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HomeMy WebLinkAboutWQ0000672_Modification_20200817State of North Carolina Department of Environmental Quality Division of Water Resources a—W R —fig WATER QUALITY REGIONAL OPERATIONS SECTION d Division of Re uos rces, NON -DISCHARGE APPLICATION REVIEW REQUEST FORM August 17, 2020 To: FRO-WQROS: Trent Allen / Mark Brantley From: Ranveer Katyal, Water Quality Permitting Section - Non -Discharge Branch Permit Number:' WQ0000672 Applicant: City of Lumberton Owner Type: Municipal Facility Name: City of Lumberton RLAP Signature Authority; Corey Walters Address: PO Box 1388, Lumberton, NC 28359 Permit Type: Land Application of Residual Solids (503) Project Type: Major Modification Owner in BIMS? Yes Facility in BIMS? Yes Title: Public Works Deputy Director County: Robeson Fee Category: Non -Discharge Major Fee Amount: $395,- Major Modification Comments/Other Information: cjwalters@ci.lumberton.nc.us; envirochoice@gmail.com Attached, you will find all information submitted in support of the above -referenced application for your review, comment, and/or action. Within 45 calendar days, please -take the following actions: ® Return this form completed. ® _Return a completed staff report. ❑ Attach an Attachment B for Certification. ❑ Issue an Attachment B Certification � When you receive this request form, please write your name and dates in the spaces ,below, make a copy of this sheet, and return it to the appropriate Central Office Water Quality Permitting Section contact person listed above. RO-WQROS Reviewer: _�J (te r Date: 9 9 FORM: WQROSNDARR 09-15 Page 1 of 1 Barber, Jim From: Sent: To: Subject: Attachments: Trent Allen Fayetteville Regional Supervisor Division of Water Resources 910 433 3336 office Trent.Allen@ncdenr.gov 225 Green Street =Suite 714 Fayetteville, NC 28301 Allen, Trent Monday, August 17, 2020 8:20 PM Barber, Jim FW: [STAFF REPORT REQUEST] . QOOOOE Modification Application WQ0000672 WQROSNDARR 200817.pdf Email•correspondence to and from this address is subject to the to third parties - City of Lumberton RLAP Major Carolina Public Records Law and may be disclosed From: Thornburg; Nathaniel Sent: Monday, August 17; 202012:13 PM To: Allen,. Trent <trent.allen@ncdenr.gov>; Brantley, Mark <mark.brantley@ncdenr.gov> Cc: Williams, Kendall <kendall.williams@ncdenr.gov>; Katyal, RaInveer <Ranveer.Katyal@ncdenr.gov> Subject: [STAFF REPORT REQUEST] WQ0000672 -'City of Lumberton RLAP Major Modification Application RO Supervisors — Please assign this project to one of your staff for review. APPLICATION LINK: https://edocs.dep. nc.eov/WaterResou rces/DocV!ew.aspx?id=126771L6&d bid=0&repo=WaterResou rces Kendall, Please process the subject application received August 17, 2021 I've included the RO review request form for your use. I also in section of RO review request form. in BIMS. the Applicant email addresses in the comment 1 Please copy the RO, Reviewer, and myself on the acknowledgement letter that you send to the Applicant. Thank you, Nathaniel D. Thornburg Branch Chief Non -Discharge Branch Department of Environmental Quality 919 707 3653 office nathaniel.thornbure@ncdenr.eov, 512 N. Salisbury St. 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. z Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0000672 Applicant/Permittee City of Lumberton Applicant/Permittee Address 700 Lafayette Street, Lumberton, INC 28358 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Municipal Facility Name City of Lumberton RLAP County Robeson Fee Category Major Fee Amount $395 Is this a complete application?* r Yes r No Complete App Date 08/17/2020 Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by NI3 Staff Name * Enviro-Choice Recycling, LLC Email Address* envirochoicenc@gmail.com electronic subnittal, confirmation of receipt, and other correspondence. Project Information ........ ..................................................................................................................................................... Application/Document Type* r New (Fee Req ui red) c Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 9107385311 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WO0000672 Fbs Current Existing permt number Applicant/Permittee * City of Lumberton Applicant/Permittee Address* 700 Lafayette Street, Lumberton, NC 28358 Facility Name * City of Lumberton RLAP Please provide comments/notes on your current submittal below. Attached is the City of Lumberton Wastewater Treatment Facility request for permit modfication. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Tessa Monday at tessa.monday@ncdenr.gov or (919) 707-3660. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Specifications, Calculations, Rc.) Final Report.pdf 15.05MB Upload only 1 RCFdocurrent (less than 250 NE). NLftiple documents nest be corrbined into one R]Ffile unless file is larger than upload limit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature * Submission Date Is filled inautorraticallyonce subrrilted. PO Box 390 Lumberton, NC 28359 Phone: (910) 738-5311 Fax: (866) 768-8016 August 7, 2020 N.C. Environmental Quality-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Attention: Compliance Representative Subject: Residuals Land Application Modification for City of Lumberton Land Application Program (City of Lumberton WQ0000672) Dear Compliance Representative: The City of Lumberton is requesting a modification increasing the Annual Dry Tonnage. Enclosed is (1) copy of the Residuals Land Application Program Application as required in the modification permit for the City of Lumberton, North Carolina. This report was compiled from land application records provided by the City of Lumberton and Enviro-Choice Recycling. The report includes: 1) Residuals Land Application Program Application, 2) Residuals Source Certification, 3) Vicinity Map, 4) Process Flow Diagram, 5) Quantitative Justification, 6) Sampling Plan, 7) Laboratory Results, and 8) Copy of Existing Permit. Should you need more information regarding this land application program, please contact me at 910-738-5311. PW � 81( A 4,J Michael C. Hunt Enviro-Choice Recycling Attachment A: Residuals Land Application Program Application State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 - RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and sunnorting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General - This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): ® Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ® If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ❑ Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification 1 Major (land are permitted for > 300 acres) F_ $1,310 F $395 Minor (land are permitted for < 300 acres) F_ $810 F $245 1 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. D. >c, vir-,,.,,, ental Assessments (N", be Re"ir-ed See 15A �.Tr�G93s0) tmatmepA and stemge f4eilit4es. An E-A may also be r-e"ir-ed for- p4vate systems if apty ptiblie ftmds an&or- h-mds afe used foF INSTRUCTIONS FOR FORM: RLAP 06-16 Page 1 of 3 ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: By Courier/Special Delivery: 1617 MAIL SERVICE CENTER 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 L APPLICANT INFORMATION: 1. Applicant's name: City of Lumberton Applicant type: ❑ Individual [I Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal 17State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Corey Walters Title: Public Works Deputy Director Applicant's mailing address: P.O Box 1388 City: Lumberton State: NC Zip: 28359 Telephone number: (910) 671-3859 Email Address: ciwalters&ci.lumberton.nc.us 2. Consultant's name: Enviro-Choice Recycling, LLC License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: ) Consultant's mailing address: PO Box 390 City: Lumberton State: NC Zip: 28359- Telephone number: (910) 738-5311 Email Address: envirochoicenc(a gmail.com 3. Agronomist's name: License Number: Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: ) Agronomist's mailing address: City: State: Zip: - Telephone number: (_) _- Email Address: 4. Soil Scientist's name: License Number: Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: ) Soil Scientist's mailing address: City: State: Zip: - Telephone number: (_) _- Email Address: 5. Fee submitted: $395 (See Instruction B) IL PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00000672 Date of most -recently issued permit: April 27, 2017 Date of most -recently certified Attachment A (if different than the permit): Date of most -recently certified Attachment B (if different than the permit): FORM: RLAP 06-16 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: 700 Lafayette Street City: Lumberton State: NC Zip: 28358 Coordinates: Latitude: 34' 36' 20.1024" Longitude: 78' 59' 30.426" Datum: WGS 84 Level of accuracy: —25 It Method of measurement: Google Earth 2. County where residuals land application program is headquartered: Robeson 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Michael C Hunt Subcontractor 1006180 Back -Up ORC Eric T Locklear Subcontractor 1004579 Additional Back -Up ORCs (if applicable) Henry B Harper Jr. Chief Operator 1009036 If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 2000 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 34.82 47.82 69640 95640 Five -Year Maximum Adjusted 51.084 60.74 102168.1 121475 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops 475.4 Hay 123.7 Pasture 162.7 Total: 761.8 Methods Surface 475.4 Incorporation or Injection 286.4 Total: 761.8 FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 1392.8 1912.8 2043.361 2429.361 100 696.4 956.4 1021.681 1214.75 150 464.2667 637.6 681.1204 809.8336 200 348.2 478.2 510.8403 607.3752 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): Applicant will dewater residuals and haul solids to landfill and/or compost facility if needed. 7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. R Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Im Land Application Siite Certification. doc FORM: RLAP 06-16 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. Field � Zone Design -a Number- ox � Maximum Application � Design Annual Loading tit Y Nozzles Rafe (eal4o H'i LV4 FORM: RLAP 06-16 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. H Yes 0 No, Explain; I, Corey Walters Public Works Deputy Director (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for City of Lumberton WWTP (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement. representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. �gh ) Signature: Date: hj)( - FORM: RLAP 06-16 Page 5 of 5 Attachment B: Residuals Source Certification State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ❑ For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: City of Lumberton Status Code ° Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current n Proposed M City of Lumberton City of Lumberton Wastewater Treatment Plant Robeson WQ0000672 1500 2000 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: City of Lumberton 2. Facility permit holder is: Federal, 0 State, K Local Government, or ❑ Private. Facility permit issued by: Div. of Water Resources, Div. of Environmental Health, or Other (explain: M. 3. Facility contact person and title: Corey Walters, Public Works Deputy Director Complete mailing address: P.O Box 1388 City: Lumberton State: NC Zip: 28359-0— Telephone number: (910) 671-3856 E-mail address: ciwalterskci.lumberton.nc.us 4. Facility physical address: 700 Lafayette Street City: Lumberton State: NC Zip: 28358 Coordinates: Latitude: 34' 36' 20.1024" Longitude: 78' 59' 30.426" Datum: WGS 84 Level of accuracy: —25 ft Method of measurement: Google Earth 5. Purpose of the facility: treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, treatment of potable water, ❑ treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: = % industrial and = % domestic) other (explain: = ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: E MGD and facility average daily flow: 6_2 MGD 8. Average amount of residuals being generated at this facility M dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: NA Type and volume of residuals storage (i.e., outside of residuals treatment units): II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no If yes, list the number(s): = b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes U no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: ENCO Laboratories and Date of analysis: 7/13/2020 Passed corrosivity test: yes IR no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes ❑ no. Flashpoint 200 OF (> 140°F) Passed reactivity test: Eyes Ono. HCN: M mg/kg (<250) & HzS: M mg/kg (<500) TCLP Parameter Limit (mgfi) Result (mgfi) TCLP Parameter Limit (mgfi) Result (mgfi) Arsenic 5.0 0.380 Hexachlorobenzene 0.13 0.0006 Barium 100.0 0.0550 Hexachloro-1,3-Butadiene 0.5 0.02 Benzene 0.5 0.071 Hexachloroethane 3.0 0.0006 Cadmium 1.0 0.0180 Lead 5.0 0.155 Carbon Tetrachloride 0.5 0.094 Lindane 0.4 0.000021 Chlordane 0.03 0.00036 Mercury 0.2 0.000230 Chlorobenzene 100.0 0.072 Methoxychlor 10.0 0.000020 Chloroform 6.0 0.08 Methyl Ethyl Ketone 200.0 0.45 Chromium 5.0 0.0700 Nitrobenzene 2.0 0.0006 m-Cresol 200.0 0.02 Pentachlorophenol 100.0 0.002 o-Cresol 200.0 0.02 Pyridine 5.0 0.0007 p-Cresol 200.0 0.02 Selenium 1.0 0.310 Cresol 200.0 0.06 Silver 5.0 0.0950 2,4-D 10.0 0.007 Tetrachloroethylene 0.7 0.076 1,4-Dichlorobenzene 7.5 0.02 Toxaphene 0.5 0.00048 1,2-Dichloroethane 0.5 0.063 Trichloroethylene 0.5 0.089 1, 1 -Dichloroethylene 0.7 0.094 2,4,5-Trichlorophenol 400.0 0.0008 24-Dinitrotoluene 0.13 0.02 2,4,6-Trichlorophenol 2.0 0.001 Endrin 0.02 0.000014 2,4,5-TP (Silvex) 1.0 0.00044 Heptachlor and its Hydroxide 0.008 0.000018 Vinyl Chloride 0.2 0.071 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: ENCO Laboratories and Date of analysis: 7/13/2020 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg1kg) Monthly Average Concentration Limits (Class A Only) (mg1kg) Result (mg1kg) Arsenic 75 41 14.8 Cadmium 85 39 0.504 Copper 4,300 1,500 276 Lead 840 300 19.8 Mercury 57 17 2.13 Molybdenum 75 n/a 7.24 Nickel 420 420 41.3 Selenium 100 100 19.0 Zinc 7,500 2,800 613 �:��e�r�.�rss�rr�riner��ssins�reesss�rsnner�esrs�:�r_sr�rrs�Rsrsee�rr.�s��esrss� .eerarasrs� Distance fFom Disposal to BoundaFy to Closest Pr-opeFty Line iM to R . h e o Arsenie '" -0 } NickeUnit f } �ll--\ 1�-vt4 r25 -344 z�4 2444 � 25bt4 4 59 34 210 244 59'�5 3-9 2-69 2�8 n �':75bt4< loo 46 4W 328 n ll nn_�,,.15 52 360 494 �4- 25 62 4-59 429 Results lg4fg� FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 2.1 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutnent parameters: Laboratory: ENCO Laboratories and Date of analysis: 7/13/2020 Parameter Result (mg1kg) Aluminum 23100 Ammonia -Nitrogen 13000 Calcium 12300 Magnesium 2180 Nitrate -Nitrite Nitrogen 110 pH (Standard Unit) 7.3 Phosphorus 16000 Potassium 4030 Sodium 11400 Total Kjeldahl Nitrogen 49000 c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 3.60 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): 0 default value, or 0 actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1st) Year PAN Five -Year Maximum Adjusted PAN (mg1kg) (mg/kg) Surface 17,410 25,542 Injection/Incorporation 23,910 30,369 Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): 14 Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. J Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. J Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: 77 composting, [J heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: JQ Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.1106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: 19 aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, oi I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above. J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above. J Exempt - If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T. I106(a)(2)]. J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.11071 specify how residuals will meet the VAR requirements: d Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). E] Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). El Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T. I107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes. El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization. E] Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals. E] Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals. E] Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection. d Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Attachment C: Vicinity Map 41 E9T.•iSi A. 'i I I1I }Romdand Norment: E 8TH ST OAK ST v ` I Elem t Sch E 7Tr,':ST U �. f STH IST E TH ST r- E 41'h S7 5 3RE Sr WIND ST - f AND 57 �r F ISTS� rl Janie _ C Hargrave EIem `h.. Sch r U '•BACON ST hq l- S ^JQ`F ems! City of Lumberton Wastewater Treatment Plant J� - O 17 :ti^c L P'' USGS The National Map: National Boundaries Dataset; 3DEIP Elevation Program, Geographic Names4nformation System, National Hydrography Dataset, National Land Cover Database, National Structures Dataset, and National Transportation Dattaset; USGS Global Ecosystems; U.S. Census Bureau TIGER/Line data; SFS Road Data; Natural Earth Data; U.S. Department of State Hur) unitarian Information Unit; and NOAA National - Centers for Environmental, Information, U.S. Coastal Relief Model. Data -- / refreshed February, 2020� Graphical Scale 0 700 1,400 2,800 4,200 5,600 FigureFeet Site Location E Date: Permit Number: Drawn By: August 4 2020 W00000672 MCH Attachment D: Process Flow Diagram �l EFFLUENT SAMPLE �! FOMT/ EFF. FLOW METER (AVG,4<74 MG1l? i I f I f i'A.TF (1 : T LUMBERTON RYWTP PIPING AND VALVE SCHEMATIC HOLDING TANK 1 HEALS WORKS NF FLOW METERS (AVG. 5.32 MGD) Attachment E: Quantitative Justification Quantitative Justification for Residuals Production Rate During the current permit year (2020) the City has produced 1546 dry tons of residuals. In 2018 Lumberton produced 1291 dry tons. However, due to Hurricanes Florence and Matthew, production was limited to 476 tons in 2018 (no records online for 2017). Therefore, it is predicted that an additional 1,104 tons will be produced in 2020. In order to determine the maximum dry tonnage that could be applied on the fields in the current permit, an average PAN assuming the lowest feasible values for row crop plantings (corn) and actual values for pasture/hay crops the weighted average PAN is approximately 150 lbs PAN/acre. Our field network consists of 38% hay/pasture and 62% row crops. So we concluded that 2,000 dry tons per year would be the maximum we would be able to apply with the current permitted acreage using: Assumed Application Rate (lbs PAN/ac yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 1392.8 1912.8 2043.361 2429.361 100 696.4 956.4 1021.681 1214.75 150 464.2667 637.6 681.1204 809.8336 200 348.2 478.2 510.8403 607.3752 Since the five-year maximum will require the most acreage it was used to determine the maximum amount of dry tonnage to be permitted. At 2,000 dry tons: 681.12 x 0.38 (pasture/hay) + 809.83 x 0.62 (row crops) = 258.83 + 502.09 = 760.92 acres We currently have 761.8 acres permitted, which is how we determined 2,000 dry tons for our max. Should the City ever come close to this dry tonnage in the future, alternative dewatering means will be utilized at that point to ensure we remain below the permit limits. Attachment F: Sampling Plan Residuals Sampling Plan Treatment Plant Description The Lumberton Wastewater Treatment Plant (WWTP) is located at 700 Lafayette St in Lumberton North Carolina. The WWTP is under continuous operation to treat incoming wastewater prior to effluent discharge to the Lumber River. The majority of wastewater influent is domestic with some industrial. Residuals are produced constantly during this process; all residuals produced are stabilized via aerobic digestion. A plant diagram is attached below: 1lFilild]DiINA7l(YA1 Sewage Treatment Process Treatment Process fl LUI PH The wastewater treatment process includes the headworks, grit chamber, aeration basins, secondary clarifiers and chlorine contact tanks for disinfection, digesters, and holding tanks. The receiving stream is the Lumber River. Waste activated sludge and primary sludge are mixed and fed to an aerobic digester for stabilization. The digested biosolids are then transferred to holding tanks for storage until loaded into transportation vehicles and transported to the land application sites. Pathogen Reduction Class B Alternative 1 pathogen reduction requirements are met by having the geometric mean of the density of fecal coliform in the samples collected be less than 2,000,000 per gram of total solids on dry weight basis. The fecals are collected quarterly to maintain compliance. Vector Attraction Reduction Vector Attraction reduction is achieved through Option 4, which states that the specific oxygen uptake rate (SOUR) for biological residuals treated in an aerobic process shall be equal to or less than 1.5 milligrams of oxygen per hour per gram of total solids on a dry weight basis corrected to a temperature of 20 degrees Celsius. The SOUR is calculated quarterly. Pollutants Representative sampling of the aerobically digested residuals is conducted by a subcontractor on a quarterly schedule. This is the required minimum monitoring frequency based upon annual residuals production for land application. The samples that are collected are analyzed at Environmental Conservation Laboratories, Inc (NC Lab ID #591) and Cameron Testing Services (NC Lab ID #654). The quarterly representative residuals are collected in teflon plastic bottles from the holding tanks on -site. The samples are packed on ice and delivered to the following labs: Environmental Conservation Laboratories, Inc. 102 Woodwinds Industrial Ct. Ste. A Cary, NC 27511 Cameron Testing Services 219 S. Steele Street Sanford, NC 27330 The laboratory analyzes the residuals for the following parameters: Arsenic ( 5. 0) 1, 4-Dichlorobenzene ( 7. 5) Nitrobenzene ( 2. 0) Barium ( 100. 0) 1, 2- Dichloroethane ( 0. 5) Pentachlorophenol ( 100. 0) Benzene ( 0. 5) 1, 1 - Dichloroethylene ( 0. 7) Pyridine ( 5. 0) Cadmium (1. 0) 2, 4- Dinitrotoluene ( 0. 13) Selenium ( 1. 0) Carbon tetrachloride ( 0. 5) Endrin ( 0. 02 Silver ( 5. 0) Chlordane ( 0. 03) Hexachlorobenzene ( 0. 13) Chlorobenzene ( 100. 0) Heptachlor ( and its hydroxide) (0. 008) Toxaphene ( 0. 5) Chloroform ( 6. 0) Hexachloro-1, 3- butadiene ( 0. 5 Trichloroethylene ( 0. 5) Chromium (5. 0) Hexachloroethane ( 3. 0 2, 4, 5 - Trichlorophenol 400.0) m -Cresol ( 200. 0) Lead ( 5. 0) 2, 4, 6 -Trichlorophenol ( 2. 0) o -Cresol ( 200. 0) Lindane ( 0.4) 2, 4, 5 - TP ( Silvex) ( 1. 0) p -Cresol (200.0) Mercury ( 0. 2) Vinyl chloride ( 0. 2) Cresol ( 200. 0) Methoxychlor ( 10. 0) 2, 4- D ( 10. 0) Methyl ethyl ketone ( 200. 0) Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percert Total Solid TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) Attachment G: Laboratory Analyticals ENCO Laboratories 9g Accurate, Timely. Responsive. Iuuovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, July 31, 2020 Hunt Environmental Associates (HU017) Attn: Jordan Davis 3330 Saddletree Road. Lumberton, NC 28360 RE: Laboratory Results for Project Number: [none], Project Name/Desc: City of Lumberton ENCO Workorder(s): CD07944 Dear Jordan Davis, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Wednesday, June 24, 2020. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, OLdcc-'----�A Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 23 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: WW-1 Lab ID: CD07944-01 Sampled: 06/23/20 13:45 Received: 06/24/20 08:47 Parameter Preoaration Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 1010A NO PREP 07/07/20 07/02/20 15:00 07/02/20 15:30 EPA 6010D EPA 3010A 12/20/20 12/29/20 07/02/20 13:36 07/03/20 12:47 EPA 7470A EPA 7470A 07/21/20 07/29/20 07/01/20 12:07 07/02/20 10:55 EPA 8081B EPA 3510C 06/30/20 08/10/20 07/01/20 11:20 07/07/20 16:43 EPA 8151A EPA 3510C 06/30/20 08/11/20 07/02/20 09:00 07/07/20 20:38 EPA 8260D EPA 503013_MS 07/07/20 07/15/20 07/01/20 13:17 07/02/20 01:04 EPA 8270E EPA 3510C_MS 06/30/20 08/10/20 07/01/20 13:30 07/06/20 16:19 SW-846 Ch.7 Sec.3 NO PREP 07/07/20 07/07/20 10:00 07/07/20 16:00 SW-846 Ch.7 Sec.3 NO PREP 07/07/20 07/07/20 10:00 07/07/20 17:00 Client ID: WW-2 Lab ID: CD07944-02 Sampled: 06/23/20 13:45 Received: 06/24/20 08:47 Parameter Preoaration Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) CALC 9056A WETS-88 Soil 03/19/23 06/25/20 08:42 06/25/20 08:42 Leaching EPA 350.1 WETS-88 Soil 07/21/20 07/22/20 06/24/20 15:46 06/26/20 12:51 Leaching EPA 351.2 Same 07/21/20 07/02/20 08:10 07/06/20 11:22 EPA 365.4 Same 07/21/20 07/02/20 08:10 07/09/20 10:33 EPA 6010D EPA 3050B 12/20/20 06/26/20 14:48 06/30/20 14:04 EPA 7471B EPA 7471B 07/21/20 07/01/20 10:31 07/02/20 18:13 EPA 9045D Same 07/31/20 11:29 07/31/20 11:15 07/31/20 11:15 EPA 9056A WETS-88 Soil 06/26/20 06/26/20 13:04 06/24/20 13:04 06/24/20 19:44 Leaching SM 254OG-2011 NO PREP 06/30/20 06/28/20 10:10 06/28/20 10:10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 23 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: WW-2 Lab ID: CD07944-02 Analvte Results Flag MDL 2 Units Method Notes Aluminum - Total 23100 97.1 462 mg/kg dry EPA 6010D Ammonia as N 13000 D 420 920 mg/kg dry EPA 350.1 Cadmium - Total 0.504 J 0.444 2.31 mg/kg dry EPA 6010D Calcium - Total 12300 259 1160 mg/kg dry EPA 6010D Chromium - Total 228 4.62 23.1 mg/kg dry EPA 6010D Copper - Total 276 8.78 23.1 mg/kg dry EPA 6010D Lead - Total 19.8 J 5.55 23.1 mg/kg dry EPA 6010D Magnesium - Total 2180 43.0 1160 mg/kg dry EPA 6010D Molybdenum - Total 7.24 J 4.62 23.1 mg/kg dry EPA 6010D Nickel - Total 41.3 J 16.6 116 mg/kg dry EPA 6010D Nitrate as N 97 JB 95 460 mg/kg dry EPA 9056A J-01 Nitrate/Nitrite as N 110 9.5 23 mg/kg dry CALC 9056A Nitrite as N 13 JB 3.7 46 mg/kg dry EPA 9056A J-01 pH 7.3 1.0 1.0 pH Units EPA 9045D Phosphorus 16000 D 670 1800 mg/kg dry EPA 365.4 Potassium - Total 4030 185 1160 mg/kg dry EPA 6010D Sodium - Total 11400 277 1160 mg/kg dry EPA 6010D Temperature for pH (deg. C) 22 pH Units EPA 9045D Total Kjeldahl Nitrogen 49000 1600 1800 mg/kg dry EPA 351.2 Total Solids 2.1 0.0010 0.0010 % by Weight SM 2540G-2011 Zinc - Total 613 50.9 116 mg/kg dry EPA 6010D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 23 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-1 Lab Sample ID:CD07944-01 Received: 06/24/20 08:47 Matrix: Waste Water Sampled:06/23/20 13:45 Work Order: CD07944 Project: City of Lumberton Sampled By:CARRIGAN HARRIS TCLP Metals by 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes Arsenic [7440-38-2]^ 0.380 U mg/L 50 0.380 0.500 0G02038 EPA 6010D 07/03/20 12:47 JDH Barium [7440-39-3]^ 0.0550 U mg/L 50 0.0550 0.500 0G02038 EPA 6010D 07/03/20 12:47 JDH Cadmium [7440-43-9]^ 0.0180 U mg/L 50 0.0180 0.0500 0G02038 EPA 6010D 07/03/20 12:47 JDH Chromium [7440-47-3]^ 0.0700 U mg/L 50 0.0700 0.500 0G02038 EPA 6010D 07/03/20 12:47 JDH Lead [7439-92-1]^ 0.155 U mg/L 50 0.155 0.500 0G02038 EPA 6010D 07/03/20 12:47 JDH Selenium [7782-49-2]^ 0.310 U mg/L 50 0.310 0.500 0G02038 EPA 6010D 07/03/20 12:47 JDH Silver [7440-22-4]^ 0.0950 U mg/L 50 0.0950 0.500 0G02038 EPA 6010D 07/03/20 12:47 JDH TCLP Volatile Organics by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes 1,1-Dichloroethene [75-35-4]^ 0.094 UD mg/L 100 0.094 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW 1,2-Dichloroethane [107-06-2]^ 0.063 UD mg/L 100 0.063 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW 2-Butanone [78-93-3]^ 0.45 UD mg/L 100 0.45 0.50 0GO1040 EPA 8260D 07/02/20 01:04 KKW Benzene [71-43-2]^ 0.071 UD mg/L 100 0.071 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW Carbon Tetrachloride [56-23-5]^ 0.094 UD mg/L 100 0.094 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW Chlorobenzene [108-90-7]^ 0.072 UD mg/L 100 0.072 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW Chloroform [67-66-3]^ 0.080 UD mg/L 100 0.080 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW Tetrachloroethene [127-18-4]^ 0.076 UD mg/L 100 0.076 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW Trichloroethene [79-01-6]^ 0.089 UD mg/L 100 0.089 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW Vinyl chloride [75-01-4]^ 0.071 UD mg/L 100 0.071 0.10 0GO1040 EPA 8260D 07/02/20 01:04 KKW Sunoaates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes 4-Bromofluorobenzene 0.054 1 0.0500 107 % 41-142 0GO1040 EPA 8260D 07102120 01:04 KKW Dibromofluoromethane 0.057 1 0.0500 113 % 53-146 0GO1040 EPA 8260D 07102120 01:04 KKW Toluene-d8 0.053 1 0.0500 106 % 41-146 0GO1040 EPA 8260D 07102120 01:04 KKW TCLP Semivolatile Organics by GCMS ^ - ENCO Orlando certified analyte [NC 424] Analyte MAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,4-Dichlorobenzene [106-46-7]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi 2,4,5-Trichlorophenol [95-95-4]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi 2,4,6-Trichlorophenol [88-06-2]^ 0.03 UD mg/L 5 0.03 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi 2,4-Dinitrotoluene [121-14-2]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi 2-Methylphenol [95-48-7]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi QV-01 3 & 4-Methylphenol[108-39-4/106-44-5]^ 0.04 UD mg/L 5 0.04 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi Hexachlorobenzene [118-74-1]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi Hexachlorobutadiene [87-68-3]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi Hexachloroethane [67-72-1]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi Nitrobenzene [98-95-3]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi Pentachlorophenol[87-86-5]^ 0.04 UD mg/L 5 0.04 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi Pyridine [110-86-1]^ 0.02 UD mg/L 5 0.02 0.05 0GO1036 EPA 8270E 07/06/20 16:19 jfi surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes 2,4,6-Tribromophenol 0.10 5 0.250 40 % 33-145 0GO1036 EPA 8270E 0710612016:19 jfi 2-Fluorobiphenyl 0.16 5 0.250 65 % 32-116 0GO1036 EPA 8270E 0710612016:19 jfi 2-Fluorophenol 0.10 5 0.250 40 % 11-100 0GO1036 EPA 8270E 0710612016:19 jfi Nitrobenzene-d5 0.13 5 0.250 54 % 24-107 0GO1036 EPA 8270E 0710612016:19 jfi FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 23 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-1 Lab Sample ID:CD07944-01 Received: 06/24/20 08:47 Matrix: Waste Water Sampled:06/23/20 13:45 Work Order: CD07944 Project: City of Lumberton Sampled By:CARRIGAN HARRIS TCLP Semivolatile Organics by GCMS ^ - ENCO Orlando certified analyte [NC 424] Sunoaates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vied By Notes Phenol-d5 0.060 5 0.250 24 % 10-100 0GO1036 EPA 8270E 0710612016:19 jfi Telphenyl-d14 0.19 5 0.250 78 % 52-150 0GO1036 EPA 8270E 0710612016:19 jfi TCLP Pesticides by GC ^ - ENCO Orlando certified analyte [NC 424] Analyte MAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes Chlordane (tech) [12789-03-6]^ 0.00036 U mg/L 1 0.00036 0.00050 0GO1025 EPA 8081B 07/07/20 16:43 JIB Endrin [72-20-8]^ 0.000014 U mg/L 1 0.000014 0.000050 0GO1025 EPA 8081B 07/07/20 16:43 JIB gamma-BHC [58-89-9]^ 0.000021 U mg/L 1 0.000021 0.000050 0GO1025 EPA 8081B 07/07/20 16:43 JIB Heptachlor [76-44-8]^ 0.000026 U mg/L 1 0.000026 0.000050 0GO1025 EPA 8081B 07/07/20 16:43 JIB Heptachlor epoxide [1024-57-3]^ 0.000018 U mg/L 1 0.000018 0.000050 0GO1025 EPA 8081B 07/07/20 16:43 JIB Methoxychlor [72-43-5]^ 0.000020 U mg/L 1 0.000020 0.000050 0GO1025 EPA 8081B 07/07/20 16:43 JIB Toxaphene [8001-35-2]^ 0.00048 U mg/L 1 0.00048 0.00050 0GO1025 EPA 8081B 07/07/20 16:43 JIB surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes 2,4,5,E-TCMX 0.0035 1 0.00500 70 % 38-142 0GO1025 EPA 8081B 0710712016:43 JJB Decachloroblphenyl 0.0032 1 0.00500 64 % 34-159 0GO1025 EPA 8081B 0710712016:43 JJB TCLP Herbicides by GC ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes 2,4,5-TP (Silvex) [93-72-1]^ 0.00044 U mg/L 1 0.00044 0.00050 0G02006 EPA 8151A 07/07/20 20:38 RGG 2,4-D [94-75-7]^ 0.00027 U mg/L 1 0.00027 0.00050 0G02006 EPA 8151A 07/07/20 20:38 RGG Sunoaates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes 2,4-DC4A 0.0073 1 0.0100 73 % 37-134 0GO2006 EPA 8151A 07107120 2038 RGG TCLP Metals by 6000/7000 Series Methods ^ - ENCO Orlando certified analyte [NC 424] Analyte MAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed Notes Mercury [7439-97-6]^ 0.000230 U mg/L 1 0.000230 0.00200 0GO1019 EPA 7470A 07/02/20 10:55 ]SS Classical Chemistry Parameters Analyte MAS Numberl Reactive Cyanide [57-12-5] Reactive Sulfide [57-12-5] Results Flag Units DF Q Batch Method Analyzed By Notes 250 U mg/L 1 250 0G07010 3W-846 Ch.7 Sec.- 07/07/20 16:00 PIR 500 U mg/L 1 500 0G08018 3W-846 Ch.7 Sec.- 07/07/20 17:00 PIR FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 23 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: WW-1 Lab Sample ID:CD07944-01 Received: 06/24/20 08:47 Matrix: Waste Water Sampled:06/23/20 13:45 Work Order: CD07944 Project: City of Lumberton Sampled By:CARRIGAN HARRIS Classical Chemistry Parameters Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes Flashpoint > 200 OF 1 OG02008 EPA 1O10A 07/02/20 15:30 SMA Description: WW-2 Lab Sample ID:CD07944-02 Received: 06/24/20 08:47 Matrix: Sludge Sampled:06/23/20 13:45 Work Order: CD07944 Project: City of Lumberton Sampled By:CARRIGAN HARRIS % Solids: 2.16 Metals by EPA 6000/7000 Series Methods ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes Aluminum [7429-90-5]^ 23100 mg/kg dry 1 97.1 462 OF26026 EPA 6010D 06/30/20 14:04 JDH Arsenic [7440-38-2]A 14.8 U mg/kg dry 1 14.8 23.1 OF26026 EPA 6010D 06/30/20 14:04 JDH Cadmium [7440-43-9]A 0.504 J mg/kg dry 1 0.444 2.31 OF26026 EPA 6010D 06/30/20 14:04 JDH Calcium [7440-70-2]A 12300 mg/kg dry 1 259 1160 OF26026 EPA 6010D 06/30/20 14:04 JDH Chromium [7440-47-3]A 228 mg/kg dry 1 4.62 23.1 OF26026 EPA 6010D 06/30/20 14:04 JDH Copper [7440-50-8]A 276 mg/kg dry 1 8.78 23.1 OF26026 EPA 6010D 06/30/20 14:04 JDH Lead [7439-92-1]A 19.8 J mg/kg dry 1 5.55 23.1 OF26026 EPA 6010D 06/30/20 14:04 JDH Magnesium [7439-95-4]A 2180 mg/kg dry 1 43.0 1160 OF26026 EPA 6010D 06/30/20 14:04 JDH Mercury [7439-97-6]A 2.13 U mg/kg dry 1 2.13 2.85 OG01013 EPA 7471B 07/02/20 18:13 KAH Molybdenum [7439-98-7]1 7.24 J mg/kg dry 1 4.62 23.1 OF26026 EPA 6010D 06/30/20 14:04 JDH Nickel [7440-02-0]A 41.3 J mg/kg dry 1 16.6 116 OF26026 EPA 6010D 06/30/20 14:04 JDH Potassium [7440-09-7]A 4030 mg/kg dry 1 185 1160 OF26026 EPA 6010D 06/30/20 14:04 JDH Selenium [7782-49-2]A 19.0 U mg/kg dry 1 19.0 23.1 OF26026 EPA 6010D 06/30/20 14:04 JDH Sodium [7440-23-5]^ 11400 mg/kg dry 1 277 1160 OF26026 EPA 6010D 06/30/20 14:04 JDH Zinc [7440-66-6]1 613 mg/kg dry 1 50.9 116 OF26026 EPA 6010D 06/30/20 14:04 JDH Classical Chemistry Parameters Analyte rCAS Numberl Results Flag Units DF MDL 2 Batch Method Analyzed By Notes Ammonia as N [7664-41-7] 13000 D mg/kg dry 20 420 920 OF24036 EPA 350.1 06/26/20 12:51 JAH Nitrate as N [14797-55-8] 97 JB mg/kg dry 1 95 460 OF24022 EPA 9056A 06/24/20 19:44 LJI J-01 Nitrate/Nitrite as N 110 mg/kg dry 1 9.5 23 OF25007 CALC 9056A 06/25/20 08:42 LJI Nitrite as N [14797-65-0] 13 JB mg/kg dry 1 3.7 46 OF24022 EPA 9056A 06/24/20 19:44 LJI 3-01 pH 7.3 pH Units 1 1.0 1.0 OG31023 EPA 9045D 07/31/20 11:15 LJI Phosphorus [7723-14-0] 16000 D mg/kg dry 5 670 1800 OG02010 EPA 365.4 07/09/20 10:33 JAH Temperature for pH (deg. C) 22 pH Units 1 OG31023 EPA 9045D 07/31/20 11:15 LJI Total Kjeldahl Nitrogen 49000 mg/kg dry 1 1600 1800 OG02011 EPA 351.2 07/06/20 11:22 JAH Total Solids 2.1 % by Weight 1 0.0010 0.0010 OF28001 SM 2540G-2011 06/28/20 10:10 BDC FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch OF26O26 - EPA 3050E Blank (OF26026-BLKI) Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:41 Spike Source a/oREC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Aluminum 2.42 1 10.0 mg/kg wet Arsenic 0.320 U 0.500 mg/kg wet Cadmium 0.00960 U 0.0500 mg/kg wet Calcium 5.60 U 25.0 mg/kg wet Chromium 0.100 U 0.500 mg/kg wet Copper 0.190 U 0.500 mg/kg wet Lead 0.120 U 0.500 mg/kg wet Magnesium 0.930 U 25.0 mg/kg wet Molybdenum 0.100 U 0.500 mg/kg wet Nickel 0.360 U 2.50 mg/kg wet Potassium 4.00 U 25.0 mg/kg wet Selenium 0.410 U 0.500 mg/kg wet Sodium 6.00 U 25.0 mg/kg wet Zinc 1.10 U 2.50 mg/kg wet LCS (OF26026-BSI) Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:44 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Aluminum 104 10.0 mg/kg wet 106 97 80-120 Arsenic 10.3 0.500 mg/kg wet 10.6 97 80-120 Cadmium 1.07 0.0500 mg/kg wet 1.06 101 80-120 Calcium 116 25.0 mg/kg wet 106 109 80-120 Chromium 10.3 0.500 mg/kg wet 10.6 97 80-120 Copper 10.2 0.500 mg/kg wet 10.6 96 80-120 Lead 10.6 0.500 mg/kg wet 10.6 100 80-120 Magnesium 105 25.0 mg/kg wet 106 99 80-120 Molybdenum 10.5 0.500 mg/kg wet 10.6 99 80-120 Nickel 10.8 2.50 mg/kg wet 10.6 101 80-120 Potassium 533 25.0 mg/kg wet 532 100 80-120 Selenium 10.2 0.500 mg/kg wet 10.6 96 80-120 Sodium 508 25.0 mg/kg wet 532 96 80-120 Zinc 10.9 2.50 mg/kg wet 10.6 103 80-120 Matrix Spike (OF26026-MS1) Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:49 Source: CD09771-38 Spike Source %REC RPD Analvte Result FFFlau Q Units Level Result %REC Limits RPD Limit Notes Aluminum 8630 11.3 mg/kg dry 119 3850 NR 75-125 QM-07 Arsenic 11.4 0.564 mg/kg dry 11.9 0.383 93 75-125 Cadmium 1.06 0.0564 mg/kg dry 1.19 0.0108 U 89 75-125 Calcium 315 28.2 mg/kg dry 119 201 96 75-125 Chromium 15.6 0.564 mg/kg dry 11.9 3.02 106 75-125 Copper 14.4 0.564 mg/kg dry 11.9 1.83 106 75-125 Lead 245 0.564 mg/kg dry 11.9 274 NR 75-125 QM-07 Magnesium 540 28.2 mg/kg dry 119 313 191 75-125 QM-07 Molybdenum 11.2 0.564 mg/kg dry 11.9 0.113 U 94 75-125 Nickel 13.1 2.82 mg/kg dry 11.9 0.581 105 75-125 Potassium 1230 28.2 mg/kg dry 594 485 126 75-125 QM-07 Selenium 8.33 0.564 mg/kg dry 11.9 0.463 U 70 75-125 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch OF26O26 - EPA 3050E - Continued Matrix Spike (OF26026-MSI) Continued Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:49 Source: CD09771-38 Spike Source a/oREC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Sodium 583 28.2 mg/kg dry 594 9.21 97 75-125 Zinc 24.6 2.82 mg/kg dry 11.9 9.55 127 75-125 QM-07 Matrix Spike Dup (OF26026-MSD1) Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 13:57 Source: CD09771-38 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Aluminum 7220 11.3 mg/kg dry 115 3850 NR 75-125 18 20 QM-07 Arsenic 10.5 0.564 mg/kg dry 11.5 0.383 88 75-125 8 20 Cadmium 1.04 0.0564 mg/kg dry 1.15 0.0108 U 90 75-125 1 20 Calcium 286 28.2 mg/kg dry 115 201 74 75-125 10 20 QM-07 Chromium 14.1 0.564 mg/kg dry 11.5 3.02 97 75-125 10 20 Copper 13.1 0.564 mg/kg dry 11.5 1.83 98 75-125 10 20 Lead 225 0.564 mg/kg dry 11.5 274 NR 75-125 8 20 QM-07 Magnesium 461 28.2 mg/kg dry 115 313 128 75-125 16 20 QM-07 Molybdenum 10.5 0.564 mg/kg dry 11.5 0.113 U 91 75-125 7 20 Nickel 12.2 2.82 mg/kg dry 11.5 0.581 101 75-125 7 20 Potassium 1080 28.2 mg/kg dry 576 485 103 75-125 13 20 Selenium 8.39 0.564 mg/kg dry 11.5 0.463 U 73 75-125 0.6 20 QM-07 Sodium 543 28.2 mg/kg dry 576 9.21 93 75-125 7 20 Zinc 21.6 2.82 mg/kg dry 11.5 9.55 105 75-125 13 20 Post Spike (OF26026-PSI) Prepared: 06/26/2020 14:48 Analyzed: 06/30/2020 14:00 Source: CD09771-38 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Aluminum 65.7 0.200 mg/L 2.00 64.8 45 80-120 QM-08 Arsenic 0.220 0.0100 mg/L 0.200 0.00645 107 80-120 Cadmium 0.0215 0.00100 mg/L 0.0200 -0.000365 108 80-120 Calcium 5.53 0.500 mg/L 2.00 3.38 108 80-120 Chromium 0.260 0.0100 mg/L 0.200 0.0509 104 80-120 Copper 0.243 0.0100 mg/L 0.200 0.0309 106 80-120 Lead 4.71 0.0100 mg/L 0.200 4.61 49 80-120 QM-08 Magnesium 7.31 0.500 mg/L 2.00 5.27 102 80-120 Molybdenum 0.218 0.0100 mg/L 0.200 0.000870 109 80-120 Nickel 0.229 0.0500 mg/L 0.200 0.00978 110 80-120 Potassium 19.4 0.500 mg/L 10.0 8.17 112 80-120 Selenium 0.191 0.0100 mg/L 0.200 -0.0258 96 80-120 Sodium 10.9 0.500 mg/L 10.0 0.155 107 80-120 Zinc 0.370 0.0500 mg/L 0.200 0.161 105 80-120 Batch 0GO1O13 - EPA 7471E Blank (OG01013-BLKI) Prepared: 07/O1/2020 10:31 Analyzed: 07/02/2020 18:09 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.0460 U 0.0617 mg/kg wet FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA Metals by EPA 6000/7000 Series Methods - Quality Control Batch 0GO1013 - EPA 7471E - Continued LCS (OG01013-BSI) Prepared: 07/O1/2020 10:31 Analyzed: 07/02/2020 18:11 Spike Source a/oREC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.594 0.0617 mg/kg wet 0.600 99 80-120 Matrix Spike (OG01013-MSI) Prepared: 07/O1/2020 10:31 Analyzed: 07/02/2020 18:16 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 29.8 3.17 mg/kg dry 30.8 2.36 U 97 80-120 Matrix Spike Dup (OG01013-MSD1) Prepared: 07/01/2020 10:31 Analyzed: 07/02/2020 18:17 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 32.1 3.42 mg/kg dry 33.3 2.55 U 96 80-120 7 20 Post Spike (OG01013-PSI) Prepared: 07/01/2020 10:31 Analyzed: 07/02/2020 18:19 Source: CD07944-02 Spike Source %REC RPD Analyte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 5.72 0.514 ug/L 5.00 0.122 112 75-125 TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 0GO2038 - EPA 3010A Blank (OG02038-BLKI) Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 11:47 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Arsenic 0.380 U 0.500 mg/L Barium 0.0607 1 0.500 mg/L Cadmium 0.0180 U 0.0500 mg/L Chromium 0.0700 U 0.500 mg/L Lead 0.155 U 0.500 mg/L Selenium 0.310 U 0.500 mg/L Silver 0.0950 U 0.500 mg/L LCS (OG02038-BSI) Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 11:52 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Arsenic 0.190 0.0100 mg/L 0.200 95 80-120 Barium 0.201 0.0100 mg/L 0.200 101 80-120 Cadmium 0.0193 0.00100 mg/L 0.0200 96 80-120 Chromium 0.192 0.0100 mg/L 0.200 96 80-120 Lead 0.195 0.0100 mg/L 0.200 97 80-120 Selenium 0.190 0.0100 mg/L 0.200 95 80-120 Silver 0.191 0.0100 mg/L 0.200 95 80-120 Matrix Spike (OG02038-MS1) Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:38 Source: CD10423-01 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Arsenic 8.99 0.500 mg/L 10.0 0.380 U 90 75-125 Barium 10.3 0.500 mg/L 10.0 0.779 95 75-125 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 0GO2O38 - EPA 3O1OA - Continued Matrix Spike (OG02038-MS3) Continued Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:38 Source: CD10423-01 Spike Source a/oREC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Cadmium 0.925 0.0500 mg/L 1.00 0.0180 U 92 75-125 Chromium 9.12 0.500 mg/L 10.0 0.0700 U 91 75-125 Lead 9.37 0.500 mg/L 10.0 0.155 U 94 75-125 Selenium 9.24 0.500 mg/L 10.0 0.310 U 92 75-125 Silver 9.07 0.500 mg/L 10.0 0.0950 U 91 75-125 Matrix Spike Dup (OG02038-MSDI) Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:40 Source: CD10423-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Arsenic 8.93 0.500 mg/L 10.0 0.380 U 89 75-125 0.7 20 Barium 10.2 0.500 mg/L 10.0 0.779 94 75-125 1 20 Cadmium 0.904 0.0500 mg/L 1.00 0.0180 U 90 75-125 2 20 Chromium 9.06 0.500 mg/L 10.0 0.0700 U 91 75-125 0.7 20 Lead 9.20 0.500 mg/L 10.0 0.155 U 92 75-125 2 20 Selenium 9.10 0.500 mg/L 10.0 0.310 U 91 75-125 1 20 Silver 9.16 0.500 mg/L 10.0 0.0950 U 92 75-125 1 20 Post Spike (OG02038-PSI) Prepared: 07/02/2020 13:36 Analyzed: 07/03/2020 12:42 Source: CD10423-01 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Arsenic 0.182 0.0100 mg/L 0.200 -0.00291 91 80-120 Barium 0.206 0.0100 mg/L 0.200 0.0156 95 80-120 Cadmium 0.0185 0.00100 mg/L 0.0200 0.000100 92 80-120 Chromium 0.183 0.0100 mg/L 0.200 0.000195 92 80-120 Lead 0.187 0.0100 mg/L 0.200 0.00295 92 80-120 Selenium 0.190 0.0100 mg/L 0.200 -0.000449 95 80-120 Silver 0.188 0.0100 mg/L 0.200 -0.000292 94 80-120 Classical Chemistry Parameters - Quality Control Batch OF24O22 - WETS-88 Soil Leaching Blank (OF24022-BLKI) Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 19:09 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Nitrate as N 2.0 1 10 mg/kg wet J-01 Nitrite as N 0.19 1 1.0 mg/kg wet J-01 LCS (OF24022-BSI) Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 19:26 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Nitrate as N 48 B 10 mg/kg wet 50.0 97 80-120 Nitrite as N 9.7 B 1.0 mg/kg wet 10.0 97 80-120 Matrix Spike (OF24022-MSI) Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 20:02 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Nitrate as N 820 B 460 mg/kg dry 925 97 78 80-120 QM-07 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OF24022 - WETS-88 Soil Leaching - Continued Matrix Spike (OF24022-MSI) Continued Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 20:02 Source: CD07944-02 Spike Source a/oREC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Nitrite as N 440 B 46 mg/kg dry 462 13 93 80-120 Matrix Spike Dup (OF24022-MSD3) Prepared: 06/24/2020 13:04 Analyzed: 06/24/2020 20:19 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Nitrate as N 810 B 460 mg/kg dry 925 97 78 80-120 0.1 15 QM-07 Nitrite as N 440 B 46 mg/kg dry 462 13 93 80-120 0.1 15 Batch OF24036 - NO PREP Blank (OF24036-BLKI) Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:44 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Ammonia as N 0.45 U 1.0 mg/kg wet LCS (OF24036-BSI) Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:49 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Ammonia as N 10 1.0 mg/kg wet 10.1 101 90-110 Matrix Spike (OF24036-MSI) Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:53 Source: CD07944-02 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Ammonia as N 13000 D 920 mg/kg dry 187 13000 NR 90-110 QM-07 Matrix Spike Dup (OF24036-MSDI) Prepared: 06/24/2020 15:46 Analyzed: 06/26/2020 12:54 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Ammonia as N 13000 D 920 mg/kg dry 187 13000 169 90-110 3 10 QM-07 Batch OF28001 - NO PREP Duplicate (OF28001-DUPI) Prepared & Analyzed: 06/28/2020 10: 10 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Total Solids 2.1 0.0010 % by Weight 2.1 0.6 25 Batch 0GO2010 - Same Blank (OG02010-BLK3) Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:31 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Phosphorus 2.6 U 7.2 mg/kg wet LCS (OG02010-BSI) Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:32 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Phosphorus 120 8.0 mg/kg wet 126 92 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 0GO2010 - Same - Continued Matrix Spike (OG02010-MSI) Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:34 Source: CD07944-02 Spike Source a/oREC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Phosphorus 20000 D 1800 mg/kg dry 2250 16000 146 80-120 QM-07 Matrix Spike Dup (OG02010-MSDI) Prepared: 07/02/2020 08:10 Analyzed: 07/09/2020 10:35 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Phosphorus 19000 D 1800 mg/kg dry 2350 16000 97 80-120 5 25 Batch 0GO2011 - Same Blank (OG02011-BLKI) Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:19 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 32 U 35 mg/kg wet LCS (OG02011-BSI) Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:21 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 990 38 mg/kg wet 946 104 90-110 Matrix Spike (OG02011-MSI) Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:24 Source: CD07944-02 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 63000 1800 mg/kg dry 16800 49000 87 90-110 QM-07 Matrix Spike Dup (OG02011-MSDI) Prepared: 07/02/2020 08:10 Analyzed: 07/06/2020 11:26 Source: CD07944-02 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Total Kjeldahl Nitrogen 65000 1800 mg/kg dry 17600 49000 93 90-110 3 10 Batch OG31023 - Same LCS (OG31023-BSI) Prepared & Analyzed: 07/31/2020 11:15 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes pH 6.9 1.0 pH Units 7.00 99 99-101 Duplicate (OG31023-DUP3) Prepared & Analyzed: 07/31/2020 11:15 Source: CD11905-01 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes pH 5.4 1.0 pH Units 5.4 0.7 25 TCLP Volatile Organics by GCMS - Quality Control Batch 0GO1040 - EPA 5030E MS Blank (OG01040-BLKI) Prepared: 07/01/2020 13:17 Analyzed: 07/02/2020 00:02 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Volatile Organics by GCMS - Quality Control Batch 0GO1O4O - EPA 5030E MS - Continued Blank (OG01040-BLKI) Continued Prepared: 07/O1/2020 13:17 Analyzed: 07/02/2020 00:02 Analyte Result Flaa Q Units 1,1-Dichloroethene 0.00094 U 0.0010 mg/L 1,2-Dichloroethane 0.00063 U 0.0010 mg/L 2-Butanone 0.0045 U 0.0050 mg/L Benzene 0.00071 U 0.0010 mg/L Carbon Tetrachloride 0.00094 U 0.0010 mg/L Chlorobenzene 0.00072 U 0.0010 mg/L Chloroform 0.00080 U 0.0010 mg/L Tetrachloroethene 0.00076 U 0.0010 mg/L Trichloroethene 0.00089 U 0.0010 mg/L Vinyl chloride 0.00071 U 0.0010 mg/L Spike Source a/oREC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 0.054 m91L 0.0500 108 41-142 Dibromofluoromethane 0.057 m91L 0.0500 114 53-146 Toluene-d8 0.053 m91L 0.0500 107 41-146 Blank (OG01040-BLK2) Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 23:31 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.094 UD 0.10 mg/L 1,2-Dichloroethane 0.063 UD 0.10 mg/L 2-Butanone 0.45 UD 0.50 mg/L Benzene 0.071 UD 0.10 mg/L Carbon Tetrachloride 0.094 UD 0.10 mg/L Chlorobenzene 0.072 UD 0.10 mg/L Chloroform 0.080 UD 0.10 mg/L Tetrachloroethene 0.076 UD 0.10 mg/L Trichloroethene 0.089 UD 0.10 mg/L Vinyl chloride 0.071 UD 0.10 mg/L 4-Bromofluorobenzene 0.054 m91L 0.0500 108 41-142 Dibromofluoromethane 0.054 m91L 0.0500 109 53-146 Toluene-d8 0.056 m91L 0.0500 113 41-146 LCS (OG01040-BSI) Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 21:26 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 0.0080 0.0010 mg/L 0.0100 80 47-139 Benzene 0.0096 0.0010 mg/L 0.0100 96 56-136 Chlorobenzene 0.010 0.0010 mg/L 0.0100 100 51-139 Trichloroethene 0.0092 0.0010 mg/L 0.0100 92 62-135 4-Bromofluorobenzene 0.055 m91L 0.0500 111 41-142 Dibromofluoromethane 0.056 m91L 0.0500 113 53-146 Toluene-d8 0.055 m91L 0.0500 111 41-146 Matrix Spike (OG01040-MSI) Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 21:57 Source: CD07944-01 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 1.8 0.10 mg/L 2.00 0.094 U 91 47-139 Benzene 2.1 0.10 mg/L 2.00 0.071 U 103 56-136 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Volatile Organics by GCMS - Quality Control Batch 0GO1O4O - EPA 5030E MS - Continued Matrix Spike (OG03040-MS3) Continued Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 21:57 Source: CD07944-01 Spike Source a/o RE RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Chlorobenzene 2.1 0.10 mg/L 2.00 0.072 U 104 51-139 Trichloroethene 2.1 0.10 mg/L 2.00 0.089 U 103 62-135 4-Bromofluorobenzene 5.4 m91L 5.00 109 41-142 Dibromofluoromethane 5.5 m91L 5.00 110 53-146 Toluene-d8 5.4 m91L 5.00 108 41-146 Matrix Spike Dup (OG01040-MSDI) Prepared: 07/O1/2020 13:17 Analyzed: 07/O1/2020 22:28 Source: CD07944-01 Spike Source %REC RPD Anala Result Flag Q Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 1.7 0.10 mg/L 2.00 0.094 U 87 47-139 4 16 Benzene 2.0 0.10 mg/L 2.00 0.071 U 102 56-136 0.8 14 Chlorobenzene 2.2 0.10 mg/L 2.00 0.072 U 112 51-139 7 13 Trichloroethene 2.1 0.10 mg/L 2.00 0.089 U 107 62-135 4 20 4-Bromofluorobenzene 5.7 m91L 5.00 114 41-142 Dibromofluoromethane 5.6 m91L 5.00 112 53-146 Toluene-d8 5.5 m91L 5.00 111 41-146 TCLP Semivolatile Organics by GCMS - Quality Control Batch 0GO1O36 - EPA 351OC MS Blank (OG01036-BLK3) Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 12:49 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.0006 U 0.002 mg/L 2,4,5-Trichlorophenol 0.0008 U 0.002 mg/L 2,4,6-Trichlorophenol 0.001 U 0.002 mg/L 2,4-Dinitrotoluene 0.0006 U 0.002 mg/L 2-Methylphenol 0.0007 U 0.002 mg/L 3 & 4-Methylphenol 0.002 U 0.002 mg/L Hexachlorobenzene 0.0006 U 0.002 mg/L Hexachlorobutadiene 0.0008 U 0.002 mg/L Hexachloroethane 0.0006 U 0.002 mg/L Nitrobenzene 0.0006 U 0.002 mg/L Pentachlorophenol 0.002 U 0.002 mg/L Pyridine 0.0007 U 0.002 mg/L 2,4,6-Tribromophenol 0.037 m91L 0.0500 74 33-145 2-Fluorobiphenyl 0.042 m91L 0.0500 84 32-116 2-Fluorophenol 0.031 m91L 0.0500 63 11-100 Nitrobenzene-d5 0.040 m91L 0.0500 80 24-107 Phenol-d5 0.021 m91L 0.0500 43 10-100 Terphenyl-d14 0.046 m91L 0.0500 92 52-150 Blank (OG01036-BLK2) Prepared: 07/01/2020 13:30 Analyzed: 07/06/2020 13:19 Spike Source %REC RPD Analvte Result Flag Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.003 U 0.01 mg/L 2,4,5-Trichlorophenol 0.004 U 0.01 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Semivolatile Organics by GCMS - Quality Control Batch 0GO1O36 - EPA 351OC MS - Continued Blank (OG01036-BLK2) Continued Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 13:19 Anala Result Flaa Q Units 2,4,6-Trichlorophenol 0.006 U 0.01 mg/L 2,4-Dinitrotoluene 0.003 U 0.01 mg/L 2-Methylphenol 0.004 U 0.01 mg/L 3 & 4-Methylphenol 0.008 U 0.01 mg/L Hexachlorobenzene 0.003 U 0.01 mg/L Hexachlorobutadiene 0.004 U 0.01 mg/L Hexachloroethane 0.003 U 0.01 mg/L Nitrobenzene 0.003 U 0.01 mg/L Pentachlorophenol 0.008 U 0.01 mg/L Pyridine 0.004 U 0.01 mg/L Spike Source a/o REC RPD Level Result %REC Limits RPD Limit Notes 2,4,6-Tribromophenol 0.14 m91L 0.250 54 33-145 2-Fluorobiphenyl 0.13 m91L 0.250 51 32-116 2-Fluorophenol 0.098 m91L 0.250 39 11-100 Nitrobenzene-d5 0.12 m91L 0.250 47 24-107 Phenol-d5 0.069 m91L 0.250 28 10-100 Terphenyl-d14 0.24 m91L 0.250 97 52-150 Blank (OG01036-BLK3) Prepared: 07/02/2020 10:30 Analyzed: 07/06/2020 13:49 Analvte Result Flao Q Units 1,4-Dichlorobenzene 0.0006 U 0.002 mg/L 2,4,5-Trichlorophenol 0.0008 U 0.002 mg/L 2,4,6-Trichlorophenol 0.001 U 0.002 mg/L 2,4-Dinitrotoluene 0.0006 U 0.002 mg/L 2-Methylphenol 0.0007 U 0.002 mg/L 3 & 4-Methylphenol 0.002 U 0.002 mg/L Hexachlorobenzene 0.0006 U 0.002 mg/L Hexachlorobutadiene 0.0008 U 0.002 mg/L Hexachloroethane 0.0006 U 0.002 mg/L Nitrobenzene 0.0006 Ll 0.002 mg/L Pentachlorophenol 0.002 U 0.002 mg/L Pyridine 0.0007 U 0.002 mg/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 2,4,6-Tribromophenol 0.041 m91L 0.0500 82 33-145 2-Fluorobiphenyl 0.046 m91L 0.0500 93 32-116 2-Fluorophenol 0.035 m91L 0.0500 70 11-100 Nitrobenzene-d5 0.046 m91L 0.0500 91 24-107 Phenol-d5 0.025 m91L 0.0500 50 10-100 Terphenyl-d14 0.051 m91L 0.0500 102 52-150 LCS (OG03036-BSI) Prepared: 07/01/2020 13:30 Analyzed: 07/06/2020 14:19 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.04 0.002 mg/L 0.0500 76 10-101 Pentachlorophenol 0.03 0.002 mg/L 0.0500 50 5-139 2,4,6-Tribromophenol 0.035 m91L 0.0500 70 33-145 2-Fluorobiphenyl 0.043 m91L 0.0500 86 32-116 2-Fluorophenol 0.031 m91L 0.0500 62 11-100 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Semivolatile Organics by GCMS - Quality Control Batch 0GO1O36 - EPA 351OC MS - Continued LCS (OG01036-BSI) Continued Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 14:19 Spike Source a/o RE RPD Anal a Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Nitrobenzene-d5 0.038 m91L 0.0500 75 24-107 Phenol-d5 0.024 m91L 0.0500 48 10-100 Terphenyl-d14 0.039 m91L 0.0500 78 52-150 Matrix Spike (OG03036-MS1) Prepared: 07/01/2020 13:30 Analyzed: 07/06/2020 14:50 Source: AD04219-01 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.19 D 0.05 mg/L 0.250 0.02 U 76 10-101 Pentachlorophenol 0.06 D 0.05 mg/L 0.250 0.04 U 25 5-139 2,4,6-Tribromophenol 0.14 m91L 0.250 58 33-145 2-Fluorobiphenyl 0.21 m91L 0.250 84 32-116 2-Fluorophenol 0.14 m91L 0.250 55 11-100 Nitrobenzene-d5 0.17 m91L 0.250 68 24-107 Phenol-d5 0.10 m91L 0.250 42 10-100 Terphenyl-d14 0.20 m91L 0.250 81 52-150 Matrix Spike Dup (OG01036-MSDI) Prepared: 07/O1/2020 13:30 Analyzed: 07/06/2020 15:20 Source: AD04219-01 Spike Source %REC RPD Analvte Result Flao POLL Units Level Result %REC Limits RPD Limit Notes 1,4-Dichlorobenzene 0.22 D 0.05 mg/L 0.250 0.02 U 87 10-101 13 18 Pentachlorophenol 0.07 D 0.05 mg/L 0.250 0.04 U 26 5-139 5 23 2,4,6-Tribromophenol 0.15 m91L 0.250 60 33-145 2-Fluorobiphenyl 0.23 m91L 0.250 91 32-116 2-Fluorophenol 0.15 m91L 0.250 61 11-100 Nitrobenzene-d5 0.19 m91L 0.250 74 24-107 Phenol-d5 0.11 m91L 0.250 45 10-100 Terphenyl-d14 0.20 m91L 0.250 82 52-150 TCLP Pesticides by GC - Quality Control Batch 0GO1O25 - EPA 351OC Blank (OG01025-BLKI) Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 11:22 Anala Result Flao POLL Units Chlordane (tech) 0.000072 U 0.00010 mg/L Endrin 2.8E-6 U 0.000010 mg/L gamma-BHC 4.2E-6 U 0.000010 mg/L Heptachlor 5.2E-6 U 0.000010 mg/L Heptachlor epoxide 3.6E-6 U 0.000010 mg/L Methoxychlor 4.0E-6 U 0.000010 mg/L Toxaphene 0.000096 U 0.00010 mg/L 2,4,5,E-TCMX Decachlorobiphenyl Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 0.00066 m91L 0.00100 0.00070 m91L 0.00100 66 38-142 70 34-159 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Pesticides by GC - Quality Control Batch 0GO1025 - EPA 3510C - Continued Blank (OG01025-BLK2) Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 11:35 Spike Source a/oREC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Chlordane (tech) 0.00036 U 0.00050 mg/L Endrin 0.000014 U 0.000050 mg/L gamma-BHC 0.000021 U 0.000050 mg/L Heptachlor 0.000026 U 0.000050 mg/L Heptachlor epoxide 0.000018 U 0.000050 mg/L Methoxychlor 0.000020 U 0.000050 mg/L Toxaphene 0.00048 U 0.00050 mg/L 2,4,5,E-TCMX 0.0034 m91L 0.00500 67 38-142 Decachlorobiphenyl 0.0034 m91L 0.00500 69 34-159 Blank (OG01025-BLK3) Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 11:48 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Chlordane (tech) 0.00036 U 0.00050 mg/L Endrin 0.000014 U 0.000050 mg/L gamma-BHC 0.000021 U 0.000050 mg/L Heptachlor 0.000026 U 0.000050 mg/L Heptachlor epoxide 0.000018 U 0.000050 mg/L Methoxychlor 0.000020 U 0.000050 mg/L Toxaphene 0.00048 U 0.00050 mg/L 2,4,5,E-TCMX 0.0038 m91L 0.00500 76 38-142 Decachlorobiphenyl 0.0025 m91L 0.00500 50 34-159 Blank (OG01025-BLK4) Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 12:00 Spike Source %REC RPD Anala Result Flao Q Units Level Result %REC Limits RPD Limit Notes Chlordane (tech) 0.00036 U 0.00050 mg/L Endrin 0.000014 U 0.000050 mg/L gamma-BHC 0.000021 U 0.000050 mg/L Heptachlor 0.000026 U 0.000050 mg/L Heptachlor epoxide 0.000018 U 0.000050 mg/L Methoxychlor 0.000020 U 0.000050 mg/L Toxaphene 0.00048 U 0.00050 mg/L 2,4,5,E-TCMX 0.0038 m91L 0.00500 77 38-142 Decachlorobiphenyl 0.0027 m91L 0.00500 54 34-159 Blank (OG01025-BLKS) Prepared: 07/02/2020 09:30 Analyzed: 07/07/2020 12:12 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Chlordane (tech) 0.000072 U 0.00010 mg/L Endrin 2.8E-6 U 0.000010 mg/L gamma-BHC 4.2E-6 U 0.000010 mg/L Heptachlor 5.2E-6 U 0.000010 mg/L Heptachlor epoxide 3.6E-6 U 0.000010 mg/L Methoxychlor 4.0E-6 U 0.000010 mg/L Toxaphene 0.000096 U 0.00010 mg/L 2,4,5,E-TCMX 0.00075 m91L 0.00100 75 38-142 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Pesticides by GC - Quality Control Batch 0GO1025 - EPA 3510C - Continued Blank (OG01025-BLKS) Continued Prepared: 07/02/2020 09:30 Analyzed: 07/07/2020 12:12 Spike Source a/o RE RPD Anal a Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Decachlorobiphenyl 0.00054 m91L 0.00100 54 34-159 LCS (OG03025-BSI) Prepared: 07/01/2020 11:20 Analyzed: 07/07/2020 12:25 Spike Source %REC RPD Analvte Result FFF`lao Q Units Level Result %REC Limits RPD Limit Notes Endrin 0.00089 0.000010 mg/L 0.00100 89 28-143 2,4,5,E-TCMX 0.00076 m91L 0.00100 76 38-142 Decachlorobiphenyl 0.00083 m91L 0.00100 83 34-159 Matrix Spike (OG01025-MS3) Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 12:37 Source: AD03718-02 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes Endrin 0.0014 0.000010 mg/L 0.00100 2.8E-6 U 135 28-143 2,4,5,E-TCMX 0.00095 m91L 0.00100 95 38-142 Decachlorobiphenyl 0.0010 m91L 0.00100 103 34-159 Matrix Spike Dup (OG03025-MSDI) Prepared: 07/O1/2020 11:20 Analyzed: 07/07/2020 12:49 Source: AD03718-02 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Endrin 0.0011 0.000010 mg/L 0.00100 2.8E-6 U 111 28-143 20 22 2,4,5,E-TCMX 0.00077 m91L 0.00100 77 38-142 Decachlorobiphenyl 0.00088 m91L 0.00100 88 34-159 TCLP Herbicides by GC - Quality Control Batch 0GO2006 - EPA 3510C Blank (OG02006-BLKI) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 16:27 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.000088 U 0.00010 mg/L 2,4-D 0.000054 U 0.00010 mg/L 2,4-DC4A 0.0017 m91L 0.00200 87 37-134 Blank (OG02006-BLK2) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 16:52 Spike Source %REC RPD Analvte Result FFF`lao Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.00044 U 0.00050 mg/L 2,4-D 0.00027 U 0.00050 mg/L 2,4-DC4A 0.0072 m91L 0.0100 72 37-134 Blank (OG02006-BLK3) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 17:17 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.00044 U 0.00050 mg/L 2,4-D 0.00027 U 0.00050 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Herbicides by GC - Quality Control Batch 0GO2006 - EPA 3510C - Continued Blank (OG02006-BLK3) Continued Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 17:17 Spike Source a/o RE RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 2,4-DC4A 0.0066 m9/L 0.0100 66 37-134 Blank (OG02006-BLK4) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 17:42 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.00044 U 0.00050 mg/L 2,4-D 0.00027 U 0.00050 mg/L 2,4-DC4A 0.0086 m9/L 0.0100 86 37-134 LCS (OG02006-BSI) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 18:07 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.0024 0.00010 mg/L 0.00200 122 24-135 2,4-D 0.0022 P 0.00010 mg/L 0.00200 111 20-134 2,4-DC4A 0.0018 m9/L 0.00200 88 37-134 Matrix Spike (OG02006-MS3) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 18:32 Source: AD04272-03 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.0022 0.00010 mg/L 0.00200 0.000088 U 108 24-135 2,4-D 0.0022 P 0.00010 mg/L 0.00200 0.000054 U 108 20-134 2,4-DC4A 0.0018 m9/L 0.00200 88 37-134 Matrix Spike (OG02006-MS2) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 19:48 Source: AD04158-01 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes 2,4,5-TP (Silvex) 0.0096 0.00050 mg/L 0.0100 0.00044 U 97 24-135 2,4-D 0.0084 0.00050 mg/L 0.0100 0.00027 U 84 20-134 2,4-DC4A 0.0078 m9/L 0.0100 78 37-134 Matrix Spike Dup (OG02006-MSD3) Prepared: 07/02/2020 09:00 Analyzed: 07/07/2020 18:57 Source: AD04272-03 Analvte 2,4,5-TP (Silvex) 2,4-D Result Flao 2 0.0021 0.00010 0.0018 P 0.00010 Units mg/L mg/L Spike Level 0.00200 0.00200 Source Result 0.000088 U 0.000054 U %REC 104 88 %REC Limits RPD 24-135 5 20-134 20 RPD Limit Notes 19 19 QM-11 2,4-DC4A 0.0017 m9/L 0.00200 83 37-134 TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 0GO1019 - EPA 7470A Blank (OG01019-BLKI) Prepared: 07/O1/2020 12:07 Analyzed: 07/02/2020 09:42 Anale Mercury Spike Source %REC RPD Result Flaa Q Units Level Result %REC Limits RPD Limit 2.30E-5 U 0.000200 mg/L Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 23 (� �Eo www.encolabs.com QUALITY CONTROL DATA TCLP Metals by 6000/7000 Series Methods - Quality Control Batch 0GO1019 - EPA 7470A - Continued Blank (OG01019-BLK2) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 09:45 Spike Source a/oREC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.000230 U 0.00200 mg/L Blank (OG01019-BLK3) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 09:48 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.000230 U 0.00200 mg/L LCS (OG01019-BSI) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 09:57 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.00536 0.000200 mg/L 0.00500 107 80-120 Matrix Spike (OG01019-MSI) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 10:03 Source: AD04219-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.0537 0.00200 mg/L 0.0500 0.000230 U 107 75-125 Matrix Spike Dup (OG01019-MSDI) Prepared: 07/01/2020 12:07 Analyzed: 07/02/2020 10:07 Source: AD04219-01 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes Mercury 0.0553 0.00200 mg/L 0.0500 0.000230 U 111 75-125 3 20 Classical Chemistry Parameters - Quality Control Batch 0GO7010 - NO PREP Blank (OG07010-BLKI) Prepared: 07/07/2020 08:30 Analyzed: 07/07/2020 16:00 Spike Source %REC RPD Analvte Result Flao Q Units Level Result %REC Limits RPD Limit Notes Reactive Cyanide 250 U 250 mg/L LCS (OG07010-BSI) Prepared: 07/07/2020 10:45 Analyzed: 07/07/2020 16:00 Spike Source %REC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Reactive Cyanide 47 UD 6200 mg/L 99.9 47 22-100 Duplicate (OG07010-DUPI) Prepared: 07/07/2020 09:15 Analyzed: 07/07/2020 16:00 Source: CD07944-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Reactive Cyanide 250 U 250 mg/L 250 U 30 Batch 0GO8018 - NO PREP Blank (OG08018-BLKI) Prepared: 07/07/2020 08:30 Analyzed: 07/07/2020 17:00 Spike Source %REC RPD Analvte Result FFF`lau Q Units Level Result %REC Limits RPD Limit Notes Reactive Sulfide 500 U 500 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 23 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 0GO8018 - NO PREP - Continued (� �Eo www.encolabs.com LCS (01308018-13SI) Prepared: 07/07/2020 10:45 Analyzed: 07/07/2020 17:00 Spike Source a/oREC RPD Anala Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Reactive Sulfide 210 U 500 mg/L 249 84 50-150 Duplicate (01308018-DUPI) Prepared: 07/07/2020 09:15 Analyzed: 07/07/2020 17:00 Source: CD07944-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Reactive Sulfide 500 U 500 mg/L 500 U 30 Classical Chemistry Parameters - Quality Control Batch 0GO2008 - NO PREP Duplicate (OG02008-DUP3) Prepared: 07/02/2020 15:00 Analyzed: 07/02/2020 16:10 Source: CD07944-01 Spike Source %REC RPD Analvte Result Flaa Q Units Level Result %REC Limits RPD Limit Notes Flashpoint > 200 U OF > 200 5 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 23 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. J-01 Result may be biased high due to positive results in the associated method blank at a concentration above the MDL and/or greater than one-half the MRL. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-08 Post -digestion spike did not meet method requirements due to confirmed matrix effects (dilution test). QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 23 14 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com ri �� 10775 Central Pori Dr. 4810 Executive Park Court, Suite 111 102-A Woodwmds !ndusrrial Ct. CCE Nk"Orlando, F432824 Jacksonville, FL 32216-6069 Cary- NC 27511 (407) 826-6314 (9W) 296-3007 Fax (904) 296-6210 9193 .r67.3090 Fax (919j 467-3515 Page Of Client Name Project Number Requested Analyses Requested Turnaround Hunt Environmental Associates HU017) Finmel z < Times Address PTo)ect Name[Desc Q r j Note : Rush requests subject tb 3330 Saddletree Road. Ci of Lumberton �m m > co� acceptance by the Facil{Sy City/STMp PO #! Billing Info U Lumberton, NC 28360 T X ~ ��, Standard Tel Fax Reporting Contact$ I� l 0 $ d Ci. U) (9'10) 738-5311 Jordan Davis �� a � � � U c� �rA " o m _ Expedited 5 mpler(s) Name, Affiliation (Print) Biling Contact - a a (� u Q � � 1 X N Cody Hunt if'A r T- F- m O E � a � x Due / 1 mplerls) Sign Site Location Dime zone jig T- r .- pp ti C t O Lab 1NoTkorder M c7 O N cta La,r r oD CYJ Q 0it IL Z T+Qfj�Q � Preservation (See CodesJ (Combine as necessary) �J 0 �}�} Collection Matrix ToW A of Hem # Sample ID (Fie?d idant)lication) Collection Dale n T!me omp! rab (see codes) Containers Sample Comments WW-1 ') v �1 t WW 10 X X X X X X WW-2 SL 4 X X X < Total # of Containers Sample Kit Prepared By Date ime Rolinqui ad By DateMme Rem d Ry DateMme - UzY1 J, 9 ` 11.E-�awe�,- Comments/Special RepotbKgTlig0roments I R quished By Daternme c ' ed By Da Ime Relinquished By DateRme Received By DatelTime Cooler #'s & Temps on Receipt !3 Cendition Upon Receipt Acceptable Unacceptable Matrix . GW-Groundwa!er SO-Soit 1]W-Drinking Water SE -Sediment SW -Surface Water INW-Waslewater A -Air 0.01her (detail in comments) Preservation: )-Ice H-HCl N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in commentg) Note: All Samples submitted to );NCO Labs are in accordance with the terms and conditions listed on the reverse of this form. unless prior written agreements exist ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.coml CO 13775 Central Port Dr. 4810 Executive Park Court. Suite 111 102-A Woodwinds lndustdal Ct. Orlando, FL 32824 Jacksonville- FL 32216-6060 Cary. NO 27511 (Um(407) 826-5314 (904) 296-3007 Fax (904) 296-6210 (919) 467-3090 Fax (919) 467-3515 Page of Client Name Project Number Requested Analyses Requested Turnaround Hunt Environmental Associates HU017 none Times Address Project Name/Desc Note: Rush requests subject to (L acceplance by the facility 3330 Saddletree Road_ Ci of Lumberton( City/STrZip PC it i Billing talo l ' Lumberton, NC 28360 C F Standard Tel Fax Reporting Contact F d (910) 738-5311 Jordan Davis � �a _ Expedited RV Sampler(s) Name, Affiliation (Print) Billing Contact - C'V d F (� G�I('i Cody Hunt a ta 4 Due / 1 samplers) signature Site Location / Time Zane , d J Lab Workorcier U d" U C ❑07 {] /t /( Preservation (See Codes) (Combine as necessary) �J �+�{� � Collection Matrix Total # of Item # Sample ID (Field identification) Collection Date jj-F�t amp / Grai] (see codes) Containers Sample Comments WW-1 2 `1� WW 10 X X X WW-2 St_ A c Total # of Containers Sample Kit Prepared By Oates imle /J Relin ished By i Dateir7i fm�e 7� Recei d By Dat Commentsispecia-Mepordfig Requirements quished By Datefrime Re ed By flat ime 'jiRelinquished By Daterrime Received By Daiemme Cooler #'a & Temps on Receipt Condition Upon Receipt [, -A Acceptable Unacceptable Matrix : GW-Groundwater SO -Sail DIN -Drinking Water SE -Sediment SW -Surface Water WW-Waslewater A -Air O-Other (detail in comments) Preservation: t-Ice H-HCi N-HNO3 S-H2SO4 NO-NaOH O-Other (detail in comments) Note : All samples submitted to ENCO labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist Cameron Testing Services, Inc. Laboratory Report Client; Enviro- hoice Recycling CTS Pro], Project: City of Lumberton Requiatory Sample Information sampled Date 0612 + Q Receiv4ct Analyses and Results 00-'I 0 M. S:ms Lab ID Saillple I - E {A y = m r �o 0 Analyte Result J ro e O NC DEN #654 NC PHHS #3779� US EPA #NCol 918 pato 06123120 .: Std. Moth ods Reference 2006-21 0 - _1,d;c a Fac. Coliforrn,S <46700 crUeg 46700 06f24!20 RL 92220 - NI - �399 CFU9 46600 <46800 cFU+,j 46800 -4 46600 CFW9 46600 -5 <46500 CFU19 +46500 0 <48700 CFwo 4VO -7 <461DOO ORNg 46900 Geomean 54600 2006- 10 -1 31vd¢t Gr TS {561 2.14% D.DT DFW24120 RL 2540 G -T -2 2.14% n.oi -3 2.14% 0.01 -4 .15% 0.01 -5 2.15% o.oi 0 _14 % a.m Report PeifiE'YV - 9�- 4� ProjectNlanager --6s 219 S. Steele Sir. Sanford NC 27330 919-208-424,a eh r is ray o amrnon r es to ng _ c Dora 219 S_ Sleaze Str. Sanhad. NC 27330 Phone - 919-208-4240 Cameron Testing Services, inc_ NC Wb`1 GVd CPr1 0654 NC PHHS Cart 4 �7799 US EPA NC019Ta Chain of Custody Page of 05mpany Contact, Address {Clip, State_ Zip} Proyect yy V'z T E,nall: A5 Phow Fig: , � Noles: TO�} i i C l C1 #i1 .� "A- P ( ` i sarrCT lab use — — +Ple Temp Pro). !b ice (YIN� . Perma (YM) Rush (M) Dare Sample Marna; C ❑I IKiow Signature Sample Information Number of bottles * preservative Required TestinglAnalysis t1l1@Llt Sample S M DR a c7 a � � O m > O Preservatives ;l}npresery H(C}I. H2{SK 4, H(N}03, (Na)TNosulfata, WOK (P1kw twnrec, 00w M, lrxjkmi•. CT Sample ID _ 12b �1 f � _F I Y I ' Fe \ 4-� I - 1 L I uished. DatofTii_me yReli. {j} / Check -in Rush work will esquire PhOr approval Addillonal charges YAII apply City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 7/15/2020 7:03am TES Dig# 2 Day 1 Total Solids Sample volume used for total solids test: 5 mL Weight of dish: tl9:3.0:652 .9 008 g Weight of dish + dried solids: g Weight of dried solids: .1044 g Total Solids: 20.88 g/L SOUR Time (Minutes) Temperature oC Dissolved Oxygen (mg/L) 0 24.00 3.30 1 24.00 2 24.00 1.20 3 24.00 0.89 4 24.00 -- 0.61 -- 5 24.00 0.53 6 24.00 _ _ 0.48 7 24.00 _ 0.42 8 24.00 0.38 9 24.00 0.34 10 24.00 0.31 11 24.00 0.30 12 24.00 0.28 13 24.00 0.28 14 15 24.00 24.00 _ 0.27 0.27 Oxygen Consumption Rate SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 24 If sewage sludge is > 20°C, SOUR = If sewage sludge is < 20°C, SOUR = 0.12 mg/L/minute 0.34 (mg/g)/hr J 0.26 (mg/g)/hr (mg/g)/hr SOUR passes if result is < 1.5 (mg/g)hr Version 11/1/11 City of Lumberton Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 7/16/2020 7:50am T�S Dig# 2 Day 2 Total Solids Sample volume used for total solids test: Weight of dish: Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR 1.2455 5 12 121.3447 0.0988 19.76 Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 24.00 3.79 1 2 24.00 24.00 _ 1.64 1.35 3 24.00 1.20 4 5 24.00 24.00 1.16 1.06 6 _ 24.00 _ 1.01 7 24.00 6.96 8 24.00 0.80 9 24.00 0.71 10 24.00 0.66 11 24.00 0.63 12 24.00 0.47 13 24.00 0.36 14 24.00 0.30 15 24.00 0.27 Oxygen Consumption Rate SOUR SOUR Temperature Correction mL 9 9 9 g/L 0.14 mg/L/minute 0.42 (mg/g)/hr I Average Sewage Sludge Temperature During Test °C 24 If sewage sludge is > 20°C, SOUR = 0.35 (mg/g)/hr If sewage sludge is < 20°C, SOUR = I _ (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr Version 11/1/11 City of Lumbe on Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 7/17/2020 6:18am T11, S Dig# 2 Day 3 Total Solids Sample volume used for total solids test: Weight of dish. - Weight of dish + dried solids: Weight of dried solids: Total Solids: SOUR 5 F 558558 000 20 Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 24.00 1 1 24.00 _6.70 5.20 2 _ 24.00 3.66 3 24.00 _ 1.82 4 24.00 �0.70 5 24.00 0.51 6 24.00 7 24.00 0.39 8 24.00 0.37 9 24.00 0.35 10 24.00 0.33 11 24.00 _ 0.31 12 24.00 0.30 13 24.00 0.29 14 24.00 0.27 15 24.00 ----^ 0.27 Oxygen Consumption Rate SOUR SOUR Temperature Correction mL 9 9 9 g/L 0.32 mg/L/minute 0.95 (mg/g)/hr Average Sewage Sludge i Temperature During Test oC 24 If sewage sludge is > 20°C, SOUR = (mg/g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is <_ 1.5 (mg/g)hr Version 11/1/11 City of Lumber on Environmental Lab ratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 7/20/2020 5:39am kcl Dig# 2 Day 4 Total Solids Sample volume used for total solids test: 5 mL Weight of dish: _ 121.2458 g Weight of dish + dried solids: 121._33_86 g Weight of dried solids: 0.0928 g Total Solids: 18.56 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) oC 0 25.00 1 _ 25.00 _5.20 2.96 2 25.00 1.74 3 25.00 0.93 4 25.00 0.71 5 25.00 ­ 0.68 _ 6 25.00 0.44 7 25.00 0.40 j 8 25.00 0.37 -- 9 25.00 _ 0.36 10 25.00 0.35 11 25.00 0.34 12 26.00 0.33 13 1 26.00 0.33 14 25.00 0.32 15 _ !, 25_00 _ 0.32 _ Oxygen Consumption Rate SOUR SOUR Temperature Correction 10.20 rTig/L/minute 0.63 (mg/g)/hr Average Sewage Sludge Temperature During Test oC 25.125 If sewage sludge is > 20°C, SOUR =ion (mg/g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is < 1.5 (mg/g)hr Version 11/1/11 City of Lumberlon Environmental Lab ratory Specific Oxygen Uptake Rate (SOOR) Worksh Date & Analyst: 7/2112020 6:01am kicI Dig# 2 Day 5 Total Solids Sample volume used for total solids test: Weight of dish: Weight of dish + dried solids: Weight of dried solids: Total Solids: mL 9 9 9 g/L SOUR 5 123.1048 123.1981 0.0933 18.66 Time (Minutes) TeW_D,Dissolved Oxygen (mg/L) 0 6.20 1 _ 5.10 _ 2 -_— 3.723 2.504 1.415 0.626 0.457 V 0.39 8 25.00 0.36 9 25.00 __ 0.34 10 25.00 _ 0.33 11 25.00 _ 0.32 12 25.00 _ 0.32 13 25.00 0.31 14 __ 25.00 0.31 15 25.00 0.31 Oxygen Consumption Rate 0.32 mg/L/minute SOUR 1.03 (mg/g)/hr SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 25 If sewage sludge is > 20°C, SOUR = _ o.ao (mg/g)/hr If sewage sludge is < 20°C, SOUR = (mg/g)/hr SOUR passes if result is S 1.5 (mg/g)hr Version 11/1/11 City of Lumbert n Environmental Laboratory Specific Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 7/22/2020 5:43am kcl Dig# 2 Day 6 Total Solids Sample volume used for total solids test: 5 mL Weight of dish: 125.4574 g Weight of dish + dried solids: 125.5489,g Weight of dried solids: 0.0915 g Total Solids: 18.3 g/L SOUR Time (Minutes) Temperature Dissolved Oxygen (mg/L) aC 0 _ 24.00 6.11 1 25.00 5.11 2 _ 25.00 3.87 3 25.00 3.82 4 _ 25.00 3.36 5 25.00 3.07 6 25.00 2-�71 7 _ 25.00 2.56 8 25.00 2.11 i 5.00 5.00 5.00 5.00 Oxygen Consumption Rate 0.36 mg/L/minute SOUR 11.17 (mg/g)/hr SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 24.9375 If sewage sludge is > 20°C, SOUR = 0.92 (mg/g)/hr If sewage sludge is < 20°C, SOUR = 0.84 (mg/g)/hr SOUR passes if result is S 1.5 (mg/g)hr Version 11/1/11 City of Lumbert n Environmental Laboratory SpeclfiC Oxygen Uptake Rate (SOUR) Worksheet Date & Analyst: 7/23/2020 5:48arn kc! Dig# 2 Day 7 Total Solids "j-1;2� mL Sample volume used for total solids test:g Weight of dish: g Weight of dish + dried solids: g Weight of dried solids: g/L Total Solids: SOUR Oxygen Consumption Rate 0.20 SOUR SOUR Temperature Correction Average Sewage Sludge Temperature During Test °C 25.125 If sewage sludge is > 20°C, SOUR = If sewage sludge is < 20°C, SOUR = Version 11/1/11 1 •: mg/L/minute (mg/g)/hr (mg/g)/hr L� - 0.48 -- (mg/g)/hr SOUR passes if result is 5 1.5 (mg/g)hr Attachment H: Existing Permit s�;'•a Wa ter R esources ENVIRONMENTAL QUALITY April 27, 2017 WAYNE HORNE - CITY MANAGER CITY OF LUMBERTON POST OFFICE BOX 1388 LumBERToN, NORTH CAROLINA 28359 Dear Mr. Horne: ROY COOPER Governor MICHAEL S. REGAN Secretary S. JAY ZIMMERMAN Director Subject: Permit No. WQ0000672 City of Lumberton RLAP Land Application of Class B. Residuals Robeson County In accordance with your permit major modification and renewal request received February 6, 2017, and subsequent additional information received March 30, 2017, we are forwarding herewith Permit No. WQ0000672 dated April 27, 2017, to the City of Lumberton for the continued operation of the subject residuals management program. Modifications to the subject permit are as follows: 1. Removal of Lumberton WTP as a residuals source with a reduction of 400 tons/year. 2. Removal of 40 fields in Robeson County totaling 862.4 acres, those fields being: NC-RO-16- 20, NC-RO-21, NC-RO-19-01, NC-RO-19-05, NC-RO-19-08, NC-RO-19-09, NC-RO-19-10, NC-RO-19-11, NC-RO-19-12, NC-RO-19-13A, NC-RO-19-13B, NC-RO-19-15, NC-RO-19- 20, NC-RO-19-21, NC-RO-19-22, NC-RO-19-23, NC-RO-19-23, NC-RO-19-25, NC-RO-19- 29, NC-RO-19-30, NC-RO-19-34, NC-RO-19-35, NC-RO-19-36, NC-RO-19-37, NC-RO-19- 38, NC-RO-20-05, NC-RO-22-01, NC-RO-22-02, NC-RO-22-03, NC-RO-27-01, NC-RO-27- 02, NC-RO-27-06, NC-RO-27-07, NC-RO-37-01, NC-RO-37-02, NC-RO-37-03, NC-RO-37- 04, NC-RO-37-05, NC-RO-37-06, NC-RO-38-01 and NC-RO-38-02. This permit shall be effective from the date of issuance until March 31, 2022, shall void Permit No. WQ0000672 issued May 12, 2008, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachment A for they may differ from the previous permit issuance. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. -7.-Nothing Compares f State of North Carolina' Environmental Quality I Water Resources I Water Quality Permitting { Non -Discharge Penmitting 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919-807-6332 Mr. Wayne Horne April 27, 2017 Page 2 of 3 Please note the following permit conditions have been removed since the last permit issuance dated May 12, 2008: ➢ Old Condition 111.4. — There is no need to void the permit since other land can be found. ➢ Old Condition I11.7. — Redundant since covered by Old Condition I1I.6. and Condition I1I.9. ➢ Old Condition III.11.h. — Redundant since covered by agronomic rate requirements of Conditions 11.11.k. ➢ Old Condition IV.9. — Length of time for record keeping is specified in individual condition. Please note the following permit conditions are new since the last permit issuance dated May 12, 2008: ➢ Condition I.2. — Permittee to be in compliance within 90 days of new permit date of notification requirements of Condition IH.3. ➢ Condition 1.3. — Permittee to be in compliance within 180 days of new permit date of signage requirements of Condition 111.13. ➢ Condition It.12. — When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by 25%. ➢ Condition IH.3. — Mooresville Regional Office to be notified at least 24 hours prior to land application of residuals. ➢ Condition IIIA. — Operation & Maintenance Plan required. ➢ Condition 111.6. — Similar to Old Condition II1.5., but now a copy of the O&M plan also required, Please note that "copy" can include an electronic copy on a device. ➢ Condition M.11.1. — Bulk residuals are not to be applied above agronomic rates. ➢ Condition III.13. — Signage requirements provided. ➢ Condition iV.7.d., g., j. — Similar to Old Condition IV.8., but now records to be kept include approximate area (acres), predominant soil mapping, and nitrogen application rate. ➢ Condition VI.6. — Similar to Old Condition VI.6., but now 60-day notice required before modification or revocation. ➢ Condition VI.7. — Expansion of facility not permitted without waiver if Permittee has exhibited behavior detrimental to environment. If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding. Mr. Wayne Horne April 27, 2017 Page 3 of 3 If you need additional information concerning this permit, please contact Troy Doby at (919) 807- 6336 or troy.dobygncdenr. og_v. Sincerely, ;44e'06-�- -2> d'� Jay Zimmerman, P.G., Director Division of Water Resources cc: Robeson County Health Department (Electronic Copy) Fayetteville Regional Office, Water Quality Regional Operations Section (Electronic Copy) Chad Hayes - Synagro (Electronic Copy) Beth Buffington -- Protection and Enforcement Branch (Electronic Copy) Digital Permit Archive (Electronic Copy) Central Files THIS PAGE BLANK NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENTAL QUALITY RALEIGH LAND APPLICATION OF CLASS B RESIDUALS PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO City of Lumberton Robeson County FOR THE continued operation of a residuals management program for the City of Lumberton and consisting of the land application of Class B residuals generated by the approved facility listed in Attachment A to the approved fields listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application received February 6, 2017, and subsequent additional information received by the Division of Water Resources, and in conformity with other supporting data subsequently filed and approved by the Department of Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from the date of issuance until March 31, 2022, shall void Permit No. WQ0000672 issued May 12, 2008, and shall be subject to the following specified conditions and limitations: I. SCHEDULES No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0I05(d) requires an updated site map to be submitted with the permit renewal application. [15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109] 2. The Permittee shall be in full compliance with the regional office notification requirements established in Condition III.3. within 90 days of the effective date of this permit. [ 15A NCAC 02T .0108(b)(2)] 3. The Permittee shall be in full compliance with the signage requirements established in Condition I11.13. within 180 days of the effective date of this permit. [ 15A NCAC 02T .0108(b)(2)] WQ0000672 Version 4.0 Shell Version 170401 Page 1 of 13 IL PERFORMANCE STANDARDS The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease land applying residuals, contact the Fayetteville Regional Office supervisor, and take any immediate corrective actions. [G.S. 143-215.1] 2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [I 5A NCAC 02B .0200, 02L .0100] 3. Only residuals generated by the facility listed in Attachment A are approved for land application in accordance with this permit. [G.S. 143-215.1] 4. Only the fields listed in Attachment B are approved for residuals land application. [G.S. 143-215.1] 5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs): Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 The Permittee shall determine compliance with the CPLRs using one of the following methods: a. By calculating the existing cumulative level of pollutants using actual analytical data from all historical land application events of residuals, or b. For land where residuals application has not occurred or for which the required data is incomplete, by determining background concentrations through representative soil sampling. [15A NCAC 02T. 11051 6. Residuals that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .11061 7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A) that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1107(a). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1107] WQ0000672 Version 4.0 Shell Version 170401 Page 2 of 13 8. Setbacks for Class B land application sites shall be as follows: Setback by application type (feet) Setback Description Vehicular Irrigation Surface Surface Injection / Application Application Incorporation Habitable residence or place of public assembly under separate ownership or not to be maintained as part of 400 400 200 the project site Habitable residence or places of public assembly owned by the Permittee, the owner of the land, or the 0 200 0 lessee/operator of the land to be maintained as part of the project site Property lines 50 150 50 Public right of way 50 50 50 Private or public water supply 100 100 100 Surface waters (streams — intermittent and perennial, 100 100 50 perennial waterbodies, and wetlands) Surface water diversions (ephemeral streams, 100 25 waterways, ditches)25 Groundwater lowering ditches (where the bottom of 25 100 25 the ditch intersects the SHWT Subsurface groundwater lowering system 0 100 0 Wells with exception to monitoring wells 100 100 100 Bedrock outcrops 25 25 25 Top of slope of embankments or cuts of two feet or 15 15 15 more in vertical height Building foundations or basements 0 15 0 Water lines 0 10 0 Swimming pools 100 100 100 Nitrification fields 0 20 0 [15A NCAC 02T .1108] 9. Land application areas shall be clearly marked on each site prior to and during any residuals application event. [15ANCAC 02T .0108(b)(1)] WQ0000672 Version 4.0 Shell Version 170401 Page 3 of 13 10. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (h ://nutrients.soil.nesu.edu/ ields/index. h ). A copy shall be kept on file and reprinted every five years in accordance with Condition IVA. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 (http://www.ncagUov/SWC/tech/documents/9th Guidance_Doc _100109.pdf). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf1. d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. [15A NCAC 02T .I 109(b)(1)(k)] 11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by 25% in accordance with the USDA-NRCS 590 Nutrient Management Standards. [15A NCAC 02T .0108(b)(1)] 12. If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer and rye grass in the winter with both crops to receive residuals), then the second crop can receive an application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. [ 15A NCAC 02T .0108(b)(1)] 13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the Permittee shall obtain and implement recommendations from at least one of the following: the local Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall maintain written records of these recommendations and details of their implementation. [15A NCAC 02T .0108(b)(1)] WQ0000672 Version 4.0 Shell Version 170401 Page 4 of 13 14. These residuals land application sites were individually permitted on or after December 30, 1983; therefore, the compliance boundary is established at either 250 feet from the residual land application area, or 50 feet within the property boundary, whichever is closest to the residual land application area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to remediation action according to 15A NCAC 02L .0106(d)(2) as well as enforcement actions in accordance with North Carolina General Statute 143-215.6A through 143-215.6C. Any approved relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B. [15A NCAC 02L .0107(a)] 15. The review boundary shall be established midway between the compliance boundary and the residual land application area. Any exceedance of groundwater standards at the review boundary shall require action in accordance with 15A NCAC 02L .0106. [15A NCAC 02L .0108] III. OPERATION AND MAINTENANCE REQUIREMENTS The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. [15A NCAC 02T .1110] 2. The Fayetteville Regional Office, telephone number (910) 433-3300, and the appropriate local government official (i.e., county manager, city manager, or health director) shall be notified at least 48 hours prior to the initial residuals land application to any new land application site. Notification to the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. [15A NCAC 02T .0108(b)(1)] 3. The Fayetteville Regional Office shall be notified via email or telephone, (910) 433-3300, at least 24 hours prior to conducting any land application activity. Such notification shall indicate, at a minimum, the anticipated application times, field IDs, and location of land application activities. If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. [15A NCAC 02T .0108(b)(1)] 4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a. Operational functions; b. Maintenance schedules; c. Safety measures; d. Spill response plan; c. Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to betaken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f. Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; WQ0000672 Version 4.0 Shell Version 170401 Page 5 of 13 iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). [15A NCAC 02T .11001 Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 1SA NCAC 08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition 111.4.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Protection and Enforcement Branch at (919) 707-9105. [ 15A NCAC 02T .0117] 6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. [15A NCAC 02T .0108(b)(1)] 7. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. [15A NCAC 02T .1110] 8. Residuals shall not be stored at any land application site, unless written approval has been requested and received from the Division. f G.S. 143-215.1 ] 9. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. fG.S. 143-215.1] 10. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. f 15A NCAC 02T .1109(b)(1)] WQ0000672 Version 4.0 Shell Version 170401 Page 6 of 13 11. Bulk residuals shall not be land applied under the following conditions; a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; i. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; j. If the vertical separation of bedrock and the depth of residuals application is less than one foot; k. Application exceeds agronomic rates. [15A NCAC 02T .1109] 12. The following public access restrictions apply to residual land application sites: a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted for 365 days after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land application event. [15A NCAC 02T .1109(b)(2)] 13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g., 1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and contact information, including the Permittee or applicator's telephone number. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a land application event, and for as long as the public access restrictions required under Condition III.12. apply. [ 15A NCAC 02T .0108(b)(1)] WQ0000672 Version 4.0 Shell Version I70401 Page 7 of 13 14. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: Harvesting and Grazing Description Restricted Duration Animals shall not be allowed to graze during land application activities and restricted period. Sites that are to be used for grazing shall have fencing to 30 days prevent access after each land application event. Food crops, feed crops and fiber crops shall not be harvested for: 30 days Turf grown on land where residuals have been applied shall not be harvested for: 12 months Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) 14 months shall not be harvested for: When the residuals remain on the land surface for four months or longer prior to incorporation into the soil, food crops with harvested parts below the land 20 months surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for: When the residuals remain on the land surface for less than four months prior to incorporation into the soil, food crops with harvested parts below the land 38 months surface shall not be harvested for: [15A NCAC 02T .1109(b)(3)] 15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that have been applied to the site, and a copy of the most recent Nutrient Management Plan (NUT) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (MRCS) or other State Agencies. The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMW), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. [15A NCAC 02T .0108(b)(1), 02T .1104(c)(3)] 16. No residuals shall be land applied unless the submitted Land Owner Agreement between the Permittee and landowners or lessees/operators of the land application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. [ 15A NCAC 02T .1104(c)(4)] WQ0000672 Version 4.0 Shell Version 170401 Page 8 of 13 IV. MONITORING AND REPORTING REQUIREMENTS 1. Any Division -required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. [ 15A NCAC 02T .0108(c)] 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40 CPR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses). Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1, 1 -Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) 0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichl oro phenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be Iess than once per permit cycle. [I5A NCAC 13A .0102(b), 02T .1101, 02T .1105] WQ0000672 Version 4.0 Shell Version 170401 Page 9 of 13 3. An analysis shall be conducted on residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) [15A NCAC 02T .1101] 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c), and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [15A NCAC 02T .1106, 02T .1107, 02T .1111(c)] An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website (http://www.ncag_r.gov/agronomi/,pubs.httn). The Permittee shall maintain these results and a description of the sampling methodologies used to determine soil fertility for a period of no less than five years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exchangeable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH [15A NCAC 02T .0108(c), 15A NCAC 02T. 1111 (d)] 6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .0505] WQ0000672 Version 4.0 Shell Version 170401 Page 10 of 13 7. The Permiee shall maintain records tracking all residual land application events. At a minimum, these records shall include the following: a. Source of residuals; b. Date of land application; c. Location of land application (i.e., site, field, or zone number as listed in Attachment B); d. Approximate areas applied to (acres); e. Method of land application; f. Weather conditions (e.g., sunny, cloudy, raining, etc.); g. Predominant Soil Mapping Unit (e.g., CbB2); h. Soil conditions (e.g., dry, wet, frozen, etc.); i. Type of crop or crops to be grown on field; j. Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years); k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet ton per acre; 1. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or wet tons per acre; in. Volume of soil amendments (e.g., time, gypsum, etc.) applied in gallons per acre, dry ton per acre, or wet tons per acre; and n. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other sources of nutrients (e.g., if applicable), annual and cumulative pounds per acre of each heavy metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury, molybdenum, nickel, selenium, and zinc), annual pounds per acre of PAN, and annual pounds per acre of phosphorus applied to each field. (15A NCAC 02T .0109(a)] Three copies of an annual report shall be submitted on or before March 1'. The annual report shall meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms. Instructions for reporting and annual report forms are available at http: //deg .ne. gov/about/divisions/water-resources/water-resources-perm its/wastewater-branch/non- discharge-permittin -ug nit/reportin -fg orms, or can be obtained by contacting the Non -Discharge Permitting Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [15A NCAC 02T .1111(a)] WQ0000672 Version 4.0 Shell Version 170401 Page 11 of 13 9. Noncompliance Notification The Permittee shall report by telephone to the Fayetteville Regional Office, telephone number (910) 433-3300, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Land application of residuals abnormal in quantity or characteristic. b. Any failure of the land application program resulting in a release of material to surface waters. c. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(l), 02T .0108(b)(1)] V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)] 2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals processing, storage, transport and application facilities to identify malfunctions, facility deterioration and operator errors that could result in discharges to the environment, a threat to human health or a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)] 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)] VI. GENERAL CONDITIONS Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to 143-215.6C. [G.S. 143-215.6A to 143-215.6C] 2. This permit shall become voidable if the residuals Iand application events are not carried out in accordance with the conditions of this permit. [15A NCAC 02T .0110] 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. [G.S. 143-215.1] WQ0000672 Version 4.0 Shell Version 170401 Page 12 of 13 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A NCAC. 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. [15A NCAC 02T .0105(c)(6)] 5. In the event the residuals program changes ownership or the Permittee changes his name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. [15A NCAC 02T .0104] 6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 02T .0110. [15A NCAC 02T .0110] 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b). [15A NCAC 02T .0120] 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T .01 O5(e)(3)] Permit issued this the 27' day of April 2017 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION --z>. cjz" — S. Jay Zimmerman, P.G., Director Division of Water Resources 0 By Authority of the Environmental Management Commission Permit Number WQ0000672 WQ0000672 Version 4.0 Shell Version 170401 Page 13 of 13 THIS PAGE BLANK ATTACHMENT A - Approved Residual Sources City of Lumberton Certification Date: April 27, 2017 Permit Number: WQ0000672 Version: 4.0 Monitoring Monitoring Monitoring Permit Biological Maximum Frequency far Frequency for Frequency for Approved Owner Facility Name County Number Residuals Dry Tons Non -hazardous Metals and Pathogen & Mineralization per Year I Characteristics 2 Nutrients 3, s Vector Attraction Rate Reductions 4,5 City of Lumberton Lumberton WWTP Robeson NC0024571 Yes 17500 Annually See Table Below See Table Below 0.3 Total 1,500 I . Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. 3. Testing of metals and nutrients as stipulated under permit Condition IV.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IVA. 5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Applied short tons per ear(Established Monitoring Frequency in 40 CFR 503 and 15A NCAC 02T A 111 <319 l/Year —>319 - <1,650 l/ Quarter 4 times per ear =>1,650 - <16,500 1/60 Days 6 times per ear =>16,500 1/month (12 times per ear If no land application events occur during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to make up the missed sampling, contact the EPA for additional information and clarification. WQ0000672 Version 4.0 Attachment A Page 1 of 1 THIS PAGE BLANK ATTACWWENT B - Approved Land Application Sites City of Lumberton Certification Date: April 27, 2017 Permit Number: WQ0000672 Version: 4.0 Field Owner Lessee County Latitude Longitude Net Acreage Dominant Soil Series Footnotes NC-RO-16-01 Baker, Arrin Ozzell Robeson 34.7064920 -79.1275390 16.9 Ra - Rains sandy 1 NC-RO-16-02 Baker, Arrin Ozzell Robeson 34.7037250 -79.127292" 3.6 GoA - Goldsboro 1 NC-RO-16-03 Baker, Arrin Ozzell Robeson 34.7054580 -79.1256780 3.4 GoA - Goldsboro 1 NC-RO-16-04 Baker, Arrin Ozzell Robeson 34.7047250 -79.125203" 3.6 Ra - Rains sandy 1 NC-RO-16-05 Baker, Arrin Ozzell Robeson 34.7067360 -79.1231920 8.7 Ra - Rains sandy I NC-RO-I 6-06 Baker, Arrin Ozzell Robeson 34.7051970 -79.1221220 14.8 NoA - Norfolk I NC-RO-16-07 Baker, Arrin Ozzell Robeson 34.7067170 -79.120431 ° 17.5 NoA - Norfolk 1 NC-RO-16-08 Baker, Arrin Ozzell Robeson 34.7064610 -79.1179750 7.6 WaB - Wagram I NC-RO-16-16 Campen, James T.; Surles, Mary Sydney Baker, Ozzell Robeson 34.7148190 -79.1014140 5.0 WaB - Wagram 2 NC-RO-16-17 Campen, James T.; Surles, Mary Sydney Baker, Ozzell Robeson 34.7152970 -79.1003030 6.0 WaB - Wagram 2 NC-RO-16-18 Campen, James T_; Surles, Mary Sydney Baker, Ozzell Robeson 34.7129530 -79.0988640 12.3 WaB - Wagram 2 NC-RO-16-19 Campen, James T., Surles, Mary Sydney Baker, Ozzell Robeson 34.710797' -7%099344° 1.6 WaB - Wagram 2 NC-RO-17-01 Lumberton Municipal Airport Allen, Delois Robeson 34.6107330 -79.0540080 36A Jo— Johns Sandy 3 NC-RO-17-02 City of Lumberton Allen, Delois Robeson 34.599369" -79.0748500 25.4 Lu - Lumbee 4 NC-RO-17-03 City of Lumberton Allen, Delois Robeson 34.6007670 -79.0718970 28.0 Lu --- Lumbee 4 NC-RO-17-04 Lumberton Municipal Airport Allen, Delois Robeson 34.6073640 -79.0581030 47.7 Jo — Johns Sandy 3 NC-RO-18-01 Pittman, Bobby Keith Robeson 34,6303720 -78.8542940 16.6 WaB - Wagram 5 NC-RO-18-02 Floyd, Polly Nanatte McLean; McLean, Christopher; Parker, Judy Gray McLean; Vukovich, Gwendolyn A. M., Life Estate; Vukovich, Vanessa Lynn; Vukovich, Craig, Jr. Robeson 34.6150780 -78.8710560 49.3 NoA - Norfolk 6 NC-RO-20-03 Hammonds, Ronald G. Robeson 34.7882360 -79.096525' 24.90 WkB - Wakulla 7 NC-RO-20-04 Brown, Charles H. Hammonds, R. G. Robeson 34.7795610 -79.0864110 31.2 WkB - Wakulla 8 NC-RO-20-06 Hammonds, Ronald G. Robeson 34,7251280 -79.0415860 6.7 NoA - Norfolk 10 NC-RO-20-07 Hammonds, Ronald G. Robeson 34.7244750 -79,0393780 13.0 GoA — Goldsboro I0 NC-RO-20-08 Hammonds, Ronald G. Robeson 34.729978" -79,034169° 73.2 GoA — Goldsboro to NC-RO-20-14 Taylco, Inc. Hammonds, R. G. Robeson 34.7267640 -79.0362920 10.6 GoA - Goldsboro IO WQ0000672 Version 4.0 Attachment B Page 1 of 2 ATTACHMENT B - Approved Land Application Sites City of Lumberton Certification Date: April 27, 2017 Permit Number: WQ0000672 Version: 4.0 Field Owner Lessee County Latitude Longitude Net Acreage Dominant Soil Series Footnotes NC-RO-21-01 Oxendine, Fannie Cummings, Lacy Robeson 34.7071790 -79.0928790 36.1 NoA—Norfolk l I NC-RO-21-02A Oxendine, Fannie Cummings, Lacy Robeson 34.7063920 -79.0892860 38.4 NoA—Norfolk 11 NC-RO-21-02B Oxendine, Fannie Cummings, Lacy Robeson 34.7041060 -79.0886670 5.1 WaB - Wagram 1 I NC-RO-21-03 Oxendine, Fannie Cummings, Lacy Robeson 34.7050640 -79.0938580 3.4 WaB — Wagram 11 NC-RO-21-04 Oxendine, Fannie Cummings, Lacy Robeson 34,7027030 -79,0911440 11.3 WaB — Wagram 11 NC-RO-21-05 Oxendine, Fannie Cummings, Lacy Robeson 34.7107680 -79.0904940 15.1 GoA - Goldsboro 1 I NC-RO-28-01 Baskcrvil le, Robert D., Jr. Locklear, Carnell Robeson 34.7299590 -79,1029140 1 L6 Ra - Rains sandy 12 NC-RO-28-02 Baskerville, Robert D., Jr. Locklear, Carnell Robeson 34.7325940 -79.1001530 56.9 GoA - Goldsboro 12 NC-RO-28-03 Baskerville, Robert D., Jr. Locklear, Camell Robeson 34,7278030 -79,0946860 10A GoA - Goldsboro 12 NC-RO-39-01A Bullard, Lindbergh, Heirs Bullard, Patrick Robeson 34.603064° -79.2193530 5.3 GoA - Goldsboro 13 NC-RO-39-01B Bullard, Lindbergh, Heirs Bullard, Patrick Robeson 34.6019030 -79.2186920 2.6 GoA - Goldsboro 13 NC-RO-39-02 Bullard, Lindbergh, Heirs Bullard, Patrick Robeson 34.6019390 -79.2176220 1.4 GoA - Goldsboro 13 NC-RO-39-03 Bullard, Quindale; Bullard, Luzette Bullard, Patrick Robeson 34.5999190 -79.2204920 5.1 Ra- Rains sandy 13 NC-RO-39-04 Bullard, Quindale; Bullard, Luzette Bullard, Patrick Robeson 34.5999580 -79.2187420 14.8 Ly - Lynchburg 13 NC-RO-39-05 Bullard, Barbara Bullard, Patrick Robeson 34.6002140 -79.2173030 3.8 Ly - Lynchburg 13 NC-RO-39-06 Bullard, Barbara Bullard, Patrick Robeson 34.6009390 -79.2168030 2.9 WaB — Wagram 13 NC-RO-39-07 Bullard, Lyndon; Bullard, Anissa Emanuel Robeson 34.6867360 -79.033389' 3.7 GoA - Goldsboro 14 NC-RO-39-08 Bullard, Lyndon Robeson 34.686931° -79.0317360 7A NoA—Norfolk 14 NC-RO-39-09 Bullard, Tracy Elizabeth Robeson 34.407389° -79.0732670 62.5 WaB — Wagram 15 Total 761.8 1 to 15. See Figures 1 to 15, respectively. WQ0000672 Version 4.0 Attachment B Page 2 of 2 First year First year Year 1 Year 2 Year 3 Year 4 Year 5 5 Year Par (Ibs PAN/a = enter valu 2) JOAN -surface = 17411 PAN injection 1 - 23915 Surface TKN PAN PAN I (mg/Kg) (mg/Kg) (Ibs/DT)j 49000 17410 34.82 31590 4738.5 9.477 26851.5 2013.863 4.027725 24837.64 931.4114 1.86282? 23906.23 448.2417 0.89648? 25542.021 510840 3) lopprations log calcs Assumed Rate Acri Surface 50 100 150 200 (acres) 1392.8 696.4 464.266 i 348.2 4) 1PANIsitinmary, PAN First year Five year max. adjusted 11 t Application Number: W00000672 Project Name: Lumbcton, City Auto$ludge v2.1 Review Engineer. FRO by DJB 9/10/1990 Date: 24-Aug-20 Modified RLK 123/1998 Modifed JRP 4/9/1999 - Decimal % Total Solids 0.000 0.021 PH 7.30 - Gallons/yr Dry Tons/yr Volume .2,000.00 mg/kg mgll Ibs/dry ton Ibs/yr TKN 49,000.000 10.290 98.000- 196,000.000 (Ammonia as N) NH3 13,000.000 2.730 26.000 52,000.000 NO3-NO2-N 110.000 0.023 0.220 440.000 Phosphorus (P) 16.000.000 3.360 32.000 64,000.000 Potassium(K) 4,030.000 0.846 8.060 16,120.000 Sodium (Na) 11,400.000 2.394 22.800 45,600.000 Calcium (Ca) 12,300.000 2.583 24.600 49,200.000 40 CFR Pan 503 Magnesium (Mg) 2,180.000 0.458 4.360 8,720.000 Ceiling Concentrations Arsenic (At) 14.800 0.003 0.030 59.200 mpjkg 14.80 ok m 75 Cadmium (Cd) 0.504 0.000 0.001 ' 2.016 0.50 ok 85 copper(Cu) 276.000 0.058 0.552 1,104.000 276.00 ok 4,300 Lead (Pb) 19.800 0.004 0.040 79.200 19.80 ok 840 Mercury (Hg) 2.130 0.000 0.004 8.520 2.13 ok 57 Molybdenum (Mb) 7,240 0.002 0.014 28.960 7.24 ok 75 Nickel (Ni) 41.300 0.009 0.083 165.200 41.30 ok 420 Selenium (Sl) 19 000 0.004 0.038 76.000 19.00 ok 100 Zinc Zn 613.000 0.129 1.226 2.452.0001 613.00 1 ok 1 7,500 WQOOOObi PAN Calculations mg/kg Ibs/dry ton Ibs/year First -Year Surface App. 17,410.000 34.820 69640.000 First Year Subsurface App. 23,910.000 47.820 95640.000 Five -Year Surface App 21,488.253 42977 85953.012 Five -Year Subsurface App 27,988.253 55.977 111953.012 Mineralization Factor, K: 0.3 K = 0.4 for raw sludge 0.3 for aerobically digested sludge 0.2 for anaerobically dig. sludge 0.1 for compost SAR Calculation 0.36 24-Aug-20 Page 2 ' Allowable Residual Loadin(per ear Allowable PAN First -Year Surface Application First Year SubsurfaceApplication Five -Year Surface Application Five -Year Subsurface Application Proposed Crop(s) (Ibs./ac./yr.) Dry Tons/acre Gallons/acre Acres required Dry Tons/acre Gallons/acre Acres required Dry Tons/acre Gallons/acre Acres required Dry Tons/acre Gallons/acre Acres required Crop Level #1 50 1.436 1639781.143 1,392.80 1.046 1194002.079 1,912.80 1.163 1328567.272 1,719.06 0.893 1020020.424 .2,239.06 Crop Level #2 y�Crop _ 100 2872 ' 3279562.286 696.40° 2.091 ' 2388004.157 ;95642� ' 2.327 2657134.545 859.53 •� 1.786 • 2040040 947 1,119.53 Level 43 150 4.308 4919343.429 464.27 _3.137 3582006.236 637.60 _ 3.490 3985701.817 573.02� _ 2.680 3060061.271 746.35 Crop Level #4 200 5.744 6559124.572 348.20 4.182 4776008.314 478.20 4.654 5314269.090 429.77 3.573 4080081.695 559.77 Site Life Most Restrictive Crop: Most Restrictive PAN:) Level 92 ", 100.00 Ibs PAN/acre/yr _ FIELD INFORMATION Site number . number of acres Existing Sites 40.00 Acres required: ?i 696.40 acres for surface application (virgin) 0.00 Acres required: S59.53 acres for surface application (repeated) 0.00 Tons Applied/Acre/Yr.: ; 2.87 (surface -virgin) 0.00 Tons Applied/Acre/Yr.:, 2.33 (surface -repeated) 0.00 Actual tons appJAcre/Yr.:( _ 50.00___J 0.00 Pollutants Part 503 Surface Subsurface • Actual 0.00 " Cummulative Site Life Site Life Site Life 0.00 (Ibs. per acre) (years) (years) (years) 0.00 0.00 Arsenic (At) 36 423.49 522.69 24.32 0.00 Cadmium (Cd) 34 11744.84 14496.04 674.60 0.00 Copper (Cu) 1,338 844.01 1041.71 48.48 0.00 - Lead (Pb) 267 2347.71 2897.66 134.85 0.00 Mercury (Hg) 15 1226.06 1513.26 70.42 0.00 Molybdenum (Mb) 16 384.75 474.88 22.10 0.00 Nickel (Ni) 374 1576.60 1945.91 90.56 0.00 Selenium (Sp 89 815.52 1006.56 46.84 0.00 Zinc Zn 2,498 709.46 875.66 40.75 ' Total Acres: 40.00 ATTACM[ENT B Approved Land Application Sites City of Lumberton Certification Date: April 27, 2017 Permit Number: WQOOOOb,72 Version: 4.0 -is F►PPUC4 Field Owner. Lessee County Latitude Longitude Nei Acreage Dominant Soil, .Series . Footnotes Baker, Arrin. Ozzell Robeson 34.706492" -79.127539° ' 16.9 �$E ? ;ta - Rains sandy " , 9 .I NC-RO-16-02 Baker, Arrin Ozzell 'Robeson 34.7037250 49.1272920 3.6' GoA- G6ldsboro I NC-RO-16-03 Baker, Arrin..Ozzell Robeson 34.7054580 -79.1256780 3A GoA - Goldsboro 1 NC-RO-16-04 Baker, Arrin Ozzell Robeson 34.7047250 -79.1252030 3.6 Ra - Rains sandy 1 NC RU=16=0 Baker, Arrin Ozzell. Robeson 34.706..136" -79.123192R 8.7 E _ - ns dy �„p 1 1t0- 6- Baker, Arrin Ozzell Robeson 34.7051970 1 -79.1221220 14,81 NoA-'4Norfo k (G; Zp,jAt e Baker Arrin Ozzell Robeson 34.706717° -79,120431° 17.5 (l NoA -Norfolk ` S 7ar � lC NO=RO-16-08 Baker, Arrin Ozzell Robeson 34.706461 79.117975. 7.6 ' NVaB - Wagram 1 C-RU l;(i l Campen, James T.; Surles, Mary Sydney Baker,.Ozzell Robeson. 34.7148`19° -79.101414° 5..0 g. WaB -. Wagr C� 9 br/n c Nan' 6 Campen, James T.; Surles, Mary Sydney Baker, Ozzell Robeson 34.7152970 -79.1.003030 6.0 2, WaB - WagramaTAc Wt@-1;6_18 Campen, James T.; Surles, Mary Sydney Baker, Ozzell Robeson 34.712953° -79.098864R 12.3 WaB - Wagr �y ,S D7 Campen, James T.; Surles, Mary Sydney Baker, Ozzell. Robeson 34.7107970 -79.0993440 1.6 f �WaB - Wagrw)i NC-RO-17-01 Lumberton Municipal Airport Alien, Delois Robeson 34.6107330 -79.0540080 36.4 Jo —Johns Sandy 3 NC-RO-17-02 City of Lumberton Allen, Delois Robeson 34.5993690 -79.0748500 25.4 Lu'- Lumbee 4 C t20 1f 4 City of Lumberton Allen, Delois Robeson 34.600767° -79.071897" 28.0 �Q. Lu — Lumbe c _ NC-RO-17-04 Lumberton. Municipal Airport Allen, Delois Robeson 34:607364° -79.0581030 47.7 Jo —Johns Sandy 3 NC-110-18-01 Pittman, Bobby Keith Robeson 34.6303720 -78.8542940' 16.6 WaB - Wagram 5 NC-RO-18-02 Floyd, Polly Nanatte McLean; McLean, Christopher; Parker, Judy -Gray McLean; Vukovich, Gwendolyn A. M., Life Estate; Vukovich, Vanessa Lynn; Vukovich, .Crai , Jr. Robeson 34.6150780 -78.8710560 49.3 NoA -3N Ik 6 N 2t0 03W Iiam.monds, Ronald G. Robeson 34.7882360 -79.0865250 24.90 4Q - Wakull a G R()-20-04 Brown, CharlesH. Hammonds, R. G. Robeson 34.7795610 =79.08641 to 31 q_-WkB - 'Wakulls c - A(�RO=201-07 Hammonds, Ronald G. Robeson 34.725128° -79.041M60 6.7 `� NoA - Norfolk 71,T 10� C R?=20�65� Hammonds; Ronald G. Robeson 34.7244750 49.0393780. 13.0 �? ggqA-: Golds bo o 1 r 0 Haammonds, Ronald G. Robeson 34.7299780 -79.0341690 73.2`q GoA—Goldsbo o n1jp > ( 1ft7`20�[ Ta Icor Inc. Y Hammonds > R. G. Robeson 34.7267640 -79.036292° 10.6 �rotl-Goldsbor 0 WQ0000672 Version 4.0 - Attachment B Page i orz ATTACHMENT B = Approved Land, Application Sites ci ; tyo(Itumberton., Certification Date:.. April 27,2017 Permit,Number: WQ0000672 Version: 4.0' DTs Field 'OWner Lessee- county Latitude Longitude. Net Mr6age. Dominant -Soil Series I !Footnotes Qicendine,.Fanuie Cummings, Lacy, Robeson ,34.707179?, -79,0928.790 36.1 NoA - Norlik YI 7NOR-Owl, =102- Oxdndine, Fannie Cuni'mings, Lacy Robeson 34.706392' 49,0802I66, 38.4 r4 NdA - Noifol c NC-RO-21-02B Oxendine, Fannie Ciunmings, Lacy Robeson 34,704106? -79.0886670 5.1 WaB - Wagram 11 NC-RO-11-0 Oxendifte., Fannie Cummings, Lacy Robeson 34.165060' -79.0938586 3.4 WaB - W4gram 11 NC4641-04 OxMdffic, Fannie Cummingsjacy Robeson. 343027030 -79.0911440 14.3 WaB - Wagram I I NO-W.=2 t-05 Oxendind;-Fannie Curnmifigsj Lacy Robeson 34.7107680- -79.0904940 15.1 GoA - Goidsboro NC-RO-28-01 Rasketville, Robert D., Jr. Locklear., Carnell Robes'O'fl 34.7299580 -79.1029140 11.6 Ra - Rain's'sandy 12 .N- asko rvuie�,Robeft' D.- Jr.Goldsboro-) L&Icleg,'Carnell- 'Robeson. 34.M5�46 479.1001530 ia GoA - 0 1 / I NC-RO-2'8-03 I Msketvilic,'Robert D., Jr. Locklear,.Camell Robeson 34.7278036 -70946860 10.4 GoA - Goldsboro 12 NC-RO-39-0IA Bullard, Liridberg4, Heirs BidlardiPatrick Robeson 34.6030640 -79.219353P 5.3 GoA - Goldsboro 13, NC-RO-39-OIB Bullard, Lindbergh; Heirs Bullard, Patrick Robeson 34.6019030 -79.2186920 2.6 GoA - Goldsboro 13 NC-RO-39-02 Bullard, Lindbprgh Heirs Bullard, -Patrick- Robeson 34MI9.390 49.2176220 11.4 GoA - Goldsboro 13 NC-RO-39-01 13ultard,,Quindale,- Bullard., Luzette Bullard, Patrick Robeson 34.5999190 -79.220492" 5.1 Ra - Rains sandy 13 NC-RO-39-04 Bullard, Q.uindale; Bullard, Luzette Bullard,Patriek Robeson 34.599958' -791118742' 14.8 Ly - Lynchburg 13 NC-RO-39,05, . Bullard, Barbara BullarkPatrick Robeson --79.2171030 3.8 Ly - Lpchburg. 13 NC-RO-39-06 Bullard, Barbdra Bul . lardTatric'k Robeson 34.6001930- -79.2 168030 2.9 WaB - Wagrain 13 NC-'RO-39z07 -Bullard, Lyndon;:Bullard, AnissaErnanuel -Robeson 34.6867369 -79.0333890 3.7 GoA - Goldsboro 14 `N&RO-39:-08 Bullard, Lyndon R6beson 34.686911' -19,6317360 7.4 NoA - Norfolk \ 14 EMT MIMIC Bullard, Tracy rnizabeth Rbbd-sbn'\ 34.407389', -79.073267' 62.5 ',,?--WaB - Wagr . a Total 761X I to 15, See Figures I to 15, respectively. WQ0000672. Version 4.0 Attachment B Page 2 of 2 6.31 (,o.7 .302./ ,I+ *r Resources ENVIRONMENTAL QUALITY April 27, 2017 WAYNE HORNE - CITY MANAGER CITY OF LUMBERTON POST OFFIa BOX 1388 LUMBERTON, NORTH CAROLINA 2,8359 M MUP#l; a iT ROY COOPER Governor MICHAEL S. REGAN secrelOry S. JAY ZlM1VIERMAN Director: Subject: Permit No. WQ0000672. City of Lumberton RLAP Land Application of Class B' Residuals Robeson County . In accordance with your permit major modification and -renewal request received February 6, 2017, and subsequent additional information received March 30, 2017, we are forwarding herewith. Permit No. WQ0.000672 dated April 27, 2617, to the City of Lumberton for the continued operation of the subject residuals management program. Modifications to the subject permit are as follows: 1. Removal of Lumberton WTP as a residuals source with a reduction of 400 tons/year.. 2, Removal of 40 fields in Robeson County totaling 862.4 acres, those fields being: NC-RO-16- 20, NC-RO-21, NC-RO-19-01, NC-RO-19-05, NC-RO-19-08, NC-RO-19-09, NC-R049-10, NC-RO-19-11, NC=RO-19-12, NC-RO-19-13A, NC-RO-1943B, NC-RO-1945, NC-RO-19- 20, NC-RO-19-21, NC-RO-19-22, NC-RO-19-23, NC-RO-19-23, NC-RO-19-25, NC-RO-19- 29, NC-RO-19-30, NC-RO-1.9-34, NC-RO-19-35, NC'-R0=19-36, NC-R0-19-37,_NC-R0-19- 38, NC-RO-20-05, NC-RQ-22-01, NC-RO-22-02, NC-R0-22=03, NC-RO-27-01, NC-RO-27- 02, NC-R0-27-06, NC-RO-27-07, NC-RO-37-01, NC-110-37-02, NC=RO-37-03,:NC-RO-37- 04, NC-RO-37-05, NC-110=37-06, NC-RO-38-01. and NC-RO-38-02. This permit shall be effective from the date of issuance until March 31, 2022, shall void Permit No. WQ0000672 issued May 12, 2008, and shall be subject to the conditions and limitations as specified therein. Please -pay particular attention to the monitoring requirements listed in Attachment A for they may differ from the previous permit issuance. -Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. •' "�' Nc�rlaira3 Compares-,,, , State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919-807-6332 ATTACHMENT A - Approved Residual Sources City of Lumberton C _ L Certification.Date: April 27, 2017 Permit Dumber: WQ000067Z Version 4-.0 r Maximum Monitoring Monitoring Monitoring Frequency for Approved Owner Facility Name County Permit Biological Dry Tons Frequency for Frequency for Pathogen & Mineralization Number Residuals Per Year t Non -hazardous Metals and VReducti Rate Characteristics z .. Nutrients 3, _ Reriuctions as Reductions City of Lumberton Lumberton WWI? Robeson N00024571 Yes. - 1,500 Annually See Table Below. See Table Below 70.3 Total 1,500 1. Maximum .Dry Tons per Year.is the amount of residuals approved•for land application from each permitted -facility. 2. Analyses to demonstrate that.residuals are non=hazardous (i.e. TCI,I'; ignitability,:reactivity, and corrosivity). as stipulated under permit Condition IV:2. 3. Testing of metals and nutrients as stipulated under. permit Condition IV.3. 4. Analyses of pathogen and ve.ctor;attraction reductions as stipulated under permit Condition IVA. 5. Monitoring frequencies are based on the actual Ary tons applied peryear using ther table below, unless specif ed above. Dry Tons Applied short tons per ear . Monitoring Frequency Established in 40 CFR 503 and 15A`NCAC 02T .l 11 l <319 1/Year =>319 - <1;650 1/ Quarter. 4 times peryear) =>1,650 - <16,5K 1160 Days 6 times per ear) >] 6,500 1/month (12 times, er ear If no land application events occur -during a required sampling period (e.g. no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to EPA may be required to makeup the missed sampling, contact the EPA for additional'information and clarification.- WQ9000672 Version 4.0 Attachment A Page 1 of 1 Field # Dry Tons Applied Gallons _RQ-39-09� ;07. i 307.1455 3372800 R0L;28-2T i 60.731 539400 RO-16=08 92r, 1 ' 92.1437 818400 RO-16=07' Gov. �� 100.5204 892800 RO-116=7& 2 , q - 24.432 279000 R046=17 /y,` 7 14.6592 167400 RO`-16=1R' g 54.8363 626200 RO-16z19 R. ,7 8.6869 99200 110=17=073 6, O 76.0108 868000 R0=20=-03' p2, 5 102.921 1175300 R0=2-0=04- 162. te 162.643 1857300 RO=20=-08? Z , 1 296.054 2833400 RO--207-1'411 z11, p 40.9527 458800 RQ721zzAf 6,3 6.2825 55800 JRQF16_053 S, $ 35.8336 409200 R.O.-16-019 (, S , '7 ' 65.695 750200 RO-20307P (v (, . 0 65.695 750200 130-20:A6v 31, .,q 31.4201 358800 Total S` g 1546:6627 1631 200 d m ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON . PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-16-01 Acres Utilized: 16.9 Land Owner: Ozzell Baker Annual Dry Tons Applied: �65.6950 ' Site #: I Acres Permitted: 16.9 Operator: Ozzell Baker • Ra-Rains Sandy Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Crop 1 Max. PAN: 151 Crop 2 Name:. Crop 2 Max. PAN: c ° A Volume applied enter one Solids/ ( ) Li Liquid 4 Cu. Yds Gallons 310000 % Solids 2.1 Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert:, Animal Waste, etc) Soil Cond. (Dry. Wet, Moist Precip: Past 24 Hi•s inches y � n E o o a o C O ;� ^; ?' * w w m * °c TKN mg/kg 490001 Z a o 0 Qo E a • mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type P YP Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 7/9 `-. A.606 W00000672 Dry 0 1 S 0.5 1 0.3 13000 -110 55.932 55.932 7/10 440200 2.1 2.281 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 79.423 79.423 0.000 0.000 0.000 6.000 ` 0.000 0.000 0.000 0.000 0.000 A000 0.000 0.000 ,."-0.000 0.000 ` 0.000 ;.,, 0.000 -0A00 9.600 " - 0.000 ` 0 000 0.000 ,0.000 " 0.000 0.000 0.000 0.000 0.000 0.000 :' 0.000' . 0 . 0- 0;000 . ' Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000- O'.000 , ..-... TOTALS ": : ; o. ' 'Zsozoo Cd Cu ' Cr Pb H Mo -Ni Se -Zn P 135.355 ,135'355' Lime A lied Annual Ibs/acre 0.003 0.000 2.146, 1.772 0.154 0.000 0.056 . ' 0.056 0.321 0.321 0002 , 0.002 . ` 4,765 " 4 765 124.384 Date lbs/ac Prior Years Cumulative lbs/a c Current Cumulative lbs/ac ,, ' 0.'003, " 0.000 2.146 `..'1.772 , 0.154° 0.000. Permitted C. P. L. R. ** ** Permit PAN Limit l st/2nd Crop . ::;. ......:....... :<.<:;<.:::>::<.:<: ... 151" . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS'BLANK FORM TO BE COMPLETED AND`SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-16-05 Acres Utilized: 8.7 Land Owner: Ozzell Baker Annual Dry Tons Applied: ;358336 Site #: 5 Acres Permitted: 8.7 Operator: Ozzell Baker Ra-Rains Sandy -Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Crop 1 Max. PAN: 151 Crop 2 Name: Crop 2 Max. PAN: S. o •S ° p 4 ° Q Volume applied PP � (enter one) Solids/ Liquid Cu. Yds Gallons % Solids 2.1 Volume Applied per Acre (Dry Tons/Ac) Residual (NPDES #, WQ#, . Fert. Animal Waste, etc) Soil Cond. (Dry' Wet, Moist Precip. Past 24 -H. rs inches a 4'a � b o 0 < o � �; w * N' w -+ * TKN mg/kg 490001 Z Y �t 6 o S I: a mg/kg Nitrate and Nitrite mg/kg PAN Applied'. (lbs/acre) Name of CropType YP Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 7/27 161200 -.1.623 "" WQ0000672 Dry 0 S 1 0.5 0.3 13000 110 56.498 56.498 7/28 248000 2.1 2.496 . , WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 86.919 86.919. 0.000' s 0.000 0.0001 0.000 0.000 0.000 `.0.000 0.000 `0.000 0.000 0.000 6'.000' 0.000 r 0.000 ; 0.000, 0.0011 .{. 0.000 0.000` 0000 0.000 0.000 .. 0.000 0.000 0.000 " 0.000. 0.000 0.000 0.000, 0.000 0.000 . ..,. , . :0" "; : < 0 "0.000 •;. Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 ,0.000 ,, TOTALS "'.' 0 409200 .. ;: Cd Cu Cr Pb Hg Mo Ni Se Zn P 143,417 143,417 __Lime Applied Annual lbs/acre "0.003 . 0.003 0.000 0.000' "2.274 2.274 1.878 1.878 0.163 0.163 0.000 0.000 0.060 0.060. 0.340 0.340. 0.003 0.003 5.050 5.050 131.808Date .... lbs/ac Prior Year 'Cumu at v I i e lbs/ac s Current Cumulative lbs/ac Permitted C. P. L. R. Permit PAN Limit Ist/2nd Crop :: ,:. ...... ...:.: 151 ' "I certify, under penalty of law; that -this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated,the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L:R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION: FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #E WQ0000672 Field #: NC-R0-16-06 Acres Utilized: 14.8 Land Owner: Ozzell Baker Annual Dry Tons Applied::92.1437' Site #: 6 Acres Permitted: 14.8 Operator: Ozzell Baker . NoA-'Norfolk Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Crop 1 Max. PAN: 230 Crop 2 Name: Crop 2 Max. PAN: ° ��" ° 7�4° M : Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons o �o Solids 2.7 Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist)'inches Precip. past 24 13rs. y b ter- o w. ° o' o o ° N' *' °= 0 . `D c; * N' * ma. °a TKN mg/kg 53000 Z Y o w o `3 R. ° mg/kg Nitrate and Nitrite mg/kg PAN Applied (]bs/acre) Name of Crop Type Receiving Residual g Application Crop 1 Crop 2 Crop 1 Crop 2 3/21 279000 :2.122.•. WQ0000672 Dry 0 S 0.5 0.3 6200 94 73.157: 73.157 3/28 390600 2.7 '2.971 WQ0000672 Dry 0 S 0.5 0.3 53000 6200 94 102.420 102.420 3/30 148800 2.7 ",1.132 - WQ0000672 Dry 0 S 0.5 0.3 53000 6200 94 39,017 39.017, 0.000` '"' - 0.000 0.000 0.000., 0.000 0.000. 0.000 0.000 . ' 0.600' "0.000-, 0.000 '0.000 0.000 _ 0.006 0.000 x 0.000 . 0:000. 0.600 0.000 0.000. 0.000 0.000 ` 0.000 ' 0.000. 0:000, Residuals A hcations totals on FORM FSF su attach FORM FSF su to this form 0.000 0.000 TOTALS: ` . .' " 0 818400 <':; :.... . Cd Cu Cr Pb H Mo Ni Se Zn P 214:595 214.595 Lime Applied Annuallbs/acre 0.151 0.006 5.068 . 0.000 0.269 0.022 0.097 0A89 0.194 8.480 1.170 Date lbs/ac Prior Years Cumulative lbs/ac 0.097 ' 0.489 0.194 8.480 Current Cumulative lbs/ac 0:151 0.006 5.068 0.000 .0.269 .01022 Permitted C. P. L. R. **** Permit PAN Limit Ist/2nd Crop 230 . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost"-0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. - Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-16-07 Acres Utilized: 17.5 Land Owner: Ozzell Baker Annual Dry Tons Applied: 100.5204; Site #: 7 Acres Permitted: 17.5 Operator: Ozzell Baker Predominant Soil Series: NoA-Norfolk Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Crop 1 Max. PAN: 230 Crop 2 Name: Crop2 Max. PAN: o 0 o A Volume applied (enter one) Solids/ Liquid Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D Dry, " Wet,Cu. Moist Precip. Past 24 Hrs.p inches a b , b o a o 7O 2 CD y * N w rF ., cF 0 # 0 TKN mg/kg 53000 l Z a ix S q 0 ao 5 " �• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 3/20 204600 2.7 1316 W00000672 - Dry 0 S 0.5 0.3 6200 94 45.372 45.372,1 3/21 248000 2.7 1.596 WQ0000672 Dry 0 S 0.5 0.3 530001 6200 94 54.996` 54.996 3/27 142600 2.7 O:917;. WQ0000672 Dry 0 S 0.5 0.3 53000 6200 94-- 31.623 .3LM .3/29 148800 2.7 '0:957; ".' WQ0000672 Dry 0 S 0.5 0.3 53000 6200 . 94 32.997 32.997- 3/31 148800 2.7 0:957'.. W00000672 Dry 0 S 0.5 0.3 53000 6200 94 '32.997 32.997 0.000'L 0.000 0.000 • 0.000 0.000 6.000_, ' 0.000 - 0.1000 0.009, , 0.000 - 0.000_• 'uoo 0.000 ".. 0.000 . 0.000,- 0.000, A000. 0.000 0.000 0.000' 0:000.: ...., ,. U ,..; 0" " 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000, TOTn1 a s92soo �> As Cd Cu Cr Pb. H Mo Ni Se Zn P 197.985 197:985' Lime Applied Annual lbs/acre 0.139 0.006 4.676 0.000 0:248 0.020 0.090 0.451 0.179" 7.823 ;; Date lbs/ac Prior Years Cumulative lbs/ac ,.. Current Cumulative lbs/ac 0.139 0.006 .4.676 0.000 0.248 0.020 0.090 0.451 0.179 7.823 Permitted . C. P. L. R.**** Permit PAN Limit l st/2nd Crop - ........ ......... " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified 'personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE: Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-110-16-16 Acres Utilized: 5. Land Owner: James Campen Annual Dry Tons Applied: 24.4320 Site #: 16 Acres Permitted: 5 Operator: Ozzell Baker Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503): Crop I Name: Bermuda . Crop 1 Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN: o c` o A Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids - Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Moil[ Preci P Past 24 Hrs. finches y 4 b cc b 0 C x � K. * d' 83 3 . W ? a R. * w' 0 TKN mg/kg 490001 Z a c`r o as o a w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/27 161200 ' 2.1 -. 2.823 WQ0000672 Dry 0 S 0.5 1 0.3 13000 110 98.306 98.306 7/16 117800 2.1 2.063 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 "71.839 71.839 .0.000 0.000 . 0.000 ` 0.000 -' ; 0.000 0.000 40.000 0.000 .0.000 - 0.000 , . 0.000 0.000 0.000 0.000 0:000 6:000 0.000 0.000" 0.000 -0.000 0.000 ' 0.000 0.000. 0.000 0.000 0.000 0:000 :. 0.. '-; '0 '0.000 , ., ; ` Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS ...', 0 379000 AS ' Cd Cu Cr Pb H Mo Ni Se Zn P 170.145 170.145 Lime Applied Annual lbs/acre 0.070 0.010 0.003 0.003 3.442 3.442 0.941 0.941 0.204 , 0.204 0.010. 0.010 '0.074. 0.074 0.393 0.393 -0.090 0.090 6.384 6.384 66.548 .:. Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative ,lbs/ac Permitted C. P. L. R. **** Permit PAN Limit Ist/2nd Crop ....... ;% ;:.:.:.. J. " 192 ." " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I -am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON - PLACE A "N/A" IN A• BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-110-16-17 Acres Utilized: 6 Land Owner: James Campen Annual Dry Tons Applied: ;14.6592 Site #: 17 Acres Permitted: 6.0 Operator: Ozzell Baker Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503): Crop I Name: Bermuda Crop 1 Max. PAN: 192• Crop 2 Name: Crop 2 Max. PAN: ' q cYa Q Volume applidd enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per PP p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#,- Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist Precip.y� Past 24 Hrs. inches 4,10 o m a a o � °: 0 - * N' 0 4 CD ^+ - 0 TKN mg/kg 1 49000 z Y o El caQo E mg/kg ' Nitrate and Nitrite mg/kg PAN Applied (]bs/acre) Name of Crop Type Receiving Residual Application Crop' I Crop 2 Crop l Crop 2 4/25 167400 2.1 2.443 WQ0000672 Dry 0 S 1 0.5 0.3 -13000 110 85.072 85.072. 0.000 -0.000 0.000 _ ; ,.0.000 , 0.000 0.000 . . 0.000'-, :0.000 0.000 0.000 .: 0:000 . 0.000, . 0:000. 1 0.000. 0.000 �- --��- _--��- �morT,T,lri= 0.000 u.uuu u.uuu 0 .; , - ' 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000, TOTALS " .0 ' i67400 ..........:.:.: AS Cd Cu Cr Pb Hg Mo Ni Se Zn P 85.072. 85.072 Lime Applied Annuallbs/acre 0.002 0.000' 1.349 1.114 0.097 0.000 0.035 0.202 0.002 2.995 78.176 Date lbs/ac Prior Years Cumulative Ibs/ac Current Cumulative lbs/ac 0.002 0.000 1.349 1.114 . `0.097 0.000 0.035 0.202 0.002' 2.995 Permitted C. P. L. R, *** Permit PAN Limit 1st/2nd Crop 192 - "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - lA Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELRAPPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit it: WQ0000672 Field #: NC-RO-16-18 Acres Utilized: 12.3 Land Owner: James Campen Annual Dry Tons Applied: ?54.8363 Site M.18 Acres Permitted: 12.3 Operator: Ozzell Baker Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503): Crop I Name: Bermuda Crop I Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN: o A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (DryTons/Ac) Residual Sources (NPDES #, WQ#, . Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist Precip. Past 24 Ham• inches- y b �' c ?; � o ?; -- _ * °p 4 w `5° . * =. * °p TICN mg/kg 49000; Z a o a, a mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 . 4/22 167400 2.1 1.192 WQ0000672 Dry 0 S 0.5 1 0.3 13000 110 41.499 41.499 4128 192200 2.1 1368 WQ0000672 Dry 0, S 0.5 0.3 490001 13000 110 47.647 47.647 4/29 6200 2.1 : 0:044 •, WQ0000672 Dry 0 S - 0.5 0.3 49000 13000 110 1.537 1.531 , 7/15 260400 2.1. 1:854 WQ0000672 Dry 0 S 0.5, 0.3 49000 13000 110 64.554 64.554 .0`.000. 0.000 0.000 0:000 0.000 0.000-, 0A00 0.000 .0.000 V.000 ` "-0.000 0.000 . 0:000:..: ( 0.006 " 6.000 0.000 • , 0.000 � 0.000 0.000 0.000 0.000 0.,000 0.000 '. 0:000 0 ...; „0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0:000 TOTALS r =' "; " . o - 626200 ...... ,; As Cd I Cu Cr Pb Hg Mo Ni Se I Zn P 155.236 155.236 Lime Applied Annual Ibs/acre 0.003 0.000 2.461 2.033' 0.177 0.000 0.065 0.368 0.003 5.466 142.656 ! Date lbs/ac Prior'Years Cumulative lbs/ac , Current Cumulative Ibs/ac 0.003 0.000 2.461 2.033 0.1773 6.000 0.065 0.368 0.003 5.466 Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop 192 . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing -violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization, Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land"Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANKFORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-110-16-19 Acres Utilized: 1.6 Land Owner: James Campen Annual Dry Tons Applied: 8.6869 ' Site #: 19 Acres Permitted: 1.6 Operator: Ozzell Baker Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503): Cron 1 Name: Bermuda Crop 1 Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN: F ° p a ° A Volume applied (enter one) Solids/ Li uid 9 Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES.#, WQ#, Fert., Animal Waste, etC) Soil Cond. (Dry' Wet, Moist)inches preci p• past 24 Hrs. a 410 b o �, o < o m _ * N• R. p g• w * ~• w * p TKN mg/kg 490001 Z = E3 o E n o CD ° o w mg/kg Nitrate and Nitrite mg/kg PAN Applied pp ( lbs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 4/29 99200 2.1 5.429 W00000672 Dry 0 S 0.5 1 0.3 13000 110 189:050 189.050 .0.000 0.000 0.000 0`.000 0.000 0.000 - 0.0001 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000' 0.000 6.000 0.000 0.000 0.000 0.000: -0.000. :0.000 0.000 ° 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0.000 Residuals Applications totals on FORM FSF supp (attach, FORM FSF supp to this form): 0.000 0.000 TOTALS 0 99200 As Cd Cu Cr Pb H Mo Ni Se Zn P 189.050 189.050 Lime Applied Annuallbs/acre 0.004 0.001 2.997 2.476 0.215 0.000 0.079 0.448 0.003 6.656 173.728 _. . ::< Date lbs/ac Prior Years Cumulative lbs/ac 0.003 6.656 Current Cumulative (bs/ac 0.004 1 0.001 2.997 2.476 0.215 0.000 0.079 0.448 Permitted C. P. L. R. **** Permit PAN Limit lst/2nd Crop _'' 192 " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that. qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5,, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION.FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK -FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-17-03 Acres Utilized: 28 Land Owner:c City of Lumberton ` Annual Dry Tons Applied: , 76.01,08 Site M 3 Acres Permitted: 28 Operator: Delois Allen Predominant Soil Series: Lu-Lumbee Cation Exchange Capacity (non 503): Crop I Name: Soybeans Crop I Max. PAN: 137 Crop 2 Name: Crop 2 Max. PAN: o t i 0 o A Volume applied pp (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist Preci . p Past,24 Hrs. inches y b ° o o' n o 0 C ° m ° -- :0 5 m =° . ?'_ * N °o TKN mg/kg 490001 Z Y i~ o 11 � 0 a �,• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5/14 192200 -2.1 0.601; W00000672 " Dry 0 S 0.5 1 0.3 13000 110 20.930 20.930 5115 192200 2.1 0.601 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 20.930. ' 20.930 5/16 148800 2.1 0.465. W00000672 Dry 0 S 0.5 0.3 49000 13000 110 '16.204 16.204 5/18 334800 2.1 1.047 WQ0000672 Dry 0 S 0.5 0.3 49000 .13000 110 36.460 36.460 A000. 0.000 0.000 0.000 0.060 - O.00Q 0.000 0.000 0.000:. 0.060 0.000 0,.000 6.000 0.000 '0.0001, 0.000 , 0.000 0..000. - 0.000 6.000 ' 0.000 0 a0 _.:;:: 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 _. 0.000 ..................................... ..;::! TOTALS : ' .,. 0 868000 ..,.._...._ AS Cd Cu Cr Pb H Mo Ni Se Zn P .94.525 94.525 Lime Applied Annuallbs/acre _ 0.002, 0.000 1.499 1.238 0.108 0.000 0.039 0.224 0.002 3.329 86.880 . . _ .:...._ :......._: Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.002 0.000 1.499. 1.238 0.108 0.000 0.039 0.224 • 0.002 . 3 329 Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop ........... -'..;. ......:. 137 "I certify, under penalty of law, that this document was prepared (under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation =1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-03 Acres Utilized: 24.9 Land Owner: Ronald Hammonds Annual Dry Tons Applied: ' 102.9210 Site #: 3 Acres Permitted: 24.9 Operator: Ronalld Hammonds Predominant Soil Series: Wkb-Wakulla Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Crop 1 Max. PAN: 147 Crop 2 Name: Crop 2 Max. PAN: G Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons o /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Wasie, etc) Soil Cond. We ' Moist Precip. past 24 Ham• inches y b a o o w °: * w 0 g * TKN mg/kg 49000 Z > o o0 0 E. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) -Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1, Crop 2 4/10 564200 2.1 •1.984% " WQ0000672 Dry 0 S 0.5 0.3 13000 110 69.090' 69.090V 4115 266600 2.1 ' 0.938' W00000672 Dry . 0 S 0.5 0.3 49000 13000 110 32:647 32.647 ' 4/16 303800 2.1 =• 1068 ., WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 37.203 .37.203; 7/17 40700 2.1 - 0143 W00000672 Dry 0 S 0.5 0.3 49000 13000 110 4.994 4.984 0.000 0.000-,, 0.000" 0000 0.000 , . 0.000 0.000 .' , ; 0.000 0.000 0.000' 0.006- -.0.000 • 0.000 0:000 0.000 0.00,0 0.000. 0.000 0.000 10.000 A • 1175300 0.000.' Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS '01 2330600 : ;:. As Cd Cu Cr Pb H Mo Ni Se Zn P 143.924 143.924 Lime Applied Annual lbs/acre 0.003 0.000 2.281 1.885 0:164 0.000 0.060 0.341 0.003 5.067 132 256 < Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.003 0.000 2.281 ' 1.885 0.164 0.000 0.060 0.341 0.003 5.067 Permitted C. P. L. R.****:77777 Permit PAN Limit 1st/2nd Crop :;. .:.... { ....... fi47„ "I certify, under penalty of law, that this document was.prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false ' information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation -**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 - Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-04 Acres Utilized: 31.2 Land Owner: Charles Brown Annual Dry Tons Applied::162.6438 Site #: 4 Acres Permitted: 31.2 Operator: Ronald Hammond Predominant Soil Series: WkB-Wakulla Cation Exchange Capacity (non 503): Crop 1 Name:' Bermuda Crop I Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN: H o N A Volume applied (enter one) Solids/ - Liquid' Cu. Yds Gallons o �o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert.,.Animal.. Waste, etc) Soil Cond. (Dry, �= Moist)_inches Precip. Past 24 Hrs• y a b - 0 o - o o ;v �; R * T m coo -, c; 'v * a TIW mg/kg 49000 z o 9 aq o a. mg/kg Nitrate and Nitrite mg/kg PAN Applied (]bslacre) Name of Crop Type Receiving Residual Application App Crop 1 Crop 2 Crop I Crop 2 5/4 266600 2.1 0.748- W00000672 Dry 0 S 0.5 1 0.3 13000 1 110 26.055 26.055 5/8 297600 2.1 0.835 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 1 110 29.085. 29.085' 5111 241800., 2:1 0:679 W00000672 Dry 0 S 0.5 0.3 49000 13000 110 2$.631 23.631 5/12 235600 2.1 6.661 WQ0000672. Dry 0 S 0.5 0.3 49000 13000 110 - 23.025 23.025. 7/18 229400 2.1 0.644.' WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 '22.419 . 22.419 7/20 173600 2.1 0.487,. W00000672 Dry 0 S 0.5 0.3 49000. 13000 110 16.966 16.9666 7/22 1 186000 2.1 0.522 W00000672 Dry 0 S 0.5 0.3 490001 13000 110 18.178 18.178 7/23 186000 2.1 0:522 W00000672 Dry 0 S 0.5 0.3 49000 13000 110 18.178 18.178 7/17 40700 2.1 Ot114 WQ0000672 Dry 0 S 0.5 03 49000 13000 110 3.978 3:978 0.000 1 0.00.0. 0.000 0.000 0.000 0.000 0.000 .. 0.000 -1 0.000 ;; .0 �. 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 - 0.000, _.. TOTALs o 1857300 ......._.... As Cd Cu Cr Pb H Mo Ni Se Zn P 181:515 181.515 Lime Applied Annual lbs/acre 0.004 0.001 2.878 2.377 0.206 0.000 0.075 0.431' 0.003 6.391 ' 166.816 Date Ibs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.004 0.001 : 2.878 2.377 0.206 0.000 0.075 0.431 0.003 - 6.391 Permitted C. P. LrR. **** >:> Permit PAN Limit I st/2nd Crop 192 "I certify, under penalty of law, that this document was prepared under my direction or supervision4n accoraance wrtn a system aestgnea to assure teat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates ;Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field M NC-RO-20-07 Acres Utilized: 6.7 Land Owner: Ronald G. Hammonds Annual Dry Tons Applied::31.4201 , r Site #: 7 Acres Permitted: 6.7 Operator: Ronald G. Hammonds Predominant Soil Series: NoA-Norfolk Cation Exchange Capacity (non 503): - Crop 1 Name: Soybeans Crop 1 Max. PAN: 164 Crop 2 Name: Crop 2 Max. PAN: 0 N q A Volume applied PP (enter one) Solids/ Li uid 9 Cu. Yds Gallons % , Solids Volume Applied per Acre - (Dry Tons�Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist Precip Past 24 Hrs. inches y 4 b cob o 0 a o p; ?: -• rT * °= w CD c; ^ * N * N °a TKN mg/kg z Y a El o El as o cl ? mg/kg Nitrate and Nitrite mg�kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7/13 18600 2.1 1 0.243 WQ0000672 Dry 1 0- S 0.5 0.3 49000 13000 1 110 8.465 8.465 7/17 340200 2.1 4.446 WQ0000672 Dry 0 S 0.5. 0.3 49000 13000 110 154.826 154.826 .0.000'- , '0.000 0:000 0.000 - 0.000 -0.0001 0.600 - - 0.000 •0.000. - 0.000 0.000 0.000' 0:000 0.006 '.0.000' --`0.000 0.060 0.000" 0.000' .0:000 0:0001 - 0.000 0.000 ` 0.000 0.000 ' 0.000 -0.000 0.000 0.000 0 Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop 0.000' Residuals Applications totals on -FORM FSF supp ( attach FORM FSF supp to this form): I 0:1 As Cd1 Cul Cri PblHglMol Nil Sel ZnJ P 1163 0.004 1-0.001 1 2.589 1 2.139 1 0.186 1 0.000 1 0.068'1 0.387 1 0.003 1 5.750 150.080 0.004 1 ,0.001 .1 2.589 1 2.139' 1 0.186 1 0.000 1 0.068 1 0.387 1 0.003 ,1 5.750 164 Date " I certify, under penalty of law, that this document -was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier _ Date *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton Land Owner: Ronald Hammonds Operator: Ronald Hammonds WQ Permit #: WQ0000672 Annual Dry Tons Applied: 296.05412 , Predominant Soil Series: GoA-Goldsboro Field #: NC-RO-20-08 Acres Utilized: 73.2 Site #: 8 Acres Permitted: 73.2 Cation Exchange Capacity (non 503): Crop 1 Name: Corn , Crop 1 Max. PAN: 147 Crop 2 Name: Crop 2,Max. PAN: o = cad ° Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet Moist Preci P Past 24 Firs. inches 3 •� b o w C ,d w `D* N' 0 ? # N 0 TKN mg/kg 1 53000 Z a �o o = ? mg/kg Nitrate and Nitrite . mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 1/9 241800 2.7 0.372 W00000672 Dry 0 S 1 0.5 0.3 6200 1 94 12.819 12.819 1/10 210800 2.7 0.324 WQ0000672 Dry 0 S 0.5 0.3 53000 6200 94 11.176 11.176 1/11 99200 2.7 0,153 WQ0000672 Dry 0 S 0.5 0.3 53000 6200 94 5.259 5.259 1/23 173600 2.7 0.267 WQ9000672 Dry 0 S 0.5 0.3 53000 6200 94 9.204 9.204 1/24 179800 - 2.7 0.277, W00000672 Dry 0 S 0.5 0.3 53000 6200 94 9.532 9.532 3/13 272800 2.7 0.420 WQ0000672 Dry 0 S 0.5 0.3 53000 6200 , 14.463 14.463 3/14 396800• 2.7 0.610 W00000672 Dry 0 S 0.5 0.3 53000 6200 i'9 21.037 21.037 3/30 62000 2.7 0.09$- WQ0000672 Dry 0 S 0.5 0.3. 53000 6200 -1287 -3.287 3/31 279000 2.7 0.429 -W00000672 Dry 0 S 0.5 0.3 53000 6200 14.791 14.791, 4/2 248000 2.1 0.297 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 10.331 10.331 4/3 223200 2.1 0.267 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 9.298 9.298 4/4 217000 2.1 0.260 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 9.039. 9.039. 0 -229400 0.274 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS 0 2833400 As Cd Cu Cr Pb Hg Mo Ni Se I Zn P 130.235 130.235 Lime Applied Annual lbs/acre 0.072 0.003 3.005 0.501 0.171 0.010 0.062 0.322 0.093 5.360 35.690 ' ' Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.072 0.003 3.005 0.501 0.171 0.010 0.062 0.322 0.093 5.360 Permitted C. P. L. 12.**** Permit PAN Limit I st/2nd Crop P .....:. ........ , . ....:: .::.......... 147 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM Supplemental Information PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton - WQ Permit #: W00000672 Field #: ;NC-RO-20-08 , ; Acres Utilized: ; 73.2 ' Land Owner:.Ronald Hammonds Annual Dry Tons Applied:'296.054154 ' . Site #: Acres Permitted: ;73.2 - Operator: ' Ronald Hammonds Predominant Soil Series: GoA-Goldsboro . Cation Exchange Capacity (non 503): ; Crop 1 Name:, Corn Crop 1 Max. PAN:: 147.00 Crop 2 Name: Crop 2 Max PAN: O G o Q Volume applied (enter one ) Cu. Yds Gallons 229400 % Solids 2.1 Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert.,,Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Dry Precip. Past 24 Hrs. inches a b F "S o w a o ° C o w '?: N• * ^, � 0.5 o �, 0 N' w TICN mg/kg 49000 Z % =+ > aro o mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (]bs/acre) Name of CropType YP Receiving Residual Application pp Crop 1 Crop 2 Crop 1 Crop 2 4/6 0.274 WQ0000672 0 1 S 0.3 r13000 110 1 9.556 9.556 0.000 0.000 0.000 0.006-, 0.000 , 0.000. 0.000 0.000 0.000 0.000' 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS: 01 229400 0.274 9.556 9.556 "I certify, under penalty of law, that this document was prepared -under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, 'including' the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (SUPP) (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-28-2 Acres Utilized: 56.9 Land Owner: Robert Baskerville Annual Dry Tons Applied: .60.73 10 Site #: 2 Acres Permitted: 56.9 Operator: Carnell Locklear Predominant Soil Series: Goldsboro GoA Cation Exchange Capacity (non 503): Crop 1 Name: Corn Crop 1 Max. PAN: 147 Crop 2 Name: Crop 2 Max. PAN: ° ° a 3 ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons 31000 J % Solids 2.7 Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert.; Animal Waste, etc) Soil (Dry' Wet, Moist Precip. Past.24 Hrs. inches 10 0 b .. o * o _ ] R _ _ * N' * ? r, * N * d TKN mg/kg 53000 4 > o � o0 0 ro' mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbslacre) Name of Crop Type Receiving Residual Application Crop 1 . Crop 2 Crop 1 Crop 2 3/2 6.061 -WQ0000672 Dry 0 S 0.5 0.3 6200 94 1 2.114 2.114 3/3 105400 2.7 0:209 WQ0000672 Dry 0 _ S 0.5 0.3 53000 6200 94 7.189 7.189 3/4 18600 2.7 �0.037° W00000672 Dry 0 S 0.5 0.3 53000 6200 94 1.269 1.269 3/10 68200 2.7 0.135 W00000672 Dry 0 S .0.5 0.3 53000 6200 94 4.651 4.651 3/11 55800 2.7 0.110. " W00000672 Dry 0 S 0.5 0.3 53000 6200, 94 3.806' 3:806 3/12 43400 136400 2.7 0.086 '. WQ0000672 Dry 0 S 0.5 0.3 53000 6200 94 .2.960 2.960 . 3/16 2.7 0.270. W00000672 , Dry 0 S 0.5 0.3 -53000 6200 94 9.303' 9.303 3/19 80600 2.7 .0 159 - W00000672 Dry 0 S 0.5 0.3 53000 6200 94 5.497, 5.497. 0.000. " ' . 0.000, 0.000 0.000-. 0.000 0.000 0.000 0.000 0.000, 0:000 . '0'.000 "0'000 -0 :0 .. __ 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 D.000 .............................. TOTALS Q1 539400 ...........AS Cd Cu Cr Pb H Mo Ni Se Zn P 36.789 36.789 Lime Applied_ Annual lbs/acre 0.026 0.001 0.869 0.000 0.046 0.004 0.017 0.084 0.033 1.453 0.201 ", . ::: Date lbs/ac Prior Years Cumulative lbs/ac 0.617 0.084 0.033 1453 ...::......... Current Cumulative lbs/ac 0.026 . 0.001 0.869, 0.000 0.046 0.004 Permitted C. P. L: R.**** Permit PAN Limit Ist/2nd Crop 14T . - "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and. evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations," *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate:. Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field M NC-RO-21-2A Acres Utilized: 38.4 Land Owner: Fannie Oxendine Annual Dry Tons Applied:,6.2825 Site #: 2A Acres Permitted: 38.4 Operator-: Lacy Cummings Predominant Soil Series: NoA- Norfolk Cation Exchange Capacity.(non 503):, Crop 1 Name: Soybeans Crop 1 Max. PAN: 164 Crop 2 Name: Crop 2 Max. PAN: o y G o A 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre - (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Co,nd. (Dry, Wet Moist Precip. Past 24 - inches a d r� �. p o � o m �' _ * °a . 70. 5' m `D * .P- * * °a TKN mg/kg . 14000 Z = R . o 9 °�° a a E• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 . Crop 1 Crop 2 2/4 18600 2.7 1 0.055. W00000672 Dry 1 0 S 0.5 0.3 6200 94 0.604 0.604 2/27 6200 2.7 -0.018 WQ0000672 Dry 0 S • ' 0.5 0.3 14000 6200 94 0.201 0.201 2/28 31000 2.7 0.091, WQ0000672 'Dry 0 S 0.5 0.3 14000 6200 94 1.006 1.006'. 0:000 0.000 , 0.000 0.000 ' 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 . 0.000`. 0.000 0.000 0.000. 0.000 -,0.000 . '0.000,- 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0: 0 0.000 . -. Residuals Applications totals on FORM FSF supp (.attach FORM FSF supp to this form): 0.600 0.000 TOTALS ' 0 - '55800 ....,;.-. As Cd. Cu Cr Pb Ha Mo Ni Se -Zn P 1.811 1.811 Lime Applied Annual lbs/acre 0.004 0.000 0.133 0.000 0.007 0.001 0.003 0.013 0.005 0.223 0.031 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0:004 0.000 0.133 0.000 0.007 0.001 0.003 0.013 . -0.005 0.223 Permitted C. P. L. R.**** Permit PAN Limit l st/2nd Crop 144, 9 certify, under penalty of law, that this document was prepared undermy direction or supervisionlin accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fiaes and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P:L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: WQ0000672 Field #: NC-RO-20-14 Acres Utilized: 10.6 Land Owner: Taylco, Inc Annual Dry, Tons Applied: ,40.9527 Site #: 14 Acres Permitted: 10.6 Operator:- Ronald G. Hammonds Predominant Soil Series: GoA-Goldsboro Cation Exchange Capacity (non 503): Crop 1 Name: Corn Crop 1 Max. PAN: 147 Crop 2 Name: Crop 2 Max. PAN: ° ° ° A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/AC) Residual Sources NPDES #, W # ( Q Fert., Animal.. Waste, etc) Soil Cond. (Dry, Wet, Moist Precip. past 24 Hrs. inches a b o'• °a o o ?: io -- * � F ? * �. * N `�' °p TKN mg/kg z Y co o a �, mg/kg Nitrate and' Nitrite mg/kg PAN Applied (]bs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 1/8 31000 2.7 0.329 W00000672 Dry 0 S 0.5 0.3 53000 6200 94 11.349 11.349 4/7 217000 " 2.1 1.793 WQ0000672 Dry 0 S 0.5 0.3 490001 13000 110 62.422 62.422' 4/17 210800 2.1 1.741. WQ0000672. Dry 0 S 0.5 0.3 49000 13000 110 60,639 60.639 "0.000 _' 0.000 0.000 0.600 0.000 0.0001, 0.000 0.000 0,000 -.n nnn 0.000 .0.000 -- 0.000. 0.000 0.000 • 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000"0.000 :.. TOTALS -01 458800 ...... As Cd Cu Cr Pb Hg Mo Ni Se - Zn P 134.410 134.410 Lime Applied Annuallbs/acre 0.011. 0.001 2.219 1.762 0.154 0.001 0.056 0.318 0.012 4.781 124.274 Date lbs/ac Prior Years Cumulative lbs/ac ... Current Cumulative lbs/ac 0.011 0.001 2.219 1.762 0.154 0.001 0.056 0.318 0.012 4.781 Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop 147. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 r ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton . WQ Permit #: WQ0000672 Field #: NC-RO-39-09 Acres Utilized: 62.5 Land Owner: Tracy Bullard Annual Dry Tons Applied: i307.1455 Site #: 9 Acres Permitted: 6i5 Operator: Tracy Bullard Predominant Soil Series: WaB-Wagram Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Crop I Max. PAN: 192 Crop 2 Name: Crop 2 Max. PAN: '� a) q c�a o Q Volume applied enter one Solids/ ( ) Liquid 9 Cu. Yds Gallons o /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources NPDES # W # ( Q Fert., Animal Waste, etc) SO1l Cond. (Dry' Wet, Moist Precip. . Past 24 Hrs.. inches y b Er o ° o � o w N' * °= o g * ~ * K• °a TIiN mg/kg 53000 z `{ a°c o `D o o mg/kg Nitrate and Nitrite mg/kg PAN Applied PP ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 3/29 285200 2.7 1, 0.M4,.. W00000672 Dry 0 S 0.5 0.3 6200 1 94 17.709- 17.709 3/30 186000 2.7 0.335 WQ0000672 Dry 0 S 0.5 0.3 53000 6200 94 11.549 11.549 6/2/2020 12400 2.1 .0.017 W00000672 Dry 0 S 0.5 0.3 49000 13000 110 0.605 - .0.605 6/3/2020 322400 2.1 0.452 WQ0000672 Dry 0 S 0.5 0.1 49000 13060 110 115.729 15.729 6/4/2020 434000 2.1 ' 0.608 W00000672, Dry 0 S 0.5 0.3 ]-49000 13000 110 ; 21.174 21.174 6/5/2020 105400 2.1 0.148 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 5.1.42 5.142 6/8/2020 55800 2.1 0.078 W00000672 Dry 0 S 0.5 0.3 49000 13000 110 -.2.722 2.722 6/9/2020 192200 2.1 0.269 W00000672 Dry 0 S 0.5 0.3 49000 13000 110 9.377 9.377 6/10/2020 260400' 2.1, ' ." 0.365., WQ0000672 Dry 0 S - : 0.5 0.3 49000. 13000 110 12.704 • 12.704 6/11/2020 117800 2.1 0.165 WQ0000672 .Dry 0 S 0.5 0.3 490,00 13000 Ito 5.747 5.747 6/19/2020 297600 2.1 0.417, W00000672 Dry 0 S 0.5 0.3 1 490001 13000 110 , 14.519 14.519 6/22/2020 173600 2.1 0.243 ' WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 8.469, '8.469 0 930000 1.303 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): -45.372 45 372 .. TOTALS. 01 ........... As Cd Cu Cr Pb Hg Mo Ni Se Zn P 170.818 170.818 Lime A plied Annuallbs/acre 0.024 0.001 2.935 1.854 0.198 0.003 0.072 0.403 0.029 6.140 130.240 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac 0.024 0.001 2.935 '1.854 -0.198, 0.003 .0.072 '0.403 0.029 .6.140 Permitted C. P. L. R.****" Permit PAN Limit 1st/2nd Crop -. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed, to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations ` *Application Method: S - Surface, IN - Injection; INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/incorporation -1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.-: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM Supplemental Information PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Lumberton WQ Permit #: W00000672 Field #: NC-RO-39-09 Acres Utilized: '.62.5 Land Owner: Tracy Bullard -Annual Dry Tons Applied:,307.14552 Site #: 9 Acres Permitted:'62.5 Operator: Tracy Bullard Predominant Soil Series:. WaB-Wagram Cation Exchange Capacity (non 503): Crop 1 Name: Bermuda Crop 1 Max. PAN: 192.00 Crop 2 Name:' Crop 2 Max PAN: ° N q p QSolids Volume applied (enter one) Cu. Yds Gallons % Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist Precip. Past 24 Hrs. inches �y �: d a 0' o ° o �, w _. co * N' F. ;v w ?' co N a TKN mg/kg 49000 Z > = o as o m o w• mg/kg Nitrate and - Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 /23/2020 186000 2.1 0.261 WQ0000672 Dry 0 S 0.5 0.3 13000 1 110 9.074 9.074 /24/2020 179800 2.1 0.252 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 8.772 8.772 /27/2020 192200 2.1 0.269 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 9.377 , 9.377, /28/2020 186000 2.1 0.261 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 9.074 9.074 /30/2020 186000 2.1 0.261 WQ0000672 Dry 0 S 0.5 0.3 49000 13000 110 9.074 9.674 0.000 0.000 0.000 0.000 0.000 0000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS: 0 930000 1.303 "' '' ' ' 45.372 . 45.372 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate DENR'FORM FSF (SUPP) (12/2006) Barber; Jim From: envirochoicenc@gmail.com Sent: Friday, July 31, 2020 4:23 PM To: Barber, Jim Cc: Honeycutt, Tony; 'Eric Locklear'; Allen, Trent, 'Matthew Markus'; cwalters@ci.lumberton.nc.us; 'Carrigan Harris'; Thornburg, Nathaniel Subject: RE: [External] Adding Fields to City of Lumberton Attachments: Dry tons and Total Gallons.pdf, All Fields.pdf Mr. Barber, Per previous emails the ORC was confirmed to be updated. Attached are the loading sheets for each field including what is planted. I have also attached an sheet which has all of the dry ton limits and total gallons thus far. Rlease let us know.if you need anything additional, 40 "NV - E Michael "Cody" Hunt President Enviro-Choice Recycling, LLC P.O. Box 390 Lumberton, NC 283S9 0: (910) 738-5311 F. (866) 768-8016 envirochoicenc@smail.com From: Barber, Jim <jim.barber@ncdenr.gov> Sent: Tuesday, July 28, 2020 12:11 PM To: envirochoicenc@gmail.com Cc: Honeycutt, Tony <tony.honeycutt@ncdenr.gov>; 'Eric Locklear' <etiocklear@gmail.com>; Allen, Trent <trent.allen@ncdenr.gov>;'Matthew Markus' <heamarkus@gmail.com>; cwalters@ci.lumberton.nc.us;'Carrigan Harris' <heacharris@gmail.com>; rarmstrong@ci.lumberton.nc.us; Thornburg, Nathaniel <nathaniel.thornburg@ncdenr.gov> Subject: RE: [External] Adding Fields to City of Lumberton Cody Hunt; Trent, Tony and I could be available for a conference call at 2pm this afternoon. If this time works, call Trent's office number at 910-433-3336. If 2pm this afternoon doesn't work, then propose a time for tomorrow and we'll try and make it work. If you are the ORC for the Lumberton land application program (our database currently has Nate Roth as the ORC with no Back Up ORC listed); we need some information concerning the exceedance of the dry ton limit in the current permit. Provide the following information for review: '