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HomeMy WebLinkAbout820144_ENFORCEMENT_20171231RECENEDIDENPOWR Water Quarrty Regional FES 1 .a ns Section NCDENR FSY1111181irille Regional Offrcr North Carolina Department of Environment and Natural Resources Pat McCrory Donald R. van der Vaart Governor Secretary January 27, 2015 CERTIFIED MAIL RETURN RECEIPT REQUESTED Jim Walker Southern Cross Farm PO Box 242 Garland, NC28441-8441 Subject: Notice of Deficiency Southern Cross Farm Permit Number: AWS820144 Sampson County Dear Permittee, As of this date, our records indicate that the above -referenced permit issued to your facility has overdue fees. It is both a condition of your permit and required by Rule 15A NCAC 2T .0105(e) (2) to pay the annual administering and compliance fee within thirty (30) days of being billed by the Division of Water Resources (Division) - The following invoices are outstanding: Invoice Number Due Date Outstanding Fee S) 2014PR005631 8/9/2014 360 Failure to pay the fee accordingly may result in the Division initiating enforcement actions, to include the assessment of civil penalties. Failure to comply with conditions in a permit may result in a recommendation of enforcement action, to the Director of the Division of Water Resources who may issue a civil penalty assessment of not more that twenty-five thousand ($25,000) dollars against any "Person" who violates or fails to act in accordance with the terms, conditions, or requirements of a permit under authority of G.S. 143-215.6A. Therefore, it is imperative that you submit the appropriate fee as requested within thirty (30) days of this Notice of Deficiency. Please remit the payment, made payable to the North Carolina Department of Environment and Natural Resources (NCDENR), in the above amount. Please include Permit Number on your check and mail this payment to: Division of Water Resources — Budget Office Attn: Teresa Revis 1617 Mail Semite Center Raleigh, NC 27699-1617 Phone: (919) 807-63I6 -eoittd.- 1636 Mail Service Center, Raleigh, North Carolina 27699-1636 Phone: 919-807-64641 Internet: httpJlwww.ncwater,org An Equal Opportunity 4 Affirmative Acton Employer — Made in part by recycled paper If you have any questions concerning this Notice, please contact the Animal Fecding Operations Branch staff at (919) 807-6464. Sincerely, Debra J. Watts, Supervisor Animal Feeding Operations, and Ground Water Protection Branch cc: Fayetteville Regional Office, Water Quality Regional Operations Section WQROS Central File (Permit No AWS820144) Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Coleen Sullins, Director Division of Water Quality July 17, 2008 CERTIFIED MAIL RETURN RECEIPT REQUESTED Mr. Jim Walker PO Box 242 Garland, North Carolina 28441 Subject: NOTICE OF VIOLATION-NOV-2008-DV-0282 Administrative Code 15A NCAC 2H .0217 Southern Cross Farm Facility No. 82-144 Sampson County Permit No. AWS820144 Dear Mr. Walker: You are hereby notified that, having been permitted to have a non -discharge permit for the subject animal waste disposal system pursuant to 15A NCAC 2H .0217, you have been found to be in violation of your 2H .0217 Permit. Violation 1: Land application rates shall be in accordance with the CAWMP: (Permit No. AWS820144 Section II 4) On May 21, 2008 a flight over your farm by EPA and DWQ it appeared that you had ponding and possible run off of waste from a spray application. A site visit was conducted and it was observed that you did have ponding and runoff into the woods. Required Corrective action for Violation 1: If you Have not already done so, immediately cease discharging and begin efforts to recover the discharged animal waste. This waste must be handled as prescribed by your CAWMP and applicable state law. Additionally, take all necessary steps to ensure this violation does not reoccur. NorthCarolina Alatmra!!ry North Carolina DWQIAquifer Protection Section 225 Green St./ Suite 714 Fayetteville, NC 28301 Phone (910) 433-3300 FAX (910) 486-0707 Internet: h2o.enr.state.nc us Customer Service 1-877-623-6748 An Equal Opportuno/Athrmative Action Employer — 50% Recyded110°% Post Consumer Paper Mr. Walker Date July 7,2008 Page 2 The Division of Water Quality requests that, in addition to the specified corrective action above, please submit the following items on or before August 10,2008 unless another time frame is indicated below: 1. Copies of all the pumping records, lagoon levels, rainfall records and waste analyses for this farm from January 1, 2004 to the present along with a copy of your CAWMP. 2. Please have the 01C for this farm include an explanation as to how this violation occurred. 3. Please have the OIC include a list of the steps that will be taken to prevent this violation from occurring in the future. Please be advised that this notice does not prevent the Division of Water Quality from taking enforcement actions for this violation or any past or future violation. Furthermore, the Division of Water Quality has the authority to levy a civil penalty of not more than $25,000.00 per day per violation. If you have any questions concerning this matter, please do not hesitate to contact either Mr. Steve Guyton Environmental specialist or myself at (910) 433-3300 Sincerely, Stephen A. Barnhardt Regional Aquifer Protection Supervisor SB/tab cc: APS Central Files FRO APS Files Danny Edwards-SWC, FRO Murphy -Brown, LLC SOUTHERN CROSS FARMS INC. P.O. BOX 242 GARLAND, NC 28441 August 19, 2008 Mr. Stephen A. Barnhardt Regional Aquifer Protection Supervisor Division of Water Quality Dear Mr. Barnhardt: AUG 2 6 BOB AEI�R-fA1tE1T�Vl_ L�'O;�ALOffiIE In response to your letter received on August 13, 2008 1 would like to explain you what happened on May 21, 2008 at the Southern Cross Farm. On the above mention date we were pumping on field # 7 and field #3 with two different irrigation riels. On field #7 we had a slope going towards the lower part of the field, next to the woods that we were aware of, on that particular pull we retrieve the riel as fast as possible in order to avoid any run off, and that was the way it was set up this particular day. When we first started this unit we checked it and it was working properly with no run off, unfortunately due to saturation of the soil the water being pumped was not going into the ground totally and some started to run towards the lower part of the field next to the woods, we noticed this during the follow up check up within 2 hours of operation and proceed to turn the pump off. At this time your staff stopped by the farm and noticed that even though the unit was off the water was running into the woods due to soil saturation and slope. We immediately proceed to block the runoff and extract the water out of the wooded area before it will reach any other water source. In order to avoid this to happen again we went ahead and graded field #7 in a way that the possibility of runoff has been reduce to a minimum. Copy of the invoice attached. We take this job seriously and we will do what is needed in order to stay in compliance as we had been for over 15 years. el ;tc5 f'�:26 9106692732 - v°:,z�t�2z *0-- I _ �. t.0 FAX COVER SHEET 910 401-1920 r FROM: r DATE: E: 9 r- S.,/ -0 PAGES (INCLUDING COVER): NOTE: s- RFCOIVED .SUN 23 2008 DENR-f0i1'E TALLEREGONAIWCE FORM IRR-1 Lagoon Liquid Irrlgallon Fields Reoord For Recording ltrigation Events on Ditterent Fleids Farm Owner Vt 4�rrrY"1 Faalllty Plumber • � � � T _ - P. MM �, w . • 4� ►� +W.,• • r ' * I "11111 M "ME11111 =I MMI "i MI O r' � ' MMMININIM + • r' +• ��� �� ' it ��� ,1 S — - W-- " Weather Codes: C-Clear, PC -Partly Cloudy, CI -Cloudy, R-Haln, S-SnowiSleet, W-Wflndy W14fOS " Parsons completing the trrlgailon inspectlons must Initial to signify that Inopectlons were completed et least every 12U minutes. Nate: If conditions beyond the permittee s. control have caused noncompiiance with the CIAWMP or permit, explain on reverse. J J FaFtm MR-1 lagoon Liquid Irrigation fields Record For Recording Irrigation Events on Different Fkelda Farm Owner rx�u� �n V'C a � Facillty Number Operator r , Traci & d # Rate mm/ddi r Crop Type Flold S1xe acres Start The Irri allon Time End The To lnu e # Sprinklers .000raling Operator Initials .'Weather Code "Inepeottons Inf a a � oo ?a q U cO $ it 9' 6 =3o ? L/O .� -3 r�3 rr 7 6'�30 0�.d0/C� .to T1,3a - g'.c o .3r1a 6 :oc> 0" 10 990 fLo ' 99 2 %co I ; 00 2,40 ]a " Weather Codes: C-Clear, PC -Partly CIOUdy, CI -Cloudy. R-Saln, &Snow/Sleet, W-Windy ** persona completing the InIgstion Inspections must Initial to signify that inspections were completer) at least every 120 minutes. Note; if conditions beyond the permitteds control have caused noncompliance with the CAWMP or permit, explain on reverse. 3114M o, 19 i s FORM IRR-1 Lagoon Liquid Irrigation Fields Reoord For Recording irrigation Events on Oitierent Fields Farm Owner .�-� i l r`1 .. ,.c�f� �� faciNly Number�' Operator-- C Tract Field # hate mrnld r Crop T e Field Size acres Ird atlon Tlme 0 Sprinklers er Operator 'Weather Initials Code "Inspections Initla s Start time End Time Total M u s 2rf 73 A 9c�o� S.�o / ff_ n � .� 1J' �[_ � 2S +l �' C i F3 I � �• �Z.! � 11 `-'" � �� Y1�7,�7 �:� o e2 1<P /PO A- � F� ''^7 j �iyrP►% �r ^ Oyj� 1 'c i r ,30 e2 �Irs /�� 1.61 ! I '19Q Weather Codas: C•Ciear, PC -Partly Cloudy, Cl-Cloudy, R-Rein, S-Snowl5leet, W-Windy 31141D3 •` Persons oompleling the Irrigation inspections must initial to signify that inspections were completed at least every 120 minutes. Note:11 canditione beyond the permlltee's control have caused noncompilance with the CA►WN1P or permit, explain on reverse. 9 Foram Inn-1 Lagoon Liquid Irrigation Fields Record For recording Irrigation Events on Different Fields Farm Owner ec \i "J f . t` 4 Fad" Numbe r Operator L� �� c7 D _ 2� " Weather Codes: C-Clear, PC -Partly Cloudy, CI -Cloudy, R-Rain, 9-SnowlSleal, W-Windy - Persona completing the Irrigation inspections must inMal to aignity that Inspections were completed at least every 120 minutes. Note: If conditions beyond the permittee's control have caused noncompliance with the CAWMP or permit, explain on reverse. V14M3 u Report toille Regional Office WATER QUALITY SECTION Page of CHAIN OF CUSTODY (COC) RECORD d NC DENR/DWQ LABORATORY (check one): [XI CENTRAL [ [ ARO [ [ WaRO For Investigation of: Waste Spill -Southern Cross Farm Sample collector (print name) Steve Guyton Christine Blanton and DM-1 forms completed by: - fa Guy ry Sample collector's signature: Field storage conditions and location (when applicable): I RECEIVED ---I Lab Use Only LAB NO, STATION NO. STATION LOCATION I MAY 27 2 DATE SAMPLED TIME SAMPLED NUOF CONTAINERS I {{ EltiiR _ FarEfrl�. G REG'0N�AL 0FRCE A O�rz 1 dos T E nrtA .) r 41 c7 3 Co o � (u e- IgI r � >~ 3 ft3n 5 C/6 143S fin i hed by signat i17 Dat s l Time i :A, R ed by (signatu IAI& ate ADat Time Relinquished by (signature): Date Time Receive y (signature): Time Relinquished by (signature): Date Time Received by (signature): Date Time Method of Shipment (circle one): State Courier fland-delivered Federal Express UPS Other: Security Type and Conditions: Sealed b Bro by: i INTRALABORATORY CHAIN OF CUSTODY - Lab Use Only LAB NUMBERS FROM THROUGH NUMBER BOTTLES ANALYSES REQUESTED RELINQUISHED BY: RECEIVED BY: DATE TIME 39� 3b 59 J fliJ 363950 D ! ;� 2 0� f. hT>� 1 i QANFormslSample ReceivinglCOC form WQ 4/10I01dbs County: SAMESON River Basin CAPE FEAR Report To FROSP Collector: C WANTON Region: FRO Sample Matrix: Wastewate Loc.Typw EFFLUENT Emergency Yes/No COC Yes/No YES REGEAIED JUN 10 2008 DENR-FAYETiEI UEREGIONAL OFFICE Visitl0 Loc. Descr.: UPSTREAM Sample ID'. PO Number # Date Received: Time Received. Labworks LoginlD Date Reported: Report Generated: A"M II Location ID: FROAPSSAMP82-1" I Collect Date: 0512112008- 1Collect Time:: 16:10 I Sample Depth ' Sample Qualifiers and Comments AS30388 8W3713 05/22/2008 06:00 MMATHIS 615108 06/0512008 �/Co /0?, Routine Qualiflers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and ?MDL B1-Countable membranes with <20 colonies; Estimated NE -No established PQL B2- Counts from all fillers were zero. 83- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution 84-Filters have counts of both >60 or SD and < 20; Estimated 01-Holding time exceeded prior to receipt at lab. B5-Too many colonies were present; too numerous to count (TNTG) 02- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The lab analysis was from an unpresarved ar improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory section» 1623 Mali Service Center, Raleigh, NC 27699-1623 (919) 733.3908 Page 1 of 2 NC DWQ, La6oratory Section W§sufts Sample ID AB303$$ Location 4D: FROAPSSAMP82-144 Collect Date: 0512112008 Loc. Descr.-. UPSTREAM Collect Time:: 18:10 Visit ID j GAS tt Analyte Name PqL Result Qualifier Units Anaiysttuate Approved By 1Date Method Reference 5f22108 5122108 MIC BOD, 5-Day in liquid 2.0 2. U mg/L ADEXTER MOVERMAN Melhod Reference APHA52100 5122108 5130MB Conform, MF Fecal In liquid 1 510 134B601 CFU11OOMI PCOTTEN MOVERMAN Method Reference APHA9222D-20th 5122108 5130108 Conform, MF Total In liquid 1 NA Z CFU1100ml PCOTTEN MOVERMAN Method Reference APHA92226-20th 5122108 5=108 NUT NH3 as N In liquid 0.02 0.04 mg/L as N MOVERMAN CGREEN Method Reference Loci 0-107.06-1.1 5128108 614108 Total IQeldshl N as N In liquid 0.2 1.0 mg1L as N GBELK CGREEN Method Reference Lechatt07.06-2-H 612108 814106 NO2+NO3 as N in liquid 0.02 23 mg1L as N MOVERMAN CGREEN Melhod Reference Loci 0.107.04.1-c 5128f08 614108 Phosphorus total as P In liquid 0.02 0.07 mg/L as P MAJAYI CGREEN Method Reference Loc10-115-01-1EF V29108 614108 Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 COUNTY LAmm RIVER BASIN : r REPORT TO Regional Office Other : COLLECTOR(S) : Eslimated ROD Range: Seed: Chlorinated: Station 871,oca lion Code _ Date we=in (yy/pmMd BOD 3 10 mR'L COD High 340 mwL. COD Low 335 mg'L Cobform: Wt Fecal 31616 /100ml Coliform hff To[ai 31504 11001,111 Col form tube Fecal 316l5 1100nd Coliform, Fecal Strep 11673 /100m1 Residut' Total 500 mglL Volatile 305 mg/L Fixed 510 mg1L Residue. Suspended 530 mg7L Volatile 535 nq/L. Fixed 540 my/L pH 403 units Acid Vly to pH 4.5 436 mgl1. Acidity to pH 8 3 435 mgfL, Alkalinity to pH 8.3 415 rtwx Alkalinity to pH 4.5 410 mg/L TOC 680 mg/L Turbidity 76 NFU Coliform Total Tube 1100 nil COKNfE NTS : Ul/ DiViSION OF WATER QUALITY Chemistry Laboratory Report/ Water Quality El pluQia AMBENT QA ❑ ❑ COMPLIANCE CHAIN OF CUSTODY EMERGENCY VISIT rD 01 oC Station Location: Remarks: 6w 3`113 A�MpI F TYPM ❑ STREAM A EFFLUENT LAKE. El INFLUENT ESTUARY ❑ Pate End (yy/mmidd) I Tjme Begin I Time End I Depth - DM, DB, DRM I Value Type- A, I{, L Chloride 940 MgI Chlorophyll a EPA 445,0 modified option uglL Color True 80 cu. Color. (pH) 83 PH. c U. Color: pH 7.6 82 c u, Cyanide 720 mg/I, Fluoride 951 mglL Formaldehyde71880 mgiL Cease and Oils 556 mgli, Hardncaa Total 900 mWL Specific Cond- 95 unthoslcm M$AS 18260 mglL Phenols 32730 ugrl. Sulfate 945 m Sulfide 745 nVL Boron Tannin & Li6min ug/L Hexaval ant Chromium ug/L Bicarbonate mglL Carbonate m&rL Total Dissolved Solids MWL NH7 as N 610 mgft, TKN an N 625 mp/], NO2 plus NO3 as N 630 mSfL P: Total as P 665 mg/L PO4 as P 70507 m8/I, P- 1)Issolved as P 666 L mg1L K-Potass,um MPJI, Cd- Cadmium 1027 ug1L Cr-Ch romiu mToral 1034 ugfL Cu. Copper 1042 ug,'L NI -Nickel 1067 ug/L Pb- Lead 1051 ug/L Zn-'Zinc 1092 uwL V•Vanad,um uWL Ag- Silver 1077 uWL Al- Aluminum 1 105 ugR, Be- Beryllium 1012 ul;L Ca- Calcium 916 m jVL Co- Coball 1037 uglL Fe- Iron 1045 ul 4 Ma -Molybdenum ug%L Sb-Anlimnny upVL Sn-Ter ug/L Tknallium upl, Ti-Titanium uglL. Hg-1631 ng/L Lab �m e3o� e Date RtCe,sed 2 z ' RecReceive Received B�' Data Released Date Reported Compotite-T, S. R 4 Sample Type Li -Lithium 1132 ug/L Mg. Magnesium927 MO. Mn-Manganese 1055 u&1L Na- Sodium 929 m&1L 'Arsenic Total 1002 dg/L Se- Selenium 1147 uWL Hg. Mercury 71900 uS/L Ba-Barium uS(L Organechlorine Pesticides Organophosphorus Pesticides Organonitrogen Pesticides ACid Herbicides Basc/Neutral&Acid Extractable Organ its TPH Diesel Range Purgeabl a Organics (VOA bottle req d) TPH Gasoline Range TPHIBTEX Gasoline Range Phytnplankton Temperature on arrival (aC). Report to: _Fayetteville Regional Office Lab Number: Station Location: A B30388 upstream ample Type: Effluent Date collected: 05/21/08 Affected Parameter(s): Total Coliform NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Sample ID: County: Sampson FROAPSSAMP82-144 Region: Cape Fear Priority: Chain of Custody Collector: Date received: 05/22/08 Date analyzed: Analytical Area (check one): ❑WCH ❑METALS ❑NUT ®MICRO The following anomalies occurred (check all that apply): Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ®Mislabeled as to tests, preservatives, etc. ❑Holding time expired El Prior to receipt in lab ❑After receipt in lab ❑Insullicient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH): ❑improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): Bianton / Gu ton 05/22/08 ❑VOA ❑SVOA ❑PEST ®Quality Control ❑Instrument failure — no reportable results ❑Analyst error — no reportable results ❑ Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards ❑Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Sample bottle was labeled for fecal coliform only, therefore, samples were not run for total coliform. Corrective Action: Suggest resample to collect total coliform data. ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:Z []Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: JPam Cotted VOLM ( Date. 5/27/2008 Lead Chemist Rev�iee%(initial): IWBiOCHEM i©PEST ❑SVOA ❑METALS f t jn ❑VOA Branch Head Review (initial): 1V ^� y " v r QAIQC Review (initial)- Logged into database by (initial): QATF slr.abomlory\SAR 10/23101dbs Report to: _Fayetteville Regional Office Lab Number: AB30388 Station Location: upstream ample Type: Effluent Date collected: 05/21/08 Affected Parameter(s): Fecal Coliform NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Sample ID County: Sampson FROA PSSA M P82-144 Region: Cape Fear Priority: Chain of Custody Collector: Bianton / Gu ton Date received: 05/22/08 Date analyzed: 05/22/08 Analytical Area (check one): ❑ W CH ❑METALS ❑NUT MMICRO The following anomalies occurred (check all that apply): ❑Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): ❑VOA ❑SVOA ❑PEST MQuality Control ❑Instrument failure — no reportable results ❑Analyst error — no reportable results ❑Surrogates []None added ❑Recovery outside acceptance limits []Spike recovery ❑None added ❑Rccovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards 9131ank contamination []QC data reported outside of controls (e.g., QCS, LCS) El Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Two blanks were run after first series of samples (including A1330388), both were contamined with counts of 19 and 4 respectively. Values are estimates since blank contamination was evident. Corrective Action: ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:B6 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: Lead Chemist Review (initial): U213I0CHEM ❑PEST' ❑METALS �'(� S�L�❑VOA Branch (dead Review (initial):' QA/QC Review (in- --,\ QA51= s\Laboratory45 AR Date. 5/27/2008 EISVOA Logged into database by (initial): IW23101 dbs z La 6orato ection esuCts County: SAMPSON Sample ID: A830390 River Basin CAPE FEAR �p� ArFgO PO Number # OW3715 Report To FROSP �O q Date Received: 05/2212008 y Time Received: 08:00 Collector: Region: C MANTON FRO } �� a Labworks LoginlD MMATHIS UN J 1, Date Reported: 61510e Sample Matrix: Wastewater Loc. Type: EFFLUENT �ltERfG101lAlOWIIA Report Generated: 06/05/2008 Emergency Yes/No pENR-fAY�1iEti COC Yes/No YESVisitln f Q � � Loc.Oescr.: SOURCE � ,, �11 1 0 u Location Q FROAPSSAMP82-144 Collect Date: 0512112008 Coliect Time:: 116:35 Sample Depth Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < POL and >MDL 131-Countable membranes with <20 colonies; Estimated NE -No established PQL 132- Counts from all filters were zero. P-Elevated PQL due to matrix interference and/or sample dilution B3- Countable membranes with more than 60 or 80 colonies; Estimated Q1-Holding time exceeded prior to receipt at lab. B4-Filters have counts of both >60 or 80 and < 20; Estimated 85-Too many colonies were present; too numerous to count (TNTC) 02- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected J6-The fob analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound N1-The component has been tentatively identified based on mass spectral library search and has an estimated value LAB Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Page 1 of 2 - NC ��WQ Laboratory Section �esuCts Sample ro AB30390 Location ID: FROAPSSAMP82-144 Collect Dale'. 05121/2008 Loc. Descr.: SOURCE Collect Time:: 16:35 Visit ID CAS # Analyte Name PCIL Result Qualifier units AnmysvUate Approved by mate Method Reference 5,22108 522108 MIC BOO, 5-Day In liquid 2.0 100 mg/L ADEXTER MOVERMAN Method Reference APHAS2108 522108 5130/D8 Conform, MF Feel In liquid 1 600000 B5B6Q1 CFL11100mi PCOTTEN MOVERMAN Method Reference APHA9222D-20th 522108 5/30/08 Conform, MF Total In liquid 1 NA Z CFLl/100ml PCOTTEN MOVERMAN Method Reference APHA9222B.20th 522108 5130108 NUT NH3 as N In Ilquld 0.02 160 mg/L as N MOVERMAN CGREEN Method Reference LaclO-107.06-1ti1 52a108 614108 Total igeldshl N as N in liquid 0.2 190 mg/L as N GBELK CGREEN Method Reference Lechet107.06.2-1-1 529/D8 614108 NO2+NO3 as N In liquid 0.02 0.12 mg1L as N MOVERMAN CGREEN Method Reference Lac10.107-1)4-1•c Sn8/08 61V08 Phosphorus total as P In liquid 0.02 25 mg/L as P MAJAYI CGREEN Method Reference Lec10.115-01.1EF 5129/08 6/4108 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27899-1623 (919) 733-3908 Page 2 of 2 r� Cz DIVISION OF WATER QUALITY �JJ�����jj�� O3 Chemistry Laboratory Report! Water Quality LabN�hnber L@11BQY SAMPLE TYPE Dare Receive COUNTY Time Receive HIVER BASIN: AMBIENT QA STREAM kjEFFLUENT Received 8y REPORT TO r%/�/C�Regional Office COMPLIANCE CHAIN OF CUSTODY LAKE INFLUENT Other EMERGENCY VISIT m ESTUARY Data Released COLLECTOR(S) C� Dom Rtponed . Estimated BOD Range: Station CC ill Seed: Chlorinated: Remarks: Station 1llLocation Code Date 1 in (yy! !dd) Date End (yy/mmldd) "rne Ii�pjn Time End Ilnpth - Dyt, DB, DBM Value Type - A, If, 1, COmpo,ite•T, 5, B Sample Type FWDAKSAlowZ I BOD 310 ml /L COD High 340 mg/L COD Low 335 mg/L Cu I Sorm: MT Fecal 31616 / 100ml Coliform. MY Total I I Sk 1100m1 Coldorm'tube Fecal 31615 /looml ColiformFecal Strep 31673 1100ml Residue. Total 500 mg/L Volatile 505 mg$, Fixed 510 orl Rcidtw Suspended 530 mg/L Volelile 535 mWL Fixed 540 mwL. pH 403 units Acidity to pH 4.5 436 mglL Acidity to p118.3 435 mWL Alkahnity to PH 8.3 415 mg/L Alkalinity to pH 4 5 410 mg/L TOC 680 mWL Turhidiry 76 NTU Cal ifomt Total Tube 1100 ml COMMENTS : Chloride 940 ❑s3/L Chlorophyll a EPA 445,0 modifted Option uvfL Color: True 80 c U. Color.(PH) 83. pH� c.u, Color: pH 7,6 82 c.u, Cyanide 720 mg L Fluoride 951 mg/L Formaldehyde 71890 mg/L Grease and OOs 556 111g1L Hardness Total 900 mp/L. Specific Cond. 95 urnhos/cm MBAS 38260 mgJL Phenols 32730 ug/L Sulfate 945 mg(L Sulfide 745 1110, Boron Tannin & Lignin ug!L Hexavalent chromium ug L Bicarbonate mWL Carbonate mg/L Total Dissolved Solids mg/L NH3 as N 610 mWL TKN an N 625 n 1. NO2 plus NO3 as N 630 mVL P: Iotal as P 665 mg/L PO4 as P 70507 mg/L P, Dissolved as P 466 1 mb/l. K-Potassium mpjL Cd- Cadmium 1027 uWL Cr-Chromium Total 1034 ugIL Cu- Copper 1042 ug/L Ni-Nicktl 1067 u6/L Ph- Lead 1051 uwL Zn- Zinc 1092 ug/l, V-Vanadium ug/L ' AS. Silver 1077 ug/L Al. Aluminum l l05 uW4. Be- Berylhum 1012 uW'L Ca- Calcium 916 ml Co -Cobalt 1037 ug/L Fc-Iron 1045 ull MG -Molybdenum ug1L S b-Antimony "prL Sn-Tin ug/L TI-Tltall ium ug/l. Ti-Titanium uil Hg-1631 nglL Li -Lithium 1132 u8lL Mg- Mapeaium 927 mg/L Mn-Manganese 1055 ugjL Na- Sodium 929 mgA- Arsenic Total 1002 ug/L Se- Selenium 1147 ugJL Hg- Mercury 71900 uW'L Ba-Barium u" Organochlorine Pestieides Organo hosphorus Pesticides Organoni«ogen Pestioide6 Acid Herhirndes 5&sdNeulral&.Aeid Extractable Orgn¢s TPH Dtscl Range Purgeable Organics ( VOA bottler 'd) TPH Gasoline Range TPHIBTEX Gmohre Range Phytoplankron Temperatuve on arrival Report to: _Fayetteville Regional Office NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: AB30390 Station Location: Source ample Type: Effluent Date collected: 05/21/08 Affected Parameter(s): Total Coliform Sample ID: FROAPSSAMP82-144 County: Sampson Region: Cape Fear Priority: Chain of Custody Collector: Bianton / Guyton Date received: 05/22/08 Date analyzed: 05/22/08 Analytical Area (check one): ❑WCH ❑METALS ❑NUT ®MICRO The following anomalies occurred (check all that apply): WSampies ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace []Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fteldshecl ®Mislabeled as to tests, preservatives, etc. ❑Holding time expired []Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record p1l): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): ❑VOA ❑SVOA [-]PEST ❑Quality Control El Instrument failure — no reportable results ❑Analyst error — no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards []Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insuffcient sample volume Comments: Sample bottle was labeled for fecal coliform only, therefore, samples were not run for total coliform. Corrective Action:Suggest resample to collect total coliform data. ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:Z ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: �. Form completed by: Pam Lead Chemist Review (initial): �BIOC14EM (^0 DPEST METALS A�10 ©VOA Branch Head Review (initial): QA/QC Review (initial fS11-3 4YOjy Date: 5/27/2008 EISVOA Logged into database by (initial): QMFormsk[AboratoryLSAR 1 3/61dbs Report to: _Fayetteville Regional Office Lab Number: AB30390 Station Location: Source ample Type: Effluent Date collected: 05/21/08 Affected Parameter(s): Fecal Coliform NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Sample ID: County: Sampson FROAPSSAM P82-144 Region: Cape Fear Priority: Chain of Custody Collector: Bianton / Cuyton Date received: 05/22/08 Date analyzed: 05/22/08 Analytical Area (check one): ❑ WCH ❑ METALS []NUT ®MICRO The following anomalies occurred (check all that apply): ❑Samples []improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheel ❑Samples received, but not listed on fieldshect ❑Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction []Sample bottle broken in lab - no reportable results ❑Other (specify): ❑VOA ❑SVOA ❑PEST OQuality Control ❑instrument failure — no reportable results ❑Analyst error — no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits El Failed to meet criteria for precision ❑Internal standards ®Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) El Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Two blanks were run after first series of samples (including A830390), both were contamined with counts of 19 and 4 respectively. Values are estimates since blank contamination was evident. Corrective Action: ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:136 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: am Cone ~ Date: 5/27/2008 Lead Chemist Review (initial): Q9610CHF,M l%,>._ ❑PEST ❑SVGA []METALS hV0 [-]VOA Branch Head Review (initial): tF�"��pp"�"�� v ss , r0 QA/QC Review (initi 5��� /O Logged into database by (initial): QAlrormAAb"orySSAR l/ I OP_3/G1(1b5 ' County: SAMPSON River Basin Report To FROSP Collector: CC BIANTON Region: FRO Sample Matrix: Wastewater Loc. Type:. EFFLUENT Emergency Yes/No COC Yes/No YES JUN 18 2008 DENR - FATIMILLE.REGIONAL OFRCE Location ID: FROAPSSAMP82-144 Q� wAr�,�pG a -c ViSItID Loc. Descr.: CONFLUENCE Collect Date: 06/21/2008 Collect Time:: 16:15 Sample Qualifiers and Comments Sample ID: PO Number # Date Received: Time Received: Labworks LoginlD Date Reported: Report Generated: ef—'41 Sample Depth AB30389 8W3714 05/2212008 08:00 MMATHIS 6110/08 06/10/2008 &//o/og Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations 131-Countable membranes with <20 colonies; Estimated N3-Estimated concentration is < PQL and >MDL NE -No established PQL 132- Counts from all filters were zero. P-Elevated PQL due to matrix Interference and/or sample dilution B3- Countable membranes with more than 60 or 80 colonies; Estimated 01-Holding time exceeded prior to receipt at lab. BG-Filters have counts of both >60 or 80 and < 20; Estimated Q2- Holding time exceeded following receipt by lab B5-Too many colonies were present; too numerous to count (TNTC) PQL- Practical Quantitation Limit -subject to change due to Instrument sensitivity J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated U- Samples analyzed for this compound but not detected J3-The sample matrix interfered with the ability to make any accurate determination; Estimated X1-Sample not analyzed for this compound J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated W-The component has been tentatively identified based on mass spectral library search and has an estimated value I AR Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 .rVC DWQ Laboratory Section 1§sufts Sample I D AB30389 Location ID: FROAPSSAMP82-1" Collect Date: 06/21/2008 Loc. Oescr.: CONFLUENCE Collect Time:: 16:15 Visit ID Analyte Name POL Result Qualifier Units AnalystlDate Approved By /Date LAB - Sample temperature at recelpt by lab 1.9 °C DSAUNDERS MMATHIS Method Reference 5122/08 5122108 MIC BOO, 5-Day In liquid 2.0 21 mg/L ADEXTER MOVERMAN Method Reference APHA5210B 5122108 5130100 Coliform, MF Fecal in liquid 1 6000 B5B601 CFU1100ml PCOTTEN MOVERMAN Method Reference APHA9222D-20th 5122108 5/30108 Collform, MF Total In liquid 1 NA Z CFU/100m1 PCOTTEN MOVERMAN Method Reference APHA9222B-20th 5122/08 5130/08 NUT NH3 as N in liquid 0.02 0.46 mg1L as N MOVERMAN CGREEN Method Reference LBC10.107-06-1-J 5/28108. 614/08 Total KJeldahl N as N in liquid 0,2 4.6 J2 mg/L as N GBELK CGREEN Method Reference Lachat107-06-2-H 613108 6/10/08 NO2+NO3 as N In liquid 0.02 18 mg/L as N MOVERMAN CGREEN Method Reference Lac10-107-04-1-c 5128108 814/08 Phosphorus total as P In Ilquld 0,02 1.0 mg/L as P MAJAYI CGREEN Method Reference Lac10-115-01-lEF 5129108 614108 Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 DIVISION OR WATER QUALITY Chemistry Laboratory Report! Water Quality SAMPLE TYPE COUNTY eBl4ar�i RIVER BASIN t AMBIENT QA STREAM FFLUENr / REPORT TO Regional Office El COMPLIANCE � CHAIN OF CUSTODY LAKE INFLUENT Other EALERGENCY visa m ESTUARY COLLECTOR(S) ❑ Estimated NOD Range; Station {,ocatioa: ' Seed: Chlorinated: Remarks: Station AILocatlon Cade Data vegin (y)Immldd) Dale End fyylmmldd] Tjrge Negin I Time End I Depth - DM, DR, DBM Value Type -A, H, L BOD 3 10 mWL COD High 340 mg/L COD Lew 335 mgrL Co6form, Leff Fecal 11616 1100m1 Colifams MF Total 31504 1100ml Cohfoms: tube Fecal 31615 110017111 Coltform Feca! Strap 31673 /loom] Residue: Total 500 mWL Volatile 505 mp/L Fixed 510 mWL Residue: Suspended 530 niwt, Volatile 535 mg/L.. Fixed 540 mg1L pH 407 units Acidity to pH 4,5 436 mgL Acidity to pH 9 3 435 awl. Alkalinity to pH 8.3 415 mr/L Alkalinity to pH 4 5 410 mgfL TOC 680 m?/L 'rurbiday 76 NTU Conform Total Tube AGO nil CONt"IENTS : Chloride 940 mglL Chlorophyll a EPA 443 0 modified option ugr1. Cal or. True 60 c U. Color: (pH ) 83 PH. c.0 Calar, pH 7.6 82 c U. Cyanide 720 mWL Fluoride 951 mWL Formaldehyde 71880 mwL Grease and Oils 556 niWL Hardness Total900 mg1L Specific Cond. 95 umhoslem MBAS 18260 m6/L Phenols 32710 ucf1. Sul rate 945 mgll. Sulfide 745 mgrL Boron Tannin & Ligtin uWL Hexavaleni Chromium ugrL Bicarbonate mgrL Carbonate mWL Total Dissolved Solids mg/1- NH3 as N 6 10 mglL TKN an N 625 mgvL NO2 plus NO3 ss N 630 mglL P: Total as P 665 PO4 as P 70507 mglL P. Dissal\,ad as P 666 ra611- K-Pota3sium mWL Cd- Cadmium 1027 uglL Cr•Chrami a m.Total 1034 ug(L. Cu- Co per 1042 up/L Nehrick el 1061 ug/L, Pb- Lead 1051 ugfL Zn- Zinc 1092 up! V-Vanadium uWL AS -Silver 1077 ug/L Al- Aluminum 1 105 ug'L Be- Beryllium 1012 ug7L Ca- Calcium 916 mg/L Cc -Cobalt 1037 u811. Fe- Iron 1045 ug/L, Ma -Ma lybdenum ug(L Sb-Antimony ugrL Sn-Tin ul;l. TT-TTnaI Iium ug/L Ti-Tnaniurn ugrL Hg.1631 „WL Date Receive �22 Time Recei Received B Data Released Dare Reported. Coin posi te-T, S,01 Sample Type Li -Lithium 1132 uSIL MS. Magnesium 927 mel. Mn-Manganese 1055 uglL Na- Sodium 929 Arsenic.Total 1002 ug/L Se -Selenium 1147 ug/L Hg- Mcreuny 71900 uWL. Be -Barium ug/L Orlpnochlorine Pealicicics Organo hos horus Pesticides Orpranitrogen Pesticides Acid Herbicides Base[Nculral& Acid Extractable Organics TPH Diesel Range Purgeable Organics (VOA bottler 'd) TPH Gasoline Range TPW13TFX Gasoline Range Phytoplankton OOA Temperature on arrisrel ('C): 4 Report to: _ FROSP NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: AB30389 Sample ID Station Location: C�Iu County: SAMPSON Sample Type: Date collected: 5/21/08 Affected Parameter(s): WASTEWATER TKN Priority: _ Date received: Analytical Area (check one): ❑WCH ❑METALS ®NUT ❑MICRO The following anomalies occurred (check all that apply): ❑Samples ❑Improper container used []VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab []Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly [:]pH out of range (record pH): ❑improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): 5/22/08 rp'D"s 5A-++ 22- lye{ Region: FRO Collector: C BIANTON Date analyzed: 0 9 C- ❑VOA ❑ WARO [-]PEST ❑SVOA Quality Control El Instrument failure— no reportable results ❑Analyst error — no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards ❑Blank contamination ®QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to! ❑Insufficient sample volume Comments: LFB RESULT REPORTED AT 118% RECOVERY, OUTSIDE OF ACCEPTNESS RANGE OF (90% TO l 10%). Corrective Action:. ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:J2 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: _ Form completed by: O W ENDOL Lead Chemist Review (initial): IOCHEM METALS []PEST ❑VOA _ Branch Head Review (initial ' — (, -;L o ° r /J QA/QC Review (init' QA'Xor=s LabaratoryLSAR (� Date: 6/4/2008 ❑SVGA Logged into database by (initial): 10r-3101 dbs Report to: _Fayetteville Regional Office NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: AB30389 Station Location: Confluence ample Type: Effluent Date collected: 05/21/08 Affected Parameter(s): Total Coliform Sample ID: County: Sampson Priority: Chain of Custody Date received: 05/22/08 Analytical Area (check one): ❑ WCH ❑METALS [-]NUT ®MICRO The following anomalies occurred (check all that apply): Q9samples ❑Improper container used []VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ®Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity []Sample not chemically preserved properly ❑pH out of range (record pH): El Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): FROAPSSAMP82-144 Region: Cape Fear Collector: Bianton / Guyton _ Date analyzed: 05/22/08 ❑VOA ❑SVOA ❑PEST Quality Control ❑ Instrument failure - no reportable results ❑Analyst error - no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision [-]Internal standards ❑Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Irival id instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Sample bottle was labeled for fecal coliform only, therefore, samples were not run for total coliform. Corrective Action:Suggest resample to collect total coliform data. ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:Z ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: Pam Cotten! UOLM ( 10T Date. 5/27/2008 Lead Chemist Review (initial): �BIOCHEM []PEST ❑SVOA ❑METALS VV ❑VOA Branch Head Review (initial): S '�° QA/QC Review ' (initialp -S�� Logged into database by (initial): QAXFomrsll_ahomtory\SAR ] 0l23101 dbs Report to: —>:ayetteville Regional Office NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: Station Location A 830389 Confluence ample Type: Effluent Date collected: 05/21/08 Affected Parameter(s): Fecal Coliform Sample ID: FROAPSSA M P82-144 County: Sampson Region: Cape Fear Priority: Chain of Custody Collector: Bianton / Guyton Date received: 05/22/08 Date analyzed: 05/22/08 Analytical Area (check one): ❑ WCH ❑METALS ❑NUT ®MICRO The following anomalies occurred (cheep all that apply): ❑Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑Mislabeled as to tests, preservatives, etc. ❑I folding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): ❑VOA ❑SVGA ❑PEST XQuality Control El Instrument failure — no reportable results El Analyst error — no reportable results ❑ Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards ®Blank contamination ❑QC data reported outside of controls (e.g„ QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Two blanks were run after first series of samples (including A1330389), both were contamined with counts of 19 and 4 respectively. Values are estimates since blank contamination was evident. Corrective Action: ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:B6 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: +Pam Cone -VLM t_-3XVj Date: 5/27/2008 Lead Chemist Review (initial): CMDIOCHEM MO ❑PEST ❑SVGA [IMETALS ❑VOA Branch Head Review (initial): QA/QC Review (initi t24�E::-C 0610jo Cogged into database by (initial): QASFM"s\ aboMory\SAR E0123/0Idbs County: SAMPSON Sample ID: AB30389 River Basin Report To 0FWA7-�c QG PO Number# SW3714 FROSP �0� Date Received: 05/2212008 Collector: C BIANTON Time Received: 08:00 Region: FRO p Y Labworks LoginiD MMATHIS Sample Matrix: Wastewater Date Reported: 6/10I08 Loc. Type: EFFLUENT Report Generated: 06110/2008 Emergency Yes/No COG Yes/No YES Visitl0 e,- //d Q g Loc. Descr.: CONFLUENCE 1 Location 0: FROAPSSAMP82-144 I Collect Date: 05/21/2008 I Collect Time:: 16:16 1 Sample Depth I Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL B1-Countable membranes with <20 colonies; Estimated NE -No established PQL B2-Counts from all filters were zero. 63- Countable membranes with more than 60 or 80 colonies; Estimated P-Elevated PQL due to matrix interference andlor sample dilution 134-Filters have counts of both >60 or 80 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab. B5-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quantitatian Limit -subject to change due to instrument sensitivity U- Samples analyzed for this compound but not detected J3-The sample matrix interfered with the ability to make any accurate determination; Estimated X1- Sample not analyzed for this compound J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated N1-The component has been tentatively identified based on mass spectral library search and has an estimated value I AR Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 1 of 2 NC WQQ Laboratory Section 1�esults ampe AB30389 Location ID: FROAPSSAMP82-144 Collect Date: 05121/2008 Loc. Obscr.. CONFLUENCE Collect Time:: 16:15 Visit ID Analyte Name PQL Result Qualifier Units Analyst/Date Approved By !Date LAB Sample temperature at receipt by lab 1.9 'C OSAUNDERS MMATHIS Method Reference 5122/O8 5=08 MIC BOD, 5-Day in liquid 2.0 21 mg/L ADEXTER MOVERMAN Method Reference APHA5210B 5122108 5/30108 Coliform, MF Fecal in liquid 1 6000 B58601 CFU/100ml PCOTTEN MOVERMAN Method Reference APHA9222D-20th 5122/08 5130108 Colform, MF Total In liquid 1 NA Z CFU1100m1 PCOTTEN MOVERMAN Method Reference APHA922213-20th 5/22/08 5/30108 NUT NH3 as N In Ilquld 0.02 0.46 mg1L as N MOVERMAN CGREEN Method Reference Lac10.107-06.1-J 5128/08. 614108 Total KJeldahl N as N In liquid 0.2 4.6 J2 mglL as N GBELK CGREEN Method Reference Lachat107-06.2-H 613108 6110/08 NO2+NO3 as N in liquid 0.02 18 mg1L as N MOVERMAN CGREEN Method Reference LacIO-107.04-1-c 5128108 614108 Phosphorus total as P In liquid 0.02 1.0 mg1L as P MAJAYI CGREEN Method Reference Lec10.115-01-1EF 5129108 514105 Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27699-1623 (919) 733-3908 Page 2 of 2 .. COUNTY RIVER BASIN REPORTTO /�� Regional Office Other COLLECTORS}; aMMTM z t�(j Estimated 801) Ratige Seed: Chlorinated: Station NfLocmion Code Date Wgin (y)hnmldd) Date End (yylmmldd) ROD 3 10 .&I COD H,0 340 mglL COD Low 335 mglL Cohform MF Fecal 31616 1100mE Colifomt MFTotal 31504 1100ml Cohform-tube Fecal 31615 /100ml Cohform Fecal Strep 31673 1100m1 Residue Total 5C0 my/L Volatile 505 n*L. Fixed 510 mgI, Rmdue, Suspended 530 nWL Volatile 335 m8fl- Pucd 540 mv1L pl 1403 umts Acidity to pH 4 5 436 mRA, Acidity to pH 8-3 435 mWL Alkalinity to pH 8.3 415 ntnJL Alkshrioy to pH d 5 AM mWL TOC 680 mWL Tutbidny 76 NTU Cal ife m Total Tuhe 1100 till COMWNTS : cez--) DIVISION OF WATER QUALITY Chemistry Laburatory Repartl Water Quality SAMPLE TYPE PRIORM' AMRMNT QA STREAM COMPLIANCE CHAIN OF CUSTODY ID LAKE EMERGENCY ��V^^II�SI�T -1^0 � ESTUARY Station Location: n Remarks: Time Enid I Depth - DM, OB, DBM Chloride 940 mgA. Chlorophyll a EPA 445 0 modified option ug1L Color: True 80 c U. Color: (pH) 83 pH- c U.- -Color, pH 7,6 82 c.u, Cyanide 720 my1L. Fluoride 951 mgfL Formaidehyde 71880 m L Grease and Oils 556 n4VL Hardness Total 900 mWL Specific Cond. 95 umhos/cm MBAS 38260 mg/L Phenols 92736 uSIL Sul file 945 mg/L Sulfide 745 mg/L Boron Tannin & Ligtin ugJL, Htxa+ralent Chromium ugfL Btcarbonare mg3. Carbonate mg/L, Total Dissolved Solids nWL Received B Date Receis'e . -2Z Time Recei ye UFFLUEYI' Value Type - A, 11, L I corn porniaT, S, B ( Sample Type NH3 as N 610 tngR, TKN an N 625 mg/L NO2 pius NO3 as N 630 mg1L P: Total as P 665 MOIL PO4 as P 70507 mg1L P' Dissolved as P 666 rrmg/L K-Potassium mg1L Cd- Cadmium 1027 u64L. Ct-ChrotlriumTotai L 1034 u Cu- Copper 1042 u L N,-Nickel 1067 UiX Pb- Lead 1051 ug/L Zn-Zinc1092 ugrL. V-Vanadium ugfL Ag-Silver 1077 ug1L AI -Aluminum 1105 uprL Be- Beryllium 1012 ug1L, Ca- Calcium 916 mWL -Cobalt 1037 ug/L Fe -Iran 1045 ugrL Me -Molybdenum ug/L Sb-Antimon u L Sn-Tin ug1L TI-Thailium ue/L Ti-Titanium ug/L Hg-1631 ng/L Li -Lithium 1132 ug/L Mg- Magnesium 927 rng11. Mn-Manganese 1055 uglL Na- Sodium 929 mg/L Auenic.Tote11002 ug1L Se- Selenium 1 147 "WL Hg- Mercury 71900 uglL BA -Barium ug+4 Organochlorine Pesticides Organo has horns Pesticides Organanitrogen Pesticides Acid Herbicides Base/Neutral&Acid Extractable Organ ic3 TPH Mesel Range Purgeable Organics (VOA bottle req'd) TPH Gasoline Range TPWBTEX Gasoline Range Phytoplankton Temperature on attival cCl: 6 Li -Lithium 1132 ug/L Mg- Magnesium 927 rng11. Mn-Manganese 1055 uglL Na- Sodium 929 mg/L Auenic.Tote11002 ug1L Se- Selenium 1 147 "WL Hg- Mercury 71900 uglL BA -Barium ug+4 Organochlorine Pesticides Organo has horns Pesticides Organanitrogen Pesticides Acid Herbicides Base/Neutral&Acid Extractable Organ ic3 TPH Mesel Range Purgeable Organics (VOA bottle req'd) TPH Gasoline Range TPWBTEX Gasoline Range Phytoplankton Temperature on attival cCl: 6 Report to: —Fayetteville Regional Office NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: Station Location: AB30389 Confluence ample Type. Effluent Date collected: 05/21/08 Affected Parameter(s): Total Coliform Sample ID: County: Sampson Priority: Chain of Custod Date received: 05/22/08 Analytical Area (check one): ❑WCH ❑METALS ❑NUT ®MICRO The following anomalies occurred (check all that apply): Samples El improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on tieldsheet ®Mislabeled as to tests, preservatives, etc_ ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results []Other (specify): FROAPSSAMP82-144 Region: Cape Fear Collector: Bianton / Ga ton Date analyzed: 05/22/08 ❑VOA ❑SVOA [-]PEST CRQuality Control ❑Instrument failure — no reportable results ❑Analyst error-- no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits EIS pike recovery ❑None added ❑Recovery outside acceptance limits [Railed to meet criteria for precision ❑Intemal standards ❑Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration []Elevated detection limits due to: ❑Insufficient sample volume Comments: Sample bottle was labeled for fecal coliform only, therefore, samples were not run for total coliform. Corrective Action:Suggest resomple to collect total coliform data. ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:Z ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: Pam Cotten tfMM (1O$ Date: 5/27/2008 Lead Chemist Review (initial): MBIOCHEM "`q __ []PEST ❑SVOA []METALS (WO {/ ❑VOA Branch Head Review (initial): QA1QC Review (initial) - Lagged into database by (initial): �3 QA%Form LaborxorylSAR NOW/Olr$s Report to: -Fayetteville Regional Office NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: Station Location: ample Type: A B30389 Confluence Effluent Date collected: 05/21/08 Affected Parameter(s): Fecal Coliform Sample ID: County: Sampson FROAPSSAMP82-144 Region: Cape Fear Priority: Chain_ of Custody Collector: Date received: 05/22/08 Date analyzed: Analytical Area (check one): ❑WCH ❑METALS ❑NUT ®MICRO The following anomalies occurred (check all that apply): ❑Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldshect ❑Samples received, but not listed on fieldsheet ❑Mislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab' ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved property ❑pH out of range (record pH): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): Bianton / Cuyton 05/22/08 _ ❑VOA ❑SVOA ❑PEST MQuality Control ❑Instrument failure - no reportable results ❑Analyst error -no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards ®Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Two blanks were run after first series of samples (including A1330389), both were contamined with counts of 19 and 4 respectively. Values are estimates since blank contamination was evident. Corrective Action: ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:136 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: Form completed by: Pam Cotten `IG-01 L-MaA) Date: 5/27/2008 Lead Chemist Review (initial) ERBIOCHEM Ma []PEST❑SVOA METALS f\v D ,/ ❑VOA Branch Head Review (initial): i=7d�"4 QA/QC Review (initi �--:r / Logged into database by (initial): QAVt: s"borgaw)ASAR l/ tazzroiens County: SAMPSON River Basin Report To FROSP Collector: C BIANTON Region: FRO Sample Matrix: W sty ewater Loc. Type: EFFLUENT Emergency Yes/No COC Yes/No YES O�O�W,Ar�EgQG "'U' .7. 1 VisitlD Loc. Descr.: DOWNSTREAM Sample ID: AB30391 PO Number # 8W3716 Date Received: 06/22/2008 Time Received: 08:00 Labworks LoginlD MMATHIS Date Reported: 6/10108 Report Generated: 06/10/2008 11 Location ID: FROAPSSAMP82-144 I Collect Date'. 05/2112008 Collect Time:: 16:45 j Sample Depth I Sample Qualifiers and Comments Routine Qualifiers For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MDL B1-Countable membranes with <20 colonies; Estimated NE-Na established PQL 82- Counts from all filters were zero. P-Elevated PQL due to matrix interference and/or sample dilution B3- Countable membranes with more than 60 or 80 colonies; Estimated Q1-Holding time exceeded prior to receipt at lab. B4-Filters have counts of both >60 or 80 and < 24; Estimated 02-Holding time exceeded following receipt by lab B5-Too many colonies were present; too numerous to count (TNTC) PQL- Practical Quantitation Limit -subject to change due to instrument sensitivity J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated J3-The sample matrix interfered with the ability to make any accurate determination; Estimated X 1 Samples analyzed for this compound but not detected -Sample not analyzed for this compound J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated N1-The component has been tentatively identified based on mass spectral library search and has an estimated value IAR Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 733-3908 Page 1 of 2 AC DWQ Ga6oratory Section 1f suits Sample 115 A1930391 Location ID: FROAPSSAMP82-144 Collect Date: 05/21/2008 Loc. Descr.: DOWNSTREAM Collect Time:: 16:45 Visit 16 Ana yte Name PQL Result Qualifier Units AnalysYDate Approved By 1 ate LAB - Sample temperature at receipt by lab 1.9 °C DSAUNDERS MMATFIIS Method Reference 5/22/08 5122/OB MIC SOD, 5-Day In liquid 2.0 27 mg/L ADEXTER MOVERMAN Method Reference APHA52105 5122108 5130108 Coliform, MF Fecal in liquid 1 6000 195121601 CFU/100mi PCOTTEN MOVERMAN Method Reference APHA9222D-20th 5/22108 5/30/08 Coliform, MF Total in liquld 1 NA Z CFU/100ml PCOTTEN MOVERMAN Method Reference APHA92226-20th 5122108 5/30108 NUT NH3 as N In liquid 0.02 2.6 mg/L as N MOVERMAN CGREEN Method Reference LaciO-107-06-1-,1 5/2M8 614/08 Total Kjeldahl N as N in liquid 0.2 12 mg/L as N GBELK CGREEN Method Reference Lnchat107.06-2-H 5129108 e14108 NO2+NO3 as N In liquid 0.02 11 mg/L as N MOVERMAN CGREEN Method Reference Lac10-107-04-1-c 613108 8/10/08 Phosphorus total as P In liquid 0.02 2.8 mg/L as P MAJAYI CGREEN Method Reference Lac10-115-01-1EF 5129108 ' 614108 Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919)•733-3908 Page 2 of 2 COUNTY RIVER BASIN REPORT TO Regional Office Other : COLLECTOR(S) Fsiimated ROD Range: Seed: Chlorinated: Station p/Luca Goo Code _ Date Begin (yylpnmldd) I Date End (yylmmldd) BOD 310 mg/L COD High 340 m8/1- COD Law 335 m$1L Coliform_ MF Fecal 31616 1100ml Coliform MF Total 31504 1t00m1 Colifomr. tube Fecal 31615 11 OOml Coliform Fecal Strep 31673 1100ml Residue: Total 500 mWL. Volatile 105 mg!L Fixed 510 T LL Residue Suspended $30 mv/L Volatile 535 mg/L Fixed 540 mglL pH 401 units Acidity to pH 4.5 4)6 mg/L Acidity to pH 8.3 435 m87L Alkalinity to pH 8.3 415 mp/L- Alkalinity to pH 4.5 410 M91L TOC 680 mg/L Turbidity 76 NTU Coiiform-r=l Tube 1100 ml COMMENTS: DIVISION OF WATER QUALM Chemistry Laboratory Report / W ater Quality SAMPLE TYPE PRIORITY A;',IBIETT QA STREAM COMPLIANCE CHAIN OF CUSTODY LAKE EMERGENCY VISff ID ESTUARY Station Location!.�/�]�J�]'1 Remark.,: Tipte Begin ^_ l Time End Depth - DM, DR, DBM r j Chloride 940 mSlL Chlorophyll a EPA 445.0 modified option ug/L Color: True 80 au. Color: (pH ) 83 pH- c.u. Color: pH 7.6 82 eu. Cyanide 720 mwL Fluoride 951 mg/L Fomtaldeh de 71880 mgR- Greene and Oils 556 mgtL. Hardness Total 9OU mgfL Specific Cond. 95 mnhos/cm MBAS 39260 mg/L Phenols 32730 ugt Sulfate 945 mglL Sulfide 745 mplL Boron Tannin & Ligtin ug/L Hcxavalent Chromium ug/L Bicarbonate mg/L. Carbonate m Total Dissol+ d Solid., mg/l, sw-�sq((o EFFLUENT nJFLuENT Value Type - A, II, L NH3 as N 610 mglL TKN an N 625 rrtglL NO2 plus NO3 as N 630 mg(L, P: Total as-P 665 PO4 as P 70507 nWL P: Dissolved as P 666 I mglL K-Potassium -A Cd- Cadmium 1027 ug/L Cr-Chromium:Total 1034 uWL Cu- Copper 1042 41. M-Mcket 1067 uty`L, Pb- Lead 1051 ug(L, Zn- Zinc 1092 ug/L V-Vanadium ug/L AS- Silver 1071 uglL Al- Aluminum 1105 _upfL Be- Beryllium 1012 ug/L Co- Calcium 916 mg/L. Co. Cobalt 1037 ug1L, Fe- lroo 1045 uWL Mo-Molvbdenum uglL- Sb-Antimony -uwL Sn-Tin ug'L TI-Thal I iuno ug/L Ti-Titanium uµ(L kg-1631 n um r Dare Receive _ 1Z Time Receive Recei.ed By Data Released Date Reported Composite-T, S, R I So mple Type Li -Lithium 1132 ug'L Mg- Magnesium 927 mvL Mn-Manganese 1055 ufVL Na- Sodium 929 mg/L Arsenic:Total 1002 ug/L- Se- Selenium 1 147 ug/L. Hg-Mercury 71900 UWI- Ba-Barium ug1L Orlymachlorine Pwicides OTETophosphorus Paticides OrtytnanihOwn Pesticides Acid Herhi6des Base/Neutral&Acid Extractable Organics TPH Diesel Range Purpable Organirs (VOA bottle ra;'d) TPH Gasoline Range TP"'MX Gasoline Range Phytoplankton Temperature on arrival (*Cl: Report to: _Fayetteville Regional Office NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: Station Location: AB30391 Downstream ample Type: Effluent Date collected: 05/21/08 Affected Parameter(s): Fecal Coliform Sample ID: FROAPSSAMP82-I44 County: Sampson Region: Cape Fear Priority: Chain of Custody Collector: Bianton / Gu ton Date received: 05/22/08 Date analyzed: 05/22/08 Analytical Area (check one): ❑ WCH ❑ METAL S ❑NUT ®MICRO The following anomalies occurred (check all that apply): ❑Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not listed on fieldsheet ❑Mislabele-d as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pH): ❑Improper chemical ❑Residual chlorine present in sample []Color interference ❑Heavy emulsion formed during extraction ❑Sample bottle broken in lab - no reportable results ❑Other (specify): ❑VOA ❑SVGA ❑PEST Quality Control ❑Instrument failure — no reportable results ❑Analyst error — no reportable results []Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Intemal standards ®Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Two blanks were run after first series of samples (including A1330391), both were contamined with counts of 19 and 4 respectively. Values are estimates since blank contamination was evident. Corrective Action: ❑Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:136 ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: _ Form completed by: Pam Cotten[J-Z-M ( - Date: 5/27/2008 Lead Chemist Review (initial): 1WBIOCHEM Mp ❑PEST ❑SVGA ❑MFTALS ❑VOA Branch Head Review (initial): y� QA/QC Review (initial �� �J � 1Logged into database by (initial): QANForM1uL4boMory\sAR f`Y y`� �j ;a23101dt3 Report to: -Fayetteville Regional Office NC DENR/DWQ Laboratory Sample Anomaly Report (SAR) Lab Number: Station Location: ample Type: A R30391 Downstream Effluent Date collected: 05/21/08 Affected Parameter(s) Total Coliform Sample ID: FROAPSSAMP82-144 County: Sampson Priority: Chain of Custody Date received: 05/22/08 Analytical Area (check one): ❑ WC [-]METALS ❑NUT ®MICRO The following anomalies occurred (check all that apply): ®Samples ❑Improper container used ❑VOA vials with headspace ❑Sulfide samples with headspace ❑Samples not received, but listed on fieldsheet ❑Samples received, but not Iisted on fieldsheet MMislabeled as to tests, preservatives, etc. ❑Holding time expired ❑Prior to receipt in lab ❑After receipt in lab ❑Insufficient quantity for analysis ❑Sample exhibits gross non -homogeneity ❑Sample not chemically preserved properly ❑pH out of range (record pl-1): ❑Improper chemical ❑Residual chlorine present in sample ❑Color interference ❑Heavy emulsion formed during extraction []Sample bottle broken in lab - no reportable results ❑Other (specify): Region: Cape Fear Collector: _Bianton /_Guyton Date analyzed: 05/22/08 ❑VOA ❑SVOA ❑PEST ❑Quality Control ❑ Instrument failure - no reportable results ❑Analyst error- no reportable results ❑Surrogates ❑None added ❑Recovery outside acceptance limits ❑Spike recovery ❑None added ❑Recovery outside acceptance limits ❑Failed to meet criteria for precision ❑Internal standards ❑Blank contamination ❑QC data reported outside of controls (e.g., QCS, LCS) ❑Incorrect procedure used ❑SOP intentionally modified with QA and Branch Head approval ❑Invalid instrument calibration ❑Elevated detection limits due to: ❑Insufficient sample volume Comments: Sample bottle was labeled for fecal coliform only, therefore, samples were not run for total coliform. Corrective Action:Suggest resample to collect total coliform data. []Samples were rejected by DWQ Lab. Authorized by: Date: ❑Accepted and analyzed after notifying the collector or contact person and determining that another sample could not be secured. ❑Sample(s) on hold until: ®Sample reported with qualification. Data qualification code used:Z ❑Other (explain): Notification Required? ❑ Yes ❑ No Person Contacted: Date: I,-% Form completed by: Pam Cotten-V'd yl ( Ov-" Date: 5/27/2008 Lead Chemist Review (initial): (IBiOCHEM MR ❑PEST ❑SVOA ❑METALS A,Vo ❑VOA Branch Head Review (initial): QA/QC Review (initi C� logged into database by (initial): r j QAIFonnALabo=ory�SAR IM13101dhn n.i EM C Y k 9 v v lvlichaet F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Coleen Sullins, Director Division of Water Quality July 17, 2008 CERTIFIED MAIL RETURN RECEIPT REQUESTED Mr. Jim Walker PO Box 242 Garland, North Carolina 28441 Subject: NOTICE OF VIOLATION-NOV-2008-DV-0282 Administrative Code 15A NCAC 2H .0217 Southern Cross Farm Facility No- 82-144 Sampson County Permit No. AWS820144 Dear Mr. Walker: You are hereby notified that, having been permitted to have a non -discharge permit for the subject animal waste disposal system pursuant to 15A NCAC 2H .0217, you have been found to be in violation of your 2H .0217 Permit. Violation 1: Land application rates shall be in accordance with the CAWMP: (Permit No. AWS820144 Section II 4) On May 21, 2008 a flight over your farm by EPA and DWQ it appeared that you had ponding and possible run off of waste from a spray application. A site visit was conducted and it was observed that you did have ponding and runoff into the woods. Required Corrective action for Violation 1: If you have not already done so, immediately cease discharging and begin efforts to recover the discharged animal waste. This waste must be handled as prescribed by your CAWMP and applicable state law. Additionally, take all necessary steps to ensure this violation does not reoccur. loon` Carolina Naturally North Carolina DWQ/Aquifer Protection Section 225 Green SU Suite 714 Fayetteville, NC 28301 Phone (910) 433-3300 FAX (910) 486-0707 Internet, h2o_enrstate.nc.us Customer Service 1-877-673-6749 An Equal OpportunitylAffirmalive Action Employer — 50% Recycledfl0% Post Consumer Paper NCDAUS Ay66omic Division Phone: (919)7312655' - WeWSlW- Ww nca�r:com/al�oti6>Aii/' �"�G ��' �, °k sj.� .�� 1�::..r�� :,�, !Report: W00399 . Grower Southern Cross Farms Copies To: I ISDA-NRCS-Sampson PO Box 242 ��lJ 1:�:.t,. Garland NC 28441 aste nalysis eport - ,.am: 7/14/2008 Sampson County Sample Information Laboratory Results (parts per. mi;Iion unless otherwise noted) Sample 1D: N P K Ca 09 S Fe AM Zn C11 B MO G/ C 000001 7,001 372 56.7 464 154 61.1 54,1 4.10 0.25 1.87 0.47 1.62 1N N Waste Code: -N114 ALS -NO3 Na Ni cd Pb Al Se Li /r 11 SS C.•N DM% ("Cf.% A1.E ftil) 147 7.53 Description: OR-N Swine La oon 1.4. Urea Recommendations: Nutrients Available for First Crop lbsll000 gallons Other Elements lbs/1000 gallons :Application Metbod N P205 K20 Ca Mg S Fe Mn Zn Cu 13 MO Cl Na Ni Of Pb ;tl Se U Irrigation 1.6 0.76 3.7 0.90 0.36 0.32 0.02 T 0.01 T 0.01 1.2 Broadcast 1.6 0.76 3.7 0.90 0.36 0.32 0.02 T 0.01 T 0.01 1.2 Sam to lntormatlon p ,. La boratory Results (parts per million anless otlterwise'nated)� t Sample 1D: N P K 0, Mg S Fe 111n 711 Cu B 1190 l.7 C 000002 T'vral 364 50,6 432 165 61.9 48,9 3.83 0.23 I'M 0,45 1.53 IN -IV Waste Code: -N114 ALS -NO3 Na Ni (Id Pb Al Nil Li p H SS C:N VAI% CCG% ALF.( ,al) Description: OR-N 148 7.49 Swine Lagoon Lit . Urea Recommendations: Nutrients Available For First Crop_M11000 aeons Other Elements lbsll000 gallons Application Method N P205 K20 Ca Mg S Fe Mn Zn Cu H MO Cl Na Ni Crf Pb Al Se Li Irrigation 1.5 0.68 3.5 0.97 0.36 0.29 0.02 T 0.01 T 0.01 1.2 Broadcast 1.5 0.68 3.5 0.97 0.36 0,29 0.02 T 0.01 T 0.01 1.2 NCDAKS A 6namic Division Phone: (.91,9),733`:`,2655r Weti;Site.4w�vw' _ R .coriilagroif omi/il�r . ,`lt�'; r' ,z�. ar.' yj Repert:X 8309 Grower: Southern Cross Farms Copies To: USDAMCS-Sampson PO Box 242 Waste AnalysisRehort Garland, IBC 28441 farm; 5/30f2008 Sampson County Sample luformation Laboratory Results, (parts`per millloa unless atherwise noted)F;•;. , �� r . `_. � i .;;`t ��!,..<'� .:: _ r•;.. , �.�, . •. 3 Sample ID: N P K Ca Af S Pe Mn Zn Cu B A40 Cl C AN/ 392 44.4 444 128 45.9 48.4 3.23 0.20 1.25 0.30 1.03 000001' . IN--N Waste Code: -NM ALS -NQ3 Na Ni Cd A Al Se Li P 11 SS C:N DM% CCE% ALG(Kgd) Description: OR-N 148 7.48 Swine Lagoon Li . !Urea Recommendations: Nutrients Available for First Crop MOM allons , Other Elements M11000 allons Application Method N P205 K20 Ca Mg S Pe Mn A Cu B MO Cl Na Ni Cd A Al Se Li Irrigation 1.6 0.59 3.6 0.75 0.27 0.28 0.02 T 0.01 T 0.01 1.2 'Bahr leluformation . P.•. Laboratory Results `arts er nnillion unless otherwise noted Ty EP. P.. a ,}�,''�l'_l3,'�'� Sample ID: N P K Ca M S Pe Mn Zu Ca B Ma Cl C 000002 "blal 387 46.5 465 167 55.5 49.4 4.30 0.23 1.12 0.41 1.04 IN-N Waste Code: -N114 ALS NO3 Na Ni Cd A Al Se Li pIl SS C:•N DM% CCE% ALIT( a1) Description: 0R-N 157 7.49 Swine Lagoon Lic . Urea Recommendations: Nutrients Available for First Crop lbs/1000 allons Other Elements 1bs1I000 jZ#Ilons Application Method N P205 K20 Ca Mg S Pe Mn Zn C'u B Mo Cl Na Ni Cd A Al Se l i Irrigation 1.6 0.62 3.7 0,97 0.32 0.29 0.03 T 0.01 T 0.01 1.3 .... ..... w.,..•,„ :.r N{{/n.Y1,, l�A &.C. S.lA. o_n. amic Aiv_i.a..i.o. ..n.. ., :..•: k Pi ... ..... .ahone.:n1.,9/733l x655! .- b S rL-Ylwe' 'I5070t-'.,- ,r : ,�.r�' i,j.yo- ,�,,� K>;�F+%1,w Sr,,yer�,�y4•,:5�w, ,�1 Grower.- Southern Cross Farms Copies To: USDAMCS-Sampson PO Box 242 ®Garland, 1 -Waste Analysis Report NC 28441 Farm: 4/16/2008 Sampson County p.,. ;5am�'la.lnforiiiatioA; , ,N,:. k�xI.M:'.�1�1�-1i •-�tr N� r'4 ' 'jG <, r n, � .e; �! k. iT,F .; +.� �, ..,,+. I:V - i', r�, •.i Labocu o ` Re, a .. ,o '"r.'wis :�.� 'a��� ,I�r3. ,,�;7r'�;�, •�� ,,�•.,;i� , rr , U. � ��:,-,', r F ��,� ,.. t sults� 'arts;"ai�milll n,uiiless the e_not'ed �ir••�,. � � � e, � � � .�,: � ,;, {'i.. „, lN,..,..1�...-.... .,. ._ .- ...,"...,ww..w.�,. .�.�t, .�.�::�.,. �""`hr�wi� .,,14€�c"�hrr_.t�,.:i,.<�1c..�,�.,�,..�?,i«i5k;��daa3..-,�:�,.,- ,r.•_r,.,;r3..,#�,,s;. �hr:, k* • �. ,r� Sample ID: N P K Ca M S Pe Mn 7n CU R Mn (;1 C A��'//���nn'y� 000001. 355 IN-N 45.3 399 154 43.3 39.5 3.87 0.21 1.04 0.41 1.10 Waste Corte. -N114 ALS -NO3 Na Ni Cd Pb Al Se Li P I1 SS C.•N DM% CCPN ALE( ) Description: OR-N 135 7.51 370 ! Swine Lagoon Li . Urea -Recommendations: Nutr[66 Avallable for First C60 ` 'M11Q0p alklis " Otii'e .B]emeats; lbs/IQ00ga11 Appllcafion Melbod N P205 K20 Ca Mg S Fe "Mri. Zn . Cu. , yB . , '; M' Cl - Na Nf. Cd Pb AP , � "'Se ` ! irrigation 1.5 0.61 3.2 0.90 -. 6,25 0.23 0.02•-' ._.; �T"' 0.01 T- w-r0.01-- -- •' . 1;1 ! ., °amn4le Itifartriatioa�. 5 -+r.i'..1..J�.f:r�:k�.r.6"7. .,.�! � sum. , r ,k:!'Y "_ 4�'iti;r�•' i[l >.,i y -.y�., _ Gabrato�r�j Results �n-arts /{cr million uul'e's`s otherwise noted ixl� ���' .µr^^, T ' �:. er ';1'...11. r.',j„ Sample ID: N P K Ca M S Pe M11 711 C11 R M0 (,11 C 11011d 342 IN N 46.6 404 134 39.2 37.4 2.81 0,19 9.45 0.31 1.16 Waste Code: -NH4 ALS -NO3 Na Ni W P6 Al Se Li PH SS CN DM% CCE% ALIi(1d) Description: OR-N 136 7.5 Swine Lagoon Li . Urea Rec6mm " ' o s: Nutrients Available for First Cro ., , lbs 10Q0 allons ', ;` Dther:Blemen O .: lbs/1000 'dllons ApplicationMelbad Irrigation N P205 K20 Ca MS' S Fe ''"Mti' . Zri "G11 1.4 0.62 3.2 0.78 0.23 0.22 0.02 T 0:06 "�"B'`""'"`iN¢' 'Cl .T "0.01 Na.- Wi Cd A 1 A Al Se 1, ivlsion Pho&'- -�I r Analysis I.IfI III1 Grower: Southern Cross Farms PO Box 242 Garland, NC 28441 Farm: Copies To: USDA-NRCS-Sampson 2/18/2008 Sampson County :.. .. >.. �, o .,.r.. , �- .,-:-:,,� ... .,...... � .�� .,,: ......: ... .... .., ,r . �.•,.. ., cy • : !. �. Lj:�rl P • 'ram " i IrR • _ u... . a k e.. {k. � � . r .I.' r S e for Hdu' , Lal�orato Results;/ arts er gailllon uhless, otherwise.noted i !1{E ; s ,xr m , ,i w ^"� at�1�1�...:](Il. ,.-1.... ,.. , ..... ,lp,,..,..1�m�mi,.'�1 41.1k...n4s.tid,r,.w 1, w�.ra .. r,,,hts5..+r�... I ., 'ra.•. [fS?k,:.�,. Ifi�/lt:: Vamp le 1D. A' P K Ca N 4 Fe Mn 2'n Ca B Mo C1 C O0Oa1;00 - - " ' � • , Total IN-N 370 5o.6 433 141 41.2 35.4 4.11 0.26 1.45 0.33 0.92 Waste Code: -N114 ALS -NO3 Na Ni Cd A At Se Li PH SS C,N DM% CCE% ALE(KO) Description: OR-N 140 7.38 Swine L oon Li . Urea Recommendations: • Nutrients Available for First Ci•o . lbs/1000" allots otherFleih tdts' . lbs 1000gallons Application Method N P205 K20 Ca Mg S Fe Mn A Cu B Mo CI Na Ni Cd Pb A/ Se U Irrigation 1.5 0.68 3.5 0.82 0:24 0.21 0.02 T 0.01: T 0.01 1.2 ..I � 0 on Sam 1e Inf rmati . 1�....i...,n.:,.,.,... _ .,i-.. 'n L horato Re ul ( is r mi an u ss o rwi n }s, a s' is ar 11i " n1e the , se ated w ll.,,..,.,.,ll!�„.fi ,. �;.,..,:.f,.,, .:•jy:y %k,F,. Y+,�l S,i: �L,T i.l.! k��l,r M^r` .k,'1:bll!' '�! { j<il, Y� rA.'r k ! F'S, " , '.G „�. .k •fj>p1 -r r !. r kx, u FI >... at'"'MR .ki,fNei ?!r.E,e,;:r�-n .#.r..:Jl.f,,it; �w :I ,:w.: ufniui efrr Y`,.,3,.•r 'IG•.a,r .,.ww,r.•..e• '.li `•'. Sample ID: N P K Ca M S Fe Mn 71r fie B Mo l,'f C 00 " • �_. 000aaz Torat 358 49.0 430 145 41.2 33.8 3.71 0.22 1.21 0.31 0.94 Waste Code: -N114 ALS -NO3 Na Ni Lit Pb Al Se Li pit SS CN DM% CCE% ALIT(al) Description: OR -IV 143 7.38 Swine Lagoon Li . llrea Re' en tuns: Nutrients Available for"First Crop "' ..:' lbs 1000 allons; Other.: Elemeatsr' " !bs 1000 ullons° Application Method N P205 K20 Ca Mg S Fe Mn -zh'. Cu B Mo Cl Na ' - Ni Cd A At Se Li Irrigation 1.5 0.65 3.4 0.85 0.24 0,20 0.02 T 6Al T 0.01 1.2 NCAA&CS Agronomic Division Phone: (919)733-2655: 4 (mower, Southern Cross Farms Copies TO: USIM-NRCS-Sampson PO Box 242 Garland, NC 28441 Waste A nalv sisRohort _ ✓ I" Farm: 12/0/2007 Sampson County Sample•ldorinatlan laboratory Results #ts. er million as „ „_..., (P' .. P less othei�svise noted) Sample ID: N P R Ca Mg S Pe Mn 7.n Crt B MO (,'l C 000001 Tula) 339 48.1 465 137 44.2 31,8 2.76 0.18 0.58 0.20 1.13 IX-N Waste Lode: 4114 ALS -NQ3 Na Ni L'rl 11b it/ Se Li P11 b,S CN 9M% C(1,M, AI,L( tQ 153 7.17 Description: OR-N Swine Lagoon Li . Urea Recommendations: Nutrients Available for First Crop lbsll000 galtons Other Elements MONO gallons Application Method N P205 K20 Ca Mg S Fe AN Zn 04 B Mo Cl Na Ni Cd Pb Al Se Li Irrigation 1.4 0.64 3.7 0.80 0.26 0.19 0.02 T T 'r 0.01 1.3 Sam ple_lyiformatiion Laborato Etesults: arts' >er,difl ion unless otherwise;ootcd : ; , ; ,u ;, , i;, Sample ID. N P !v Ca S Pe AM 7n R Mn 000002 Total 322 47.7 466 130 43,2 30.7 2.63 0.18 0.66 0.19 1.13 IN•N Waste Code: -N114 ALS 403 Na Ni (,'d Pb Al Se Li P H SS (,':N DM% CCEW) ALL(I(gal) Description: OR-N 150 7.15 Swine Lagoon Liq . Urea Recommendations: Nutrients Available for First Cro M11000 allons Other Elements 1&11000 allons Application Method N P205 K20 Ca Mg S Fe Mn Zrt Cu B Afo C1 Na Ni Cd Pb :11 Se Li Irrigation 1.3 0-(A 3.7 0.76 0.25 0.18 0.02 T T 'r 0.01 1.3 KDA&CS Agronomic Division Phone:, (919) 7.33=2655'-' , WeWSite . www:'nca�r com%agrai omi/ , ; ri ; �� f, cif f 'y i N� ' � epo R rt: W01778 Grower: Southern Cross Farms Copies 1'o: USDA-NRCS-Sampson PO Box 242 r Garland, NC 28441 Waste Analysis RD11ort Farm: 9/14/2007 Sampson County $am' le,laformation Laboratory Results (parts..per million unless.otherwise noted)- Sample 1D: N P K Ca Mg S Fe Mn 711 Cu B _ Alo ("I C 000001 Nal 310 56.0 516 153 61.8 273 4.61 0.22 0.79 0.53 1.21 IN-N Waste Code: -N114 ALS n`03 Na Ni Cd Pb A/ Se Li p H SS C.•N DMY0 C(,'F% ALE(R al) Description: OR -IV 169 7.37 Swine Lagoon Li . Urea Recommendations: Nutrients Available for First Crop lbs11000 gallons, Other Elements lbs/1400 allolrs Applicalion Method N P205 K20 Ca Mg S Fe Mn Z►i Cu B Mo Cl Na Ni Cd Pb Al Se Li Irrigation 1.3 0.75 41 0.89 0.36 0.16 0.03 T 0._01 T 0.01 1.4 Completed: September 13, 2007 Sumpie Information l Laboratory Results ,(parts`per •n „h „i, e, n, .wln ii.ti3u,. H, i . . 1�1 .c, ,a,,C., z Sample ID: 000002 Waste Code: ALS Description: Swine L• oon Li . N P K Ca M S Fe Mn %n Cu B Alf) Cl C Tolal 312 IN-N 4114 -NO3 OR-N Urea 58.0 531 137 59.0 25.6 4.15 0.22 0.63 0.40 1.27 Na Ni Cd Pb Al Se M PI! SS C-N DAf% CCEN ALE(' ai) 173 7.35 Recommendations: Nutrients Available for First Crop W11000 allons Other Elements lbs11000 allons Applicalion Method Irrigation N 1.3 P205 K20 Ca A1g S Fe 0.78 4.3 0,80 0.34 0.15 0.02 Mn T A (,'u T T B Mo Cl 0.01 Na 1.4 Ni Crl A Al Se Li INCDAUSAftono>aiic,Dfihi6n Phone ':.',(9!9)733-265V ."' -WhAt" ' ­ -1 4 W.", , -. e:,�W.ww.n 00 'No rt. 0279 Grower., Southern Cross Farms CoPies To: USDA-NRO-Sampson P0 Box 242 Garland, NC 28441 -I pWaste A naiysis RDhort VF Farm: 7/17/2007 Sampson County On 6ihji4t1on,.-' fl LA oiitor u e" b Sample ID. 0600.1:. Waste code.. A Description: Aerobic Liquid - Swine N P K Ca Afg S Fe Mn Z" Cu B Mn Cl C Total 415 IN -IV _N114 -NO3 OR-N (Irea 51.6 507 135 51.0 28.6 3.83 0,24 o'84 0.42 1.34 Na Ni Cd Pb Al Se Li p H SS C,-N DM% CCF% Al.l(KpA) 167 6.79 Recommendati 011060-kallb&,... A0t&f:Ekmeoti WON gallow Application Meth6d Irrigation N 1.7 P205 K20 Cd Mg S Ph A 0.69 4.1 0.79' 030 0.17 0.02 J� ". Zh, Q'b, .',!B MCl T-' T"". Na Ni Cd Pb Al Se Li SOME OF ME WASTE'SAMPLE BOTTLES THAT WE RECENTLY RECEIVED FROM YOU WERE FILLED TO THE VERY TOP. THIS IS A POTENTIAL. IIAZARD FOR OUR CHEMISTS WIZEN THEY IIOMO(;ENizr THE WASTE SAMPLE OR IF THE TEMPERATURE OF THE SAMPLE INCREASES. PLEASE LEAVE AT LEAST A 2 INCH SPACE IN THE TOP OF THE BOTTLE TO ALLOW FOR EXPANSION. THANK YOU. BRENDA R. CLEVELAND PLANT WASTE AND SOLUTION, SECTION CHIEF ;e,jbf4niiatik Laboratory Results (parts per million unless otherwise noted),,.: Sample 1D.- N P K Ca Mg S Fe Mn zn Cu B M0 ("I C 0.00021. 406 IN -IV 53.3 510 121 49,o 26.9 3.36 0.21 0,82 0.34 1.33 Waste Code: 4114 AES -NO3 Na Ni Cd Pb Al se li pH_ SS C-N DM% CCE% ALE(Kpd) Description: OR-N 169 6.91 Aerobic Liquid - Swine ffrea Recommendations: Nutrients Available for First Ck6, lbs11060 galibm - Other Elements lbsIM00 gallons Application Method N P'205 K,20 Ca Mg S Fe Mn Zn Cu B Afo Cl Na Ni Cd Pb Al Se Li Irrigation 1.7 0.71 4.1 0.70 0.29 0.16 0.02 T T T 0.01 1.4 NCDA&CS-AOonomic Division Phone: (91.9)7337-2655 Web..Site::www:nea ;:com/a .onomW ;s Report: W09367 Grower: Southern Cross Farms Copies To: F PO Sox 242 Garland, NC 28441 F Waste Analysis Re Fhor t FA: 5/23/2007 Bladen County Sam leInformation Laboratu .Results arts`"er}millionririlessiotlieiviseiaated `cy, �� ;G'" a'' ifs'', .rian'�'=1'{ik',F'i Sample 1D. 0006% •' ' Waste Code: AES Description: Aerobic Liquid - Swine N P K Ca Afg S Fo Mn Zn Cu B Ma Cl C 710fal 497 IN-N -N114 -NO3 OR-N Urea 53.8 512 189 51.7 54.4 4.10 0,21 0,80 0.31 1.09 Na Ni Cd Pb Al Se Li P 11 SS C.N UM% CCE% 163 7.25 Recommendations: Nutrients Avallabfe;for`FirsCCro !... _.. lbs`1000 dllof_rs: Othor Elements'_ M11000 allons Application Metbod Irrigation N P205 K20 2.1 0.72 4.1 Ca Mg S Fe Mn 11, 0.30 0.32 0.02 T Zn T Cu B MO T. 0.01 C1 Na Ni Cd Pb 1.4 Al Se Li Sample information Laboiotnry'Results (parts ger iriillian unless'othcrwise�noted}� Sample ID: N P K Ca M S Fe Mu A Cid 8 Mrs Cl C 1 6060" k Waste Code. AES Description: Aerobic Liquid - Swine 7bild 497 IN-N -N114 -NO3 OR-N Urea 54.5 545 144 44.1 54.1 3.45 0.20 0.82 0.20 1.07 Na Ni Cd Pb Al Se Li p 11 SS C.-N I)M% CCE% ALL( 4) 171 7.17 ' Recommendations: Nutrients Available: for: First CroO lbs 1000:0llorri.. i0tUr Ele'nteats. M110017 also Application Metbod Irrigation N P205 K20 2.1 0.73 4.4 Cd Mg S Fe Mn 0.84 0.26 0.32 0.02. T ., M T Cu ' B Mo T 0.01 Cl 'Nu ' Ni Cd Pb 1.4 Al Se Li E r SitNWA �hl NCDA&CS"" g ," r Grower Southern Cross Farms Copies To; USDA-NRCS-Sampson PO Box 242 Garland, NC 28441 M Waste Analysis Rtrarm: Vohor _ 3/14/2007 Sampson County dr�fl.. �.L b6rato R661 - P" -, -�-j -rI -,& Sample ID: N P K Ca Mg S Fe Mn Zn Cu B MO 0 C 0 1 0,600, f 701111 419 68.2 500 160 46.5 53,2 4.05 0.26 1.12 0,43 1.34 IN-N Waste Code. -A114 ALS -AI03 Na Ni Cd Pb Al so U P 11 SS C.-N DMA ccf.% AI,F,(Kgal) Description: OR-N 159 6.95 I Swine Lagoon Licl, Urea Recommendations: Nutrients Available for FirstIU60-'t'-.- *her'.:EIe'fiIeUts-.L Ibs1IOOOy_aIIqtis:-- Application Method C -'Mo r N P205 K20 Ca Afg, S Fd!' In', u Cl.- "': '. k-Ni-"" Pb:. !, r :1. Cd '�';.'N, Al Se' Ui Irrigation 1.8 0.91 4.0 0,93. -0-27 0.31 0;02 0.0.1- T. The pH of the lagoon Hyfid is below the ideal range for bacterial action and.waste treatment. Gra6ally,' us of llq�id remaining in the lagoon. Sample the lagoon toll by I lb, of time per,1000cu. ft 9 'adj monthly mid continue to adjust pli until it is within the desired ilm-le of 7-0'-8O' Sam le lnforttiation. borato Results; P swo . AWO ""Mav'! h� 616 Ilb M- "", N'." IN�' Sample ID: N P K Ga M8 S Fe Mn 71, Cu H MO (11 C 6620-6-62 TO/a/ 489 64.4 505 156 46.6 47.8 3.59 0.25 1.17 0,40 1.44 IN-N Waste Code: -NIN ALS -NO3 Na Ni Cd Pb Al so U P if SS C.-N DM% C(IIIIN Al.r(I(gal) Description: OR-N 161 7.04 Swine Lagoon UQ. Urea Recommendations: Nytiknts Available for First V661'.' j6s 1006jaild ''Oth6116nifits I6s1I000j#II6Lk.` Application Method Irrigation N h03 2.0 0.86 K20 Ca Mg S Pe. 4.0 0.91 0.27 0.28 6.02 T 0.01' M6.- Cl T 0.61, Na'Ni!. I Cd - A 1 q3' Al so Li d Division - , Phony Wacto A"a.111cic /1 alInrt Grower.• Southern Cross Farms Copies To: USDA-NRCS-Sampson PO Box 242 Garland, NC 28441 NWW_ 12/11/20o6 Farris, Sampson County Sample Information Laboratory Results (parts per million unless otherwise noted) Sample 10: 000001 Waste Code. AES Description: Aerobic Liquid - Swine N P K Ca Mg S Fe Mra /n Cu B MO Cl Total 353 IN-N -N114 -NO3 OR-N Urea 47.8 405 104 39.7 31.9 2.99 0,t6 0.61 0.27 0.78 Na Ni Cd Pb A/ Se Li p H SS C.•N DM% CCI,,% ALIT{ sd) 131 6.98 Recommen tions: Nutrients Available for First:Cro" IbS11000 allons other. Elements IbS1IOO 1, allons Applteation Met Irrig,,ifion N 1.5 P205 K20 Ca Mg S Fe Mn 0.64 3.2 o,61 0.23 0.19 0.02 T 7.n Cu T T B Mo T Cl Na 1.1 Ni Cd Ph Al 'Se Li Sample Information Laboratory Results (parts per million unless otherwise noted) Sample 1D: 000002 Waste Code: AES Description: Aerobic Liquid - Swine N K ca MS S Fe AN Zrr Mu CI C Total 332 IN-N -NH4 -NO3 OR-N Urea _P _ _Cti _B 48.8 392 ill 41.5 �32,0 2.92 0.15 0.50 0.30 0,77 + Na Ni Cd A Al Se Li p H SS CN DM% cc % 127 TO Recommendations: Nutrients Available for First Ciop Ibs 1000 gallons . Other Elements, . 'Ibs/1000 allortS Applleation Method Irrigation N 1A P205 K20 Ga Mg S Pe Mn 0.65 3.1 0.65 0.24 0.19 0.02 T Zn Cu T T B Mo T Cl Na 1.1 Ni Cd A Al Se Li IVCDA&CS gnomic Divisioa Ph'one"(919),733 f2655 Web Si#e www'f cagt.com/a nnami/, 3F ' �;:"; i �; a : t'.'rMr' Re'ort�' W0194p Grower- Southern Cross Farms Copies. To: PO Box 242 �Q Garland, PVC 28441 Waste A nalysis Rohort Darn): 9/11/2006 Sampson County Samole-laf6rrnation ,.�I:aboratory Resifts (pits per, million`unless otheraise3gofed);` , " r; .,�; k <'r: v } ,Sample ID: 000001 Waste Code: AES Description: Aerol)ic Liquid - Swine N P K Ca M S Pe Mn Zn Cu B MO CI C Total 276 IN-N 4114 -NO3 OR-N Urea 71.0 480 154 66.0 40A 3.53 o.37 0.73 0.11 0.90 Na Ni Crl Pb A/ tie Li pll SS C-N DAI% ("CIN UE(Kg,-d) 175 7.3 Recommendations* I Nutrients Available for First Crop W11000 allons Other Elements lbs/1DOD gallons Application Melbod Irrigation N 1.2 P205 0.95 K20 3.8 Ca Afg S Be 0.90 0.39 0.24 0.02 Mr, T 7n T Cu B MO T 0.01 (.'I Na Ni 1.5 Cd Pb Al Se Li Sam le Information LaboratoryIRes1�lts,(parta- er million unlca"s otherwise notedAC il,rIiM , Sample ID: N P K Ca M S Pe MI, /,n Cu B MO l.'! C 000002' Waste Code: AES Description: Aerobic Lic uid - Swine Total IN -IV 4114 403 OR-N Urea 288 72.7 448 150 65.9 39.3 3.70 0.39 0.73 0.11 0.88 No Ni Cd Pb Al Se Li p 11 SS L',N UM% C(:h'% ALE,(4-A) 163 7.33 Recommendations: Nutrients Available for First Crop 1bs/1000 gallons Other Elements lbs/1000 gallons Application Metiwd Irrigalion N 1.2 P205 0.97 K20 3.6 Ca Mg S Pe 0.87 0.38 0.23 0.02 Mn T /.n T Cu 8 Iwo 11, 0.01 C! Na Ni 1.4 Cd Ph A! Se Li NCDA&CS Agronomic Division Phone: (919)733-2655 , Web.Site: www.n5agr.cpm/at9nond/ Report: W08091 Grottier: Southern Cross Farms Copies To: Waste A naiysis Relhort F 4/20/2006 PO Box 242 Garland, NC 28441 Farm: Sampson County Sampjejhf6ftqklon I , ry Ub6rat6 ;Resuli�,(patt�'por.Wilidii.tioli�s�.oth6r*lie noted ) - Sample ID: 000001 Waste Code. ALS Description: Swine Lagoon Licl. N P K Ca M S 1'e Mn 7n Gu 8 Mo c/ 7,01al 545 IN-N -NI14 NO3 OR-N Urea 66.5 640 191 58.6 68.1 5.28 o,46 1.81 0,32 1.03 Na Ni cd Pb Al Se Li P11 SS C.-N DM% ('6111('CIAO ALIT( Kg,,d) 233 7.2 Recomfiien&tlons: Nutrients Available for First Crop MOM Ualkw, Other Elements lbsll 000 jZallons Application. ' Metb6d Irrigation N P205 K20 2.3 0189 5,1 Ca Mg S F& 1.1 0.34 0.40 0.03 Mn T Z11 0.01 Cu B T 0.01 Mo 'Cl Na 2.0 Ni Cd Pb A/ Se M SaiA0.k,;1fi.f6,f.fi*tion Laboratory Results (parts �pcfftiflhon unl6sothiMk noted) Sample ID: 000002, Waste Code: ALN Description: Swine Lagoon Lig. N 1) K Ga A119 N AM Z?1 Cu 13 Mo Cl C Total 549 IN-N -Nn4 NO3 OR-N Urea 65.1 586 196 59.8 61.2 5.04 047 1,25 020 ().98 Na Ni Cd Pb Al Se Li I/ SS C-Al 9M% ALE A) 210 7.2 Recommendations. Nutrients Available for First -Crop MOM p_allons-.- Other Elements bs11q0 M Application Metbod Irrigation N P205 X20 2.3 0.87 4.7 Ca Mg S Fe 1.1 0.34 0.36 0.03 Mr, T 7n 0.01 Cu B T 0.01 Mo Cl Na 1.8 Ni Cd Pb _qjZallons Al so Li NGDA&CS A "oriomic Dlvi siPp Pfione:.(9I9)733-265.5 , Web: Site: www.ncagr.cotn/agronomi/ Report:: W05991. Grower: Southern Cross Farms Copies To, IISDAMCS-Sampson PO Box 242 Garland, NC 28441 WasteAnalysis Report - F(11'1 N: 211612006 Sampson County Sample Information Laboratory. Results (parts per million udless.othertvise noted) Sample in: N P K Ca M S Fe Mtt/.n Cu B hlo CI 000.001 Total 411 52A 464 174 51.2 49.4 3.77 o.36 0.70 0.11 0.96 IN-N Waste Code: -N114 ALS -NO3 Na Ni Cd A :Il Se l.i PI/ 5S C:N DAM M.E.(kd) Description: OR-N 164 7.24 swiite kwoam Liu. 11rea Application Melhod N P205 K20 Ca Mq S Pe Mrt A Cu B MO Cl Na Ni Of Pb Al Se Y Irrigation 1.7 0.70 3.7 1.0 0.30 0.29 0.02 T T 'I' 0.01 1.4 Broadcast 1 1.7 0.70 3.7 1.0 0.30 0.29 0.02 'l' T T 0.01 1.4 Sample Information, Laboratory Results, (parts per million unless, otherwise noted) sample 1D: N P K Crr Mg S Fe Ali) 7n Cn H Aio CI C 000002 rota! 396 49.8 421 144 42.8 45.8 4.09 0,29 0,64 0,10 0.92 IN-N Waste Code: -NIN Al S NO3 Na Ni Cd A A/ &I Ii P I1 SS (,' N IJrtM ("Ch', Al Eftal) Description: OR-N 151 7,19 Swine La nnn Li . Urea Recommendations: Nutrients Available for First Crop M11000 allons Other Elements W11000goallons e1pplicalion Method N 1205 K20 Ca Aig S Fe MI; hi Cie a Mn U Na Ni Cd Pb A/ Se Li lrrigation 1.7 0.67 3.4 0.81 0.25 0.27 0.02 T T 'i 0.01 1.3 Broadc:Lst 1.7 0.67 3.4 0.84 0.25 0,27 0.02 T T T 0.01 1.3 NCDA&CS Agronomic Division Phone: (919)733-2655 Web Site: www.ncagr.com/agrononii/ Report: W03992 WasteAnalysis eport 11/22/2005 Grower: Southern Cross Farms Copies To: PO Box 242 Garland, NC 28441 Farm: Sampson County Sample information � Laboratory Results (parts per million unless otherwise noted) Sample ID: N P K Ca Mg S Fe Ahl Z71 Cu I3 MO ("I C 000001 waste Code: AIS Description: Swine Lqgooii Li( . 1161al IN-N -NH4 -NO3 OR-N Urea 301 48.0 434 121 45.2 40.3 3.11 0.26 0.53 0.08 0.87 Na Ni Cd Pb Al Se Li P 11 SS C:N 1111% CCI'Y Al.li([i al) 149 7.39 Recommen • tions: Nutrients Available for First Crop lbs11000 allons Other Elements lbs1IOOO gallons tpplicalion Method Irrigation N 1.3 P205 0.64 K20 3.5 G'a mg S Fe 0.71 0.26 0.23 0.02 Mn 11' Z» Cu 8 T 0.01 Ma Cl Na 1.2 Ni Cd A :I/ Se Li Sample Information Laboratory Results (parts per million unless otherwise noted) Sample ID: N P K Ca Mg S Fe Mu 771 Crr 8 M0 Cl C 000002 Waste Code: ALS Description: Swine Lagoon Li , T'OMI IN-N -NI14 -NO3 OR-N Urea 313 49.8 418 141 50.4 42.2 3,25 0.30 0.52 0,08 0.87 Na Ni cel A Al Se Li P 11 SS C:N DM% CG'G'Y ALF (4-:11) 153 7,36 Recommendations: Nutrients Available for First Crop W11000 gallons Other Elements lbs/1000 gallons Application Method Irrigation N 1.3 11205 0,67 K20 3.3 Ga Mg S Fe 0.82 0.29 0.25 0.02 Mrt T Zrt '1' Gu B T 0.01 MO Cl Na 1.:3 Ni Cd Ply Il Se U NCDAB�GS�'A ono"mic'Division F Phone. ((9pi: 733'=265.51,E 'Web Site.E'p�Qip/ Aca' con 7�Q' ''onomil`ii. s, , ,, , , , y "�' + ''` ' �f '1Re `ort�iW0103.41': .... .. ...... .. ..... .......... �,..,.. ..- _... ., .--.. ,....I I.. ..__.., ...{ `J. �). - - .'.•; 1`.�.`.=. E., "b.... ,t �. R .!. . 3-.... . rt'�:.. ri�_: .,e!L! , - ! sr _ Grower: Southern Cross Farms Copies To: USDA-NRCS-Sampson PO Sox 242 ® a _Waste A nalysis Reh,ort Garland, NC 28441 Farm: 8/25/2005 Sampson County _ I S4 le`,Informafion, �.P .�,.. Y. •V. :IP!'sf � fY -41 `I i--- A♦;r � j -i_ .�l�. `;7} .! !� 4 �!.' r� ♦ ^� `� ',��i }V.; - y;2W { I ! I ,}li•. { f•;5:'1}.. '.i" F.il':�( <II'1 yaw �r� ' Y { LL n -� a:; t �!! • f� : � +I_ !' 3 ;L"aborato . Results"i "at't8 'e'r viillia"n ual'ess otherwise mated �• . E:c� ,�, >>,,' ;, /jii tl „r{ it fatl�� . ,: �1Y =t ,p,,l f •,� ,. ..!'Y.� ........�P.. ..P..n ..,I�.......� �._.. .)flu:.�.�..la���._.�.�.ti.�....l..t�...�.>�....>.....�....r Y..._...,��.:.�_..:��. 4ample ID: N P K Ca M IS' Fe Mr, Zrr Cu R Ma Cl C 00000i ., Nal 425 54.5 376 127 54.1 32.3 3.50 0.31 0.65 0.06 0.86 IN-N Waste Code: -NH4 ALS -1V03 Na Ni Cd A Al Se Li p H SS C'N DM% CCIs% AE td) description: OR-N 148 7.41 Swine Lagoo Li , Urea Recomme dations: Nutrients Availible•fa"rlfirst Crop. 1bs11000 allons I. ;Other Elements lbs/1000 allons 4pplication Method N P205 K20 Ca Mg S Fe Mn Zn Cu B Mo Cl -Na" Ni Cd Pb Al Se U Irrigation 1.8. 0.73 . .3.0.- 0.74 0.32 0.19 0.02- T T- T 0.01 1.2•- nnle Infor""oration„ 33 .IGaliorat'o .'Results' nu�arts„er inilliou uirl'essiotlticr`wisetnotcd1 .11 Y.yw .. ?' . i!, 1 H -'1fa 4'-} -.1.11 NC.. - F 4_� r{.• �., Sample ID: N P K Ca M1 S Fe Mrs Zn Cu B Mn C! C 00,60,0, Total 355 57.3 404 140 58.9 35.1 3A 0.33 o.63 0.07 0.89 , I . IN-N Waste Code: -Nl14 A1.S -NQ3 Na Ni Cd P6 Al Se Li pH SS C.-N DM% CCh.`% ALI:(!(},d) Description: OR-N 149 7.41 Swine Lagoon Li . Urea Recommendations:' Nutrients Available.kf F1rsf.Cr'o lbs11000 iillons ,"`.. , 'Athei Rlements. lbs11000 gallons 4pplication Method N P205 K20 'Ca Mg ' S Fe," Mri Zn Cu B Mo Cl ,' Na " Ni Cd' Pb' Al Se U Irrigation 1.5 0.77 3'2 0,82 0,34 0.20 0.62 T 'T- T 0.01 ; L-3 NCDA Agronomic Division 4300 Reed�Creek Road Raleigh, NC 27607.6465 (919) 733.2655 Report No: W01634 W Grower' Southern Cross Farms Copies To, USDA•NRCCS-Sampson - PO Box 242 Garland, NC 28441 r�wd,ry•Waste A naiyszs Reh.rort Farm, Sample Info. Laboratm Results arts Der million unless otherwise noted Sample 000002 Waste Code. ALS Description, Swine La oon Li , a KQ S Fe Mn Zn u 8 U0 0 Total 355 1N -N -NH4 -NO3 OR-N L1ree 573 404 140 58.9 35.1 3.18 033 0,63 0.07 0.89 Na N1 Cd Pb Al Se Lf PH SS CrN DMA CCE% ALE K a! 149 7.41 Recommendations: Nutrients Palla6le for First Crop lbsIlE Qallo5s Other Elements N1100 0 gallons Application Method Irrigatlon N P2O5 K20 1.5 0.77 3.2 Ca Mg S Fe Mn 0.82 0.34 0.20 0.02 T Zn Cu 8 T T 0,01 Mo Cl Na` 1.3 N! Cd Pb Al Se L! Grower- Southern Cross Farms Copies To: USDA -MRCS -Sampson PO Box 242 r N �} r aste f A naiysis Report Garland, NC 28441 Farm: 5/11/2005 Sampson County L462 Sample ID.- N P K ca, MS S- F6 Mn Zn Cu B MO Cl C Told 514 72.5 566 197 55.0 51.3 5.68 0.52 1.47 0.23 1.23 IN-N Waste code: -NI14 ALS -NO3 Na Ni Cd Pb Al se Li 11 SS C-N DM%, CCLN ALE( al) 197 7.37 Description: OR-N Swine Lgoon Lig, Urea Rkommendations:i Nutrients Available for Mt Crop Ibs1I 000,jjaWlans Oth&Eleihefits ML1000lallons Application Methbd N P205 K20 Ca Mg S h Mn Zn Cu H Mo Cl Na Ni Cd A Al Se Li Irrigation 2.1 0.97 4.5 1.2 0.32 00. 0,03. T .0,011 T 0,01 1-6 SW, I. M - IMt o 'Results nits, all Sample ID.- N P K Ca Mg S Fe MFI 711 04 8 MO Cl C 545 194 70.9 561 53.9 5U 1.49 1.18 5.77 0,51 0.23 IN-N Waste Code: -NI14 ALS -NO3 Na Ni Cd A Al Se U P H SS CIN DM% CM ALE(KgoJ) Description: OR-N 197 7.35 Swine La Loon Lig. Urea Recotnmehdons: Nutrients Available for First Crop lbs/1000-gollons other Elemeats lbs'11000jeallons Application Method N P205 X20 Ca Mg S Fe Mn ZI, Cu B Mo Cl Na Ni Cd Pb Al Se Li Irrigation 2.3 0,95 4.5 1.1 0,31 0.29 0.03 T 0.01 T 0:01 1.7 47 60"1 '), 7SP265 5� 'tNt' '64K 19Y w 7 L-O Grower: Southern Cross Farms copies TO: PO Box 242 Garland, NC 28441 wste Rehort na ysis 111,.r 11ann: 12/21/04 Sampson County iairiele ID: N P K Ca M S 1,.e A111 A Cu 8 AN ("I C i0000 f Tolul 338 47.4 397 134 39.6 39.6 3.12 0.31 0.74 ().15 0.83 IN -N Waste Code: -N114 .kES -NO3 Na Ni 01 Pb A/ Sc b P/1 SS C.-N R-11% CCEN ALEAjal 146 7.35 Description: OR-N kerobic Liquid - Swine Urea W69 'N utr en ailibW belleif MOM kolfbni r.Ewin6ts. 1bS11 000IgEllons, 4ppUcdqd;(Ae1bO v. X20 Ca :T n IlP, ncu' M' BilMo, -N" Cd Pb Al­S6 Lfd 79 iiL4 tt --,­l,4L'­!-- T 1:2 r U, ibilli6dun ess ot e-:"' pe Sample ID: N P K Cf, Mg. S Pe Alit zill (1,14 B ,No Cl C o60002 T01141 327 42.5 385 99.4 31.9 31.1 2.29 (H8 0.52 0.07 0.79 IN -N Waste Code: -N114 N E S NO3i Na Ni al PbA Al�11 Se IVII SS G:N DA1% CCP% ALE(Kgal) 137 7.40 Description: OR -IV Aerobic Liquid - Swine uru(j owo mmen t ofts. 4k;. !,- r"'.. enf94MAW rs ropq j, , _., . �V. 1#066M. 110 I "ga us 2 WWI en s - Aj)jjh6fioh"M'-e'AW'd`, N, ho 5,i (','a" k.T, "', I,.-,., . g, Hn Z11 : dl'! -'-f " CW' Pb Ali' _­Sd H Irription 1.4 ;57; 3 1 �8 0. 0.18 �­J 0' .0,01"', T ItIP:WU`r6z6VX9t0731- 26551f3�,, I Grower.- Southern Cross Farms Copies To: PO Box 242 � 4 V i,� 1, %6 Garland, NC 28441 Waste A R A� Nil. naiysis Phort Farm: 10/18/04 Sampson County widoia Sample ID: N P K Ca A19 S_ Fe Mn A Cu B MO (d c OOOOD Total 353 62.1 440 117 55.6 47.7 2,55 0.18 1.63 0.74 0.86 IN _N Waste code: -NH4 Na Ni Cd Pb Al Se Li PH SS ON DM% CCE% ALB AES -NO3 158 7.42 Description: OR-N Aerobic Li uid -Swine Urea rop: oififiiOi WE L'OthirEWE&C 'iEMIV VINE; T T in 11'11� r. I 1g: Z, �,�po _P�Ae,4*�IOPIT 11, —0. Alliokf6ryi. MRIM MiRIMM IMMM ;r; Owl& iii� mRZ � U& Sample ID: N P K Ca M S Pe Mn zn Cu B c 0 02, Total 352 68.6 462 136 62.1 31.7 5.45 0.21 1.05 0.20 0.95 IN -N Waste Code: -NH4 AES 403 Na Ni Cd Pb Al Se Li PH Ss C.-N DM% CCR% ALB Kgal L 167 TO DescHption: OR-N Aerobic Liguld - Swine Urea ��Xglqjv RM . lefw& El Offif"I AN el A MeIbU �OVPA�OIN& 1? • 1 PwFJ 4i yl, k-M, NaI'UNAIMO M O�9 49 nr.L 7' 1"." CDA ' `unomic:Dfvision ' Oi] Reed"'CreekRaad�Ralei°N°27G 7=64G 19 '�33255. Grove : 'C4i ; rt-No:4,W00 10 P .2 �u'le� i, 'Lab "t'o -lteaufis r,'q�i ioA�uniess'a er�ise:nated �t .� 4� P Sample LD: N P K Ca S Pe Mn Zn Cu B Mo C1 C `' ' Total 542 44.2 557 135 45.9 29.4 3.22 0.31 0.76 0.06 1.15 IN -N Waste Code: -NH4 Na M Cd Pb Al Se Li PH SS C.N DM% CCB% Ammap AES -NO3 Description: OR-N 188 7.44 Aerobic Liquid - Swine Urea Recommendations: Nutrients Available for First lbsqo00 gallom Other Eleitie' tv 1bOo00 allons ApplkatlofjMethod N P205 K20 CaMg S Pe "P,Mrt k' Zn.'ii, GY ,FB;F'.v Mo C! Na ".' 11RIF, Cd-.",Pb Al Se Ll Irrigstian 2.3 0.59 4.5 0.79 ^'`"0.27 0.17 0.02 .' q i; ' ?� _`.. •T 0.01 1.6 Sam le'Ido: LaboratoEy Results Or million unless otherwise ndt'ed Sample ID: 4 Waste Code: AES Description: Aerobic Liquid - Swine N P K Ca mg S Pe Mn Zn Cu B Mo C1 C Total 546 IN-N -NH4 403 OR-N Urea 53.6 666 136 50.8 33.7 3.71 0.31 0.93 0,11 1.25 Na Ni Cd Pb Al Se L! pH SS CN DM% GCE% ALB al 225 7.54 Recommendali"'" : Nutrients Available for First CO lb81000 allons Other Elements lbS11000 allasls Apfiftcafio& °' . Ir:lgalion 1FJ I:J N P 205 K 20 2.3 0' 32 5.3 Ca ?� ! ' Mg S Pa `• Ml1 i Zn 0 79 ,: 0.30 0.20 0.02 T r f� F 0 01 , d��il - t.l1• ill!{:.Yh.+w.•, Cu T 9 i 0.01 ..c, Mo CI • I Na 1:9 N! Cd. Pb Al Se L! "„"'Wlnfo::�.*P 4,. LabomtotyResults is kr'million unless Otliei wiso ttoted ; c ly' Sampk LO.- Waste Code: AES Description: Aerobic Liquid - Swine N P K Ca MR S Pe Mn Zn Cu B MO Cl C Total 441 IN -N -NH4 -NO3 OR-N Urea 44.9 448 113 41.1 19.3 2,14 0.25 0.59 0.16 1.00 Na Ni Cd Pb Al Se Ll PH SS ON DM% CCh% ALB al 159 7.65 Recommen ations: Nutrients Available for First Crg. M11000. allons Other Elements lbS11000 allons p fM#onI Metbod rrrigulon N P205 K20 1.8 0 66 3.6 Ca; Mg S Pe 0.%. 0.24 0.11 0.01 .Mn Z" T T Cu T B 0.01 Mo C1 Na 1.3 Nl Cd Pb Al Se Li NGDAA otleWivDivision. 4300 Reedy Creek Road; Raleig4, NC, 27,661.4465; 1 ,15S12655 ;. Grower: We Erlarms Inc. Re' 'rt,No: W00610 P9 3 Sam ' le �l O. I.etboroto Results of iaiilion unless otherwise noted "' <: Sample M. Waste Code: AES Description: Aerobic Liquid - Swine N P K Ca Mg S Pe Mn Zn Cu B Mo C! C Total 389 IN -N -NH4 -NO3 OR-N Urea 46.3 403 129 41.2 19.0 2.46 0.27 0.58 0.07 1.00 Na Ni Cd Pb Al Se if Pff SS C.•N DM% CCB% ALB al 141 7.62 ]kCcommetidations: Nutrients Available for First Crop. lbs/T000 galloni Other Elements lbs 1000 allow "' katari Metbod IrOpilon N P205 K20 1.6 0.62 3.2 CaS Fe Mn 0.75,~ 0.24 0.11 0.01 T Zn T Cu B Mo T, 0.01 ' Cl. Na Ni Cd Pb Al Se - Li Sam le info Laboratory Results rts. ' r million unless otherwise noted Sample ID: 7 Waste Code: AES Descrtplion: Aerobic Liquid - Swtne N P K . Ca 99 S Pe Mn Zn Cu B Ma Cl C Total 481 is -N -NH4 -NO3 OR-N Uroa 59.0 435 121 37.0 27.9 2.81 0.34 0.71 0.09 0.98 Na Ni Cd Pb Al Se Li pH SS C.N DM% CCB% ALB al 156 7.31 R"eomine>idations: Nutrients Available for First Oro lbs/T000 allans Other Elements W11000 gallaw plication Metbod Hgation N P205 K20 2.0 0.79 3.5 Ca Mg S Fe Mn 0.71 0.22 0.16 0.02 T A T Cu B MO T 0.01 Cl Na 1.3 Ni Cd Pb Al Se Li Sam 1e.hdo. Laboratory Results Per.milfien unless otherwise noted Sample ID: N P K Ca M9 S Pa Mn Zn Cu B Mo Cl C 8 Total 499 75.5 576 126 42.8 34.4 3.41 0.37 1.39 0.15 1.17 IN -N Waste Code: 1V114 AES -NO3 Na M Cd Pb Al Se Li pH SS C.•N DM% CC696 ALB(1C�� cdpNon.' OR-N 200 7.04 _ Aerobic Liquid - Swine Urea Recommendations: Nutilents Available for, First,Cre , 1411060 all & Other El'eliients lbs/1000; allows plicallonMetbod N P205 K20 Cap Mg' S Fe Mn Zn Cu B, Mo Cl Na ' Ni Cd Pb Al Se M Irrigation 2.1 1.0 4.6 0.73 0.25 0.20 0.02 T 0.01 T 0.01 1.7 IA Agronomic.Division 4300 Reed :Creek Raid Raleigh, NC 27647=6465 919 "733-2 55, Re rt',N6:. W04610. W Grower: Webber Farms Inc. Copies To: 350 Old White hall Rd 7/28/04 Ivanhoe, NC 28447 Wa is te Ana iys is RqP6, port Par= Sampson County le info. Laboratory Results arts per million unless otherwise noted ple ID. to Coder ription: bic Liquid - Swine N P K Ca M S Fe Mn Zn Cu B Mo 61 C Total 574 1N -N -N114 -NO3 OR-N Urea 39.9 626 117 33.9 19.2 3.03 0.25 0.76 0.16 1.26 Na Nf Cd Pb Al Se Li PH SS C:N DM% CCE% ALB al 212 7.65 ammendations: Nutrients Available for First Crop 1 s/1000 allons Other Elements 1bs11000 allmrs (cation Method rigation N P205 X20 2.4 0.53 5.0 Ca Mg S Pe Mn 0.68 0.20' m i 0.02 T Z-h Cu B Mo Cl T T 0.01 Na Ni Cd 1.8 Pb Al Se Lt c tuture, muttliple1arm samples need to be submitted on separate informatlon sheets per farm. This will aid in trucking and documenting your information through the Agronomic Division and the Division of r Quality. Thank you for your assistance. n Casteeli Agronomist - - le1dfo.. Laboratory Results is per million unless otherwise noted iple L11: ate Code: cription: ibic Liquid - Swine N P K Ca X S Fe Mn Zn Cry B Mo C1 C Tots! 432 IN -N -NH4 -NO3 OR-N Urea 41.1 637 127 38.3 19.6 3.90 0.30 7.33 0.15 1.37 Na Ni Cd P6 Al Se L1 H SS ON DM% CCE% ALB K al 218 7.48 ommendations: Nutrients Available for First Crop lbs/1000 allons Other Elements lbs/1000 Raubw lfcatfon Method •rigation N P205 K20 1.8 0.55 5.1 Ca Mg S Fe Mn Zn 0.74 0.22 0.11 0.02 T 0.04 Cu B Mo C1 T 0.01 Na Ni Cd 1.8 Pb Al Se Li 6 '�i - 6V r At, 0 1,�L04655 """ LX "K.43'66v Creek 'F" cc! 'C' k: Wi t'd -j -[277607-�.-�" Oj�..LY Wgio" i o'M""WDi n. ;Iel -,7 Grower- Southern Cross Farms Copies To: PO Box 242 4. Garland, NC 28441 Waste o rt Far.: Analysis RL,.,, 5/3/04 Sampson County Sample M, N P K Ca Afg S Fe Mn Z?i Cu R Mo G Total 625 60.7 453 196 49.7 18.3 5.66 0.54 1.76 0.42 0.49 IN -N Waste Code.- -N114 Na Ni Cd Pb Al Se Li PH SS ON /)M% CCF% ILEIAgal) AES -NO3 168 7.52 Description: OR-N Aerobic Liquid - Swine Urea Recommendations:" 11171T"e Nutflehts AVai AI 1"ii1V-1��lS , " ' : ' 6tig..le AppUqafioq'Mqtb4';`,— arriga!ion � -1 , Z r A 'C N B MO R 001"�lr 0 �29 n 4T, L"." "M ;7, lit W, Nqllsvio .,fLa oiratoey.11601 (Aitg,06, 0 4� SampleID: Jv P K Ca Mg IS Fe Mn 7n Ca B MO Cl C 02a Total 625 54.7 435 179 44.2 14.8 5.53 0.47 1.60 0,31 0.45 IN -N Waste Code. -N114 Na Ni Cd A At Se Li PH SE C-N l)M% CCE% ALL (Kgal) AES - NO3 161 7.63 Description: OR-N Aerobic Liquid - Swine Urea lk6C'O"M""M--6&t1 Onk"', 1�' T 420 .,"Ca ML zjii & e6 , i;i a XD;Z.� , - 411icOo ""0 26'j�. -y,0'09. 0 0 Itt �Ta "T.- ir4v9 A73 35 j,-��11,. Ard NN I -d . j V '�� Ali I Q C NCbA 'i',h ,,Reoovt!No: IW05921 Grower- Southern Cross Farms Copies To: Idaw4bkl PO Box 242 Garland, NC 28441 Waste nalysis Reh.rort l,ann: 2/6/04 Sampson County Sample Info: Laborato!y. Results (Pa ts.per;milli6n,unless.-otherwise'noted);: Sample ID: N P K (I'a Igg S k'e Mn 711 cl, B 01 Waste Code: AEIS 7101,11 546 IN -N -NIN -NO3 41,6 421 152 28.5 28.7 3.13 0.29 0.94 0.17 0.96 Na Ni Cd Pb Se U fiff SS (".1 Description: OR-N 147 Aerobic Uquid - Swine Urea A R&o&Mifl&t.iO"fi"§* Nutii` Apph�dlioij'M46d.,;, IVh05; 120, .'C RO 'N . ..... Mai 7 "VIO )M% L W, Alf P A S si " a b bartS,enniill wun ess,ot erw Z 'A. Sample ID.- 02 Waste Code: AES Description: Aerobic Liquid - Swine N P K Ca M s Fe Mn In Cu B MO CI C Total 553 IN -N -NIN -NO3 OR-N Urea 37.5 399 189 31.4 26.7 3.49 0,39 0.86 0.14 0.90 Na Ni Cd A 211 Se Li P/I ss C.-N /),Vf% (,CE% ALE(Kgal) 145 7.58 Recommenditibni: W1100OLallons MOON, gallons Application Method Irripflon N P205 K20 2.3 0.50 3.2 Ca Mg. I" 0 Mh, 2n 1.1 o.iB 0.,16 0.02 T 0.01 Cu B MO CI T 0,01 .6the"r'Tle'ments Na. Ni 1.2 Cd Pb 211 so Li ern 2008 Daily Rainfall/Weekly Lagoon Level Record Farm: c _ January Freeboard s ww" a+.a February Freeboard SwLeft" c+rat SUN MON F; WED THUR PFU SAT G G C) E) O Q 7 e 9 10 11 1'2 s 7 O O 0 o kJ `� 97 D © O J� 0 f1`� `� O O .�j ✓ 3 14 s is 17 is 19 10 1t 12 13 14 115 1s 27 20 r 22 23 24 n m 1 is 19 20 r C) C, CD o O., o 97 �) V �) V 79 L/ v V T �' ✓ O 1�7 March Freeboard srvvhr Chen April Freeboard ssl,ca w Q`M` SUN MON E VVED THUR m SAT SUN MON UR Fm I SAT 3 4 5 7 e r e 9 to 11 n C) C)".q L/ /,, 03 r� �U �� C C) L/ Q 9 to 11 12 14 is 97 13 14 1s 1tf 17 1e 1s is 11 1e 1920122 202, 22 27 4 25 m 23 24 25 25 26 29 3D 30 31 SwImars D4fea ¢� May Freeboard June Freeboard -SUN MON TUE WED (� U N WED UR FR1 SAT 1 2 3 ems'`' , 5 a7 e 9 10 a 9 10 11 12 13 14 11 O 12 /. 13 14 15 `/ 10 (�, 177 L/ 2 �✓ 15 L/ 1e L/ 17 16 19 20 21 V to V If 19 G 20 f� fL n I r L/ Y1 ,f L/ 73 G 4 C "Z Lr Yl `- 23 C_ ////�y�''' m 27 �) 25 r 4 25 C x> 31 20 Record rainfall daily. H dalhr rainfall totals 1 Inch or greater, initial in box that lagoon integrity has been checked. If pmdpWftn jamnowvvAto as S on date. Page 1 of 2 RMjE0 `: WIM Murphy -Brown- iM V A Daily Rainfall Record Retention Period: 3 Years Farm: _. — Revised: M1106 Page iof2 January February SUN MO TUE WED THUR FRI SAT SUN MON TUE WED THUR FRI SAT 12 3 5 3 d. �)' U C C 1 I6 C )` e9 f0 11 12 13 s 6 7 10 V o O. 4 c, u c c c V U c, c, o f f4 15 ,6 11 1e 19 2D 11 12 13 14 15 16 17 G l,-/ C/ � � � � 7 �.7 � // � l/ C. C� a 232A 2S 26 27 18 19 23 24 ^ r F3 29 30 31 n 1 26 27 26 C) v �', i✓ March April SUN MON TUE WED THUR FRI SAT SUN MON TUE WED I THUR FRI SAT 1 2 3 1 2 } 4 5 6 7 C? 1 � D O D D C) 3� 5 8 7 6 9 10 6 10 1, 12 13 14 C, G G O C) C, C, O D 3( 11 12 1u u 1s 16 17 15 16 v 1a 19 2D 21 ?- O C) C) C)r."� o Q C)D O O O 3 111 19 24 2� C) O D D D o D o O 26 127 29 30 31 2930 31 O o 0 C) C) o O D May June SUN MON TUE WED THUR FRI SAT SUN MON TUE WED THUR FRI SA 1 s t G O o D O C) 10 11 12 5 7e 3] C)O o C)O O C)%" C) 0. O D D S 0 �� 3 u 15 to 17 19 19 10 11 12 13 u 1.5 to 39 0 0 o C) D 1 122 24 25 26 17 1e 19 20 21 O 0 5 o O O o C) 2e 29 30 31 24 25 26 27 29 29 30 Yo D O O D �n In O D 0 O 0 Record rainfall daily. if daily rainfall totals 1 Inch or greater, initial In box that lagoon integrity has been checked and secondary containment is OK. If precipitation is snow, note as S on date. Fax to LNM at the end of every month. Murphy - Brown -Farm: -- ------ Daily Rainfall Record JLvvr Retention Period: 3 Years Revised: 8l31106 Pao-- 2 of 2 3q 9� July August SUN MON TUE WED THUR FRI SAT SUN E WED THUR FRI SAT 1 2 3 5 5 7 1 2 3 4 06 o u u e) o 0-� o 0 0 0 9 10 11 12 13 14 6 78 9 10 11 C0 © O C-) c� �� v Q c� O 0 C? c� 15 18 17 18 19 21 12 13 14 15 III VI III (fJ� fJy C, V C) (!) 0 : ` 1 Q D 22 23 24 25 25 27 28 19 21 22 21 24 25 c� o o o c� �} o d29 39 31 20 V 20 29 30 31 ,{ September October SUN MON TUE WED THUR FRI SAT SUN MON TUE WED THUR FRI SAT 1 1 2 5 V K' 1.0 3 4 7 8 7 8 9 10 11 12 53 C) 10 11 12 13 1• 15 14 15 s8 17 18 19 EIr/'�, O O 18 1 to 1 1 22 1 22 23 24 N 28 Q o CDQ D D //''�J o l Q �3 Q 1/ /f'� _-3•D ; 24 25 L o d November December SUN MON TUE WED THUR FRI _WT SUN MON TUE WED 1 THUR FRI SAT 1 2 3 1 5 8 7 8 9 10 3 5 8 7 8 01 C) o c 11 12 13 14 15 Te 17 51 10 11 12 13 14 15 C C D 0• � (0 C 0,(D 0 C,--) 0, 18 19 20 1 24 18 17 18 19 20 21 -: C)C rcE% D cn o 0 5 29 27 28 29 30 23 74 25 28 Z7 211 29 e Q 23 31 rceovra ra>Imall aairy. R carry ratrnan totais 1 inch or greater, Initial in box that lagoon integrity has been checked and secondary containment is OVL If precipitation is snow, note as S on data. Fax to LNM at the end of every month. 3C?h C l 0 q0 yo 3 33D p ')(0 02/07/2008 TUE 0:01 FAA 9102033138 WRLNNI 0 001/002 BitfW�l ..r 200$ MMY RsirdWMW"dy Limon Lave! Record Few junmv Fed mk.0 Fttm ry Frecb08Td era ffi1�[ IMM RIPa ku= Tanm aa. ea. R" Cial� ■ ffiffismEffiffims FAJ PAAJ son man@ smseemmmm FPFMPAENM,, A09A 519A M" ENO I mm,., mmomm. It daily reinfeti totes 1 inch or gre&W, ka! In Ism do "am intagdty has been chocked. ��� 02/07/2006 TUB 9:01 FAX 9102933138 WRLNNI 19002/002 Alurphy-Brown,., 2006 Daily RainfalllWeekly Lagoon Level Record farm• July Freeboard skucc,s August Freeboard swuakwsl SUN MM TUES vsED THUR FRr SAT C1oft SUN NON TUES WM THUR M SAT a'e` 1 � o o o d Ca ).o 33 10 C) �8 to ti n 14 is M l) 1, » ,s a is » 1 22 20 21 23 isss © o•q o c> O �� d �� I.0 C) 0 3� M ft 29 77 22 A 27 p 30 CJ al O l 1 Septeetber Freeboard stmrsaM October Freeboard UwAse SUN UON TT*S WED TI*M FM SAT Cho* stm mom TUES WED THUR FM SAT s2 5� i 2 s c) 4 c, c 7 a Q a 15 r ,IN 6 c 0 p.s 10 0 $1 GC', r2 t] C) w c: � 17 » 1 o O© ( 0 0 a 7 1� o� f00 it snf 14 17 71 a ii 7a C', 75 C', C) TI November Freeboard $VN MON TOES WeD THUR FM SAT swuu" a"`* December Freeboard sty MON TUES WED THUR FM SAT sr.ce:r Gnaw 1 G T c , js 1 O 11 3. G t? 0 $4 L5 M 17 R ro ( n » u ! 29 C' 70 G 2. �.% 25 C/ 29 28 V tf daft rairdaJI totAs 1 Inch Or breMer_ tndlal to box that iar50bn intanrity hnA hoon r-har_kad. �VILir P1 i V "LJ f v ", . F of v n /Z _ SS Daily Rainfall/Weekly Lagoon Level Record Farm: , r J��� January Freeboard February Freeboard m ns MMffiMMMMM;,O■�iii�ii March Freeboard April Freeboard Freeboard oa" yr war, auE - I uuww" Has Omw cieeC- Daily Rainiall/Weekly Lagoon Level Record Farm: Cl July Freeboard SUIKA al August Freeboard Stuca m CAeck SUN MON TUES WED THUR FRI SAT Crock SUN MON TUES WED THUR FRI SAT i D 0 0-;, 0 D 0 X 2 3 D O O b O D D � j�o O 0 �} 0 d C) 0 , 12 13 14 s 6 4 5 a T a V (`� O 0 D O 0 1.1 D © O D D(D T 6 920i 22 i D D 0 o 0 O-q 30 0 o © o O o 0 0 1 0.b September Freeboard Se„ I&xal I October Freeboard Sracbmal SUN MON TUES WED THUR FRI SAT Check 5UN MON TUES WED THUR FRI SAT Chetic A.ku x- by -Brown Farm. -. Daily RainfalINVeekly Lagoon Level Record LUU4 January Freeboard St1„a1,ra1 February Freeboard s9ur�,rar SUN MON TUES WED THUR FRI SAT ctlee1 SUN MON TUES WED THUR FRI SAT r'rback 1 2 3 1 2 3 4 s a 7 O D C U 0 (� 0 0 4 15 6 7 a 9 10 a 9 10 11 12 13 14 ©� o 0 n o 11 12 13 14 15 lie 17 15 16 V to 19 20 21 D o o 1a 19 20 21 22 23 24 22 23 24 25 26 27 28 V.a� t7 O 0 o 0 0 0 0.6 0 0 0 1�- 25 26 27 26 29 30 31 29 lJ D 0 Q 0 March Freeboard Srucalrai April Freeboard s�umrdt SUN MON TUES WED THUR FRI SAT a1eC SUN MON TUES WED THUR FRI SAT aleck 1 2 3 4 5 6 1 2n/�, 3 0 G 0 © v 7 a 9 10 11 17 13 4 5 6 R 7 6 9 10 u D d o CD 0 0 o.q- 1 0 0 14 1s is 17 16{{��� 19 20 11 12 13 14 15 10 17 D O C)C Q Q D C)C)© Q 21 22 23 24 25,,,((�� 26 27 16 19 20 21 ?s 23 24n 0 C)0 V 0 0 0 0 © *� 26 29 30 31 25 29 27 23 79 30 o© o o. 0 h? o© 0 D May Freeboard Svumrai I June Freeboard sanrmm-211 SUN MON TUES WED THUR FRI SAT rheck SUN MON TUES WED THUR FRI SAT C*(* 1 1 1 12 14 s o.s o 13 0 0 0.s 2 3 4 5 a 7 is 6 7 a 9 110 11 12 10 0 0 (9 0 G C) c Q O O' S O 9 10 11 12 /3 14 15 13 14 15 to 17 16 19 0 o os o C) 0 n o O 0 .S 16 17 10 19 20 21 22 26 21 22 23 2� 25 20 0 0 0 0[ 3 24 25 25 27 25 29 27 ze 29 30 os © � ° � o ° 0.3 p p •� n 31 �� fl 02/12/03 't �-1'• • --a-���� 4�a�1� 4 ;..,..4.........-�4ar inifisl in Iv1r thaf I�nnnn int4anrity has hwa>!n (:hRC_ICAf1. klur=,tsn own ,,,: Y�o�.+-ti-. � -1� �' N�Daily RainfalllWeek#y Lagoon Level Record Farm;� (J July Freeboard Swcwral August Freeboard Svucwrai SUN MON TUES WED THUR FRI SAT Check SUN MON TOES WED THUR FRI SAT Cpeck 1 2 3 1 2 3 4 5 fi 7 n.3 0 030S0.1 110 0.9 o-+ 0 s 6 7 6 9 10 e 9 10 11 12 13 14 �p 0.3 0 © D o p 0.8 D o c� o o 09 .4 11 12 13 14 15 16 17 is 16 17 to 19 20 21 ry7 0--7 0-3 0 0 0 0 0 1-a a o-44 n 0 r_o 16 19 20 21 22 23 24 22 23 24 25 26 27 20 03 0.9l, p d 0 0 0 0 0 0 0 0 08 5 26 27 2e 29 30 31 29 30 31 0 0 0 0 10 0 0 0-s 0-g o September Freeboard S9uclural October Freeboard Sbixb"I SUN MON TUES WED THUR FRI SAT Check SUN MON TUES WED THUR FRI SAT Check 1 2 3 l i 2 1.1D 0 0 0 0 o .1 e 7 e 9 10 11 3 4 5 5 1 6 9 o 0 0 0 0 0 0 0 12 13 14 15 16 17 is 10 11 12 13 14 15 19 n© o© 0 0 0.9 o 0 0 0 0 o.4 0 19 20 21 22 23 24 25 17 10 19 20 21 22 23 p +0 d 0 o 0 0 0 0 0 0© 0 0 27 26 29 30 24 25 26 27 74 29 36 iC) 0 0 0 0© 0 0 31 0 November Freeboard S1nxalrai December Freeboard s:uc>,xal SUN MON TUES WED THUR FRI SAT check SUN MON TUES WED THUR FRI SAT Check t 2 3 4 5 11 2 3 4 0 0 o O 03 0 © 0 0 7 6 9 10 12 13 5 6 7 e 9 1p 11 0 0 0 o o 0 13 O o D 0 0 14 fs it 17 1a 19 20 12 13 14 1s 19 17 18 0 0 0 0 0 0 0 0 0 0 0 0 o v 1 22 23 24 25 25 27 19 20 21 22 23 24 25 o o- q 0.91 0 0 0 0 0 0 0 03 0 29 30 25 27 2e 29 30 31 p p. 0.4 0 0 p cD 02112103 •• • _•• -- . _.- . 1.__l_ _- _-..-- 9..1a:-1 :.. 6.... N..�4 h..w.+++ in9nnriflr Mao Moen rhaa!`4eA t ❑ Yes ❑ No ❑ NA ONE ❑ Yes ❑ No *® NA ❑ NE ❑ Yes ❑ No ❑ NA W NE ❑ Yes ❑ No ❑ NA EKNE ❑ Yes [3 No ❑ NA ❑ NE ❑ Yes ❑ No ❑ NA 29NE ❑ Yes ® No ❑ NA ❑ NE ❑ Yes ❑ No ❑ NA ® NE ❑ Yes XNo ❑ NA ❑ NE 5a Yes ❑ No ❑ NA � N�_ ❑ Yes JF,No ❑ NA ❑ NE 0 Yes ❑ No ❑ NA ❑ NE Facility Number: — Date of Inspection S"" 1- Required Records & Documents 19. Did the facility fail to have Certificate of Coverage & Permit readily available? ❑ Yes ❑ No ❑ NA ® NE 20. Does the facility fail to have all components of the CAWMP readily available? If yes, check ❑ Yes ® No ❑ NA ❑ NE the appropirate box. ❑ WUP ❑ Checklists ❑ Design ❑Maps ❑Other 21. Does record keeping need improvement? If yes, check the appropriate box below. ❑ Yes ❑ No ❑ NA ONE ❑ Waste Application ❑ Weekly Freeboard ❑ Waste Analysis ❑ Soil Analysis ❑ Waste Transfers ❑ Annual Certification ❑ Rainfall ❑ Stocking ❑ Crop Yield ❑ 120 Minute Inspections ❑ Monthly and 1" Rain Inspections ❑ Weather Code 22. Did the facility fail to install and maintain a rain gauge? 23. If selected, did the facility fail to install and maintain rainbreakers on irrigation equipment? 24. Did the facility fail to calibrate waste application equipment as required by the permit? 25. Did the facility fail to conduct a sludge survey as required by the permit? 26. Did the facility fail to have an actively certified operator in charge? 27. Did the facility fail to secure a phosphorus loss assessment (PLAT) certification? Other Issues 28_ Were any additional problems noted which cause non-compliance of the permit or CAWMP? 29. Did the facility fail to properly dispose of dead animals within 24 hours and/or document and report the mortality rates that were higher than normal? 30. At the time of the inspection did the facility pose an odor or air quality concern? If yes, contact a regional Air Quality representative immediately 31. Did the facility fail to notify the regional office of emergency situations as required by General Permit? (ie/ discharge, freeboard problems, over application) 32. Did Reviewer/Inspector fail to discuss review/inspection with an on -site representative? 33. Does facility require a follow-up visit by same agency'? Additional -Comments and/or Drawings: ry K /`urn p� i r► To T%ti 1,Uo Dds �rs Page 3 of 3 12128104 Facility Number: —% Date of Inspection Waste Collection & Treatment 4. Is storage capacity (structural plus storm storage plus heavy rainfall) less than adequate? ❑ Yes ❑ No ❑ NA R] NE a. if yes, is waste level into the structural freeboard? ❑ Yes ❑ No ❑ NA ❑ NE Structure I Structure 2 Structure 3 Structure 4 Structure 5 Structure 6 Identifier: Spillway?: Designed Freeboard (in): Observed Freeboard (in): 5. Are there any immediate threats to the integrity of any of the structures observed? ❑ Yes ❑ No ❑ NA (2 NE (ie/ large trees, severe erosion, seepage, etc.) 6. Are there structures on -site which are not properly addressed and/or managed ❑ Yes ❑ No ❑ NA t4 NE through a waste management or closure plan? If any of questions 4-6 were answered yes, and the situation poses an immediate public health or environmental threat, notify DWQ 7. Do any of the structures need maintenance or improvement? ❑ Yes ❑ No ❑ NA W NE 8. Do any of the stuctures lack adequate markers as required by the permit? ❑ Yes ❑ No ❑ NA ONE (Not applicable to roofed pits, dry stacks and/or wet stacks) 9. Does any part of the waste management system other than the waste structures require ❑ Yes ❑ No ❑ NA NE maintenance or improvement? Waste Application 10. Are there any required buffers, setbacks, or compliance alternatives that need ❑ Yes g No ❑ NA ❑ NE maintenance/improvement? l . Is there evidence of incorrect application? If yes, check the appropriate box below. ayes ❑ No ❑ NA ❑ NE 19 Excessive Ponding CR Hydraulic Overload ❑ Frozen Ground ❑ Heavy Metals (Cu, Zn, etc.) [:]PAN ❑ PAN > 10% or l0 lbs ❑ Total Phosphorus ❑ Failure to Incorporate Manure/Sludge into Bare Soil ❑ Outside of Acceptable Crop Window ❑ Evidence of Wind Drift ❑ Application Outside of Area 12. Crop type(s) `7) eVrmujn 13. Soil type(s) 14. Do the receiving crops differ from those designated in the CA W M P? ❑ Yes CQ No ❑ NA ❑ NE 15. Does the receiving crop and/or land application site need improvement? ❑ Yes ❑ No ❑ NA ® NE 16. Did the facility fail to secure and/or operate per the irrigation design or wettable acre determination?❑ Yes ❑ No ❑ NA M NE 17. Does the facility lack adequate acreage for land application? ❑ Yes ❑ No ❑ NA CONE 18. Is there a lack of properly operating waste application equipment? ❑ Yes ❑ No ❑ NA ONE �Comments'3{refer to yuestton:#) Explain y YES-"answerstandloreny. recommendations or aoy other#eomme_nts. Use drawings of facility to hetter�eaphunrsEtuations. (use additi "I.pages assnecessary } �e'F�� u1 @ v- FGy o�,c� �-; (6lortri� CP J'a a/- F,,U s,, i��"'-4'T� ZX / �e+sd�i� cue,s':5�jpor? e. �am_� /ZOjj irrFT rI�aJ Guam ST /fret acted Th c 1���` Ovy�v�" /f4�,� �d�7�F Reviewer/inspector Name hone: 3 t� Reviewer/Inspector Signature: Date: •' rage 6 Of J alJLO/VV %-Uralarauca (8'Division of Water Quality LLM2� Number 0 Division of Soil and Water Conservation D Other Agency Type of Visit ompliance Inspection 0 Operation Review 0 Structure Evaluation 0 Technical Assistance Reason for Visit 0 Routine O Complaint ollow up O Referral O Emergency O Other ❑ Denied Access Date of Visit: Arrival Time: ��' [� Departure Time: O County: Region: Farm Name: Owner l✓mail:. Owner Name: V 'I m- W JA J1 N'—e- Phone: Mailing Address: D • L A, t/ e. Physical Address: Facility Contact: ��ir� i a s o Vet 2_ ., Zi - Z Title: Onsite Representative: Certified Operator: 15110_� Sack-up Operator: Location of Farm: Swine. Phone No: 9 Integrator: 4DLO YL- Operator Certification Number: / 9A%41K Back-up Certification Number: Latitude: 0 0 0 I = 11 Longitude: = ° = 6 = f4 Design Current Design Current Capacity Population Wet Poultry Capacity Population ❑ La er ❑ Non -Layer ❑ Wean to Finish ❑ Wean to Feeder ❑ Feeder to Finish ❑ Farrow to Wean ❑ Farrow to Feeder ❑ Farrow to Finish ❑ Gilts ❑ Boars Other ❑ Other Dry Poultry ❑ La ers ❑ Non -Layers ❑ Pullets Turkeys ❑ Turkey Poults 1❑ E1 Other Discharges & Stream Impacts 1. is any discharge observed from any part of the operation? Discharge originated at: ❑ Structure ❑ Application Field ❑ Other a. Was the conveyance man-made? Design Current Cattle Capacity Population ❑ Dairy Cow ❑ Dairy Calf ❑ Dairy Heifer ❑ Dry Cow ❑ Non -Dairy ❑ Beef Stocker ❑ Beef Feeder ❑ Beef Brood Co Number of Structures: b. Did the discharge reach waters of the State? (If yes, notify DWQ) c. What is the estimated volume that reached waters of the State (gallons)? d. Does discharge bypass the waste management system? (if yes, notify DWQ) 2. Is there evidence of a past discharge from any part of the operation? 3. Were there any adverse impacts or potential adverse impacts to the Waters of the State other than from a discharge? ❑ Yes ❑ No ❑ NA ®,NE ❑ Yes ❑ No ❑ NA ❑ NE ❑ Yes ❑ No ❑ NA ❑ NE ❑ NA ❑ NE ❑ Yes ❑ No ❑Yes ❑No ❑NA ®NE ❑ Yes ❑ No ❑ NA $-NE Page I of 3 12128104 Continued Facility Number: X Date of Inspection Waste Collection & Treatment 4. Is storage capacity (structural plus storm storage plus heavy rainfall) less than adequate? ❑ Yes ❑ No ❑ NA C! NE a. If yes, is waste level into the structural freeboard? ❑ Yes ❑ No ❑ NA ❑ NE Structure 1 Structure 2 Structure 3 Structure 4 Structure 5 Structure 6 Identifier: Spillway?: Designed Freeboard (in): Observed Freeboard (in): 5. Are there any immediate threats to the integrity of any of the structures observed? ❑ Yes Cl No ❑ NA E9 NE (ie/ large trees, severe erosion, seepage, etc.) 6. Are there structures on -site which are not properly addressed and/or managed [:]Yes []No ❑ NA ONE through a waste management or closure plan? If any of questions 4-6 were answered yes, and the situation poses an immediate public health or environmental threat, notify DWQ 7. Do any of the structures need maintenance or improvement? ❑ Yes ❑ No ❑ NA ® NE 8. Do any of the stuctures lack adequate markers as required by the permit? [:]Yes ❑ No ❑ NA [3NE (Not applicable to roofed pits, dry stacks and/or wet stacks) 9. Does any part of the waste management system other than the waste structures require ❑ Yes ❑ No ❑ NA (9 NE maintenance or improvement? Waste Application 10. Are there any required buffers, setbacks, or compliance alternatives that need ❑ Yes ❑ No ❑ NA ®.NE maintenance/improvement? 11. Is there evidence of incorrect application? If yes, check the appropriate box below. ❑ Yes ❑ No ❑ NA [ZNE ❑ Excessive Ponding ❑ Hydraulic Overload ❑ Frozen Ground ❑ Heavy Metals (Cu, Zn, etc.) ❑ PAN ❑ PAN > 10% or 10 lbs ❑ Total Phosphorus ❑ Failure to Incorporate Manure/Sludge into Bare Soil ❑ Outside of Acceptable Crop Window [:]Evidence of Wind Drift ❑ Application Outside of Area 12. Crop type(s) 13. Soil type(s) 14. Do the receiving crops differ from those designated in the CAWMP? ❑ Yes ❑ No ❑ NA PR�NE 15. Does the receiving crop and/or land application site need improvement? ❑ Yes ❑ No ❑ NA C12111.NE 16. Did the facility fail to secure and/or operate per the irrigation design or wettable acre determination?[:] Yes ❑ No ❑ NA 4NE 17. Does the facility lack adequate acreage for land application? ❑ Yes ❑ No ❑ NA LONE 18. Is there a lack of properly operating waste application equipment? ❑ Yes ❑ No ❑ NA RIVE h fir, rJ u,:;,. ��°�'�" ! ,�. w�oo[s lra� 6,��,�,p j_--a% 7- 11 4Q 1'L 4,C Q-_-:� 7 a Lj brrlt Gt� /4 d:�_4e_II - t'� 7-D Reviewer/inspector NameI '�' p-'^ Phone: ,3r3 3 �0 Reviewer/Inspector Signature: Dater D Page 2 of 3 12128104 Continued Facility Number: — Date of Inspection Re aired Records & Documents 19. Did the facility fail to have Certificate of Coverage & Permit readily available? ❑ Yes ❑ No ❑ NA M NE 20. Does the facility fail to have all components of the CAWMP readily available? If yes, check ❑ Yes ❑ No ❑ NA ®NE the appropriate box_ ❑ WUP ❑ Checklists ❑ Design ❑Maps ❑Other 21. Does record keeping need improvement? If yes, check the appropriate box below. ❑ Yes ❑ No ❑ NA ® NE ❑ Waste Application ❑ Weekly Freeboard ❑ Waste Analysis ❑ Soil Analysis ❑ Waste Transfers ❑ Annual Certification ❑ Rainfall ❑ Stocking ❑ Crop Yield ❑ 120 Minute Inspections ❑ Monthly and V Rain Inspections ❑ Weather Code 22. Did the facility fail to install and maintain a rain gauge? ❑ Yes ❑ No ❑ NA PNE 23. If selected, did the facility fail to install and maintain rainbreakers on irrigation equipment? ❑ Yes ❑ No ❑ NA t.NE 24. Did the facility fail to calibrate waste application equipment as required by the permit? ❑ Yes ❑ No ❑ NA [ NE 25. Did the facility fail to conduct a sludge survey as required by the permit? ❑ Yes ❑ No ❑ NA aNE 26. Did the facility fail to have an actively certified operator in charge? ❑ Yes ❑ No ❑ NA (INE 27. Did the facility fail to secure a phosphorus loss assessment (PLAT) certification? ❑ Yes ❑ No ❑ NA (ONE Other Issues 28. Were any additional problems noted which cause non-compliance of the permit or CAWMP? ❑ Yes ❑ No ❑ NA [ENE 29. Did the facility fail to properly dispose of dead animals within 24 hours and/or document ❑ Yes ❑ No ❑ NA D9NE and report the mortality rates that were higher than normal? 30. At the time of the inspection did the facility pose an odor or air quality concern? ❑ Yes ❑ No ❑ NA aNE If yes, contact a regional Air Quality representative immediately 31. Did the facility fail to notify the regional office of emergency situations as required by ❑ Yes ❑ No ❑ NA 9NE General Permit? (ie/ discharge, freeboard problems, over application) 32. Did Reviewer/Inspector fail to discuss review/inspection with an on -site representative? ❑ Yes ZNo ❑ NA ❑ NE 33. Does facility require a follow-up visit by same agency? ❑ Yes allo ❑ NA ❑ NE Ad"diti6nal,Co7rhments:and/or Drawitigs - F,� 74- 'vie c< �/�t31z- we'l­i3 e-o l/eC 7rp/ ` Page 3 of 3 12128104 #D6x6 ?.LGi FAX COVER SHEET 910401-1920 T0: i FROM: DATE: RE: PAGES (INCLUDING COVER); NOTE, C,5/ "2/20C-; 1 53 y10S3-72="_ 5u__a�1`3- :ASS n?`! rG516 ?.E62 ER Srq., Z UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION 4 ATLANTA FEDERAL CENTER 61 FORSYTH STREET fq< ptE� ATLANTA, GEORGIA 30303-8960 IMY 7 Wg CERTIFIED MAIL 7008 2810 0000 4316 5074 RETURN RECEIPT REQUESTED Webber Farms Inc - Santiago Vazquez, Farm Manager 350 OId Whitehall Road Ivanhoe, North Carolina 28447 RE: Southern Cross AWG100000 (Certificate of Coverage Number AWS820144)---:�, Dear W. Vazquez: On May21, 2008, the U.S. Environmental Protection Agency (EPA) and North Carolina Department of Environment and Natural Resources (NCDENR) perforated a Compliance Evaluation Inspection (CEI) on the Southern Cross (Facility). The results of BPA's CEI are surainarized in the enclosed report. EPA's participation in this inspection was to evaluate the Facility's compliance with the requirements of Section 402 of the Clean Water Act, 33 U.S.C. § 1342, the regulations promulgated thereunder at 40 Code of Federal Regulations Part 122.23. If you have specific questions or need additional information, please contact Nk. Maurice Horsey of my staff at (404) 562-9764. Sincerely, CikA'-07 - Christopher P1ymale, Chief East NPDES Enforcement Section Water Protection Division Enclosure cc: Keith Larick, DNER, NC Division of Water Quality Steve Guyton, NC DNER. Fayetteville Regional Office Intemet Address (URL) - httpJlwww.epa.gov RecvdedlAecyctabte • Printed with Vegetable 09 Based Taft ae BcgdM PNW (LW&nurn 30 k Po-4 5'D2i2iiy _Q3 �I%,:,3220=_ i United States Environmental Protection Agency Washington, Q.C. 20460 &EM Wow Compliance Inspec&m Report Section A: Ng nal Data Svstem Codi i.e., p Transaction Code NPOES yr/mdday Inspectim Type Inspector Fac Type N AWS8MI44 200IIAOS21 = T 3 Remarks I—Peofim Wait Days Facility Sall -Monk ruig Evaluation Rwirq Bi QA .----�.......� ._. Section B. Faci[14 Data Name and Loon of Fad* Inspected (Fork4aftW users aschargrrg fo PO7W, also i wkjde P07'W name and NPDES pemrft numb r Frr>ry Tunfi/flate Date Webba Fear* Inc., (Southern Cross) 3403 W. Mag:soha Lisbon Rd Rose tLiEI NC 28458-7750 (. NC) ]PemilEffecve 2.15 05J2I M8July I- 20(Y7 F,ct Time/Date 4 05pM 05J21108 Permit F�etati0n Data September 20. 2008 Name(s) of oil -Site Representative(s)ffitie(syphone and Fax Numbers) t�go 3350 OId Whctzhall Ltd Other Fa fity Data rre.g", SIC NAIC& and olfrer deseripDve rnfomre�on) Ivanhoe. Ne 28a47 Name, Address of ResoonsUe OffoaVrdelFftne and Fax NwbeT Vazquez, Farm!ufanager 350Whitehall Rd Ivanhoe, NC 29447 910.6692663 (o). 910.669.2gWf) Section C: Areas Evaluated Durina I Check only otiose areas evaluated Permit Self-M ordming Program Pretreatment M54 R eports Gpmpli 0100 Schedules Ponubm Prevention x I=acility Site Review Labor=ry Storm water EfituentlReceiving Waters Operations & Maintenance Combined Sewer overflow Flow Mmsurement Sludge HandlinglDisposat Sanitary Sewer Overflow . Section D: Summary of lindsngsCComments Affach additional sheers of ►rarraiive and checklists mludyiy S" Ie Event Vlolairon codesas necessa SEV Codes SEV Description ❑�r, �id Name(s) and S" re s of ! s /OtNce/Pharte and Fax Numbem Date Lisa McKinley. Environmardat SGi 5t 404 56Region 4 404.5622- .9403 (0), 404.5629Ci4a (f) 5/4k Maurice Horse Eovironrnental Engin y EPA Region 4 404.562.9764 (0). 404"562"9343 (f) � � l a re of Management Q A Reviewer 44JUCChief DES Ento�Section Agency/Ofk&T hone and Fax Numbers US.EPA Region 4 404"562"9794 (0), 404.562.9M (i) Date �' 06/02/2009 -.: a y105322681 SOU_i12RN-CROSS nPARM #0646 P.004 EPA Reeion 4 CAFO Itt�on Checklist Date: May 21, Zl1il8 Entry Time: 2:15pm Emit Time: 4:05pm Inspector's Name: Maurice Horsey Inspector's Phone Number: 404562.9764 The EPA, State and Facility contacts are present on site during inspection. Name Aaencv/Offlce/Phone Numbers Lisa McKinley US EPA, Environmental Scientist, 404-562-9403 Christine D. Blanton NCDENR, Animal Feeding Operations Unit, 919-715-6627 Steve Guytoa NCDENR, Fayetteville Regional Office, 919-433-3300 Santiago Vazquez Webber Farms, Farm Manager, 910-669-2663 A. FACILITP BACKGROUND 1. Type of Inspection - mark one: x Compliance Complaint Follow-up Other 2. Facility Name Address LatitudedLongitude Owner Name Phone Number Mailing Address (street) City/StateJZip Weather Conditions Webber Farms Inc_, (Southern Cross) 3403 W. Magnolia Lisbon Rd. Rose Hill, NC 28458-7750 (Garland, NC) 34 54 52.3 N, - 7819 35.1 W Santiago Vazquez, Farm Manager 910-669-2663 Webber Farms Inc. 350 Old Whitehall Rd. Ivanhoe, NC 29447 P. Cloudy 3. Location -Provide directions 3403 w Magmlia Ubbon Rd Rose Hill, NG 2S458 (910) 552-Mi 2 _... _ 3.6 ni (abort 9 u knij 157 8 2.9 mi 0.7 mi 06/02/2C,CU !0:54 9105322E41 SOITHER`i CROSc F ;Rh1 #Q6�6 P. GD5 B. CONCENTRATED ANIMAL FEEDING OPERATION (CAFO) DETERNUNATION Number and Type of animals confined and feeding at this facility: (Note that this and the days confined must be verified with the site representative or through site records) Type of Animal Maintamed or fed targc CAM (No. of Animab) Medium CAM (No. of Anima$) No. Animals Dairy Cause 700 200 - 699 Cagle (sir) low 300 - 999 swioc (over 551txs) moo 750 - 2.499 3600 Swine (k= 9= 55 UN) 10,000 3 OOO - 9.999 Horse 500 150 - 499 Steep or L garbs 10.000 3,000.9,999 Turkeys 55.000 16.500 - 54.999 Laying Heal or Boilers ( Wet Sys-) 30.000 9,000-29.949 Cb *= 125.000 375W - 124 999 Laying liens 82.000 25,000 - 81.999 Duda 30.000 10.000 - 29,999 Duds ( Wet Sys-) 5,000 1 S00 - 4,999 otlxr. TUTALS 3600 1. Number of days animals are stabled/confined and fed/maintained over any Twelve month period: X 45 Days or more Less than 45 days 2. Note that much of the remained of this section can be verified by OBSERVATION! i Name and location of surface water (stream, river, canal, lake) to which a discharge would be received? UT to Beaver Dam Creek thence to Clear Run ii. Did you see an actual discharge to the aforementioned surface water? X Yes No iii. is potential to discharge from the facility through a man. -made device? Yes X No 3 061C'2/2009 -I C • jY �iC-�322B=i c ' _G�.i_..=�.�i-CP.GS� _—?S: #0645 2.DG5 3. What is the 25-year, 24 hour rainfall amount for this location (in inches)? (question is best answered by contacting the MRCS or weather station) 6.5 1 inches 4. Can the animals confined on the CAFO come into direct contact with surface water of the United States? Yes X Na If YES, please provide location and name of receiving stream: 5. Are fences used to restrict access? 7i Yes No C. PERNUT INFORMATION NPDES Permit Number AWS820144 (Please make note of any general permit) Note: General State Permit or Certicate of Coverage Issued July 1, 2007. Date Issued: _July 1, 2007 Expiration Date: September 30, 2009 Compliance Schedule(s)? Yes X No Note if any compliance schedule exists - If so, provide a brief description CommenwSwnmary. The Facility is not permitted under NPDES General Permit but rather has a North Carolina, Certificate of Coverage (COC): Certificate of Coverage No. AWS820144 issued to Jim Walker, authorizing the operation of the subject animal waste management system in accordance with (State) General Permit AWG 100000 Environmental Protection Agency (EPA) Region 4's Water Protection Division and North Carolina Department of Environment and Natural Resources, Division of Water Quality staff inspected Webber Farms Inc., Southern Cross (The Facility), located off of Southern Cross Road, Rose Hill (Garland) North Carolina, on May 21, 2008 to assess the compliance status of this farm with the Clean Water Act (CWA). Weather condition on the day of the inspection was P. Cloudy but clear when arriving at the facility. Mr. Vazquez, Farm Manager, informed EPA and NC DENR that the facility had. seven (7) barns and 3600 sows on -site at the time of inspection. Liquid animal waste from the 7 barns flushed into a six (6) acre lagoon. 4 16:55 9103322541 2Ou__._�N-rapac -Ap.M_ #0645 ?.irc D. WASTE HANDLING Provide a brief sketch of the site: Based on information available on the day of the inspection, are solid and/or liquid waste handled properly to prevent surface and/or ground water pollution? Yes No If no, explain: A Based on information available qn the day of inspion, has tie iqW&=s6pfip6 facility ' been maintained at a level so it will reta% a 25 year -year 4=�iour�.fall event?- . - ..., 2 - Yes f No y If no, explain: { Is manure stored onsite? Yves -".,No If YES, what type "bf storage is used?= t:" Clay -lined ea &en basin Above -ground concrete tank Poured concrete's Manure pack on lot or floor Earthen holding basis-. Glass lined steel tank Concrete block or stale pit Aerated lagoon Stacking slab } "� other .r ;w- How often is the storage area scraped or emptied? _ times per year. What is the slope of the storage area? 0-4% 4-8% 8-12% 12% or more The topography in the manure storage area is: (check one) Hilltop Hillside Foot of Hill Low Land Narrow ravine Valley Other What additional process wastes are generated at the facility? C•l ii0-a322_ARM #0646 ?.00; wash water from cleaning pens dust from ventilation systems litter and/or bedding wash water from cooling animals pesticides/fertilizers/herbicides wormers cleaning solutions carcasses (dead livestock) other Are any of the following used for odor control? Daily/Weekly measure of water level in retention lagoon: Yes No Number of freeboard violations: Weekly measure of water level in storm water retention/detention facility Yes No Daily rainfall records (from on -site rain gauge) - Yes No 7 05/C,2/2009 10:55 9105322$4i SDu: 2r*+—CtiOSS =?;Rri ##G&s5 P.{LL{ Log of manure sold or given away Yes No Date, location, and amount of manure and/or lagoon basin waste applied to cropland/sprayfield? - Yes No Did you perform sample calculation? -Yes No Weekly. quarterly, annual inspection, maintenance and inspection reports maintained? Yes NO Log of preventive maintenance and For those question in Part E marked as "No," NbWtoring Records......contmued a. Has the facility had a discharge Discharge reported to EPA? Description and cause of d- �} Period of dischargeW Sampling date, tinA and flow path Individual co yarnp le Analyses dates and t" n.6 Individual perforininhWyses Analytical methods/techni 't;k F. POLLUM completed Yes No amide some additional details. "-6' Yes No � .. Yes No Yes No Yes No =Yes No Yes No -_� Yes No Yes No PPP on file, si ''* updated, maintained and/or implemented. M -* Yes No The PPP shall include, at.. urn: A. Description of potential pollutant sources 1. Site map indicating an outline of the drainage area; each structural control measure, surface water bodies. Yes No 2. List of significant materials that are used, stored, and disposed of at CAFO. Yes No 3. List of significant spills. Yes No 4. List of significant spills, such as pesticides, cleaning agents, fuel, and other pollutants. Yes No 8 QElC2i2C{y 10:56 9-10S322c:1 30:_-E,N—C309a Waste Management Controls 1. Permanent marker installed and maintained within the lagoon to show water level? Yes No Does it show the water level required for a 25-year, 24-hour rainfall event? Yes No 2. Rain gauge installed and maintained? Yes No 3. Design standards for retention facility embankments? Yes No 4. Is there a schedule for liquid waste remd_V_C S. Liner requirements information a, Documentation and certification of n hydrologic connecti b. Liner construction in rdance to S.S. 716 or its current eauiv ` t 5. Adequate wasteater removal anInd application a. irrigated washes, ater removal ~ land applic b. irrigate when the ga5und is frozen . r saturatedor while it is raining equi mew 1`8Pp11c:allCrn G. SAMPLING Has the facility had a discharge? If Yes, continue to the nei f:gtiestions-. if NOT, STOP! Sample Collected? Is the location adequate for a representative sample? Yes No icWnote P Yes No :i'es No Yes No Yes No Yes No Yes No Yes No Parameters and sampling agzee with the requirements set forth in the permit? Yes No Sample collection procedures adequate proper preservation techniques used, Yes No sample holding tunes before analysis in conformance with 40 CFR 136? Yes No 0 . `7'..-_. _ r �.r.OSS i,z?r•� �G5;6 ?.C+i[" If No, please explain: Laboratory Information EPA approved analytical testing procedures used? Yes No If alternative analytical procedures are used, proper approval has been obtained? Yes No Contract laboratory used? Contract laboratory state certifi41 es Lab Name: -� Lab Address) Lab Telephi3a;e: Lab Come8 A 10 December 5, 2001 Mr. Santiago Vasquez 350 Old Whitehall Rd. Ivanhoe, NC 28447 Dear Santiago, Regarding the problems cited in the NOV issued for Southern Cross Farm, will outline the likely causes of the problems and the remedial recommendations we discussed in our previous meetings at the farm. L Maintaining Coastal Bermudagrass Stand in Waste Application Fields. The sudden loss of stand in the traveller application areas in the spring of 2000 was the result of prolonged suppression of spring "green -up" due to competition from the overseeded winter annual. I see this problem often on swine operations which are land -tight or storage -limited on their CAWMPs. The management of a system where overseeding bermudagrass hayfields with winter annuals must be done every year will always be problematic, and will sometimes require new, inconvenient, and more expensive practices in order to make these systems work. When hybrid bermudagrass is managed for hay, stands will already be relatively thin in terms of the abundance of growing points (stolon nodes) at the ground surface. Some of those growing points are routinely lost during the winter. During the fall, winter, and early spring, although dormant, bermudagrass is still alive and is therefore respiring and using up reserves of carbohydrate stored in the roots. Overseeding bermudagrass with cereal rye or other winter grasses always delays the green -up of the bermudagrass in the springtime, and the longer the overseeded crop remains on the field, the slower the recovery of the bermudagrass will be. If the overseeded crop is not harvested until May (or later), the bermudagrass will be in a weakened condition and will have lost a lot of growing points. After the overseed is harvested, the field will have a lot of bare ground and and very little coverage by bermuda stolons or crowns. Temperatures will favor weed emergence, and there will be no bermuda foliage there to compete with the predictable explosion of crabgrass and other summer annual weeds. At this time we do not have any labelled pre-emegrent herbicides to control these summer weedy grasses. There can be additional factors in the growing environment that exacerbate the delay in green -up and the early -season vigor of the bermudagrass, and I believe that is the case at Southern Cross. Following my initial consultation on July 18, 2001 regarding the stand loss problem, I returned to the site and took a diagnostic sample from the edge of the affected area in field 1 for a nematode assay. The results of that assay revealed a substantial population of Sting nematode attacking the roots of the bermudagrass. This organism is a pest to many crops, including turf and forage grasses, but problems are not frequently observed due to the particular soil requirements of the nematode. Because it is physically the largest phytoparasitic nematode, it requires substantial pore space in soil, L e. coarse sandy soil, for populations to thrive. You are farming on just such soils at Southern Cross. Once we have the assay results of the samples we collected yesterday (December 4, 2001) we can determine the extent to which this pest has been spread across the farm. This does not mean that you can't grow good bermudagrass on this site, but it adds another degree of stress to the crop (and the manager). In most years the symptoms of Sting nematode are most pronounced in (1) early spring when soils are cool and/or (2) during periods when the crop is under moisture and nutrient stress. The Latter conditions are unlikely to be a factor on a large swime farm, but the early spring nematode stress exacerbates the effects of the overseeding stress I previously mentioned and further reduces early vigor. Recommendations: 1. Identify and map the areas in the fields with poor stand now before the rye cover obscures them, and estimate acreage that will need to be replanted. 2. Apply lime as recommended by soil test. 3. Graze heavily the fields that have areas to be replanted in February, and have the land prepared by early March. 4. Dormant sprigs can be replanted anytime after mid February. I definitely recommend planting dormant sprigs rather than sprigs which have already broken dormancy. Make sure the sprigs are freshly dug, preferably on the same day they are planted. Plant at least 40 bushels of sprigs per acre. 5. Once the replanted bermuda starts to emerge, use your irrigation to reduce stress during dry weather, but be aware that you will also be stimulating the growth of summer annual grasses and broadleaf weeds. 6. Allow the emerged bermuda to root well before grazing so that cows won't pull up sprigs. 7. But do make judicious use of grazing and mowing (for hay) to reduce the competition from summer annual grasses. Herbicides can be used for broadleaf weeds, if needed. 8. Expedite the addition of fields to your waste plan so that you can periodically give some relief to fields from annual overseeding. 9. Continue using grazing animals as much as possible to manage both the bermudagrass and the overseed. Grazing will be the best way to maintain a dense and healthy sward. I rarely see stand loss problems where the sprayfields are rotationally grazed rather than hayed. 10. Make sure that overseeded crops are heavily grazed by early April, preferably to the point that they cover no more than one-third of the ground at that time. If haying is used again, harvest the overseeded crop at or before boot stage. This will usually mean harvesting as silage or wrapped balage. A second harvest of regrowth will usually be necessary. 11. If haying management is used again, harvest the bermudagrass at least four times during the season in order to promote lateral spreading and maintain an acceptable number of growing points at the ground surface. 11. Remediation of Erosion on Lagoon Dam Based on our discussion, the erosion on the back side of the lagoon dike began with the torrential rains of the storms of 1999. That sort of erosion was probably facilitated by the character of the vegetation on the slope, clumpy grasses and tall weeds. That type of vegetation (1) fails to provide sufficient cover to break the impact of raindrops striking the soil, (2) offers little resistance to slow the flow of water down the slope, and (3) shades out the spreading dense types of grass, such as bahiagrass and bermudagrass that are preffered. Preventing erosion is critical in order to maintain the strength and integrity of the structure. I'm not qualified to evaluate the threat posed in this particular situation, but it clearly needs repair. Some portions of the dam slope could be graded and reseeded, but there are some long stretches that have severe gullies and will need to be filled in and resloped in order to protect the integrity of the structure. Recommendations. 1. We discussed using your tractor and front loader to spread soil on the dam, but in reconsideration, I would suggest that you hire a contractor with a small tracked loader to do both the hauling and grading. The tracked loader can be used more effectively and safely to grade and "track" or compact the fill. 2. You'll need to consult with Wilson Spencer or with a Murphy -Brown engineer to make sure you get the slope restored to design specifications. 3. Try to obtain a sandy clay loam soil for fill rather than the sands available on the farm; you'll want a soil that will compact well. Avoid using ublack creek" clay. 4. As soon as the fill is graded, take a soil sample, but don't wait for lab results. Go ahead and apply immediately one tonlac lime and 500 Ib/ac 10-10-10 fertilizer. Incorporate these in the graded area 4 inches deep with a disk or rotovator. Then track" compact the slope — one time over should suffice. You want the slope firm but you don't want to destroy soil structure in the root zone. You can apply the additional lime and fertilizer recommended later. 5. Immediately seed rye at 140 Iblac or tall fescue at 40 Iblac, mulch well with wheat straw, and secure the mulch in place with plastic or jute netting. 6. In April or early May you should consider the permanent vegetation. If you seeded tall fescue and have obtained a good stand, you can maintain the dam in that grass. If you planted rye, you will need to mow and remove it and plant either bahiagrass or common bermudagrass. That can be done by no -till drilling seed or vegetatively with plugs planted on a 2' x2' alternating grid. 7. Mow frequently (every other week) to control competition from summer weeds. 8. The inner face of the dike can also be revegetated by planting plugs. Some filling or grading may be warranted at the spots where we noted erosion. Again, regular mowing will help greatly in obtaining a stand and stimulating lateral spreading of bermudagrass and/or bahiagrass. I hope these recommendations will prove useful to you and I will be happy to work with you to implement them. Sincerely, Tim Hall Regional Agronomist NCDA&CS PO Box 444 Richlands, NC 28574 91 D-324-9924 tim.hali@ncmail.net AL. ' . State of North Carolina Department of Environment, Health and Natural Resources Fayetteville Regional Office James B. Hunt, Jr., Governor Jonathan B. Howes, Secretary fflu�w'j 1DEHNR DIVISION OF WATER QUALITY June 17, 1997 CERTIFIED MAIL REMRN RECEIPT REQUESTED Mr. Mike Leu Murphy Family Farms P. O. Box 759 Rose I-ML N. C. 28458 SUBJECT: NOTICE OF DEFICIENCY Southern Cross Swine Farm Facility No. 82-144 Sampson County Dear Mr. Leu: On May 27, 1997 and June 13, 1997, staff from the Fayetteville Regional Office of the Division of Water Quality conducted compliance inspections as a result of a complaint at Southern Cross Swine Farm to determine compliance with their certified animal waste management plan (CAWMP). At the time of the investigation our staff confirmed that the facility had a CAWMP, however, no waste application fields were available. A third party agreement with an adjacent land owner had been rescinded and the swine farm owner was in the process of preparing waste application fields for planting Bermuda grass. In addition, the lagoon level was high and the lagoon dikes were in the process of modification. The lagoon dikes had been elevated approximately twelve inches to allow for more storage capacity . One area of the dike had approximately twelve inches of freeboard at the time of the initial inspection. On the subsequent inspection the area of the dike with the 12 inches of freeboard had been filled with a sandy material. This repair and the elevation of the lagoon dikes must be inspected and approved by the local NRCS office to confirm and document that this modification meets their standards of construction. On the return inspection of the Southern Cross facility on June 13, 1997 approximately 15 acres of bermuda grass had been sprigged. Pumping had been initiated by Santiago Vasquez the certified operator for the Shadow Glen and Webber Swine Facilities, however, the registered operator with the Division of Water Quality for this facility is no longer employed with Southern Cross. The Division of Water Quality may proceed with additional actions against Southern Cross Swine Farm, unless the following items are addressed: Wachovia Building, Suite 714, Fayetteville N%aW FAX 910-486-0707 North Carolina 28301-5043 C An Equal Opportunity Affirmative Action Employer Voice 910-486-154 i 50% recycled/10% post -consumer paper Page 2 Mr. Mike Leu June 17, 1997 1. Immediately plant the required crop (coastal bermuda) per your Certified Animal Waste Management Plan (CAWMP) in the proposed waste application fields to allow for the application of waste at agronomic rates. 2. Immediately register the certified operator for the Southern Cross Swine Facility. 3. Immediately consult with the Sampson County MRCS office in regard to the modification of the Lagoon dikes and appropriate action required to meet their construction standards, and in regard to the issuance of a new CAWMP with the appropriate waste application fields, crops, application rates, etc. 4. Consult with the Sampson County Agriculture Extension Office in regard to possible options available for establishing a cover grass to prevent erosion on the lagoon dikes. Nothing in this letter should be taken as absolving this facility of the responsibility and liability of any violations that have or may result from these deficiencies. If you have any questions concerning this matter, please do not hesitate to contact me at (910) 486-1541. Sincerely, Robert Heath Environmental Specialist KTS/RFH cc: Operations Branch Central Files Audrey Oxendine, FRO, NC DSWC Wilson Spencer, Sampson County NRCS F A M I L Y F A R M S Paul E. Rawls Regional Water Quality Supervisor Fayetteville Regional Office Division of water Quality 225 Green Street Suite 714 Fayetteville, NC 28301-5043 Mr. Rawls, n 19 2000 I am writing on behalf of the Southern Cross Farm, Facility No. 82-144, in response to the NOV issued by your office on 11/22/D0. Before responding to the complaint, please understand that your letter regarding this offense was received on 12/12/00. As required, we are responding within 7 days of knowledge of notification. It is alleged in your notice that `an investigation reveakcd that wastewater was being over sprayed onto the adjacent property'. To the best of our knowledge, any over spray that might have occurred would have fallen on a farm path adjacent to the field in question. The farm path is on the property of the farm, therefore, not on `adjacent property'. The reports that 1 received from the on farm representative present during the inspection indicated that there was no waste ponding on the road, only a damp area of soil. We do not dispute that the damp area was due to irrigation water, however, it appears that only 15-20' of the spray pattern was out of the field area. In calculating acreage covered by an irrigation pattern, the outside 10-22% receives no credit. This is because the amount of water falling on this area of the spray pattern, as compared to the inner portion, is of little oonsequence. In fad, many irrigation designs that I have seen, many done by PE's, allow this `ineffective' area to fall in non -wetland areas bordering the spray field. If the investigator in this case is aware of areas on adjacent land, not owned by the producer, or wetland areas that were sprayed with effluent, then we concur with the violation as issued If, however, his findings were based solely on the damp area observed on the path, we would ask that you reconsider the issuance of this NOV- The Southern Cross Farm will make every effort to irrigate its effluent in compliance with all rules and regulations. Care will be taken in the future, as in the past, to prevent over spray from occurring outside of the field and property boundaries. If there are any questions or concerns regarding this docun—, please feel Alee to call meat (910) "a 11 11. 12/14/W Post Office Box 759, Rose Hill, North Carolina 28458, (910) 289-2111, FAX (910) 289-6400 NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES FAYETPEVILLE REGIONAL OFFICE DIVISION OF WATER QUALITY March 20, 2000 Lacwmml Di�� L '4_1..►a!_.1_ 1 1 Mr- Jim Walker P.O. Box 798 Garland, NC 28441 SUBJECT: NOTICE OF VIOLATION Permit No. AWS 820144 Southern Cross Farm Facility No- 82 - 144 Sampson County Dear Mr. Walker: You are hereby notified that, Having been permitted to have a non -discharge permit for the subject animal waste disposal system pursuant to 15A NCAC 2H .0217, you have been found to be in violation of your 2H -0217 Permit. On February 24, 2000, staff from the Fayetteville Regional Office of the Division of Water Quality performed a routine fly -over of the Southern Cross Farm looted off Highway 903 in Sampson County. During the fly -over, it was observed that the facility was irrigating and wastewater was ponding and appeared to be entering a wooded area adjacent to the field. After the fly -over, a site visit was made to the facility to confirm the observations from the flight. An inspector upon arriving at the farm investigated the sprayfield and the adjacent woodland and confirmed the discharge. The Division of Water Quality requests that the following items be addressed: 1. Provide a detailed explanation as to why the runoff from the spray field occurred. 2. Inspect the waste application field prior to pumping to ensure that future discharges of this nature do not recur. 225 GREEN STREET, SUITE 714, FAYETTEVILLE, NORTH CAROLINA 28301 -5043 PHONE 910-486-154t FAX SIO-4a6-0707 AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/SO% POST -CONSUMER PAPER Mr. Walker Page 2 March 20, 2000 3. Immediately evaluate and determine what corrective actions can be implemented to prevent wastewater from running off the field in the future. Your response should be received by this office on or before March 30, 2000. Failure to comply with the above conditions may result in the facility's General Permit being revoked and being required to obtain an individual non discharge permit for the facility. Please be advised that this notice does not prevent the Division of Water Quality from taking enforcement actions for this violation or arty past or future violation. Furthermore, the Division of Water Quality has the authority to levy a civil penalty of not more than $25,000.00 per day per violation. If you have any questions concerning this matter, please do not hesitate to contact either Mr. Robert Heath, Environmental Specialist or myself at (910) 486-1541. S r , 0. Paul E. Rawls Regional Aer Quality Supervisor cc: Sonya Avant - Compliance Group Wilson Spencer - Sampson Co. NRCS Trent Allen - DSWC Fayetteville Office Central Files - Raleigh Dr. Garth Boyd - Murphy Farms NORTH CAROL.INA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY FAYETTEVILLE REGIONAL OFFICE November 22, 2000 CERTIFIED MAIL RETURN RECEIPT REQUESTED 7099 3400 0011 1134 5486 Mr. Jim Walker P.O. Box 798 Garland, NC 28441 SUBJECT: NOTICE OF VIOLATION Permit No. AWS820144 Southern Cross Farm Facility No. 82-144 Sampson County r Dear Mr. Walker: You are hereby notified that, having been permitted to have a non -discharge permit for the subject animal waste disposal system pursuant to 15A NCAC 2H .0217, you have been found to be in violation of your 2H .0217 Permit. On November 13, 2000, staff from the Fayetteville Regional Office of the Division of Water Quality, performed a site visit in response to a complaint concerning over spray of wastewater from the Southern Cross Farm located off Highway 903 in Sampson County. Inspectors, upon arriving at the farm, investigated the spray field and the adjacent area. The investigation revealed that wastewater was being over sprayed onto the adjacent property. Confirmation of the over spray was based on wet areas of wastewater beyond the designated boundaries. The Division of Water Quality requests that the following items be addressed: Provide a detailed explanation as to why the over spray from the spray field occurred. 2. Inspect the waste application field prior to pumping to ensure that future discharges of this nature do not recur. 3. Immediately evaluate and determine what corrective actions can be implemented to prevent over spray and wastewater from the field in the future. : fR GROUNDWATER SECTION 225 GREEN STREET, SUITE 714 / SYSTEL 13L0. FAYETTEVILLE, NORTH CAROLINA 28301-5043 PHONE: 910.486-1541 FAX: 910-486-0707 AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED / 10% POST -CONSUMER PAPER DENR TOLL FREE HOTLINE: 1-877-623-6748 Mr. Walker Page 2 November 22, 2000 Your response should be received by this office on or before November 30, 2000. Failure to comply with the above conditions may result in the facility's General Permit being revoked and being required to obtain an individual non -discharge permit for the facility. Please be advised that this notice does not prevent the Division of Water Quality from taking enforcement actions for this violation or any past or future violation. Furthermore, the Division of Water Quality has the authority to levy a civil penalty of not more than $25,000.00 per day per violation. If you have any questions concerning this matter, please do not hesitate to contact either Ms. Belinda Henson, Environmental Chemist, or myself at 910-486-1541. Sinc e , ul E. Raw s Regional Water Quality Supervisor BE:PER/bs cc: Sonya Avant - Compliant Group Wilson Spencer - Sampson Co. NRCS Trent Allen - DSWC, Fayetteville Office John Bizic - Murphy Farms Central Files - Raleigh '�Iv NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES FAYETTEVILLE REGIONAL OFFICE DIVISION OF WATER QUALITY - March 20, 2000 CERTIFIEDA! Mr. Jinn Walker P.O. Box 798 Garland, NC 28441 SUBJECT: NOTICE OF VIOLATION Permit No. AWS 820144 Southern Cross Farm Facility No. 82 - 144 Sampson County Dear Mr. Walker: You are hereby notified that, having been permitted to have a non -discharge permit for the subject animal waste disposal system pursuant to 15A NCAC 2H .0217, you have been found to be in violation of your 2H .0217 Permit. On February 24, 2000, staff from the Fayetteville Regional Office of the Division of Water Quality performed a routine fly -over of the Southern Cross Farm located off Highway 903 in Sampson County. During the fly -over, it was observed that the facility was irrigating and wastewater was ponding and appeared to be entering a wooded area adjacent to the field. After the fly -over, a site visit was made to the facility to confirm the observations from the flight. An inspector upon arriving at the farm investigated the sprayfield and the adjacent woodland and confirmed the discharge. The Division of Water Quality requests that the following items be addressed: 1. Provide a detailed explanation as to why the runoff from the spray field occurred. 2. Inspect the waste application field prior to pumping to ensure that future discharges of this nature do not recur. 225 GREEN STREET, SUITE 714, FAYETTEVILLE, NORTH CAROLINA 28301-5043 PHONE 91 O.4a6-1541 FAX OIO-466-0707 AN EQUAL OPPORTUNITY /AFFIRMATWE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER r . Mr. Walker Page 2 March 20, 2000 3. Immediately evaluate and determine what corrective actions can be implemented to prevent wastewater from running off the field in the future. Your response should be received by this office on or before March 30, 2000. Failure to comply with the above conditions may result in the facility's General Permit being revoked and being required to obtain an individual non -discharge permit for the facility. Please be advised that this notice does not prevent the Division of Water Quality from taking enforcement actions for this violation or any past or future violation. Furthermore, the Division of Water Quality has the authority to levy a civil penalty of not more than $25,000,00 per day per violation. If you have any questions concerning this matter, please do not hesitate to contact either Mr. Robert Heath, Environmental Specialist or myself at (910) 486-1541. S' r , c GN Paul E. Rawls Regional Water Quality Supervisor cc: Sonya Avant - Compliance Group Wilson Spencer - Sampson Co. MRCS Trent Allen - DSWC Fayetteville Office Central Files - Raleigh Dr. Garth Boyd - Murphy Farms State.of North Carolina Department of Environment and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Director Jim Walker 3403 West Magnolia Lisbon Road Rose Hill NC 28458 Dear- Jim Walker: October 22, 1998 1•• NCDENR NORTH CAROUNA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RECEIVED 2 S 1998 FAYET��i;;E ��LgLI Subject: Notice of ViolatiotPi kPJc:ar_tid"n`for Nonpayment Southern Cross Farm Permit Number: AWS820144 Sampson County In accordance with North Carolina General Statute 143-215.10G, all animal operations who receive an animal waste management system permit will be charged in each year of the term an annual permit fee. Annual permit fees are billed following the issuance of the permit and then annually thereafter on the anniversary of that date_ Your animal waste management system permit was issued on 8/10/98. Y,.'nir annual permit fee for the period of 8/10/98 - 8/9/99 is $200.00. Your payment was due 10/3/98. Because this fee was not fully paid within 30 days after being billed, this letter initiates action to revoke the subject permit. pursuant to 15 NCAC 2H .0205 (c) (4). and G.S. 143-215.1 (b) (3). Effective 60 days from receipt of this notice, the subject permit is hereby revoked unless the required Annual Animal Waste Management System Permit fee for your animal operation is received within that time. Operation of an animal waste management system without a valid permit is a violation of North Carolina General Statute 143-215.1 and is subject to the assessment of a civil penalty of up to $10,000 per day. Your payment should be sent to: N.C. Department of Environment and Natural Resources Division of Water Quality Budget Office P.O. Box 29535 Raleigh, North Carolina 27626-0535 If you have any questions, please contact Fran McPherson at (919) 733-7015 ext. 210. Since ly, cc: Non -Discharge Branch Compliance/Enforcement Unit Fayetteville Regional Office Sampson County Health Department Permit File P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled / 10% post -consumer paper NORTH CAROLINA DEFARTMENTrOF ENVIRONMENT AND NATURAL RESOURCES FAYETCEVILLE REGIONAL OFFICE DIVISION OF WATER QUALITY April 20, 1998 Mr. Tun Walker 3403 West Magnolia Lisbon Road Rose ITill, N. C. 28458 SUBJECT: NOTICE OF VIOLATION Southern Cross Swine Farm Facility No. 82-144 Sampson County Dear Mr. Walker: On February 24, 1998, staff from the Fayetteville Regional Office of the Division of Water Quality conducted a follow up inspection at Southern Cross Swine Farm to determine compliance with their certified animal waste management plan (CAWMP). At the time of the investigation our staff confirmed that the facility had overapplied animal waste to the spray fields resulting in ponding and runoff into wetlands. The lagoon structure had approximately 14 inches of freeboard at the time of the inspection. The Division of Water Quality requests that the following items be addressed: 1. Begin immediately to investigate the condition of the sprayfields prior to waste application and apply waste at agronomic rates to prevent ponding and runoff. 2. Lower the lagoon level to the required freeboard on a suitable crop at agronomic rates as soon as weather permits. st�•�r.`.=.iatii4L:. 'tip?Y 1' v 225 GREEN STREET, SUITE 714, FAYETTEVILLE, NORTH CAROLINA 28301-5043 PHONE 91 O-486-1541 FAX SI O-486-0707 AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/1 O% POST -CONSUMER PAPER Mr. Walker Page 2 April 20, 1998 Please be advised that this notice does not prevent the Division of Water Quality from taking enforcement actions for this violationn or any past or future violation. Furthermore, the Division of Water Quality has the authority to levy a civil penalty of not more than $10,000.00 per day per violation. Please provide a written response to this office on or before May 15, 1998, regarding corrective actions taken or planned. If you have any questions concerning this matter, please do not hesitate to contact either myself or Mr. Robert Heath, Environmental Specialist, at (910) 486-1541. If you have any questions concerning this matter, please do not hesitate to contact me at (910) 486-1541. Sincerely, r C" Kerr T. S ens Regional upervisor KTS/RFH cc: Operations Branch Central Files Audrey Oxendine, FRO, NC DSWC Wilson Spencer, Sampson County NRCS A NCDENR. , JAMES 8. HUNTJR}' . GOVERNOR 4. f n Y s WAYNE MCDZVIfT .� SECRETARY 41V NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES FAYETTEVILLE REGIONAL, OFFICE DIVISION OF WATER QUALITY December 28, 1998 CERTIFIED MAIL RETURIN RECEIPICREQUESTED Mr. Jim Walker P. O. Box 759 Rose Hill, N. C. 28458 SUBJECT: NOTICE OF DEFICIENCY Southern Cross Swine Farm Facility No. 82-144 Sampson County Dear Mr. Walker: On December 8, 1998, staff from the Fayetteville Regional Office of the Division of Water Quality conducted an annual compliance inspection at the Southern Cross Facility. At the time of the investigation our staff confirmed that the facility had several deficiencies requiring correction. The lagoon dikes have received excessive traffic resulting in the loss of vegetation. Waste application records (IRR-1 forms) were available for the year; however, no IRR-2 forms have been completed for the facility resulting in posble over - application. In addition, the certified operator is no longer affiliated with the facility. The Division request that the following items be addressed: immediately complete the waste application records for the facility (IRR-2 forms) for the previous 12 months and submit a copy to this office for review. 2. Immediately register the certified operator for the Southern Cross Swine Facility. 225 GREEN STREET, SUITE 714, FAYETTEVILLE, NORTH CAROLINA 20301-5043 PHONE 810-486-1541 FA% OI O-486-0707 AN EQUAL OPPORTUNITY /AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER Southern Cross Farm Page 2 December 28, 1998 3. Consult with the Sampson County Agriculture Extension Office in regard to possible options available for establishing a cover grass to prevent erosion on the lagoon dikes. Nothing in this letter should be taken as absolving this facility of the responsibility and liability of any violations that have or may result from these deficiencies. If you have any questions concerning this matter, please do not hesitate to contact me at (910) 486-1541. Sincerely, Robert Heath Environmental Specialist KTS/RFH cc: Operations Branch Central Files Audrey Oxendine, FRO, NC DSWC Wilson Spencer, Sampson County NRCS N-CDENR. u '- JANIES B. HUNT.IR:ij'��; `' ' '•IWAYNE MCL3EVITi;t e ' SECRETA_RY'`" NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES FAYETTEVILLE REGIONAL OFFICE DIVISION OF WATER QUALITY December 28, 1998 + RTI>FEEn3t4IL RETURN RECEIPT REQUESIED Mr. Jim Walker P. O. Box 759 Rose Hill, N. C. 28458 SUBJECT: NOTICE OF DEFICIENCY Southern Cross Swine Farm Facility No. 82-144 Sampson County Dear Mr. Walker: On December 8, 1998, A fifrom the Fayetteville Regional Office of the Division of Water Quality conducted an annual compliance inspection at the Southern Cross Facility. At the time of the investigation our staff confirmed that the facility had several deficiencies requiring correction. The lagoon dikes have received excessive traffic resulting in the loss of vegetation. Waste application records (IRR-1 forms) were available for the year, however, no IRR-2 forms have been completed for the facility resulting in posible over - application. In addition, the certified operator is no longer affiliated with the facility. The Division request that the following items be addressed: Immediately complete the waste application records for the facility (IRR-2 forms) for the previous 12 months and submit a copy to this office for review. 2. Immediately register the certified operator for the Southern Cross Swine Facility. 225 GREEN STREET, SUITE 714, FAYETTEVILLE, NORTH CAROLINA 28301-5043 PHONE 910-486-1541 FA% 91 O-486-0707 AN EQUAL OPPORTUNITY / AFFIRMATIVE ACT10N EMPLOYER - 30% RECYCLED/10% POET -CONSUMER PAPER Southern Cross Farm Page 2 December 28, 1998 Consult with the Sampson County Agriculture Extension Office in regard to possible options available for establishing a cover grass to prevent erosion on the lagoon dikes. Nothing in this letter should be taken as absolving this facility of the responsibility and liability of any violations that have or may result from these deficiencies. If you have any questions concerning this matter, please do not hesitate to contact me at (910) 486-1541. Sincerely, Robert Heath Environmental Specialist KTSIRFH cc: Operations Branch Central Files Audrey Oxendine, FRO, NC DSWC Wilson Spencer, Sampson County NRCS Li AY 1 1 1998 FAYETTEVIL.LE REG. OFFICE SoudmM CMN Swine Form. 3M Waal MWoliaUmbm Rd. Rose Hell, N.C, 2USS Mr. Km r wcnoa WVmm •f Weter Qaity 2n maw Strad. Sd W 714, msymsv■e, Wsmtk Ca<+ay" 2030"m beck Res feaae N Mice of VldmdmL Fwft Nmrabef 82-144. co.ety May 3, Ing i► _ _Tm i received yaw kfier is May 4. 1"ll ad fly 1 cadatsed Mr. FmAn Moray the pzamm diet mpmvbm my Sams to Noah Cm*m m and Mr Jamb de Is Tom*, the cesti&ed aperntor and farm nears d Saatlawe GlnM Thep &ddl kmar a ebm6 ibis pebvuhw case of Violaboo ffid took plsce m Febmarp the 246L Tky daWt racft around to date *d you meatian I" told me dtd is due lest hmpedioa, me hmpecktr fend serene tra& of funnius webs in am of the feel& and be r m*vd the dosest wadmd for aam bpm water, and he didWt find my. bowever m hk report be wrotr: owsh r nm a$ an the f eld'. bat this happened an March due 318L And eamaa}ag d and &e iac� of Febmnsry &a 24tlf. 190 we we not trying to my " d didaft lnppeo, vdt we are ssyimg is that we dddt know about it. 0o600y cammficl6d ns mitber ves aNy aar by wrWA& Howmar, m dlembd do Divisma of Wsmr QmhW - We bane RIM* inveadgated by deodl me cmdbioo of id of oar mprry fields, We have been c>:e&igg every specific field prior to wsate spphcmfiom L- Our hWeaa ievel is new 36 mdm Sroe board I would 1e3oe to Wbe dim qpmoily to let you know thel we have been wmlang bard to kVnwe our epnqfi,,idq we leave umde ognsficaat =Wmveame for the last year nut vie will keep ivVg*v" usd your staff as well as aara we a 100% sEftfied with our Saeoerely 9'oers. Sa &= Chat Fmmm Ix WATER QUALITY COMPLAINT FORM County: Date Received: Time: Complainant (if known) : Telephone No. z- 7 2 Address: e��6rr Nature of complaint: ,tom,, t Locations and Directions: - 4 Z1-,V ,✓ �' Investigator:/ - Date: 7 Time In: 3 1 Time Out: Observations:---- 1,2 Supervisor Approval Signature: Date Murphy -Brown LLc December 6, 2001 Mr. Paul Rawls Water Quality Regional Supervisor NC Dept. of Environment and Natural Resources 225 Green St., Suite 714 Fayetteville, NC 28301-5043 Re: NOV issued to Southern Cross Farm, Sampson Co. Mr. Rawls, PO Drawer 856 2822 Hwy. 24 West Warsaw, NC 28398 Tel: 910-293-3434 Fax: 910-293-6957 D -F ENR � IDEC 10 2001 On behalf of the Southern Cross Farm, I am forwarding the following response to a NOV issued by you to the Southern Cross Farm in Sampson County. In the NOV letter, three items were outlined as reasons for the issuance of the violation These reasons were poor bermuda stand in some areas of the spray fields, isolated erosion of the lagoon dike, and farm records being off -site at the time of the inspection. I will respond to each of these items individually. In your letter, there was concern expressed with regard to the stand of bermudagrass in certain areas of the spray field. We understand that it is important to maintain a viable stand of the desired grass species in areas receiving animal wastes. The Southern Cross Farm has worked diligently on this issue since it was noted on the 2000 inspection of this facility. They had been in contact with Mr. Tim Hall, NCDA Regional Agronomist, on numerous occasions, and he had visited the site on July 18, 2001, to provide recommendation to the farm on this issue. Mr. Hall provided recommendations, and the farm has been following these recommendations. You understand, however, that issues regarding bermuda stands can not be fixed immediately in most cases, and implemented changes take time to produce results. We feel that the farm acted responsibly in identifying this deficiency and soliciting the appropriate professional help. I have attached a letter from Mr. Hall to the farm outlining his recommendations. These recommendations will be fully implemented, and should correct any future deficiencies in this area. in addition, I feel that it is important to note that this farm applies far fewer nutrients to its fields than are outlined in the WMP. This is due to management of water usage and the efficiency of the lagoon on this site. This is important to note because not fully fertilizing bermuda stands can lead to stand issues, and the intrusion of weed grasses. This farm removes forages in a timely manner, and records indicate that nitrogen that has been applied, has been removed. The second issue noted was an erosion area on the back side of the lagoon. This area of erosion began in 1999, and there have been numerous efforts since this date to correct the problem. Once again, Mr. Tim Hall has provided recommendations on addressing this issue, and these recommendation are being implemented. The third issue referenced records not being on site at the time of inspection. The farm manager was not made aware of the inspection of this farm in advance of the visit. This farm was visited on the spur of the moment, and the manager had the records at his horn While this is technically a violation of permit requirements, the records are usually at the farm. Given the above responses, we ask that you reconsider the issuance of the NOV against this facility. If you have any further questions or concerns, please feel free to call me or the farm. Sincerely, ►'sAJ 4J Westerbeek of Environmental Compliance Brown, LLC tz' �' -I.,, �- . cv NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES FAYETTEVILLE REGIONAL OFFICE DIVISION OF WATER QUALITY December 28, 1998 CERTIFIED MAIL RETURN RECEIPT REQUESTED Mr. Jim Walker P. O. Box 759 Rose Hill, N. C. 28458 SUBJECT: NOTICE OF DEFICIENCY Southern Cross Swine Farm Facility No. 82-144 Sampson County Dear Mr. Walker: On December 8, 1998, staff from the Fayetteville Regional Office of the Division of Water Quality conducted an annual compliance inspection at the Southern Cross Facility. At the time of the investigation our staff confirmed that the facility had several deficiencies requiring correction. The lagoon dikes have received excessive traffic resulting in the loss of vegetation. Waste application records (IR.R 1 forms) were available for the year; however, no IRR-2 forms have been completed for the facility resulting in posible over - application. In addition, the certified operator is no longer affiliated with the facility. The Division request that the following items be addressed: Immediately complete the waste application records for the facility (IRR-2 forms) for the previous 12 months and submit a copy to this office for review. 2. Immediately register the certified operator for the Southern Cross Swine Facility. 225 GREEN STREET, SUITE 714, FAYETTEVILLE, NORTH CAROLINA 26301-5043 PHONE 910-466-1 S41 FAX 910-466-0707 AN EQUAL OPPORTUNITY / AFFIRMATIVE ACTION EMPLOYER - 50% RECYCLED/10% POST -CONSUMER PAPER Southern Cross Farm Page 2 December 28, 1998 3. Consult with the Sampson County Agriculture Extension Office in regard to possible options available for establishing a cover grass to prevent erosion on the lagoon dikes. Nothing in this letter should be taken as absolving this facility of the responsibility and liability of any violations that have or may result from these deficiencies. If you have any questions concerning this matter, please do not hesitate to contact me at (910) 486-1541. Sincerely, Robert Heath Environmental Specialist KTS/RFH cc: Operations Branch Central Files Audrey Oxendine, FRO, NC DSWC Wilson Spencer, Sampson County NRCS h J 1 T}, 4 F A,;k , t i 71 j �I 4 � ®\: � \: \� \� � � / , \ c:��i &v � ©`a� ©) k�����/j :wr .. �d/2\%»/ ».� #y\?f : «.� � 6�%e y#•�`�`: ..� \� � . 9� < \ � � v a � \ � \� % d /2� G:, ,:��.�§ � ? 7 « §!� � C� � �\'�\�/�\/�\\ %;«¥ »e\? ©d c (4 \�yf�,�: , » � �\ \ >z � � � kf/ //2 ��� \ �\ \ \ � ~