HomeMy WebLinkAboutWQ0031314_Application_20200910tWoInslon-Salern / Forsyth County
tl l hies
Water • Wastewater • Solid Waste
Administration, P.O. Box 2511, Winston-Salem, NC 27102
O: 336-727-8000, F: 336-727-8432, cityofws.or [i es
July 24, 2020
Mr. Nathaniel Thornburg �� ���
North Carolina Department of Environmental Quality 17
Aquifer Protection Unit — Land Application Unit
1617 Mail Service Center 0111-tDischar9
Raleigh, NC 27699-1617 Pennitting Unit
Dear Mr. Thornburg,
The City of Winston-Salem owns and operates three water treatment facilities in Forsyth County; the
P.W. Swann, R.W. Neilson and R.A. Thomas Water Treatment Plants. The Swann Plant currently has a
Class A Distribution Permit (WQ0031314) for the residuals produced. In 2012, the city added the
Neilson and Thomas WTP's as additional generating facilities under the Swann WTP's permit. We are
requesting a renewal of permit WQ0031314 with one exception of a major modification increasing the
R.W. Neilson's generating limit to 2,500 dry tons. This request is due to NOD-2020-PC-3075 where the
Neilson WTP exceeded its current limit of 1,499 dry tons per year (see attached letter from Lon T. Snider
dated July 7, 2020 and Bill Brewer's response dated July 13, 2020). By increasing the permitted dry
tonnage for Neilson, we should eliminate future exceedances if we are unable to haul of-e year due to
rainfall or other issues.
Below is a summary of the documents included in this renewal application package.
P.W. Swann Water Treatment Plant
• Application Fee in the amount of $395.00 for a Major Modification being requested increasing
the quantity of the R.W. Neilson's generating limit to 2,500 dry tons per year
• Completed form DCAR 08-11 indicating this request as a renewal of our existing distribution
permit WQ0031314 which includes the following:
✓ A copy of documentation of NOD-2020-PC-0375 as justification for our Major Permit
Modification Request for the Neilson WTP generating facility
✓ A copy of the P.W. Swann's current distribution permit WQ0031314
✓ Scope of work from our bid documents showing how our contracts for residuals land
application are structured. Material from all plants are hauled in bulk
Completed form RSC 11-13 which includes the following:
✓ Completed Form RSC 11-13
✓ Map of plant site and adjacent fields proposed for application when available
✓ Process diagram (waste facilities highlighted in green)
✓ Black & Veatch's design criteria estimated residuals quantitative production rates
✓ P.W. Swann's Solids Handling Plan
✓ TCLP and corrosivity sample results dated April 8, 2016
✓ Nutrient metal results from our most recent sampling events from samples collected
September 17, 2019 and November 25, 2019
City Council: Mayor Allen Joines; Denise D. Adams, Mayor Pro Tempore, North Ward; Dan Besse, Southwest Ward; Robert C. Clark, West Ward; John C. Larson,
South Ward; Jeff Macintosh, Northwest Ward; Morticia'Tee-Tee" Parmon, Northeast Ward; Annette Scippio, East Ward; James Taylor, Jr., Southeast Ward;
City Manager: Lee D. Garrity
County Commissioners: David R. Plyler, Chair; Don Martin, Vice Chair; Fleming El -Amin; Ted Kaplan; Richard V. Linville; Tonya McDaniel; Gloria D. Whisenhunt;
Call 311 or 336-727-8000 County Manager: Dudley Watts,Jr.
Winston-salem/Forsyth County Utility Commission: Randall S. Tuttle, Chair; L. Wesley Curtis, Jr., Vice Chair; Harold E. Day; Tom Griffin; Yvonne H. Hines;
citylink@cityofws.org Duane Long; Hugh W. Jernigan; Chris Parker; Donald R. Stewart; Allan Younger
✓ Fecal coliform data dated April 8, 2016
The P.W. Swann WTP has acreage adjacent to the residuals lagoons available for land application. In
addition to this area, the City of Winston-Salem has been working with local area farmers to place
residuals on pastureland as the need arises.
W. Neilson Water Treatment Plant
Completed form RSC 11-13 which includes the following:
✓ Form RSC 11-13
✓ Map of plant site (field for land application varies based on contractor)
✓ Process diagram (waste facilities highlighted in green)
✓ Black & Veatch's design criteria estimated residuals quantitative production rates
✓ R.W. Neilson's Solids Handling Plan
✓ TCLP and corrosivity sample results dated March 1, 2016
✓ Nutrient metal results from our most recent sampling events from samples collected
April 25, 2019 and September 11, 2019
✓ Fecal coliform data dated March 1, 2016
The R.W. Neilson WTP's land application sites vary based on the current contractor. Contracts are
awarded to the lowest responsive responsible bidder. Our contracts are structured that each contractor
is responsible for finding additional land to apply the material as per our permit conditions.
R.A. Thomas Water Treatment Plant
• Completed form RSC 11-13 which includes the following:
✓ Form RSC 11-13
✓ Map of plant site
✓ Process diagram (waste facilities highlighted in green)
✓ Black & Veatch's design criteria estimated residuals quantitative production rates
✓ R.A. Thomas's Solids Handling Plan
✓ TCLP and corrosivity sample results dated April 26, 2016
✓ Nutrient metal results from our most recent land application samples collected August
30, 2017
✓ Fecal coliform data dated April 26, 2016
In 2018, residuals generated at the R.A. Thomas WTP were hauled to the Hanes Mill Road Landfill.
located at 325 W. Hanes Mill Road, Winston-Salem 27105 and plans are to continue this practice until
further notice.
Once reviewed, should you have any questions regarding this application, please contact Bill Brewer at
(336) 397-7727.
Sincerely,
Courtne L. river, P.E.
Utilities Director
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
S. DANIEL SMITH
Director
NORTH CAROLINA
Environmental Quality
July 7, 2020
Mr. Bill Brewer
Winston-Salem/Forsyth County Utilities Commission
Post Office Box 2511
Winston-Salem, North Carolina 27102
SUBJECT: Notice of Deficiency (NOD-2020-PC-0375)
2019 Annual Report Review
Swann WTP, Neilson WTP, and Thomas WTP
Distribution of Class A Water Treatment Plant Residuals
Permit No. WQ0031314
Forsyth County
Dear Mr. Brewer:
The Division of Water Resources (DWR) acknowledges receipt of your 2019 Annual Report for the subject
permit. A review of this report was conducted by DWR staff person Jim Gonsiewski. The following
deficiency was noted from the review:
Attachment A of the Permit states that the yearly maximum dry tons to be distributed annually from the Neilson
WTP is 1,499 dry tons. A total of 2,334.69 dry tons from the Neilson WTP were distributed in 2019. This is
an exceedance of 835.69 dry tons for the year.
Please provide a response to this letter within 30 days of receipt by your office indicating the corrective actions
taken to address this deficiency. If you anticipate this condition occurring again, this office recommends that
you apply for a permit modification to increase the permit limit. If this exceedance occurs again without a
permit modification, a Notice of Violation may be issued.
If you or your staff have any questions concerning this letter, please contact me or Jim Gonsiewski at (336)
776-9800 or via email at jim.,-,onsiewski_�i_ncdenr.gov.
Sincerely,
ED—Signed by:
LoriT.T*Alier
Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ — WSRO
cc: Forsyth County Environmental Health (Electronic Copy)
Courtney Driver — City of Winston-Salem (Electronic Copy)
WSRO Electronic Files
Laserfiche Files
North Carolina Department of Environmental Quality Division of Water Resources
Winston-Salem Regional Office V 450 West Hanes Mill Road. Suite 3001 Winston-Salem, North Carolina 27105
"� 336.776.9800
.Winston-Salem / Forsyth County
! J : ti f It1e5
Water • Wastewater • Solid Waste
P.W. Swann Water Treatment Plant, 2800 River Ridge Road, Pfafftown, NC 27040
0: 336-727-8000, F: 336-946-2574, wsfcutilities.org
July 13, 2020
Mr. Lon T. Snider —Regional Supervisor
NC DEQ- Water Quality regional Operations Section
450 West Hanes Mill Road
Suite 350
Winston-Salem, NC 27105
Subject: Notice of Deficiency (NOD-2020-PC-3075)
2019 Annual Permit Review
Swann WTP, Neilson WTP and Thomas WTP
Distribution of Class A Water Treatment Plant Residuals
Permit No. WQ0031314
Forsyth County
Dear Mr. Snider,
This letter is in response to your Notice of Deficiency (NOD-2020-PC-3075) letter dated July 7, 2020
regarding an exceeciance of the Neilson WTP's permit distribution limit of 1,499 dry tons of residuals.
This hauling event represents residuals generated over a 34-month period for an average annual
production rate of 824 dry tons per year ([2,334.69 DT's _ 34 months] X 12 Months). Lagoon #2 was in
service from January 2016 until April 2017 and lagoon #3 was in service from April 2017 until October
2018. Under normal circumstances at the Neilson Plant, one lagoon is clean and ready for service, one
lagoon is drying and one lagoon is in service. During the 2015 and 2017 calendar years, the Neilson WTP
did not distribute any residuals, which created a "backlog" that was caught up in 2019 by hauling more
than one lagoon. The residuals hauled in calendar year 2019 eliminated any backlog and we have
returned to our normal schedule. In addition we will be applying for a major modification to our permit
for the Neilson WTP requesting a generating limit of 2,500 dry tons to eliminate this from being an issue
should we be presented with the same situation in the future. Our existing permit expires in February
2021 and I am currently preparing the renewal application.
If you have any questions regarding this matter, please contact me at 336-397-7727.
Sincerely,
William C. Brewer
Water Treatment Superintendent
City Council: Mayor Allen Joines; Den Ise D. Adams, Mayor Pro Tempore, North Ward; Dan Besse, Southwest Ward; Robert C. Clark, West Ward; John C. Larson,
South Ward; Jeff Maclntosh, Northwest Ward; Morticia "Tee -Tee" Parmon, Northeast Ward; Annette Scippio, East Ward; James Taylor, Jr., Southeast Ward;
City Manager: Lee D. Garrity
County Commissioners: David R. Plyler, Chair; Don Martin, Vice Chair; Fleming El -Amin; Ted Kaplan; Richard V. Linville; Tonya McDaniel; Gloria D. Whisenhunt;
Call 311 or 336-727-8000 County Manager: Dudley Watts, Jr.
Winston-Salem/Forsyth County Utility Commission: Randall S. Tuttle, Chair; L. Wesley Curtis, Jr., Vice Chair; Harold E. Day; Tom Griffin; Yvonne H. Hines;
citylink@cityofws.org Duane Long; Hugh W. Jernigan; Chris Parker; James Ruffin; Donald R. Stewart; Allan Younger
State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted. the Ai)vlicant shall submit one original and two conies of the application and
sunportino_ documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permittin Unit website
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
❑ Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
❑ The project name should be consistent on the plans, specifications, etc.
❑ The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106( h i. An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
[✓]/If this project is for a modification of an existing permit, submit one copy of the existing permit.
[✓Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification New Permit Major Modification I
Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395
Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245
1 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
❑ List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 06-16 Pagel of 3
D. Pro ram Information (All Application Packages)
Provide a narrative explaining the following:
9w the materials will be handled and transported from where the residuals were produced to where it will be treated.
w the residuals will be processed/treated (attach process flow diagram).
9 [W
ow leachate collection will be handled.
Where the residuals will be stored until processed.
Vthe final product will be distributed (packaging, bulk, etc.)
t nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
2 ach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
Prttovide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
info ation:
[me and address of the person who prepared the residual that is sold or given away.
L'7 A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
Wi formation sheet.
rstatement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
3911duals into any surface waters.
VA
ormation on all applicable setbacks in accordance with 15A NCAC 02T .1�b..
tatement that the residuals shall be applied at agronomic or recommended rates for intended uses.
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INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3
H. Op e ation and Maintenance Plan (New and Renewal Application Packages)
For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
FZK,qS,ubmit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum:
511"Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
�aintenance schedules; may include equipments calibration, maintenance of signs, etc.
[/Safety measures; may include safety training program, manuals, signs, etc.
pill response plan; including control, containment, remediation, emergency contact information, etc.
[Inspection plan including the following information;
/[]Fames and titles of personnel responsible for conducting the inspections.
requency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
[cation(s) and inspection frequency are representative of the residuals management program.
Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
hat noncompliance is observed.
ampling and monitoring plan including the following information;
ames and titles of personnel responsible for conducting the sampling and monitoring.
Vj�)etailed
description of monitoring procedures including parameters to be monitored.
frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: (919) 807-6464
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: (919) 807-6496
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3
State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
1. APPLICANT INFORMATION:
1. Applicant's name: Winston-Salem/Forsyth County Utilities Commission
Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership Privately -Owned Public Utility
❑ Federal 0 State ® Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Courtney L. Driver Title: Utilities Director
Applicant's mailing address: 101 N. Main Street
City: Winston-Salem State: NC Zip: 27101-
Telephone number: (336) 727-8000 Email Address: courtneyd(&cityofws.org
2. Consultant's name: Jeff Coggins License Number (for P.E.): NC - 20626
Affiliation: N On Staff ® Retained (Firm: Black & Veatch -Charlotte Office)
Consultant's mailing address: 10715 David Taylor Drive, Suite 240
City: Charlotte State: NC Zip: 28262-
Telephone number: (704) 510-8415 Email Address: cogginsjdkbv.com
3. Fee submitted: $0.00 — None required for Permit Renewal (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, 0 renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00031314
Date of most -recently issued permit: March 1, 2016
Date of most -recently certified Attachment A (if different than the permit): March 28, 2016
III. FACILITY INFORMATION:
1. Name of residuals processing facility: P.W. Swann Water Treatment Plant
City: Pfafftown State: NC Zip: 27040-U
Coordinates: Latitude: N36° 8' 51.5" Longitude: W80° 25' 14"
Datum: DMS Level of accuracy: 100%
Method of measurement: Survey
County where facility is located: Fors h
2. Facility contact (person familiar with residuals preparation):
Name: Bill Brewer Title: Water Treatment Superintendent
Mailing address: 2800 River Ridge Road
City: Pfafftown State: NC
Telephone number: (336) 397-7727
Zip: 27040-8435
E-mail address: billbacityofws.org
FORM: DCAR 06-16 Page 1 of 3
3. Is the residual process facility also the generator? ® Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: Until distributed. Please refer to Operation and Maintenance Plan for Swann, Neilson
and Thomas WTP's for information on how residuals will be processed at each facility. days (Note: the Division requires
minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other (explain); Please refer to Operation and Maintenance Plans submitted with this application for how residuals will be
distributed or managed b, each water treatment facility.
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
er 1.0 dry ton of residuals ton)
Not a licable
Not applicable
3. Approximate amounts of the residuals received and processed at the facility: Swann WTP — 750, Neilson -1.499 and Thomas
— 750 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 2,999 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Please refer to the Operation and Maintenance Plans submitted for how each
facility will store and handle residuals produced.
6. Does the facility have a stormwater management plan? ❑ Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: When necessan: silt
fence and/or earthen berms will be used to prevent storm water runoff from entering surface waters as per the Operation and
Maintenance Plans.
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
-- i
RSC 06-16.doc
FORM: DCAR 06-16 Page 2 of 3
Professional Engineer's Cer-tifleation! (Appheation invelying New or- Changes to Treatment or- Storage Units)
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
I, ,Courtney L. Driver Winston-Salem/Forsylh Counly Utilities Director
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for WO031314 P.W. P.W. Swann WTP. R.W. Neilson WTP and R.A. Thomas WTP
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
0I
Signature: Date: &4,
FORM: DCAR 06-16 Page 3 of 3
Water Resources
ENVIRONMENTAL QUALITY
PAT MCCRORY
{iamneir
DONALD R. VAN DER VAART
Secrem y
S. 'JAY ZIMMERMAN
Direciar
February 9, 2016
ROT] I.IARGRovE — DIRECTOR or. UTILITIES
WINsTON-SALEWFORsyni COUNTY UTILiTMS COMMISSION
POST OFFICE Box 2511
WINsTON-SALEM, NORTIi CAROLINA 27102
Dear Mr. Hargrove:
Subject: Permit No. WQ0031314
P. W. Swann WTP
Distribution of Class A Water
Treatment Plant Residuals
Forsyth County
In accordance with your permit renewal request received December 2, 2015, we are forwarding
herewith Permit No. WQ00313I4 dated February 9, 2016, to Winston-Salem/Forsyth County Utilities
Commission for the continued operation of the subject residuals management program. Please'note that
this renewed permit shall become effective on March 1, 2016 (i.e. the day after the expiration date of the
existing permit).
This permit shall be effective from March 1, 2016, until February 28, 2021, shall void Permit No.
WQ0031314 issued November 30, 2012, and shall be subjeetto the conditions and limitations as specified
therein. Please pay particular attention to the monitoring requirements listed in Attachment A for they may
differ from the previous pexmit issuance. Failure to establish an adequate system for collecting and
maintaining the required operational information shall result in future compliance problems.
Please note the following permit conditions are new since the last permit issuance dated
November 30, 2012:
➢ Condition 111.9. — There are new provisions for the utilization agreement compared to Old
Condition I1I.9., e.g., can be dissolved at request of those receiving residuals or sale of land;
the length of agreement is up to parties concerned, Read carefully.
D Condition II1.13. — Similar to Old Condition III.13., but now if the Permittee knows that those
receiving residuals are over -applying, the Permittee shall report this to the Winston-Salem
Regional Office.
There was a request to remove Condition III.B.h, from the Perinit, i.e., the soil pH requirement.
The laboratory results showed that the pH of the residuals to be applied was less than 6.5. Because the pH
is this low, Condition 111.81, remains in the permit even though it is water treatment plant residual being
applied.
State ofNortli Carolina lEnvkomaontal Quality Wator Resoorces i water Quality Permitting l ] Ion-DIScharge Aennitting
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919 807 54&
Mr. Ron Hargrove
February 9, 2016
Page 2 of 2
If any pants, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes; and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Troy Doby at (919) 807-
6336 or troy.doby@ncdenr.gov
Sincerely,
/
�Jay Zimmerman, P. G., Direct
O Division of Water Resources
cc, Forsyth County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Beth Buffington -- Protection and Enforcement Branch (Electronic Copy)
Digital Permit Archive (Electronic Copy)
Central Piles
NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
DISTRIBUTION OF CLASS A WATER TREATMENT PLANT RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Winston-Salem/Forsyth County Utilities Commission
Forsyth County
FOR THE
continued operation of a residuals management program for Whiston-Salem/Forsyth County Utilities
Commission and consisting of distribution of CIass A Water Treatment Plant residuals generated by the
approved facilities listed in Attachment A with no discharge of wastes to suuface waters, pursuant to the
application received December 2, 2015, and in conformity with other supporting data subsequently tiled
and approved by the Department of Environmental Quality and considered a past of this permit. The use
and disposal of residuals are regulated under Title 40 Code of Federal Regulations Pail 257. This permit
does not exempt the Permittee from complying with the federal regulations.
This permit shall be effective from March 1, 2016, until February 28, 2021, shall void Permit No,
WQ0031314 issued November 30, 2012, and shall be subject to the following specified conditions and
limitations:
1. ti CHEDULES
1. No later than six months prior to the expiration of this permit, the Pennittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renew the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application.
[15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109)
H. PERFORMANCE STANDARDS
1. The subject residuals management program shall be effectivelymaintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance
conditions due to improper operation and maintenance, the Permittee shall immediately cease
distribution of residuals, contact the Winston-Salem Regional Office supervisor, and take any
immediate corrective actions. [G.S. 143-215.11
WQ0031314 Version 2.0 Shell Version 151201 Pagel of I I
2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02B .0200,
02L -.0100]
3. only residuals generated by the facilities listed in Attachment A are approved for distribution in
accordance with this permit. [G.S. 143-215.11
4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed
the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(ndiligrams per kilogram)
Monthly Average
Concentration
(ni ligrams per kilogram) -
Arsenic
_l 75
- - - —41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
Mercury
57
17
Molybdenum
75
n/a
-
Nickel
420
420
Selenium
100
100
i Zinc
7,500
2,800
[15A NCAC 02T .11051
5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T
.1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [I 5A NCAC
02T .1106]
6. Setbacks for treatment and storage facilities shall be as follows:
Setback Description Setback
_ (feet_
Habitable residence or place of public assembly under separate ownership or not 100
to be maintained as part of the project site
Property lines 50
Private or public water supply 100
Surface waters (streams — intermittent and perennial, perennial waterbodies, and 50
wetlands)
Wells with exception to monitoring wells 100
All treatment and storage facilities were originally permitted prior to September 1, 2006
[15A NCAC 02T .1108]
WQ0031314 Version 2.0 Shell Version 151201 Page 2 of 11
7. Setbacks for Class Aland applied built residuals shall be as follows:
Setback by residual type
Setback Description
(feet)
Liquid
Cake*
Private or public water supply
100
100
Surface waters (streams — intermittent and perennial,
100
25
perennial waterbodies and wetlands)_
Surface water diversions (ephemeral streams,
0
waterways, ditches)25
Groundwater lowering ditches (where the bottom of
25
0
the ditch intersects the SRWT)
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15%
solids by weight and can be stacked without flowing, as well as can be handled, transported and
spread as a solid (e.g., using a backhoe, front end loader, clinger spreader, broadcast spreader or
other equipment designed for handling solid materials) without leaving any significant liquid
fraction behind,
[15A NCAC 02T ,1108]
8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based on the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http-//nutrients.soil.nesu.edu/yields/index.Ilip). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(htt3�://www.ncggr.aov/SWC/tech/documents/9tb Guidance Doc 100109.>.4f).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards (Ltl; i.,-fe.so.errov.usda.-Lov/NH:.)/i.)ractice-standards/standards/590.p a..
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action,
[I SA NCAC 02T .1109(b)(1)(k)]
WQ0031314 Version 2.0 Shell Version 151201 Page 3 of 11
The Permittee shall not distribute Class A Water Treatment Plant residuals that have a sodium
adsorption ratio (SAR) of I0 or higher without prior written Division approval. The Permittee may
seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high
SAR content; has agreed on proper residual application rates; and has agreed to- operational
considerations to ensure that the high SAR content will not adversely impact the receiving sites.
Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a
mechanism for maintaining site integrity and conditions conducive to crop growth, ran be obtained
from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services,
the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist.
[ISANCAC 02T .0108(b)(1)]
III. OPERATION AND MAINTENANCE RE, QU REMENTS
1. The residuals management program shall be properly maintained and operated at all times. The
program shall be effectively mauitained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. [ 15A NCAC 02T .1110]
2. The Permittee shall maintain. an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan,
at the minimum, shall include:
a. Operational functions;
b. Maintenance schedules;
e. Safety measures;
d. Spill response plan;
e. Inspection plan including the following information:
i. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC, and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions to be taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
notification requirements under the monitoring and reporting section of the permit;
f. Sampling and monitoring plan including the following information:
i. Names and/or titles of personnel responsible for conducting the sampling and monitoring;
I Detailed description of monitoring procedures including parameters to be monitored;
iii. Sampling frequency and procedures to assure that representative samples are being collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The safnpling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen reduction requirements (e.g. facilities that land apply multiple times per year
but have an annual sampling fiequency, may need to sample during winter months when
pathogen reduction is most likely to be negatively affected by cold temperatures).
[15A NCAC 02T A 1001
WQ0031314 Version 2.0 Shell Version 151201 Page 4 of i l
3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification ofthe facility, the Permittee shall designate and employ a certified operator in responsible
charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC
08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 080. 0204,
or as specified in the most recently approved O&M plan (i.e., see Condition III. 2), and shall comply
with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement '
Branch at (919) 707-9105. [15A NCAC 02T .0117]
4. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be
maintained at the land application sites during land application activities. [15A NCAC 02T
.0108(b)(1)]
5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained In all residuals transport and application vehicles. [15A NCAC 02T .1110]
6, When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind
erosion and surface runoff from conveying residuals from the land application sites onto adjacent
properties or into surface waters. [G.S. 143-215.1]
7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
management plan outlined by the local Cooperative Extension Office, the Department of Agriculture
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. [15A NCAC 02T .1109(b)(1)]
8. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulkresiduals or the application causes the contravention of surface
water or groundwater standards;
d. Ifthe land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur,
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
IS% for injected or incorporated bulk liquid residuals;
It. If the soil pH is not maintained at 6.0 or greater, unless Sufficient amounts of lime are applied to
achieve a final soil pH of at least 6.0, or if an agronomist'provides information indicating that the
pH ofthe soil, residuals and Tune mixture is suitable for the specified crop, Any approved variations
to the acceptable soil pH (6.0) will be noted in this permit;
i. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
tJSDA no -till program shall be exempted from meeting this vegetative cover requirement;
j. If the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
k. If the vertical separation of bedrock and the depth of residuals application is less than one foot,
WQ0031314 Version 2.0 Shell Version 151201 Page 5 of 11
1. Application exceeds agronomic rates.
[15A NCAC 02T ,11091
9, A Utilization Agreement between the Permittee, his subcontractor distributing and applying the
residuals, and the entity agreeing to accept Class A bulk residuals shall be in place prior to distribution
of the bulk residuals. The agreement shall specify the subcontractors and the agreeing entity's
responsibilities. The Permittee, the subcontractor, and the entity accepting the Class A bulk residuals
shall sign the Utilization Agreement, The Utilization Agreement shall have a clause allowing the
recipient of the residuals to end the Utilization Agreement at any time by notifying the Permittee in
writing. If the recipient of the residuals sells the property, the Utilization Agreement shall automatically
terminate. If the permit is rescinded, the Utilization Agreement shall automatically terminate. The
duration of the Utilization Agreement shall be one to which the Permittee, the subcontractor, and the
recipient of the residuals agree. Any changes in the agreement that are necessitated by changes in the
permit shall be mailed to the subcontractor and the recipient of the residuals by certified mail with
return receipt. The Permittee shall keep these records on file for inspection by the Division for each
Utilization Agreement while that Utilization Agreement is in force. 115A NCAC 02T .0108(b)(1), 02T
.1104j
10. At a minimum, the Utilization Agreement shall stipulate the following;
a. By agreeing to accept the bulk Class A residuals, it is recognized that the application of these
residuals is allowed under the conditions of this agreement including the prohibitions contained in
Condition 111.8. Land application of Class A residuals is considered the beneficial reuse of a waste
under 15A NCAC 02T .1100, and has been deemed permitted under 15A NCAC 02T .1103(4)
provided the conditions of this agreement are met. Any action resulting in damages to surface water
or groundwater, caused by failure to follow the conditions of this agreement, is subject to Division
enforcement action;
b, Application of Class A residuals shall meet the following application requirements:
i. Residuals shall not be stockpiled for more than 60 days (after the delivery of the last load)
unless the permittee notifies the Winston-Salem Regional Office and receives approval to
exceed the 60 day limit. At a minimum, the information provided shall be, the location, the
date that the last load was delivered, the quantity of residuals stockpiled, the percent solids of
the residuals stockpiled, measures taken to prevent stockpile runoff (e.g. placement, perimeter
berms, etc.) and the anticipated date the residuals will be spread.
ii. Application of bulk residuals shall not occur within 100 feet of a public or private water supply
source;
iii. Application of bulk residuals shall not occur within 100 feet of any well, with the exception of
Division approved monitoring wells;
iv. Application of bulk residuals shall not occur within 25 feet of surface waters.
c. The generator of the Class A bulk residuals shall provide information on the proper use of the
residuals, including information on the recommended application rates.
d. The applicator or party accepting bulk residuals from the Permittee shall supply all third parties
receiving bulk residuals with documentation specifying that application shall occur consistent with
the utilization agreement,
e. Instructions, including contact information for key personnel, shall be provided to the applicator or
party receiving bulk residuals in the event that any requirements specified in the utilization
agreement are not met.
f, A copy of the Utilization Agreement shall be maintained at the land application sites when bulk
residuals are being applied.
[15A NCAC 02T .0108(b)(1), 02T .11041
WQ0031314 Version 2.0 Shell Version I51201 Page 6 of 11
I I . All residuals shall be adequately stored to prevent untreated leaohate runoff. The finished product may
be placed on a concrete pad, placed under shelter or physically covered until it is distributed to the
buyer. If an alternate storage site is used, approval must be obtained from the Division. [15A NCAC
02T .0108(b)(1)]
12. A label shall be affixed to the bag or other container in which residuals are sold or given away for land
application, or an information sheet shall be provided to the person who receives Class A residuals. At
a minimum, the label or information sheet shall contain the following:
a, The name and address of the person who prepared the residuals;
b, A statement that residual land application is prohibited except in accordance with the instructions
on the label or information sheet,
c. A statement identifying that this material shall be prevented from entering any public or private
water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.);
d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its
intended use.
[I5ANCAC 02T .I 109(a)]
13. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals
contrary to the condition of the signed Utilization Agreement. The Permittee shall report to the
Winston-Salem Regional Office as per repotting conditions under Condition IV.8. any person or entity
known to be applying residuals contrary to the condition of the signed Utilization Agreement. [I5A
NCAC 02T .1103(a)]
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IV. MONITORING AND REPORTING RC UMMENTS
1. Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses)
necessary to ensure groundwater and surface water protection shall be established, and an acceptable
sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)]
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40
CFR Part 261 shall not be used or disposed under this permit. The analyses [eorrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the
frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter
is in parentheses):
Arsenic (5.0)
1,4-Diehlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Diehloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Tetrachloroethylene (0.7)
Chlordane (0.03)
Chlorobenzene (100.0)
Hexachlorobenzene (0.13)
Heptachlor (and its hydroxide)
OA08
Toxaphene (0.5)
Triohloroethylene (0.5)
Chloroform (6.0)
Chromium (5.0)
IIexachloro-1,3-butadiene (0.5)
Hexachloroethane (3.0)
2,4,5-Trichlorophanol (400.0)
m-Cresol (200.0)
o-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
Vinyl chloride (0.2)
p-Cresol (200.0)
Mercury (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200A)
[15A NCAC 13A A 102(b), 02T .1101, 02T .11051
3. An analysis shall be conducted on residuals from each source generating facility at the frequency
specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years.
The analysis shall include the following parameters:
Aluminum
Mercury
Molybdenum
Potassium
Ammonia -Nitrogen
Selenium
Sodium
Arsenic
Nickel
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
_
Percent Total Solids
pH
TKN
Calcium
Copper
Zinc
Lead
Phosphorus
Plant Available Nitrogen
Magnesium
(by calculation)
WQ0031314 Version 2.0 Shell Version 151201 Page 8 of 11
[ 15A NCAC 02T .1101 ]
4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency
specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the
approved O&M plan. The required data shall be specific to the stabilization process utilized, and
sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC
02T .1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be
specified in Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .1111(c)]
5. Laboratory parameter analyses shall be petforined on the residuals as they are distributed, and shall be
in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .0505]
6. The Permittee shall maintain records tracking all bulk residual distribution or land application events
performed by the Permittee. At a minimum, these records shall include the following:
a. Source of residuals;
b. Date of distribution/land application;
c. Name and address of recipient of residuals; ,
d. Volume of residuals distributed to each recipient;
e,. Intended use of residuals;
f. If land application events performed by the Permittee -Nitrogen Application Rate based on RYES
(if using data obtained from the North Carolina State University Department of Soil Science
Website, the printout page shall be kept on file and reprinted every five years).
[15A NCAC 02T .0109(a)]
7. Three copies of an annual report shall be submitted on or before March 11t. The annual report shall
meet the requirements described in the Instructions for Residuals AV lication AnnualRtorting Forms.
Instructions for reporting and - annual report forms are available at
http;l/portal.ncdenr.oralweb/wy/atas/lau/reporting, or can be obtained by contacting the Land
Application Unit directly. The annual report shall be submitted to the following address;
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
(15ANCAC 02T .1111(a))
WQ0031314 Version 2.0 Shell Version 151201 Page 9 of 11
8. Noncompliance Notification
The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (3 36)
776-9800, as soon as possible, but in no case more than 24 hours or on the next working day following
the occurrence or first knowledge of the occurrence of any of the following:
a. Distribution of residuals abnormal in quantity or characteristic.
b. Any failure of the distribution program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
e. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency
Response personnel at telephone number(800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons
reporting such occurrences by telephone shall also file a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)]
V. INSPECTIONS
1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)]
2. Prior to each bulk residuals distribution event, the Permittee or his designee shall inspect the residuals
processing and storage facilities to identify malfunctions, facility deterioration and operator errors that
could result in discharges to the environment, a threat to human health or a public nuisance. The
Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection,
observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall
maintain this inspection log for a period of five years from the date of inspection, and this log shall be
made available to the Division upon request. [15A NCAC 02T .0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or facilities permitted herein
at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy
any records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples. [G.S.143-215.3(a)(2)]
VL GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to
143-215.6C. [G.S.143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals land application events are not carried out in
accordance with the conditions of this permit. [ 15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation. [G.S. 143-215.11
WQ0031314 Version 2.0 Shell Version 151201 Page 10 of 11
The issuance of this permit does not exempt the Permittee from complying with any and all statutes,
miles, regulations, or ordinances, which may be imposed by other jurisdictional government agencies
(e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in
15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Permit NCG010000; any requirements pertaining to wetlands under 15A
NCAC 02B ,0200 and 0211.0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [I 5A NCAC 02T .0105(c)(6)]
S. In the event the residuals program changes ownership or the Permittee changes his name, a formal
permit modification request shall be submitted to the Division. This request shall be made on official
Division forms, and shall include appropriate documentation from the parties involved and other
supporting documentation as necessary. The Permittee of record shall remain fully responsible :For
maintaining and operating the residuals program permitted herein until a permit is issued to the new
owner. [15A NCAC 02T .0104]
6. This permit is subject to revocation or unilateral modification upon 60 days notice fioin the Division
Director, in whole or part for the requirements listed in 15A NCAC 02T .0110, [15A NCAC 02T .0110]
7, Unless the Division Director grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittee exemplifies any of the criteria in I SA NCAC 02T .0120(b),
[I 5A NCAC 02T .0120]
S. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T
.0105(e)(3)]
Permit issued this the 9 h day of February 2016
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
S. Jay Zimmerman, P.G., Director
Division of Water. Resources
By Authority of the Environmental Management Commission
Permit Number WQ00311314
WQ0031314 Version 2.0 Shell Version 151201 Page 11 of 11
THIS PAGE BLANK
Water Resources
ENVIRONMENTAL OUALITY
PAT MCCRORY
Gulvraar
DONALD R_ VAN DER VAART
Secretary
S. JAY ZIMMERMAN
Director
March 28, 2016
RON HARGROV}s — DIRECTOR OF UTILITIES
WINSTON—SALEMMORSYTH COUNTY UTILITIES COMMISSION
POST OFFICE BOX 2511
WINSTON—SALEM, NORTH CAROLINA 27102
Dear Mr. Hargrove:
Subject: Permit No. WQ0031314
Correction
P. W. Swann WTP
Distribution of Class A Water
Treatment Plant Residuals
Forsyth County
In accordance with an oral request received March 28, 2016 fiom you, we are forwarding herewith
corrected Attachment A of Permit No. WQ0031314 issued February 9, 2016.
The correction to the subject permit is as follows:
1. The residuals quantities for Thomas WTP and Nielsen WTP were reversed.
Please replace Attachment A of Permit No. WQ0031314 issued February 9, 2016 with the
enclosed corrected Attachment A.
If you need additional information concerning this permit correction, please contact Troy Doby at
(919) 807-6336 or troy.doby@ncdenr.gov.
Sincerely,
S. Jay Zimmerman, P.G., Direct
Division of Water Resources
Enclosure
cc: Forsyth County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Beth Buffington, Public Water Supply Section — Protection and Enforcement Branch
Digital Permit Archive WQ0031314 (Electronic Copy)
Central Files
State of North Carolina I Environmental Quality I WaterResourcea ( Water Quality Permitting I Non -Discharge Permitting
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919 807 6464
- r--z-
This Page Blank
ATTACHMENT A - Approved Residual Sources Certification Date: February 9, 2016 -
Winston-Salem/Forsyth County Utilities Commission Permit Number: WQ0031314 Version: 2.0-
Class A Water Treatment Plant Residuals Product Generated for Distribution
Owner
Winston-Salem/Forsyth County
Utilities Commission
Winston-Salem/Forsyth County
Utilities Commission
Winston-Salem/Forsyth County
Utilities Commission
Total
Facility Name County permit
Number
Swann WTP
Neilson WTP
Forsyth i NCO079821
Forsyth I NCO086011
Biological
Monitoring
Maximum
Frequency for
Monitoring
Frequency for
Monitoring
Frequency for
Approved
Residuals
Dry
D Tons
per Years Non -hazardous
Metals and
Pathogen &
Mineralization
Characteristics I
Nutrients 3•11
See Table Below
Vector Attraction
Reductions° e
None
state
No 750
Once per permit
cvele
No 1,499
Once per r permit
See Table Below
`None
Thomas WTP I Forsyth I NCO086762 I No
750 Once per cycle
See Table Below None
2,999
1. Maximum Dry Tons per Year is the amount of residuals approved for distribution from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV,2.
3. Testing of metals and nutrients as stipulated under permit Condition 1V.3.
4. Analyses of pathogen reductions as stipulated under pen -nit Condition IV_4.
S. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Distributed
short tons l2er ear
Monitoring Frequency
Established in 40 Cr, R 503 and 1SA NCAC 02T .1111
<319
i/Year
==-319 - c1,650
11 Quarter (4 times per ear)
- 1,650 - <-16,500
1/60 Days 6 times er ear)
—16500
lhnonth I times wear)
6. Water Treatment Plant residuals are exempt from meeting the pathogen & vector attraction reduction requirements in Condition IVA, provided they are not mixed with residuals that have
been generated during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The Water Treatment
Plant residuals must be treated and processed in a manner as to not meet the definition of "Biological Residuals" as defined in 15A NCAC 02T .I 102(6).
If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring
is required), then no sampling data is required during the period of inactivity. The annual report shalI include an explanation for missing sampling
data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional
information and clarification.
WQ0031314 Version 2.0 Attachment A Page 1 of 1
SCOPE OF WORK
SWANK LAGOON CLEANOUT
Furnish all labor, materials, equipment, supervision, insurance and abide by all local, state
and federal codes applicable to perform the alum residuals removal and land application
from the P.W. Swann Water Treatment Plant lagoon #2 as per the city's current Land
Application Permit #WQ0031314. The Contractor will provide the following services:
1. Removal of residuals from lagoon #2 and haul it to an approved land application
site provided by the Contractor.
• The Contractor is responsible for coordinating and acquiring suitable land
for application of the residuals and maintaining records of quantities of
residuals applied to each parcel in accordance with agronomic rates as
defined in Permit WQ0031314.
• The Contractor shall be responsible for collecting and testing a
representative set of soil pH's for each parcel of land residuals are to be
applied to. Should the pH of these samples be below 6.0 on average the
Contractor shall be responsible for calculating the amount of lime required
to bring the soil above 6.0 as required by our residuals permit. The
Contractor shall provide a unit cost for lime per ton with their bid which
shall include purchasing the lime, transportation to the parcel's and
application of a sufficient quantity to satisfy the requirements of our land
application permit.
• Special attention is required as not to disturb the Bentonite clay liner at the
bottom of lagoon #2.
2. The Contractor will be required to show certified volumes of tankers used to haul
residuals.
The Contractor will have the responsibility of keeping the roads at and along the
haul route and Swann WTP clean at all times. If it is necessary to have any roads
scraped due to debris it will be done at the expense of the Contractor. The Swann
Plant lagoon area and site roads must be returned to their original condition at the
end of the work. This includes replacing gravel on the gravel road at/around the
lagoons if deemed necessary by the Plant Supervisor.
4. The Contractor will be required to provide maps of the application sites with drawn
boundaries and documentation of the amount of residuals applied on each field per
acre. The Contractor will be required to provide the Plant Supervisor with soil
testing results and maps detailing the approximate locations of soil tests and land
application sites with drawn boundaries delineating where residuals were applied
and documentation regarding the quantity of residuals applied on each field (per
acre).
5. The Contractor shall provide restroom facilities for their employees.
Page 19 of 23
SPECIFICATIONS
Safety
The Contractor is responsible for complying with all applicable OSHA standards during the entire
project duration.
General Site Conditions
Each bidder will be responsible for having knowledge of the site conditions and submitting bids
based on the conditions that exist at the site. A site inspection may be arranged by contacting the
Swann Water Plant Supervisor, Bill Goss, at (336) 945-1179.
Work Hours
Work hours for this project are limited to 7:00 a.m. to 5:00 p.m., Monday through Friday. .
Schedulin--
The Contractor will be expected to begin work within thirty (30) days after receiving a Notice to
Proceed. Work shall progress continuously with sufficient personnel to complete the work within
sixty (60) days. Time extensions may be granted for unusually inclement weather but no change
in price will be allowed.
Equipment
The Contractor will be responsible for furnishing and operating all necessary equipment. The
equipment used will be left to the Contractor's discretion. The Contractor will be required to show
certified volumes of tankers used to haul residuals.
Residuals Removal
The Contractor will be responsible for removing the residuals from the lagoon, hauling to the
deposition site and applying the residuals to the site as per the city's Land Application Permit
WQ031314. The removal of the residuals will be completed without disturbing the bentonite clay
bottom of the lagoon. The Contractor will be responsible for any damage to the clay bottom, or
any other facility that is caused by his work.
Sediment Consistence
The Owner will coordinate with the Contractor on adding water to get the residuals to the desired
consistency for removal. The Contractor is responsible for all equipment necessary to properly
mix, pump, haul and land apply the residuals.
Sediment Volume and PaN-ment
It is estimated there is an average of 3 to 7 feet of residuals present in the lagoon depending on
conditions. The low bidder will be determined by the lowest unit price per gallon. It will be the
Contractor's responsibility to do any surveying or other calculation to determine
approximate volume. Contractors will be provided as builts of lagoon #2 to assist in estimating
volumes of residuals. The Contractor will be paid for based on the calculation (Gallons Removed
X Price/Gallon) as per the Contractor's bid.
No adjustments in price or quantities will be made for items such as mobilization, ramp
construction or removal, sediment fluffing during loading, fuel surcharges, etc. All costs are to be
covered in the unit price per gallon.
Page 20 of 23
Transporting
The Contractor shall furnish all necessary vehicles to transport the materials from the lagoon to
the designated deposition site. The City is requiring that all transport vehicles be of a type that is
watertight to prevent any leakage or spillage along the haul route. In order to prevent excess
damage to the plant grounds and facilities, the haul route across the plant property must be
approved by the Swann Plant Supervisor or his duly appointed representative. Upon completion
of the project, the Contractor will restore the haul route to its original condition. All travel on state
maintained roads shall be in accordance with all local, state and federal transportation rules and
regulations.
Deposition
The material removed from the lagoon shall be applied at a location approved for land application
of alum residuals which is to be coordinated and provided by the Contractor. The Contractor shall
maintain a log documenting the number of gallons removed from lagoon and quantity of gallons
applied to each field each day. This log should be available for inspection by Plant Supervision as
needed. The Contractor shall calculate and adhere to agronomic rates as outlined in Permit
WQ0031314
Dust Control and Road Cleaning
The Contractor shall control dust throughout the entire contract period within project areas and at
all other areas affected by the project. This includes, but is not limited to, paved and unpaved
roads, haul roads, access roads, disposal sites, and material and equipment storage sites. Dust
control measures may include, but are not limited to, wetting down disturbed earth surfaces or
eliminating traffic across them, removing accumulations of dirt from paved areas by hand or
mechanical means, and washing roads at the end of each work day.
Roads utilized by the Contractor during the execution of the work related to this project shall be
inspected by the Contractor frequently on each day that work is being conducted. Any material
spilled onto the roads along the haul route or material tracked onto the road at the lagoon entrance
or at the deposition site during the day shall be removed and the road scraped or washed by a
company normally involved in this type of work at the end of each work day at the expense of the
Contractor. All roads shall be left clear and free of mud, dust, dirt, debris, etc. prior to the
Contractor leaving the project site at the end of each work day. The Commission reserves the
right to require that roads be cleaned more frequently than once a day if it determines that it is
necessary to do so. Additional road cleanings will be at no additional expense to the Commission.
Site Clean Up
The Contractor shall keep the project areas at the lagoon and the disposal site free at all times from
accumulations of waste materials, rubbish, and debris. All wastes shall be removed from the
project areas and disposed of in a manner complying with local ordinances and antipollution laws.
Contractor Field Superintendent
The Contractor shall provide a Project Field Superintendent to supervise this Contract throughout
its duration. The Field Superintendent's responsibilities shall include, but not be limited to, the
following:
The Project Field Superintendent shall be full-time on site during all project activities,
including those of any subcontractor, and shall be the main point of contact for the Project
Page 21 of 23
Manager and Swann Plant staff.
- Be available for contact after working hours should it become necessary
- Coordinate all work and work schedules
- Supervise all field work
- Coordinate with property owners and the public
- Ensure that all work meets all Contract requirements.
- Maintain logs of gallons removed, hauled and applied to each site on a daily basis.
Residuals Testing. Sample Collection and Annual Reyorting
The Contractor shall have on site at all times a foreman responsible for overseeing the work being
performed. The foreman shall coordinate with the Swann WTP Plant Supervisor/ORC regarding
the work performed.
The Contractor shall be responsible for the following:
Soil SamNin��
• Collection and analysis of representative soil samples from all parcels residuals are applied
to prior to residuals application.
• Actual application quantities per acre for lime applied to each parcel.
• Soil reports for each parcel residuals are applied to.
Residuals Sampling and Reporting Deliverables
• The Contractor shall maintain logs for each application site detailing the rate of application
per site (PAN), maps with boundaries drawn showing disposal area for each site and
sodium absorption rate (SAR)/exchangeable sodium percentage (ESP) for the residuals
applied.
• Collection and analysis of residuals to demonstrate that residuals are non -hazardous (i.e.
TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
NOTE: These samples are required once per permit cycle and were collected during
residuals removal in April 2016, therefore, they are not due again until 2021.
• Collection, analysis and delivery of final report to owner of required metals and nutrient
samples as stipulated under permit Condition IV.3 by a NC certified laboratory.
• Adherence to monitoring frequencies based on dry tons as outlined in Condition 5. of
permit Attachment A for metals and nutrients.
• Obtaining signed Land Use Agreements by land owners/entities receiving residuals, City
of Winston-Salem ORC, and representative from company land applying residuals for each
parcel of land residuals are applied to.
• Completion of the following reports necessary for annual reporting which must be
delivered to the ORC no later than February 1 following the year in which residuals were
applied to allow the ORC ample time to review and submit the annual report to the State
of North Carolina.
- DENR Form DMSDF — Class A Annual Distribution and Marketing/Surface
Disposal Certification and Summary Form signed by preparer.
- DENR Form DMSDF — Supplemental Form - Class A Annual Distribution and
Marketing/Surface Disposal Certification and Summary Form — Supplemental
information signed by preparer.
- DENR Form RSSF — Annual Residual Sampling Summary Form signed by
preparer.
Page 22 of 23
- DENR Form RSSF — B Annual Residual Sampling Summary Form signed by
preparer.
- All sample analysis final reports, laboratory data sheets and chain of custodies
supporting above forms.
- Maps of each residuals distribution site with boundaries of residuals application
clearly delineated.
- Soil reports for each parcel residuals applied to.
- Contractor logs for each application site detailing the rate of application per site
(PAN).
- Contractor logs detailing sodium absorption rate (SAR)/exchangeable sodium
percentage (ESP) for the residuals applied for each parcel.
Page 23 of 23
DETAILED SPECIFICATIONS
RESIDUALS REMOVAL AT THOMAS WTP
Scope Of Work
Furnish all labor, materials, equipment, insurance and supervision and abide by all local, state and
federal codes applicable to haul alum residuals from the R.A. Thomas Water Treatment Plants to the
WSFU Utilities Hanes Mill Road Landfill located at 325 W. Hanes Mill Road, Winston-Salem NC
27105. There are two lagoons on the plant site. These lagoons are cleaned out on an approximately
1-year rotation and each lagoon averages approximately 800 cubic yards of material (this number is
an approximation based on historical quantities and can differ, the city cannot guarantee volumes as
they are subject to change based on many factors). Only one lagoon is cleaned each year. The
contractor will provide the following services:
a. Removal of residuals from each lagoon and haul it to WSFC Utilities landfill located at 325
W. Hanes Mill Road, Winston-Salem NC 27105.
b. The Contractor shall provide one price per cubic yard to remove and haul material.
c. WSFC Utilities will pay all tipping fees at Hanes Mill Road Landfill.
d. The residuals may be dry to wet and may have the consistency of cake batter.
e. Residuals will be removed down to the solid bottom of the lagoon being careful not to
remove material from the perimeter of the lagoon and side slopes.
2. The contractor will have the responsibility of keeping the Thomas Water Plant and the road frontage
along Martin Luther King, Jr. Drive clean at all times. If it is necessary to have any roads washed
due to debris on the road, or from complaints by any resident along the route of transport due to
spilled material it will be the financial responsibility of the contractor. The Thomas Plant must be
returned to its original condition at the end of each cleaning. This includes replacing gravel on the
gravel road at/around the lagoons if deemed necessary by the Plant Supervisor.
3. The Contractor shall provide restroom facilities for their employees.
Safety
The Contractor is responsible for complying with all applicable OSHA standards during the entire project duration.
General Site Conditions
Each bidder will be responsible for having knowledge of the site conditions and submitting bids based on the
conditions that exist at the site. A site inspection can be coordinated by contacting the Thomas Water Plant
Supervisor, Donna Lankford, at (336) 788-0152.
Work Hours
Work hours for this project are limited to 7:00 a.m. to 4:00 p.m., Monday through Friday.
Schedulin
The work may commence upon Notice to proceed. The contractor will be expected to begin work within 30 days
after receiving a Notice to Proceed. Work shall progress continuously with sufficient personnel to complete the work
within 30 days of the start of residuals removal. Time extensions may be granted for unusually inclement weather
but no change in price will be allowed.
Equipment
The Contractor will be responsible for furnishing and operating all necessary equipment. The equipment used will
be left to the Contractor's discretion. The, contractor will be responsible for any damage to the gravel, underdrain
system, or any other facility or structure that is the result of their work.
Residuals Removal
The Contractor will be responsible for removing the residuals from the lagoon and hauling them to WSFC Utilities
Hanes Mill Road Landfill. When all residuals removal is complete the lagoon reservoir floor and sides are to be
graded smooth.
IF2082 Residuals Removal at Thomas WTP Page 23 of 32
Residuals Consistency
It is anticipated the material should have a percent solids of approximately 20% or more. However, the owner cannot
guarantee this condition.
Sediment Volume and Payment
It is estimated there is an average of 3.0 feet of sediment present totaling approximately 800 cubic yards in each
lagoon. The low bidder will be determined by the lowest unit price per cubic yard. A contracted licensed surveying
company, hired by the City of Winston-Salem, will perform a grid topographical survey of the material prior to the
Contractor beginning work and after the contractor has completed his work. The contractor will be paid the product
of their submitted unit price in cubic yards multiplied by the volume as determined by the contracted licensed
surveying company's measurements. Therefore, actual quantities may be higher or lower than estimated. The City
of Winston-Salem shall hire a licensed survey company to perform this work and will be the sole basis for
compensation under this contract.
No adjustments in price or quantities will be made for items such as mobilization, ramp construction or removal,
sediment fluffing during loading, fuel surcharges, etc. All costs are to be covered in the unit price per cubic yard.
Transportinn
The Contractor shall furnish all necessary vehicles to transport the materials from the lagoon to the designated
deposition site. The City is requiring that all transport vehicles be of a type that is watertight to prevent any
leakage or spillage along the haul route. In order to prevent excess damage to the plant grounds and facilities, the
haul route across the plant property must be approved by the Thomas Plant Supervisor or his/her duly appointed
representative. Upon completion of the project, the Contractor will restore the haul route to its original condition
which may include reseeding, deposition of stone or other methods to repair worn surfaces of travel. All travel on
state maintained roads shall be in accordance with all local, state and federal transportation rules and regulations.
Dust Control and Road Cleaning
The Contractor shall control dust throughout the entire contract period within project areas and at all other areas
affected by the project. This includes, but is not limited to, paved and unpaved roads, haul roads, access roads,
disposal sites, and material and equipment storage sites. Dust control measures may include, but are not limited to,
wetting down disturbed earth surfaces or eliminating traffic across them, removing accumulations of dirt from paved
areas by hand or mechanical means, and washing roads at the end of each work day.
Roads utilized by the Contractor during the execution of the work related to this project shall be inspected by the
Contractor frequently on each day that work is being conducted. Any material spilled onto the roads along the haul
route or material tracked onto the road at the lagoon entrance or at the disposal site entrance during the day shall be
removed and the road washed at the end of each work day. All roads shall be left clear and free of mud, dust, dirt,
debris, etc. prior to the Contractor leaving the project site at the end of each work day. The Commission reserves
the right to require that roads be cleaned more frequently than once a day if it determines that it is necessary to do so.
Additional road cleanings will be at no additional expense to the Commission.
The awarded Contractor must have an approved Spill and Control Plan that satisfies the North Carolina's
Department of Environmental Quality Aquifer Protection Section's requirements for the material being
hauled. This plan must be submitted for review by the Plant Supervisor prior to residuals being hauled.
Site Clean Up
The Contractor shall keep the project areas at the lagoon and the disposal site free at all times from accumulations of
waste materials, rubbish, and debris. All wastes shall be removed from the proj ect areas and disposed of in a manner
complying with local ordinances and antipollution laws.
Contractor Field Superintendent
The Contractor shall provide a Project Field Superintendent to supervise this Contract throughout its duration. The
Project Field Superintendent shall make routine visits to the plant to monitor his crew's activities and to ensure
smooth operation.
Residuals Samnlin, and Reportine Deliverables
Collection and analysis of one percent (1%) total solids to be used to determine the total dry tons of material hauled.
It is the contractor's responsibility to collect the sample and have it analyzed by NC certified laboratory for
wastewater analysis for percent total solids.
IF2082 Residuals Removal at Thomas WTP Page 24 of 32
SPECIFICATIONS
Safe
The Contractor is responsible for complying with all applicable OSHA standards during the entire project
duration.
General Site Conditions
Each bidder will be responsible for having knowledge of the site conditions and submitting bids based
on the conditions that exist at the site. A site inspection may be arranged by contacting the Neilson
Water Plant Supervisor, Gabe Sparks, at (336) 766-9885.
Work Hours
Work. hours for this project are limited to 7:00 a.m. to 4:00 p.m., Monday through Friday.
Scheduling
It is anticipated that work could begin in early 2018. The contractor will be expected to begin work
within 30 days after receiving a Notice to Proceed, if necessary. Work shall progress continuously
with sufficient personnel to complete the work within 120 days of the start of residuals removal. Time
extensions may be granted for unusually inclement weather but no change in price will be allowed.
Equipment
The Contractor will be responsible for furnishing and operating all necessary equipment. The equipment
used will be left to the Contractor's discretion. The contractor will be responsible for any damage to
the gravel, underdrain system, or any other facility or structure that is caused by their work.
Residuals Removal
The Contractor will be responsible for removing the residuals from the lagoon, hauling them to the
application site and land applying as per the City of Winston-Salem's Land Application Permit
#WQ0031314. The Contractor shall be responsible for removing and disposing of any vegetation that
may have grown on top of the residuals in the lagoons prior to hauling. The residuals will be removed
down to the top of the clay bottom being careful not to remove clay from the perimeter of the lagoon,
bottom and side slopes. When all residuals removal is complete the lagoon reservoir floor and sides are
to be graded smooth.
Residuals Consistency
It is anticipated the material should have a percent solids of approximately 20% or more. However, the
owner cannot guarantee this condition.
Sediment Volume and Pavment
It is estimated there is an average of 3.0 feet of sediment present totaling approximately 3,500-4,000
cubic yards in each lagoon. The low bidder will be determined by the lowest unit price per cubic yard
for residuals land applied. A contracted licensed surveying company, hired by the City of Winston-
Salem, will perform a grid topographical survey of the material prior to the Contractor beginning work
and after the contractor has completed his work. The contractor will be paid the product of their
submitted unit price in cubic yards multiplied by the volume as determined by the contracted licensed
surveying company's measurements. Therefore, actual quantities may be higher or lower than estimated.
The City of Winston-Salem shall hire a licensed survey company to perform this work and will be the
sole basis for compensation under this contract.
IF18145 Residuals Removal From Lagoons at R.W. Neilson WTP Page 24 of 30
No adjustments in price or quantities will be made for items such as mobilization, ramp construction or
removal, sediment fluffing during loading, fuel surcharges, etc. All costs are to be covered in the unit
price per cubic yard.
Transoortin�
The Contractor shall furnish all necessary vehicles to transport the materials from the lagoon to the
designated deposition site. The City is requiring that all transport vehicles be of a type that is watertight
to prevent any leakage or spillage along the haul route. In order to prevent excess damage to the plant
grounds and facilities, the haul route across the plant property must be approved by the Neilson Plant
Supervisor or his duly appointed representative. Upon completion of the project, the Contractor will
restore the haul route to its original condition which may include reseeding, deposition of stone or other
methods to repair worn surfaces of travel. All travel on state maintained roads shall be in accordance
with all local, state and federal transportation rules and regulations.
Deposition
The material excavated from the lagoons shall be deposited as per the city's land application permit.
The contractor is solely responsible for locating suitable land in sufficient acreage for the application of
the material.
Dust Control and Road Clean
The Contractor shall control dust throughout the entire contract period within project areas and at all
other areas affected by the project. This includes, but is not limited to, paved and unpaved roads, haul
roads, access roads, disposal sites, and material and equipment storage sites. Dust control measures may
include, but are not limited to, wetting down disturbed earth surfaces or eliminating traffic across them,
removing accumulations of dirt from paved areas by hand or mechanical means, and washing roads at
the end of each work day.
Roads utilized by the Contractor during the execution of the work related to this project shall be inspected
by the Contractor frequently on each day that work is being conducted. Any material spilled onto the
roads along the haul route or material tracked onto the road at the lagoon entrance or at the disposal site
entrance during the day shall be removed and the road washed at the end of each work day. All roads
shall be left clear and free of mud, dust, dirt, debris, etc. prior to the Contractor leaving the project
site at the end of each work day. The Commission reserves the right to require that roads be cleaned
more frequently than once a day if it determines that it is necessary to do so. Additional road cleanings
will be at no additional expense to the Commission.
The Contractor must have an approved Spill and Control Plan that satisfies the North Carolina's
Department of Environmental Quality Aquifer Protection Section's requirements for the material being
hauled. This plan must be submitted for review by the Plant Supervisor prior to residuals being hauled.
Site Clean Uv
The Contractor shall keep the project areas at the lagoon and the disposal site free at all times from
accumulations of waste materials, rubbish, and debris. All wastes shall be removed from the project
areas and disposed of in a manner complying with local ordinances and antipollution laws.
Contractor Field Superintendent
The Contractor shall provide a Project Field Superintendent to supervise this Contract throughout its
duration. The Field Superintendent's responsibilities shall include, but not be limited to, the following:
- The Project Field Superintendent shall be full-time on site during all project activities, including
IF18145 Residuals Removal From Lagoons at R.W. Neilson WTP Page 25 of 30
those of any subcontractor, and shall be the main point of contact for the Project Manager and
Neilson Plant staff.
- Be available for contact after working hours should it become necessary
- Coordinate all work and work schedules
- Supervise all field work
- Coordinate with property owners and the public
- Ensure that all work meets all Contract requirements.
- Maintain logs of residuals removed, hauled and land applied to each site on a daily basis.
Residuals Sampling and Renortim-, Deliverables
• The Contractor shall maintain logs for each application site detailing the rate of application per
site (PANT), maps with boundaries drawn showing disposal area for each site and sodium
absorption rate (SAR)/exchangeable sodium percentage (ESP) for the residuals applied.
• Collection and analysis of residuals to demonstrate that residuals are non -hazardous (i.e. TCLP,
ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. NOTE:
These samples are required once per permit cycle and were collected during residuals removal
in March 2016, therefore they are not due again until 2021.
• Collection, analysis and delivery of final report to owner of required metals and nutrient samples
as stipulated under permit Condition IV.3 by a NC certified laboratory.
• Collection and analysis of representative soil samples and application of lime when/as required
by Land Application Permit #WQ0031314.
• Adherence to monitoring frequencies based on dry tons as outlined in Condition 5. of permit
Attachment A for metals and nutrients.
• Obtaining signed Land Use Agreements by land owners/entities receiving residuals, City of
Winston-Salem ORC, and representative from company land applying residuals for each parcel
of land residuals are applied to.
• Completion of the following reports necessary for annual reporting which must be delivered to
the ORC no later than February 1 following the year in which residuals were applied to allow the
ORC ample time to review and submit the annual report to the State of North Carolina.
IF18145 Residuals Removal From Lagoons at R.W. Neilson WTP Page 26 of 30
DWR,
State of North Carolina
Department of Environmental Quality
Division of Water Resources
Divislon of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and
supporting, documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Res' uals Source Certification (FORM: RSC 11-15):
[Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
VO
r new or renewed permits, submit a separate certification for each source facility.
Vr modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
omplete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Res' duals Source -Generating Facility Information:
Res
Vach source facility, attach the following:
icinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Ike siduals Land A lication Permits"'.
Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
e to be generated, treated, processed, and stored at the facility.
Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
_Jdocessing.
Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Re ' uals Quality Information:
[��oteac
Fh source facility, attach the following:
[aboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
action reduction requirements.
For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16
Page 1 of 1
RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Winston-Salem/Forsyih County Utilities Commission (P.W. Swann Water Treatment :Plant)
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
R
Swann WTP
Swann WTP
Forsyth
WQ0031314
750
750
R
Swann WTP
Neilson WTP
Forsyth
WQ0031314
2,500
1,499
R
Swann WTP
Thomas WTP
Forsyth
WQ0031314
750
750
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1
State of North Carolina
nWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: P.W. Swann Water Treatment Plant
2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Bill Brewer — Water Treatment Superintendent
Complete mailing address: 2800 River Ridge Road
City: Pfafftown State: NC Zip: 27040-8435
Telephone number: (336) 397-7727 E-mail address: billb@cjtyofws.org
4. Facility physical address: 2800 River Ridge Road
City: Pfafftown State: NC Zip: 27040-8435
Coordinates: Latitude: N36° 8' 51.5" Longitude: W80° 25' 14"
Datum: DMS Level of accuracy: 100%
Method of measurement: Survey
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 25.0 MGD and facility average daily flow: 12.4 MGD
8. Average amount of residuals being generated at this facility 750 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: The treatment facilities for wash water consists of one 1 equalization basin with
a capacity of 0.489 MG's and two 2) residuals lagoons for settling and duving solids with an effective storage volume of
3.2 MG's each.
Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 021.110Z O as:
d Biological Non -Biological
FORM: RSC 06-16 Page 1 of 5
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Research & Analytical Laboratories, Inc, and Date of analysis: 4/8/2016
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: >212 OF (> 140°F)
Passed reactivity test: ®yes ❑no. HCN: <250 mg/kg (<250) & H2S: <500 mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
0.192
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
Trichloroethylene
2,4,5-Trichlorophenol
0.5
0.5
400.0
ND
ND
ND
1,2-Dichloroethane
0.5
ND
1, 1 -Dichloroethylene
0.7
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105,
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: WaN 1�oint Analytical Virginia Inc. and Date of analysis: 11/25/2019
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average Result
Concentration Limits
(Class A Only)
(mg1kg) (mglkg)
41 <27.8
39 <5.56
Arsenic
75
Cadmium
85
Copper
4,300
1,500
70.6
Lead
840
300
25.4
Mercury
57
17
<0.811
Molybdenum
75
n/a
<13.9
Nickel
420
420
23.8
Selenium
100
100
<27.8
Zinc
7,500
2,800
503
b. For Surface Disposal Unit llandfllj: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Research & Analytical Laboratories Inc. and Date of analysis: 4/8/2016
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic Chromium
(mg/kg) (mg/kg)
Nickel
(mg/kg)
210
> 0 but < 25
❑ > 25 but < 50
30
200
34
220
240
::[![] > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)
<27.8
36.7
23.8
FORM: RSC 06-16 Page 3 of 5
5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 14.2 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical Vir .inia Inc. and Date of analysis: 11/25/2019
Parameter
Result
(mg/kg)
Aluminum
160,000
Ammonia -Nitrogen
11,400
Calcium
4,520
Magnesium
2,400
Nitrate -Nitrite Nitrogen
<262
pH (Standard Unit)
6.3
Phosphorus
4,920
Potassium
2,120
Sodium
<1,390
Total Kjeldahl Nitrogen
25,700
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.61
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0.4 or 40 %.
This rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: Accepted formula for water
plant residuals.
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
I Application Method
Surface
Injection/Incorporation
First (111) Year PAN
(mg/kg)
11,682
N/A
Five -Year
Maximum Adjusted PAN
(mg/kg)
15,187
N/A
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A -water plant residuals
FORM: RSC 06-16 Page 4 of 5
7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land A lication o -Class A or Er uivalent:
10 A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance.
B
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)( )] -
Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, [] heat drying, ❑heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land A lication o Class B:
❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [15A NCAC 02T.1106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction WAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)1 - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
Page 5 of 5
FORM: RSC 06-16
ce
04-
i� r
A A ;
I
P.W. Swann Water Treatment Plant
Water System Facility ID = TP3
Production Capacity = 25.0 MGD
City of Winston-Salem Yadkin River
NPDES# = NCG590003 - -
50 MG
Raw Water Off Stream
Storage Basin #1
100 MG
Raw Water Off Stream
Storage Basin #2
The Northwest WTP has two
treatment trains that are
Mix
12.5 MGD each for a total
Flash
plant capacity of 25.0 MGD.
Flocculation
Sedimentation
Basins
25 MGD
Chlorine
Alum
10
Filters 1-6
Caustic So(
Chlorine
Fluoride
Ortho-Phc
Alum
25 MGD
T
Chlorine
KMn04
Caustic Soda
Alum
Residual Lagoon Residual Lagoon
(4.3 MG)� (4.3 MG)
A
—0.5 MGD
25 MGD
30 MGD
Entry Point-EP3
Chlorine
5.0 MG
Clearwell
�I
0.489 MG
Equalization Basin
Distribution
System
BLACK & VEATCH LLP
CIVIL DESIGN MEMORANDUM
1lP
S«� ?Alt-
Winston-Salem/Forsyth County Utility Commission B&V Project 37604
Winston-Salem, North Carolina First Issue: July 31, 1998
Northwest Water Treatment Plant Latest Revision: October 30, 1998
3. Flow Measurement.
Initial Ultimate
Type Magnetic Magnetic
Number of meters 1 2
Size, each, inches 30 30
Flow measurement range, mgd 10-37.5 10-37.5
Control: Flow signal will be transmitted to the plant control room and
local indication will be provided in the pumping station.
F. WASH WATER AND RESIDUALS HANDLING
1. General.
a. Initial Wash Water and Residuals Handlin 7 . Spent wash water and
filter -to -waste will discharge by gravity to a wash water
equalization basin. The collected water will gravity discharge from
the equalization basin to the residuals storage lagoons. Gravity
flow rates from the equalization basin will be controlled by a rate
control valve.
The wash water drainage system upstream of the equalization basin
will be designed to allow six filters (two treatment trains) to be
simultaneously wasted at the design filtration rate. This drainage
capacity is provided for an emergency condition when water quality
dictates the basins be wasted until necessary treatment adjustments
are made. Because this is an emergency condition and not part of
the normal plant operation, the facilities downstream of the
equalization basin will not be designed to accommodate this
increased emergency flow. Flows in excess of the equalization
basin drainage capacity will overflow to the plant overflow drain.
Unthickened residuals from the sedimentation basins will discharge
by gravity through the viewing pit to the residuals storage lagoons.
I-19
BLACK & VEATCH LLP
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 37604
Winston-Salem, North Carolina First Issue: July 31, 1998
Northwest Water Treatment Plant Latest Revision: October 30, 1998
Decant/overflow from the residuals lagoons will discharge to the
creek in accordance with the NPDES permit.
The initial wash water equalization basin will be designed to be
readily converted to a future clarifier by installation of circular
clarifier equipment. Piping provisions will be made to allow the
residuals to drain to future residuals thickeners when the basin is
converted to a clarifier.
b. Future Wash Water and Residuals Handlin•,. Provisions will be
made to allow the future addition of a dedicated filter -to -waste drain
to a future equalization basin for filter -to -waste recycle. The future
filter -to -waste equalization basin will be equipped with pumps for
recycling to the plant raw water influent piping. The existing
equalization basin will be dedicated to handling filter backwash
water.
Provisions will be made to allow the addition of a second
equalization basin dedicated to filter backwash water handling. The
future wash water equalization basin will be equipped with pumps
to pump wash water to the existing equalization basin which will be
converted to a clarifier for wash water treatment.
Wash water and residuals handling and treatment facilities will be
designed to allow a possible future addition of the following.
• Equalization basins.
• Wash water clarifiers.
• Residuals thickeners.
• Residuals dewatering facilities.
I-20
BLACK & VEATCH LLP
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 37604
Winston-Salem, North Carolina First Issue: July 31, 1998
Northwest Water Treatment Plant Latest Revision: October 30, 1998
2. Wash Water and Residuals Flows and Solids Production.
Initial
Ultimate
Filter Backwash Water
Per filter(l), gal
164,000
164,000
Avg�Z�, gpd
492,000
984,000
Max(3), gpd
984,000
1,968,000
Filter -to -Waste
Per filter(4), gal
58,300
58,300
Avg�2��4�, gpd
174,900
349,800
Max�3��4�, gpd
349,800
699,600
Total Residuals Production
Avg�6�, lb/day
3,600
7,200
Max('), lb/day
7,500
15,000
Unthickened Residuals Flow to LaL oons
Avg�6��8�, gpd
216,000
432,000
Max�'��8�, gpd
450,000
900,000
Thickened Residuals Production
Avg�6��9�, gpd
21,600
43,200
Max�'��9�, gpd
45,000
90,000
Free Liquid from Residuals(io)
Avg, gpd
194,400
388,800
Max, gpd
405,000
810,000
Overflow from LaL,00ns�5�
Avg, mgd
0.95
1.89
Max, mgd
1.91
3.83
(1) Flow rate of 22.5 gpm/sf for 10 minutes.
(2) Half of the filters backwashed in one day.
I-21
BLACK & VEATCH LLP
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 37604
Winston-Salem, North Carolina First Issue: July 31, 1998
Northwest Water Treatment Plant Latest Revision: October 30, 1998
(3) All filters backwashed in one day.
(4) Flow rate of 4 gpm/sf for 20 minutes.
(5) Backwash water, plus filter -to -waste, plus free liquid from residuals, plus
10 percent (miscellaneous plant flows).
(6) Two hundred forty pounds per million gallons, using average flow rate
(Initial flow 15 mgd, ultimate flow 30 mgd).
(7) Three hundred pounds per million gallons, using maximum flow rate
(Initial flow 25 mgd, ultimate flow 50 mgd).
(8) 0.2 percent solids.
(9) 2.0 percent solids.
(10) Unthickened residuals flow minus thickened residuals flow.
3. Wash Water EQualization Basin.
Number of basins
Design criteria, each
Volume, each, gal
Basin type
B asin shape
Dimensions, ft
Inside diameter
Sidewall water depth
Bottom slope to center hopper
Water depth at top of hopper
Initial Ultimate
1 2
Storage volume of two
filter wash cycles plus
10 percent
489,000
Reinforced concrete
Circular
85
12
12:1
15.25
Controls: A ball valve will be provided on the -equalization basin drain
line in a vault to control flow rates from the equalization
basin to the residuals storage lagoons. The valve will be
controlled manually from the control room or locally from the
valve vault.
A level sensor will be provided in the equalization basin.
Basin level will be transmitted to each filter console and to
the plant control room. At basin overflow level, an overflow
alarm will be transmitted to the control room.
I-22
BLACK & VEATCH LLP
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 37604
Winston-Salem, North Carolina First Issue: July 31, 1998
Northwest Water Treatment Plant Latest Revision: October 30, 1998
4. Residuals Storage LaLoons.
The residuals storage lagoons will receive all
plant residuals and wash water
for treatment and storage.
Initial Ultimate
Number of lagoons
2 3
Lagoon type
Earthen lagoon with concrete
slope protection and underdrain
Dimensions, each, ft
Length
350 350
Width
235 235
Max residuals depth
8 8
Max water depth
10 10
Freeboard
2 2
Perimeter slope
3:1 3:1
Liquid volume, each, mg
4.3 4.3
Storage volume, each, mg
3.2 3.2
Effective storage, each lagoon,
days
365 183
Access Ramp
Width, ft
12 12
Slope, percent
12 12
Decant
Discharge to creek
Sludge removal method
Air drying, excavate with front-end
loader or clam bucket
Cleaning duration, years
1 1
G. OPERATIONS BUILDING
An operations building will be provided for administrative facilities, chemical feed and
storage, and maintenance and control facilities. Figures I-13 and I-14 showing the floor
plans for the basement and operating floor and Figure I-15 showing the building
elevations are attached.
I-23
P.W. Swann Water Treatment Plant
Solids Handling Plan
The Swann Water Treatment Plant is a 25.0 MGD water treatment facility. Solids are
generated by sludge removal from two sedimentation basins, backwashing six filters, and
filter -to -waste after filter backwashes are completed. Solids produced from filter backwashes
and filter -to -waste are routed to a flow equalization basin before entering one of two residual
lagoons. Solids removed from the sedimentation basins are routed directly to one of two
residual lagoons. The equalization basin volume is 0.489 MG, and each of the two residual
lagoons has a volume of 3.2 MG.
Permits and Classifications:
1. The discharge from the residuals lagoons is authorized by NPDES Permit NCG590003.
The classification for the discharge is Grade 1 Physical/Chemical.
2. The distribution of the residuals removed from the lagoons is authorized by permit
WQ0031314. The residuals are classified as Class A.
Operation:
1. The system consists of a 0.489 MG equalization basin (EQ basin) and two (2) residuals
lagoons with a capacity of 4.3 MG's each.
2. Routine inspections of equipment will be conducted Senior Utility Plant Supervisor to
ensure proper operation of equipment. Any equipment not functioning properly are
reported through the water division's asset management program, MAXIMO, to the
appropriate support group for repair/replacement.
3. Each lagoon consists of an oval concrete apron, a clay bottom, and an access ramp used
for residuals removal. The solids stream enters on one end of the lagoon and there is an
adjustable weir on the opposing end allowing decant to flow to the discharge.
4. Backwash and filter -to -waste water from the plant process flow by gravity to the EQ
basin. The backwash and filter -to -waste water then flows by gravity into the lagoon in
service. A regulating valve prevents flow spike from entering the residuals lagoons.
5. A flow meter measures flow leaving the EQ basin and 38% Sodium bisulfite is applied to
the EQ basin discharge for dechlorination of effluent being sent out discharge
NCG590003.
6. All sedimentation basin residuals flow by gravity directly to the residuals lagoon in
service.
P.W. Swann Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
7. Each lagoon has the capacity to accept and store the solids produced by the plant for
approximately 18 months. This allows one lagoon to accept the daily waste stream of
solids while the other is out of service.
8. Residuals are removed from the lagoons in liquid form and hauled to land application sites
by a private contractor.
Monitoring and Reporting Requirements:
1. Residuals generated by each source -generating facility must be analyzed to demonstrate
that they are non -hazardous based on the most current permit requirements (Attachment
A). Sampling will be conducted under supervision of the Senior Water Treatment Plant
Supervisor by WSFC Utilities current contractor as described below in compliance with
permit requirements.
2. Analysis will be performed by a NC Certified Laboratory.
3. Analyses made according to monitoring and reporting requirements must be certified for
the required parameter(s).
4. Corrosivity, ignitability, reactivity, and a Toxicity Characteristics Procedure analysis are
required once each permit cycle. The TCLP analysis includes the following parameters
(i.e., note the regulatory level in milligrams per liter in parentheses):
Arsenic (5.0)
Barium (100.0)
Benzene (0.5)
Cadmium (1.0)
Carbon tetrachloride (0.5)
Chlordane (0.03)
Chlorobenzene (100.0)
Chloroform (6.0)
Chromium (5.0)
m-Cresol (200.0)
o-Cresol (200.0)
p-Cresol (200.0)
Cresol (200.0)
2,4-D (10.0)
1,4-Dichlorobenzene(7.5)
1,2-Dichloroethane (0.5)
1, 1 -Dichloroethylene (0.7)
2,4-Dinintrotolulene (0.13)
Endrin (0.02)
Hexachlorobenzene (0. 13)
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Hexachloroethane (3.0)
Lead (5.0)
Lindane (0.4)
Mercury (0.2)
Methoxychlor(10.0)
Methyl ethyl ketone (200.0)
Nitrobenzene (2.0)
Pentachlorophenol (100.0)
Pyridine (5.0)
Selenium (1.0)
Silver (5.0)
Tetrachloroethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,6-Trichlorophenol (2.0)
2,4,5-TP (Silvex) (1.0)
Vinyl chloride (0.2)
5. Analyses of the following parameters are also required with each application event:
Aluminum
Ammonia -Nitrogen
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Nitrate -Nitrite Nitrogen
Phosphorous
Potassium
P.W. Swann Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
pH
Plant Available Nitrogen
(by calculation)
Selenium
Sodium
% Total Solids
TKN
Zinc
2
6. Data to verify pathogen reduction and vector attraction reduction of the residuals is
maintained on file for five years. The required data is specific to the stabilization process
utilized, and is also sufficient to demonstrate clear compliance with the Class A pathogen
requirements and restrictions noted in 15A NCAC 02T .1106 (a) and (b) and vector
attraction reduction requirements in 15A NCAC 02T .1107 (a).
7. Proper records are maintained tracking all residuals activities. These records include the
source, volume, analysis, and recipient of the residuals.
8. Three copies, per application event, of all required monitoring and reporting requirements
are submitted annually before March 1, to NC DEQ-DWQ.
Performance Standards:
1. The pollutant concentrations in any residuals that are land applied to any land application
site shall not exceed the following Ceiling and Monthly Average Concentrations (i.e.
dry weight basis):
Parameter
Monthly Average
Concentration
(milligrams per kilogram)
Ceiling Concentration
(milligrams per kilogram)
Arsenic
41
75
Cadmium
39
85
Copper
1,500
4,300
Lead
300
840
Mercury
17
57
Molybdenum
n/a
75
Nickel
420
420
Selenium
100
100
Zinc
2,800
7,500
2. If residuals are sold or given away, one of the Class A pathogen requirements in 15A
NCAC 02T .I 106(b) must be met.
Application Requirements:
1. Bulk residuals are not applied under the following conditions:
i. If the residuals are likely to adversely affect a threatened or endangered species.
ii. If the application causes prolonged nuisance conditions.
iii. If the land fails to assimilate the bulk residuals or the application causes the
contravention of surface water or groundwater standards.
P.W. Swann Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
3
iv. If the land is flooded, frozen, or snow-covered or is otherwise in a condition such that
runoff of the residuals would occur.
v. Within the 100-year flood elevation, unless the bulk residuals are injected or
incorporated within a 24-hour period following the residuals application event.
vi. During a precipitation event or within 24 hours following a rainfall event of 0.5
inches or greater in a 24-hour period.
vii. If the slope of the land is greater than 10 percent when the bulk residuals are surface
applied, and if the slope of the land is greater than 18 percent when bulk residuals are
injected or incorporated.
viii. If pH maintained in the soil and residuals mixture is greater than 6.0.
ix. If the land does not have an established vegetative cover.
x. If the vertical separation of the seasonal high water table and the depth of the
residuals application is less than one foot.
xi. If the vertical separation of the depth to bedrock and the depth of residuals application
is less than one foot.
xii. Application exceeds agronomic rates.
xiii. For residuals treatment and storage facilities, the following minimum setbacks shall
be adhered to:
Minimum Setback
Description of Setback
(feet)
Habitable residence or place of public assembly under separate ownership or
not to be maintained as part of the project site
100
Property lines
50
Private or public water supply
100
Surface waters (streams, -intermittent and perennial, perennial waterbodies,
and wetlands)
50
Wells with exception to monitoring wells
100
2. When land applying bulk residuals to any land application site, the following minimum
setbacks are maintained at all times:
Setback By TY a of
Residual feet
Description of Setback
Liquid
Cake
Private or public water supply
100
100
Surface waters (streams -intermittent and perennial,
perennial waterbodies, and wetlands)
100
25
Surface water diversions (ephemeral streams,
waterways, ditches)
25
0
Groundwater lowering ditches (where bottom of
The ditch intersects SHWT)
25
0
Subsurface groundwater lowering system
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
3. Specific bulk residuals land application area boundaries are clearly marked on each land
application site prior to and during a residuals land application event.
P.W. Swann Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
4
4. Bulk residuals and other sources of PAN (Plant Available Nitrogen) are applied to all land
application sites at or below agronomic rates. Appropriate agronomic rates are calculated
using expected nitrogen requirements based on the Realistic Yield Expectations (RYE)
field cover for each approved land application site.
Spills and Noncompliance Notification:
1. The Winston-Salem Regional Office, telephone number (336) 771-5000, will be notified
within 24 hours or the next working day following the occurrence or first knowledge of
the occurrence of any of the following:
i. Any occurrence with the distribution program, which results in the land application of
significant amounts of wastes, which are abnormal in quantity or characteristic.
ii. Any failure of the distribution program resulting in a release of materials to receiving
waters.
iii. Any time that self -monitoring information indicates that, the facility has gone out of
compliance with the conditions and limitations of the permit or the parameters on
which the system was designed.
iv. Any process unit failure, due to known or unknown reasons, that renders the facility
incapable of adequate residual treatment.
v. Any spillage or discharge from a vehicle or piping system during transportation of
residuals.
2. Persons reporting such occurrences by telephone shall also file a written report in letter
form within (5) days following first knowledge of the occurrence. This report must outline
the actions taken or proposed to be taken to ensure that the problem does not recur.
3. Emergency Contacts: Swann Water Treatment Plant (336) 945-1179 (Main)
Billy Goss, Plant Supervisor (336) 397-7728 (0)
(336) 399-3264 (M)
Bill Brewer (336) 397-7727 (0)
Water Plants Superintendent (336) 745-5277 (M)
Winston-Salem/Forsyth County (336) 727-8418
Utility Administration
DEHNR Regional Office (336) 771-5000
General Emergency 911
HazMat
P.W. Swann Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
Ifs 1EsEARCh ANA1yTiCAi
LAboRAT®R1F-5r INC. . :
z.
Analytical/Process Consultations �.% Q.r
Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Lagoon 1
(A City of Winston-Salem Swann WTP Prai ect, collected 08 April 2016)
Lagoon I
EPA HW
Quantitation
Results
Characteristic
Number Contaminant
Limit(me1L)
(melt)
Level(me/L)
EPA Method
1
TCLP METALS
D-004 Arsenic
0.010
BQL
5.00
6010C
D-005 Barium
0.040
0.192
100
6010C
D-006 Cadmium
0.005
BQL
1.00
6010C
D-077 Chromium
0,010
BQL
5.00
6010C
D-008 Lead
0-005
BQL
5.00
6010C
D-009 Mercury
0.0020
BQL
0.200
7470A
D-010 Selenium
0.100
BQL
1.00
6010C
D-011 Silver
0.010
BQL
5.00
6010C
II .
TCLP VOLATILES
0,050
BQL
0.500
8260B
D-018 Benzene
D-019 Carbon Tetrachloride
0.050
BQL
0.500
8260E
D-021 Chlorobenzene
0.050
BQL
100
8260B
D-QT? Chloroform
0.500
BQL
6.00
8260E
D-028 12-D-rchlorocthane
0-050
BQL
0.500
8260B
D-D29 1.1-Dichloroethylene
0-050
BQL
0.700
8260E
0-035 Methyl Ethyl Ketone
0.500
BQL
200
8260E
D-039 Tetrachloroe1hylene
0.050
BQL
0.700
8260B
D-040 Trichloroethylcne
0.050
SQL
0.500
8360E
D-043 Vinyl Chloride
0.050
BQL
0.200
8260E
III.
TCLP SEMI-VOLATILES
20.0
BQL
200
8270D
D-023 O-Creosol
D-024 M-Creosol
20-0
BQL
200
8270D
D-025 p-Creosol
2010
BQL
200
8270D
D-026 Creosol
20.0
BQL
200
8270D
D-027 1,4-Dichlorobenzene
0.750
BQL
730
8270D
D-030 2,4-Dinitrotolucne
0.050
BQL
0.130
8270D
D-032 Hexachlorobenzene
0.050
BQL
0.130
8270D
D-033 Hexachlorobutadiene
0.050
BQL
0.500
8270D
D-034 Hexachloroethane
0.300
BQL
3.00
8270D
D-036 Nitrobenzene
0.200
BQL
2.00
8270D
D-037 Pentachlorophenol
10.0
BQL
100
9270D
D-038 Pyridine
0,500
BQL
5.00
82700
D-041 2,4,5-Trichlorophenol
40.0
BQL
400
8270D
D-042 2,4,6-Trichlorophenol
0.200
SQL
2.00
8270D
IV,
TCLP PESTICIDESlHERBICIDES
0.003
BQL
0.030
8081 B
D-020 Chlordane
D-016 2,4-D
1.000
BQL
10.0
8151 A
D-012 Endrin
0.002
BQL
0.020
8081 B
D-031 Heptachlor
0.0008
BQL
0.008
8081 B
D-013 Lindane
0.040
BQL
0.400
8081 B
D-014 Methoxychlor
I.ODO
BQL
BQL
10.0
0.500
8081 B
8081 B
D-015 Toxaphene
D-017 2.4.5-TP(Silvex)
01050
0.100
BQL
1.00
8151 A
V.
REACTIVITY
2.0
BQL
9010
D-003 Cyanide
D-003 Sulfide
10.0
BQL
9030
VI.
CORROSIVITY
Std. Units
5.40
9045
D 00R pH
Vli.
TCLP,VIISCELLANEOUS
Paint Filter rest
NFL
VIII, IGNITABILITY
NVNI
1010
D-001 Ittnitability
Sample Number
17319-01
Sample Date
04/08/16
Sample Time (hrs)
0745
Sample Matrix
Solid
BOL = Below Ouantitation Limits
mgfL -milligrams per Liter = pamper million (ppm)
NFL = No Free Liquids
a
,¢ r
t
ICAL
Y X
z ✓r
Way nt
PA .
9/2712019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-262-0017
Project Description: Winston WTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalydcaf.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) an 9/19/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 16 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated_ This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 6
(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint,
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number:
19-262-0017
Client Project Description:
Winston WTP
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SM-4500-NH3C
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
9045D
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
4500NO3F-2011
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
6010D
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SW-7471B
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SM-4500-NH3C-TKN
WTN
68269
Winston WTP
Solids
09/17/2019 14:00
09/19/2019
SM-254OG
WIN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #460181 - Virginia
Page 2 of 6
Report Number: 19-262-0017
.rs�rr
C i 4ny gip',
fir`: �- po
Account Number: 46622
7621 Whitepine Road, Richmond, VA 23237
)int..Main
$04-743-9401 ° fax BD4-271-6446
ANALY
www.waypo inta nalydca I -corn
Send To: Synagro Central LLC/ Technical
Project, Winston
WTP
Mary Brewer
284 Boger Road
Mocksville , NC 27028
REPORT OF ANALYSIS
Date Sampled: 9/17/2019 14:00:00
Lab Number. 68259
Date Received: 09/19/2019 00:00
Sample Id : Winston WTP
Date Reported: 09/27/2019
•
METHOD
.
D
Total Solids "
3.42
ADM
09/20/2019 16:38 SM-254OG
Moisture *
96.60
ADM
09120/2019 16:38 SM-2540G
Total ICeldahl Nitrogen
2.09
20900
250
JPJ
09/26/2019 13:00 SM-4500-NH3C-TKN
Phosphorus
0.29
2870
50.0
BKN
09/24/2019 21:47 60100
Potassium
0.11
1120
50.0
BKN
09/24/2019 21:47 6010D
Sulfur
0.41
4110
50.0
BKN
09124/2019 21:47 6010D
Calcium
0.53
5290
250
BKN
09/24/2019 21:47 6010D
Magnesium
0.17
1670
50.0
BKN
09/24/2019 21:47 6010D
Sodium
0.03
302
250
BKN
09/24/2019 21:47 6010D
Iron
24200
50.0
BKN
09/24/2019 21:47 6010D
Aluminum
120000
500
BKN
09125/201913.37 6010D
Manganese
1120
5.00
BKN
09/24/2019 21:47 6010D
Copper
49.3
2.50
BKN
09/24/2019 21:47 6010D
Zinc
442
12.5
BKN
09/24/2019 21:47 6010❑
Ammonia Nitrogen
0.62
6180
100
JPJ
09/26/2019 13:00 SM-4500-NH3C
Organic N
1.47
14720
250
09/2612019 13:00 CALCULATION
Nitrate+Nitrite-N
<4.90
4.90
ZBD
09/241201915:33 4500NO3F-2011
All values are on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet
basis.
B-Analyte detected in blank H - Beyond holding time
t it: #1C 101' Y
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made Pauric McGroary
to the work, the results, or the company in any advertising, news release, or other, public announcements without obtaining our prior written authorization. Agronomist
Page 3 of 6
Report Number. 19-262-0017
Account Number: 46622
Send To: Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksviile , NC 27028
Lab Number: 66269
Sample Id : Winston WTP
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
pH *
Molybdenum
Comments:
Waypoint.(D
ANALYTICAL
Project: Winston WTP
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 'Fox 804-271-6446
www.waypointanalytical.com
Date Sampled: 9/17/2019 14:00:00
Date Received: 09/19/2019 00:00
Date Reported: 09/27/2019
<1.00
1.00
BKN
09/24/2019 21:47
601 OD
48.9
2.50
BKN
09/24/2019 21:47
6010D
22.9
2.50
BKN
09/24/2019 21:47
601 OD
12.6
3.00
BKN
09/24/2019 21:47
6010D
8.73
5.00
BKN
09/24/2019 21:47
601 OD
0,0332
0.0155
TJS
09/24/2019 13:43
SW-7471 B
<5.00
5.00
BKN
09/24/2019 21:47
6010D
6.7
JSL
09/24/2019 06:50
9045D
<2.50
2.50
BKN
09/24/2019 21:47
6010D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
B-Analyte detected in blank H - Beyond holding time
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced In whole or part, nor may any reference be made
to the worn, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pauric McGroary
Agronomist
Page 4 of 6
s:
aN FAIr
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax 804-271-6446
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLCI Technical
Report Number: 19-262-0017
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 Other, `
is UPS 0 Client 0 Courier
Thermometer ID:
Shipping container/cooler uncompromised?
ISYes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No Not Required
Custody seals intact on sample bottles?
0 Yes
0 No ® Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
® Yes
0 No
All samples received within holding time?
® Yes
0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. 0 Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No
NIA
Water - VOA vials free of headspace
0 Yes
0 No
* NIA
Trip Blanks received with VOAs
0 Yes
0 No
0 NIA
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
49 N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
F- High concentration pre -weighed (methanol -14 d) F- Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments
Signature: Brandi Watson Date & Time: 09119/2019 13:42.28
Page 5 of 6
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WiP 9/17/2019 91112019-1213112019 0.1709
LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (302 x 3.4200) + 100 = 10.3294
Ca mgll = (Ca mg/kg x °/a Solids) + 100 = (5290 x 3,4200) 100=180.918
Mg mg1I = (mg mg/kg x % Solids) + 100 = (1670 x 3.4200) + 100 = 57.114
Na meq = Na mg/I + Molec.Wgt.Na = 10.3284 + 23 = 0.449061
Ca meq = Ca mg/I + Molec.Wgt.Ca = 180.918 + 20 = 9.0459
Mg meq = Mg mgll+Molec.Wgt.Mg = 57.114 + 12 = 4.7595
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0,449061 + SgrRool[0.5(9.0459+4.7595)] = 0.170921
Printed: 1/22/2020
17:02
Page 1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointa nalytica Isom
12/5/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref; Analytical Testing
Report Number: 19-330-0005
Project Description: Winston 2nd
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/2612019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P&A iff �r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
6
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL
www.waypointanalytical.com
Sample Summary Table
Report Number: 19-330-0005
Client Project Description: Winston 2nd
Lab No
Client Sample ID
Matrix
Date Collected
Date Received Method
Lab ID
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019 SM-4500-NH3C
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019 9045D
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019 4500NO3F-2011
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019 6010D
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019 SW-74718
WTN
69698
Winston 2nd
Solids
11/25/2019 13AS
11/2612019 SM-4500-NH3C-TKN
WTN
69698
Winston 2nd
Solids
11/25/2019 13:45
11/26/2019 SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
PaaP 2 of 6
Waypointo
ANALYTICAL
46622
Synagro Central LLC/ Technical
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointa nalytical.com
Mary Brewer Project Winston 2nd
284 Boger Road Information
Mocksville , NC 27028
Report Number:19-330-0005
Lab No: 69698
Sample ID: Winston 2nd
Test
Moisture
Test
Ammonia Nitrogen
Nitrate+Nitrite-N
Organic N
PH
Total Solids
Total Kjeldahl Nitrogen
Phosphorus
Aluminum
Arsenic
Calcium
Cadmium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
REPORT OFANAL YSIS
Results Units MQL
98.2 % 0.010
Results Units MQL
10800
mg/Kg - dry
5560
<273
mg/Kg - dry
273
23600
mg/Kg - dry
13900
6.3
S.U.
1.84
%
0.010
34400
mg/Kg dry
13900
4440
mg/Kg - dry
278
160000
mg/Kg - dry
278
<27.8
mg/Kg - dry
27.8
3670
mg/Kg - dry
1390
<5.56
mg/Kg - dry
5.56
34.2
mg/Kg - dry
13.9
65.6
mg/Kg - dry
13.9
35800
mg/Kg - dry
278
25.4
mg/Kg - dry
16.7
2110
mg/Kg - dry
278
1130
mg/Kg - dry
27.8
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quandtation Limit
Report Date : 12/05/2019
Received : 11/26/2019
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11/ 25/ 2019 13:45
DF Date / Time By Analytical
Analyzed Method
1 12/02/1918:43 ADM SM-2540G
DF
Date I Time
By
Analytical
Analyzed
Method
1
12/05/19 08:30
JPJ
SM-4500-NH3C
1
12/05/19 12:05
ZBD
4500NO3F-2011
1
12/04/19 09:00
CALCULATION
1
12/03/19 07:06
JSL
9045D
1
12/02/1-918:43
ADM
SM-2540G
1
12/04/19 09:00
3PJ
iM-4500-NH3C-TKP
1
12/03/19 19:27
BKN
6010D
1
12103/1919:27
KKM
60100
1
12/03/19 19,27
BKN
6010D
1
12/03/19 19:27
KKM
6010D
1
12/03/19 19:27
BKN
6010D
1
12/0311919:27
BKN
6010D
1
12/03/19 19:27
BKN
6010D
1
12/03/19 19:27
KKM
6010D
1
12/03/19 19:27
BKN
6010D
1
12/03/19 19:27
KKM
6010D
1
12/03/19 19:27
BKN
6010D
L Limit Exceeded
---- , -4 C
h
7621 Whitepine Road, Richmond, VA 23237
Waypoit
Main 804-743-9401 ° Fax 804-271-6446
ANALYTICAL
www,waypolntanalytical.com
46622
Synagro Central LLC/ Technical
Report Date : 12/05/2019
Mary Brewer
Project
Winston 2nd
Received, 11/26/2019
284 Boger Road
Information
:
Mocksville , NC 27028
�Vw"' zG X 60wr
Pauric McGroary
Report Number :19-330-0005
REPORT OFANAL YSIS
Agronomist
Matrix: Solids
Lab No : 69698
Sampled: 11/25/2019 13:45
Sample ID : Winston 2nd
Test
Results
Units
MQL
DF Date I Time By Analytical
Analyzed Method
Mercury
<0.850
mg/Kg - dry
0.850
1 12/04/19 15:23 KKM SW-7471B
Molybdenum
<13.9
mg/Kg - dry
13.9
1 12/03/19 19:27 BKN 6010D
Nickel
22.3
mg/Kg - dry
13.9
1 12/03/19 19:27 BKN 6010D
Potassium
2110
mg/Kg - dry
278
1 12/03/19 19:27 KKM 6010D
Selenium
<27.8
mg/Kg - dry
27.8
1 12/03/19 19:27 BKN 6010D
Sodium
<1390
mg/Kg - dry
1390
1 12/03/19 19:27 BKN 6010D
Zinc
387
mg/Kg - dry
69.4
1 12/03/19 19:27 BKN 6010D
Sulfur
6110
mg/Kg - dry
278
1 12/03/19 19:27 BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quandtation Limit
L Limit Exceeded
Para 4 of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLCI Technical
Report Number: 19-330-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other -
UPS 0 Client 0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
n Yes
0 No
0 Not Present
Custody seals intact on sample Mottles?
0 Yes
0 No
19 Not Present
Chain of Custody (COC) present?
Yes
0 No
COG agrees with sample label(s)?
0 Yes
0 No
COG properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
0 Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No
0 NIA
Water - VOA vials free of headspace
0 Yes
0 No
0 NIA
Trip Blanks received with VOAs
0 Yes
0 No
• N/A
Soil VOA method 5035 -- compliance criteria met
0 Yes
0 No
ID NIA
F_ High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments:
Signature: Bran& Watson Date & Time: ,11126/2019 13:37:11
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Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 1112512019 ! ! - 1 1 0.6116
LIQUID
Na mg1I = (Na mg/kg x % Solids) � 100 = (1390 x 1.8400) 100 = 25.676
Ca mgll = (Ca mg/kg x % Solids) + 100 = (3670 x 1.8400) + 100 = 67.528
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2110 x 1.8400) + 100 = 38.824
Na meq = Na mgll + Molec.Wgt.Na = 25.576 = 23 = 1.112
Ca meq = Ca mgll + Molec.Wgt.Ca = 67.528 = 20 = 3.3764
Mg meq = Mg mgA + Molec.Wgt.Mg = 38.824 - 12 = 3,23533
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.112 + SgrRoot[0.5(3.3764+3.23533)] = 0.611592
Printed: 1/2812020
13:25
Page i
Waypointo
ANALYTICAL
12/5/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-330-0006
Project Description: Winston 3rd
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www,waypofntanalocal.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
?W,. W r77�
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Pars I of 9
0
7621 Whitepine Road, Richmond, UA 23237
Waypoint
Main 804-743-9401 ° Fox
804-271-6446
ANALYTICAL
www.waypointanalytical.corn
Sample
Summary Table
Report Number: 19-330-0006
Client Project
Description: Winston 3rd
Laic No
Client Sample ID
Matrix
Date Collected
Date Received
Method —
Lab ID
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C
WTN
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
9045D
WTN
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
4SOONO3F-2011
WTN
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
6010D
WTN
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SW-7471B
WTN
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SM-4500-NH3C-TKN
WTN
69699
Winston 3rd
Solids
11/25/2019 13:45
11/26/2019
SM-254OG
WTN
WTN: Waypoint Analytical - TN, Memphis, TN
Pane 2 of 6
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-271-6446
www.waypointa n alvbcal.corn
Mary Brewer Project Winston 3rd
284 Boger Road Information
Mocksvilie . NC 27028
Report Number :19-330-0006
Lab No : 69699
Sample ID : Winston 3rd
Test
Moisture
Test
Ammonia Nitrogen
Nitrate+ N itrite-N
Organic N
pH
Total Solids
Total Kjeldahl Nitrogen
Phosphorus
Aluminum
Arsenic
Calcium
Cadmium
Chromium
Copper
Iron
Lead
Magnesium
Manganese
REPORT OFANAL YSl'S
Results Units
Report Date ; 12/05/2019
Received : 11/26/2019
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11/ 25/ 2019 13:45
MQL DF Date I Time By Analytical
Analyzed Method
97.8
%
0.010
1
12/0211918:43
ADM
SM-254OG
Results
Units
MQL
DF
Date lTime
By
Analytical
Analyzed
Method
B270
mg/Kg - dry
4550
1
12/05/19 08:30
JPJ
SM-4500-NH3C
<225
mg/Kg - dry
225
1
12/05/19 12:06
ZBD
45DONO3F-2011
20500
mg/Kg - dry
11400
1
12/04/19 09:00
CALCULATION
6.3
S.U.
1
12/03/19 07:06
JSL
9045D
2.19
%
0.010
1
12/02/1918:43
ADM
SM-2540G
26700
mg/Kg - dry
11400
1
12/04/19 09:00
JPJ
;M-4500-NH3C-TKO
3610
mg/Kg - dry
227
1
12/03/19 19:43
BKN
60101)
127000
mg/Kg - dry
227
1
12/03/19 19:43
KKM
6010D
<22.7
mg/Kg - dry
22.7
1
12/03/19 19:43
BKN
6010D
2840
mg/Kg - dry
1140
1
12/03/19 19:43
KKM
6010D
<4.55
mg/Kg - dry
4.55
1
12/03/19 19:43
BKN
6010D
27.5
mg/Kg - dry
11A
1
12/03/19 19:43
BKN
601OD
54.5
mg/Kg - dry
11.4
1
12/03/19 19:43
BKN
6010D
29100
mg/Kg - dry
227
1
12/03/19 19:43
KKM
6010D
19.1
mg/Kg - dry
13.6
1
12/03/19 19:43
BKN
6010D
1800
mg/Kg - dry
227
1
12/03/19 19:43
KKM
6010D
836
mg/Kg - dry
22,7
1
12/03/19 19:43
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Pava 3 of 6
7621 Whitepine Road, Richmond, VA 23237
WaypoiMain
�t
804-743-9401 ° Fax 804-271-6446
ANALYTICAL
www.waypointanalyticai.eom
46622
Synagro Central LLC/ Technical
Mary Brewer
Project
Winston 3rd
Report Date : 12/05/2019
284 Boger Road
Information :
Received : 11/26/2019
Mocksville , NC 27028
10 �(JO7---
Pauric McGroary
Report Number :19-330-0006
R,6PORT OFANALYSls
Agronomist
Lab No : 69699
Matrix: Solids
Sample ID : Winston 3rd
Sampled: 11/255/2019 13:45
Test
Results
Units
MQt-
DF Date I Time By Analytical
Analyzed Method
Mercury
<0.686
mg/Kg - dry
0.686
1 12/04/19 15:24 KKM SW-74718
Molybdenum
<11.4
mg/Kg - dry
11.4
1 12/03/19 19:43 BKN 6010D
Nickel
18.0
mg/Kg - dry
11.4
1 12/03/19 19:43 BKN 6010D
Potassium
1730
mg/Kg - dry
227
1 12/03/19 19:43 KKM 6010D
Selenium
<22.7
mg/Kg - dry
22.7
1 12/03/19 19:43 BKN 6010D
Sodium
<1140
mg/Kg - dry
1140
1 12/03/19 19:43 BKN 6010D
Zinc
260
mg/Kg - dry
56.8
1 12/03119 19:43 BKN 6010D
Sulfur
5000
mg/Kg -dry
227
1 12/03/19 19:43 BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L. Limit Exceeded
to4
W-a 0 ypoin
i
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 *Fax 804-271-W6
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number 19-330-0006
0 Fed Ex 0 US Postal
® UPS 0 Client
Shipping Method
0 Lab 0 Other.
0 Courier Thermometer ID:
Shipping container/cooler uncompromised? Yes
Number of coolers/boxes received 1
Custody seals intact on shipping container/cooler? 0 Yes
Custody seals intact on sample bottles? 0 Yes
Chain of Custody (COC) present?
COC agrees with sample label(s)?
10 Yes
0 Yes
1�1M
0 No i Not Present
0 No 19 Not Present
0 No
0 No
COC properly completed 40 Yes 0 No
Samples in proper containers? 0 Yes n Na
Sample containers intact? • Yes 0 No
Sufficient sample volume for indicated test(s)? ti Yes 0 No
All samples received within holding time? • Yes 0 No
Cooler temperature in compliance? 0 Yes 0 No
Cooler/Samples arrived at the laboratory on ice. • Yes 0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved 0 Yes 0 No _
Water - VOA vials free of headspace 0 Yes 0 No
Trip Blanks received with VOAs 0 Yes 0 No
0 N/A
0 N/A
41 N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) [_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments: - �-
Signature: I.Brandi Watson Date & Time: ,11/26/2019 13:38:171
n 9 _4, r_
SAMPLING LOG # Z
A 8s L Er
'aRS. INC.
j,
7621 W'
(CHABN OF (CUSTODY
CUSTOMER: suer®
m
Ri°gym°
IlI�lllt111111111111�1r1llllllll�llllllll�
C ANALYsus
RECORD
1 r
�'
ao41���
earo �nlfal LLC/ Technical
l��ll>fi1!l111l1�
uv`nslan
�s.zsz.00v
4S62z
09
PROJECT MANAGER: I ;ILK k _ .�
wTp
Tg za,s
npling procedures
"7 at these Samples.
Phone: ( 33 W 7�3 �o`b �
-
—
J
-
SAMPLER
-- ----
A & L CUSTOMER SAMPLING SAMPLE
LAB # I.D. LOCATION TYPE
# OF SAMPLING
CONTAINERS DATE
METHOD METHOD
_SAMPLE
_
TIME
PRESERVED SHIPPED
nu,lnquisneo oy Sampler:
Relinquished by:
Relinquished by:
SPECIAL INSTRUCTIONS:
ba e Time �
j
Date Time
Date Time
11 I /1 -
d by: REMARKS:
Recleved by:
WWI For monitoring purposes. p0#:
�3TATE)
SAMPLE ANALYSIS REQUEST
I.D. Organic
SL8 SL2 NH4 N NO3-N N Cd Cr Ni Pb As Hg $e PH CaCO3 Volatile Mo CI NO -N
equiv. Solids z
SLI: Total Solids (Moisture), Total Kjeldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Page 6 of 6
SAIMP! NG LOG I;
_ �.�-S' INC.
_ ? CUSTOMER: SYNAG ;
Svnaaro Central LLCTechnical Q 5 RECORD
13:37:50
Winston 3rd
PROJECT MANAGER: _-.--_.— /L-?'� — i'as Thal the proper herd samplirrg;orocedures
a used d''__
urig� t j collection of these samples.
I ?1z �
I
:•. L L C.US' OMER SAMPLING SAMPLE OF SAMPLING MIETHOD MET110D
I B SAMPLE I.D. LOC TIOrd TYPE"
CONTAINERS DATE TIME PRESERVED SHIPPED
J .
Relinquished by Sampler r J — — J — -- Daie Time Recieved by:
_ REMARKS:
Rc?I6 �gLIlSiled by: - ---•-- -
uS� tllllr"? Recieved by:
Relinqui,";hed by:
Date Tinier Recieved by � --
i j a
SPECIAL INSTRUCTIONS: —
purposes.
S� MIPLE ANALYSIS REQUEST
I.0 SL9 S-L2 Organic
s N { Cd Cr } Ni I b i As lig Sc! PH i 'aCO3 VGtatile Me Cl I NO N
r I equiv. Solids ,
I
xocv �l✓ � �` �I� 77�� 7/r p I ' f
a
i
r ✓4
i
i SLI: Total Solids (Moisture), Total l<jr-idafil'N4rogen, Phlosphorus, and Potassiulll
SL2: Basic irst SI_ i plus Sulfur, Calcium, MagneSlUrn, Sodium, Iron, Alurninurn. Ma"ganese, Copper and Zir-Ic
Page 6 cf 6
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
Sam pie Date Report Range Ratio
2055-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 11/25/2019 ! 1 - ! 1
0.6070
LIQUID
Na mg/I = (Na mglkg x % Solids) + 100 = (1140 x 2.1900) + 100 = 24.966
Ca mgll = (Ca mglkg x % Solids) + 100 = (2840 x 2.1900) + 100 = 62.196
Mg mgli = (mg mglkg x % Solids) + 100 = (1800 x 2.1900) + 100 = 39.42
Na meq = Na mg/I + Mofec.Wgt, Na = 24.966 + 23 = 1.08548
Ca meq = Ca mgll + Molec.Wgt.Ca = 62.196 20 = 3.1098
Mg meq = Mg mgll + Molec.Wgt.Mg = 39.42 4 12 = 3.285
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.08648 SgrRoo1[0.5(3.1098+3.285)] = 0,607047
Printed: 1/28/2020
13:32
Page 1
Waypointo
ANALYTICAL
12/5/2019
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 19-330-0007
Project Description: Winston 4th
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 904-271-6446
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 11/26/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 138 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certaln parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 16 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
P'_« P'a-/-
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Pace 1 of 6
0
7fi21 Whitepine Road, Richmond, VA 23237
Waypoint,Main
804-743-9401 ° Fax 8o4-271-6446
ANALYTICAL
www.waypointanalytical.coni
Sample
Summary Table
Report Number: 19-330-0007
Client Project Description: Winston 4th
Lab No
Client Sample ID
Matrix
Date Collected
Date Received Method —
Lab ID
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019 SM-4500-NH3C
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019 9045D
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019 450oNO3F-2011
WTN
69700
Winston 4th
Solids
11/25/2019 13AS
11/26/2019 6010D
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019 SW-7471B
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019 SM-4500-NH3C-TKN
WTN
69700
Winston 4th
Solids
11/25/2019 13:45
11/26/2019 SM-2540G
WTN
WrN: Waypoint Analytical - TN, Memphis, TN
Dana i of 9
7621 Whitep€ne Road, Richmond, VA 23237
Main 804-743-9401 o Fax 804-271-6446
www.waypoi n tanalyti ca I.com
Mary Brewer Project Winston 4th
284 Boger Road Information
Moci<svllle , NC 27028
Report Number:19-330-0007 REPORT OFANALYSIS
Lab No : 69700
Sample ID: Winston 4th
Test
Results Units
Report Date : 12/05/2019
Received
/: 11/26/2019
pwyj
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 11 / 25 / 2019 13:45
MQL DF Date ITime By Analytical
Analyzed Method
Moisture
98.2
%
0.010
1
12/02/1918:43
ADM
SM-254OG
Test
Results
Units
MQL
DF
Date ITime
By
Analytical
Analyzed
Method
Ammonia Nitrogen
11.400
mg/Kg - dry
5560
1
12/05/19 08:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<262
mg/Kg - dry
262
1
12/05/19 12:06
ZBD
4500NO3F-2011
Organic N
14300
mg/Kg - dry
13900
1
12/04/19 09:00
CALCULATION
pH
6.3
S.U.
1
12/03/19 07:06
JSL
9045D
Total Solids
1.78
%
0.010
1
12/02/19 18:43
ADM
SM-254OG
Total Kjeldahi Nitrogen
25700
mg/Kg - dry
13900
1
12/04/19 09:00
JPJ ;M-4500-NH3C-TKP
Phosphorus
4920
mg/Kg - dry
278
1
12/03/19 19:48
BKN
6010D
Aluminum
160000
mg/Kg - dry
278
1
12/03/19 19:48
KKM
6010D
Arsenic
<27.8
mg/Kg - dry
27.8
1
12/03/19 19:48
BKN
6010D
Calcium
4520
mg/Kg - dry
1390
1
12/03/19 19:48
KKM
6010D
Cadmium
<5.56
mg/Kg - dry
5.56
1
12/03/19 19:48
BKN
6010D
Chromium
36.7
mg/Kg - dry
13.9
1
12/03/19 19:48
BKN
6010D
Copper
70.6
mg/Kg - dry
13.9
1
12/03/19 19:48
BKN
6010D
Iron
36i00
mg/Kg - dry
278
1
12/03/19 19:48
KKM
6010D
Lead
25.4
mg/Kg - dry
16.7
1
12/03/19 19:48
BKN
6010D
Magnesium
2400
mg/Kg - dry
278
1
12/03/19 19:48
KKM
6010D
Manganese
1360
mg/K9 - dry
27.8
1
12/03/19 19:48
BKN
6010D
Qualifiers/ DF
Dilution Factor
L
Limit Exceeded
Definitions MQL
Method Quandtation Limit
Paqe 3 of 6
m
7621 Whitepine
Road, Richmond, VA 23237
Waypoint,
Main 804-743-94010 Fax 804-271-6446
ANALYTICAL
www.waypointanalytical.corn
46622
Synagro Central LLC/ Technical
Report Date : 12/05/2019
Mary Brewer
Project
Winston
4th
Received : 11/26/2019
284 Boger Road
Information
:
Mocksville , NC 27028
��lcc IV 6gorr�
Pauric McGroary
Report Number .19-330-0007
REPORT OFAIVALYSIS
Agronomist
Matrix: Solids
Lab No: 69700
Sampled: 11/25/2019 13:45
Sample ID : Winston 4th
Test
Results
Units
MQL.
DF Date/Time By Analytical
Analyzed Method
Mercury
<0.811
mg/Kg - dry
0.811
1 12/04/19 15:25 KKM SW-7471B
Molybdenum
<13.9
mg/Kg - dry
13.9
1 12/03/19 19:48 BKN 6010D
Nickel
23.8
mg/Kg - dry
13.9
1 12/03/19 19:48 BKN 6010D
Potassium
2120
mg/Kg - dry
278
1 12/03/19 19:48 KKM 6010D
Selenium
<27.8
mglKg - dry
27.8
1 12/03/19 19:48 BKN 6010D
Sodium
<1390
mg/Kg - dry
1390
1 12/03/19 19:48 BKN 6010D
Zinc
503
n)g/Kg - dry
69.4
1 12/03/19 19:48 BKN 6010D
Sulfur
5720
mg/Kg - dry
278
1 12/03/19 19:48 BKN 6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
L Limit Exceeded
Para 4 of 6
Waypointe
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax 804-Z71-6446
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 19-330-0007
Shipping
Method
0 Fed Ex 0 US Postal 0 Lab
0 Other .
1
41 UPS 0 Client 0 Courier
Thermometer ID:
�.vA
Shipping container/cooler uncompromised?
rp Yes
0 No
Number of coolers/boxes receivedL�
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not present
Custody seals intact on sample bottles?
0 Yes
0 No
, Not Present
Chain of Custody (COC) present?
Yes
0 No
CDC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
* Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
i Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
s Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No
I* N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
s N/A
Soil VOA method 5035 -- compliance criteria met
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d
Special precautions or instructions included?
Comments:
Signature: Brandi Watson
0 Yes 0 No 0 N/A
(— Low concentration EnCore samplers (48 hr)
F_ Low cone pre -weighed vials (Sod Bis -14 d)
0 Yes * No
Date & Time: ,11/2612019 13:40:02
SAMPLING LOG # A & L EASTERN AGRICI-11 T o F^
76?rt u�"°' CHAIN OF r2m�DS�f'O®�'T
CUSTOMER: SYV�AGRO Ftolllllllllilll�llllllll � z ' RECORD
��® RECORD �v�°�
lalllllllllllllllllllllll 8156
PROJECT
'�
Illlllll�lltlll
1TJ _� . _.
•operfield sampling procedures
MANAGER:..___. 7'. C.
_ /
Svnaur6C£PtralLLCITech���ai
Winston Atli
section of these samples.
--��++77
Phone:-�._J 7>.�
`
7d 6 (� i
_
- A (f �_Z—
_
SA
A & L
CUSTOMER
SAMPLING
SAMPLE # OF
SAMPLING METHOD METHOD
LAB #
SAMPLE I.D.
LOCATION
TYPE CONTAINERS
DATE TIME PRESERVED SHIPPED
Relinquished by Sampler: !"^ D to Time Recieved by:
Relinquished by:
— - Relinquished by:
SPECIAL INSTRUCTIONS:
For
V�nonitoring purposes.
Date Time Recieved by:
ate Time Recieved by:
a
REMARKS:
_4 cr v
SAMPLE
ANALYSIS REQUEST
I.D.
SLi
5L2
NHq N
NO.-N
Organic
Cd
Cr
Ni
Pb
As
HS Se FPH
CaCO3
equi v.
Volatile
Solids
Mo
Cl
NO
SL1: Total Solids (Moisture), Total Kjoldahl Nitrogen, Phosphorus, and Potassium
SL2: Basic Test SL'1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
Page 6 of 6
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2065-04-WPL-NC WINSTON-SALEM, NC PW SWANN WTP 11/25/2019 1 1 - 1 1 0.5526
LIQUID
Na mg/I = (Na mg/kg x % Solids) � 100 = (1390 x 1.7800) + 100 = 24.742
Ca mg1I = (Ca mg/kg x % Solids) = 100 = (4520 x 1.7600) = 100 = 80.456
Mg mg/I = (mg mg/kg x % Solids) + 100 = (2400 x 1.7800) + 100 = 42.72
Na meq = Na mg/l ; Molec.Wgt.Na = 24.742 _ 23 = 1.07574
Ca meq = Ca mg/l Molec.Wgt.Ca = 80.456 + 20 = 4.0228
Mg meq = Mg mg/I _ Molec,Wgt.Mg = 42.72 =12 = 3.66
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.07574 _ SgrRoot[0.5(4.0228+3.56)] = 0.552468
Printed: 1 /28/2020
Page 1 13:37
ESEARCN ANALYTiCA1
LA ORATORIES, INC.
Analytical/Process Consultations
May S, 2016
City of Winston-Salem Swann WTP
2800 River Ridge Road
Pfafftown, NC 27040
Attention: Bill Brewer
Chemical Analysis for Selected Parameters and Sampling Location Identified as Lagoon 1
(A City of Winston-Salem Swann WTI' Project, collected 08 April 201.E
I. Miscellaneous 1 2 3 4 5
Parameters Unit Results Results Results Results Results
Fecal Coliform MPN/g TS <2 <2 <2 <2 <2
Sample Numben 17319-02 17319-03 17319-04 17319-05 17319-06
Sample Collected Date: 04/08/16 04/08/16 04/08/16 04/08/16 04/08/16
Sample Collected Time: __ -_--
MPN/g TS = Most Probable Number per gram Total Solids
Norm } rm
RESEARCh & A,NA1yTICA[
TAbORATORIES, INC. CHAIN OF CUSTODY RECORD
Analytical / process Consultations
Phone 1336) 696-pRdj
DWR
Division of Water Resources
State of North Carolina
tal Quality
io Resources
1DUANCffl"fff-RVTIFICA ION
TRUCTIONS FOR FORM: RSC 6-16
Please use the following instructions as a checklist in order to ensure all requirep items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker revie time anN#ffDidQhA&Vvt of addi ional
information requested. Failure to submit all of the required items will lead to a ditional���i� view time f r the
permit application. Unless otherwise noted. the Applicant shall submit one Spliqtio and
sunoortina documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Reoduals Source Certification (FORM: RSC 11-15):
Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
/application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
[/ For new or renewed permits, submit a separate certification for each source facility.
or modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
[/Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Res uals Source -Generating Facility Information:
[For each source facility, attach the following:
Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Matz Guidance for
esiduals Land Application Permits".
Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
,afe to be generated, treated, processed, and stored at the facility.
Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
rocessing.
Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
M Pordach source facility, attach the following:
aboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
action reduction requirements.
Lid For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16
Page 1 of 1
RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Winston-Salem/Forsyth County Utilities Commission (R.W. Neilson Water Treatment Plant)
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
R
Swann WTP
Swann WTP
Forsyth
WQ0031314
750
750
R
Swann WTP
Neilson WTP
Forsyth
WQ0031314
2,500
1,499
R
Swann WTP
Thomas WTP
Forsyth
WQ0031314
750
750
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1
DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: R.W. Neilson Water Treatment Plant
2. Facility permit holder is: ❑ Federal, ❑ State, 0 Local Government, or ❑ Private.
Facility permit issued by: Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Bill Brewer — Water Treatment Superintendent
Complete mailing address: 2800 River Ridge Road
City: Pfafftown State: NC Zip: 27040-8435
Telephone number: 336) 397-7727 E-mail address: billb@cityofws.org
4. Facility physical address: 5725 Frye Bridoe Road
City: Clemmons State: NC Zip: 27012
Coordinates: Latitude: N35° 59' 40.7" Longitude: W80° 21' 4"
Datum: DMS Level of accuracy: 100%
Method of measurement: Survey
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 48.0 MGD and facility average daily flow: 21.0 MGD
8. Average amount of residuals being generated at this facility 1,499 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: The Neilson WTP has a residuals pump station that recycles filter backwash
water directly to the head of the plant. This pump station has three (3) 6.48 MGD pumps. The treatment facilities for
basin residuals (heavy solids) consists of three (3) residuals lagoons for settling and drying of solids. Each lagoon has an
effective storage volume of 2.1 MG's each.
Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257,
2. Specify if residuals are defined under 15A NCAC 02T.1102(6} as:
❑ Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ED no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Research & Analytical Laboratories, Inc. and Date of analysis: 3/1/2016
Passed corrosivity test: [D yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: >212 OF (> 140°F)
Passed reactivity test: ® yes ❑no. HCN: <250 mg/kg (<250) & H2S: <500 mg/kg (<500)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
TCLP Parameter
Limit Result
(Mg/1) (mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
0.376
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
0.011
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
0.020
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1, 1 -Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical Laboratories, Inc. and Date of analysis: 9/11/2019
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
6.54
Cadmium
85
39
0.353
Copper
4,300
1,500
44.9
Lead
840
300
27.1
Mercury
57
17
0.0846
Molybdenum
75
n/a
<0.625
Nickel
420
420
22.5
Selenium
100
100 <2.36
Zinc
7,500
2,800 137
b. For Surface Disposal Unit Randfll): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical Laboratories, and Date of analysis: 9/11/2019
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
® > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
6.54
48.1
22.5
FORM: RSC 06-16 Page 3 of 5
5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 20.8 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analvtical Laboratories. Inc. and Date of analysis: 9/11/2019
Parameter
Result
(mg/kg)
Aluminum
112,000
Ammonia -Nitrogen
480
Calcium
1,080
Magnesium
2,440
Nitrate -Nitrite Nitrogen
<21.1
pH (Standard Unit)
6.2
Phosphorus
2,500
Potassium
2,150
Sodium
1,010
Total Kjeldahl Nitrogen
1,150
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.64
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0.40 or 40 %
%. This rate is a (check one): 10 default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: Accepted formula for water
plant residuals.
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (J.") Year PAN
Five -Year
Maximum Adjusted PAN
(mg�kg)
(m9/k9)
824
Surface
634
Injection/Incorporation
N/A
N/A
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A -Water plant residuals
FORM: RSC 06-16 Page 4 of 5
7 Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Eq uivalent:
® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Applicationot Class B:
❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Colifonn Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Dis ?osal.
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item I1. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [ 15A NCAC 02T.I 106(a)(2)].
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction ( VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5
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R.W Neilson Water Treatment Plant
Water System Facility ID = TP2
Production Capacity = 48.0 MGD
City of Winston-Salem
NPDES # = NCO086011
Yadkin River
100.0 MGD
Idol's Raw Water Pump Station
Raw Water Reservoir Raw Water Reservoir Outfall 001
15.0 MG 15.0 MG ! (Currently Inactive)
J
48.0 MGD 20.0 MGD
Chlorine
Caustic Soda/Lime 48.0 MGD ■
Alum
Coagulation
j Waste Pump Station
V (3) 4,500 GPM Pumps
Flocculation 1.15 MGD
2.0 MGD
Lagoon �
Residuals Lagoons Decant
Sedimentation Basins ( )
(3) 2.1 MG25 Each � ~ 400
GPM
Chlorine i Pumps
Filtration Filter Backwash
Filter to Waste
Caustic Soda/Lime 48.0 MGD
Fluoride 48.0 MGD
Chlorine 10
Ortho-phosphate
■
1.0 MG Clearwell 1.0 MG Clearwell '
1.0 MG Clearwell 1.0 MG Clearwell
Entry Point-EP2
Distribution
System
jeA) 4,el-P
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
2.7 WASH WATER AND RESIDUALS HANDLING
�ua.►� �w�� JliS� c�iati..
S,-L eu,�.� A -as
ZJJ Wash Water and Residuals Handling
The existing wash water and residuals generated at the WTP consist of four main flow streams:
Spent wash water,
Filter -to -waste,
Sedimentation basin residuals, and
Miscellaneous drains.
The existing facilities available to process the wash water and residuals include three residuals
lagoons, a lagoon decant pumping station, and a waste pumping station. The plant currently
recycles the plant wash water and residuals decant to the head of the plant. In this project, the
wash water and residuals handling system will change in the following ways:
Abandon the practice of recycling plant wash water and residuals decant,
Demolish the existing lagoon decant pumping station,
Remove all existing pumps and electrical equipment from the waste pumping station.
Abandon the waste pumping station in place.
Cap all lines that provide flow to the existing waste pumping station,
Construct new wash water equalization basin and wash water clarifier,
Demolish existing inlet and decant structures in residual storage lagoons,
Install new inlet structures in residual storage lagoons to receive residuals from new
hoseless vacuum system and wash water clarifier,
Construct new decant structures in residual storage lagoons and tie discharge decant in
new wash water equalization basin,
The proposed wash water and residuals handling system will consist of a new wash water
equalization basin and wash water clarifier, while retaining the use of the existing residual storage
lagoons. For the proposed wash water handling system, spent wash water, filter -to -waste,
sedimentation basin drain, basin overflow, and miscellaneous drain flows for Neilson and East will
be combined in an existing manhole upstream of the waste pumping station and discharged to the
new wash water equalization basin. Each residual storage lagoon will have a new decant structure
installed which will collect and convey the decant by gravity to the new wash water equalization
basin. Submersible pumps in the wash water equalization basin will pump the collected wash
water flows to the new wash water clarifier. The wash water equalization basin effluent will be
dechlorinated in the force main before discharging to the wash water clarifier. The wash water
clarifier effluent and equalization basin overflow will discharge to the creek in accordance with the
existing NPDES permit.
The wash water drainage system upstream of the wash water equalization basin will be designed to
allow one filter to be wasted while one filter is backwashing at the design filtration rate. In
addition, continuous flows from the miscellaneous drains will be discharged to the wash water
equalization basin.
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2_26
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
Residuals collected from the track vacuums and wash water clarifier will discharge by gravity to the
existing storage lagoons in new inlet structures.
Operations of the lagoons will not change in this project to maintain existing redundancy in the
residuals storage lagoons. The existing system consists of three lagoons that are rotated for storage
on an annual basis. Throughout the year, one lagoon receives residuals from the plant while the
previous year's residuals air dry in the other lagoon. The third lagoon is offline and acts as a
standby available for emergencies. In the lagoon that is operating, residuals are thickened
throughout the year, and decant and overflow are discharged to the existing equalization basin.
When a lagoon has reached its storage capacity at the end of the year, it is taken off-line for
approximately one year and allowed to dry through evaporation. After one year of drying, the
residuals are removed with a front-end loader and transported off -site for disposal. The remaining
lagoon is off-line and remains as a standby in case of emergencies.
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-27
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
2.7.2 Wash Water and Residuals Flows and Solids Production
Table 2-24 Wash Water and Residuals Flows Production
Filter Backwash Water
Per filter', gal
63,000
Avg2, gpd
378,000
Maxi, gpd
1,008,000
Filter -to -Waste
Per filter4, gal
24,996
Avg2,4, gpd
149,976
Max3.4, gpd
399,936
Total Residuals Production
Avgs, lb/day
8,551
Max6, lb/day
44,295
Unthickened Residuals Production (track vac+clarifier effluent to lagoons)
Avg5.7, gpd
580,875
Max6.$, gpd
601,231
Thickened Residuals Production (dewatered cake)
Avgs•9, gpd
7,313
Max6,9, gpd
37,846
Free Liquid from Residuals10 (lagoon decant flow to EQ)
Avg, gpd
573,562
Max, gpd
563,385
Clarifier Effluent (to creek)
Avg", gpd
1,229,143
Max12, gpd
2,078,570
1. Flow rate of 20 gpm/sf for six minutes and 5 gpm/sf for one minute.
2. Six filters backwashed in one day.
3. All filters backwashed in one day.
4. Flow rate of 4.13 gpm/sf for 12 minutes.
5. 267 lb/MG, using average flow rate of 32 mgd and 50th percentile turbidity.
6. 9231b/MG, using max flow rate of 48 mgd and 90th percentile turbidity.
7. 0.17 percent solids (from track vacs to EQ basin).
8. 0.88 percent solids (from track vacs to EQ basin).
9. 14.0 percent solids.
10. Unthickened residuals flow minus thickened residuals flow.
11. Pumped flowrate from wash water equalization basin to wash water clarifier under average daily conditions of six
filter washes per day.
12. Pumped flowrate from wash water equalization basin to wash water clarifier under maximum daily conditions of
sixteeen filter washes per day.
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-28
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
2.7.3 Wash Water Equalization Basin
A wash water equalization basin will be provided for flow equalization of wash water prior to
treatment in the wash water clarifier. Depending on the daily flow to the equalization basin, one or
up to three pumps will be required to pump the contents of the basin to the wash water clarifier.
An additional fourth pump will be provided as a standby.
Under average daily conditions of six filter wash cycles per day, one pump is required with three
standby pumps available. Under maximum daily conditions of sixteen filter wash cycles per day,
two pumps are required with two standby pumps available. In the event of a sedimentation basin
drain, all three pumps are required with one standby pump available.
Submersible mixers will not be provided. Operations staff will be required to wash down settled
solids on an as needed basis.
Table 2-25 Wash Water Equalization Basin Design Parameters
Number of basins
Design criteria
Equalization volume, gal.
Basin type
Basin shape
Basin Dimensions
Inside diameter, ft
Average sidewall water depth, It
Average sidewall depth, ft
Slope to sump
Water depth at top of sump, ft
Pumps
Number of pumps
Rated capacity, each, gpm
Rated head, ft
Operating head range, ft
Motor brake horsepower, bhp
Flow Meter
Number of units
Type
Size, inches
Flow measurement range, mgd
1
Storage volume of 6 average filter wash cycles plus 10%
595,000
Reinforced concrete
Circular
75
18
20
1:75
18.5
4
920
35
34-43
15
1
Magnetic
12
1-5
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-29
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
Controls Level sensors will be provided in the equalization basin for level
monitoring and control of the wash water equalization pumps.
Basin level will be transmitted to the PCs. At basin overflow
levels in the basin, an overflow alarm will be transmitted to the
PCs.
Chemical Feed Point
The wash water equalization basin pumps will be automatically
alternated and started and stopped based on level in the wash
water equalization basin. Provisions will be made to start/stop
the pumps locally and from the PCs. Pump status and alarm
conditions will be indicated locally and transmitted to the PCs.
The signal from the flowmeter will be used by the chemical feed
system for pacing of the calcium thiosulfate. The signal will be
transmitted to the PCs for indication.
Calcium thiosulfate will be fed at the wash water equalization
basin valve vault in the clarifier influent force main.
Table 2-26 Wash Water Equalization Basin Flow Conditions
Average daily flow Six filter wash cycles and misc. drains
Pumps required
Maximum daily flow
Pumps required
Maximum daily flow with sedimentation basin drain
Pumps required
2.7.4 Wash Water Clarifier
1 active (3 standby)
Sixteen filter wash cycles and misc. drains
2 active (2 standby)
Sixteen filter wash cycles, misc. drains, and
sedimentation basin drain
3 active (1 standby)
A new wash water clarifier will be constructed to accept wash water equalization basin effluent and
treat the wash water prior to discharge in the creek. Prior to entering the plant discharge line, the
wash water clarifier effluent flow will be measured in a metering manhole. These measurements
will be compiled in a monthly report and sent to NCDEQ to comply with the existing NPDES permit.
The residuals drain in the wash water clarifier will be exercised twice per day to send accumulated
residuals to the storage lagoons.
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-30
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
Table 2-27 Wash Water Clarifier Design Parameters
COMPONENT
Number of basins
1
Basin type
Reinforced concrete
Proposedgoo
Inside wall diameter, ft
80
Inside weir diameter, ft
73.67
Sidewall water depth, ft
12
Total sidewall depth, ft
14
Water depth at center pier, ft
15.1
Floor radial slope to center
loadingHydraulic
1:12
Average daily
Max daily
Max daily with sedimentation basin drain
Detention time, hr
Average daily
Max daily
Max daily with sedimentation basin drain
Weir type
Weir loading rate, gpm/ft
Average daily
Max daily
Max daily with sedimentation basin drain
Controls
0.18
0.37
0.55
8.81
4.40
2.94
Perimeter; sharp -crested, V-notch
11.54
23.08
34.61
Clarifier drive status and alarm conditions will be indicated
locally and transmitted to the PCS.
The clarifier residual drain valve will be opened and closed
automatically either (1) based on an operator selectable
cycle time set point for number of hours of plant operation
or (2) a total accumulated wash water clarifier flow
volume between blow -downs. In "time" mode, the PCS will
open the valve for an operator -entered duration and close
the valve for the remainder of the cycle. In "flow" mode,
the valve open duration will be the same as the "time"
mode "open duration set point". The basis for automatic
control ("time" or "flow"), the cycle time set point, and the
flow volume set point is entered at the PCS workstation
computers. Provisions will be made to open and close the
residuals drain valve locally and from the PCS.
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-31
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
2.7.5 Residuals Storage Lagoons and Decant Structures
Each existing storage lagoon can hold all of the solids produced in one year, assuming that the
design thickened residual concentration is 14% and the plant is consistently receiving median raw
water turbidity based on the existing monthly operating reports. According to plant data, the
existing average flowrate is 19.2 mgd. In the future, it is anticipated that the average flowrate of the
plant will increase up to 32 mgd. The existing and anticipated residuals production is detailed in
the table below.
Table 2-28 Residuals Solids Production
Filtered Flow, mgd
19.2
32
Turbidity, NTU
16.0
16.0
Coagulant, mg/L
16.8
20
Carbon (PAC), mg/L
0.17
0.84
Solids Production, ppd
4,802
8,551
Solids Production, lbs/yr
1,752,789
3,121,016
Solids Production, lb/MG
250
267
In the future, to maintain annual turnover of the storage lagoons with increased solids production,
the lagoons will need to be enlarged. For lagoons 1 and 2, two additional feet will be excavated and
the length of the lagoons will be extended to the north for future growth. For lagoon 3, two feet will
be excavated.and the width and length will remain unchanged. The expansion and excavation of
the lagoons will not be completed in this project, but the future elevations will be used for the
proposed decant structure design and construction.
Table 2-29 Residuals Storage Lagoons Dimensions
Bottom surface area, ft2
22,498
22,617
29,506
Top surface area, ft2
36,949
36,983
43,107
Residuals depth, ft
7
7
7
Freeboard,ft
1
1
1
Available lagoon volume, gal
1,556,322
1,560,328
1,901,008
Solids storage, lbs/yr
1,817,162
1,821,839
2,219,617
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-32
Winston-Salem/Forsyth County Utility Commission I DESIGN MEMORANDUM
11
11
11
Bottom surface area, ft2
36,021
36,021
24,868
Top surface area, ftz
58,068
58,068
43,107
Residuals depth, ft
9
9
9
Freeboard,ft
1
1
1
Available lagoon volume, gal
3,167,036
3,167,036
3,050,718
Solids storage, ibs/yr
3,697,831
3,697,831
3,562,018
The proposed changes to the residuals handling system will require the existing residuals lines to
be cut, capped, and abandoned in place. The existing inlet and decant structures will be demolished
and replaced. The proposed hoseless track vacuum system will have new residuals headers
installed from the sedimentation basins to the residuals storage lagoons. In the proposed inlet
structure, the clarifier drain lines will discharge to the lagoons. The residuals and effluent drain
lines will be isolated from each other despite sharing the same inlet structure. The proposed
lagoon decant structures will include weirs and manual slide gates that can be adjusted throughout
the collection year. The decant structures for the three lagoons will tie together with manholes and
discharge by gravity to the wash water equalization basin.
Table 2-30 Residuals Storage Lagoons
Number of lagoons 3
Lagoon type Earthen lagoon with existing bentonite liner
Perimeter Slope 2:1 (future)
Effective storage, each lagoon, days 365
Influent 8" residuals line from track vacs and 8" clarifier drain
Decant Discharge to equalization basin
2.8 CHEMICAL FEED AND STORAGE BUILDING
The following chemicals are used in the existing treatment processes: sodium hypochlorite,
aluminum sulfate, hydrofluosilicic acid, zinc orthophosphate, and sodium hydroxide. These
chemicals, with the exception of the sodium hypochlorite holding tanks, are stored in and pumped
out of the chemical storage building. Sodium hypochlorite is stored outside in an outdoor
containment structure with a canopy cover. The existing floor drains located in each chemical
storage room drain to the lagoons.
In this project, the existing storage tanks and chemical metering pumps will be removed and
replaced. A more detailed description of the Chemical Building modifications can be found in
section 3.0 - Chemical Feed Design Memorandum.
BLACK & VEATCH I Civil and Process Mechanical Design Memorandum 2-33
R.W. Neilson Water Treatment Plant
Solids Handling Plan
The Neilson Water Treatment Plant is a 48 MGD water treatment facility. Solids are
generated by manual sludge removal from sedimentation basins, backwashing filters, and
filter -to -waste after filter backwashes are completed. Solids produced from filter backwashes
and filter -to -waste is routed to a waste pump station and is then pumped to the head of the
water treatment process. Solids removed from the sedimentation basins are routed directly to
one of three residual lagoons.
Permits and Classifications:
1. The discharge from the residuals lagoons is authorized by NPDES Permit NCO086011.
The classification for the discharge is Grade 1 Physical/Chemical.
2. The distribution of the residuals removed from the lagoons is authorized by permit
WQ0031314. The residuals are classified as Class A.
Operation:
1. The system consists of a waste station with (3) Fairbanks Morse single stage pumps rated
at 6.48 MGD each, (2) Fairbanks Morse basin sludge pumps rated at 1.0 MGD each, (2)
lagoon pumps rated at 0.65 MGD each and (3) residuals lagoons (3 lagoons at —2.0 MG).
Each residuals lagoon consists of an oval earthen lagoon with clay bottom.
2. Routine inspections of equipment will be conducted Senior Utility Plant Supervisor to
ensure proper operation of equipment. Any equipment not functioning properly will be
reported through the water division's asset management program, MAXIMO, to the
appropriate support group for repair/replacement.
3. Backwash and filter -to -waste water from the plant process flows to the waste station and
then is pumped by the waste station pumps to raw water reservoirs at the head of the plant
treatment process.
4. All sedimentation basin and hopper blow downs are pumped by the basin sludge pumps
directly to one of three residuals lagoons.
The solids stream enters on one end of each lagoon and decant is pumped from the
opposite end by the lagoon pumps to the waste station where it is returned to the head of
the treatment process.
6. Residuals lagoons are rotated with one cleaned and ready for use, one in service and one
drying at all times.
R.W. Neilson Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
7. Residuals are removed from the lagoons and hauled to the application site by a private
contractor.
Monitoring and Reporting Requirements:
1. Residuals generated by each source -generating facility must be analyzed to demonstrate
that they are non -hazardous based on the most current permit requirements (Attachment
A). Sampling will be conducted under supervision of the Senior Water Treatment Plant
Supervisor by WSFC Utilities current contractor as described below in compliance with
permit requirements.
2. Analysis will be performed by a NC Certified Laboratory.
3. Analyses made according to monitoring and reporting requirements must be certified for
the required parameter(s).
4. Corrosivity, ignitability, reactivity, and a Toxicity Characteristics Procedure analysis are
required once each permit cycle. The TCLP analysis includes the following parameters
(i.e., note the regulatory level in milligrams per liter in parentheses):
Arsenic (5.0)
Barium (100.0)
Benzene (0.5)
Cadmium (1.0)
Carbon tetrachloride (0.5)
Chlordane (0.03)
Chlorobenzene (100.0)
Chloroform (6.0)
Chromium (5.0)
m-Cresol (200.0)
o-Cresol(200.0)
p-Cresol (200.0)
Cresol (200.0)
2,4-D (10.0)
1,4-Dichlorobenzene(7.5)
1,2-Dichloroethane (0.5)
1, 1 -Dichloroethylene (0.7)
2,4-Dinintrotolulene (0.13)
Endrin (0.02)
Hexachlorobenzene(0.13)
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Hexachloroethane (3.0)
Lead (5.0)
Lindane (0.4)
Mercury (0.2)
Methoxychlor (10.0)
Methyl ethyl ketone (200.0)
Nitrobenzene (2.0)
Pentachlorophenol (100.0)
Pyridine (5.0)
Selenium (1.0)
Silver (5.0)
Tetrachloro ethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,6-Trichlorophenol (2.0)
2,4,5-TP (Silvex) (1.0)
Vinyl chloride (0.2)
5. Analyses of the following parameters are also required with each application event:
Aluminum
Ammonia -Nitrogen
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Nitrate -Nitrite Nitrogen
Phosphorous
Potassium
pH
Plant Available Nitrogen
(by calculation)
Selenium
Sodium
% Total Solids
TKN
Zinc
6. Data to verify pathogen reduction and vector attraction reduction of the residuals is
maintained on file for five years. The required data is specific to the stabilization process
utilized, and is also sufficient to demonstrate clear compliance with the Class A pathogen
R.W. Neilson Water Treatment Plant
Solids Handling Plan -Permit 4WQ031314
Revised 07/14/2020
2
requirements and restrictions noted in 15A NCAC 02T .1106 (a) and (b) and vector
attraction reduction requirements in 15A NCAC 02T .1107 (a).
7. Proper records are maintained tracking all residuals activities. These records include the
source, volume, analysis, and recipient of the residuals.
8. Three copies, per application event, of all required monitoring and reporting requirements
are submitted annually before March 1, to NC DEQ-DWQ.
Performance Standards:
The pollutant concentrations in any residuals that are land applied to any land application
site shall not exceed the following Ceiling and Monthly Average Concentrations (i.e.
dry weight basis):
Parameter
Monthly Average
Concentration
milligrams per kilo,i am)(milligrams
Ceiling Concentration
per kilogram)
Arsenic
41
75
Cadmium
39
85
Copper
1,500
4,300
Lead
300
840
Mercury
17
57
Molybdenum
n/a
75
Nickel
420
420
Selenium
100
100
Zinc
2,800
7,500
2. If residuals are sold or given away, one of the Class A pathogen requirements in 15A
NCAC 02T .I 106(b) must be met.
Application Requirements:
1. Bulk residuals are not applied under the following conditions:
i. If the residuals are likely to adversely affect a threatened or endangered species.
ii. If the application causes prolonged nuisance conditions.
iii. If the land fails to assimilate the bulk residuals or the application causes the
contravention of surface water or groundwater standards.
iv. If the land is flooded, frozen, or snow-covered or is otherwise in a condition such that
runoff of the residuals would occur.
v. During a precipitation event or within 24 hours following a rainfall event of 0.5
inches or greater in a 24-hour period.
vi. Within the 100-year flood elevation, unless the bulk residuals are injected or
incorporated within a 24-hour period following the residuals application event.
R.W. Neilson Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
vii. During a precipitation event or within 24 hours following a rainfall event of 0.5
inches or greater in a 24-hour period.
viii. If the slope of the land is greater than 10 percent when the bulk residuals are surface
applied, and if the slope of the land is greater than 18 percent when bulk residuals are
injected or incorporated.
ix. If pH maintained in the soil and residuals mixture is greater than 6.0.
x. If the land does not have an established vegetative cover.
xi. If the vertical separation of the seasonal high water table and the depth of the
residuals application is less than one foot.
xii. If the vertical separation of the depth to bedrock and the depth of residuals application
is less than one foot.
xiii. Application exceeds agronomic rates.
xiv. For residuals treatment and storage facilities, the following minimum setbacks shall
be adhered to:
Minimum Setback
Description of Setback
(feet)
Habitable residence or place of public assembly under separate ownership or
not to be maintained as part of the project site
100
Property lines
50
Private or public water supply
100
Surface waters (streams, -intermittent and perennial, perennial water bodies,
and wetlands)
50
Wells with exception to monitoring wells
100
2. When land applying bulk residuals to application site, the following minimum setbacks
are maintained at all times:
Setback By Type of
Residual feet
Description of Setback
Liquid
Cake
Private or public water supply
100
100
Surface waters (streams -intermittent and perennial,
perennial water bodies, and wetlands)
100
25
Surface water diversions (ephemeral streams,
waterways, ditches)
25
0
Groundwater lowering ditches (where bottom of
The ditch intersects SHWT)
25
0
Subsurface groundwater lowering astern
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
3. Specific bulk residuals land application area boundaries are clearly marked on each land
application site prior to and during a residuals land application event.
4. Bulk residuals and other sources of PAN (Plant Available Nitrogen) are applied to all land
application sites at or below agronomic rates. Appropriate agronomic rates are calculated
R.W. Neilson Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
4
using expected nitrogen requirements based on the Realistic Yield Expectations (RYE)
field cover for each approved land application site.
Spills and Noncompliance Notification:
1. The Winston-Salem Regional Office, telephone number (336) 771-5000, will be notified
within 24 hours or the next working day following the occurrence or first knowledge of
the occurrence of any of the following:
i. Any occurrence with the distribution program which results in the land application of
significant amounts of wastes which are abnormal in quantity or characteristic.
ii. Any failure of the distribution program resulting in a release of materials to receiving
waters.
iii. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate residual treatment.
2. Persons reporting such occurrences by telephone shall also file a written report in letter
form within (5) days following first knowledge of the occurrence. This report must
outline the actions taken or proposed to be taken to ensure that the problem does not recur.
3. Emergency Contacts: Neilson Water Treatment Plant (336) 766-9885 (Main)
Gabriel Sparks, Plant Supervisor (336) 747-7471 (0)
(336) 944-1222 (M)
Bill Brewer (336) 397-7727 (0)
Water Treatment Superintendent (336) 745-5277 (M)
Winston-Salem/Forsyth County (336) 727-8418
Utility Administration
DEQ Regional Office (336) 771-5000
General Emergency 911
HazMat
R.W. Neilson Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
5
RESEARCh & lANAlyT7CAI
LAboRAToFtks, INC.
AnaWloal/Process Consultations
Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Neilson WTP
_(A City of Winston-Salern Neilson WTP Project collected 011VIarch 2016
Nelson WTP
EPA HW
Quantitating
Results
Characteristic
Number
Contaminant
Lita(t(msrll.)
{melt.)
LavellmWL)
EPA Method
i.
TCLP METALS
1:1.004
Aronle
0.0I0
BQL
S.00
6010C
1)
Barium
0.040
0.376
100
6010C
1)•006
Cadmium
0.005
BQL
1.00
6010C
D-077
Chromium
0.010
0.020
5.00
6010C
D-008
Lead
0.60S
06011
5.00
601DC
13-009
Mercury
0.0020
BQL
0,200
7470A
D•010
selenlum
0.100
BQL
1.00
6010C
D-01I
Silver
01010
BQL
5,00
6010C
IL
TCLP VOLATILES
D-018 Benzene
0.050
BQL
0.500
8260B
D-019
Carbon Tetrachloride
0.050
BQL
0.500
82609
D-021
Chlorobenzene
0.030
BQL
too
8250B
D-022
Chloroform
0.500
BQL
6.00
8260B
D-028
1,2-Dichlomthnne
0.050
BQL
0,500
8260E
D-029
1,i-Dichloroethytene
0.050
BQL
0.700
8260E
D-035
Methyl Ethyl Ketone
0.5u0
BQL
200
8260E
D-039
Tetmehlomethylene
0.050
BQL
0.700
8260B
D•040
Trichlemethylene
0.050
BQL
0.500
8z6OB
D-043
Vinyl Chlodde
0.050
BQL
0.200
9260B
I[I�
TCLF SEMI-VULATILES
D-023 (I -Creosol
20.0
BQL
200
8270D
D-024
M-Creosol
2010
BQL
200
82701)
D-025
p-Crcosol
2010
BQL
200
817013
D-026
Creosol
20.0
BQL
20D
8270D
D-027
1,4-Dichlorobenzene
0.750
BQL
7.50
8270D
D-030
2,40nitrotoluene
0.050
BQL
0.130
8270D
D-032
Hexachlorobenzene
0.050
BQL
0.Do
8270D
D-035
Hexaehlorobutadiene
050
BQL
0.500
8270D
D•034
Hexachloroethane
0.300
BQL
3.OD
8270D
1)•036
Nitrobemzeno
0.200
BQL
2.0D
MOD
D-037
Pentachlarophenol
10.0
BQL
too
9270D
D-038
Pyridine
0.500
BQL
5.00
8270D
D-041
2,4,5-Trichloruphenol
40.0
BQL
400
8270D
D-042
2,4,6-Trich1orophenol
0.200
BQL
2.00
8270D
iv.
TCLP PLSTICIDESl01il111CIDES
0.003
BQL
0.030
BOB] B
D-020
D-016
Chlordane
2,4-D
1.000
BQL
10.0
B15I A
D-012
Endrin
0.002
SQL
0.020
8091 B
D-031
Heptachlor
0.0008
BQL
0.008
8031 B
D-013
Lindane
0.040
BQL
0.400
8081 B
D-014
Medwxyahlor
1-000
BQL
1010
8081 B
D-015
Toxaphene
0.050
BQL
0.500
8081 B
D-017
2A5-TP(Silvex)
0.100
BQL
1.00
8151 A
V.
REACTIVITY
0-003
Cyanide
2.0
BQL
9010
D-003
Sulfido
10.0
BQL
9030
VL
CORROSIVITY
D-002
pH
Std. Units
i.30
9045
VII.
TCLPMiscELLANEOUS
Paint Filter Test
NFL
VIILIGNITABILITY
D-001
Ipnitability
WNI
1010
Sample Number 15606-08
Sample Date 03/01/16
Sample Time (hrs) 0800
Sample Matrix Solid
BQL = BelowQuentitationLimiu rnWL cmiltigcamaper Liter =parts per million (ppm) NFL No Fret Liquids
Waypoint,o
ANALYTICAL
5f7/2019
EMA Resources Inc
Brent Collins
755 Yadkinviile Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-116-0282
Client Project Description: Neilson WTP
2790 Whitten Road, Memphis, TN 38133
Main 901.213,24001 Fax 901.213.2440
www.waypointa nalytical. com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/26/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be heldiare available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulflte...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysls(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability In any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015
mississippi California #2904
Kentucky #90047 Tennessee #TN02027
•=�>"1
FP
s
e
VA NELAP 4460181
NC #415
EPA #TN00012
Texas #TI04704180 Arkansas #88-0650
Oklahoma #9311 5C #84002
Kentucky UST #80215 PA DEP #68-03195
Page 1 of 13
d
.a-
Waypoinx-
ANALYTICAL
Client: EMA Resources Inc
Project: Neilson WTP
Lab Report Number: 19-116-0282
Date: 5/7/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400" Fax 901.213.2440
www.waypointanalytica Isom
CASE NARRATIVE
Metals Analysis Method 601 OD
Analyte: Aluminum
QC Batch No: L434240
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Calcium
QC Batch No: L434067
MS/MSD Recovery failed, DT confirmed matrix interference
Analyte: Iron
QC Batch No: L434240
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L434240
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Magnesium
QC Batch No: L434067
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was not within the method limits. Matrix interference is suspected.
Analyte: Manganese
QC Batch No: L434067
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was not within the method limits. Matrix Interference is suspected.
Analyte: Molybdenum
QC Batch No: L434067
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Analyte: Lead
QC Batch No: L434067
Page 2 of 13
Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax 901.213.2440
www.waypointanalytical.com
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range due to
the analyte concentration being greater than 25 times the method quantitation limit (MQL). A dilution test was
performed and the recovery was not within the method limits. Matrix interference is suspected.
Analyte: Selenium
QC Batch No: L434067
The matrix spike (MS) and/or the matrix spike duplicate (MSD) was out of the acceptable recovery range. Due to
the analyte concentration being less than 25 times the method quantitation limit (MQL) a post digestion spike was
performed and the recovery was within the method limits. No matrix interference is suspected.
Page 3 of 13
P
WlJFpainry 2790 Whitten Road, Memphis, TN 38133
® a Main 901.213.2400 0 Fax 901.213.7440
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Neilson WTP Report Date: 05/07/2019
755 Yadkinville Rd Information : Received : 04/26/2019
Macksville , NC 27028
Report Number :19-116-0282 REPORTOFANALYSIS Danyale Love
Project Manager
Lab No : 92234
Sample ID: Neilson WTP #'1
Matrix: Solids
Sampled: 4/25/2019 8:30
Test
Results
Units
MDL
MOL
DF
Date I Time
By
Analytical
Analyzed
Method
% Moisture
78.4
%
0,010
1
04/26/19 16:25
ADM
SW-DRYWT
Ammonia Nitrogen
284
mg/Kg - dry
116
1
05/06/19 15:00
JPJ
4500NH3C-2011
Nitrate+ N itrite-N
75.9
mg/Kg - dry
21.5
21.5
1
05/03/19 12:45
ZBD
4500NO3F-2011
Organic N
5050
mg/Kg - dry
323
1
05/06/19 15:00
CALCULATION
pH
7.1
s.u.
1
05/06/19 07:11
JSL
9045D
Total Solids
21.6
%
0.010
0.010
1
04/26/19 16:25
ADM
2540G-2011
Total Volatile Solids
25.1
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Kjeldahl Nitrogen
5320
mg/Kg - dry
323
1
05/07/19 14.22
CLP 4500NORGD-2011
Phosphorus
2990
mg/Kg - dry
11.9
23.1
1
05/01/19 22:34
BKN
6010D
Aluminum
117000
mg/Kg - dry
94.0
231
10
05/02/19 13:57
BKN
6010D
Arsenic
6.67
mg/Kg - dry
1.94
2.31
1
05/01/19 22:34
BKN
6010D
Cadmium
<0.229
mg/Kg - dry
0.229
0.463
1
05/01/19 22:34
BKN
6010D
Calcium
861
mg/Kg - dry
77.8
116
1
05/01/19 22:34
BKN
6010D
Chromium
35.0
mg/Kg - dry
0.879
1.16
1
05/01/19 22:34
BKN
6010D
Copper
34.6
mg/Kg - dry
0.671
1.16
1
05/01/19 22:34
BKN
6010D
Iron
3280D
mg/Kg - dry
1916
23.1
1
05/01/19 22:34
BKN
6010D
Lead
23.1
mg/Kg - dry
0.689
1,39
1
05/O1/19 22:34
BKN
6010D
Magnesium
1500
mg/Kg - dry
10.3
23.1
1
05/01/19 22:34
8KN
6010D
Manganese
359
mg/Kg - dry
0.847
2.31
1
05/01/19 22:34
BKN
60101)
Mercury
0.0912
mg/Kg - dry
0,0150
0.0681
1
05/02/19 11:25
KKM
7471A
Molybdenum
0.787J
mg/Kg - dry
0,601
1.16
1
05/01/19 22:34
BKN
6010D
Nickel
16.2
mg/Kg - dry
0.763
1.16
1
05/O1/19 22:34
BKN
6010D
Potassium
1440
mg/Kg - dry
13.8
23A
1
05/01/19 22:34
BKN
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 4 of 13
O
W point,
ay
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 yadkinville Rd
Mocksville , NC 27028
Report Number :19-116-0282
Lab No: 92234
Sample ID : Neilson WTP #1
Test
Selenium
Sodium
Zinc
Sulfur
Sodium Absorption Ratio
Qualifiers/ B
Definitions I
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax 901.213.2440
www.waygointanalytical.com
Project Neilson WTP
Information :
REPORT OFANALYSIS
Results Units MOL
Report Date : 05/07/2019
Received : 04/26/2019
0C"'6&s� Q�-a
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/25/2019 8:30
MQL DF Date I Time By Analytical
Analyzed Method
<2.27 mg/Kg - dry 2.27 2.31 1 05/O1/19 22:34 BKN 6010D
<357 mg/Kg - dry 357 1160 10 05/02/19 13:57 BKN 6010D
96.3 mg/Kg - dry 5.00 5.79 1 05/01/19 22:34 BKN 6010D
2780 mg/K9 - dry 22.6 23.1 1 05/01/19 22:34 BKN 6010D
<5.00 Ratio 5.00 1 05/01/19 22:34 CALCULATION
Analyte detected in blank
Estimated value
OF Dilution Factor
MQL Method Quantitation Urnit
Page 5 of 13
0
2790 Whitten Road, Memphis, TN 38133
Waypoint.Main 901.213.2400 0 Fax 901.213.2440
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc
Brent Collins Project Neilson WTP Report Date : 05/07/2019
755 Yadkinville Rd Information: Received: 04/26/2019
Mocksville , NC 27028
Report Number: 19-116-0282
Lab No : 92235
Sample ID : Neilson WTP #2
REPORTOFANALYSlS
a Love
Proect Manager
Project
Matrix: Solids
Sampled: 4/25/201.9 8:30
Test
Results
Units
MDL
MOL
DF
Date/Time
By
Analytical
Analyzed
Method
% Moisture
78.7
%
0.010
1
04/26/19 16:25
ADM
SW-DRYWT
Ammonia Nitrogen
445
mg/Kg - dry
117
1
05/06/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
54.0
mg/Kg - dry
22.9
22.9
1
05/03/19 12:45
ZBD
4500NO3F-2011
Organic N
5120
mg/Kg - dry
245
1
05/06/19 15:00
CALCULATION -
pH
6.6
S.U.
1
05/06/19 07:11
JSL
9045D
Total Solids
23.8
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Volatile Solids
24.9
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Kjeldahl Nitrogen
5540
mg/Kg - dry
245
1
05/07/19 14:23
CLP 4500NORGD-2011
Phosphorus
2590
mg/Kg - dry
12.1
23.5
1
05/01/19 22:39
BKN
6010D
Aluminum
140000
mg/Kg - dry
95.3
235
10
05/02/19 14:02
BKN
6016D
Arsenic
7.46
mg/Kg - dry
1.97
2.35
1
05/01/19 22:39
BKN
6010D
Cadmium
0.3713
mg/Kg - dry
0.232
0.469
1
05/01/19 22:39
BKN
6010D
Calcium
869
mg/Kg - dry
78.9
117
1
05/01/19 22:39
BKN
6010D
Chromium
60.6
mg/Kg - dry
0.892
1.17
1
05/01/19 22:39
SKN
6010D
Copper
50.7
mg/Kg - dry
0.681
1.17
1
05/01/19 22:39
BKN
6010D
Iron
6060D
mg/Kg - dry
199
235
10
05/02/19 14:02
BKN
6010D
Lead
37.2
mg/Kg - dry
0.699
1.41
1
05/01/19 22:39
BKN
6010D
Magnesium
2330
mg/Kg - dry
10.4
23.5
1
05/01/19 22:39
BKN
6010D
Manganese
402
mg/Kg - dry
0.859
2.35
1
05/01/19 22:39
BKN
6010D
Mercury
0.0859
mg/Kg - dry
0.0160
0.0723
1
05/02/19 11:27
KKM
7471A
Molybdenum
1.27
mg/Kg - dry
0.610
1.17
1
05/01/19 22:39
BKN
6010D
Nickel
26.9
mg1Kg - dry
0.774
1.17
1
05/01/19 22:39
BKN
6010D
Potassium
2310
mg/Kg - dry
14.0
23.5
1
05/01/19 22:39
BKN
6010D
Qualifiers/ B Analyte detected in blank
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 6of13
e
2790 Whitten Road, Memphis, TN 38133
Waypoint.
Main 901.213.2400 ° Fax 901.213.2440
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Neilson VdTP
Report Date : 05/07/2019
Brent Collins
Received : 04/Z6/2019
755 Yadkinvilie Rd
Information
:
Mocksville , NC 27028
Danyale Love
Report Number :19-116-0282
REPORT OFANAL YSIS
project Manager
Matrix: Solids
Lab No: 92235
Sampled; 4/25/2019 8:30
Sample ID: Neilson WTP #2
Test
Results
Units
MQL
MQL DF Date I Time By Analytical
Analyzed Method
Selenium
<2.30
mg/Kg - dry
2.30
2.35 1 05/01/19 22:39 BKN 6010D
Sodium
<362
mg/Kg - dry
362
1170 10 05/02/19 14:02 BKN 6010D
144
mg/Kg -dry
5.07
5.87 1 05/01/19 22:39 BKN 6010D
Zinc
Sulfur
3030
mg/Kg - dry
23.0
23.5 1 05/O1/19 22:39 8KN 60100
Sodium Absorption Ratio
<5.00
Ratio
5.00 1 05/01/19 22:39 CALCULATION
Qualifiers/ B Anaiyte detected in blank
Definitions 3 Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 7 of 13
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :19-116-0282
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.2440
w w w.wa y p o i n t a n a lyti ca I -co m
Project Neilson WTP
Information :
REPORT OFANALYSiS
Report Date: 05/07/2019
Received : 04/26/2019
00,'6acb Q�.a
Danyale Lave
Project Manager
Lab No : 92236 Matrix: Solids
Sample ID :!Neilson WTP #3 Sampled: 4/25/2019 8:30
Test
Results
Units
MDL
MQL
DF
Date lTime
By
Analytical
Analyzed
Method
%Moisture
70.4
°/a
0.010
1
04126/1916:25
ADM
SW-DRYWT
Ammonia Nitrogen
358
mg/Kg - dry
84.5
1
05/06/19 15:00
IP]
4500NH3C-2011
Nltrate+Nltrite-N
47.3
mg/Kg - dry
15.7
15.7
1
05/03/19 12:46
ZBD
4500NO3F-2011
Organic N
3990
mg/Kg - dry
281
1
05/06/19 15:00
CALCULATION
pH
6.4
SM.
1
05/06/19 07:11
JSL
9045D
Total Solids
29.6
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Volatile Solids
22.5
%
0.010
0.010
1
04/26/19 16:25
ADM
2540G-2011
Total Kjeldahl Nitrogen
4360
mg/Kg - dry
281
1
05/07/19 14:24
CLP 4500NORGD-2011
Phosphorus
2070
mg/Kg - dry
8.68
16.9
1
05/01/19 22:44
BKN
6010D
Aluminum
1.16000
mg/Kg - dry
68.6
169
10
05/02/19 14:07
BKN
6010D
Arsenic
7.26
mg/Kg - dry
1.42
1.69
1
05/01/19 22:44
BKN
6010D
Cadmium
0.378
mg/Kg - dry
0.167
0.338
1
05/01/19 22:44
BKN
6010D
Calcium
652
mg/Kg - dry
56.8
84.5
1
05/01/19 22:44
BKN
6010D
Chromium
44.3
mg/Kg - dry
0.641
0.844
1
05/01/19 22:44
BKN
6010D
Copper
37.8
mg/Kg - dry
0.490
0,845
1
05/01/19 22:44
BKN
6010D
iron
49300
mglKg - dry
143
169
10
05/02/19 14:07
BKN
6010D
Lead
28.7
mg/Kg - dry
0.503
1.01
1
05/01/19 22:44
BKN
6010D
Magnesium
2040
mg/Kg - dry
7.50
16.9
1
05/01/19 22:44
BKN
6010D
Manganese
588
mg/Kg - dry
0.618
1.69
1
05/01/19 22:44
BKN
6010D
Mercury
0.0912
mg/Kg - dry
0.0114
0.0514
1
05/02/19 11:28
KKM
7471A
Molybdenum
1.05
mg/Kg - dry
0.439
0.844
1
05/01/19 22:44
BKN
6010D
Nickel
19.7
mg/Kg - drY
0.557
0.844
1
05/01/19 22:44
BKN
6010D
Potassium
1950
mg/Kg - dry
10.1
16.9
1
05/01/19 22:44
BKN
6010D
Qualifiers/ 8
Analyte detected in blank
DF
Dilution
Factor
Definitions J
Estimated value
MQL
Method Quantitation Limit
Page 8 of 13
46245
EMA Resources Inc
Brent Collins
755 yadkinville Rd
Mocksville , NC 27028
Report Number :19-116-0282
Lab No: 92236
Sample ID : Neilson WTP #3
Test
Selenium
Sodium
Zinc
Sulfur
Sodium Absorption Ratio
ww"
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax 901.213.244D
www.waypointa nalyti cal.com
Project Neilson WTP Report Date : 05/07/2019
Information : Received ; 04/2612019
Q'"
Danyale Love
REpORTOFANALY.SIS project Manager
Matrix: Solids
sampled: 4/25/2019 8,30
Results units MDL MQL DF Date 1 Time By Method l
Analyzed
<1.66
mg/Kg - dry 1.66
1.69
1
05/01/19 22:44 BKN
6010D
<261
mg/Kg - dry 261
845
16
05/02/19 14:07 BKN
6010D
106
mg/Kg - dry 3.65
4.22
1
05/01/19 22:44 BKN
6010D
2470
mg/Kg - dry 16.5
16.9
1
05/01/19 22:44 BKN
6010D
<5.00
Ratio
5.00
1
05/01/19 22:44
CALCULATION
DF Dilution Factor
Qualifiers/ B Analyze detected in blank MQL Method Quantization L"smit
Definitions 7 Estimated value
Page 9 of 13
0
Waypoinic-
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 1 Fax 901.213.2440
ANALYTICAL. www.waypointanalytical.com
46245
EMA Resources Inc
Brent Coffins Project Neilson WTP Report Date: 05/07/2019
755 Yadkinville Rd Information: Received : 04/26/2019
Mocksville , NC 27028
Report Number :19-116-0282
Lab No : 92237
Sample ID : Neilson WTP #4
Test
RrPORTOFANALYSIS
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/25/2019 8:30
Results Units MDL MQL DF Date i Time By Analytical
Analyzed Method
% Moisture
71.7
%
0.010
1
04/26/19 16:25
ADM
SW-DRYWF
Ammonia Nitrogen
392
mg/Kg - dry
88.3
1
05/06/19 15:00
JPJ
4500NH3C-2011
Nitrate+Nftrite-N
32.0
mg/Kg - dry
17.7
17.7
1
05/03/19 12:47
ZBD
4500NO3F-2011
Organic N
4060
mg/Kg - dry
248
1
05/06/19 15:00
CALCULATION -
pH
5.9
s.u.
1
05/06/19 07:11
ISL
9045D
Total Solids
28.3
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Volatile Solids
23.3
%
0.010
0.010
1
04/26/19 16:25
ADM
254OG-2011
Total Kjefdahl Nitrogen
4450
mg/Kg - dry
248
1
05/07/19 14.25
CLP
4500NORGD-2011
Phosphorus
2210
mg/Kg - dry
9.08
17.7
1
05/01/19 22:50
BKN
6010D
Aluminum
118000
mg/Kg - dry
71.7
177
10
05/02/19 14:12
BKN
6010D
Arsenic
7.81
mg/Kg - dry
1.48
1.77
1
05/01/19 22:50
BKN
6010D
Cadmium
0.382
mg/Kg - dry
0.175
0.353
1
05/01/19 22:50
BKN
6010D
Calcium
809
mg/Kg - dry
59.4
88.3
1
05/01/19 22:50
BKN
6010D
Chromium
43.5
mg/Kg - dry
0,671
0.883
1
05/01/19 22:50
BKN
6010D
Copper
37.8
mg/Kg - dry
0.512
0.883
1
05/01/19 22:50
BKN
6010D
Iron
47700
mg/Kg - dry
150
177
10
05/02/19 14:12
BKN
6010D
Lead
29.1
mg/Kg - dry
0.526
1.06
1
05/01/19 22:50
BKN
6010D
Magnesium
1880
mg/Kg - dry
7.84
17.7
1
05/01/19 22:50
BKN
6010D
Manganese
537
mg/Kg - dry
0.646
1.77
1
05/01/19 22:50
BKN
6010D
Mercury
0.0746
Ong/Kg - dry
0.0123
0.0555
1
05/02/19 11:29
KKM
7471A
Molybdenum
0.985
mg/Kg - dry
0.459
0.883
1
0S/01/19 22:50
BKN
6010D
Nickel
19.5
mg/Kg - dry
0.583
0.883
1
05/01/19 22:50
BKN
6010D
Potassium
1780
mg/Kg - dry
10.5
17.7
1
05/01/19 22:50
BKN
6010D
Qualifiers/ B Analyte detected in blank
DeFnitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 10of13
�4�,�Y,�7.
v
Waypoint`--
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :19-116-0282
Lab No : 92237
Sample ID : Neilson WTP #4
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.2440
www.waypointa nalyti cal. com
Project Neilson UUTP
Information :
REPORT OFANALYSIS
Results Units
MDL
Report Date : 05/07/2019
Received
-�((: 0,�,4�/.2}612019
Q� `,R7�ti
Danyale Love
Project Manager
Matrix: Solids
Sampled: 4/25/2019 8:30
MOIL OF Date / Time By Analytical
Analyzed Method
<1.73
mg/Kg - dry
1.73
1.77
1
05/01/19 22:50
BKN
6010D
Selenium
<273
mg/Kg - dry
273
863
10
05/02/19 14:12
BKN
6010D
Sodium
1.08
mg/Kg - dry
3.82
4.42
1
05/01/19 22:50
BKN
6010D
Zinc
2590
mg/Kg - dry
17.3
17.7
1
05/01/19 22:50
BKN
6010D
Sulfur
Ratio
5.00
1
05/01/19 22:50
CALCULATION
Sodium Absorption Ratio
<5.00
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 11 of 13
Wayo
',
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.7-400 1 Fax 901.713.2440
www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 19-116-0282
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: Fi5
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
COC agrees with sample label(s)?
COC properly completed
0 Yes
• Yes
is Yes
0 No
0 No
0 No
Samples in proper containers?
it Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
Water - VOA vials free of headspace
Trip Blanks received with VOAs
Soil VOA method 5035 — compliance criteria met
0 Yes
0 Yes
0 Yes
0 Yes
0 No
0 No
0 No
0 No
0 NIA
* N/A
N/A
�* N/A
F High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F— High concentration pre -weighed (methanol -14 d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes No
Comments:
Signature: oryPhillips _ Date & Time: 4/26/2019 13:35:27
Page 12of13
ME
Client Name/Address
Client Project Manager/Contact
Sitting Information
For laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 YadkinAlle Rd
Mocksville, NC27028
Mf
1l['�I I 111` 1`j'�V�` j�j��
Il
Project Description
Project/site location (City/State)
RUSH —Additional charges apply
Special Detection Unilt(s)
L
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iter
1�l11 1 1��� 11111111 11���
Date Results Needed
I"
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111H ul `u ��Z6620192 I —Oil
Eh1AResources Ine 13:32:42
Pu.
Neilson WTP
Project Number
Project Manager Phone 0
Project Manager Email
336-399-3646
brent.callins@emaresources.com
A Coal a 10C Na2S203 (Mlao Only)
��as /�a
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ANALYTICAL
A
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E NaOH pHa10
2790 Whitten Road
Unless noted, all carttainers
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43
ca
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Memphis, TN 38133
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per Table II of 40 CFR Part
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136.
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Sample Identification
Required
Analysis / Prese•rva9wo
Comments/Notes
Ne;1-4
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}(Metals:AI,As,Ca,Cd,Cr,Cu,Fe,Pb
912;5
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Mn,M9,Mo,H9,Ni,Se,Na,P,S,K,Zn
3
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For Laboratory Use Only
Sam
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21ii
Client Remarks/Comments
Sludge SamplesReport Dry Weight
Ice
CSeals
LahGomments
�y�Seals
N
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Date
Time
Received
by. {SIGNATURE)
Date rime
V
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Rel aq shed by. (SIGNATURE)
, J
thank% oolerTe ti
Date Time
Recelved : (SI NATURE)
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Data
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' Lr 0
0 Cl'' CrD
Waypointo
ANALYTICAL
9/24/2019
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 19-255-0023
Client Project Description: Winston- Salem, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.2440
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 9/12/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule August 2017) and NELAC unless otherwise indicated. Any
parameter for which the laboratory is not officially NELAP accredited is indicated by a '-'symbol. These are not
included in the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015 VAN ELAP #460181 Texas #T104704180 Arkansas #88-0650
Mississippi California #2904 NC 4415 Oklahoma #9311 SC #84002
Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST #90215 PA DEP 468.03195
.c_c.a.
Page 1 of 13
d
Way
PA A A
Client: EMA Resources Inc
Project: Winston- Salem, NC
Lab Report Number: 19-255-0023
Cate: 9/24/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.7-400 0 Fax 901.213.2440
www.waypointa nalytical.corn
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 92694 (Neilson WTP #1)
Analyte: Aluminum
QC Batch No: L454349IL453670
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: 1-454349/1-453670
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: 1-454188/1-453670
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92596 (Neilson WTP #3)
Analyte: Aluminum
QC Batch No: L4543231L453733
The matrix spike and/or the matrix spike duplicate was outside qualify control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Iron
QC Batch No: L454323IL453733
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Analyte: Potassium
QC Batch No: L4543231L453733
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L454101IL453733
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Phosphorus
QC Batch No: L454101/1-453733
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Page 2 of 13
WayPANAE.YTlCAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 fax 901.213.2440
www.waypointanalytical.com
Analyte: Sulfur
QC Batch No: L4541011L453733
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix Interference is suspected.
Sample 92697 (Neilson WTP #4)
Analyte: Aluminum
QC Batch No: 1-454323/1-453811
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Analyte: Iron
QC Batch No: 1-454323/1-453811
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix Interference is suspected.
Analyte: Potassium
QC Batch No: L454323/L453811
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Analyte: Manganese
QC Batch No: L454137/1-453811
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Analyte: Mercury
QC Batch No: 1-454339/1-454229
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges, A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 3 of 13
• =poina
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksvilie , NC 27028
Report Number :19-255-0023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901,213.2440
www.waypoin tana lytical.com
Project Winston- Salem, NC
Information :
REPORT OPANALWS
Report Date : 09/24/2019
Received : 09/ 1212019
0on`.6&sb- W-Q
Danyale Love
Project Manager
Matrix: Solids
Lab No: 92694
Sampled: 9111/2019 9:00
Sample ID : Neilson WTP *1
Test
Results
Units
MDL
MQL
DF Date 1 Time
Analyzed
By
Analytical
Method
76.6
%
0.010
1 09/16/19 16:43
ADM
SW-DRYWT
°k Moisture
1290
mg/Kg - dry
107
1 09/23/19 15:00
JPJ
4500NH3C-2011
Ammonia Nitrogen
<21.4
mgJKg - dry
21.4
21.4
1 09/23/19 14:16
ZBD
4500NO3F-2011
Nitrate+Nitrite-N
mg/Kg - dry
214
1 09/23/19 15:00
CALCULATION -
Organic N
2680
6.1
S.U.
1 09/23/19 07:03
JSL
9045D
pH
23.4
%
0.010
0.010
1 09/16/19 16:43
ADM
254OG-2011
Total Solids
mg/Kg - dry
214
1 09/24/19 14:40
CLP 4500NORGD-2011
Total Kjeldahl Nitrogen
3970
Phosphorus
2300
mg/Kg - dry
11.0
21.4
1 09/13/19 22:08
JTR
6010D
Aluminum
104000
mg/Kg - dry
86.8
214
10 09/17/1914:20
BKN
6010D
8.25
mg/Kg - dry
1.79
2.14
1 09/13/19 22:08
JTR
6010D
Arsenic
<0.212
mg/Kg - dry
0.212
0.427
1 09/13/19 22:08
JTR
6010D
Cadmium
974
mg/Kg - dry
71.8
107
1 09/13/19 27:08
JTR
6010D
Calcium
44.0
mg/Kg - dry
0.811
1.07
1 09/13/19 22:08
ITR
6010D
Chromium
45.3
mg/Kg - dry
0.620
1.07
1 09/13/19 22:08
JTR
6010D
Copper
45300
mg/Kg - dry
181
214
10 09/17/19 14:20
BKN
6010D
Iron
24.9
mg/Kg - dry
0.636
1.28
1 09/13/19 22:08
JTR
6010D
Lead
2260
mg/Kg - dry
9.49
21.4
1 09/13/19 22:08
JTR
6010D
Magnesium
551
mg/Kg - dry
0.782
2.14
1 09/13/19 22:08
JTR
60101)
Manganese
0.0739
mg/Kg - dry
0.0150
0.0679
1 09/17/19 14:07
TJS
7471A
Mercury
1.50
mg/Kg - dry
0.555
1.07
1 09/13/19 22:08
JTR
6010D
Molybdenum
22.0
mg/Kg - dry
0.705
1.07
1 09/13/19 22:08
JTR
6010D
Nickel
1920
mg/Kg - dry
12.7
21.4
1 09/13/19 22:08
JTR
6010D
Potassium
<2.09
mg/Kg - dry
2.09
2.14
1 09/13/19 22:08
JTR
6010D
Selenium
J
Estimated value
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions L
Limit Exceeded
Page 4 of 13
l
2790 Whitten Road, Memphis, TN 38133
point,
901.213.24.00 °
Fax 901.213.2440
.VIMain
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins
Project
Winston-
Salem, NC
Report Date : 09/24/2019
755 Yadkinville Rd
Information :
Received : 09/12/2019
Mocksville , NC 27028Danya
a Love
Report Number: 19-255-0023
REPORT OPANALYSi'S
Proect Manager
Project
Lab No: 92694
Matrix: Solids
Sample ID : Neilson WTP #1
Sampled: 9/11/2019 9:00
Test
Results
Units
MDL
MOL DF
Date ITime By Analytical
Analyzed Method
Sodium
79.53
mg/Kg - dry
33.0
107 1
09/13/19 22:08 JTR 6010D
Zinc
123
mg/Kg - dry
4.62
5.34 1
09/13/19 22:08 JTR 6010D
Sulfur
2220
mg/Kg - dry
20.9
21.4 1
09/13/19 22:08 IT'R 6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00 1
09/13/19 22:08 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
Estimated value
MQL Method Quandtation Limit
Page 5 of 13
�r
b
Waypoint.
ANALYTICAL
46245
CMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :19-255-0023
Lab No: 92695
Sample ID : Neilson WTP #2
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901,213.2440
www.wayp ointanalytical. corn
Project Winston- Salem, NC
Information :
Results
REPORT OFANAL YSIS
Units
Report Date : 09/24/2019
Received : 09/12/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 9:15
MDL MOL DF Date ITime By
Analyzed
Analytical
Method
76.8
%
0.010
1 09/16/19 16:59
ADM
SW-DRYWT
0/6 Moisture
741
rng/Kg - dry
108
1 09/23/19 15,00
JPJ
4500NH3C-2011
Ammonia Nitrogen
<21,6
mg/Kg - dry
21.6
21.6
1 09/23/19 14:17
ZBD
4500NO3F-2011
Nitrate+Nitrite-N
mg/Kg - dry
216
1 09123/19 15:00
CALCULATION -
Organic N
845
1 09/23/19 07:03
JSL
9045D
PH H
5.9
SM.
23.2
%
0.010
0.010
1 09/16/19 16:59
ADM
2540G-2011
Total Solids
mg/Kg - dry
216
1 09/24/19 14:41
CLP 4500NORGD-2011
Total Kjeldahl Nitrogen
1590
mg/Kg - dry
11.1
21.6
1 09/13/19 18:55
JTR
6010D
Phosphorus
2470
109000
mg/Kg - dry
43.5
108
5 09/16/19 19:02
BKN
6010D
Aluminum
6.51
mg/Kg - dry
1.81
2.16
1 09/1311918:55
JTR
6010D
Arsenic
0.3441
mg/Kg - dry
0.213
0.431
1 09/13/19 18:55
JTR
6010D
Cadmium
1030
mg/Kg - dry
72.4
108
1 09/13/19 18:55
JTR
6010D
Calcium
49.1
mg/Kg - dry
0,818
1.08
1 09/13/19 18:55
JTR
6010D
Chromium
46.6
mg/Kg - dry
0,625
1.08
1 09/13/19 18:55
JTR
6010D
Copper
50000
mg/Kg - dry
91.4
108
5 09/16/19 19:02
BKN
6010D
Iron
28.0
mg/Kg - dry
0.642
1.29
1 09/13/19 18:55
JTR
6010D
Lead
2450
mg/Kg - dry
9.57
21.6
1 09/13/19 18:55
JTR
6010D
Magnesium
582
mg/Kg - dry
0.788
2.16
1 09/13/19 18:55
JTR
6010D
Manganese
0.0780
mg/Kg - dry
0.0140
0.0634
1 09/17/19 14:18
TJS
7471A
Mercury
0.7713
mg/Kg - dry
0.560
1.08
1 09/13/19 18:55
JTR
6010D
Molybdenum
22.1
mg/Kg - dry
0.711
1.08
1 09/13/19 18:55
JTR
6010D
Nickel
2130
mg/Kg - dry
64.2
108
5 09/16/19 19:02
BKN
6010D
Potassium
<2.11
mg/Kg - dry
2.11
2.16
1 09/13/19 18:55
JTR
6010D
Selenium
J
Estimated value
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions L
Limit Exceeded
Page 6 of 13
a
Waypoint
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 'Fax 901.213.2440
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins
Project
Winston- Salem, NC Report Date : 09/24/2019
755 Yadidnville Rd
information :
Received : 09/12/2019
Mocksville , NC 27028
Danyale Love
Report Number :19-255-0023
REPORTOFANALYSIS
Project Manager
Lab No ; 92695
Matrix; Solids
Sample ID: Neilson WTP #2
Sampled: 9/11/2019 9:15
Test
Results
Units
MDL MQL DF Date ITime By Analytical
Analyzed Method
Sodium
1023
mg/Kg - dry
33.3 108 1 09/13/19 18:55 JTR 6010D
Zinc
130
mg/Kg - dry
4.66 5.39 1 09/13/19 18:55 JTR 6010D
Sulfur
2420
mg/Kg - dry
21A 21.6 1 09/13/19 18:55 JTR 6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00 1 09/13/19 18:55 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 7 of 13
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number :l9-255-0023
Lab No: 92696
Sample ID : Neilson WTP #3
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901.213.2440
vvww.way poin to nal yticat.com
Project Winston- Salem, NC
Information :
REPORT OFANAL YSIS
Report Date : 09/24/2019
Received : 09/12/2019
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 9:30
Results Units MDL MQL DF Date I Time By Analytical
Analyzed Method
0/0
0.010
1 09/1611916:59
ADM
SW-DRYWT
0/6 Moisture
71.6
mg/Kg - dry
88.0
1 09/23/19 15:00
JPJ 4500NH3C-2011
Ammonia Nitrogen
683
mg/Kg - dry
17.6
17.6
1 09/23/19 14:18
ZBD 4500NO3F-2011
Nitrate+Nitrite-N
<17.6
mg/Kg - dry
176
1 09/23/19 15:00
CALCULATION -
Organic N
489
1 09/23/19 07:03
JSL
9045D
PH
5.6
S.U.
%
0,010
0.010
1 09/16/19 16:59
ADM
2540E-2011
Total Solids
28.4
mg/Kg - dry
176
1 09/24/19 14:42
CLP 4500NORGD-2011
Total Kjeidahl Nitrogen
1170
mg/Kg - dry
9.05
0.6
1 09/13/19 19:01
JTR
60100
Phosphorus
2510
107000
mg/Kg - dry
35.6
88.0
5 09/16/19 19:07
BKN
6010D
Aluminum
5.39
mg/Kg - dry
1.48
1.76
1 09/13/19 19:01
JTR
6010D
Arsenic
0.359
mg/Kg - dry
0.174
0.352
1 09/13/19 19:01
JTR
6010D
Cadmium
$38
mg/Kg - dry
59.2
88.0
1 09/13/19 19:01
JTR
6010D
Calcium
43.0
mg/Kg - dry
0,669
0.880
1 09/13/19 19:01
JTR
60101)
Chromium
4M8
mg/Kg - dry
0.511
0.880
1 09/13/19 19:01
JTR
6010D
Copper
44000
mg/Kg - dry
74.6
88.0
5 09/16/19 19:07
BKN
6010D
Iron
25.3
mg/Kg - dry
0,524
1.06
1 09/13/19 19:01
JTR
6010D
Lead
2140
mg/Kg - dry
7.82
17.6
1 09/13/19 19:01
JTR
6010D
Magnesium
521
mg/Kg - dry
O.644
1.76
1 09/13/19 19:01
JTR
6010D
Manganese
0.0856
mg/Kg - dry
0.0119
0.0539
1 09/17/19 14:22
TJS
7471A
Mercury
0.6023
mg/Kg - dry
0.457
0.880
1 09/13/19 19:01
JTR
6010D
Molybdenum
19.4
mg/Kg - dry
0.580
0.880
1 09/13/19 19:01
JTR
6010D
Nickel
1680
mg/Kg - dry
52.5
Salo
5 09/16/19 19:07
BKN
6010D
Potassium
<1.73
mg/Kg-dry
1.73
1.76
1 09/13/19 19:01
JTR
6010D
Selenium
3
Estimated value
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions L
Limit Exceeded
Page 8 of 13
waypoint."'."-
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadldnville Rd
Mocksville , NC 27028
Report Number : 19-255-0023
Lab No ; 92696
Sample ID : Neilson WTP #3
Test
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax 901,213.2440
www.waypoln tanalytical.com
Project Winston- Salem, NC
Information :
REPORT OF'ANALYSIS
Results Units MDL
Report Date : 09/24/2019
Received : 09/12/2019
Qc"'6& WD-
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/1112O19 9:30
MQL DF Date I Time By Analytical
Analyzed Method
Sodium
60.93
mg/Kg - dry 27.2
88.0
1 09/13/19 19:01 JTR
6010D
Zinc
115
mg/Kg - dry 3.80
4.40
1 09/13/19 19:01 JTR
6010D
Sulfur
2450
mg/Kg - dry 17.2
17.6
1 09/13/19 19:01 JTR
6010D
Sodium Absorption Ratio
<5.00
Ratio
5.00
1 09/13/19 19:01
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 9 of 13
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Report Number:19-255-0023
Lab No: 92697
Sample ID; Neilson WTP #4
Test
2790 Whitten Road, Memphis, TN 38133
Main 901,213.2400 0 Fax 901.213.2440
www.way pain to nalyticaLcom
Project Winston- Salem, NC
Information :
REPORrOPANALYSIS
Report Date : 09/24/2019
Received
,_,(�:09/ 12/2019
Q0 6&� w-,D-
Danyale Love
Project Manager
Matrix: Solids
Sampled: 9/11/2019 9,45
Results Units MDL MQL DF Date ITime By Analytical
Analyzed Method
Moisture
79.2
0/0
0.010
1
09/26/1916:59
ADM
SW-DRYvrr
Ammonia Nitrogen
480
mg/Kg - dry
120
1
09/23/19 15:00
3P3
4500NH3C-2011
Nitrate+Nitrite-N
<21.1
mg/Kg - dry
21.1
21.1
1
09/23/19 14:18
ZBD
4500NO3F-2011
Organic N
673
mg/Kg - dry
240
1
09/23/19 15:00
CALCULATION -
pH
6.2
s.u.
1
09/23/19 07:03
JSL
9045D
Total Solids
20.8
%
0.010
0.010
1
09/16/19 16:59
ADM
2540G-2011
Total Kjeldahl Nitrogen
1150
mg/Kg - dry
240
1
09/24/19 14:43
CLP 4500NORGD-2011
Phosphorus
2500
mg/Kg - dry
12.4
24.0
1
09/13/19 17:35
JTR
6010D
Aluminum
112000
mg/Kg - dry
97.6
240
10
09/16/19 18:13
BKN
6010D
Arsenic
6.54
mg/Kg - dry
2.01
2.40
1
09/13/19 17:35
JTR
6010D
Cadmium
0.3533
mg/Kg - dry
0.238
0.481
1
09/13/19 17:35
JTR
6010D
Calcium
1080
mg/Kg - dry
80.8
120
1
09/13/19 17:35
3TR
6010D
Chromium
48.1
mg/Kg - dry
0.913
1.20
1
09/13/19 17:35
JTR
6010D
Copper
44.9
mg/Kg - dry
0.697
1.20
1
09/13/19 17:35
JTR
6010D
Iron
48600
mg/Kg - dry
204
240
10
09/16/19 18:13
BKN
6010D
Lead
27.1
mg/Kg - dry
0.716
1.44
1
09/13/19 17:35
JTR
6010D
Magnesium
2440
m9/Kg - dry
10.7
24.0
1
09/13/19 17:35
JTR
6010D
Manganese
625
mg/Kg - dry
0.879
2.40
1
09/13/19 17:35
JTR
6010D
Mercury
0,0846
mg/Kg - dry
0.0151
0.0688
1
09/17/19 14:23
TIS
7471A
Molybdenum
<0.625
mg/Kg - dry
0.625
1.2D
1
09/13/19 17:35
JTR
6010D
Nickel
22.5
mg/Kg - dry
0.793
1.20
1
09/13/19 17:35
JTR
6010D
Potassium
2150
mg/Kg - dry
143
240
10
09/16/19 18:13
BKN
6010D
Selenium
<2.36
mg/Kg - dry
2.36
2.40
1
09/13/19 17:35
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions L
Limit Exceeded
MQL
Method Quantitation Limit
Page 10 of 13
C
Wavpoint2790
Whitten Road, Memphis, TN 32133
AF
Main 901.213.2400 ° Fax 901.213.2440
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Mr. Brent Collins
Project Winston- Salem, NC
Report Date ; 09/24/2019
755 Yadkinville Rd
Information :
Received : 09/12/2019
Mocksville , NC 27028
Report Number :19-Z55-OD23
REPORTOFANALY5t5
Danyale LoveProject
Manager
Lab No: 92697
Matrix: Solids
Sample ID : Neilson WTP 44
Sampled: 9/11/2019 9:45
Test
Results units
MDL
MQL DF Date ITime By Analytical
Analyzed Method
Sodium
1017 m9/Kg - dry
37.1
120 1 09/13/19 17:35 TFR 6010D
Zinc
137 mg/Kg - dry
5.19
6.01 1 09/13/19 17:35 7TR 6010D
Sulfur
2450 mg/Kg - dry
23.5
24.0 1 09/13/19 1735 ]TR 6010D
Sodium Absorption Ratio
<5.00 Ratio
5.00 1 09/13/19 17:35 CALCULA71ON
Qualifiers/ DF Dilution Factor
Definitions L Limit Exceeded
J Estimated value
MQL Method Quantitation Limit
Page 11 of 13
nt+Ir" r ::
ANALYTICAL
Customer Number: 46245
Customer Name: EMA Resources inc
Report Number: 19-255-0023
• Fed Ex Q US Postal
Q UPS Q Client
2790 Whitten Road, Memphis, TN 38133
Main 901.2112400 0 Fax 901.213.2440
www.waypointa nalyticai.co m
Cooler Receipt Form
Shipping Method
Q Lab Q Other. r—�---�
Q Courier Thermometer ID: l 4't 5
Shipping container/cooler nuncompromised?-;
NI.—iharof rnlers received 1 '
Yes Q No
Custody seals intact on shipping container/cooler?
Q Yes
(�} No
Q No
�
Not rcegwrea®Not Required
Custody seals intact on sample bottles?
Q Yes
Chain of Custody (COC) present?
0 Yes
Q No
COC agrees with sample label(s)?
0 Yes
Q No
COC properly completed
0Yes
QNo
Samples in proper containers?
® Yes
No
Sample containers Intact?
0 Yes
Q No.
Sufficient sample volume for indicated test(s)?
Yes
Q No
_
All samples received within holding time?
Yes
Q No
Cooler temperature in compliance?
® Yes
Q No
Cooler/Samples arrived at the laboratory on ice.
i Yes
Q No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
Q Yes
Q No
4& N/A
Water -VOA vials free of headspace
Q Yes
Q No
Q Na
� N/A
� -
NIA
Trip Blanks received with VOAs
Q Yes
Soil VOA method 5035 — compliance criteria met
Q Yes
Q No
i N/A
r— High concentration container (48 hr)
[— Low concentration EnCore samplers (48 hr)
F— High concentration pre -weighed (methanol -14
d) F— Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Q Yes
No —
f
Comments:
Signature: arleen Qualls
Date &Time: L12/2019 08:36:46
Page 12 of 13
ClientName/Address
Client Project Manager/Contact
Billing Information
For Laboratory Use Only
EMA Resources Inc
Brent Collins
Account #46245
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project/Site Location (city/State]
RUSH - Additional charges apply
Special Detection Limit(s)
Me of Shipment Matrix Key
�
���57a,,1-�FlrtA?L/A
OateResultsNeeded
PQUSPS WW - Wastewater GW - Groundwater
❑ Fed Ex HUCI(esnt
CourieroropCS DW-Drinking Water S-Sail/Solid O-Oil
/C,
P- Product M - Misc
I V
Other
Project Number
Project Manager Phone IJ
Project Manager Email
Purchase Order Number Site/Facility iD P
336-399-3646
brent_coilins@emaresources.Gom
C
^ to z f )
;: O C U
A Cool s 10C NRM03 (Mi. Only)
e Codc-6C
WalpoinIk.
ANALYTICAL
c
e w
r O c
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�
u [ xo4 pxa
O Nenexegeired
E NaO3
279a Whimn (load
$ °
° a
f0 W
V J PHa10
Memphis, TN 3sw
Unless noted, all contalners
o t0 � w M
T G xCLp
(901) 213-2400
per Table fl of 40 CPR Part
136.
s5 (D Y ;E Q
L°
�"'
+ � x H3PG4 p<g
CL
•
s m
z
Z
1 Cool a 6C MUS203
Date I Time Sam IeIdentification
R
tilted nalyais/ PfeserwatIve
Comments/Notes
JA) j
Metals:AI,AS,Ca,Cd,Cr,Cu,Fe,Pb
I(t 1ST G LSa
#,
a
Gr
Mn,M9,M0,H9,Ni,Se,Na,P,S,K,Zn
W:3,,
�v�z� 0"
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F�L
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W
4.11
1f��CIfClIlIIiCII�I�CCIIIIC�(IIIIIiC<� �;� 193
EmA Resources Inc
08.35:46
Winston- Salem. NC
For Laboratory
Use
Only
Sampled by
(Name - Print)
Client Remarks/Comments
Ice
C�lsy
Lab Comments
C
i Y `ki7�?JJ
`�
Sludge Samples - Report Dry Weight
Y N
y
Sell she b (E A( RE
Da a Time�/
Received by: (SIGNATURE)
Date Time
/ !'
k
oe err P
Refinquished by (SIGNATURE]
a Time
Received by: (SIGNATURE)
Date Time
%� ,
^{Sian`
i /
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Relinquished by. (SIGNATURE)
Date Time
a : (SIGNATU
Date Time
,�
errs+„ream
ESEARC NA TiCAI �4`aaawuy� -
Ubo Tor$6Esr INC. €� 0 NOW of _
Anclytical/Process Consultations
March 24, 2016
i City of Winston-Salem Neilson WTP
5725 l?rye Bridge Road
CIemmons, NC 27012
Attention: Rodney Darr
Chemical Analysis for Selected Parameters and Sampling Locations Identified as Neilson WTP
j (A City of Winston-Salem Neilson WTP Project, collected 01 March 2016)
i
1. Miscellaneous 1 2 3 4 5 6 7
Parameters unit Results Results Results Results Results Results Results
Fecal Coliform NTN/g`I`S 4 <2 <2 <2 <2 <2
Sample Number:
I5606-61
15606-02
15606-03
15606-04
15606-05
I5606-06
I5606-07
SampleCollededDate:
0.3/01116
03/01/16
03/01/16
03/01/16
03/01/16
03/01/16
03101/16
Sample Collected Time:
0730
0732
0735
0740
0744
0746
07$0
MPNIg TS = Most Probable Numberper gram Total Solids
uxx....avawnm�.u�r+ ...,.� �....... � ���;�.�ar;��smn�r+x+ .. •�, .. ... a��-w�v�a+nmwx�a,mienor+.ca�u�e...�.xaamwmyanw. . ro.awr..,.wane.rR.�vm«�w�.r..wawww,..�......
North Carolina
nIA/D C44Quality
Mar r r lML NCDEd?bWW' of Wat r Resources
Division of Water Resources RURCE CE TIFICATION
j� FOR FO M: RSC 06-16
Please use the following instructions as a checklist in order to ensure ill require�I em�a�Afited. Ad rence to these
instructions and checking the provided boxes will help produce a quieter revi&81Mkt#nVJJBJte amou t of additional
information requested. Failure to submit all of the required items will lead o a i Bona w time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Res uals Source Certification (FORM: RSC 11-15):
Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application
may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
or new or renewed permits, submit a separate certification for each source facility.
[C[]� or modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
omplete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Res'duals Source -Generating Facility Information:
[?For each source facility, attach the following:
[Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
,Residuals Land Application Permits
Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
e to be generated, treated, processed, and stored at the facility.
We
justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
_41rocessing.
Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Rgoilluals Quality Information:
Fo each source facility, attach the following:
[Tf aboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
action reduction requirements.
For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16
Page 1 of 1
RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Winston-Salem/Fors\ th County Utilities Commission (R.A. Thomas Water Treatment Plant i.
Status
Code
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
R
Swann WTP
Swann WTP
Forsyth
WQ0031314
750
750
R
Swann WTP
Neilson WTP
Forsyth
WQ0031314
2,500
1,499
R
Swann WTP
Thomas WTP
Forsyth
WQ0031314
750
750
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1
DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: R.A. Thomas Water Treatment Plant
2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Bill Brewer — Water Treatment Su erintendent
Complete mailing address: 2800 River Ridge Road
City: Pfafftown State: NC Zip: 27040-8435
Telephone number: 336) 945-1179 E-mail address: billb@cityofws.org
4. Facility physical address: ,1201 S. Martin Luther King, Jr. Drive
City: Winston-Salem State: NC Zip: 27107-8435
Coordinates: Latitude: N36° 5' 11.7" Longitude: W80° 13' 8"
Datum: DMS Level of accuracy: 100%
Method of measurement: Survey
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
Z treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: �^ % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 18.0 MGD and facility average daily flow: 5_7 MGD
8. Average amount of residuals being generated at this facility 750 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: The treatment facilities for wash water consists of one (1) equalization basin with
a capacity of 0.545 MG's and one (U circular clarifier with a maximum daily hydraulic loading rate of 0.36 & m/sf. In
addition. the Thomas Plant has a residuals pumps station for pumping thickened solids to one of two (2) residuals lagoons
for settling and drying of solids. Each lagoon has an effective storage volume of 2.1 MG's each.
Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or Z. 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6] as:
Biological E Non -Biological
FORM: RSC 06-16 Page 1 of 5
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Research & Analytical Laboratories. Inc. and Date of analysis: 4/26/2016
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: 212 °F (> 140°F)
Passed reactivity test: ®yes ❑no. HCN: <250 mg/kg (<250) & H2S: <500 mg/kg (<500)
TCLP Parameter
Limit
(mglo
Result TCLP Parameter
(mgfl)
Limit
(mg/V
Result
(mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
0.454
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
N D
Lindane
0.4
ND
Chlordane
0.03
N D
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1, 1 -Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land jM ication: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Research & Analytical Laboratories. Inc. and Date of analysis: 8/30/2017
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
3.51
<0.278
33.6
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead
840
300
13.1
Mercury
57
17
0.124
<2.78
Molybdenum
75
420
100
n/a
Nickel
420
18.9
Selenium
100
<2.78
Zinc
7,500
2,800
173
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Research & Analytical Laboratories, Inc. and Date of analysis: 8/30/2017
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
® > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
3.51
ND
18.9
FORM: RSC 06-16 Page 3 of 5
5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Research & Analytical Laboratories. Inc. and Date of analysis: 8/30/2017
Parameter
Result
(mg/kg)
Aluminum
109,000
Ammonia -Nitrogen
1,380
Calcium
4,100
Magnesium
1,660
Nitrate -Nitrite Nitrogen
26.1
pH (Standard Unit)
6.54
Phosphorus
1,260
Potassium
1,510
Sodium
239
Total Kjeldahl Nitrogen
7,170
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR):
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40% or 0.40
%. This rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: Accepted formula for water
plant residuals.
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (13t) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
3,010
3,913
Injection/Incorporation
N/A
N/A
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A -Water plant residuals
FORM: RSC 06-16 Page 4 of 5
7. PathoQen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of 'Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative 1 [15A NCAC 02T. 1 106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (1'AR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T. 1 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T. 1 107(a)(6)] -Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5
R.A. Thomas Water Treatment Plant
Water System Facility ID = TP1
Production Capacity = 18.0 MGD
City of Winston-Salem
NPDES ID# = NCO079821
Potassium
Permanganate
1
Salem Lake —1.0 Billion �
Gallon Raw Water Reservoir
Alum
Caustic
Chlorine
Chlorine
Filter Aid Polymer
Chlorine
Fluoride
Ortho-Phosphate
Caustic
Entry Point-EP1
10.0 MGD
i--*[— Common Header •
a
v►
■
•
Coagulatior.
9
Flocculation
Residuals
Sedimentation Basins
■j
r
Yadkin River via Neilson
WTP Raw Water Reserviors
(2) 1.76 MG Residuals Lagoons
■
Residuals Pump Station
(3) 200 GPM Pumps
r
m
au
Polymer
Filtration
Backwash and Washwater
- Filter to Waste
■ EQ Basin
OP 0.55 MG
Ok
(4) - 1.12 MGD Pump= _
r— - Max Flow = 4.5 MGD —�
1.5 MG Clearwell
1.5 MG Clearwell
Distribution
System
24.0 MGD
r
Washwater +
Clarifier
4.5 MGD
Discharge Outfall 001
I?t4 -/-A WI-1
BLACK & VEATCH INTERNATIONAL COMPANY
,SGe' ILit, 1 - 69
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
Control: The pumps will be controlled manually from the plant control
system or locally at the finished water pumping station. A low
level sensor will be provided in each finished water storage
reservoir to stop the pumps on low water level. Pump status and
alarm conditions, pump discharge valve position, and finished
water storage reservoir levels will be indicated locally and
transmitted to the plant control system.
3. Flow Measurement.
Type Magnetic
Number of meters 1
Size, each, inches 24
Flow measurement range, mgd 4-26
Control: Flow signal will be transmitted to the plant control system and
local indication will be provided in the pumping station.
G. WASH WATER AND RESIDUALS HANDLING
1. Wash Water and Residuals Handling.
Currently, a common drainage system exists for sedimentation basin
overflow, for basin drainage and residuals drawdown, for filter backwash
and filter -to -waste drainage, and for storm water. These flow streams drain
to the wash water and residuals pumping station where they are pumped to
one of two residuals storage lagoons. This practice will be abandoned and
the clear water and residuals flow streams will be separated and treated.
Spent wash water and filter -to -waste will discharge by gravity to a new wash
water equalization basin. The collected water will be pumped from the
equalization basin to a new wash water clarifier. Wash water clarifier
effluent will discharge to the creek in accordance with the NPDES permit.
The wash water drainage system upstream of the equalization basin will be
designed to allow all four filters to be simultaneously wasted at the design
filtration rate prior to the addition of ozone, and three filters to be wasted at
I-18
BLACK & VEATCH INTERNATIONAL COMPANY
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
the design filtration rate after the addition of ozone (filter hydraulic grade
line is reduced). This drainage capacity assumes a maximum headloss of 5
feet through a filter's media and underdrain during the wasting period. This
drainage capacity is provided for an emergency condition when water
quality dictates the basins be wasted until necessary treatment adjustments
are made. Because this is an emergency condition and not part of the normal
plant operation, flows in excess of the equalization basin pumping capacity
will overflow to the plant overflow drain.
Unthickened residuals from the sedimentation basins will discharge by
gravity through the viewing pit to the residuals pumping station. Residuals
from the wash water clarifier will also discharge by gravity to the residuals
pumping station. The combined residuals will be pumped to the residuals
storage lagoons. Decant/overflow from the residuals storage lagoons will
flow by gravity back to the wash water equalization basin.
2. Wash Water and Residuals Flows and Solids Production.
Filter Backwash Water
Initial
Per filter"', gal
179,775
Avg (2), gpd
359,550
Max(3), gpd
719,100
Filter -to -Waste
Per filter"), gal 63,920
in
Avg (2)(4), gpd 127,840
Max(3)(4), gpd 255,680
Total Residuals Production
Avg('), lb/day 2,290
Max('), lb/day 4,122
Unthickened Residuals Flow to La ,00ns
Avg(S)(7) gpd W 137,290
Max(6)(7), gpd 247,122
I- l 9
BLACK & VEATCH INTERNATIONAL COMPANY
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
Thickened Residuals Production
Avg (5)(8), gpd
5,492
Max (6)(8), gpd
9,885
Free Liquid from Residuals(9)
Avg, gpd
131,798
Max, gpd
237,237
Effluent
_Clarifier
Avg( 10), mgd
1.13
Max (11), mgd
2.25
(1) Flow rate of 22.5 gpm/sf for 10 minutes.
(2) Half of the filters backwashed in one day.
(3) All filters backwashed in one day.
(4) Flow rate of 4 gpm/sf for 20 minutes.
(5) Two hundred twenty-nine pounds per million gallons, using average
flow rate of 10 mgd.
(6) Two hundred twenty-nine pounds per million gallons, using design flow
rate of 18 mgd.
(7) 0.2 percent solids.
(8) 5.0 percent solids.
(9) Unthickened residuals flow minus thickened residuals flow.
(10) Pumped flowrate from wash water equalization basin to wash water
clarifier under average daily conditions of two filter washes per day.
(11) Pumped flowrate from wash water equalization basin to wash water
clarifier under maximum daily conditions of four filter washes per day.
3. Wash Water E ualization Basin.
A wash water equalization basin will be provided for flow equalization of
wash water prior to treatment in the wash water clarifier. Depending on the
daily flow to the equalization basin, as few as one or up to four pumps will
be required to pump the contents of the basin to the wash water clarifier.
Under average daily conditions of two filter wash cycles per day, one pump
is required with three standby pumps available. Under maximum daily
conditions of four filter wash cycles per day, two pumps are required with
two standby pumps available. In the event of a sedimentation basin drain,
all four pumps are required with no standby pump available.
I-20
BLACK & VEATCH INTERNATIONAL COMPANY
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
Submersible mixers will not be provided. Operations staff will be required
to wash down settled solids on an as needed basis.
Number of basins
Design criteria, each
Volume, each, gal
Basin type
Basin shape
Dimensions, ft
Inside diameter, ft
Average sidewall water depth, ft
Average sidewall depth, ft
Bottom slope to sump
Water depth at top of sump, ft
Pumps
Number of pumps
Rated capacity, each, gpm
Rated head, ft
Operating head range, ft
Motor brake horsepower, bhp
Storage volume of two filter
wash cycles plus 10 percent
545,000
Reinforced concrete
Circular
75
16.5
18.5
1:75
17.0
4
780
18
12-33
10
Controls: Level sensors will be provided in the equalization basin for level
monitoring and control of the wash water equalization pumps
and mixers. Basin level will be transmitted to the plant control
system. At basin overflow level, an overflow alarm will be
transmitted to the plant control system.
The wash water equalization basin pumps will be automatically
alternated and started and stopped based on level in the wash
water equalization basin. Provisions will be made to start/stop
the pumps locally and from the plant control system. Pump
I-21
BLACK & VEATCH INTERNATIONAL COMPANY
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
status and alarm conditions will be indicated locally and
transmitted to the plant control system.
4. Wash Water Clarifier.
Number
I
Basin Type
Reinforced Concrete
Basin Dimensions
Inside wall diameter, ft
75
Inside weir diameter, ft
68.67
Sidewall water depth, ft
12
Total sidewall depth, ft
14
Water depth at center pier, ft
15.1
Floor radial slope to center
1:12
Hydraulic loading rate, gpm/sf
Average daily
0.18
Max daily
0.36
Sedimentation Basin Drain
0.72
Detention time, hr
Average daily
8.5
Minimum daily
4.2
Sedimentation Basin Drain
2.1
Weir type
Perimeter; sharp crested,
V-notch
Weir loading rate, gpm/ft
Average 3.62
Maximum daily 7.24
Sedimentation Basin Drain 14.48
Control: Clarifier drive status and alarm conditions will be indicated
locally and transmitted to the plant control system.
The clarifier residual drain valve will be opened and closed
automatically either (1) based on an operator selectable cycle
I-22
BLACK & VEATCH INTERNATIONAL COMPANY
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
time set point for number of hours of plant operation or (2) a
total accumulated wash water clarifier flow volume between
blow -downs. The plant control system will open the valve for an
operator -entered duration and close the valve for the remainder
of the cycle. In Flow mode, the valve open duration will be the
same as the Time mode "open duration setpoint". The basis for
automatic control ("timed" or "flow"), the cycle time set point,
and the flow volume set point is entered at the plant control
system workstation computers. Provision will be made to open
and close the residuals drain valve locally and from the plant
control system.
5. Residuals Pum in•� Station.
The existing residuals pumping station will remain. The contents of the
station will be demolished and completely renovated. The following new
facilities will be provided:
• Residuals pumps and associated pump controls
• Piping and valves
• Plumbing
• HVAC
• Doors
• Handrail and guardrail
• Protective coatings
• Electrical
• Instrumentation and control system
Under maximum residuals drainage conditions from the sedimentation
basins and wash water clarifier, two pumps are required with one standby
pump available. In the event the wash water clarifier is taken offline for
maintenance, the wash water equalization basin flow will be drained into the
pumping station wetwell, and three pumps will be required with no standby
pumps available. During this wash water clarifier maintenance period, the
I-23
BLACK & VEATCH INTERNATIONAL COMPANY
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
equalization basin level must be limited to approximately half full to limit
the flow rate into the residuals pumping station wetwell.
Residuals Pumps
Type of pump
Horizontal end suction
centrifugal
Number of pumps 3
Rated capacity, each, gpm 200
Rated head, ft 46
Operating head range, ft 24-46
Motor brake horsepower, each, bhp 10
Controls: The residuals pumps will be automatically alternated and started
and stopped based on level in the residuals pumping station wet
well. Provisions will be made to start/stop the pumps locally
and from the plant control system. Pump status and alarm
conditions will be indicated locally and transmitted to the plant
control system.
6. Residuals Storage Lagoons.
The existing residuals storage lagoons will be expanded and modified to
receive all plant residuals for storage. The design criteria provided herein is
based upon a design thickened residual concentration of 5%.
Number of lagoons
Lagoon type
Dimensions, each, ft
Length
Width
Max residuals depth
Max water depth
Freeboard
I-24
2
Earthen lagoon with concrete slope
protection and underdrain
311
157
8
10
2
BLACK & VEATCH INTERNATIONAL COMPANY
CIVIL DESIGN MEMORANDUM
Winston-Salem/Forsyth County Utility Commission B&V Project 145730
Winston-Salem, North Carolina First Issue: December 15, 2006
R.A. Thomas Water Treatment Plant Improvements Latest Revision: April 12, 2007
Perimeter slope
Liquid volume, each, mg
Storage volume, each, mg
Effective storage, each lagoon,
days
Access Ramp
Width, ft
Slope, percent
Decant
Sludge removal method
Cleaning duration, years
H. OPERATIONS BUELDING
2:1
2.8
2.1
365
12
10
Discharge to wash water equalization
basin
Air drying, excavate with front-end
loader or clam bucket
1
The existing control building will be demolished and a new operations building will be
provided for administrative facilities, chemical feed and storage, and maintenance and
control facilities. Figures I-16 and 1-17 showing the floor plans for the basement and
operating floor and Figure I-18 showing the building elevations are attached.
The following facilities will be provided:
Basement Floor
Bulk Liquid Chemical Storage Room
Coagulant (Alum) Storage Area
Zinc Orthophosphate Storage Area
Future Storage Areas
Sodium Hypochlorite Storage Room
Fluoride Storage Room
Sodium Hydroxide Storage Room
General Storage Room
Electrical Room
I-25
R.A. Thomas Water Treatment Plant
Solids Handling Plan
The Thomas Water Treatment Plant is an 18.0 MGD water treatment facility. Solids are
generated by automatic sludge removal from sedimentation basins, backwashing filters, and
filter -to -waste after filter backwashes are completed. Solids produced from filter backwashes
and filter -to -waste is routed to an equalization basin (0.545 MG), is treated with polymer, and
then pumped to a clarifier. Solids settled in the clarifier flow to the plants waste station and
are then pumped to one of two residuals lagoons (1.76 MG each) using one of three 0.288
MGD pumps. One lagoon is kept in service while the second is dried and cleaned. Clarified
water from the clarifier is discharged to an unnamed tributary of Salem Creek through the
permitted NPDES discharge NC0079821.
Permits and Classifications:
1. The discharge from the clarifier is authorized by NPDES Permit NC0079821. The
classification for the discharge is Grade 1 Physical/Chemical.
2. The distribution of the residuals removed from the lagoons is authorized by permit
WQ0031314. The residuals are classified as Class A.
Operation:
1. The system consists of a 0.545 MG equalization basin (EQ basin), (4) equalization basin
discharge pumps rated at 1.0 MGD each, a residuals clarifier rated at maximum weir
loading rate of 7.24 gpm/ft, a residuals pump station with (3) residuals pumps rated at
0.29 MGD each for transferring residuals to (2) residuals lagoons rated at 1.76 MG each.
2. Routine inspections of equipment will be conducted the Senior Utility Plant Supervisor to
ensure proper operation of equipment. Any equipment not functioning properly are
reported through the water division's asset management program, MAXIMO, to the
appropriate support group for repair/replacement.
3. Backwash and filter -to -waste water from the plant process flow by gravity to the EQ basin
and are pumped by the EQ basin pumps to the wash water clarifier.
4. 38% Sodium bisulfite is fed atone of two locations (influent or effluent to clarifier) for
dechlorination of effluent being sent out discharge NCO079821.
5. All sedimentation basin residuals and residuals from the wash water clarifier flow to the
residuals pump station and are then pumped directly to one of the two residuals lagoons.
R.A. Thomas Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
6. Clarified water from the washwater clarifier is discharged to an unnamed tributary of
Salem Creek through the permitted NPDES discharge NC0079821.
7. Residuals are dried then removed from the lagoons and hauled to the application site by a
private contractor.
Monitoring and Reporting Requirements:
1. Residuals generated by each source -generating facility must be analyzed to demonstrate
that they are non -hazardous based on the most current permit requirements (Attachment
A). Sampling will be conducted under supervision of the Senior Water Treatment Plant
Supervisor by WSFC Utilities current contractor as described below in compliance with
permit requirements.
2. Analysis will be performed by a NC Certified Laboratory.
3. Analyses made according to monitoring and reporting requirements must be certified for
the required parameter(s).
4. Corrosivity, ignitability, reactivity, and a Toxicity Characteristics Procedure analysis are
required once each permit cycle. The TCLP analysis includes the following parameters
(i.e., note the regulatory level in milligrams per liter in parentheses):
Arsenic (5.0)
Barium (100.0)
Benzene (0.5)
Cadmium (1.0)
Carbon tetrachloride (0.5)
Chlordane (0.03)
Chlorobenzene (100.0)
Chloroform (6.0)
Chromium (5.0)
m-Cresol (200.0)
o-Cresol (200.0)
p-Cresol (200.0)
Cresol (200.0)
2,4-D (10.0)
1,4-Dichlorobenzene (7.5)
1,2-Dichloroethane (0.5)
1, 1 -Dichloroethylene (0.7)
2,4-Dinintrotolulene (0.13)
Endrin (0.02)
Hexachlorobenzene (0. 13)
Heptachlor (and its hydroxide) (0.008)
Hexachloro-1,3-butadiene (0.5)
Hexachloroethane (3.0)
Lead (5.0)
Lindane(0.4)
Mercury (0.2)
Methoxychlor (10.0)
Methyl ethyl ketone (200.0)
Nitrobenzene (2.0)
Pentachlorophenol (100.0)
Pyridine (5.0)
Selenium (1.0)
Silver (5.0)
Tetrachloroethylene (0.7)
Toxaphene (0.5)
Trichloroethylene (0.5)
2,4,5-Trichlorophenol (400.0)
2,4,6-Trichlorophenol (2.0)
2,4,5-TP (Silvex) (1.0)
Vinyl chloride (0.2)
5. Analyses of the following parameters are also required with each application event:
Aluminum
Ammonia -Nitrogen
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Mercury
Molybdenum
Nickel
Nitrate -Nitrite Nitrogen
Phosphorous
Potassium
R.A. Thomas Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
pH
Plant Available Nitrogen
(by calculation)
Selenium
Sodium
% Total Solids
TKN
Zinc
FA
6. Data to verify pathogen reduction and vector attraction reduction of the residuals is
maintained on file for five years. The required data is specific to the stabilization process
utilized, and is also sufficient to demonstrate clear compliance with the Class A pathogen
requirements and restrictions noted in 15A NCAC 02T .1106 (a) and (b) and vector
attraction reduction requirements in 15A NCAC 02T .1107 (a).
7. Proper records are maintained tracking all residuals activities. These records include the
source, volume, analysis, and recipient of the residuals.
8. Three copies, per application event, of all required monitoring and reporting requirements
are submitted annually before March 1, to NC DEQ-DWQ.
Performance Standards:
1. The pollutant concentrations in any residuals that are land applied to any land application
site shall not exceed the following Ceiling and Monthly Average Concentrations (i.e.
dry weight basis):
Parameter
Monthly Average
Concentration
milli rams per kilogram)
Ceiling Concentration
(milligrams per kilogram)
Arsenic
41
75
Cadmium
39
85
Copper
1,500
4,300
Lead
300
840
Mercury
17
57
Molybdenum
n/a
75
Nickel
420
420
Selenium
100
100
Zinc
2,800
7,500
2. If residuals are sold or given away, one of the Class A pathogen requirements in 15A
NCAC 02T .I 106(b) must be met.
Application Requirements:
1. Bulk residuals are not applied under the following conditions:
i. If the residuals are likely to adversely affect a threatened or endangered species.
ii. If the application causes prolonged nuisance conditions.
iii. If the land fails to assimilate the bulk residuals or the application causes the
contravention of surface water or groundwater standards.
iv. If the land is flooded, frozen, or snow-covered or is otherwise in a condition such that
runoff of the residuals would occur.
R.A. Thomas Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
v. During a precipitation event or within 24 hours following a rainfall event of 0.5
inches or greater in a 24-hour period.
vi. For residuals treatment and storage facilities, the following minimum setbacks shall
be adhered to:
Description of Setback
Minimum Setback
feet
Habitable residence or place of public assembly under separate ownership or
not to be maintained as part of the project site
100
Property lines
50
Private or public water supply
100
Surface waters (streams, -intermittent and perennial, perennial water bodies,
and wetlands)
50
Wells with exception to monitoring wells
100
2. When land applying bulk residuals to application site, the following minimum setbacks
are maintained at all times:
Setback By Type of
Residual (feet)
Description of Setback
Liquid
Cake
Private or public water supply
100
100
Surface waters (streams -intermittent and perennial,
perennial water bodies, and wetlands)
100
25
Surface water diversions (ephemeral streams,
waterways, ditches)
25
0
Groundwater lowering ditches (where bottom of
The ditch intersects SHWT)
25
0
Subsurface groundwater lowering system
Wells with exception to monitoring wells
100
100
Bedrock outcrops
25
0
3. Specific bulk residuals land application area boundaries are clearly marked on each land
application site prior to and during a residuals land application event.
Spills and Noncompliance Notification:
1. The Winston-Salem Regional Office, telephone number (336) 771-5000 will be notified
within 24 hours or the next working day following the occurrence or first knowledge of
the occurrence of any of the following:
i. Any occurrence with the distribution program, which results in the land application of
significant amounts of wastes, which are abnormal in quantity or characteristic.
ii. Any failure of the distribution program resulting in a release of materials to receiving
waters.
iii. Any process unit failure, due to known or unknown reasons, that render the facility
incapable of adequate residual treatment.
R.A. Thomas Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
4
2. Persons reporting such occurrences by telephone shall also file a written report in letter
form within (5) days following first knowledge of the occurrence. This report must outline
the actions taken or proposed to be taken to ensure that the problem does not recur.
3. Emergency Contacts: Thomas Water Treatment Plant (336) 788-0152 (Main)
Donna Lankford, Plant Supervisor (336) 734-1577 (0)
(336) 655-9616 (M)
Bill Brewer (336) 397-7727 (0)
Water Treatment Superintendent (336) 745-5277 (M)
Winston-Salem/Forsyth County (336) 727-8418
Utility Administration
DEHNR Regional Office (336) 771-5000
General Emergency 911
HazMat
R.A. Thomas Water Treatment Plant
Solids Handling Plan -Permit #WQ031314
Revised 07/14/2020
R ESEARCh & ANAtyTiCAL
LAbORATORIESi INC.
Analyflcal/Process Consultaflons
August 17, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
NO
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
(A City of Winston-Salem Thomas WTP Project, collected 26 July 2017)
I. Miscellaneous
Thomas Lagoon #1
Parameters
Unit
Results
Aluminum, Total
mg/kg
86,400
Ammonia -Nitrogen (NH-3-N)
mg/kg
488
Arsenic,Total
mg/kg
3.48
Calcium, Total
mg/kg
744
Cadmium, Total
mg/kg
<0.325
Copper, Total
mg/kg
28.2
Lead, Total
mg/kg
8.41
Magnesium, Total
mg/kg
1,300
Mercury, Total
mg/kg
<0.105
Molybdenum, Total
rng/kg
<3.25
Nickel, Total
mg/kg
15.5
NO2+NO3
mg/kg
3.82
Phosphorus, Total
mg/kg
4,240
Potassium, Total
mg/kg
954
Selenium, Total
mg/kg
<3.25
Sodium, Total
mg/kg
209
Total Kjeldahl Nitrogen (TKN)
mg/kg
3,960
Total Solids
%
31.4
Zinc, Total
mg/kg
132
PH
Std. Units
6.31
Fecal Conform
mpn/g TS
<2
Sample Number: 37718-01
Sample Collected Date: 07/26/17
Sample Collected Time: 0845
mg/kg = milligrams per kilogram = parts per million
% = Percent Std. Units = Standard Units
RESEARCh . ANALY1FiCAt
LA ORATORiIES� INC.
Analyt€col/Process Consultations
August 17, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
(A Cites Winston-Salem Thomas WTP Project, collected 26 July 2017)
1. Miscellaneous
Parameters
PAN = [MRx(TKN-NH3-N)] + (0.5x(NH-3-N))+ (NO3+NO2) = 0.4x(3,960-488) + (0.5x(488)+3.82 =1,650 mg/kg
Sample Number:
Sample Collected Date:
Sample Collected Time:
37718-01
07/26/17
0845
PAN = Plant Available Nitrogen mg/kg = milligrams per kilogram = parts per million
LA�®RAToRIES� INC.
Analyticai/Process consultations
August 17, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
i�'�2wtJC /13q zi 3»,�
r '•.�,�,n�Fa�aNP�.,•
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
(A City of Winston-Salem Thomas WTP Project collected 26 July 2017)
I. Miscellaneous
Parameters
SAR = Na
Ca+ Ma
7_
9.09
F2337.2+108 = 1.07
Sample Number:
Sample Collected Date:
Sample Collected Time:
37718-01
07/26/17
0845
SAR = Sodium Absorption Rate maJkg = milligrams per kilogram = parts per million
RESEARCH & ANAtyTiCAt
UboiimoR[ESi INC.
Analytical/Process Consultations
September 21, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
A City of Winston-Salem Thomas WTP Pro.'ect, collected 30 August 2017
I. Miscellaneous
Thomas Lagoon #1
Thomas Lagoon #1
Thomas Lagoon #1
Sample A
Sample B
Sample C
Parameters
Unit
Results
Results
Results
Aluminum, Total
mg/kg
109,000
94,000
106,000
Ammonia -Nitrogen (NH-3-N)
mg/kg
772
1,380
735
Arsenic,Total
mg/kg
2.74
3.51
2.64
Calcium, Total
mg/kg
909
4,100
1,070
Cadmium, Total
mg/kg
<0.255
<0.278
<0.257
Copper, Total
mg/kg
25.9
33.6
29.0
Lead, Total
mg/kg
299
13.0
13.1
Magnesium, Total
n1cr CY
1,040
1,510
1,660
Mercury, Total
mg/kg
0.088
0.117
0.124
Molybdenum, Total
mg/kg
<2.55
<2.78
<2.57
Nickel, Total
mg/kg
10.9
18.9
13.8
NO2+1903
mg/kg
26.1
3.57
3.66
Phosphorus, Total
mg/kg
788
1,260
1,080
Potassium, Total
mg/kg
844
1,510
1,290
Selenium, Total
mg/kg
<2.55
<2,78
<2.57
Sodium, Total
mg/kg
138
214
239
Total Kjeldahl Nitrogen (TKN)
rng/kg
6,040
7,170
5,880
Total Solids
%
38.0
34.2
36.3
Zinc, Total
mg/kg
173
172
140
pH
Std. Units
6.54
6.62
6.54
Sample Number:
39349-01
39349-02
39349-03
Sample Collected Date:
08/30/17
08/30/17
08/30/17
Sample Collected Time:
0805
0805
0805
mg/kg = milligrams per kilogram =parts per million
%= Percent Std. Units = Standard Units
1[("11ESEARCh ANALYT'ICA1
LAb®RAT®RiESr INC.
Analytical/process Consultations
September 21, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
(A City of Winston-Salem Thomas WTP Project, collected 30 August 2017)
1. Miscellaneous
Para meters
PAN = [MRx(TKN-NH3-N)) + (0.5x(NH-3-N))+ (NO3+NO2) = 0.4x(6,040-772) + (O.Sx(772)+26.1 = 2,520 mg/kg
Sample ID:
Sample Number:
Sample Collected Date:
Sample Collected Time:
Thomas Lagoon #1-Sample A
39349-01
08/30/17
0805
PAN = Plant Available Nitrogen mg/kg = milligrams per kilogram = parts per million
RESEARCh & ANA1YTiCAl
UbotmoRiEs, INC.
Anolytical/Process Consultations
September 21, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
NO #34{
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
(A City of Winston-Salem Thomas WTP Protect, collected 30 August 2017)
1. Miscellaneous
Parameters
PAN = [MRx(TKN-NH3-N)] + (0.5x(NH-3-N))+ (NO3+NO2) = 0.4x(7,170-I,380) + (0.5x(1,380)+3.57 = 3,010 mg/kg
Sample CD:
Sample Number:
Sample Collected Date:
Sample Collected Time:
Thomas Logoon # I -Sample B
39349-02
08/30/I 7
0805
PAN = Plant Available Nitrogen ma/ka = milligrams per kilogram = parts per million
RESEARCH & ANA[YTICAL
LAbomoRirzs, INC.
Analytical/Process Consultations
September 21, 2017
City of Winston-Salem Thomas WTP
1201 South MIX Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
x � NCNsa
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
(A City of Winston-Salem Thomas WTP Project, collected 30 August 2017)
I. Miscellaneous
Parameters
PAN = [MRx(TKN-NH3-N)] + (0.5x(NH-3 N))+ (NO3+NO2) = 0.4x(5,880-735) + (O.Sx(735)+3.66 = 2,430 mg/kg
Sample ID:
Sample Number:
Sample Collected Date:
Sample Collected Time:
Thomas Logoon #1-Sample C
39349-03
08/30/17
0805
PAN = Plant Available Nitrogen mglkg = milligrams per kilogram = parts per million
RESEARCh & ANA1YTiCA1
I? '' LAORATORIES INC.
Analytical/Process Consultations
September 21, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
LrGij7- � K i/
¢ s"r�AlC#34
=�!WECt04: fiy .
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
AS City of Winston-Salem Thomas WTP Project, collected 30 August 2017)
I. Miscellaneous
Parameters
SAR = Na 6.0
T Ca+ Me — 45.5+86,7 = 0.738
2 2
Sample ID. -
Sample Number:
Sample Collected Date:
Sample Collected Time:
Thomas Lagoon #1-Sample A
39349-01
08/30/17
0805
SAR = Sodium Absorption Rate mglkg = milligrams per kilogram = parts per million
R ESEARCh & ANALYTICAL.
LAbORATORI ESQ INC.
Analyticavprocess consultations
•., EDAM *
September 21, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
Chemical Analysis for Selected Parameters and Sampling Location Identified as Residuals Sampling & Analysis
[A Cit of Winston-Salem Thomas WTP Project, collected 30 August 2017) _
I. Miscellaneous
Parameters
SAR = Na 9.30
Ca+ Me = 205+126 = 0.723
2 2
Sample ID:
Sample Number:
Sample Collected Date:
Sample Collected Time:
SAR = Sodium AbsDrpfion Rate
Thomas Lagoon ##1-Sample B
39344-02
08/30/17
0805
mglkg = milligrams per kilogram = parts per million
RESEARCh & IANAtyTiCAt
LAb4RATOR#ES? INC.
Analytical/Process consultations
September 21, 2017
City of Winston-Salem Thomas WTP
1201 South MLK Jr Drive
Winston-Salem, NC 27107
Attention: Donna Lankford
`f�fpwarggi
NO M8s
Chemical Analysis for Selected Parameters and Sampling Location Identilaed as Residuals Sampling & Analysis
A CitY of Winston-Salem Thomas WTP Project, collected 30 August 2017
I. Miscellaneous
Parameters
SAR = Na
Ca_ + Ma
2
Sample ID:
I0.4
= 53.5+I38 = 1.Ob
2
Sample Number:
Sample Collected Date:
Sample Collected Time:
Thomas Lagoon #1-Sample C
39349-03
08M/17
0805
SAR = Sodium Absorption Rate mg/kg = milligrams per kilogram = parts per million
13 RESEARCh & ANAlyTICAI
L.AbORATORIESI INC.
Analytical / Process Consultations
Phone (336) 996-2841
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FM : s :.
�Ab®RAToRiEsp INC.
Analytical/Process Consultations
Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Residuals Sampling & Analysis
(A City,of Winston-Salem Thomas WTP Project,_collected 26 April 2016)
EPA RW
Number
Contaminant
I.
TCLP METALS
D-004
Arsenic
D-005
Barium
D-006
Cadmium
D-077
Chromium
D-008
Lead
D-009
Mercury
D-010
Selenium
D-011
Silver
II.
TCLP VOLATILES
D-018
Benzene
D-019
Carbon Tetrachloride
D-021
Chlorobenzene
D-022
Chloroform
D-028
1,2-Dichloroethane
D-029
1,1-1)ichloroethylene
D-035
Methyl Ethyl Ketone
D-039
Tetrachloroethylene
D-040
Trichloroathylene
D-043
Vinyl Chloride
III
TCLP SEMI-VOLATILES
D-023
O-Creosol
D-024
M-Creosol
D-025
p-CreosoI
D-026
Creosol
D-027
1,4-Dichlorobeazene
D-030
2,4-Dinitrotoluene
D-032
Hexachlorobenzene
D-033
Hexachlorobutadiene
D-034
Hexachloroethane
D-036
Nitrobenzene
D-037
Pentachlorophenol
D-038
Pyridine
D-041
2,4,5-Trichlorophenol
D-042
2,4,6-Trichlorophenol
IV.
TCLP PESTICIDES/HERBICIDES
D-020
Chlordane
D-016
2,4-D
D-012
Endrin
D-031
Heptachlor
D-013
Lindane
D-014
Methoxychlor
D-015
Toxaphene
D-017
2,4,5 TP(Silvex)
V.
REACTIVITY
D-003
Cyanide
D-003
Sulfide
VI.
CORROSIVITY
D-002
pH
VH.
TCLP MISCELLANEOUS
Paint Filter Test
VIII IGNITABILITY
D-001 Igmtability
Sample Number
Sample Date
Sample Time (hrs)
Sample Matrix
BQL = Below Quantitation Limits
Thomas Lagoon #2
Quantitation
Results
Characteristic
Limit(mgQ
m /L
Level(mp-/L)
EPA Method
0.010
BQL
5.00
6010C
0.040
0.454
100
6010C
0.005
BQL
1.00
6010C
0.010
BQL
5.00
601 OC
0.005
BQL
5.00
6010C
0.0020
BQL
0.200
7470A
0.100
BQL
1.00
6010C
0.010
BQL
5.00
6010C
0.050
BQL
0.500
8260E
0.050
BQL
0.500
8260B
0.050
BQL
100
8260E
0.500
BQL
6.00
8260B
0.050
BQL
0.500
8260B
0.050
BQL
0.700
8260E
0,500
BQL
200
8260B
0.050
BQL
0.700
U60B
0.050
BQL
0.500
8260B
0.050
BQL
0.200
8260E
20.0
BQL
200
8270D
20.0
BQL
200
8270D
20.0
BQL
200
8270D
20,0
BQL
200
8270D
0.750
BQL
7.50
8270D
0.050
BQL
0,130
8270D
0.050
BQL
0.130
8270D
0.050
BQL
0.500
8270D
0.300
BQL
3.00
8270D
0.200
BQL
2.00
8270D
10.0
BQL
100
8270D
0.500
BQL
5.00
9270D
40.0
BQL
400
8270D
0.200
BQL
2.00
8270D
0.003
BQL
0.030
8081 B
1.000
BQL
10.0
8151 A
0.002
BQL
0.020
8081 B
0.0009
BQL
0.008
8081 B
0,040
BQL
0.400
8081 B
1,000
BQL
10.0
8081 B
0.050
BQL
0.500
8081 B
0.100
BQL
1.00
8151 A
2.0
BQL
9010
10.0
BQL
9030
Std. Units
6.28
9045
FLP
WNI
18157-01
04/26/16
0830
Scllia
mg/L = milligrams per Litec = parts•per million (ppm)
1010
NFL = No Free Liquids