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HomeMy WebLinkAboutNCG030526_DMR_20191030 Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted 4122n020 CERTIFICATE OF COVERAGE NO. NCGO3 0 5 2 6 SAMPLE COLLECTION YEAR 2019 FACILITY NAME BASIC MACHINERY CO.INC. SAMPLE PERIOD ❑Jan-June Q July-Dec COUNTY CHATS or ❑ Monthly1 (month) PERSON COLLECTING SAMPLES THOMAS M.MILHOLEN DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY SGS NORTH AMERICA INC. Lab Cert.# FL00946 RECEIVED ❑Zero-flow *Water Supply ESA ❑Other Comments on sample collection or analysis: APR 2 7 2020 CENTRAL LE.:-. PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWR SECTv • Part A:Stormwater Benchmarks and Monitoring Results No discharge this period?2 Date Sample 24-hour rainfall pH, Non-Polar O&G/ Total Toxic Outfall No. Collected' amount, Total Suspended Solids Standard units Total Copper Total Lead Total Zinc Total Petroleum Organics (mo/dd/yr) Inches' Hydrocarbons Benchmarks - - 100 mg/L or 50 mg/L` 6.0—9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 001 7/23/2019 .3" 66.9 mg/L 6.7 su <.025 <.005 .178 <5.2 mg/L Monthly sampling(instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 'See General Permit,Section B,Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals,or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample(for metal finishing use the definition as found in 40 CFR 433.11;for semiconductor manufacture use the definition as found in 40 CFR 469.12;for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify,and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver,the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Thomas M. Milholen Name(Print name) Q.A. Manager/Safety Coordinator Title(Print title) 4i2212w Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL,<PQL, Non-detect, ND,or other similar non-numerical format. When results are below the applicable limits,they must be reported in the format,"<XX mg/L",where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark,you must implement Tier 1, Tier 2,or Tier 3 responses. See General Permit text Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging>55 gal of new oil per month. ri No discharge this period?? Outfall No. Date Sample Collected' 24-hour rainfall amount, New Motor Oil or Non-Polar O&G/Total Total Suspended (mo/dd/yr) Inches' Hydraulic Oil Usage Petroleum Hydrocarbons Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2,or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245,last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO❑ IF YES,HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES❑ NO❑ REGIONAL OFFICE CONTACT NAME: Mail an original copy of this DMR, including all "No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period in the case of"No Discharge"reports)to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." Lt1221202.0 Signature of Permittee Date Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 3 of 3 4 SGS Orlando, FL 08/02/19 1 he results set lorth herein are provided by SGS North America Inc. C'-Hl//"dC'Op1' 2.0 Anion:W'd Repoli Technical Report for Basic Machinery Co Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC SGS Job Number: FA66280 Sampling Date: 07/23/19 d • Report to: Basic Machinery Co 1220 Harold Andrews Rd Siler City, NC 27344 murphy_milholen@basicmachinery.com ATTN: Murphy Milholen Total number of pages in report: 21 e r'/ Test results contained within this data package meet the requirements Caitlin Br ce, M.S. of the National Environmental laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent-Smith 407-425-6700 Certifications: FI.(I•:835101. I.A(03051),KS(E 10327). 11.120006:11,NU(5731.NJ(1,H.0021. NY)120221,S('(96036001) I)ol)It1.Al'(ANAIt 1.2229),Al(Al01100).CA(2937),TX(T104704404),1'A(Og 035731.VA(460177). AK.AR. IA.KY.MA. MS.NI), NI1.NV.OK.OR. UT.WA,WV This report shall not Ire reproduced,except in its entirety,without the written approval of SGS. Test results relate only to samples analyzed, SGS North America Inc • 4405 Vineland Road • Suite(' 15 • Orlando, 1,1 321111 • tel: 407 425 6700 • fax: 407 425 0707 SGSI of 21 I AI,/.JM0 Sections: Table of Contents Section 1: Sample Summary 3 Section 2: Summary of Hits 4 FA66280-1: BMC CATCH POND 6 Section 4: Misc. Forms 8 4=1' 4.1: Chain of Custody 9 A,,i s;., •i, fss.. 11: Prep QC MP35888: Cu,Pb,Zn 12 Section 6: General Chemistry - QC Data Summaries 18 6.1: Method Blank and Spike Results Summary 19 6.2: Duplicate Results Summary 20 6.3: Matrix Spike Results Summary 21 SGS2 of 21 I A10,:11/, t f SGS North America Inc. Sample Summary Basic Machinery Co Job No: FA66280 Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA66280-1 07/23/19 10:32 MM 07/24/19 AQ Surface Water BMC CATCH POND ' SGS Summary of Hits Page 1 of 1 :1 Job Number: FA66280 Account: Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC Collected: 07/23/19 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA66280-1 BMC CATCH POND Zinc 178 20 ug/l SW846 6010C Solids, Total Suspended 66.9 25 mg/I SM2540 D-11 pH a 6.70 su SM4500H B-11/SW9040C (a) Field analysis required. Received out of hold time and analyzed by request. SGS SGS rrLr Orlando, FL Sample Results Report of Analysis SGS5 of 21 1 Aiih:MO SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: BMC CATCH POND Lab Sample ID: FA66280-1 Date Sampled: 07/23/19 Matrix: AQ - Surface Water Date Received: 07/24/19 Percent Solids: n/a Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC Total Metals Analysis Analyte Result RL Units DF Prep Analyzed By Method Prep Method Copper <25 25 ug/l 1 07/31/19 08/01/19 LM SW846 6010C 1 SW846 3010A 2 Lead <5.0 5.0 ug/I 1 07/31/19 08/01/19 LM SW846 6010C 1 SW846 3010A 2 Zinc 178 20 ug/I 1 07/31/19 08/01/19 LM SW846 6010C 1 SW846 3010A 2 (1) Instrument QC Batch: MA16066 (2) Prep QC Batch: MP35888 RI, - Reporting Limit SGS 4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: BMC CATCH POND Lab Sample ID: FA66280-1 Date Sampled: 07/23/19 Matrix: AQ - Surface Water Date Received: 07/24/19 Percent Solids: n/a Project: Storm Water Run-off; 1220 Harold Andrews Rd, Slier City, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Oil and Grease <5.2 5.2 mg/I 1 07/31/19 11:36 CS EPA 1664A Solids, Total Suspended 66.9 25 mg/I 1 07/25/19 13:45 AG SM2540 D-11 pH a 6.70 su 1 07/25/19 11:50 BW SM4500H B-11/SW9040C (a) Field analysis required. Received out of hold time and analyzed by request. • RI. - Reporting Limit SGS , SGS xa Orlando, FL Section 4 .p Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody SGS 1' CHAIN OF CUSTODY FA11402)° PAGE_OF sarCamno a500 AmbssaeDr Ceffery Parkwoy,Scott,LA 70583 TEL.337237.4775 FAX!337.237.7838 SGS a.w. 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SW 1 , if ea.AC C Arc 3k Poesy Il 13 tt 10132 K M SW , 1 , I" 211elG CA'TCN PO4 'I 23/il ID:32 HM Sw 1 ✓ .•.T ru,.,n...l rna wer.ee y,nl 2,1"1•7.;,:••T:-;.:"l5;o:;.'3..7.1.2. •^z me.D0Ya.reOw Nampa,. ••-.. a.t.• ,..; f•.: Coment.I*WAY weuC*Wle *3:2:.`:.'.+1y:, OSwMwa lS seem..ow. -Xww.w We an.r ono ^D Cwewerelel•A•(Level 1) 0TRAP Nolo.Semple lvontcoy Is verified upon receipt in Inc labor0lory 17,ae.Ir,...D.n.IIU111 aw s Y Ceeere •Il.wl11 O Rl CSn Raleigh,n i\C 04 swine.. r.De HUSH _. �_ Q N Elbl LLT1 1 Level are i ae forme 0aawlnw•Der•RUSH _. _- 1=1 IRBT11Ler.INB 0 WDUPorm.l ^ O 1 aw,see Dar RUSH -- DrrM aetelM•C• 0(New Service Center 0,aweess Day LMENOTNCY _ __ Carmen.a'A'•.wrote UM), 0 at., —_ —. Correa,a V'•....ire•(%tweemoE Emmesnc7e RI,N'I/A ese sal Mla.a LAY*Aware'needed wH.1S1Xtneetyarcy lA 1 Co,rr_T.•I.e.•to•(IC 1_nmnwe<I1w 11M. fininia XI:a:Y tPti:'jr:"ti_z2ir+tif.:, Semple C11MWT11ttwlMdes Wow wcA a, Ise.Reap.PaaewebnyMu•'MWI.'Y sowed AEMwI.1- ._.1,L irEl...LA _rf±lif marl... ■read■. I ewn.ralwM hearse.' ..mew I '''.'0".!",i',' e _ '1 a81 rl 1 lI'bAM 1 Irt' -._—. 0 2 ----- I11or 2 --- ee ewer Imo seems. .reealeaesa err' earawF 2 �_ 3 — -.- _ 4 --_ 4 _ r,,.r, .L,�• e,rww«...lira 0M.r..e. ....OW Cmfolk Y1S area enamel wee aPa as O as 0 /3 L111A LW'IID;S CO tetra Sera SOM.rd CI x'. hep.IAwwr spa 1%SNaMerms.eed-awdtlelni. I'\66280, ( Il:lin 111' ( u`IWIN I).i21c I uI. 2 SGS9 of 21 SGS Sample Receipt Summary Job Number: FA66280 Client: BASIC MACHINERY CO. Project: STORMWATER RUN-OFF Date I Time Received: 7/24/2019 9:30:00 AM Delivery Method: FX Airbill Ws: Therm ID: IR 1; Therm CF: 1; #of Coolers: 1 Cooler Temps(Raw Measured)°C: Cooler 1:(0.3); Cooler Temps(Corrected)°C: Cooler 1:(1.3); A :-1. Cooler Information Y or N Sample Information Y or N N/A 1.Custody Seals Present v 1.Sample labels present on bottles v 2.Custody Seals Intact v 2.Samples preserved properly 3.Temp criteria achieved V 3.Sufficient volume/containers recvd for analysis: V 4.Cooler temp verification 1BSzslu 4.Condition of sample Intact 5.Cooler media Jce(Baal 5.Sample recvd within HT V 6.Dates/Times/IDs on COC match Sample Label v Trio Blank Information Y or N N/A 7.VOCs have headspace 1 Trip Blank present/cooler ye 8.Bottles received for unspecified tests 2 Trip Blank listed on COC V 9.Compositing instructions clear W or S N/A 10.Voa Soil Kits/Jars received past 48hrs? v 11.%Solids Jar received? V 3.Type Of TB Received 12.Residual Chlorine Present? v Misc.Information Number of Encores 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals Test Strip Lot ffs pH 0-3 230315 pH 10-12 219813A Other (Specify) Residual Chlorine Test Strip Lot f: Comments srnool Technician: PETERH Date, 7/24/2019 9.30 00 AM Reviewer. Dale: Rev D.I.OSMi17 ...‘66280: ( 'Main Of( 'll l(I(I\ Page 2 of 2 SGS I„ SGS Orlando, FL Metals Analysis QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Matrix Spike and Duplicate Summaries • Blank Spike and Lab Control Sample Summaries • Serial Dilution Summaries SGS " r , BLANK RESULTS SUMMARY Part 2 - Method Blanks Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Batch ID: MP35888 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/1 Prep Date: 07/31/19 Vr MB s Metal RL IDL MDL raw final _.,. Aluminum 200 14 14 1!::1 Antimony 6.0 1 1 Arsenic 10 1.3 1.3 Barium 200 1 1 Beryllium 4.0 .2 .2 Cadmium 5.0 .2 .2 Calcium 1000 50 50 Chromium 10 1 1 Cobalt 50 .2 .._ Copper 25 1 1 5.6 <25 Iron 300 17 17 Lead 5.0 1 1.1 -I.. <5.0 Magnesium 5000 15 35 Manganese 15 •5 1 Molybdenum 50 . i . 4 Nirkel 40 .4 .4 I' lassium 10000 .m00 .'110 :le t„nium in •4 •9 ::i I yet IO , I ,7 ,ud1um 1011111) 'mu ',00 :a runt lum In , , . , 'NIA l l Itan 10 1.1 1.•1 I1n ',0 'i 1 1 1 1.1 n 1 u m in 1 r 1:1.n114m 'III • , •6 i:1li• .n i I.1 n, I <20 /13 3,,..1 it•..I n unl l,•:1 MI'I .4a.4: Ill,.,'.n!-I h,.:1,1I I:t • II'I. .1i.• 3I,,W1i 13 .. I . I"r r.I1. 11.01 11 1'III••: .:1 ;•i I•u,31 I.• •.I V.• I III ry i ant A7111•1.. it 1,.q,i,•11•..I SGS • MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Batch ID: MP35888 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/1 Prep Date: 07/31/19 07/31/19 CM FA66462-3F QC FA66462-3F Spikelot QC -1 Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits t; Aluminum anr 1:::1 Antimony anr Arsenic anr Barium anr Beryllium anr Cadmium anr Calcium Chromium anr Cobalt anr Copper 0.0 1.4 200.0(a) 0-20 0.0 264 250 105.6 80-120 Iron am Lead 0.0 0.0 NC 0-20 Magnesium Manganese am Molybdenum Nickel in Potassium .elenium am Silver Ant ..o,f i um ::t I OIII I'm an Thallium Tin Titanium Vanaltum ant t.b I , 11.8 Q-.'t) 1.I. •II. ',u!1 91 - Asa ,,•I at.'I narnl,l l•a MI'1',nan: FAI.b.•n n-1 • u,. yl. vi, a:I r„I.' 1.,1 I:.r, 1„I11.,.rn•:I • i . .! . .. I,,. • !, I,.1,. ,! V 1un11., I - ••1 ' II I .. I II . .a'. Ia i .Ian,$ ... ,11 I I• . • SGS13 of 21 MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Batch ID: MP35888 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/1 Prep Date: 07/31/19 Ln FA66462-3F Spikelot MSD QC Metal Original MSD MPFLICP2 % Rec RPD Limit ter Aluminum anr Antimony anr Arsenic anr Barium anr Beryllium anr Cadmium anr Calcidm Chromium anr Cobalt anr Copper 0.0 266 250 106.4 0.8 20 Iron am Lead Magnesium Manganese am Molybdenum Nickel am ' Iutdssiurn .,•lenium .utr IIi Iv.�r ,rnr So.ltum t. ut iota .tar '111,11 1 1 unl 1 II I t ar11 tun V;111,1;ltum .tar Zl n.• t.t, .l,..1 ',no �t.'.I 0.4 ..e A:ut: • unl•.1:•:, Ml'1':rout: FA1.1,.',11-1 1•1',1111 • II'I. at.• .t:, ..•I • I..I al.'•ti.1t I::II Ivrl;n:u•:1 11111:11,1.. .:1 Qc 11I1k1!:1 1113 Mat I 1 x :',.I k.• le.,•• :::,13t,to .:I V'• 3ItnI .+ Ilit t All 11'71 t• rP:t I••;I•u•Yt,•1 • SGS SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Batch ID: MP35888 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/1 Prep Date: 07/31/19 cn BSP Spikelot QC Metal Result MPFLICP2 % Rec Limits Aluminum anr Antimony am Arsenic anr Barium am Beryllium anr Cadmium anr Calcium Chromium anr Cobalt anr Copper 251 ",n 100.4 80-120 Iron anr Lead 463 011 92.6 80-120 Magnesium Manganese am Molybdenum Nickel am Potassium ..1•Ionium am Silver am . .:nd t um an ;truntium it, Thallium Tin Titanium V.an.a.lium Int %in• 4H9 1,nn 97.8 Hn-ltn Ansurlat..d MI'1'•HHH: 1.116b.'Hfl-I 14,3,11,3 • IP1. nt•• :M.wn a:a :.•tu f,.r r.al •ul:at 1 n1 I u11.:..y.•:+ I.I 0v011'1.• .1 11' 11natln rant) Anal yt.• h..t t.•q v.••U.,1 15<,r s, SGS I Ann,'HO SERIAL DILUTION RESULTS SUMMARY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Batch ID: MP35888 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/1 Prep Date: 07/31/19 !n FA66462-3F QC ..a Metal Original SDL 1:5 %DIF Limits Aluminum anr 1:::1 Antimony anr Arsenic anr Barium anr Beryllium anr Cadmium anr Calcium Chromium anr Cobalt anr Copper 0.00 0.00 NC 0-10 Iron anr Lead 0.00 0.00 NC 0-10 Magnesium Manganese am Molybdenum Nickel am Pot assium .,•ienium ant 111Iv.1t ant ....411 um }t r"tlt lam 1111 1.11.11 I 1 um 1'I II •1.1 t an 1 un1 V.111a.11 Vt11 at11 411,• 1.bn !I.n,1 100.0(a) 'I-In A:!i.,r1 in 041 3.1n,) 1.••1 MI'1'.,u111: •,10..1 1.,•'nllt:1 • 11'1. 1,,• r11i"wn .1,1 ,•.•1.. 1'01 .•.11••1Ii 1! 1 ,1/ I.•111,,r'!.•'1 ,•1 !1111:111.1 „I cn• 1 Im i!3 latu! An.11y1„ n,! !,.1.1„•i!,..I I t1 f.•I•',•ttl 10 11,.I.•ti. 1.• •••1.! II 1,• •Ivy' !., I.'w Ib11 i.I: n lny.l,• ••.h „!:! 1 t• • tp• SGS �6 of 21 I ho!,:MO POST DIGESTATE SPIKE SUMMARY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Batch ID: MP35888 Methods: SW846 6010C Matrix Type: AQUEOUS Units: ug/1 Prep Date: 07/31/19 Sample Final FA66462-3F PS Spike Spike Spike QC Metal ml ml Raw Corr..` ug/1 ml ug/ml ug/1 % Rec Limits t,7 Aluminum Antimony 1:::1 Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper 9.8 10 107 0.2 5 100 107.0 80-120 Iron Lead 9.8 10 40.9 0.2 2.5 50 81.8 80-120 Magnosium M,,nganes,• Molybdenum Ni,:kel lot.IMsium Sel.•nium SiIVe; So.I t um ::1 I,In1 ium 1'In 'I'I t•i n l um • V.In.1,11 its /.II,,. •I.H 10 1.6 i.',.•,t .'i'I.', n..' I.•.'. .',0 94.4 Aan„'Inl,•.1 t,uut l'•.n MI't',HN,t: F71e,,.',t0_I • ! i, II., itt wn .c+ ,41,0.tt 1, l 1...11:.,1,•3 ,ri - Hit•., • Ii.m1,1,• v..l•slit.• / f In.ti v..14m.,I SGS17 of 21 SGS ,„.: Orlando, FL . Section 6 General Chemistry QC Data Summaries Includes the following where applicable: • Method Blank and Blank Spike Summaries • Duplicate Summaries • Matrix Spike Summaries SGS18 21 METHOD BLANK AND SPIKE RESULTS SUMMARY GENERAL CHEMISTRY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC MB Spike BSP BSP QC Analyte Batch ID RL Result Units Amount Result %Recov Limits HEM Oil and Grease GP33434/GN82631 5.0 0.0 mg/1 38 38.0 95.0 78-114% Solids, Total Suspended GN82587 2.5 0.0 mg/1 Associated Samples: Batch GN82587: FA66280-1 Cr) Batch GP33434: FA66280-1 (•) Outside of QC limits • SGS190121 DUPLICATE RESULTS SUMMARY GENERAL CHEMISTRY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Original DUP QC Analyte Batch ID Sample Units Result Result RPD Limits Solids, Total Suspended GN82587 FA66268-1 mg/1 28.0 29.6 5.6(a) 0-5% pH GN82594 FA66260-1 su 7.57 7.53 0.5 0-10% Associated Samples: Batch GN82587: FA66280-1 CD Batch GN82594: FA66280-1 (•) Outside of QC limits (a) RPD acceptable due to low duplicate and sample concentrations. C) SGS20 of 21 MATRIX SPIKE RESULTS SUMMARY GENERAL CHEMISTRY Login Number: FA66280 Account: BSMC - Basic Machinery Co Project: Storm Water Run-off; 1220 Harold Andrews Rd, Siler City, NC QC Original Spike MS QC Analyte Batch ID Sample Units Result Amount Result %Rec Limits HEM Oil and Grease GP33434/GN82631 FA66351-2 mg/1 1.5 U 36.63 36.6 91.3 78-114% Associated Samples: Batch GP33434: FA66280-1 (•) Outside of QC limits CD (N) Matrix Spike Rec. outside of QC limits La SGS21 "f 21