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Home My WebLink AboutNCG030427_DMR_20200229Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted ` e_a CERTIFICATE OF COVERAGE NO. NCG03 0 4 2 7 SAMPLE COLLECTION YEAR 2y Z.j FACILITY NAME GKN Driveline _ SAMPLE PERIOD Jan -June rl July -Dec COUNTY Alamance or Q Monthlyl c4,Vr' month PERSON COLLECTING SAMPLES Ricky Hiatt DISCHARGING TO CLASS ❑ORW ❑H W ❑Trout ❑PNA LABORATORY Pace Analytical —Lab Cert. # 12,40 RECEIVED ❑Zero -flow ❑Water Supply ❑SA Comments on sample collection or analysis: ❑Other [JIAR 10 2020 Part A: Stormwater Benchmarks and Monitoring Results CENT-RAL FILES DWR SECTION PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Total Copper Total Lead Total Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics' Benchmarks - - 100 mg/L or 50 mg/L4 6.0 — 9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 U� F�ara TW w� � < ti a, i'"� L v 4luar "s L zp.11'J"X U kyir� ��v L L Luw U d L .1-S• L'"3 L S , y f%r GaSI ^s ell ueJ -s L 40414� c z v,csJ.r ^s L /✓iS ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Pri t name) c/,��- Title (Print title) 1 L 2v2v Sig ure Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil er month. XINo discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches' New Motor Oil or Hydraulic Oil Usage Non -Polar O&G/ Total Petroleum Hydrocarbons Total Suspended Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L° Parameter Code - 46529 NCOIL 00552 CO530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations," l� Signature of Permittee Permit Date: 11/1/2018-05/31/2021 Date SWU-245, last revised 11/1/2018 Page 3 of 3 ;aceAnalVfical www.pacelabs.com February 24, 2020 Ricky Hiatt GKN Driveline 1067 Trollingwood Hawfield Rd. Mebane, NC 27302 RE: Project: Monthly Stormwater Pace Project No.: 92464303 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Ricky Hiatt: Enclosed are the analytical results for sample(s) received by the laboratory on February 07, 2020. This report is a summary of the results based upon our understanding of your data quality objectives. Please contact us if itemized quality control results are needed. These results relate only to the samples included in this report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Dave Bruce, GKN Driveline REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 13 aceAnalytical www.pacelabs.com Project: Monthly Stormwater Pace Project No.: 92464303 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 13 aceAnalXical www.pacelabs.com i SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Monthly Stormwater 92464303 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92464303001 Outfall 001 EPA 1664B HH 1 PASI-C EPA 608.3 SEM 29 PASI-C EPA 200.7 Rev 4.4 1994 RDT 3 PASI-A EPA 625.1 PKS 58 PASI-C EPA 624.1 SAS 34 PASI-C SM 254OD-2011 MJP 1 PASI-A EPA 9040C SMK 1 PASI-A EPA420.4 Rev 1.0 1993 KDF1 1 PASI-A 92464303002 Outfall 002 EPA 1664E HH 1 PASI-C EPA 608.3 SEM 29 PASI-C EPA 200.7 Rev 4.4 1994 RDT 3 PASI-A EPA 625.1 PKS 58 PASI-C EPA 624.1 SAS 34 PASI-C SM 2540D-2011 MJP 1 PASI-A EPA 9040C SMK 1 PASI-A EPA 420.4 Rev 1.0 1993 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 13 _ ?VceAnalyfical' www.pacelabs.com ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92464303 Sample: Outfall 001 Parameters Lab ID: 92464303001 Results Units Collected: 02/06/20 12:00 Report Limit DF Oil and Grease ND mg/L 5.0 1 Aldrin ND ug/L 0.050 1 alpha-BHC ND ug/L 0.050 1 beta-BHC ND ug/L 0.050 1 delta-BHC ND ug/L 0.050 1 gamma-BHC (Lindane) ND ug/L 0.050 1 Chlordane (Technical) ND ug/L 0.50 1 alpha -Chlordane ND ug/L 0.050 1 gamma -Chlordane ND ug/L 0.050 1 4,4'-DDD ND ug/L 0.050 1 4,4'-DDE ND ug/L 0.050 1 4,4'-DDT ND ug/L 0.050 1 Dieldrin ND ug/L 0.050 1 Endosulfan I ND ug/L 0.050 1 Endosulfan II ND ug/L 0.050 1 Endosulfan sulfate ND ug/L 0.050 1 Endrin ND ug/L 0.050 1 Endrin aldehyde ND ug/L 0.050 1 Heptachlor ND ug/L 0.050 1 Heptachlor epoxide ND ug/L 0.050 1 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 PCB-1232 (Aroclor 1232) ND ug/L 0.50 1 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 Toxaphene ND ug/L 0.50 1 Tetrachloro-m-xylene (S) 59 % 10-130 1 Decachlorobiphenyl (S) 64 % 10-130 1 Copper ND ug/L 5.0 1 Lead ND ug/L 5.0 1 Zinc 42.4 ug/L 10.0 1 Acenaphthene ND ug/L 5.0 1 Acenaphthylene ND ug/L 5.0 1 Anthracene ND ug/L 5.0 1 Benzo(a)anthracene ND ug/L 5.0 1 Benzo(a)pyrene ND ug/L 5.0 1 Benzo(b)fluoranthene ND ug/L 5.0 1 Benzo(g,h,i)perylene ND ug/L 5.0 1 Benzo(k)fluoranthene ND ug/L 5.0 1 4-Bromophenylphenyl ether ND ug/L 5.0 1 Butylbenzylphthalate ND ug/L 5.0 1 4-Chloro-3-methylphenol ND ug/L 5.0 1 bis(2-Chloroethoxy)methane ND ug/L 10.0 1 bis(2-Chloroethyl) ether ND ug/L 5.0 1 2-Chloronaphthalene ND ug/L 5.0 1 2-Chlorophenol ND ug/L 5.0 1 4-Chlorophenylphenyl ether ND ug/L 5.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2020 11:27 AM without the written consent of Pace Analytical Services, LLC. Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 13 aceAnalj6cal www.pacelabs.com ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92464303 Sample: Outfall 001 Lab ID: 92464303001 Collected: 02/06/20 12:00 Parameters Results Units Report Limit DF Chrysene ND ug/L 5.0 1 Dibenz(a,h)anthracene ND ug/L 5.0 1 3,3'-Dichlorobenzidine ND ug/L 25.0 1 2,4-Dichlorophenol ND ug/L 5.0 1 Diethylphthalate ND ug/L 5.0 1 2,4-Dimethylphenol ND ug/L 10.0 1 Dimethylphthalate ND ug/L 5.0 1 Di-n-butylphthalate ND ug/L 5.0 1 4,6-Dinitro-2-methylphenol ND ug/L 10.0 1 2,4-Dinitrophenol ND ug/L 50.0 1 2,4-Dinitrotoluene ND ug/L 5.0 1 2,6-Dinitrotoluene ND ug/L 5.0 1 Di-n-octylphthalate ND ug/L 5.0 1 bis(2-Ethylhexyl)phthalate ND ug/L 5.0 1 Fluoranthene ND ug/L 5.0 1 Fluorene ND ug/L 5.0 1 Hexachloro-1,3-butadiene ND ug/L 5.0 1 Hexachlorobenzene ND ug/L 5.0 1 Hexachlorocyclopentadiene ND ug/L 10.0 1 Hexachloroethane ND ug/L 5.0 1 Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 Isophorone ND ug/L 10.0 1 Naphthalene ND ug/L 5.0 1 Nitrobenzene ND ug/L 5.0 1 2-Nitrophenol ND ug/L 5.0 1 4-Nitrophenol ND ug/L 50.0 1 N-Nitrosodimethylamine ND ug/L 5.0 1 N-Nitroso-di-n-propylamine ND ug/L 5.0 1 N-Nitrosodiphenylamine ND ug/L 10.0 1 2,2'-Oxybis(1-chloropropane) ND ug/L 5.0 1 Pentachlorophenol ND ug/L 10.0 1 Phenanthrene ND ug/L 5.0 1 Phenol ND ug/L 5.0 1 Pyrene ND ug/L 5.0 1 1,2,4-Trichlorobenzene ND ug/L 5.0 1 2,4,6-Trichlorophenol ND ug/L 10.0 1 Nitrobenzene-d5(S) 76 % 10-120 1 2-Fluorobiphenyl (S) 55 % 15-120 1 Terphenyl-d14 (S) 91 % 11-131 1 Phenol-d6 (S) 46 % 10-120 1 2-Fluorophenol (S) 60 % 10-120 1 2,4,6-Tribromophenol (S) 86 % 10-137 1 Benzene ND ug/L 1.0 1 Bromodichloromethane ND ug/L 2.0 1 Bromoform ND ug/L 2.0 1 Bromomethane ND ug/L 2.0 1 L1 Carbon tetrachloride ND ug/L 2.0 1 Chlorobenzene ND ug/L 2.0 1 Chloroethane ND ug/L 2.0 1 REPORT OF LABORATORY ANALYSIS Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, Date: 02/24/2020 11:27 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 13 ;aceAnalXicalo � www.pacelabs.com 1 Project: Monthly Stormwater Pace Project No.: 92464303 ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Outfall 001 Lab ID: 92464303001 Collected: 02/06/20 12:00 Parameters Results Units Report Limit DF Qualifiers Chloroform ND ug/L 2.0 1 Chloromethane ND ug/L 2.0 1 Dibromochloromethane ND ug/L 2.0 1 1,2-Dichlorobenzene ND ug/L 2.0 1 1,3-Dichlorobenzene ND ug/L 2.0 1 1,4-Dichlorobenzene ND ug/L 2.0 1 1,1-Dichloroethane ND ug/L 2.0 1 1,2-Dichloroethane ND ug/L 2.0 1 1,1-Dichloroethene ND ug/L 2.0 1 cis- 1,2-Dichloroethene ND ug/L 2.0 1 trans- l,2-Dichloroethene ND ug/L 2.0 1 1,2-Dichloropropane ND ug/L 2.0 1 cis-1,3-Dichloropropene ND ug/L 2.0 1 trans- 1,3-Dichloropropene ND ug/L 2.0 1 Ethylbenzene ND ug/L 1.0 1 Methylene Chloride ND ug/L 2.0 1 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 Tetrachloroethene ND ug/L 2.0 1 Toluene ND ug/L 1.0 1 1, 1, 1 -Trichloroethane ND ug/L 2.0 1 1,1,2-Trichloroethane ND ug/L 2.0 1 Trichloroethene ND ug/L 2.0 1 Trichlorofluoromethane ND ug/L 2.0 1 Vinyl chloride ND ug/L 2.0 1 4-Bromofluorobenzene (S) 97 % 70-130 1 Toluene-d8 (S) 102 % 70-130 1 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 Total Suspended Solids 16.9 mg/L 3.3 1 pH at 25 Degrees C 6.0 Std. Units 0.10 1 H3 Phenol ND mg/L 0.020 1 Date: 02/24/2020 11:27 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 13 11�;a'ceAnalyficalo www.pacelabs.cem i Project: Monthly Stormwater Pace Project No.: 92464303 Sample: Outfall 002 Parameters Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92464303002 Collected: 02/06/20 12:25 Results Units Report Limit DF Qualifiers Oil and Grease ND mg/L 5.0 Aldrin ND ug/L 0.050 alpha-BHC ND ug/L 0.050 beta-BHC ND ug/L 0.050 delta-BHC ND ug/L 0.050 gamma-BHC (Lindane) ND ug/L 0.050 Chlordane (Technical) ND ug/L 0.50 alpha -Chlordane ND ug/L 0.050 gamma -Chlordane ND ug/L 0.050 4,4'-DDD ND ug/L 0.050 4,4'-DDE ND ug/L 0.050 4,4'-DDT ND ug/L 0.050 Dieldrin ND ug/L 0.050 Endosulfan I ND ug/L 0.050 Endosulfan II ND ug/L 0.050 Endosulfan sulfate ND ug/L 0.050 Endrin ND ug/L 0.050 Endrin aldehyde ND ug/L 0.050 Heptachlor ND ug/L 0.050 Heptachlor epoxide ND ug/L 0.050 PCB-1016 (Aroclor 1016) ND ug/L 0.50 PCB-1221 (Aroclor 1221) ND ug/L 0.50 PCB-1232 (Aroclor 1232) ND ug/L 0.50 PCB-1242 (Aroclor 1242) ND ug/L 0.50 PCB-1248 (Aroclor 1248) ND ug/L 0.50 PCB-1254 (Aroclor 1254) ND ug/L 0.50 PCB-1260 (Aroclor 1260) ND ug/L 0.50 Toxaphene ND ug/L 0.50 Tetrachloro-m-xylene (S) 44 % 10-130 Decachlorobiphenyl (S) 53 % 10-130 Copper 5.6 ug/L 5.0 Lead ND ug/L 5.0 Zinc 18.9 ug/L 10.0 Acenaphthene ND ug/L 5.0 Acenaphthylene ND ug/L 5.0 Anthracene ND ug/L 5.0 Benzo(a)anthracene ND ug/L 5.0 Benzo(a)pyrene ND ug/L 5.0 Benzo(b)fluoranthene ND ug/L 5.0 Benzo(g,h,i)perylene ND ug/L 5.0 Benzo(k)fluoranthene ND ug/L 5.0 4-Bromophenylphenyl ether ND ug/L 5.0 Butyl benzylphthalate ND ug/L 5.0 4-Chloro-3-methyl phenol ND ug/L 5.0 bis(2-Chloroethoxy)methane ND ug/L 10.0 bis(2-Chloroethyl) ether ND ug/L 5.0 2-Chloronaphthalene ND ug/L 5.0 2-Chlorophenol ND ug/L 5.0 4-Chlorophenylphenyl ether ND ug/L 5.0 1 1 1 1 1 1 1 1 1 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2020 11:27 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92464303 Sample: Outfall 002 Parameters Lab ID: 92464303002 Results Units Collected: 02/06/20 12:25 Report Limit DF Qualifiers Chrysene ND ug/L 5.0 1 Dibenz(a,h)anthracene ND ug/L 5.0 1 3,3'-Dichlorobenzidine ND ug/L 25.0 1 2,4-Dichlorophenol ND ug/L 5.0 1 Diethylphthalate ND ug/L 5.0 1 2,4-Dimethylphenol ND ug/L 10.0 1 Dimethylphthalate ND ug/L 5.0 1 Di-n-butylphthalate ND ug/L 5.0 1 4,6-Dinitro-2-methylphenol ND ug/L 10.0 1 2,4-Dinitrophenol ND ug/L 50.0 1 2,4-Dinitrotoluene ND ug/L 5.0 1 2,6-Dinitrotoluene ND ug/L 5.0 1 Di-n-octylphthalate ND ug/L 5.0 1 bis(2-Ethylhexyl)phthalate ND ug/L 5.0 1 Fluoranthene ND ug/L 5.0 1 Fluorene ND ug/L 5.0 1 Hexachloro-1,3-butadiene ND ug/L 5.0 1 Hexachlorobenzene ND ug/L 5.0 1 Hexachlorocyclopentadiene ND ug/L 10.0 1 Hexachloroethane ND ug/L 5.0 1 Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 Isophorone ND ug/L 10.0 1 Naphthalene ND ug/L 5.0 1 Nitrobenzene ND ug/L 5.0 1 2-Nitrophenol ND ug/L 5.0 1 4-Nitrophenol ND ug/L 50.0 1 N-Nitrosodimethylamine ND ug/L 5.0 1 N-Nitroso-di-n-propylamine ND ug/L 5.0 1 N-Nitrosodiphenylamine ND ug/L 10.0 1 2,2'-Oxybis(1-chloropropane) ND ug/L 5.0 1 Pentachlorophenol ND ug/L 10.0 1 Phenanthrene ND ug/L 5.0 1 Phenol ND ug/L 5.0 1 Pyrene ND ug/L 5.0 1 1,2,4-Trichlorobenzene ND ug/L 5.0 1 2,4,6-Trichlorophenol ND ug/L 10.0 1 Nitrobenzene-d5 (S) 79 % 10-120 1 2-Fluorobiphenyl (S) 59 % 15-120 1 Terphenyl-d14 (S) 94 % 11-131 1 Phenol-d6 (S) 48 % 10-120 1 2-Fluorophenol (S) 60 % 10-120 1 2,4,6-Tribromophenol (S) 86 % 10-137 1 Benzene ND ug/L 1.0 1 Bromodichloromethane ND ug/L 2.0 1 Bromoform ND ug/L 2.0 1 Bromomethane ND ug/L 2.0 1 L1 Carbon tetrachloride ND ug/L 2.0 1 Chlorobenzene ND ug/L 2.0 1 Chloroethane ND ug/L 2.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2020 11:27 AM without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 13 (��a'cieAnalXical www.pacelabs.com ANALYTICAL RESULTS Project: Monthly Stormwater Pace Project No.: 92464303 Sample: Outfall 002 Lab ID: 92464303002 Collected: 02/06/20 12:25 Parameters Results Units Report Limit DF Chloroform ND ug/L 2.0 1 Chloromethane ND ug/L 2.0 1 Dibromochlorom ethane ND ug/L 2.0 1 1,2-Dichlorobenzene ND ug/L 2.0 1 1,3-Dichlorobenzene ND ug/L 2.0 1 1,4-Dichlorobenzene ND ug/L 2.0 1 1,1-Dichloroethane ND ug/L 2.0 1 1,2-Dichloroethane ND ug/L 2.0 1 1,1-Dichloroethene ND ug/L 2.0 1 cis-1,2-Dichloroethene ND ug/L 2.0 1 trans- 1,2-Dichloroethene ND ug/L 2.0 1 1,2-Dichloropropane ND ug/L 2.0 1 cis-1,3-Dichloropropene ND ug/L 2.0 1 trans-1,3-Dichloropropene ND ug/L 2.0 1 Ethylbenzene ND ug/L 1.0 1 Methylene Chloride ND ug/L 2.0 1 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 Tetrachloroethene ND ug/L 2.0 1 Toluene ND ug/L 1.0 1 1,1,1-Trichloroethane ND ug/L 2.0 1 1,1,2-Trichloroethane ND ug/L 2.0 1 Trichloroethene ND ug/L 2.0 1 Trichlorofluoromethane ND ug/L 2.0 1 Vinyl chloride ND ug/L 2.0 1 4-Bromofluorobenzene (S) 101 % 70-130 1 Toluene-d8 (S) 101 % 70-130 1 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 Total Suspended Solids 25.2 mg/L 4.2 1 pH at 25 Degrees C 5.9 Std. Units 0.10 1 Phenol ND mg/L 0.020 1 Date: 02/24/2020 11:27 AM H3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 13 11eAnalytical www.pacelabs.com i QUALIFIERS Project: Monthly Stormwater Pace Project No.: 92464303 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/24/2020 11:27 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 13 Document Name: Document Revised: February 7, 2018 ace Anal /cal ' Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville( , Condition Client Name:Upon Receipt r ` Project a: Wo# : 9246430 3 Courier: ❑Fed Ex [—]UPS [—]LISPS [—]Client II'll' I� UI ❑ Commercial ❑Pace ❑Other: 82464303 Custody Seal Present? ❑Yes []No Seals Intact? ❑Yes QNo c` 'Ci Date/Initials Person Examining Contents: Packing Material: []Bubble Wrap ❑Bubble Bags ❑None ❑ Other Blologlcal Tissue Frozen? Thermometer: Dyes ❑No ❑N/A ❑1RGun ID: 92TO58 Type of Ice: ❑Wet []Blue ❑None Cooler Temp ('C): / y- Correction Factor: Add/Subtract IT) O.00C Temp should be above freezing to 6'C Cooler Temp Corrected ('C): ; ❑Samples out of temp criteria. Samples an ice, cooling process has begun USDA Regulated Soil (❑ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, r-lvo. I Includine Hawaii and Puerto Ricol? 71Yes nNo Comments/Dlscrepa ncy: Chain of Custody Present? - Yes ❑No ❑N/A 1. Samples Arrived within Hold Time? []Yes [:]No ❑N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes ❑No []N/A 3. Rush Turn Around Time Requested? Elves []NO ❑N/A 4. Sufficient Volume? es EJNo []N/A S. Correct Containers Used? -Pace Containers Used? ❑Yes ❑Yes ❑No ❑No ❑N/A ❑N/A 6. Containers Intact. Dyes []No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes []No ❑N/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: ❑Yes ❑No ❑N/A 9. Headspace in VOA Vials (>5-6mm)? ❑Yes ❑No ❑N/A 10. (i t / r''? (J tj/%7�/C.. Trip Blank Present? Trip Blank Custody Seals Present? Oyes ❑Yes []No [:]No ❑N/A ❑N/A 11, COMMENTS/SAMPLE DISCREPANCY Field Data Requlred? ❑Yes [:]NO Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/- ime: Project Manager SCURF Review: `� Date: A� I(o 17 o Project Manager SRF Review: ✓k Date: rt Page 11 of 13 Document Name: Document Revised: February 7, 2018 aCeAnalytical Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project # WO# : 92464303 PM: MWB Due Date: 02/21/20 CLIENT: 92-GKN Z E a n n E v1 eY > V ao u n a E O N > M to a n b a E O C. > N m v m C d > .-1 co V n 2 a .n m = o Z A n E O InN 2 11'1 6 m a G N a E N Q a m n x O Z a E ut V C n m c ro m �0 y O v LL Z m o. a E `v =' ♦-1 D U a ry n S n E v _ e� 2 - 0Q a v a n c = E Q E N D M a = o N 2 E u = U' a N n ry S E a E 0 N 1n M Q a Z E Q o Ln ran 1z.1 C] Q M U a z V a O E O S Q1 V' C Z N ra < O > E H 01 0 > z n C a O E o V D CM 0 > ,Q v fr) a O 6 Q1 IDO G a y o `u a 3 a > i° �' n V � > 2 G ,� E N N a of Z C y v1 E Vl N a N Z a E N M a to a E t7 4 ¢ 1a 1n E N Ji > S E E O l7 O 2 3 4 FS 6 7 8 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added tot p Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 12 of 13 CHAIN -OF -CUSTODY / Analytical Request Document aCeAnalytical The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Pa e : Of 1 Company: GKN Dmel ne- Alamnnce Report TO: Ricky Hiatt Attention Address: 1067 Trollingwood Hawfields Rd Copy To. Company Name. Meh—, NC 27302 Address Req.I.Wy Agency Email Purchase Order #: Pace Quote Phony. (919)215-1066 JFa,, Project Name: Monthly Stormwater Pace Project Manager. Matthewbrainartl pacelabs. corn, State 1 Location Requested Due Date Project #. Pace Profile # 4804-5 NC Requested Anal sis Filter od(YIN a Z AUITRIX CODE o U COLLECTED Z Preservatives } D-kin9 Water DW Water U O (.7 wine Water ww = < IX w Z P.ed°a P SAMPLE ID SL oli of c� V START END u I H m c One Character per box. War WP w a z (A-Z, 0.9 / , _I A,, AR 01M1ee OT o r ¢ Z m Z t7 to T m o c U # Sample Ids must be unique T ,- TS U x w O m O c tp a r j W ¢ t- a a m O rn 0O S O rn — •- c — c O o t— h DATE TIME DAT/E TIME z z Z. O n ~ O in aL. c (, 1 Outfall 001 WT X X X X X I X X X Cu. Pb, Zn 2 Outfall 002 WT 1' xva ( `s l ' X X X X X X X X I I Cu. Pb, Zn 3 4 S 6 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY l AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 51 -1 SAMPLER NAME AND SIGNATURE c 'n `c a PRINT Name of SAMPLER: a o m a SIGNATURE of SAMPLER: DATE Signed: Z! 2t4D L -0 ~ Z °' Y u o Z r N U E Z A c Y