NCG030027_DMR_20200323

, N
• Scott K. Bailey
Plant Director
[phone] (phone)
[phone] (fax)
scottkbailey(a,eaton.com
R E F l\'r r.
March 23, 2020
APR 0 6 2020
Division of Water Quality
1617 Mail Service Center CENTRAL FILES
Raleigh, North Carolina 27699-1617 DER S CT;pf,�
Attn: DWQ Central Files
RE: March 2020 Monthly Tier Ill Discharge Monitoring Report
Attached are the analytical results and associated chain of custody for the March 3, 2020, monthly Tier III
stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater
General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility.
Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North
Carolina Division of Water Quality (NCDWQ).
I certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with the system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,
or other persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violations.
Sincerely,
Scott K. Bailey
Plant Director
Attachments

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted 03/23/2020
CERTIFICATE OF COVERAGE NO. NCGO3 0 0 2 7 SAMPLE COLLECTION YEAR 2020
FACILITY NAME Eaton Corporation SAMPLE PERIOD ®Jan-June fl July-Dec
COUNTY Person County or E Monthly'. March (month)
PERSON COLLECTING SAMPLES Colin Betchan DISCHARGING TO CLASS ❑ORW fHQW I 'Trout ❑PNA
LABORATORY Pace National Lab Cert.# ENV375/DW21704/BI0041 (Zero-flow nWater Supply fSA
Comments on sample collection or analysis: nOther ws-Ili;NSW
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -*
Part A: Stormwater Benchmarks and Monitoring Results
No discharge this period?'
Non-Polar O&G/
Date Sample 24-hour rainfall pH, Total Toxic
Outfall No. Collected) amount, Total Suspended Solids Standard units Total Copper Total Lead Total Zinc Total Petroleum Organics
(mo/dd/yr) Inches3 Hydrocarbons
Benchmarks - - 100 mg/L or 50 mg/L4 6.0—9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L
Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141
Tool Room Trench(005) 03/03/20 0.13 2.67 7.8 0.00700 0.00200 0.00340 0.843 0.03304
1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit, Section B,Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor
manufacture use the definition as found in 40 CFR 469.12;for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver,the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott K. Bailey
Name(Print name)
Plant Director
Title(Print title)
,g71 Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non-detect, ND, or other similar non-numerical
format. When results are below the applicable limits,they must be reported in the format, "<XX mg/I.", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month.
No discharge this period?'
Outfall No. Date Sample Collected' 24-hour rainfall amount, New Motor Oil or Non-Polar O&G/Total Total Suspended
(mo/dd/yr) Inches' Hydraulic Oil Usage Petroleum Hydrocarbons Solids
Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4
Parameter Code - 46529 NCOIL 00552 C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO❑
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES❑ NO❑
REGIONAL OFFICE CONTACT NAME: Danny Smith
Mail an original copy of this DMR, including all"No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period in the
case of"No Discharge"reports)to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate,and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee bate
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3

aceAnalytical® A \ A L Y T I C A L R I— S O R T ,
— National Center for Testing&Innovation March 11, 2020 p
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Eaton Corporation
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Sample Delivery Group: L1195680
Samples Received: 03/05/2020 5Sr
Project Number: 28091-R
6
Description: Eaton Corp Monthly Stormwater Qc
Site: ROXBORO, NC 7
GI
Report To: Dustin LeClair
2564 Durham Road Al
Roxboro, NC 27573
9
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Entire Report Reviewed By: ()
Heather J Wagner
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
• reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace ` '
4`° Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the Information provided,
and as the samples are received.
II
411 vow) iii
•
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE.

TABLE OF CONTENTS ONE LAB.NATIONWIDE. it
Cp:Cover Page 1
Cp
Tc:Table of Contents 2
Ss:Sample Summary 3
III
Cn:Case Narrative 4
Sr:Sample Results 5 3SS
2020-03-03-005 L1195680-01 5
4Cn
Qc:Quality Control Summary 9
Gravimetric Analysis by Method 2540 D-2011 9 5Sr
Wet Chemistry by Method 1664B 10
6
Metals(ICP) by Method 200.7 11 Qc
Volatile Organic Compounds(GC/MS)by Method 624.1 12
GI
Pesticides(GC) by Method EPA 608.3 14
Polychlorinated Biphenyls(GC)by Method EPA-608.3 16 6AI
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 17
9
GI:Glossary of Terms 22 Sc
Al:Accreditations& Locations 23
Sc:Sample Chain of Custody 24
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

SAMPLE SUMMARY ONE LAB.NATIONWIDE. .111
Collected by Collected date/time Received date/time
2020-03-03-005 L1195680-01 WW Cohn Betchan 03/03/20 16:16 03/05/20 08:30 LE_
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Gravimetric Analysis by Method 2540 D-2011 WG1440134 1 03/08/2012:22 03/08/2015:01 TH Mt.Juliet,TN
Wet Chemistry by Method 1664B WG1440691 1 03/09/20 06:46 03/09/20 23:19 MBP Mt.Juliet,TN IIMetals(ICP)by Method 200.7 WG1438221 1 03/05/2016:20 03/08/20 23:27 CCE Mt.Juliet,TN
Volatile Organic Compounds(GC/MS)by Method 624.1 WG1439275 1 03/06/2016:30 03/06/2016:30 ADM Mt.Juliet,TN
Pesticides(GC)by Method EPA 608.3 WG1439046 1 03/06/2015:11 03/07/20 08:55 HMH Mt.Juliet,TN 4Cn
Polychlorinated Biphenyls(GC)by Method EPA-608.3 WG1439046 1 03/06/2015:11 03/07/2011:04 MTJ Mt.Juliet,TN
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 WG1440652 1.01 03/09/2017:09 03/10/20 05:59 SHG Mt.Juliet,TN
5Sr
6
Q(
7GI
aAI
9Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

CASE NARRATIVE ONE LAB.NATIONWIDE.
Cp
All sample aliquots were received at the correct temperature, in the proper containers,with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within 2
the report. Where applicable, all MDL(LOD) and RDL(LOQ)values reported for environmental samples TC
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative,a non-conformance form
or properly qualified within the sample results.By my digital signature below, I affirm to the best of my 3Ss
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
5Sr
6QC
7GI
Heather J Wagner 8Al
Project Manager
9
SC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

2020-03-03-005 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. lit
Collected date/time: 03/03/20 16:16 L1195680
Additional Information
Result Units Cp
Analyte
z
pH(On Site) 7.8 su TC
Temperature(on-site) 13.4 Deg.C
3Ss
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier MDL RDL Dilution Analysis Batch a
Analyte mg/I mg/1 mg/I date/time Cn
Suspended Solids 2.67 J 0.585 4.18 1 03/08/202015:01 WG1440134
ill
Wet Chemistry by Method 1664B
6
Result Qualifier MDL RDL Dilution Analysis Batch Qc
Analyte mg/I mg/1 mg/1 date/time
TPH-Oil&Grease U 0.843 5.81 1 03/09/2020 23:19 WG1440691 7GI
Metals (ICP) by Method 200.7 8
Result Qualifier MDL RDL Dilution Analysis Batch Al
Analyte mg/I mg/I mg/I date/time
9
Copper U 0.00700 0.0100 1 03/08/2020 23:27 WG1438221 SC
Lead U 0.00200 0.00500 1 03/08/2020 23:27 WG1438221
Zinc 0.0290 J 0.00340 0.0500 1 03/08/2020 23:27 WG1438221
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/1 mg/1 date/time
Acrolein U 0.00887 0.0500 1 03/06/202016:30 WG1439275
Acrylonitrile U 0.00187 0.0100 1 03/06/202016:30 WG1439275
Benzene U 0.000331 0.00100 1 03/06/202016:30 WG1439275
Bromodichloromethane U 0.000380 0.00100 1 03/06/202016:30 WG1439275
Bromoform U 0.000469 0.00100 1 03/06/202016:30 WG1439275
Bromomethane U 0.000866 0.00500 1 03/06/202016:30 WG1439275
Carbon tetrachloride U 0.000379 0.00100 1 03/06/202016:30 WG1439275
Chlorobenzene U 0.000348 0.00100 1 03/06/202016:30 WG1439275
Chlorodibromomethane U 0.000327 0.00100 1 03/06/202016:30 WG1439275
Chloroethane U 0.000453 0.00500 1 03/06/202016:30 WG1439275
2-Chloroethyl vinyl ether U 0.00301 0.0500 1 03/06/202016:30 WG1439275
Chloroform U 0.000324 0.00500 1 03/06/202016:30 WG1439275
Chioromethane U 0.000276 0.00250 1 03/06/202016:30 WG1439275
1,2-Dichlorobenzene U 0.000349 0.00100 1 03/06/202016:30 WG1439275
1,3-Dichlorobenzene U 0.000220 0.00100 1 03/06/202016:30 WG1439275
1,4-Dichlorobenzene U 0.000274 0.00100 1 03/06/202016:30 WG1439275
Dichlorodifluoromethane U 0.000551 0.00500 1 03/06/202016:30 WG1439275
1,1-Dichloroethane U 0.000259 0.00100 1 03/06/202016:30 WG1439275
1,2-Dichloroethane U 0.000361 0.00100 1 03/06/202016:30 WG1439275
1,1-Dichloroethene U 0.000398 0.00100 1 03/06/202016:30 WG1439275
trans-1,2-Dichloroethene U 0.000396 0.00100 1 03/06/202016:30 WG1439275
1,2-Dichloropropane U 0.000306 0.00100 1 03/06/202016:30 WG1439275
cis-1,3-Dichloropropene U 0.000418 0.00100 1 03/06/202016:30 WG1439275
trans-1,3-Dichloropropene U 0.000419 0.00100 1 03/06/202016:30 WG1439275
Ethylbenzene U 0.000384 0.00100 1 03/06/202016:30 WG1439275
Methylene Chloride U 0.00100 0.00500 1 03/06/202016:30 WG1439275
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 03/06/202016:30 WG1439275
Tetrachloroethene U 0.000372 0.00100 1 03/06/202016:30 WG1439275
Toluene U 0.000412 0.00100 1 03/06/202016:30 WG1439275
1,1,1-Trichloroethane U 0.000319 0.00100 1 03/06/202016:30 WG1439275
1,1,2-Trichloroethane U 0.000383 0.00100 1 03/06/202016:30 WG1439275
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

2020-03-03-005 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. ak
Collected date/time: 03/03/20 16:16 L1195680
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
Trichloroethene U 0.000398 0.00100 1 03/06/2020 16:30 WG1439275 2
Tc
Trichlorofluoromethane U 0.00120 0.00500 1 03/06/2020 16:30 WG1439275
Vinyl chloride U 0.000259 0.00100 1 03/06/2020 16:30 WG1439275 s
(S)Toluene-d8 101 80.0-120 03/06/2020 16:30 WG1439275 SS
(S)4-Bromofluorobenzene 95.3 80.0-120 03/06/2020 16:30 WG1439275
(S)1,2-Dichloroethane-d4 105 70.0-130 03/06/202016:30 WG1439275 4Cn
Pesticides (GC) by Method EPA 608.3
111
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
6
Aldrin U 0.00000813 0.0000500 1 03/07/2020 08:55 WG1439046 Qc
Alpha BHC U 0.0000166 0.0000500 1 03/07/2020 08:55 WG1439046
Beta BHC U 0.0000184 0.0000500 1 03/07/2020 08:55 WG1439046 7G1
Delta BHC U 0.0000197 0.0000500 1 03/07/2020 08:55 WG1439046
Gamma BHC U 0.0000176 0.0000500 1 03/07/2020 08:55 WG1439046 8
Chlordane U 0.0000977 0.000500 1 03/07/2020 08:55 WG1439046 Al
4,4-DDD U 0.0000170 0.0000500 1 03/07/2020 08:55 WG1439046
4,4-DDE U 0.0000164 0.0000500 1 03/07/2020 08:55 WG1439046 9
SC
4,4-DDT U 0.0000177 0.0000500 1 03/07/2020 08:55 WG1439046
Dieldrin U 0.00000751 0.0000500 1 03/07/2020 08:55 WG1439046
Endosulfan I U 0.0000179 0.0000500 1 03/07/2020 08:55 WG1439046
Endosulfan II U 0.0000176 0.0000500 1 03/07/2020 08:55 WG1439046
Endosulfan sulfate U 0.0000196 0.0000500 1 03/07/2020 08:55 WG1439046
Endrin U 0.0000189 0.0000500 1 03/07/2020 08:55 WG1439046
Endrin aldehyde U 0.0000142 0.0000500 1 03/07/2020 08:55 WG1439046
Endrin ketone U 0.0000170 0.0000500 1 03/07/2020 08:55 WG1439046
Heptachlor U 0.0000108 0.0000500 1 03/07/2020 08:55 WG1439046
Heptachlor epoxide U 0.0000175 0.0000500 1 03/07/2020 08:55 WG1439046
Hexachlorobenzene U 0.0000134 0.0000500 1 03/07/2020 08:55 WG1439046
Methoxychlor U 0.0000193 0.0000500 1 03/07/2020 08:55 WG1439046
Toxaphene U 0.000168 0.000500 1 03/07/2020 08:55 WG1439046
(S)Decachlorobipheny/ 94.9 10.0-144 03/07/2020 08:55 WG1439046
(S)Tetrachloro-m-xylene 72.0 10.0-135 03/07/2020 08:55 WG1439046
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
PCB 1016 U J4 0.000100 0.000500 1 03/07/2020 11:04 WG1439046
PCB 1221 U 0.0000730 0.000500 1 03/07/2020 11:04 WG1439046
PCB 1232 U 0.0000420 0.000500 1 03/07/2020 11:04 WG1439046
PCB 1242 U 0.0000470 0.000500 1 03/07/2020 11:04 WG1439046
PCB 1248 U 0.0000860 0.000500 1 03/07/2020 11:04 WG1439046
PCB 1254 U 0.0000470 0.000500 1 03/07/2020 11:04 WG1439046
PCB 1260 U 0.000120 0.000500 1 03/07/2020 11:04 WG1439046
(S)Decachlorobipheny/ 86.4 10.0-144 03/07/202011:04 WG1439046
(S)Tetrachloro-m-xylene 91.0 10.0-135 03/07/2020 11:04 WG1439046
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Acenaphthene U 0.000319 0.00101 1.01 03/10/2020 05:59 WG1440652
Acenaphthylene U 0.000312 0.00101 1.01 03/10/2020 05:59 WG1440652
Anthracene U 0.000294 0.00101 1.01 03/10/2020 05:59 WG1440652
Benzidine U 0.00436 0.0101 1.01 03/10/2020 05:59 WG1440652
Benzo(a)anthracene U 0.0000985 0.00101 1.01 03/10/2020 05:59 WG1440652
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

2020-03-03-005 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. API
Collected date/time: 03/03/20 16:16 L1195680
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/1 mg/I date/time
Benzo(b)fluoranthene U 0.0000905 0.00101 1.01 03/10/2020 05:59 WG1440652 2
Tc
Benzo(k)fluoranthene U 0.000359 0.00101 1.01 03/10/2020 05:59 WG1440652
Benzo(g,h,i)perylene U 0.000163 0.00101 1.01 03/10/2020 05:59 WG1440652 3
Benzo(a)pyrene U 0.000343 0.00101 1.01 03/10/2020 05:59 WG1440652 SS
Bis(2-chlorethoxy)methane U 0.000332 0.0101 1.01 03/10/2020 05:59 W61440652
Bis(2-chloroethyl)ether U 0.00164 0.0101 1.01 03/10/2020 05:59 WG1440652 4Cn
2,2-Oxybis(1-Chloropropane) U 0.000449 0.0101 1.01 03/10/2020 05:59 WG1440652
4-Bromophenyl-phenylether U 0.000338 0.0101 1.01 03/10/2020 05:59 WG1440652
2-Chloronaphthalene U 0.000333 0.00101 1.01 03/10/2020 05:59 WG14406521111
4-Chlorophenyl-phenylether U 0.000306 0.0101 1.01 03/10/2020 05:59 WG1440652
Chrysene U 0.000335 0.00101 1.01 03/10/2020 05:59 WG1440652 6
QC
Dibenz(a,h)anthracene U 0.000282 0.00101 1.01 03/10/2020 05:59 WG1440652
3,3-Dichlorobenzidine U 0.00204 0.0101 1.01 03/10/2020 05:59 WG1440652 7
2,4-Dinitrotoluene U 0.00167 0.0101 1.01 03/10/2020 05:59 WG1440652 GI
2,6-Dinitrotoluene U 0.000282 0.0101 1.01 03/10/2020 05:59 WG1440652
1,2-Diphenylhydrazine U 0.000321 0.0101 1.01 03/10/202005:59 WG1440652 8A1
Fluoranthene U 0.000313 0.00101 1.01 03/10/2020 05:59 WG1440652
Fluorene U 0.000326 0.00101 1.01 03/10/2020 05:59 WG1440652 9
Hexachlorobenzene U 0.000344 0.00101 1.01 03/10/2020 05:59 WG1440652 SC
Hexachloro-1,3-butadiene U 0.000332 0.0101 1.01 03/10/2020 05:59 WG1440652
Hexachlorocyclopentadiene U 0.00235 0.0101 1.01 03/10/2020 05:59 WG1440652
Hexachloroethane U 0.000369 0.0101 1.01 03/10/2020 05:59 WG1440652
Indeno(1,2,3-cd)pyrene U 0.000282 0.00101 1.01 03/10/2020 05:59 WG1440652
Isophorone U 0.000275 0.0101 1.01 03/10/2020 05:59 WG1440652
Naphthalene U 0.000376 0.00101 1.01 03/10/2020 05:59 WG1440652
Nitrobenzene U 0.000371 0.0101 1.01 03/10/2020 05:59 WG1440652
n-Nitrosodimethylamine U 0.00127 0.0101 1.01 03/10/2020 05:59 WG1440652
n-Nitrosodiphenylamine U 0.00120 0.0101 1.01 03/10/2020 05:59 WG1440652
n-Nitrosodi-n-propylamine U 0.000407 0.0101 1.01 03/10/2020 05:59 WG1440652
Phenanthrene U 0.000370 0.00101 1.01 03/10/2020 05:59 WG1440652
Benzylbutyl phthalate U 0.000278 0.00303 1.01 03/10/2020 05:59 WG1440652
Bis(2-ethylhexyl)phthalate U 0.000716 0.00303 1.01 03/10/2020 05:59 WG1440652
Di-n-butyl phthalate U 0.000269 0.00303 1.01 03/10/2020 05:59 WG1440652
Diethyl phthalate U 0.000285 0.00303 1.01 03/10/2020 05:59 WG1440652
Dimethyl phthalate U 0.000286 0.00303 1.01 03/10/2020 05:59 WG1440652
Di-n-octyl phthalate U 0.000281 0.00303 1.01 03/10/2020 05:59 WG1440652
Pyrene U 0.000333 0.00101 1.01 03/10/2020 05:59 WG1440652
1,2,4-Trichlorobenzene U 0.000359 0.0101 1.01 03/10/2020 05:59 WG1440652
4-Chloro-3-methylphenol U 0.000266 0.0101 1.01 03/10/2020 05:59 WG1440652
2-Chlorophenol U 0.000286 0.0101 1.01 03/10/2020 05:59 WG1440652
2,4-Dichlorophenol U 0.000287 0.0101 1.01 03/10/2020 05:59 WG1440652
2,4-Dimethylphenol U 0.000630 0.0101 1.01 03/10/2020 05:59 WG1440652
4,6-Dinitro-2-methylphenol U 0.00265 0.0101 1.01 03/10/2020 05:59 WG1440652
2,4-Dinitrophenol U 0.00328 0.0101 1.01 03/10/2020 05:59 WG1440652
2-Nitrophenol U 0.000323 0.0101 1.01 03/10/2020 05:59 WG1440652
4-Nitrophenol U 0.00203 0.0101 1.01 03/10/2020 05:59 WG1440652
Pentachlorophenol U 0.000316 0.0101 1.01 03/10/2020 05:59 WG1440652
Phenol 0.000928 J 0.000337 0.0101 1.01 03/10/2020 05:59 WG1440652
2,4,6-Trichlorophenol U 0.000300 0.0101 1.01 03/10/2020 05:59 WG1440652
(S)2-Fluorophenol 35.9 10.0-120 03/10/2020 05:59 WG1440652
(S)Phenol-d5 25.1 8.00-424 03/10/2020 05:59 WG1440652
(S)Nitrobenzene-d5 570 15.0-314 03/10/2020 05:59 WG1440652
(S)2-F/uorobiphenyl 62.7 22.0-127 03/10/2020 05:59 WG1440652
(S)2,4,6-Tribromophenol 76.7 10.0-153 03/10/2020 05:59 WG1440652
(S)p-Terphenyl-d14 84.3 29.0-141 03/10/2020 05:59 WG1440652
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

2020-03-03-005 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE.
Collected date/time: 03/03/20 16:16 L1195680
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
Sample Narrative: 2
Tc
L1195680-01 WG1440652:Dilution due to sample volume.
3
Ss
4
Cn
6
Qc
7
GI
8
Al
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

WG1440134 QUALITY CONTROL SUMMARY
Gravimetric Analysis by Method 2540 D-2011 L1195680-01
Method Blank (MB)
(MB)R3506760-1 03/08/20 15:01
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Suspended Solids U 0.350 2.50
L1195703-01 Original Sample (OS) • Duplicate (DUP)
(OS)L1195703-01 03/08/20 15:01•(DUP)R3506760-3 03/08/20 15:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Suspended Solids 60.0 43.0 1 33.0 P1 5
L1195708-01 Original Sample (OS) • Duplicate (DUP)
(OS)L1195708-01 03/08/20 15:01•(DUP)R3506760-4 03/08/20 15:01
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/I mg/I % %
Suspended Solids 433 300 1 36.4 J3 5
Laboratory Control Sample (LCS)
(LCS)R3506760-2 03/08/20 15:01
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % %
Suspended Solids 773 808 105 85.0-115
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1440691 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 1664B L1195680-01
Method Blank(MB)
(MB)R3506903-1 03/09/20 23:19
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
TPH-Oil&Grease U 0.725 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)R3506903-2 03/09/20 23:19•(LCSD)R3506903-3 03/09/20 23:19
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/1 % % % % %
TPH-Oil&Grease 20.0 17.6 21.5 88.0 108 64.0-132 19.9 34
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1438221 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 200.7 L1195680-01
Method Blank(MB)
(MB)R3506577-1 03/08/20 22:12
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Copper U 0.00700 0.0100
Lead U 0.00200 0.00500
Zinc U 0.00340 0.0500
Laboratory Control Sample (LCS)
(LCS)R3506577-2 03/08/20 22:14
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % %
Copper 1.00 0.956 95.6 85.0-115
Lead 1.00 0.974 97.4 85.0-115
Zinc 1.00 0.976 97.6 85.0-115
L1195358-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1195358-01 03/08/20 22:17•(MS)R3506577-4 03/08/20 22:23•(MSD)R3506577-5 03/08/20 22:25
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier F
Analyte mg/I mg/I mg/I mg/1 % % %
Copper 1.00 ND 0.980 0.962 97.3 95.5 1 70.0-130 1
Lead 1.00 ND 1.01 0.989 101 98.9 1 70.0-130 2
Zinc 1.00 ND 1.03 1.00 101 97.7 1 70.0-130 2
L1195722-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1195722-01 03/08/20 22:28•(MS)R3506577-6 03/08/20 22:31•(MSD)R3506577-7 03/08/20 22:33
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier F
Analyte mg/I mg/ mg/I mg/ % % %
Copper 1.00 U 0.939 0.933 93.9 93.3 1 70.0-130 C
Lead 1.00 U 1.01 0.999 101 99.9 1 70.0-130 C
Zinc 1.00 0.103 1.08 1.07 97.7 96.8 1 70.0-130 C
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1439275 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 624.1 L1195680-01
Method Blank (MB)
(MB)R3506158-2 03/06/20 11:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Acrolein U 0.00887 0.0500
Acrylonitrile U 0.00187 0.0100
Benzene U 0.000331 0.00100
Bromodichloromethane U 0.000380 0.00100
Bromoform U 0.000469 0.00100
Bromomethane U 0.000866 0.00500
Carbon tetrachloride U 0.000379 0.00100
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500
2-Chloroethyl vinyl ether U 0.00301 0.0500
Chloroform U 0.000324 0.00500
Chloromethane U 0.000276 0.00250
1,2-Dichlorobenzene U 0.000349 0.00100
1,3-Dichlorobenzene U 0.000220 0.00100
1,4-Dichlorobenzene U 0.000274 0.00100
Dichlorodifluoromethane U 0.000551 0.00500
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
Methylene Chloride U 0.00100 0.00500
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
Toluene U 0.000412 0.00100
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
Trichlorofluoromethane U 0.00120 0.00500
Vinyl chloride U 0.000259 0.00100
(S)Toluene-d8 103 80.0-120
(S)4-Bromofuorobenzene 95.4 80.0-120
(S)1,2-Dichloroethane-d4 103 70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1439275 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 624.1 L119 5 6 80-01
Laboratory Control Sample (LCS)
(LCS)R3506158-1 03/06/20 10:28
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % %
Acrolein 0.0250 0.0168 67.2 60.0-140
Acrylonitrile 0.0250 0.0244 97.6 60.0-140
Benzene 0.00500 0.00477 95.4 65.0-135
Bromodichloromethane 0.00500 0.00479 95.8 70.0-135
Bromoform 0.00500 0.00440 88.0 70.0-130
Bromomethane 0.00500 0.00489 97.8 15.0-185
Carbon tetrachloride 0.00500 0.00463 92.6 70.0-130
Chlorobenzene 0.00500 0.00462 92.4 65.0-135
Chlorodibromomethane 0.00500 0.00449 89.8 70.0-135
Chloroethane 0.00500 0.00416 83.2 40.0-160
2-Chloroethyl vinyl ether 0.0250 0.0250 100 0.100-225
Chloroform 0.00500 0.00503 101 70.0-135
Chloromethane 0.00500 0.00372 74.4 0.100-205
1,2-Dichlorobenzene 0.00500 0.00481 96.2 65.0-135
1,3-Dichlorobenzene 0.00500 0.00471 94.2 70.0-130
1,4-Dichlorobenzene 0.00500 0.00452 90.4 65.0-135
Dichlorodifluoromethane 0.00500 0.00366 73.2 49.0-155
1,1-Dichloroethane 0.00500 0.00458 91.6 70.0-130
1,2-Dichloroethane 0.00500 0.00472 94.4 70.0-130
1,1-Dichloroethene 0.00500 0.00472 94.4 50.0-150
trans-1,2-Dichloroethene 0.00500 0.00469 93.8 70.0-130
1,2-Dichloropropane 0.00500 0.00463 92.6 35.0-165
cis-1,3-Dichloropropene 0.00500 0.00487 97.4 25.0-175
trans-1,3-Dichloropropene 0.00500 0.00468 93.6 50.0-150
Ethylbenzene 0.00500 0.00452 90.4 60.0-140
Methylene Chloride 0.00500 0.00480 96.0 60.0-140
1,1,2,2-Tetrachloroethane 0.00500 0.00494 98.8 60.0-140
Tetrachloroethene 0.00500 0.00485 97.0 70.0-130
Toluene 0.00500 0.00467 93.4 70.0-130
1,1,1-Trichloroethane 0.00500 0.00471 94.2 70.0-130
1,1,2-Trichloroethane 0.00500 0.00482 96.4 70.0-130
Trichloroethene 0.00500 0.00453 90.6 65.0-135
Trichlorofluoromethane 0.00500 0.00414 82.8 50.0-150
Vinyl chloride 0.00500 0.00430 86.0 5.00-195
(S)Toluene-d8 101 80.0-120
(S)4-Bromofuorobenzene 96.4 80.0-120
(S)1,2-Dichloroethane-d4 103 70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1439046 QUALITY CONTROL SUMMARY
Pesticides (GC) by Method EPA 608.3 L1195680-01
Method Blank(MB)
(MB)R3506716-1 03/07/20 08:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Aldrin U 0.00000813 0.0000500
Alpha BHC U 0.0000166 0.0000500
Beta BHC U 0.0000184 0.0000500
Delta BHC U 0.0000197 0.0000500
Gamma BHC U 0.0000176 0.0000500
4,4-DDD U 0.0000170 0.0000500
4,4-DDE U 0.0000164 0.0000500
4,4-DDT U 0.0000177 0.0000500
Dieldrin U 0.00000751 0.0000500
Endosulfan I U 0.0000179 0.0000500
Endosulfan II U 0.0000176 0.0000500
Endosulfan sulfate U 0.0000196 0.0000500
Endrin U 0.0000189 0.0000500
Endrin aldehyde U 0.0000142 0.0000500
Endrin ketone U 0.0000170 0.0000500
Heptachlor U 0.0000108 0.0000500
Heptachlor epoxide U 0.0000175 0.0000500
Hexachlorobenzene U 0.0000134 0.0000500
Methoxychlor U 0.0000193 0.0000500
Chlordane U 0.0000977 0.000500
Toxaphene U 0.000168 0.000500
(S)Decach/orobiphenyl 93.3 10.0-144
(S)Tetrach/oro-m-xylene 72.1 10.0-135
Laboratory Control Sample (LCS)
(LCS)R3506716-2 03/07/20 08:42
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % %
Aldrin 0.00100 0.000760 76.0 42.0-140
Alpha BHC 0.00100 0.000957 95.7 37.0-140
Beta BHC 0.00100 0.000923 92.3 17.0-147
Delta BHC 0.00100 0.000839 83.9 19.0-140
Gamma BHC 0.00100 0.000877 87.7 32.0-140
4,4-DDD 0.00100 0.000880 88.0 31.0-141
4,4-DDE 0.00100 0.000789 78.9 30.0-145
4,4-DDT 0.00100 0.00103 103 25.0-160
Dieldrin 0.00100 0.000875 87.5 36.0-146
Endosulfan I 0.00100 0.000903 90.3 45.0-153
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1439046 QUALITY CONTROL SUMMARY
Pesticides (GC) by Method EPA 608.3 L119 5 6 80-01
Laboratory Control Sample (LCS)
(LCS)R3506716-2 03/07/20 08:42
Spike Amount LCS Result LCS Rec. Rec.Limits LCS S Qualifier
Analyte mg/I mgA % %
Endosulfan II 0.00100 0.000905 90.5 1.00-202
Endosulfan sulfate 0.00100 0.000847 84.7 26.0-144
Endrin 0.00100 0.000908 90.8 30.0-147
Endrin aldehyde 0.00100 0.000932 93.2 56.0-128
Endrin ketone 0.00100 0.00127 127 54.0-142
Heptachlor 0.00100 0.000862 86.2 34.0-140
Heptachlor epoxide 0.00100 0.000889 88.9 37.0-142
Hexachlorobenzene 0.00100 0.000758 75.8 35.0-120
Methoxychlor 0.00100 0.00112 112 44.0-160
(S)Decachlorobiphenyl 82.6 10.0-144
(S)Tetrachloro-m-xylene 76.9 10.0-135
L1195839-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1195839-02 03/07/20 09:57•(MS)R3506716-3 03/07/20 10:09•(MSD)R3506716-4 03/07/20 10:22
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier F
Analyte mg/I mg/I mg/I mg/I % % %
Aldrin 0.00100 ND 0.000767 0.000698 76.7 69.8 1 42.0-140 c
Alpha BHC 0.00100 ND 0.000824 0.000740 82.4 74.0 1 37.0-140 1
Beta BHC 0.00100 ND 0.000886 0.000810 88.6 81.0 1 17.0-147 E
Delta BHC 0.00100 ND 0.000759 0.000669 75.9 66.9 1 19.0-140 1
Gamma BHC 0.00100 ND 0.000854 0.000797 85.4 79.7 1 32.0-140 E
4,4-DDD 0.00100 ND 0.000831 0.000765 83.1 76.5 1 31.0-141 E
4,4-DDE 0.00100 ND 0.000744 0.000672 74.4 67.2 1 30.0-145 1
4,4-DDT 0.00100 ND 0.000983 0.000906 98.3 90.6 1 25.0-160 E
Dieldrin 0.00100 ND 0.000818 0.000742 81.8 74.2 1 36.0-146 c
Endosulfan I 0.00100 ND 0.000879 0.000807 87.9 80.7 1 45.0-153 E
Endosulfan II 0.00100 ND 0.000866 0.000792 86.6 79.2 1 1.00-202 E
Endosulfan sulfate 0.00100 ND 0.000828 0.000768 82.8 76.8 1 26.0-144 7
Endrin 0.00100 ND 0.000946 0.000852 94.6 85.2 1 30.0-147 1
Endrin aldehyde 0.00100 ND 0.000876 0.000799 87.6 79.9 1 56.0-128 c
Endrin ketone 0.00100 ND 0.00120 0.00113 120 113 1 54.0-142 E
Heptachlor 0.00100 ND 0.000865 0.000779 86.5 77.9 1 34.0-140 1
Heptachlor epoxide 0.00100 ND 0.000779 0.000725 77.9 72.5 1 37.0-142 7
Hexachlorobenzene 0.00100 ND 0.000781 0.000709 78.1 70.9 1 35.0-120 c
Methoxychlor 0.00100 ND 0.000951 0.000909 95.1 90.9 1 44.0-160 4
(S)Decachlorobiphenyl 100 92.4 10.0-144
(S)Tetrach/oro-m-xy/ene 76.4 69.6 10.0-135
ACCOUNT: PROJECT: SDG: DATE/TIF
Eaton Corporation 28091-R L1195680 03/11/20 IC

WG1439046 QUALITY CONTROL SUMMARY
Polychlorinated Biphenyls (GC) by Method EPA-608.3 L1195680-01
Method Blank (MB)
(MB)R3506452-1 03/07/20 10:08
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
PCB 1260 U 0.000120 0.000500
PCB 1016 U 0.000100 0.000500
PCB 1221 U 0.0000730 0.000500
PCB 1232 U 0.0000420 0.000500
PCB 1242 U 0.0000470 0.000500
PCB 1248 U 0.0000860 0.000500
PCB 1254 U 0.0000470 0.000500
(S)Decachlorobiphenyl 78.8 10.0-144
(S)Tetrochloro-m-xylene 86.4 10.0-135
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS)R3506452-2 03/07/20 10:22•(LCSD)R3506452-3 03/07/20 10:36
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I % % % % %
PCB 1260 0.00250 0.00238 0.00231 95.2 92.4 8.00-140 2.99 38
PCB 1016 0.00250 0.00430 0.00429 172 172 50.0-140 J4 J4 0.233 36
(S)Decachlorobiphenyl 90.6 89.0 10.0-144
(S)Tetrachloro-m-xylene 93.0 9t2 10.0-135
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1440652 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1195680-01
Method Blank (MB)
(MB)R3507165-2 03/10/20 00:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/1 mg/I mg/I
Acenaphthene U 0.000316 0.00100
Acenaphthylene U 0.000309 0.00100
Anthracene U 0.000291 0.00100
Azobenzene U 0.000318 0.0100
Benzidine U 0.00432 0.0100
Benzo(a)anthracene U 0.0000975 0.00100
Benzo(k)fluoranthene U 0.0000896 0.00100
Benzo(k)fluoranthene U 0.000355 0.00100
Benzo(g,h,i)perylene U 0.000161 0.00100
Benzo(a)pyrene U 0.000340 0.00100
Bis(2-chlorethoxy)methane U 0.000329 0.0100
Bis(2-chloroethyl)ether U 0.00162 0.0100
2,2-Oxybis(1-Chloropropane) U 0.000445 0.0100
4-Bromophenyl-phenylether U 0.000335 0.0100
2-Chloronaphthalene U 0.000330 0.00100
4-Chlorophenyl-phenylether U 0.000303 0.0100
Chrysene U 0.000332 0.00100
Dibenz(a,h)anthracene U 0.000279 0.00100
3,3-Dichlorobenzidine U 0.00202 0.0100
2,4-Dinitrotoluene U 0.00165 0.0100
2,6-Dinitrotoluene U 0.000279 0.0100
Fluoranthene U 0.000310 0.00100
Fluorene U 0.000323 0.00100
Hexachlorobenzene U 0.000341 0.00100
Hexachloro-1,3-butadiene U 0.000329 0.0100
Hexachlorocyclopentadiene U 0.00233 0.0100
Hexachloroethane U 0.000365 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000272 0.0100
Naphthalene U 0.000372 0.00100
Nitrobenzene U 0.000367 0.0100
n-Nitrosodimethylamine U 0.00126 0.0100
n-Nitrosodiphenylamine U 0.00119 0.0100
n-Nitrosodi-n-propylamine U 0.000403 0.0100
Phenanthrene U 0.000366 0.00100
Benzylbutyl phthalate U 0.000275 0.00300
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300
Di-n-butyl phthalate U 0.000266 0.00300
Diethyl phthalate U 0.000282 0.00300
Dimethyl phthalate U 0.000283 0.00300
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1440652 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1195680-01
Method Blank(MB)
(MB)R3507165-2 03/10/20 00:55
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/I mg/I mg/I
Di-n-octyl phthalate U 0.000278 0.00300
Pyrene U 0.000330 0.00100
1,2,4-Trichlorobenzene U 0.000355 0.0100
4-Chloro-3-methylphenol U 0.000263 0.0100
2-Chlorophenol U 0.000283 0.0100
2,4-Dichlorophenol U 0.000284 0.0100
2,4-Dimethylphenol U 0.000624 0.0100
4,6-Dinitro-2-methylphenol U 0.00262 0.0100
2,4-Dinitrophenol U 0.00325 0.0100
2-Nitrophenol U 0.000320 0.0100
4-Nitrophenol U 0.00201 0.0100
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.000334 0.0100
2,4,6-Trichlorophenol U 0.000297 0.0100
(S)Nitrobenzene-d5 58.5 15.0-314
(S)2-Fluorobiphenyl 64.3 22.0-127
(S)p-Terphenyl-d14 75.0 29.0-141
(S)Phenol-d5 24.7 8.00-424
(S)2-Fluorophenol 39.2 10.0-120
(S)2,4,6-Tribromopheno/ 74.0 10.0-153
Laboratory Control Sample (LCS)
(LCS)R3507165-1 03/10/20 00:35
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % %
Acenaphthene 0.0500 0.0330 66.0 47.0-145
Acenaphthylene 0.0500 0.0360 72.0 33.0-145
Anthracene 0.0500 0.0354 70.8 27.0-133
Azobenzene 0.0500 0.0362 72.4 37.0-125
Benzidine 0.100 0.0293 29.3 1.00-120
Benzo(a)anthracene 0.0500 0.0372 74.4 33.0-143
Benzo(b)fluoranthene 0.0500 0.0389 77.8 24.0-159
Benzo(k)fluoranthene 0.0500 0.0383 76.6 11.0-162
Benzo(g,h,i)perylene 0.0500 0.0380 76.0 1.00-219
Benzo(a)pyrene 0.0500 0.0405 81.0 17.0-163
Bis(2-chlorethoxy)methane 0.0500 0.0303 60.6 1.00-219
Bis(2-chloroethyl)ether 0.0500 0.0307 61.4 33.0-185
2,2-Oxybis(1-Chloropropane) 0.0500 0.0317 63.4 36.0-166
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1440652 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1195680-01
Laboratory Control Sample (LCS)
(LCS)R3507165-1 03/10/20 00:35
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/ % %
4-Bromophenyl-phenylether 0.0500 0.0391 78.2 53.0-127
2-Chloronaphthalene 0.0500 0.0341 68.2 60.0-120
4-Chlorophenyl-phenylether 0.0500 0.0375 75.0 25.0-158
Chrysene 0.0500 0.0371 74.2 17.0-168
Dibenz(a,h)anthracene 0.0500 0.0411 82.2 1.00-227
3,3-Dichlorobenzidine 0.100 0.0767 76.7 1.00-262
2,4-Dinitrotoluene 0.0500 0.0373 74.6 39.0-139
2,6-Dinitrotoluene 0.0500 0.0363 72.6 50.0-158
Fluoranthene 0.0500 0.0376 75.2 26.0-137
Fluorene 0.0500 0.0363 72.6 59.0-121
Hexachlorobenzene 0.0500 0.0416 83.2 1.00-152
Hexachloro-1,3-butadiene 0.0500 0.0303 60.6 24.0-120
Hexachlorocyclopentadiene 0.0500 0.0309 61.8 10.0-120
Hexachloroethane 0.0500 0.0283 56.6 40.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0334 66.8 1.00-171
Isophorone 0.0500 0.0306 61.2 21.0-196
Naphthalene 0.0500 0.0283 56.6 21.0-133
Nitrobenzene 0.0500 0.0285 57.0 35.0-180
n-Nitrosodimethylamine 0.0500 0.0189 37.8 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0365 73.0 44.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0342 68.4 1.00-230
Phenanthrene 0.0500 0.0349 69.8 54.0-120
Benzylbutyl phthalate 0.0500 0.0386 77.2 1.00-152
Bis(2-ethylhexyl)phthalate 0.0500 0.0335 67.0 8.00-158
Di-n-butyl phthalate 0.0500 0.0393 78.6 1.00-120
Diethyl phthalate 0.0500 0.0373 74.6 1.00-120
Dimethyl phthalate 0.0500 0.0369 73.8 1.00-120
Di-n-octyl phthalate 0.0500 0.0337 67.4 4.00-146
Pyrene 0.0500 0.0376 75.2 52.0-120
1,2,4-Trichlorobenzene 0.0500 0.0287 57.4 44.0-142
4-Chloro-3-methylphenol 0.0500 0.0316 63.2 22.0-147
2-Chlorophenol 0.0500 0.0306 61.2 23.0-134
2,4-Dichlorophenol 0.0500 0.0313 62.6 39.0-135
2,4-Dimethylphenol 0.0500 0.0296 59.2 32.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0376 75.2 1.00-181
2,4-Dinitrophenol 0.0500 0.0351 70.2 1.00-191
2-Nitrophenol 0.0500 0.0305 61.0 29.0-182
4-Nitrophenol 0.0500 0.0170 34.0 1.00-132
Pentachlorophenol 0.0500 0.0461 92.2 14.0-176
Phenol 0.0500 0.0133 26.6 5.00-120
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1440652 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1195680-01
Laboratory Control Sample (LCS)
(LCS)R3507165-1 03/10/20 00:35
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/I % %
2,4,6-Trichlorophenol 0.0500 0.0341 68.2 37.0-144
(S)Nitrobenzene-d5 48.9 15.0-314
(S)2-Fluorobiphenyl 73.9 22.0-127
(S)p-Terphenyl-d14 82.4 29.0-141
(S)Phenol-d5 26.6 8.00-424
(S)2-Fluorophenol 41.5 10.0-120
(S)2,4,6-Tribromophenol 91.0 10.0-153
L1195777-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1195777-01 03/10/20 07:57•(MS)R3507165-3 03/10/20 08:17•(MSD)R3507165-4 03/10/20 08:38
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier F
Analyte mg/I mg/I mg/I mg/I % % % 5
Acenaphthene 0.0500 U 0.0292 0.0299 58.4 59.8 5 47.0-145 2
Benzidine 0.100 U ND ND 0.000 0.000 5 1.00-120 J6 J6 C
Acenaphthylene 0.0500 U 0.0309 0.0308 61.8 61.6 5 33.0-145 C
Anthracene 0.0500 U 0.0327 0.0333 65.4 66.6 5 27.0-133 1
Benzo(a)anthracene 0.0500 U 0.0348 0.0349 69.6 69.8 5 33.0-143 C
Benzo(b)fluoranthene 0.0500 U 0.0354 0.0364 70.8 72.8 5 24.0-159 2
Benzo(k)fluoranthene 0.0500 U 0.0336 0.0336 67.2 67.2 5 11.0-162 C
Benzo(g,h,i)perylene 0.0500 U 0.0336 0.0338 67.2 67.6 5 1.00-219 C
Benzo(a)pyrene 0.0500 U 0.0378 0.0376 75.6 75.2 5 17.0-163 C
1,2-Diphenylhydrazine 0.0500 U 0.0338 0.0338 67.6 67.6 5 18.0-156 C
Bis(2-chlorethoxy)methane 0.0500 U 0.0344 0.0344 68.8 68.8 5 33.0-184 C
Bis(2-chloroethyl)ether 0.0500 U 0.0276 0.0277 55.2 55.4 5 12.0-158 C
2,2-Oxybis(1-Chloropropane) 0.0500 U 0.0287 0.0282 57.4 56.4 5 36.0-166 1
4-Bromophenyl-phenylether 0.0500 U 0.0342 0.0355 68.4 71.0 5 53.0-127 3
2-Chloronaphthalene 0.0500 U 0.0303 0.0312 60.6 62.4 5 60.0-120 2
4-Chlorophenyl-phenylether 0.0500 U 0.0322 0.0337 64.4 67.4 5 25.0-158 4
Chrysene 0.0500 U 0.0333 0.0333 66.6 66.6 5 17.0-168 C
Dibenz(a,h)anthracene 0.0500 U 0.0358 0.0363 71.6 72.6 5 1.00-227 1
3,3-Dichlorobenzidine 0.100 U ND ND 0.000 0.000 5 1.00-262 J6 J6 C
2,4-Dinitrotoluene 0.0500 U 0.0333 0.0341 66.6 68.2 5 39.0-139 2
2,6-Dinitrotoluene 0.0500 U 0.0324 0.0331 64.8 66.2 5 50.0-158 2
Fluoranthene 0.0500 U 0.0342 0.0334 68.4 66.8 5 26.0-137 2
Fluorene 0.0500 U 0.0319 0.0323 63.8 64.6 5 59.0-121 1
Hexachlorobenzene 0.0500 U 0.0360 0.0362 72.0 72.4 5 1.00-152 C
Hexachloro-1,3-butadiene 0.0500 U 0.0293 0.0301 58.6 60.2 5 24.0-120 2
Hexachlorocyclopentadiene 0.0500 U 0.0206 0.0209 41.2 41.8 5 10.0-146 1
ACCOUNT: PROJECT: SDG: DATE/TI h
Eaton Corporation 28091-R L1195680 03/11/20 1C

WG1440652 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1195680-01
L1195777-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS)L1195777-01 03/10/20 07:57•(MS)R3507165-3 03/10/20 08:17•(MSD)R3507165-4 03/10/20 08:38
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier F
Analyte mg/I mg/I mg/I mg/I % % % F
Hexachloroethane 0.0500 U 0.0279 0.0272 55.8 54.4 5 40.0-120 2
Indeno(1,2,3-cd)pyrene 0.0500 U 0.0312 0.0321 62.4 64.2 5 1.00-171 2
Isophorone 0.0500 U 0.0333 0.0347 66.6 69.4 5 21.0-196 4
Naphthalene 0.0500 0.00378 0.0317 0.0320 55.8 56.4 5 21.0-133 C
Nitrobenzene 0.0500 U 0.0295 0.0307 59.0 61.4 5 35.0-180 3
n-Nitrosodimethylamine 0.0500 U 0.0437 0.0420 87.4 84.0 5 10.0-120 3
n-Nitrosodiphenylamine 0.0500 U 0.0340 0.0342 68.0 68.4 5 16.0-160 C
n-Nitrosodi-n-propylamine 0.0500 U 0.0681 0.0596 136 119 5 1.00-230 1.
Phenanthrene 0.0500 U 0.0321 0.0328 64.2 65.6 5 54.0-120 2
Benzylbutyl phthalate 0.0500 U 0.0397 0.0399 79.4 79.8 5 1.00-152 C
Bis(2-ethylhexyl)phthalate 0.0500 0.00707 0.0375 0.0383 60.9 62.5 5 8.00-158 2
Di-n-butyl phthalate 0.0500 U 0.0384 0.0383 76.8 76.6 5 1.00-120 C
Diethyl phthalate 0.0500 U 0.0349 0.0358 69.8 71.6 5 1.00-120 2
Dimethyl phthalate 0.0500 U 0.0340 0.0344 68.0 68.8 5 1.00-120 1
Di-n-octyl phthalate 0.0500 U 0.0394 0.0398 78.8 79.6 5 4.00-146 1
Pyrene 0.0500 U 0.0358 0.0369 71.6 73.8 5 52.0-120 3
1,2,4-Trichlorobenzene 0.0500 U 0.0281 0.0282 56.2 56.4 5 44.0-142 C
4-Chloro-3-methylphenol 0.0500 U 0.0556 0.0562 111 112 5 22.0-147 1
2-Chorophenol 0.0500 U 0.0296 0.0291 59.2 58.2 5 23.0-134 1
2,4-Dichlorophenol 0.0500 U 0.0318 0.0323 63.6 64.6 5 39.0-135 1
2,4-Dimethylphenol 0.0500 U 0.0462 0.0464 92.4 92.8 5 32.0-120 C
4,6-Dinitro-2-methylphenol 0.0500 U 0.0527 0.0539 105 108 5 1.00-181 2
2,4-Dinitrophenol 0.0500 U 0.0548 0.0551 110 110 5 1.00-191 C
2-Nitrophenol 0.0500 U 0.0316 0.0322 63.2 64.4 5 29.0-182 1
4-Nitrophenol 0.0500 U 0.0153 0.0162 30.6 32.4 5 1.00-132 c
Pentachlorophenol 0.0500 U 0.0630 0.0620 126 124 5 14.0-176 1
Phenol 0.0500 0.0827 0.0940 0.0873 22.6 9.20 5 5.00-120 7
2,4,6-Trichlorophenol 0.0500 U 0.0299 0.0313 59.8 62.6 5 37.0-144 4
(5)Nitrobenzene-d5 50.0 56.0 15.0-314
(S)2-F/uorobipheny/ 63.6 676 22.0-127
(S)p-Terphenyl-d14 79.0 82.5 29.0-141
(S)Phenol-d5 22.5 21.7 8.00-424
(S)2-Fluorophenol 40.4 40.6 10.0-120
(S)2,4,6-Tribromophenol 163 164 10.0-153 J1 J1
Sample Narrative:
OS:Surrogate failure due to matrix interference.Dilution due to matrix.
ACCOUNT: PROJECT: SDG: DATE/TIN
Eaton Corporation 28091-R L1195680 03/11/20 1C

GLOSSARY OF TERMS ONE LAB.NATIONWIDE. It
Guide to Reading and Understanding Your Laboratory Report C
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not Cp
intended as a comprehensive explanation,and if you have additional questions please contact your project representative.
Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, TC
Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and
Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received.
Abbreviations and Definitions 3Ss
MDL Method Detection Limit.
ND Not detected at the Reporting Limit(or MDL where applicable). Cn
RDL Reported Detection Limit.
Rec. Recovery.
RPD Relative Percent Difference. Sr
SDG Sample Delivery Group.
Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control Sample/Duplicate and 6 QC
(S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit(or MDL where applicable).
Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the a Ai
Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the
result reported has already been corrected for this factor. s
These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal SC
Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control
sample.The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was
no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL"
Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL
(Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results,including a discussion of any non-conformances to protocol
Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary Control analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not
being performed on your samples typically,but on laboratory generated material.
This is the document created in the field when your samples were initially collected.This is used to verify the time and
Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This
Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples.These results are provided
Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable;the reported value is an estimate.
J1 Surrogate recovery limits have been exceeded;values are outside upper control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination;spike value is low.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
ACCOUNT: PROJECT. SDG: DATE/TIME: PAGE:

ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE. .10
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other lab is as
accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the network 1
laboratories in our industry.The most significant benefit to our one location design is the design of our laboratory campus.The model is conducive to accelerated productivity,decreasing C p
turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
*Not all certifications held by the laboratory are applicable to the results reported in the attached report.
"Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. 2
Tc
State Accreditations
Alabama 40660 Nebraska NE-OS-15-05 3SS
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
FT4Arkansas 88-0469 New Jersey—NELAP TN002
California 2932 New Mexico' n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375 5 Sr
Florida E87487 North Carolina 1 DW21704
Georgia NELAP North Carolina 3 41
6
Georgia' 923 North Dakota R-140 Qc
Idaho TN00003 Ohio—VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002 7 GI
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LA000356
Kentucky'6 90010 South Carolina 84004 EAl
Kentucky 2 16 South Dakota n/a
Louisiana A130792 Tennessee'° 2006
Louisiana 1 LA180010 Texas T104704245-18-15 9 S c
Maine TN0002 Texas 6 LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Third Party Federal Accreditations
A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA—ISO 17025 5 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
'Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity `Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies.If you would like assistance from one of our support offices,please contact
our main office.Pace National performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

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Roxboro,NC 27573
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