HomeMy WebLinkAboutNCG030427_DMR_20191112Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCG03 0 4 2 7
FACILITY NAME GKN Driveline
COUNTY Alamance
SAMPLE COLLECTION YEAR -- U/ y
SAMPLE PERIOD Q Jan -June D July-Qec
or 0 Monthly' IV -A !>, (month)
PERSON COLLECTING SAMPLES Y DISCHARGING TO CLASS ORW HQvv Trout PNA
Rick Hiatt ❑ ❑
LABORATORY Pace Analytical Lab Cert. # 12,40 RECEIVED ❑Zero -flow ❑Water Supply [:]SA
Comments on sample collection or analysis:
Part A: Stormwater Benchmarks and Monitoring Results
AR 10 2020
CENTRAL FILES,
DWR SECTION
❑Other_
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
❑ No discharge this period?'
Outfall No.
Date Sample
Collected'
(mo/dd/yr)
24-hour rainfall
amount,
Inches3
Total Suspended Solids
pH,
Standard units
Total Copper
Total Lead
Total Zinc
Non -Polar O&G/
Total Petroleum
Hydrocarbons
Total
'
Organics'
Benchmarks
_
-
100 mg/L or 50 mg/L4
6.0 — 9.0
0.010 mg/L
0.075 mg/L
0.126 mg/L
15 mg/L
1 mg/L
Parameter Code
46529
C0530
00400
01119
01051
01094
00552
78141
Vvf/A, /_
1 % I Psi r
(� , 2
L, 1 --',4
, L
<1I1,00} 14J/4
<d, voS"'S
U. u� t� ^>�Z
4 a UOl �/✓
!�
/, / �f
�,
<U.du!^> �
�U. Uu�`
dyitS
L U, vu t r s/Z
i✓
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
° See General Permit, Section B, Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Al A //
Name (P int name) /� 1
Title(Print title)
Si ture Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical
format. When results are below the applicable limits, they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?'
Outfall No.
Date Sample Collected'
(mo/dd/yr)
24-hour rainfall amount,
Inches'
New Motor Oil or
Hydraulic Oil Usage
Non -Polar O&G/ Total
Petroleum Hydrocarbons
Total Suspended
Solids
Benchmarks
-
-
15 mg/L
100 mg/L or 50 mg/L4
Parameter Code
46529
NCOIL
00552
C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. see General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES Q NO 0
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO
REGIONAL OFFICE CONTACT NAME:
Mail an original copy of this DMR including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the
case of "No Discharge" reports) to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1 1- 1"a
e of Permittee Date
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3
aceAnalytical
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November 27, 2019
Ricky Hiatt
GKN Driveline
1067 Trollingwood Hawfield Rd.
Mebane, NC 27302
RE: Project: Monthly Stormwater
Pace Project No.: 92453652
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Dear Ricky Hiatt:
Enclosed are the analytical results for sample(s) received by the laboratory on November 13, 2019.
This report is a summary of the results based upon our understanding of your data quality objectives.
Please contact us if itemized quality control results are needed. These results relate only to the
samples included in this report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew.brainard@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Dave Bruce. GKN Driveline
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 1 of 12
;ace Analytical
www.pacelabs.com
Project: Monthly Stormwater
Pace Project No.: 92453652
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 12
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
Pace Project No.:
Monthly Stormwater
92453652
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92453652001
OUTFALL 001
EPA 1664E
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
SH1
3
PASI-A
EPA 625.1
PKS
58
PASI-C
SM 2540D-2011
CJL
1
PASI-A
SM 4500-H+B-2011
ECH
1
PASI-A
EPA420.4 Rev 1.0 1993
KDF1
1
PASI-A
92453652002
OUTFALL 002
EPA 1664E
HH
1
PASI-C
EPA 608.3
SEM
29
PASI-C
EPA 200.7 Rev 4.4 1994
SH 1
3
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 624.1
DLK
34
PASI-C
SM 254OD-2011
CJL
1
PASI-A
SM 4500-H+B-2011
ECH
1
PASI-A
EPA420.4 Rev 1.0 1993
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 12
aceAnalytical
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Project: Monthly Stormwater
Pace Project No.: 92453652
Sample: OUTFALL 001
Parameters
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Lab ID: 92453652001 Collected: 11/12/19 16:10
Results Units Report Limit OF Qualifiers
Oil and Grease
NO
mg/L
5.0
Aldrin
ND
ug/L
0.050
alpha-BHC
ND
ug/L
0.050
beta-BHC
NO
ug/L
0.050
delta-BHC
NO
ug/L
0.050
gamma-BHC (Lindane)
NO
ug/L
0.050
Chlordane (Technical)
NO
ug/L
0.50
alpha -Chlordane
ND
ug/L
0.050
gamma -Chlordane
ND
ug/L
0.050
4,4'-DDD
ND
ug/L
0.050
4,4'-DDE
ND
ug/L
0.050
4,4'-DDT
ND
ug/L
0.050
Dieldrin
ND
ug/L
0.050
Endosulfan I
NO
ug/L
0.050
Endosulfan II
NO
ug/L
0.050
Endosulfan sulfate
ND
ug/L
0.050
Endrin
ND
ug/L
0.050
Endrin aldehyde
ND
ug/L
0.050
Heptachlor
NO
ug/L
0.050
Heptachlor epoxide
NO
ug/L
0.050
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
Toxaphene
ND
ug/L
0.50
Tetrachloro-m-xylene (S)
66
%
10-130
Decachlorobiphenyl (S)
36
%
10-130
Copper
ND
ug/L
5.0
Lead
ND
ug/L
5.0
Zinc
87.3
ug/L
10.0
Acenaphthene
NO
ug/L
5.0
Acenaphthylene
NO
ug/L
5.0
Anthracene
NO
ug/L
5.0
Benzo(a)anthracene
NO
ug/L
5.0
Benzo(a)pyrene
ND
ug/L
5.0
Benzo(b)fluoranthene
NO
ug/L
5.0
Benzo(g,h,i)perylene
ND
ug/L
5.0
Benzo(k)fluoranthene
NO
ug/L
5.0
4-Bromophenylphenyl ether
NO
ug/L
5.0
Butylbenzylphthalate
NO
ug/L
5.0
4-Chloro-3-methylphenol
NO
ug/L
5.0
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
bis(2-Chloroethyl) ether
NO
ug/L
5.0
2-Chloronaphthalene
NO
ug/L
5.0
2-Chlorophenol
NO
ug/L
5.0
4-Chlorophenylphenyl ether
NO
ug/L
5.0
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /27/2019 08:55 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 12
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ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92453652
Sample: OUTFALL 001
Parameters
Lab ID: 92453652001
Results Units
Collected: 11/12/19 16:10
Report Limit DF
Chrysene
ND
ug/L
5.0
1
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
2,4-Dichlorophenol
ND
ug/L
5.0
1
Diethylphthalate
ND
ug/L
5.0
1
2,4-Dimethylphenol
ND
ug/L
10.0
1
Dimethylphthalate
ND
ug/L
5.0
1
Di-n-butylphthalate
ND
ug/L
5.0
1
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
2,4-Dinitrophenol
ND
ug/L
50.0
1
2,4-Dinitrotoluene
ND
ug/L
5.0
1
2,6-Dinitrotoluene
ND
ug/L
5.0
1
Di-n-octylphthalate
ND
ug/L
5.0
1
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
Fluoranthene
ND
ug/L
5.0
1
Fluorene
ND
ug/L
5.0
1
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
Hexachlorobenzene
ND
ug/L
5.0
1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
Hexachloroethane
ND
ug/L
5.0
1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
Isophorone
ND
ug/L
10.0
1
Naphthalene
ND
ug/L
5.0
1
Nitrobenzene
ND
ug/L
5.0
1
2-Nitrophenol
ND
ug/L
5.0
1
4-Nitrophenol
ND
ug/L
50.0
1
N-Nitrosodimethylamine
ND
ug/L
5.0
1
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
Pentachlorophenol
ND
ug/L
10.0
1
Phenanthrene
ND
ug/L
5.0
1
Phenol
ND
ug/L
5.0
1
Pyrene
ND
ug/L
5.0
1
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
Nitrobenzene-d5 (S)
82
%
10-120
1
2-Fluorobiphenyl (S)
76
%
15-120
1
Terphenyl-d14 (S)
83
%
11-131
1
Phenol-d6 (S)
55
%
10-120
1
2-Fluorophenol (S)
74
%
10-120
1
2,4,6-Tribromophenol (S)
100
%
10-137
1
Total Suspended Solids
6.6
mg/L
2.5
1
pH at 25 Degrees C
6.2
Std. Units 0.10
1 H3
Phenol
ND
mg/L
0.020
1
REPORT OF LABORATORY ANALYSIS
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
This report shall not be reproduced, except in full,
Date: 11 /27/2019 08:55 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 12
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ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92453652
Sample: OUTFALL 002
Parameters
Lab ID: 92453652002
Results Units
Collected: 11/12/19 16:30
Report Limit DF
Oil and Grease
ND
mg/L
5.0
1
Aldrin
ND
ug/L
0.050
1
alpha-BHC
ND
ug/L
0.050
1
beta-BHC
ND
ug/L
0.050
1
delta-BHC
ND
ug/L
0.050
1
gamma-BHC (Lindane)
ND
ug/L
0.050
1
Chlordane (Technical)
ND
ug/L
0.50
1
alpha -Chlordane
ND
ug/L
0.050
1
gamma -Chlordane
ND
ug/L
0.050
1
4,4'-DDD
ND
ug/L
0.050
1
4,4'-DDE
ND
ug/L
0.050
1
4,4'-DDT
ND
ug/L
0.050
1
Dieldrin
ND
ug/L
0.050
1
Endosulfan I
ND
ug/L
0.050
1
Endosulfan II
ND
ug/L
0.050
1
Endosulfan sulfate
ND
ug/L
0.050
1
Endrin
ND
ug/L
0.050
1
Endrin aldehyde
ND
ug/L
0.050
1
Heptachlor
ND
ug/L
0.050
1
Heptachlor epoxide
ND
ug/L
0.050
1
PCB-1016 (Aroclor 1016)
ND
ug/L
0.50
1
PCB-1221 (Aroclor 1221)
ND
ug/L
0.50
1
PCB-1232 (Aroclor 1232)
ND
ug/L
0.50
1
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
PCB-1248 (Aroclor 1248)
ND
ug/L
0.50
1
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
PCB-1260 (Aroclor 1260)
ND
ug/L
0.50
1
Toxaphene
ND
ug/L
0.50
1
Tetrachloro-m-xylene (S)
79
%
10-130
1
Decachlorobiphenyl (S)
97
%
10-130
1
Copper
ND
ug/L
5.0
1
Lead
ND
ug/L
5.0
1
Zinc
47.5
ug/L
10.0
1
Acenaphthene
ND
ug/L
5.0
1
Acenaphthylene
ND
ug/L
5.0
1
Anthracene
ND
ug/L
5.0
1
Benzo(a)anthracene
ND
ug/L
5.0
1
Benzo(a)pyrene
ND
ug/L
5.0
1
Benzo(b)fluoranthene
ND
ug/L
5.0
1
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
Benzo(k)fluoranthene
ND
ug/L
5.0
1
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
Butylbenzylphthalate
ND
ug/L
5.0
1
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
2-Chloronaphthalene
ND
ug/L
5.0
1
2-Chlorophenol
ND
ug/L
5.0
1
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /27/2019 08:55 AM without the written consent of Pace Analytical Services, LLC.
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
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ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92453652
Sample: OUTFALL 002
Lab ID: 92453652002
Collected: 11/12/19 16:30
Parameters
Results
Units
Report Limit
DF
Chrysene
ND
ug/L
5.0
1
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
2,4-Dichlorophenol
ND
ug/L
5.0
1
Diethylphthalate
ND
ug/L
5.0
1
2,4-Dimethylphenol
ND
ug/L
10.0
1
Dimethylphthalate
ND
ug/L
5.0
1
Di-n-butylphthalate
ND
ug/L
5.0
1
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
2,4-Dinitrophenol
ND
ug/L
50.0
1
2,4-Dinitrotoluene
ND
ug/L
5.0
1
2,6-Dinitrotoluene
ND
ug/L
5.0
1
Di-n-octylphthalate
ND
ug/L
5.0
1
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
Fluoranthene
ND
ug/L
5.0
1
Fluorene
ND
ug/L
5.0
1
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
Hexachlorobenzene
ND
ug/L
5.0
1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
Hexachloroethane
ND
ug/L
5.0
1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
Isophorone
ND
ug/L
10.0
1
Naphthalene
ND
ug/L
5.0
1
Nitrobenzene
ND
ug/L
5.0
1
2-Nitrophenol
ND
ug/L
5.0
1
4-Nitrophenol
ND
ug/L
50.0
1
N-Nitrosodimethylamine
ND
ug/L
5.0
1
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
Pentachlorophenol
ND
ug/L
10.0
1
Phenanthrene
ND
ug/L
5.0
1
Phenol
ND
ug/L
5.0
1
Pyrene
ND
ug/L
5.0
1
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
Nitrobenzene-d5 (S)
71
%
10-120
1
2-Fluorobiphenyl (S)
68
%
15-120
1
Terphenyl-d14 (S)
76
%
11-131
1
Phenol-d6 (S)
46
%
10-120
1
2-Fluorophenol (S)
60
%
10-120
1
2,4,6-Tribromophenol (S)
93
%
10-137
1
Benzene
ND
ug/L
1.0
1
Bromodichloromethane
ND
ug/L
2.0
1
Bromoform
ND
ug/L
2.0
1
Bromomethane
ND
ug/L
2.0
1
Carbon tetrachloride
ND
ug/L
2.0
1
Chlorobenzene
ND
ug/L
2.0
1
Chloroethane
ND
ug/L
2.0
1
REPORT OF LABORATORY ANALYSIS
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
This report shall not be reproduced, except in full,
Date: 11 /27/2019 08:55 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 12
aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Monthly Stormwater
Pace Project No.: 92453652
Sample: OUTFALL 002
Parameters
Lab ID: 92453652002
Results Units
Collected: 11/12/19 16:30
Report Limit DF
Chloroform
ND
ug/L
2.0
1
Chloromethane
ND
ug/L
2.0
1
Dibromochloromethane
ND
ug/L
2.0
1
1,2-Dichlorobenzene
ND
ug/L
2.0
1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
1,4-Dichlorobenzene
ND
ug/L
2.0
1
1,1-Dichloroethane
ND
ug/L
2.0
1
1,2-Dichloroethane
ND
ug/L
2.0
1
1,1-Dichloroethene
ND
ug/L
2.0
1
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
1,2-Dichloropropane
ND
ug/L
2.0
1
cis- 1,3-Dichloropropene
ND
ug/L
2.0
1
trans-1,3-Dichloropropene
ND
ug/L
2.0
1
Ethylbenzene
ND
ug/L
1.0
1
Methylene Chloride
ND
ug/L
2.0
1
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
Tetrachloroethene
ND
ug/L
2.0
1
Toluene
ND
ug/L
1.0
1
1,1,1-Trichloroethane
ND
ug/L
2.0
1
1,1,2-Trichloroethane
ND
ug/L
2.0
1
Trichloroethene
ND
ug/L
2.0
1
Trichlorofluoromethane
ND
ug/L
2.0
1
Vinyl chloride
ND
ug/L
2.0
1
4-Bromofluorobenzene(S)
102
%
70-130
1
Toluene-d8 (S)
99
%
70-130
1
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
Total Suspended Solids
11.1
mg/L
2.5
1
pH at 25 Degrees C
6.1
Std. Units
0.10
1
Phenol
ND
mg/L
0.020
1
Date: 11 /27/2019 08:55 AM
H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 8 of 12
aceAnalXical U
www.pacelabs.com
QUALIFIERS
Project: Monthly Stormwater
Pace Project No.: 92453652
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/27/2019 08:55 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 12
Document Name:
Document Revised: February 7, 2018
acekialytrealm
Sample Condltlon Upon Receipt(5CUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
Sample Condition Client Name: WO# : 92453652
Project tf:
1 i ❑
Courier: ❑Fed Ex x []UPS LISPS []Client
❑ Commercial ❑Pace ❑Other: 92453552
Custody Seal Present? ❑Yes []No Seals Intact? ❑Yes [-]No
QatL/Initials Person Examining Contents; j /C
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Blologlcal Tissue Frozen?
Thermometer: ❑Yes ❑No ❑N/A
❑IR Gun ID. _ 92TO58 Type of Ice: []Wet [-]Blue ❑None
Cooler Temp ('Cl: j, _ Correction Factor: Add/Subtract (°C) O.O°C
i Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): i ' ❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soll (❑ N/A, water sample)
DA samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samplesoriglnate from a foreign source (internationally,
11YPs MNn Indudin¢ Hawaii and Puerto Ricol? nYes IlNo
Comments/Discrepancy:
Chain of Custody Present?
❑Yes
No
' N/A
1.
Samples Arrived within Hold Time?
[]Yes
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
[]No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
❑No
❑N/A
4.
Sufficient Volume
— ❑Yes ❑No
I_iN/A
S. _
Correct Containers Used?
-Pace Containers Used?
❑Yes
❑Yes
❑Nc
flv,
[]N/A
N/A
6.
Containers Intact?
❑Yes
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
CjYes
❑No
❑N/A
B.
Sample Labels Matr`. COC?
-Includes Date/Time/ID,'',s.alysis Matrix:
❑Yes
❑No
❑N/A
9.
Headspace in VOA Vials (>S-6mm)?
❑Yes
❑No
U N/A
10. _
_
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
[:]No
❑No
❑N/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
lot ID of sp!It contiinors
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Field Data Required? []Yes []No
Date: �( �(1 ice_
Date: ,, f ILI f(if__
Page 10 of 12
aceAnaVica(
Document Name:
Sample Condition Upon Recelpt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
`Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # Wp## : 92453652
PM: MWB Due Date: 11/27/19
CLIENT: 92-OKN
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
lot H
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 11 of 12
0117I CHAIN -OF -CUSTODY / Analytical Request Document
P,�ctM eihliul The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A
Section B Section C
Required Client Information:
Required Project Information: Invoice Information:
Pa e . 1 Of
Company GKN Dnveline- Alamance
Report To Ricky Hiatt
Attention
Address 1067 Trollingwood Hawfields Rd
Copy To.
Company Name
Mebane. NC 27302
Address
Regulatory Agency
Email
Purchase Order #.
Pace Quote.
Phone (919)215-1066 JFa.
Project Name Monthly Stormwaler
Pace Protect Managermatlhew brainardppaceiabs. com.
State I Location
Requested Due Date.
Protect #
Pace ProLle # 4604-5
NC
Re uested Analysis Filtered Y!N
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COLLECTED
Preservatives
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Drmkm
Water
I Warr. DW
U
Wa;Ir
PioO
SAMPLE ID
rrr WW
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SL
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c1
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START
END
a
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WP
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Cu, Pb, Zn
I
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Outfall 002
X
X
X
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x
X
X
X
Cu, Pb, Zn --
3
4
5
6
7
8
9
10
11
12
ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY 1 AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
77
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SAMPLER NAME AND SIGNATURE
m
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PRINT Name of SAMPLER:
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SIGNATURE of SAMPLER: ) -7rT"
DATE Signed:
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