NCG030466_DMR_20200520

Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCGO3 0 ti 6 6 SAMPLE COLLECTION YEAR °-2 O
FACILITY NAME ENTON (OR PO RAI ID NI SAMPLE PERIOD !Z Jan-June E July-Dec
COUNTY b U N ( 0 M 6 F or ® Monthly' (month)
PERSON COLLECTING SAMPLES kN A CI E c K CK 41-P U r E 1 °ARCING TO CLASS ❑ORW EHQW ❑Trout ❑PNA
LABORATORY PAC E AN#LyrrI A L Lab Cert.# I? 4 (40 ❑Zero-flow ❑Water Supply [—ISA
Comments on sample collection or anaIly�sis: ! JUN 0 'NZ° ❑Other
PALE AN A LY'f rCA L k Ind' e to ra 'd o q .�._...' • .T.S aM A
�, �/ i GC;4 i r:- PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
00 $ Ca--'(��-' Oo 3) due , wr avoir �a ►✓ 10'i ‘ owri a IO
Part A: Stormwater Benchmarks and Monitoring Results
❑ No discharge this period?2
Date Sample 24-hour rainfall pH, Non-Polar O&G/ Total Toxic
P
Outfall No. Total Suspended Solids Total Co
Collected' amount, Standard units Copper Total Lead Total Zinc Total Petroleum Organics'
(mo/dd/yr) Inches' Hydrocarbons
Benchmarks _ - 100 mg/L or 50 mg/L4 6.0—9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L
Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141
00( Lf'.2qo I.q1, 16.1 m /L 6' q 0.00Q314 .o.00s'lit. o.o11T+^rA. (o•ooS Nil)I- NA
002 it,zq..?o 1. q ,' q. 6 .vn1- I 6. g 4o•ooS4J/1- 0.005^i/l 0•03►'r.i1L <0•0o5 I NA
00 3 I-t..2,q.,20 1•4 a 6. q 40.00$ .."1 it (o•coS v140.03'53 •*dlt Go.oOS M^1IL, NA
00II Nt02(1.)o l. q" 21.,z ^l /L 6, 0.0osg7l4 <o.00c4) )L0• O19$1111. <o•ooS1IL AI
1 Monthly sampling(instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here.
3The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
'See General Permit, Section B,Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample(for metal finishing use the definition as found in 40 CFR 433.11;for semiconductor
manufacture use the definition as found in 40 CFR 469.12;for electronic crystal manufacture use the definition as found in 40 CFR 469.22;and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
\ok c1 \\t\V‘-ene
Name(Print nbme)
1-k S M o.vo3—sr-
Tjtle rint itle)
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non-detect, ND, or other similar non-numerical
format. When results are below the applicable limits,they must be reported in the format, "<XX mg/L", where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
No discharge this period?2
Outfall No. Date Sample Collected' 24-hour rainfall amount, New Motor Oil or Non-Polar O&G/Total Total Suspended
(mo/dd/yr) Inches3 Hydraulic Oil Usage Petroleum Hydrocarbons Solids
Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4
Parameter Code - 46529 NCOIL 00552 CO530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3

FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO
IF YES,HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES❑ NO❑
REGIONAL OFFICE CONTACT NAME:
Mail an original copy of this DMR,including all"No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period in the
case of"No Discharge"reports)to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or
those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete. I
am a e t t ere are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
ti� os�9alao2o
Si t re f Permitte Date
Permit Date: 11/1/2018-05/31/2021 SWU-245,last revised 11/1/2018
Page 3 of 3

Pace Analytical Services,LLC
0 2225 Riverside Dr.
aceAnalytical Asheville,NC 28804
www.pacelabs.com [phone]
May 08, 2020
Chataut Khagesh
Eaton
221 Heywood Rd.
Arden, NC 28704
RE: Project: Storm Water 2020430
Pace Project No.: 92475674
Dear Chataut Khagesh:
Enclosed are the analytical results for sample(s)received by the laboratory on April 30, 2020. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
cc: Chataut Khagesh,Eaton Corporation
,z SAP/ REPORT OF LABORATORY ANALYSIS
0 ~ This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 17

Pace Analytical Services,LLC
l 2225 Riverside Dr.
aceAnalytica
Asheville,NC 28804
www.pacelabs.com [phone]
CERTIFICATIONS
Project: Storm Water 2020430
Pace Project No.: 92475674
Pace Analytical Services Charlotte
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Certification#:99006001
Louisiana/NELAP Certification#LA170028 Florida/NELAP Certification#:E87627
North Carolina Drinking Water Certification#:37706 Kentucky UST Certification#:84
North Carolina Field Services Certification#:5342 VirginiaNELAP Certification#:460221
North Carolina Wastewater Certification#:12
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
Massachusetts Certification#:M-NC030 VirginiaNELAP Certification#:460222
North Carolina Drinking Water Certification#:37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 17

Pace Analytical Services,LLC
ace Analytical
2225 Riverside Dr.
ace�(.��I l� Asheville,NC 28804
www.pacelabs.com [phone]
SAMPLE ANALYTE COUNT
Project: Storm Water 2020430
Pace Project No.: 92475674
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92475674001 Outfall 001 EPA 1664B WAM 1 PASI-C
EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A
SM 2540D-2011 RED 1 PASI-A
92475674002 Outfall 002 EPA 1664B WAM 1 PASI-C
EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A
SM 2540D-2011 RED 1 PASI-A
92475674003 Outfall 003 EPA 1664B WAM 1 PASI-C
EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A
92475674004 Outfall 004 EPA 1664B WAM 1 PASI-C
EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A
SM 2540D-2011 JNS 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services.LLC. Page 3 of 17

Pace Analytical Services,LLC
aceAnalytical® Asheville,
Riverside Dr.
NC 28804
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: Storm Water 2020430
Pace Project No.: 92475674
Sample: Outfall 001 Lab ID: 92475674001 Collected: 04/29/20 16:30 Received: 04/30/20 08:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease ND mg/L 5.0 1 05/05/20 10:33
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper 9.3 ug/L 5.0 1 05/06/20 01:48 05/07/20 07:05 7440-50-8
Lead ND ug/L 5.0 1 05/06/20 01:48 05/07/20 07:05 7439-92-1 BC
Zinc 72.2 ug/L 10.0 1 05/06/20 01:48 05/07/20 07:05 7440-66-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 16.7 mg/L 6.4 1 05/04/20 15:11
REPORT OF LABORATORY ANALYSIS
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Date:05/08/2020 07:27 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 17

Pace Analytical Services,LLC
e 2225 Riverside Dr.
aceAnalytical Asheville,NC 28804
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: Storm Water 2020430
Pace Project No.: 92475674
Sample: Outfall 002 Lab ID: 92475674002 Collected: 04/29/20 16:30 Received: 04/30/20 08:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease ND mg/L 5.0 1 05/05/20 10:11
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper ND ug/L 5.0 1 05/06/20 01:48 05/07/20 07:08 7440-50-8
Lead ND ug/L 5.0 1 05/06/20 01:48 05/07/20 07:08 7439-92-1 BC
Zinc 31.4 ug/L 10.0 1 05/06/20 01:48 05/07/20 07:08 7440-66-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 9.6 mg/L 2.5 1 05/04/20 15:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/08/2020 07:27 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 17

Pace Analytical Services,LLC
aceAnalytical® Asheville,
Riverside 2e 04
Asheville,NC 28804
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: Storm Water 2020430
Pace Project No.: 92475674
Sample: Outfall 003 Lab ID: 92475674003 Collected: 04/29/20 16:30 Received: 04/30/20 08:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664B
Pace Analytical Services-Charlotte
Oil and Grease ND mg/L 5.0 1 05/05/20 10:11
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper ND ug/L 5.0 1 05/06/20 01:48 05/07/20 07:11 7440-50-8
Lead ND ug/L 5.0 1 05/06/20 01:48 05/07/20 07:11 7439-92-1 BC
Zinc 55.3 ug/L 10.0 1 05/06/20 01:48 05/07/20 07:11 7440-66-6
•
•
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/08/2020 07:27 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 17

Pace Analytical Services,LLC
aceAnalytical® Asheville,
Riverside Dr.
NC 28804
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: Storm Water 2020430
Pace Project No.: 92475674
Sample: Duffel!004 Lab ID: 92475674004 Collected: 04/29/20 16:30 Received: 04/30/20 08:38 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method:EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease ND mg/L 5.0 1 05/05/20 10:11
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper 5.9 ug/L 5.0 1 05/06/20 01:48 05/07/20 07:20 7440-50-8
Lead ND ug/L 5.0 1 05/06/20 01:48 05/07/20 07:20 7439-92-1 BC
Zinc 98.8 ug/L 10.0 1 05/06/20 01:48 05/07/20 07:20 7440-66-6
2540D Total Suspended Solids Analytical Method:SM 2540D-2011
Pace Analytical Services-Asheville
Total Suspended Solids 21.2 mg/L 10.0 1 05/05/20 15:31
REPORT OF LABORATORY ANALYSIS
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Date:05/08/2020 07:27 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 17

Pace Analytical Services,LLC
opaceAnalytical Asheville,
Riverside Dr.
NC 28804
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Storm Water 2020430
Pace Project No.: 92475674
QC Batch: 539695 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92475674002,92475674003,92475674004
METHOD BLANK: 2876539 Matrix: Water
Associated Lab Samples: 92475674002,92475674003,92475674004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 05/05/20 10:11
LABORATORY CONTROL SAMPLE: 2876540
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 37.3 93 78-114
MATRIX SPIKE SAMPLE: 2876541
92475787001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L ND 40 36.4 90 78-114
•
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
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Pace Analytical Services,LLC
® 2225 Riverside Dr.
aceAnalytical Asheville,NC 28804
www.pscelabs.com [phone]
QUALITY CONTROL DATA
Project: Storm Water 2020430
Pace Project No.: 92475674
QC Batch: 539700 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92475674001
METHOD BLANK: 2876604 Matrix: Water
Associated Lab Samples: 92475674001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 05/05/20 10:33
LABORATORY CONTROL SAMPLE: 2876605
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 39.8 100 78-114
MATRIX SPIKE SAMPLE: 2876606
92475743002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L ND 40 42.9 102 78-114
Results presented on this page are In the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/08/2020 07:27 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 17

Pace Analytical Services,LLC
® 2225 Riverside Dr.
aceAnalytical Asheville,NC 28804
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Storm Water 2020430
Pace Project No.: 92475674
QC Batch: 539859 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92475674001,92475674002,92475674003,92475674004
METHOD BLANK: 2877505 Matrix: Water
Associated Lab Samples: 92475674001,92475674002,92475674003,92475674004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper ug/L ND 5.0 05/07/20 06:11
Lead ug/L ND 5.0 05/07/20 06:11 BC
Zinc ug/L ND 10.0 05/07/20 06:11
LABORATORY CONTROL SAMPLE: 2877506
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Copper ug/L 500 486 97 85-115
Lead ug/L 500 498 100 85-115
Zinc ug/L 500 495 99 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2877507 2877508
MS MSD
92474809001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper ug/L 6.0 500 500 6560 6610 116 126 70-130 1
mg/L
Lead ug/L 0.33 500 500 844 841 102 101 70-130 0
mg/L
Zinc ug/L 0.37 500 500 867 870 99 100 70-130 0
mg/L
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 2877509 2877510
MS MSD
92475674003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper ug/L ND 500 500 486 484 96 96 70-130 0
Lead ug/L ND 500 500 503 499 100 99 70-130 1
Zinc ug/L 55.3 500 500 559 555 101 100 70-130 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/08/2020 07:27 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 17

Pace Analytical Services,LLC
® 2225 Riverside Dr.
aceAnalytical Asheville,NC 28804
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Storm Water 2020430
Pace Project No.: 92475674
QC Batch: 539564 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92475674001,92475674002
METHOD BLANK: 2876130 Matrix: Water
Associated Lab Samples: 92475674001,92475674002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 05/04/20 14:57
LABORATORY CONTROL SAMPLE: 2876131
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 244 97 90-110
SAMPLE DUPLICATE: 2876132
92475551001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 105 100 5
SAMPLE DUPLICATE: 2876133
92475553001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 117 116 1
Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Dr.
ace Analytical® Asheville,Riverside 2e 04
NC 28804
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Storm Water 2020430
Pace Project No.: 92475674
QC Batch: 539582 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92475674004
METHOD BLANK: 2876231 Matrix: Water
Associated Lab Samples: 92475674004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 05/05/20 15:28
LABORATORY CONTROL SAMPLE&LCSD: 2876232 2876233
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units Conc. Result Result %Rec %Rec Limits RPD RPD Qualifiers
Total Suspended Solids mg/L 250 234 240 93 96 90-110 3 25
SAMPLE DUPLICATE: 2876234
92475964001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 162 174 7
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
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Pace Analytical Services,LLC
® 2225 Riverside Dr.
aceAnalytical Asheville,NC 28804
www.pacelabs.com [phone]
QUALIFIERS
Project: Storm Water 2020430
Pace Project No.: 92475674
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
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Pace Analytical Services,LLC
2225 Riverside NC
Asheville,NC 2880404
www.pacelabs.cora [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Storm Water 2020430
Pace Project No.: 92475674
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92475674001 Outfall 001 EPA 1664B 539700
92475674002 Outfall 002 EPA 1664B 539695
92475674003 Outfall 003 EPA 1664B 539695
92475674004 Outfall 004 EPA 1664B 539695
92475674001 Outfall 001 EPA 200.7 Rev 4.4 1994 539859 EPA 200.7 Rev 4.4 1994 539878
92475674002 Outfall 002 EPA 200.7 Rev 4.4 1994 539859 EPA 200.7 Rev 4.4 1994 539878
92475674003 Outfall 003 EPA 200.7 Rev 4.4 1994 539859 EPA 200.7 Rev 4.4 1994 539878
92475674004 Outfall 004 EPA 200.7 Rev 4.4 1994 539859 EPA 200.7 Rev 4.4 1994 539878
92475674001 Outfall 001 SM 2540D-2011 539564
92475674002 Outfall 002 SM 2540D-2011 539564
92475674004 Outfall 004 SM 25400-2011 539582
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/08/2020 07:27 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 17

Document Name: Document Revised:February 7,2018
(, Sample Condition Upon Recelpt(SCUR) Page 1 of 2
&CB?�Rc?ly�lGBl Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving sa ples:
Asheville[U Eden❑ Greenwood❑ Huntersville❑ Raleigh0 Mechanicsville❑
Sample Condition --- Client Name: WO# : 92475674
Upon Receipt Project f
6QA0N[(UPS CUSPS •
Client 111111111IIII1111III
Courier: ❑Fed Ex
❑Commercial [(Pace ❑Other: 92475674
Custody Seal Present? Yes 4. Seals Intact?
p "l'b Date/Initials Person Examining Contents:
• Packing Material: ❑Bubble Wrap 12117.rbble Bags [None ❑ Other Biological Tissue Fr en? •
Thermometer lltf}, +, Eyes ENO l/A
IR Gun ID: u�6 V I Type of Ice: Wet Dilute :None
Cooler Temp(`C): Or Correction Factor:Add/Subtract(`C) o'U
(} Temp should be above freezing to 6°C
Cooler Temp Corrected('C): ❑Samples our of temp criteria.Samples on Ice,cooling process
has begur
USDA Regulated Soil ( N/A,water sample)
Did samples originate In a quarantine zone within the United States:CA,NY,or SC(check maps)? Did samples originate from a foreign source(Internationally,
Dyes ❑No Inciudirg Nava and Puerto Rico)?❑Yes ❑No
Comments/Discrepancy:
Chain of Custody Present? les ❑No ❑WA 1.
Samples Arrived within Hold Time? oe ❑No ON/A 2.
Short Hold Time Analysts(<72 hr.)? ❑Yes No ©N/A 3.
Rush Turn Around Time Requested? ❑Yes /'o •N/A 4.
Sufficient Volume? 124 Quo DNA 5.
Correct Containers Used? "ales ❑No ON/A 6.
-Pace Contairers Used? „(]Yes Duo ON/A
Containers Intact? es pun ON/4 7.
Dissolved analysis:Samples Field Filtered? ❑Yes •No •N/A 8.
Sample Labels Match COC? es ❑No ON/A 5.
-Includes Date/Time/ID/Analysis Matrix:,
MedUspace1n-VC14VtaIs(a5itmmr?. Ones ❑No iA 10.
Trip Blank Present? Ores Dag- ON/A 11.
Trip Blank Custody Seals Present? Dyes a No rilN A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time: -
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Page 15 of 17

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CHAIN-OF-CUSTODY/Analytical Request Document
aeeAnalytica! The Chiin-a6Custody le a LEGAL DOCUMENT.All relevant fields rrush be completed accurately.
. rnoe.pacelalt.aa
Section A Section B Section C Pace: of
Required Client Information: Required Project Information: Inertial Information, 2066752
Company f^G (V Report To: el E/N.
H A-L E Attention:
,
Addrej-Il,, Copy To:k.1,41141,�" Company Name: REGULATORY AGENCY
A,,,,,"t�/YI N L v. 1 0 Address_ _ T- NPDES GROUND WATER r DRINKING WATER
Email To: `l _n- Purchase Order No.: Pats Cwle
�31n�(N p' CC4Vv1• (ZAP' Pare Cunt UST r RCRA ( OTHER
Phone:
5-�14j^f/ .i.D Fax: PrcOcl Name:Siorpw, w , • 2.0 20 -f 0 o Pace arntra
Manager Site Location
Requested Due 0atelTAT: Project Number. • Pate Prpfile it: STATE:
Requested Analysis F-Iltuee 1(YIN) •
•
Section D Matrix Codes a Z
RegeireaClentlnformation MATRIX r cYJDF COLLECTED Preservatives % _ ,
Drinking Water DW a o
e V O
Water Wi _
Waste Water VON3 U ooaaosnc :cn+ro•�-e
© START ENOT tAti jyj 7
Product P
SAMPLE ID Soil/Solid O1 " u o Cl) -►.-4r, 3
Wipe WP - I- W v,
(A-Z,0-9 f,-) Air AR W G Z v o
Sample lOs MUST BE UNIQUE Tissue TS O c. a F v m C^ L
Other OT H
O T `
_a O a t0 O O to � L V KS
- • .i ' DATE TIME DATC TIME �m or .n _ I = Z Z 2 O .... t" = Pace Project No/Lab I.D.
1 po 1 i if-.2i 11:30Pm 3 l l i i j
2 U�1 co t - r1 • l-j i7..zo o . 3 i l ‘ . I I p c�C..•4-
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ADDITIONAL COMMENTS __2ELINQUISHED BYI AFFILIATION DATE TIME • ACCEPTED BY!AFFILIATION DATE TIME SAMPLE CONDITIONS
•
ti . U oo f f K • 6-11 1±-di,f_____ �- (�l 5:30 _^,� /�� LiAct $':33 I I
Dot ` 2 r ( G4�„/.,.. Q 1i3emi rk ,9✓ if-4o%s �3d B,I 'Y Y Y
Doi ��6.ei O
ORIGINAL SAiIPLER NAME AND SIGNATLRF. c 3
a. PRINT Name of SAMPLER: lam, ..�v� e 1 _ a z- o c:i a z
pSIGNATURE of SAMPLER: (�( \- /,� ��� ( d Q�f�' �f� `-- U
�'Ft,rVv� M T/ ba ur
`, 'Impc;tam Note:Ry signing this form yra,we axepLng Pace's NET SO day pryment tame end agreeing toy late Chaos of 1 Sti Der moth for a - wn 3
. paid wf0 der. F-ALL-0-020rev.07,15-May-2007