HomeMy WebLinkAboutWQ0034102_Monitoring - 07-2020_20200826 (2)'31AITILIAN!,
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Enter date monitoring results were due. Will thi's mon-ftorling report 9,,WV-69 and OW-69A) Tvj�s
be submitted after the established due da", 7
r
Was i any requored infor mn iss atwiming on tille 6(3w-59 repwrt foms? YES NO
12
IF tshe answer to question I or 2 is "'YES"', fisi in the space, provided below the we idaintification nu mrber(s) and
explain the pnoul)lems encountered in obtaniing the required information.
J
'MISSEng 's Ing CaP5. YES 0 Aire any of the monitor wellshn need of repair or maintenanve (damaged casing, unlocIs
iced or M"
I'de"adification, plate, area overgrown, etc.) 9o'the answer is "Yes apg contact the Regional 0)' rice ' guldance.
F4 Are any monitored con stituonts oqual to above the established standards? uzs (NO
-4-y the ansmoler ho quesifor 4 is "NO" sk1p to section 6.
If the ans%qper to qun;sfion 41s, "'YES" list the affiected wells individually with constituent(s) and concentration(s)
exceadling standards in jlw sjoeice p`wirjfed below:
the constituents 'Identified 'in question 4 abover ave, standard, s been exceeded previously for thet S NCO
same constituent(s) in the same is In the I st two ye, rsl
_J
If the answer to question 5 is "NO�' skip to seciion 8.
If the answer to question 5 IS '11 �`FSVI fist in the space provided below, ea&, well with constituens s) e!wceed,i1n,g
standards, concentration(s) repoeted, and sample collection date for each occurrence (for the last two yearz,�).
Are the rsonitoring wells listed In section 5 'located at or beyond the revie-vurbawridary? R�,T
ff the answer is j"YES" 0 a groundwater qualiby problem may be occurring. CONTACT THE REGIONAL It
OFFICE IMMEDIATELY FOR GUIDANCE. ff the answer is 'r"NO "- manitoring wells may be impropeitv
Sr
located; contact the Regional Offlex-,1.
7 Is the pennittee Implementing prevelous�y approved a,4,Alonst requirad,11 by the D'Elvislon �1,nvolvinglithls YES N01
I groundwater quality problem?
If the answel, to qu 7 is "'YES" describe those actions in the splace. pro-vided belmlv.
If the answer to question 7 R9 coatect hg,�R�eldnal Office within 90
aqg.Vr ,#d,to,,.determ1n.jffihe ifflegct the, waite. WW_Oseal sY,.stem.!.S,-,kazLng,.RL,LtLP EMISW and S9—m-P—l-1aa
b o u n 42.64.s I Nq 0 &e4k6.,hAd1.ur0- Lo A 10. LUR X -19AISC. t the Re-M&M-22-00 0 —N.O.-t—kO -W.- 4fi
-
gena
Lln e. aj, andlor
Ps
The person -completing th' portion (OW-59A) of the monitoring report she,,,inigm hekaw and submit this
form with GW-59 for for required wells to the address provided at the fl of 7he current Gifif-59 form.
I hereby acknowledge that the above Iff ormatilon was evaluated and the informaitfora subnallitted In thhe
zoport fComplian.ce Report QW-69A) lis true and complete to the best of my knowledge-w.
Waft
Slgrbature. of Permittee (or A thorized
Microbac Laboratories, �mc. - 1---ayetteville,
CERTIRICAT, E OF ANALY'fie_ IS
KOG0111 19
Analyficali Testing Parameters
Client Sample 11D. MW 1, grab
Sam, pf�e Matrix: Moni"Coring Well
Coflected By: Poythress
Lab Sample iD- KOGO 119-01
Collection Date: 07108/2020 9:40
Field Parameters
R e s Lt
RL
Units
Dilution
Note Prepared Anai!yzed
Ana1'yst
NA
Depth
20.0
0.0830
ft
i
07/08120 0940
imp
Depth to Water Surface
8.00
ft
i
07/08/20 0940
imp
Sly 2550 B-2010
Temperature, Field
23
0.1
°c
1
07/08120 0940
imp
Sid 4500-H+ B-2011
pl-1, Field Test
6.9
1.0
S.U.
1
07/08/20 0940
imp
M- icroblology
Result
RL
Units
Dilution
Note Prepared Analyzed
Analyst
SM 9222 D-2006
Coliform, Fecal
<1.0
1.0
per 1 00mIL
1
07/08/20 1610 07/09/20 1626
MT
Inorganics Total
Result
RL
Units
Dilution
N to Prepared Analyzed
Analyst
EPA 300.0, Rv. 2.1 (1993)
Chloride as CL
10.8
1.00
mg/L
1
07108/20 1142
JDW
Nitrate as N
1.37
0.200
mg/L
1
07/08/20 1142
JDW
Sly 2540 C-2011
Total Dissolved Solids
<100
100
mg/L
2
07113/20 1615
KAIT
SM 4500-NH3 G-2011
Ammonia as N
<0.200
0.200
mg/L
1
07109/20 1540
JDW
SM 4500-P F-2011
Phosphorus, Total <0.20 0.20 mg/L 1 07,116120 1012 JDW
Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH
Inorg ganics Total Result RL Units Dilution Note Prepared Ana �'Iyzed Art
Shil 5310 C-2011
1 1.00 mg/L 1 07/14120 165"
lotal Organic Carbon - TOC 2.46 1 07/15/20 1109 DIH
Wflucrobac Laboratorie,S, hne,
2592 Hope V1.4fl'is Rd Fayetteville, NC 28306 1910.864.1920 p I �t�miw.microbac.com
Paw 3 of 12
Microbac Laboratories, Inc. - Fayetteville
CERT�RCATE- OF ANAI SIS
KOG0119
Client Sample ID: MW 2, grab
Sample Matrix: Monitoring Well
Collected By: Poythress
Lab Sample ID- KOGO 119-02
Coll�cflon Date- 07108/2020 10.55
Field Parameters
Resullit
RL
Units
Dilution
Note Prepared
Analyzed
Analyst
NA
Depth
20.0
0.0830
ft
1
07/08/20 1055
imp
Depth to Water Surface
9.00
ft
1
07/08/20 1055
imp
SM 2550 B-2010
Temperature, Field
22
0e 107108120
0C
1055
imp
Sh"I 4500-1 -2011
pH, Field Test
6.4
1.0
S.U.
1
07/08/20 1055
imp
Microbio1ogy
Result
R
Units
Dilution
Note Prepared
Analyzed
Analyst
Sly 9222 D-2006
Coliform, Fecal
<1 sO
1.0
per 100ml-
1
07/08/20 1610
07/09120 1526
MT
inorganics Total
Result
RL
Units
Dilution
Note Prepared
Analyzed
AinkMyst
EPA 300.0, Rv. 2.1 (1993)
Chloride as CL
18.2
1.00
MQI,L-
1
07/08120 1142
JDW
Nitrate as N
<0.200
0.200
Mg/L
1
07/08/20 1142
JDW
SM 2540 C-2011
Total Dissolved Solids
102
100
mg/L
2
07/13/20 1615
MT
SM 4500-NN3 G-2011
Ammonia as N
9.51
1.00
mg/L
07/09/20 1540
JDW
Sly 4500-P F-2011
Phosphorus, Total
<0.20
0.20
mg/L
1
07116120 1012
JDW
Analyses Subcontracted to: Microbac Laboratories Inc., - Marietta, OH
Inorganics Total Result �R Units Dilution N ote Prepared Analyzed Analyst
S[Vi 5310 C-2011
T 1 �00 mg/L 1 07/14120 1651 lotal Organic Carbon - TOC 4.50 07/15120 1131 DIH
Microbac Laboratories, lirm,
21592 Hope Mills Rd I Fayetteville, NC 28306 'W.864.1920 p � vrvoiti.rnicrobacxom
Page 4 of 12
Inorganics Total
SM 5310 C-2011
Total Organi*,-. Carbon - TOC
RnPAC
Microbac Laboratories, Inc, - Fayetteville
KOG01 19
Client Sample ID: MW 3, grab
Sample Matrix: Monitoring Well
Collected By: Poythrests.
Lab SaynplelD: KOGO 119-03
Collection Date: 07/08/2020 10:30
Field Parameters
Result
RL
Units
Dilution
to Prepared Analyzed
Analyst
N A
Depth
15.0
0.0830
ft
1
07/08120 1030
imp
Depth to Water Surface
7�,00
ft
07/08/20 1030
imp
SM 2550 B-2010
Temperature, Field
21
0.1
Oc
07/08/20 1030
1 M, P
SM 4500-H+ B-2011
p1d, Field Test
6.2
1.0
S.U.
07/08/20 1030
jhAp
Result
RL
Units
D i I udon
Note Prepared Anaiyzed
Analyst
SM 9222 D-200,6
Coliform, Fecal
<1.0
1.0
per 1OOrnL
1
07/08/20 1610 07/09/20 1526
MT
Inorganics Total
Resu'LI
RL
Units
Dilundon
Note Prepared Analyzed
Analyst
EPA 300.0, Rv. 2.1 (1993)
Chloride as CL
10.6
1.00
mg/L
1
07/08/20 1142
JDW
Nitrate as N
<0.200
0.200
mg/L
11,
07/08/20 114-2
JDW
Ski 2540 C-2011
Total Dissolved Solids
1,08
100
mg/L
2
07/13/20 1615
MT
SM 4500-NH3 011
Ammonia as KI
<0.200
0.200
mg/L
i
07/09/20 1540
JDW
SM 4500-P F-2011
Phosphorus, 'Total 0.90 0.20 mg/L 1 07/16/20 10412 JDW
Analyses SUbcontracted to: Microbac Laboratories Inc., - Marietta, OH
Result R L Units Dilution Note Prepared Analyzed Analyst
2.47 1.00 mg/L 1 07/14/20 1651 07/15/20 1153 DIH
,�,bac Laboratories, Inc.
2592 Hope llfflfis Rd I Fayettevipffle, MC 28306 � OUIO.864�1920 p i Page ,5 of
"P, M
iff gy
Miarobau- Laboratories, 1mc-1,, - Fayett-eviHe
KOG01 19
Client Sample ID- IOW 4, grab
Sample Matrix- Monitoring Well
Collected By� Poythress
Lab Sample 10- KOG01 19-04
Collection Date,: 07/08/2020 10: 10
Field Parameters
Result
RL
Units
Dilution
Note Prepared Analyzed
Analyst
NA
Depth
18.0
O.0830
ft
1
07/08/20 111010
imp
Depth to Water Surface
8.00
f 11
07/08/20 1010
11 1\4 P
3-1kii 2550 B-2010
Ternperpture, Field
23
0.1
0C
07/08120 1010
imp
SM 4500.H+ B-2011
pH, Field Test
6.7
1.0
'S. U
07/08/20 1010
imp
Microbiology
Result
RL
Units
Dilution
Note Prepared Analyzed
Analyst
SPI 9222 D-2006
Coliform., Fecal
<1.0
1.0
per 100mL
1
07/08/20 1610 07/09/20 1526
MT
�norqanlcs 'Total
Result
RL
Units
Dilution
Note Prepared Analyzed
Analyst
EPA 300.0, Rv. 2.1 (1993)
Chloride as CL
22.6
1.00
mg/L
11
07108/20 1142
JDW
Nitrate as N
<0.200
0.200
mg/L
1
07/08/20 1142
JDW
SM 2540 C-2011
Total Dissolved Solids
124
100
mg/L
2
07/13/220 1615
MT
SM 4500-NH3 G-2011
Ammonia as N
<0,200
0.200
mg!L
I
Al2 07109r20 1540
JDW
SM 4500-P F-2011
Phosphorus, Total <0.20 0.20 mg/L I 07/16120 1012 JDW
Analyses Subcontracted to: Microbac Laboratories Inc., - MariettCan, OH
Inorganics Total Result RL. Units Dilution Note Prepared Analyzed Anallyst
Sly 5310 C-2011
Total Organic Carbon - T0C -11.00 mglL 1 07/14120 1651 07115/20 1214 DIH
V, 1 .1
.w1'cr,oh-,ac Labworator'eS, Irp
21%'1592"! Hope jkliffls Rd I Fayettevifle, NC 28306 1910.864�1920 p 1
Page 6 of 12 1
1
e
Microbac Laboratories Inc. - Faye'tevi
CERTIFICATE OF ANALYSIS
KOG01 19
I
4IIIIIIIIpIIIIIII ��111 IIIII III III I� 1, 71 41� I pill 111111, 1
lE M7 N I I milli ol
Spike Source
%REC
RPD
Microbiology
Result
RL
Units Level Result %REC
Limits
RPD
Limit Notes
Batch KGO0907 - Wet Chem Aqueous - SM 9222 D-2006
Blank (KGO0907-BLKI)
Prepared: 07/08/2020 Analyzed: 07/09/2020
Coliform, Fecal
< 1.0
1.10
per
I OOmL
LCS (KG00907-BS1)
Prepared: 07/08/2020 Analyzed: 07/09/2020
Colliform, Fecal
31000
1.0
per
0-200
1 OOmL
Spike Source
%REC
RPD
Inorganics Total
Result
RL
Units Level Result %REC
Limits
RPD
Limit Notes
Batch KGO0804 - Wet Chem Aqueous - EPA 300.0, Rv. 2.1 (1993)
Duplicate (KGO0804-DUPI)
Source: KOG0113-01
Prepared &Analyzed, 07/08/2020
Chloride as CL
553
21.2
mg/L 557
0.8
10
Nitrate as N
5.36
4.25
mg/L 5.52
3
10
Duplicate (KGO0804-DUP2)
Source: KOG0128-01
Prepared &Analyzed: 07108/2020
Chloride as CL
14.0
1.00
mg/L 14.0
0.4
10
Nitrate as N
9.32
0.200
mg1L 9.28
03
10
Matrix Spike (KGO0804-MSI)
Source: KOG0113-01
Prepared &Analyzed: 07/08/2020
Chloride as CL
550
21.2
mgYL 10.0 557 N R
90-110
Nitrate as N
7.31
4.25
mg/L 2.26 5.52 79
90-110
Matrix Spike (KG008D4-MS2)
Source: KOG0128-01
Prepared &Analyzed: 07/08/2020
Chloride as CL
53.6
1.00
mg/L 40.0 14.0 99
90-110
Nitrate as N
17.3
0.400
mg/L 9.04 9.28 88
90-110
Matrix Spike (KGO0905-MS1) Source: 1KOG0119-04 Prepared &Analyzed: 07/09/2020
Ammonia as N 0.729 0.200 mg/L 1.00 ND 73 80-120
Matrix Spike Dup (KGO0905-MSD1) Source: KOG0119-04 Prepared &Analyzed: 07109/2020
Ammonia as N 0.938 0.200 mg/L 1.00 ND 94 80-120 25 20
71111!111liii 11 iq�111111 1��I� !III
Blank (KG01 021- L1K1) Prepared &Analyzed: 07/13/2020
Total Dissolved Solids <100 100 mg/L
LCS (KGO1021-BS1)1 Prepared &Analyzed: 07/113/2020
Total Dissolved Solids 760 100 mg/L 746 '102 90-110
Duplicate (KGO1021-DUPl) Source: KOG0116-01 Prepared &Analyzed: 07113/2020
Total Dissolved Solids 162 100 mg/L 154 5 10
LCS (KGO1434-BS1) Prepared &Analyzed: 07/16/2020
Phosphorus, Total 0.50 0,20 mg/L 0.50 99 90-110
N41crobi Laboratories, inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864,1920 p I www.microbac.com P�age7of 12
------------
MIC
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
KOGO 119
-Spike Source
%REC R P D,
Inorganics Total
Result
RL
Units Level Result %REC
Limits P Limit "Jotes
Batch KGO1434 - Wet Chem Aqueous - Sly 4500-P F-2011
Matrix Spike (KGO1434-MSI)
Source: KOGOOSI-01
Prepared &Analyzed: 07116/2020
Phosphorus, Total
3.2
0.20
mg/L 2.5 0.63 102
90-110
Matrix Spike (KGO1434-MS2)
Source: KOG0128-03
Prepared &Analyzed: 07116/2020
Phosphorus, Total
0.82
0.20
mg/L 2.5 ND 33
90-110
Matrix Spike Dup (KGO1434-MSD1)
Source: KOG0081-01
Prepared &Analyzed: 07/16/2020
Phosphorus, Total
3.2
0.20
mg/L 2.5 0.63 104
90-110 1 200
Matrix Spike Dup (KGO1434-MSD2)
Source: KOG0128-03
Prepared &Analyzed: 07/16/2020
Phosphorus, Total
1.1
0.20
mg/L 2.5 ND 43
90-110 26 200
Batch Quality Control Summary.- Microbac Laboratories Inc., - Marietta, OH
Spike Source %REC
RPD
Inorganics Total Result
MDL RL
Units Level Result %REC Limits RPO
Limit Notes
Batch B0G071 0 - Wet Clem -Default Prep - Slid 5310 C-2011
Blank (BOG0710-BLKI)
Prepared: 07/1412020 Analyzed: 07/1512020
Total Organic Carbon - TOC <0.500
0.500 1.00
mg/L
LCS (BOG0710-BSI)
Prepared: 07/14/2020 Analyzed: 07/15/2020
Total Organic Carbon - TOC 25.1
0.500 1.00
mg/L 25.0 100 85-115
LCS Dup (BOG0710-BSOI)
Prepared, 07/14/2020 Analyzed: 07/15/2020
Total Organic Carbon - TOC 25.2
0.500 1.00
mg/L 25.0 101 85-115 0.495
15
Duplicate (BOG0710-DUPl)
Source: MOG0938-01
Prepared: 07/14/2020 Analyzed: 0711512020
Total Organic Carbon - TOC 2.32
0.500 1.00
mg/L 2.23 4.22
15
Matrix Spike (BOG0710-MSI)
Source: MOG0938-01
Prepared: 07/14/2020 Analyzed: 07/15/2020
Total Organic Carbon - TOC 12.0
0.500 1.00
mg/L 10.0 2.23 97.5 85-115
Matrix Spike Dup (BOG0710-MSD1)
Source: MOG0938-01
Prepared: 07/14/2020 Analyzed: 07/15/2020
Total Organic Carbon - TOC 11.7
0.500 1.00
mg/L 10.0 2.23 94.9 85-115 2,27
15
Definitions
0c: Degrees Celsius
All 2: MS/MSD fail recovery, but the LCS passes criteria.
ft: Feet
MDL: Minimum Detection Limit
mg/L: Milligrams per Liter
RL: Reporting Limit
RPDs Relative Percent Difference
S.U.: Standard Units
Cooler ReGelpt Log
Cooler ID- Default Cooler
Temp, 3.4 " C
Laborafork'.,s, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910-864.1920 p I mnvw.m1crobac.com
Page 8 of 12
Microbac Laboratories, ,'Inc,, - Fayetteviiie
CERTIFICAJE OF ANALY SIS
==W
Ice Present or not required?
Yes
Shipping containers sealed or not required?
Yes
Custody seals intact or not required?
Yes
Chain of Custody (COC) Present?
Yes
COC includes customer information?
Yes
Relinquished and received signature on COC?
Yes
Sample collector identified on COC?
Yes
Sample type identified on COC?
Yes
Correct type of Containers Received
Yes
Correct number of containers listed on COC?
Yes
Containers Intact?
Yes
COC includes requested analyses?
Yes
Enough sample volume for indicated tests received?
Yes
Sample labels match CDC (Name, Date & Time?)
Yes
Samples arrived within hold time?
Yes
Correct preservatives on COC or not required?
Yes
Chemical preservations checked or not required?
Yes
Preservation checks meet method requirements?
Yes
VOA vials have zero headspace, or not recd.?
Yes
Project Requested Certification(s)
Microbac Laboratories Inc., - Marietta, OH
583
NC Dept. of the Environment and Natural Resources
Microbac Laboratories, Inc, - Fayetteville
North Carolina DENR NPDES
M
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents only the
sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are Brittany Smith
present and at) authorized signature is included. The services were provided under and Administration
subject to Microbac's standard terms and conditions which can be located and Reported: 07/17/2020 17:34
reviewed at <https.11wwwmicrobac.comlstat7dard-terms-cot7d!tions>.
44 Met;
fir � -it
A'1116ass 8 , , C - & m F Cy a r Typ e
Facility Name:
Permit Name
Facilit Addres
14-
Glt'111
rlulcl h I Aver
jp. County
(CRY) Slato
Contact Persow? le ii
T-7 Telephone #. 7V
Well Location/ Site Name:
No. of Wells to be Sampled:
Well Identification Number (from Permit) V For Groundwater Tmatment Systems
Well Depth% 26 ft. Well ill titer: Screened Interval: ft. to Check One: influent (98)
V 0; Effluent (99)
Depth to Water Level- —ft. below measuring pol"n'. - - -- M
Measuring Point (M.P.) Is%. �-6� ft. above land surface. Relative M.P. Elevation In ft.:
DEPARTMENT UF P.NVIKUNML-N 1 44 WA I UH44-16 =-Z'kVUnL,[4;a
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
FIALEIGH. NC ?,.7699-1636 Phone,,, (9191
NQM Values should reflect dissolved and
colloldal concentrations,
Gallons of water pumped/balled before sampling: G Date sample collected: .1-3 -zaroe> Date sample anal yzedt.�
Field analysis-, pH —.- 6--'? ' Specific Conductance uMhos Laboratory Name:
Temp. Odor ilo')9! Appearance -.L& " Certification No.
PARAM91 (Samples for metals were collected unfiltered --YES - --—NO and flold acidffled
COD
mo Nitrite (NO2) as N Mg/l
C011form: MF Fecal /1 00ml Nitrate (NO:3) as N Mg/l
Coliform: MF Totai
---/l 0071-11 PIVGSE-*�51
(Note: Use MPN method for hIghly tUrbld Samples)
Dissolved Solids: Total eC* 10 0
MgA
pH (when analyzed)
Lin
TOC
MgA
Chloride.
MgA
Arsenic
Mg/1
Grease and Oils
Mg/1
Phenol
Mg/l
Sulfate Mg/l
Specific Conductance
uMhos
Total Ammonia
Mg/1
TKN as N —
Mg/l
Orthophosphate
mg/l
Al - Aluminum
mg/l
Ba - Barium
Mg/1
Ca - Calcium
Mg/l
Cd - Cadmium
Mg/l
Ch rom 1 u m: Total
mg/1
Cu - Copper
Mg/l
Fe -
Mg/l
Mercury
Mg/l
K - Potassium
Mg/l
Mg - Magnesium
Mg/l
Mn - Manganese
mg/l
YES NO)
Ni - Nickel a-Ag/1
Pb - mg/1
Zn ^ In Mg/1
Ammonia Nitrogen Mg/1
Other (Specify Compounds and Concentration Units)
CORGANICS-M (GC,GC /M8,HPLC)
(Specify test and math ad Ob. Aftach lob FirampoOL)
HapaVt,Okirwched? Yes--�("O No,
voc method#=
method#=
Pt,armfuee (or Awhod-zed Agent) Name and Tifle - Please print or type
GW-59 Signature of Permittee (or Authpuffted Agani) (Dale)
Rava 013112000
q P9 fA,
T( - -
ON Ll S 'AM, 01
COMM; � ANU_M'__ REPOR Ct F 0 H MA
j,
Coun
ty
;L
T 9 1 a P h o n a # —_ 2541_'L_J_� 1i "' 'L I
No. of Wells to be Sampled:i.—.,__,_,,
Well Identification Number (from Permit): w(___ For Groundwater Treatment Syatoms
Well Depth: ft. Well Diameter: Check One: 13 Influent (98)
Screened Interval: ft. to fi. 0 Effluent (99)
Depth to Water Level: I _ft. below measuring po'nt.
Measuring Point (M.P.) is: A- ft. above land surface. Relative M.P. Elevation In ft,,.*
Gallons of water pumped/b, filed before sampling: 6 - Date sample collected: 7 40-1 ID
Field analysis: pH t, . . , Specific Conductance uMhos
Temp. 2-f�'- — "C, Odor, - to 0#1 e - Appearance 0 le#4r-
PERMIT #'Q' EXPIRATION DATEr-
Non-Discharge..-
NPDES
RMI OPERATION BONG MONITOIRIED
Lagoon ftmadlatlon,v Infiftraflon Gallery
Spq-ay Field
F, DMIJ Distributor Land Applicat on of Sludge
R
Other:
NQ]a Values should ref dh6solved and
colloidal
Date sample analyzed:
Laboratory Name:
Certification No.
PARANIFTFFIR Mamnlar. fn metals wt%ra enlianted unfiltered YES NO and field acidified -YES
CO1l Nitrite as Mg/lg
Coliform, MF Fecal 00MI Nitrate (NO:3) as N Mg/1
Coliform: MF Total /1 00M I Phosphorus: Total as P Mg/1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total—- 1 rng/1
pH (when ana zed)
units
Chloride- -4).
a- / I
Arsenic
mg/i
Grease and 011s
rngil
Phenol
MCIA
Uff
Sulf ate
Mg/1
Specific Conductance
uMhos
Total Ammonia 0
MC4
T NasN
�-__AMIQA
Al - Aluminum
a 11.51
mg/l
Ba - Barium
Mg/l
Ca - Calcium
mg/l
Gd, Cadmium.-
Mg/l
Chromium: Total
mg/l
Cu - Copper
Mg/1
Fe - IrQn
mQ/1
Hg - Mercury
MC-1/1
K - Potassium—__-
mg/l
Mg - Magnesium
Mg1l
Mn - Manclanese
mg/l
A
Ni - IMPI
Pb - Lead� M
Zn - Zinc nniqA
Ammonia Nitrogen M (---41
Other (Specify Compoundeo and Concentrallon UnIts)
URGANICS: (GCjGC/Nl8,HPLC)
(Specify test and method #. Attach lab report.)
report-)-"-,
ReportAttached? Yes___1,1), No..-.(O
voc method
method
_M01
Permitlee or Authorized Agent) Name and Title - Please print or type
GW-59 TDate) , F A orIzed Agent)
Rev. 03,12000
Please Print Clearly 7W&
FacIlIty Name. -
Permit Name if different)-,
Facilit Address*.
yiny^
_1614 g T 7
nnt t Persow............4 h
Count
Telephone #: ZJ
Well Location/ Site Name
No. of Wells to be Sampled,
Well Identification Number (from Permit):
/5'
For Groundwater Treatment Systems
Well Dep1h: --ft. Well Diam"eter:
In.
Check One: 13 Influent (98)
Screened Interval: ft- to - ft.
�_3 Effluent (99)
Depth to Water Level: 7 —ft. below measuring point.
Measuring Point (M.P.) is: r-' 2"t , tit. above land surface.
Relative M.P. Elevation In ft.
Gallons of water pumped/balled before sampling; -
Date sample collected: I - 9 -�zozo
Field analysis: pH._.L#2 ' Specific Conductance uMhos
Temp. '20.9..'OC, Odor, jJOAC
Appearance !a I eAr
DEPARTMENT OF ENVIKU14MM41 4 AJAI UVIA4 roGZZAJUn%4r_a
WATER QUALITY DIVISION, GROUNDWATER F00-TION
1636 MAIL SERVICE CENTER
PERMIT EXPIRATION DATE:
I 11C
Non-Dischargel
'NPDES
nu QEP—EBMIrEED OPERATION BEING MONITORED
Lagoon Ramadlation-, Infliftration Gallenj
Spray Field
Ratary Distributor Land AppfloaHort of Sludge
01hen
N -� Ve m I jould reflect dissoived agnd
K1,1E V flu m sh
caHoIdM concentrations.
Data sarnpie anad�yzod:
Laboratory Name:
Certification No.
=no
P-AB (Samples for metals were collected unfiltereV9:Q d - - _ a &M%g —NO and field acidif led
COD mg/l Nitrite (NO2) as N ring/l
Coliform: MF Fecal ._J1 00ml Nitrate (NO*,) as N mg/l
Coliform: MF Total
/1 00ml Phosohorus: Total as R M-0
(Note: Use MPN method for highly turbid samples)
q
Dissolved Solids.- T1 - potal 102)
PH (when analyzed)
S
TOC "OIL
mgil
Chloride,
mg/1
Arsenic
Mg/1
Grease, nd 01)I'ss
Mg/1
Phenol
Mg/1
Sulfate... �sxmmcaa«-- ...esum..---..�.,�w„
.� x�v, .,.,..-:.s:...ts� Mg/1
Specific Conductance
uMhos
Total Ammonia ew 0
■■® mg/i
TKN as N
Mg/1
WirthophoSphate
Mg/1
Al - Aluminum
Mg/l
Ba - Barium
mg/l
Ca - Calcium
Mg/l
Cd - Cadmium
Mg/l
Chromium: III'
Cu - Copper
Mg/1
Fe - fro.n
Mg/l
Hg - Mercury
Mg/l
K - Potasslu
Mg/1
Mg - Magneslum
M9/1
Mn - Manganese—
Mg/l
�YE S NO)
N1 - Nickel- mq/1
F-lb - LeacL. M g II
wc< t__.�a_Zn - Zi*nc 10
mg,",
Ammonia Nitrogen )l1rigli
Oth ce, r (Specify Compounds and ConceniraLion Units)
M8,MPLC)
lad
b r offt 1,"3p&.-A10,q iost and nah r�.ad§h Aflac-h ep
�4,7kspo,axrl At' chadia6`1 Ys,3--_(1) Nou (0)
vo omethod
method 01
ParMflea (or Authonized Agant) Nam a and 'ridle - Please print or type
GW-59 Signature of Peaniflee (nx 4�kuthofolzzad A gent)
Rev. 031=00 I
IV
GROUNDWATER OUALITY MONITORING,
COMPLIANCE REPORT FORM
.-A-GILLTY lNFQHKAjj!QFJ Please Print Clearly or Type
Facility Name:
} iF F f�F r : y, T. 1 fiji
Permit Name
FacH& Addre S:
County
ate) RIP)
Contact Person.- Telephone
r.
Telephone
Well Location/ Site Name-, � ��' �.� l�io® of Wells to be Sampled:
Well Identification Number (from Permit):
Check I
For Groundwater Treatment Systems
Well Depth: --.ft. Well Dismater:_ in. Check0ne:13 Influent (98)
Screened Intervals....- —ft. to ft �in noint 0 Effluent (99)
Depth to Water Level:_,,- ft. below measuring point.
Measuring Point (M.P.) is: ft. above land surface. Relative M.P. Elevation In ft.:
Gallons of water pumped/balled before sampling: Y Date sample collected:,
Field analysis,-, pH .--, 7 0 . Specific Conductance uMhos
Temp. *C, Odor AM-4 C Appearance
4-Z026
In red
MIDI -1 1.01MV
EXPIRATION DATE:,
Noa n-DischrgeZ
. 4 1
LI- u i c
NPDES
r; QE PERMITM-1 ERATION BEING MONIMRED
Lagoon Remediallon: Infiltration 0 pm lery
pray Field Hemedlatlon:
Rotary Distributor Land Application of Sludge
Other:
NQM Values should reflect dissolved and
colloidal concentrations.
Date sample analyzed:
Laboratory Name,,,
Cerfification ®
PABAMETERS (Samples for metals were collected unfiltered, -.YES --,NO and field acid1fled
COD I Nitrite (NO2) as N M911
46 0
Coliform-, MF Fecal /1 00ml Nitrate (NOoa) as N -",Z � mg/1
Coliforml: MF Total "I kc)" M C I
JI 00MI Phowhorus: Total as P __
(Note: Use MP N method for highly turbid samples)
Dissolved Solids: Total
mv
pH (when analyzed)
units
TOC
Mg/1
Chloride.,I.-,
mg/1
Arsenic
It
Mg/1
Grease and Oils
Mg/1
Phenol
M9/1
Sulfate
Mg/1
Specific Conductance _..Whos
Total Ammonia 4
Mg/l
TKN as N
Mg/l
Orthophosphate
mg/1
Al - Aluminum
mg/l
Ba - Barium
mg/l
Ca - Calcium
Mg/l
Cd - Cadmium
Mg/l
Chromium-, Total
Mg/l
Qi - Copper
Mg/l
Fs-e - IrQn
mgA
Hg - Mercury
mgA
K - Potassium
mq/1
Kg - Magnesium
mg/l
Mn - Manganese
mg/l
-YES NO)
N1 - Nickel,-.. Mg/1
Pb
Zn - Zinc Mg/1
Ammonia Nitrogen.- Mq
Other (Spedity Compounds and Con-centfallon untflisa)
0,RG-MNICS.-, �GCMCAMS,HPLC)
(SpacKy toot and misthod #,, AtUchu labumpartj
Hepof,�Affschedad`l Ye
os--
v rneihod # c
method #
rnmathod#=
PermlHas (or Aulhonized Agent) Name and Tills - Please print or type
GW-69 Signaluve of Panittes of Authmized Aganf)
Rev. 0312000
Al
M I C R 0 B A C'
o MIcrobac Laboratories, ha - FayettevN'�ie
CERTIRCVIF E 0 F A N A L"YS 'I S
KOG0116
Analytical Testing Parameters
Client Sample ID: WA, Lagoon, Grab
Sample Matrix: Aque�ou
Collected By-, S t a r.111 e y
Sample ID: K 0 G 0,1116 - 0 1
Collection
Date: WiO812020 10110,
DEFAULT GENERAL ilflETHOD
Rest-ilt
RL
Units
DiiluVon
Note
Prepared
Analyzed
Analyst
SM 2540 0-20111
Total Suspended Solids
25.5
12.5
mg)'L
IZ
07/08120 1616
TBM
S M 5210 B-2011
BOD
14. 0
2.00
MgIL
G6
071'08/20 2030
07/13/20 1530
MT
Held Parameters
ResuK
ILL
Units
i i ut 1 G n
Note
Prepared
An, alyZed
Ai,.iatyst
NA
Chlorine, Total
.70
mg/L
07/08/20 1010
ELT
MicroWok)qy
Result
KI L
Unfts
Diluflon
VII 0 te
Prepaned
AnMyzed
kiialyst
SM 9222 0-2006
Coliform, Fecal
6.6
1.0
per IOOrnL
1
07108120 1610
07/09/20 1526
MT
�norganics ToW
Result
RL
Units
Dkfflon
Xlate
Prepared
Ana�yzed
An.,Myst
Calculation
Total Nitrogen
4.73
1.00
nia/L
1
071114/20 0921
TBM
EPA 3 0 0. 0, R v. 2. 1, 9fer)
Chloride as CL
11.8
1,00
mg/L
1
07/08/20 1142
JDW
Nitrate as N
<0.200
0.200
mg/L
07/08120 1142
JDW
Nitrite as N
<0.200
0.200
mg/I
07108/20 1142
JDW
SM 2540 C-2011
Total Dissolved Solids
154
100
mg/L
2
07/13/20 1615
MT
SM 4500-NH3 G-2011
Ammonia as N
0.261
0.200
mg/L
1
07/09/20 1540
JDW
SVVI 4500-Norp j C-201 I
Total Kjeldahl Nitrogen
4.73
1.00
nag
1
07/14/20 0921
TBM
SM 4500-P F-2011
Phosphorus, Total
<0.20
0.20
mg/L
1
07/16/20 1012
JDW
rg C
a.c bru r, o r �e!os U, ! i
2592 Hope Nho'His RFd Fayetteville, NC 28306 [1910.864.1920 p www.microbac.com
Iof 7 Page 3
A
Microbac Laboratorijes-, Inc. - Fayetteville
CERT�FCAT_E OF ANAL),,"S�,,S
KOGO 116
Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayefievfllfle
Spike Source %REC
RPD
DEFAULT GENERAL
Result ILL
U n i t's Lpavel ResWt %REC LlmKs
RP1D L'qmflt
METHOD ***
Batch KGO0815 -'met Chem Aqueous - SM 2540 D-2011
Blank (KGO0815-BLKI)
Prepared & Analyzed: 07/08/2020
Total Suspended Solids
<2.50 2.50
mg/L
Biank (KG0081 5-BLK2)
Prepared &Analyzed: 07/08/2020
Total Suspended Solids
<2.50 2.50
mg/L
Mink (KGO08i 5-BL1 )
Prepared & Analyzed: 07/08/2020
Total Suspended Solids
<M 2.50
rng/L
LC S (KGO681 5-13SI)
Prepared & Analyzed: 07JO8/2020
Total Suspended Solids
35.3 2.50
mg/L 37.5 94 94.5-105.4
Duplicate (KG00815-Dup1)
Source: KOG0058-Gi
Prepared &Analyzed. 07/08/2020
Total Suspended Solids
53.9 17.7
mg/L 44.7
19 10
Duplicate (KGO0815-DUP2)
Source. 'KOG0086-01
Prepared & Analyzed: 07/08/2020
Total Suspended Solids
384 1 CJD
mg/L 348
10 10
Duplicate (KG00F6,"'L!5-0UP3)
Source- KOG0124-01
Prepared &Analyzed: 07/08/2020
Total Suspended Solids
50.0 25.0
mg/L 37.0
30 10
Batch KGO1016 - Wet Chem Aqueous - Sly 5210 B-2011
Blank (KG01016-BLK1)
Prepared: 07/08/2020 Analyzed: 07/13/2020
BOO
<2.00 2.00
mg/L
LCS (KG0,10i6-BS1)
Prepared: 07/08/2020 Analyzed: 07113/2020
BOD
171
mg/L 198 86 .59596-115.4
Duplicate M60IM-DUP1)
Source: KOG0125-01
Prepared: 07/08/2020 Analyzed: 07/13/2020
BCD
341 MO
mg/1- 348
2 10
SpHke S 0 u Lr C re %REC
RPD
111flicrobiology
Result RL
Units Level ResWt %REC Limits
RPD Lirdift Notes
Batch KG00907 - Wet Chem Aqueous - SIVi 9222 0-2006
Blank (KGO0907-BLKI)
Prepared: 07/08/2020 Analyzed: 07/09/2020
Coliform, Fecal
<1.0 1.0
per
1 OOmL
LCS (1 0907-BSI)
Prepared: 07/08/2020 Analyzed: 07/09/2020
Coliform, Fecal
31000 1.0
per 0-200
100mL
Spike Source %REC
RPD
1Diorganics Tatefl,
Result R, L
Units Leve' Resuft %REC Limits
RPD Lirnift Notes
Batch KG00804 - Wet Chem Aqueous - EPA 300.0, Rv. 2.1 (1993)
Duplicate (KGO0804-DUPI)
Source: K000113-01
Prepared & Analyzed: 07/08/2020
Chloride as CL
553 21,2
mg/L 557
0.8 10
Nitrate as N
5.36 4.25
mg/L 5.52
3 10
Micrabac. Labora1olrias,
2592 Htofpe-�� to Rd I Fayetteville, NC 28306 1910-864.1920 p I www.microbac.com
Page 4 of 7
'e--*
A, P,
U.7jcrobac Laboratories, IInc. - Fayetteville
CERTPCiV�-E
OF ANAUY&S
KOG0116
5- P, rJ ke Source
% R E CC R, P D
Inorganics Total
Result RL
Units LeVW Result %REC
Li its RPM L-ImIft Notes
Batch KGO0804 - Wet Chem Aqueous ® EPA 300.0, Rv. 2.1 (1993)
Duplicate (KGO0804-DUPI)
Source: KOG0113-Ci
Prepared &Analyzed: 07/08/2020
Nitrite as N
<4.25 4.25
mg/L N D
10
Duplicate IKGO0804-DUP2)
I
Source: KOGGiH-01
Prepared & Analyzed.- 07/08/2020
Chloride as CL
14,0 1.00
mg/L 14.0
0.4 10
Nitrate as N
0.32 0.200
mg/L 9.28
0.3 10
Nitrite as N
< 0. 221 0 0 0.200
m g /L N D
10
W"iatdx Spike (KGO0804-M, Si)
Sowrce: KOG0113-01
Prepared &Analyzed: 07/08/2022-0
Chloride as CIL
550 21.2
mg/L 10.0 557 NR
90-110
Nitrate as N
7.31 4.25
5
� 0
rng/L 2.26 5.52 1 9
90-110
Nitrite as N
<4.25 4.25
mg/L 3.04 ND 129
90-110
Matrix Spike (KG00804-RqS2)
1-jource: KOG0129-01
Prepared & Analyzed: 07/08/2020
Chloride as CL
53.6 1.00
mg/L 40-0 14.0 99
90-110
Nitrate as N
17. k`33 0.400
mg, I 9.04 9.28 88
90-110
Nitrite as N
12.1 0.200
mg/L 12.2 ND 99
90-110
Batch KGO0905 - Wet Chem Aqueous ® SM 4500-NH3 G-2011
Matrix Spike (KGO0905-MSI)
Source: KOG0119-04
Prepared &Analyzed- 07/09/2020
Ammonia as N
0.729 0.200
mg/L 1.00 ND 73
80-120
Matrix Spike Dup (KGO0905-MSDI)
Source- KDG01100-04
Prepared &Analyzed: 07/09/2020
Ammonia as N
0.938 0.200
mg/L 1.00 ND 94
80-120 25 20
Batch KGO1021 -filet Chem Aqueous
- SM 2540 C-2011
Man k (KGO1021-BLKI)
Prepared &. Analyzed. 07/1312020
Total Dissolved Solids
<100 100
mg/L
LGS (KG01021-BISI)
Prepared & Analyzed: 07/13/2020
Total Dissolved Solids
760 100
mg/L 746 102
90-110
Duplicate (KGO1 021 -DUPI)
Source: KOG0116-01
Prepared &Analyzed: 07/13/2020
Total Dissolved Solids
162 100
mg/L 154
5 10
Batch KGO1406 - We Chem Aqueous - SM 4500-Norg C-2011
Blank (KGO1406-BLKI)
Prepared &Analyzed: 071", 4/2020
Total Kjeldahl Nitrogen
<1.00 1,00
mg/L
LCS (KG01406-B31)
Prepared & Analyzed- 07/1412020
Total Kjeldahl Nitrogen
27.7 1.00
mgiL 30.0 92
80-120
Matrix Spike (KGO1406-MSI)
Source: KOG0116-01
Prepared &Analyzed. 07/14/2020
Total Kjeldahl Nitrogen
13.7 1.00
1 Mg/I L- 10.0 4.73 90
80-120
Matrix Spike Dup (KG014D6-fh,',iSD,)
Source: KOG0116-01
Prepared &. Analyzed: 07/14/2020
Total Kjeldahl Nitrogen
14.0 1-00.
mg/L 10.0 4.73 93
80-120 2 20
Batch KGO1434 ® Wet Chem Aqueous - SM 4500-P F-2011
LC"S (KG01434-6S1)
Prepared &Analyzed: 07/16/2020
2592 Hope Nfilift, Rd 1� Fay( Hcav�lffle, NI 28306 910.864.1920 p I www.hydrcrobac.corno
��, of 7
L Micmoo bac Laboratodes, tLhn�c. - Fayet'ev,'He
CERTIFi�,CPV'f E OF ANALSS
KOG01,91 16
Spilike Source %REG
RPD
Inorganics Tip ResuK RL
Units Lavell Result %REC Limits RP D
Lrtflt Notes
Batch KGO1434 - Wet Chem Aqueous - SM 4500-P F-2011
LC S (KGO1434-BSI)
Prepared & Analyzed: 07/16/2020
Phosphorus, Total 0.50 0.20
mg/L 0.50 99 90-110
iv'latrix Spike (KG01434-MS1) Source: KOGOOBI-01
Prepared &Analyzed: 07/16/2020
Phosphorus, Total 3.2 O,20
mg/L 2.5 0.63 102 90-110
Matrix Spike (KGO1434-MS2) Source: KOG0128-0-3p
Prepared &Analyzed: 07/16/2020
Phosphorus, Total 0,82 0.20
mg/L 2.5 ND 33 90-110
Matrix Spike Dup (KGO1434-MSD1). Source: KOG008,1-01
Prepared &Analyzed.- 07/16/2020
Phosphorus, Total 3.2 0 . 2- 0
mg/L 2.5 0.63 104 90-110 1
200
Matrix Spike Dup (KGO143441ASE12) source- P(D G 0 12 8 - 035,
Prepared & Analyzed: 07/16/2020
Phosphorus, Total 1.1 0.20
mg/L 2.6 N D 43 90-110 26
200
Ders
flnition
G 6 - The calculated seed corection exeeded the range of 0.6 to 1.0 mg/L.
mg/L- Milligrams per Liter
RL: Reporting Limit
RPD: Relative Percent Difference
Cooler Receipt Log
Cooler ID: Default Cooler Temp: 29.1 OC
Cooler Inspection Checkfist
ice Present or not required? Yes
Shipping containers seated or not required?
YeS,
Custody seals intact or not required? Yes
Chain of Custody (COC) Present?
Ye
'S
COC includes customer information? Yes
Relinquished and received signature on COC?
Yes
Sample collector identified on COC? Yes-3ample
J. type identified on COC?
Yes
Correct type of Containers Received yes
Correct number of containers listed on COC?
Yes
Containers Intact? Ye S
COC includes requested analyses?
Yes
Enough sample volume, for indicated tests received? Yes
Sample labels match COC (Name, Date & Time?)
Yes
Samples arrived within hold time? Yes
Correct preservatives on COC or not required?
Yes
Chemical preservations checked or not required? Yens
Preservation checks meet method requirements?
Yes
VOA vials have zero headspace, or not recd.? Yes
Project Requested Certification (s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Reviewed and Approved _By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents only the
sample(s) analyzed. This report is incomplete unless all pages indicated in the Too note are Brittany Srnith
present and an authorized signature is included. The senfices were provid4_- d Unr Jer and Administr2tion
subject to Mcrobac's standard terms and condifians vif-oWch Gan ilje located amof
reviewed at R,_�,ported: 07/17/2020 18-10
2592 Hope MIUs Rd Fayettevifle, NC 28306 910,864.1920 p, wVM,,1.MiCr0bar..com
11 Page 6 oli,'�: 7