080 Potassium, Total mg/kg 844 1,510 1,290 Selenium, Total mg/kg <2.55 <2,78 <2.57 Sodium, Total mg/kg 138 214 239 Total Kjeldahl Nitrogen (TKN) rng/kg 6,040 7,170 5,880 Total Solids % 38.0 34.2 36.3 Zinc, Total mg/kg 173 172 140 pH Std. Units 6.54 6.62 6.54 Sample Number: 39349-01 39349-02 39349-03 Sample Collected Date: 08/30/17 08/30/17 08/30/17 Sample Collected Time: 0805 0805 0805 mg/kg = milligrams per kilogram =parts per million %= Percent Std. Units = Standard Units 1[("11ESEARCh ANALYT'ICA1 LAb®RAT®RiESr INC. Analytical/process Consultations September 21, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis (A City of Winston-Salem Thomas WTP Project, collected 30 August 2017) 1. Miscellaneous Para meters PAN = [MRx(TKN-NH3-N)) + (0.5x(NH-3-N))+ (NO3+NO2) = 0.4x(6,040-772) + (O.Sx(772)+26.1 = 2,520 mg/kg Sample ID: Sample Number: Sample Collected Date: Sample Collected Time: Thomas Lagoon #1-Sample A 39349-01 08/30/17 0805 PAN = Plant Available Nitrogen mg/kg = milligrams per kilogram = parts per million RESEARCh & ANA1YTiCAl UbotmoRiEs, INC. Anolytical/Process Consultations September 21, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford NO #34{ Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis (A City of Winston-Salem Thomas WTP Protect, collected 30 August 2017) 1. Miscellaneous Parameters PAN = [MRx(TKN-NH3-N)] + (0.5x(NH-3-N))+ (NO3+NO2) = 0.4x(7,170-I,380) + (0.5x(1,380)+3.57 = 3,010 mg/kg Sample CD: Sample Number: Sample Collected Date: Sample Collected Time: Thomas Logoon # I -Sample B 39349-02 08/30/I 7 0805 PAN = Plant Available Nitrogen ma/ka = milligrams per kilogram = parts per million RESEARCH & ANA[YTICAL LAbomoRirzs, INC. Analytical/Process Consultations September 21, 2017 City of Winston-Salem Thomas WTP 1201 South MIX Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford x � NCNsa Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis (A City of Winston-Salem Thomas WTP Project, collected 30 August 2017) I. Miscellaneous Parameters PAN = [MRx(TKN-NH3-N)] + (0.5x(NH-3 N))+ (NO3+NO2) = 0.4x(5,880-735) + (O.Sx(735)+3.66 = 2,430 mg/kg Sample ID: Sample Number: Sample Collected Date: Sample Collected Time: Thomas Logoon #1-Sample C 39349-03 08/30/17 0805 PAN = Plant Available Nitrogen mglkg = milligrams per kilogram = parts per million RESEARCh & ANA1YTiCA1 I? '' LAORATORIES INC. Analytical/Process Consultations September 21, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford LrGij7- � K i/ ¢ s"r�AlC#34 =�!WECt04: fiy . Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis AS City of Winston-Salem Thomas WTP Project, collected 30 August 2017) I. Miscellaneous Parameters SAR = Na 6.0 T Ca+ Me — 45.5+86,7 = 0.738 2 2 Sample ID. - Sample Number: Sample Collected Date: Sample Collected Time: Thomas Lagoon #1-Sample A 39349-01 08/30/17 0805 SAR = Sodium Absorption Rate mglkg = milligrams per kilogram = parts per million R ESEARCh & ANALYTICAL. LAbORATORI ESQ INC. Analyticavprocess consultations •., EDAM * September 21, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis [A Cit of Winston-Salem Thomas WTP Project, collected 30 August 2017) _ I. Miscellaneous Parameters SAR = Na 9.30 Ca+ Me = 205+126 = 0.723 2 2 Sample ID: Sample Number: Sample Collected Date: Sample Collected Time: SAR = Sodium AbsDrpfion Rate Thomas Lagoon ##1-Sample B 39344-02 08/30/17 0805 mglkg = milligrams per kilogram = parts per million RESEARCh & IANAtyTiCAt LAb4RATOR#ES? INC. Analytical/Process consultations September 21, 2017 City of Winston-Salem Thomas WTP 1201 South MLK Jr Drive Winston-Salem, NC 27107 Attention: Donna Lankford `f�fpwarggi NO M8s Chemical Analysis for Selected Parameters and Sampling Location Identilaed as Residuals Sampling & Analysis A CitY of Winston-Salem Thomas WTP Project, collected 30 August 2017 I. Miscellaneous Parameters SAR = Na Ca_ + Ma 2 Sample ID: I0.4 = 53.5+I38 = 1.Ob 2 Sample Number: Sample Collected Date: Sample Collected Time: Thomas Lagoon #1-Sample C 39349-03 08M/17 0805 SAR = Sodium Absorption Rate mg/kg = milligrams per kilogram = parts per million 13 RESEARCh & ANAlyTICAI L.AbORATORIESI INC. Analytical / Process Consultations Phone (336) 996-2841 CHAIN OF CUSTODY RECORD 11 moms ON ONE on 0 IN 0 on 0 IN Ion son on ENO on mini ENO on 0 0 a 1111111 �3.�aG 1E�11p11pIp1jKi .Mc7 4Q, s+ a: �v o fu d'• ysr3M ��: *�' n o ,- tn 00 O zR C� C \/ cq f is 00 Cd V] y r-K O .� N] ~ V � 0, � N 1 ; a a �o C� p Nkn V i a 000 ca bA � rii • r., cy V O A L3 v °�° O _ 61 6-1 • 0 �+ F / �_w � z _ cl � !E 4 o co n m F wi A cq ei Q o a r = yvi 1 C 40. �,'v0 N o05 fL C Gk � . V�� U�w w rnv�� u P, RESEARCh&ANA1YTiCAt FM : s :. �Ab®RAToRiEsp INC. Analytical/Process Consultations Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Residuals Sampling & Analysis (A City,of Winston-Salem Thomas WTP Project,_collected 26 April 2016) EPA RW Number Contaminant I. TCLP METALS D-004 Arsenic D-005 Barium D-006 Cadmium D-077 Chromium D-008 Lead D-009 Mercury D-010 Selenium D-011 Silver II. TCLP VOLATILES D-018 Benzene D-019 Carbon Tetrachloride D-021 Chlorobenzene D-022 Chloroform D-028 1,2-Dichloroethane D-029 1,1-1)ichloroethylene D-035 Methyl Ethyl Ketone D-039 Tetrachloroethylene D-040 Trichloroathylene D-043 Vinyl Chloride III TCLP SEMI-VOLATILES D-023 O-Creosol D-024 M-Creosol D-025 p-CreosoI D-026 Creosol D-027 1,4-Dichlorobeazene D-030 2,4-Dinitrotoluene D-032 Hexachlorobenzene D-033 Hexachlorobutadiene D-034 Hexachloroethane D-036 Nitrobenzene D-037 Pentachlorophenol D-038 Pyridine D-041 2,4,5-Trichlorophenol D-042 2,4,6-Trichlorophenol IV. TCLP PESTICIDES/HERBICIDES D-020 Chlordane D-016 2,4-D D-012 Endrin D-031 Heptachlor D-013 Lindane D-014 Methoxychlor D-015 Toxaphene D-017 2,4,5 TP(Silvex) V. REACTIVITY D-003 Cyanide D-003 Sulfide VI. CORROSIVITY D-002 pH VH. TCLP MISCELLANEOUS Paint Filter Test VIII IGNITABILITY D-001 Igmtability Sample Number Sample Date Sample Time (hrs) Sample Matrix BQL = Below Quantitation Limits Thomas Lagoon #2 Quantitation Results Characteristic Limit(mgQ m /L Level(mp-/L) EPA Method 0.010 BQL 5.00 6010C 0.040 0.454 100 6010C 0.005 BQL 1.00 6010C 0.010 BQL 5.00 601 OC 0.005 BQL 5.00 6010C 0.0020 BQL 0.200 7470A 0.100 BQL 1.00 6010C 0.010 BQL 5.00 6010C 0.050 BQL 0.500 8260E 0.050 BQL 0.500 8260B 0.050 BQL 100 8260E 0.500 BQL 6.00 8260B 0.050 BQL 0.500 8260B 0.050 BQL 0.700 8260E 0,500 BQL 200 8260B 0.050 BQL 0.700 U60B 0.050 BQL 0.500 8260B 0.050 BQL 0.200 8260E 20.0 BQL 200 8270D 20.0 BQL 200 8270D 20.0 BQL 200 8270D 20,0 BQL 200 8270D 0.750 BQL 7.50 8270D 0.050 BQL 0,130 8270D 0.050 BQL 0.130 8270D 0.050 BQL 0.500 8270D 0.300 BQL 3.00 8270D 0.200 BQL 2.00 8270D 10.0 BQL 100 8270D 0.500 BQL 5.00 9270D 40.0 BQL 400 8270D 0.200 BQL 2.00 8270D 0.003 BQL 0.030 8081 B 1.000 BQL 10.0 8151 A 0.002 BQL 0.020 8081 B 0.0009 BQL 0.008 8081 B 0,040 BQL 0.400 8081 B 1,000 BQL 10.0 8081 B 0.050 BQL 0.500 8081 B 0.100 BQL 1.00 8151 A 2.0 BQL 9010 10.0 BQL 9030 Std. Units 6.28 9045 FLP WNI 18157-01 04/26/16 0830 Scllia mg/L = milligrams per Litec = parts•per million (ppm) 1010 NFL = No Free Liquids