NCG030459_DMR_20200519

Semi-annual Stormwater Discharge Monitoring Report
for North Carolina Division of Water Quality General Permit No. NCG030000
Date submitted
CERTIFICATE OF COVERAGE NO. NCGO3 0 yI SAMPLE COLLECTION YEAR
SAMPLE PERIOD Dian-June El July-Dec
FACILITY NAME e��'.'-" ` � _ r or ❑Monthly' (month)
COUNTY
PERSON COLLECTING SAMPLES A. f ir4 ®L'Z"` DISCHARGING TO CLASS ❑ORW DHOW (Trout EPNA
LABORATORY Lab Cert.if " f '\/F D ['Zero-flow ❑Water Supply f SA
Comments on sample collection or analysis: ❑Other
JUN 11 2020
PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
CEN-i
Part A: Stormwater Benchmarks and Monitoring Res&IWs R S'EC-(icx
n No discharge this period??
Date Sample 24-hour rainfall pH, Non-Polar O&G/ Total Toxic
Outfall No. Collected' amount, Total Suspended Solids Standard units Copper Lead Zinc Total Petroleum Organics
(mo/dd/yr) Inches' Hydrocarbons
Benchmarks===> - - 100 mg/L or 50 mg/L4 6.0—9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L
Monthly sampling(instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here.
3 The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
See General Permit,Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals,or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample(for metal finishing use the definition as found in 40 CFR 433.11;for semiconductor
manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22;and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date:11/1/2012-10/31/2017 SWU-245,last revised 10/25/2012
Page 1 of 3

Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify,and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver,the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO),I certify that to the best of my knowledge and belief,no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
14)11 f ia.n? Ye V5
Name(Print name)
� -thee
Title(Print title)
-712 /
(Signature) (Date)
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL,<PQL, Non-detect, ND,or other similar non-numerical
format. When results are below the applicable limits,they must be reported in the format, "<XX mail",where XX is the numerical value of the detection
limit, reporting limit, etc.in mg/L.
Note: If you report a sample value in excess of the benchmark,you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results:only for facilities averaging>55 gal of new oil per month.
n No discharge this period?2
Date Sample 24-hour rainfall
Outfall No. ,
Collected amount, Non-polar O&G/TPH by
(mo/dd/yr) Inches' EPA 1664(SGT-HEM) Total Suspended Solids pH
Benchmarks===> - - 15 mg/L 100 mg/L or 50 mg/L' 6.0—9.0 SU
Footnotes from Part A also apply to this Part B
"See General Permit text,Table 5,identifying the especially sensitive receiving water classifications where the more protective benchmark applies.
Permit Date: 11/1/2012-10/31/2017 SWU-245,last revised 10/25/2012
Page 2 of 3

Note: If you report a sample value in excess of the benchmark,you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera!Permit text.
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION Bo
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑NO
IF YES,HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO❑
REGIONAL OFFICE CONTACT NAME:
Mail an original and one copy of this DMR,including all"No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period
in the case of"No Discharge"reports)to:
Division of Water Quality
Attn:DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or
those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
;7?("ifip,
(Signature of Permittee) -` (Date)
Permit Date:11/1/2012-10/31/2017 SWU-245,last revised 10/25/2012
Page 3 of 3

_ " Phone: [phone]
� Shipping: Mailing: Fax [phone]
.1 ---1::.; 2401 W. 5th St. PO Box 589 Email:pam.hester-
' Lumberton NC 28358 Lumberton, NC 28359 tbl hotmail.com
TBL
FINAL REPORT OF ANALYSES
COUNCIL TOOL COMPANY PROJECT NAME:TBL-29654
345 PECAN LANE REPORT DATE:5-5-20
LAKE WACCAMAW, NC 28450
ATTN: VELTON JACOBS
: AMPLE NUMBER- 15381 SAMPLE ID - STGRMWATER SAMPLE MATRIX- WW
DATE SAMPLED- 5-5-20 SAMPLER-WILL RIVERS TIME SAMPLED-0930
DATE RECEIVED-5-5-20 DELIVERED BY-CLIENT RECEIVED BY-THI
TIME RECEIVED- 1040
PAGE 1 OF 1
QUAL DET.
ANALYSIS METHOD DATE RESULT UNITS CODE LIMIT
BIOCHEMICAL OXYGEN DEMAND SM5210-B N/R MG/L 2.0
rOTAL SUSPENDED SOLIDS SM2540D 5/5/2020 3.3 MG/L 2.6
AMMONIA NITROGEN SM4500NH3D N/R MG/L 0.1
FECAL COLIFORM SM9222D N/R MPN/100ML 1
CONDUCTIVITY SM2510B N/R UMHOS/CM 10
CHEMICAL OXYGEN DEMAND SM5220D N/R MG/L 30.0
PH SM4500 H+B 5/5/2020 6.5 STD UNITS 0.1
VOLATILE SUSPENDED SOLIDS SM2540E N/R MG/L 500
N/R=ANALYSIS NOT REQUESTED
LABORATORY DIRECTOR R/Ih )/i.,j.2 .i
NCDENR DVVQ#37, NCDENR DW#37781

•
Billing Information:.. Analysis/Container/Preservative
T B L Environmental
_
Laboratory , Inc.
2401 W. 5th St
Lumberton , NC 28358
Report to: c ,
(910) 738-6190 . _mall to: ,C fdl VERIFIED 0/G
SAMPLE VOLUME TO BE
Project
Description:] I cri ?�fo�•i AdVer .0 c llectd N !-0 1 MLS AS COMPARED
Phone: Client Project#: ESC Key: 1"' r 1 L I R R A T EO BOTTLE
FAX: .Q G `- acOS C/
Collected by:J l'�l1� Site/Facility ID#: P.O.#: cv
AM k e, ....,. .\.
Collected by(signature): Rush? (Lab MUST Be Notified) Date Results Needed: J
CoCode (lab use only)
/ Same Day 200% No.
Next Day. 100% Email?_No_Yes V s . Template/Prelogin
Two Day.. 50% or , 0 c
Immediately Packed on Ice N Three Day.. . , ,25°!° FAX? _No Yes ' Q J� . l'
Cntrs ( V v q Shipped Via:
Sample ID Comp/Grab Matrix* Depth Date Time �/ Remarks/Contaminant Sample#(lab only)
Siotrir biller 3--.5.-.zz . 5/5- 437:391/P‹ )- )4 }c. ..›.,..r.„,,d...
•
r .. it N TEMP --�
_ H NH3 C N (L1 1' N
_ 1J/7 6� P N 11(N
•
" METAt S I NT
•
*Matrix SS-Soil/Solid GW_Groundwater WW-WasteWater DW-DrinkingWater OT-Other pH Temp
Remarks:
Flow Other
Relinq fished 5igna re) Date: Time: Rec-eived byyy,,,���(((�ignat re) Samples returned via:❑UPS Condition: (lab use only)
r � c�0G 1 Gt( d V2 � 0 FedEx 0 Courier 0
Relinquished by.(Sign uji-e_)",........, Date: Time: Received by:�(Signature)( 9 ) Temp: Bottles Received:
CoC Seals Intact: Y N NA
" Relinquished by.(Suture) Date: Time: Received for lab by:(Signature) Date: Time: pH Checked: NCF:

Environmental Chemists, Inc.
envirochem 6602 Windmill Way,Wilmington,NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road,'vfanteo,NC 27954 • 252.473.5702 Lab/Fax
SM
255-A Wilmington Highway,Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL&CONSULTING CHEMISTS inf(*environmentalcheinists.com
TBL Date of Report: May 14, 2020
P.O. Box 589 Customer PO#: TBL 29654
Lumberton NC 28358 Customer ID: 11040019
Attention: Pam Hester Report#: 2020-07461
Project ID: Council Tool
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-18350 Site: Stormwater 5/5/2020 9:30 AM Water Will Rivers
Test Method Results Date Analyzed
Oil &Grease (O&G) EPA 1664 <5.0 mg/L 05/13/2020
Copper EPA 200.7 <0.01 mg/L 05/08/2020
Lead EPA 200.7 <0.01 mg/L 05/08/2020
Zinc EPA 2001 0.052 mg/L 05/08/2020
Comment:
Reviewed by: VOICO& OijkQN1)
Report#: 2020-07461 Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Winom,i; Wa.
Wilmington, NC 2840E
/r '16 392.02Sam ie R ceipt Checklist Chen! _ —T-13 t- Date to �-
Report Number p�O - Q !7
f
Receipt of sample Delivered
❑ YES 0 NO �. UPS FedEx 0 Other ❑
N/A 1. Were custody seals present on the cooler'
. ❑ YES 0 NO li' 2 If custody seals were present, were they intact/unbroken-
Original temperature upon receipt •C
How temperature takenCorrected temperature upon receipt •
0 Temperature Blank '�
IR Gun ID Thomas Traceable S/N 192511657 I: Against rC.
Bottles
❑ YESIR Gun Correction Factor 'C: 0.0
0 NO 3 If temperature of cooler exceeded 6'C, was Project Mgr./QA
�. ❑ NO 4. Were proper custody g �QA notified;'
•� y procedures (relinquished/received) followed%
❑ NO S. Were sample ►D's listed on the COC'
YES 0 NO 6 Were samples ID's listed on sample containers'
mL_ YES 0 NO 7 Were collection date and time listed on the COC'
11117g=0 NO 8 Were tests to be performed listed on the COC%
=1❑ NO 9. Did samples arrive in proper containers for each test?
ti MM.❑ NO 10. Did samples arrive in good condition for each test'
0 NO 11. Was adequate sample volume available'
`r 0 NO 12 Were samples received within proper holding time for requested tests
MEMO NO
13. Were acid preserved samples received at a pH of<2, •
❑ YES 0 NO 14. Were cyanide samples received at a pH >12
❑ YES 0 NO 15 Were sulfide samples received at a pH >9'I YES 0 NO 16 Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L' ••
❑ YES
❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L'
❑ YES 0 NO 18 Were orthophosphate samples filtered in the field within 15 minutes%
I. IOC/Volatiles are pH checked at time of analysis and recorded on the benchshee:
'" Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchshee:
Sample Preservation: (Must be completed for any sample(s) incorrect)
Samples) y preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
by adding (circle onei
H1504 HNO3 HCI
Time of preservation NaOH
If more than one preservative is needed, notate in comments beiou
Note. Notify customer service immediately for incorrectly preserved samples Obtain a new sample or
notify the state lab if directed to analyzed by the customer
Volatile Who was notified date and time
s Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002

Billing Information:. Ana slslContainerlPreservative
TBL Environmental - —
Laboratory , Inc.
2401 W. 5th St
Lumberton , NC 28358 Y
eport lo:
(910) 738-6190 k'
,
—roe
D mail lo: �C (d L VERIFIED 0/G
�' N SAMPLE VOLUME TO BE
Project f� Sforrr>1.J41r 1C CoVote 1 � MLS AS COMPARED
Descdption:�.I�r1/ r L Coll Sate
Phone: 1 Client Project#: ESC Key: �� L I R R A T E!l BOTTLE
FAX: _n L a�-y, s ,}.
Collected by4)_vev Site/Facility ID#:`�(� P.0.#: .la, id
11414,4047
Collected by(signature): Rush? Lab MUST Be Notified
Date Results Needed: V CoCode (lab use only)
1//a Same Day Next Day. 200% 4.1'S•-b No.
100% Email? NoYes Templaie/Prelogin
Two Da c
Immediately Packed on Ice N Y Three Day 255% FAX? NoYes
of J
Cntrs a t-O\ Shipped Via:
Time
�l v
Remarks/Contaminant Sample#(lab only)
Sample ID Comp/Grab Matrix* Depth Date Ti
u 1 N 1 LMP ---->
•
Dr/Hs N H 3 C N L�2— -
G ,'n H E T A . S jT— y --
"Matrix: SS-Soil/Solid GW-Groundwater WW-WasteWater DW-Drinking Water OT-Other
Remarks: CP." PH Temp —
Flow Other
Relinq fished Signa re) Date: Time:. .amples returned via:
/ ��'� j cl Recelvedb ignat re) ❑UPS Condition:
G a � C]FedEx ❑Courier 0
(lab use only)
Relinquished by:(Sign ure) Date: Time:
Rece ed (SI ature) Temp: j Bottles Received:
/r_j - •/ S-4'.° � j C CoC Seals Intact: Y_N NA
Relinquished by:`5igrfature) Dale: Time: Received for lab by: Signature
( 1 ) Uate /o Time: pH Checked: NCF:

aceAnalyticaie A \ A L Y T I C A L REPORT
National Center for Testing 8,Irmo anc• May 11, 2020
Tc
Ss
TBL Laboratory
Sample Delivery Group: L1215360 Cn
Samples Received: 05/06/2020 Sr
Project Number: TBL29654
Description: Council Tool Spring 2020 'Qc
GI
• Report To: Pam Hester
P.O. Box 589
Lumberton, NC 28359
9
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Entire Report Reviewed By:
Darren Reeder
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the information provided,
and as the samples are received.
wiES
•
s z-
ti
- a �

TABLE OF CONTENTS ONE LAB.NATIONWIDE
Cp: Cover Page .
Tc: Table of Contents 2 --•---
Ss:Sample Summary 3
Cn: Case Narrative 4
Sr:Sample Results 5 Ss
STORMWATER 5-5-2020 L1215360-01 5
Cn
Qc: Quality Control Summary 8
Volatile Organic Compounds(GC/MS) by Method 624.1 8 Sr
Pesticides (GC) by Method EPA 608.3 10
Polychlorinated Biphenyls(GC) by Method EPA-608.3 12 Qc
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 13
GI
GI: Glossary of Terms 18
Al:Accreditations& Locations 19 ^;
Sc: Sample Chain of Custody 20
Sc
Arrni PROJECT: SDG:. DATE/TIME: PAGE:

SAMPLE SUMMARY • - ONE LAB.NATIONWIDE. .
Collected by Collected date/time Received date/time
STORMWATER 5-5-2020 L1215360-01 WW 05/05/20 09:30 05/06/20 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time -TC
Volatile Organic Compounds(GC/MS)by Method 624.1 WG1472191 1 05/07/20 20:09 05/07/20 20:09 ACG Mt.Juliet,TN
Pesticides(GC)by Method EPA 608.3 WG1471543 1 05/07/20 10:54 05/08/20 04:23 RP Mt.Juliet,TN
Polychlorinated Biphenyls(GC)by Method EPA-608.3 WG1471543 1 05/07/20 10:54 05/07/20 19:32 RP Mt.Juliet,TNIIII
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 WG1472915 1 05/08/20 15:43 05/09/20 10:51 SHG Mt.Juliet,TN
4
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5
Sr
6
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Al
9
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ACCOUNT: PROJECT: SDG: DATE/WE: PAGE:

CASE NARRATIVE ONE LAB.NATIONWIDE. ipt
r,
�D
AU sample aliquots were received at the correct temperature, in the proper containers,with the
appropriate preservatives,and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL(LOD)and RDL(LOQ)values reported for environmental samples Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my 3Ss
knowledge,all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory,and no information or data have been
knowingly withheld that would affect the quality of the data. 11
s
Sr
b
Qc
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Darren Reeder Al
Project Manager
9
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STORMWATER 5-5-2020 SAMPLE RESULTS - 01 ONE LAB.NA,TioNWIDE. Apt
Collected date/time: 05/05/20 09:30 L1215360
Volatile Organic Compounds (GC/MS) by Method 624.1 _.--
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time
Acrolein ND 0.0500 1 05/07/2020 20:09 WG1472191 Tr
Acrylonitrile ND 0.0100 1 05/07/2020 20:09 WG1472191
Benzene ND 0.00100 1 05/07/2 020 20:09 WG1472191 '55
Bromodichloromethane ND 0.00100 1 05/07/2020 20:09 WG1472191
Bromoform ND 0.00100 1 05/07/2020 20:09 WG1472191
Bromomethane ND 0.00500 1 05/07/2020 20:09 WG1472191 Cn
Carbon tetrachloride ND 0.00100 1 05/07/2020 20:09 WG1472191
Chlorobenzene ND 0.00100 1 05/07/2020 20:09 WG1472191
11
Chiorodibromomethane ND 0.00100 1 05/07/2020 20:09 WG1472191
Chloroethane ND 0.00500 1 05/07/2020 20:09 WG1472191 6
2-Chloroethyl vinyl ether ND 0.0500 1 05/07/2020 20:09 WG1472191 Qc
Chloroform ND 0.00500 1 05/07/2020 20:09 WG1472191
Chloromethane ND 0.00250 1 05/07/2020 20:09 WG1472191 GI
1,2-Dichlorobenzene ND 0.00100 1 05/07/2020 20:09 WG1472191
1,3-Dichlorobenzene ND 0.00100 1 05/07/2020 20:09 WG1472191
1,4-Dichlorobenzene ND 0.00100 1 05/07/2020 20:09 WG1472191 Al
Dichlorodifluoromethane ND J4 0.00500 1 05/07/2020 20:09 W61472191
t,1-Dichloroethane ND 0.00100 1 05/07/2020 20:09 WG1472191 0
SC
1,2-Dichloroethane ND 0.00100 1 05/07/2020 20:09 WG1472191
1,1-Dichloroethene ND 0.00100 1 05/07/2020 20:09 W01472191
trans-1,2-Dichloroethene ND 0.00100 1 05/07/2020 20:09 WG1472191
1,2-Dichloropropane ND 0.00100 1 05/07/2020 20:09 WG1472191
cis-1,3-Dichloropropene ND 0.00100 1 05/07/2020 20:09 WG1472191
trans-1,3-Dichloropropene ND 0.00100 1 05/07/2020 20:09 WG1472191
Ethylbenzene ND 0.00100 1 05/07/2020 20:09 WG1472191
Methylene Chloride ND 0.00500 1 05/07/2020 20:09 W61472191
Methyl tert-butyl ether ND 0.00100 1 05/07/2020 20:09 WG1472191
Naphthalene ND 0.00500 1 05/07/2020 20:09 WG1472191
1,1,2,2-Tetrachloroethane ND 0.00100 1 05/07/2020 20:09 WG1472191
Tetrachloroethene ND 0.00100 1 05/07/2020 20:09 WG1472191
Toluene ND 0.00100 1 05/07/2020 20:09 W61472191
1,1,1-Trichloroethane ND 0.00100 1 05/07/2020 20:09 WG1472191
1,1,2-Trichloroethane ND 0.00100 1 05/07/2020 20:09 WG1472191
Trichloroethene ND 0.00100 1 05/07/2020 20:09 WG1472191
Trichlorofluoromethane ND 0.00500 1 05/07/2020 20:09 W61472191
Vinyl chloride ND 0.00100 1 05/07/2020 20:09 WG1472191
(S)Toluene-d8 111 80.0-120 05/07/2020 20:09 WG1472191
(S)4-Bromofluorobenzene 105 80.0-120 05/07/202020:09 W61472191
(S)1,2-Dichloroethene-d4 101 70.0-130 05/07/2020 20:09 WG1472191
Pesticides (GC) by Method EPA 608.3
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time
Aidrin ND 0.0000500 1 05/08/2020 04:23 WG1471543
Alpha BHC ND 0.0000500 1 05/08/2020 04:23 WG1471543
Beta BHC ND 0.0000500 1 05/08/2020 04:23 WG1471543
Delta BHC ND 0.0000500 1 05/08/2020 04:23 WG1471543
Gamma BHC ND 0.0000500 1 05/08/2020 04:23 WG1471543
Chlordane ND 0.00500 1 05/08/2020 04:23 WG1471543
4,4-DDD ND 0.0000500 1 05/08/2020 04:23 WG1471543
4,4-DDE ND 0.0000500 1 05/08/2020 04:23 WG1471543
4,4-DDT ND 0.0000500 1 05/08/2020 04:23 WG1471543
Dieldrin ND 0.0000500 1 05/08/2020 04:23 WG1471543
Endosulfan I ND 0.0000500 1 05/08/2020 04:23 WG1471543
Endosulfan II ND 0.0000500 1 05/08/2020 04:23 WG1471543
..-,ram,MIT. eon irrr. Crlf,• r ATF/TIMF. PAGE:

STORMWATER 5-5-2020 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. ip
Collected date/time: 05/05/20 09:30 L1215360
Pesticides (GC) by Method EPA 608.3 ..._..-.
Result Qualifier RDL Dilution Analysis Batch ` `
Analyte mg/I mg/I date/time -----
.
Endosulfan sulfate ND 0.0000500 1 05/08/2020 04:23 WG1471543 -Tr
Endrin ND 0.0000500 1 05/08/2020 04:23 WG1471543
Endrin aldehyde ND 0.0000500 1 05/08/2020 04:23 WG1471543
.-
Endrin ketone ND 0.0000500 1 05/08/2020 04:23 WG1471543 SS
Heptachlor ND 0.0000500 1 05/08/2020 04:23 WG1471543
Heptachlor epoxide ND 0.0000500 1 05/08/2020 04:23 WG1471543 `Cn
Hexachlorobenzene 0.000757 0.0000500 1 05/08/2020 04:23 WG1471543
Methoxychlor ND 0.0000500 1 05/08/2020 04:23 WG1471543
Toxaphene ND 0.000500 1 05/08/2020 04:23 WG14715431111
(S)Decachlorobiphenyl 82.2 10.0-144 05/08/2020 04:23 W61471543
(S)Tetrachloro-m-xy/ene 87.5 10.0-135 05/08/2020 04:23 WG1471543 "Q
Polychlorinated Biphenyls (GC) by Method EPA-608.3
GI
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time
PCB 1016 ND 0.000500 1 05/07/2020 19:32 WG1471543 /3
PCB 1221 ND 0.000500 1 05/07/202019:32 WG1471543
PCB 1232 ND 0.000500 1 05/07/2020 19:32 WG1471543 SC
PCB 1242 ND 0.000500 1 05/07/2020 19:32 WG1471543
PCB 1248 ND 0.000500 1 05/07/2020 19:32 WG1471543
PCB 1254 ND 0.000500 1 05/07/2020 19:32 WG1471543
PCB 1260 ND 0.000500 1 05/07/2020 19:32 WG1471543
Total PCBs ND 0.000500 1 05/07/202019:32 WG1471543
(S)Decachlorobiphenyl 94.5 10.0-144 05/07/2020 19:32 WG1471543
(S)Tetrachloro-m-xylene 104 10.0-135 05/07/202019:32 WG1471543
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time
Acenaphthene ND 0.00100 1 05/09/2020 10:51 WG1472915
Acenaphthylene ND 0.00100 1 05/09/2020 10:51 WG1472915
Anthracene ND 0.00100 1 05/09/202010:51 WG1472915
Benzidine ND J3 J6 0.0100 1 05/09/2020 10:51 WG1472915
Benzo(a)anthracene ND 0.00100 1 05/09/2020 10:51 WG1472915
Benzo(b)fluoranthene ND 0.00100 1 05/09/2020 10:51 WG1472915
Benzo(k)fluoranthene ND 0.00100 1 05/09/2020 10:51 WG1472915
Benzo(g,h,i)perylene ND 0.00100 1 05/09/2020 10:51 WG1472915
Benzo(a)pyrene ND 0.000200 1 05/09/2020 10:51 WG1472915
Bis(2-chlorethoxy)methane ND 0.0100 1 05/09/2020 10:51 WG1472915
Bis(2-chloroethyl)ether ND 0.0100 1 05/09/2020 10:51 WG1472915
2,2-Oxybis(1-Chloropropane) ND 0.0100 1 05/09/2020 10:51 WG1472915
4-Bromophenyl-phenylether ND 0.0100 1 05/09/2020 10:51 WG1472915
2-Chloronaphthalene ND J6 0.00100 1 05/09/2020 10:51 WG1472915
4-Chlorophenyl-phenylether ND 0.0100 1 05/09/2020 10:51 WG1472915
Chrysene ND 0.00100 1 05/09/2020 10:51 WG1472915
Dibenz(a,h)anthracene ND 0.000200 1 05/09/2020 10:51 WG1472915
3,3-Dichlorobenzidine ND 0.0100 1 05/09/202010:51 WG1472915
2,4-Dinitrotoluene ND 0.0100 1 05/09/2020 10:51 WG1472915
2,6-Dinitrotoluene ND 0.0100 1 05/09/202010:51 WG1472915
1,2-Diphenylhydrazine ND 0.0100 1 05/09/2020 10:51 WG1472915
Fluoranthene ND 0.00100 1 05/09/2020 10:51 WG1472915
Fluorene ND 0.00100 1 05/09/2020 10:51 WG1472915
Hexachlorobenzene ND 0.00100 1 05/09/2020 10:51 WG1472915
Hexachloro-1,3-butadiene ND 0.0100 1 05/09/2020 10:51 WG1472915
Hexachlorocyclopentadiene ND 0.0100 1 05/09/2020 10:51 WG1472915

STORMWATER 5-5-2020 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. ikt
Collected date/time: 05/05/20 09:30 L1215360
Semi Volatile Organic Compounds (GC MS) by Method 625.1
' Result Qualifier RDL Dilution Analysis Batch
Analyte mg/I mg/I date/time
Hexachloroethane ND 0.0100 1 05/09/2020 10:51 WG1472915 .Tc
Indeno(1,2,3-cd)pyrene / ND 0.00100 1 .05/09/202010:51 WG1472915
Isophorone ND 0.0100 1 05/09/2020 10:51 WG1472915
Naphthalene ND 0.00100 1 05/09/2020 10:51 WG1472915 Ss
Nitrobenzene ND 0.0100 1 05/09/2020 10:51 WG1472915
n-Nitrosodimethylamine ND 0.0100 1 05/09/2020 10:51 WG1472915 `Cn
n-Nitrosodiphenylamine ND 0.0100 1 05/09/2020 10:51 WG1472915
n-Nltrosodi-n-propylamine ND 0.0100 1 05/09/2020 10:51 WG1472915
Phenanthrene ND 0.00100 1 05/09/2020 10:51 WG147291511
Benzylbutyl phthalate ND 0.00300 1 05/09/2020 10:51 WG1472915
Bis(2-ethylhexyl)phthalate ND 0.00300 1 05/09/2020 10:51 WG1472915 Qc
Di-n-butyl phthalate ND 0.00300 1 05/09/202010:51 WG1472915
Diethyl phthalate ND 0.00300 1 05/09/2020 10:51 WG1472915 i
Dimethyl phthalate ND 0.00300 1 05/09/202010:51 WG1472915 GI
Di-n-octyl phthalate ND 0.00300 1 05/09/2020 10:51 WG1472915
Pyrene ND 0.00100 1 05/09/2020 10:51 W01472915 Al
1,2,4-Trichlorobenzene ND 0.0100 1 05/09/2020 10:51 WG1472915 r
4-Chloro-3-methylphenol ND 0.0100 1 05/09/2020 10:51 WG1472915 9
2-Chorophenol ND 0.0100 1 05/09/2020 10:51 WG1472915 SC
2,4-Dichlorophenol ND 0.0100 1 05/09/2020 10:51 WG1472915
2,4-Dimethylphenol ND 0.0100 1 05/09/202010:51 WG1472915
4,6-Dinitro-2-methylphenol ND 0.0100 1 05/09/202010:51 WG1472915
2,4-Dinitrophenol ND 0.0100 1 05/09/2020 10:51 WG1472915
2-Nitrophenol ND 0.0100 1 05/09/2020 10:51 WG1472915
4-Nitrophenol ND 0.0100 1 05/09/2020 10:51 WG1472915
Pentachlorophenol ND 0.0100 1 05/09/2020 10:51 WG1472915
Phenol ND 0.0100 1 05/09/2020 10:51 WG1472915
2,4,6-Trichlorophenol ND 0.0100 1 05/09/202010:51 WG1472915
(5)Nitrobenzene-d5 58.6 15.0-314 05/09/2020 10:51 WG1472915
(5)2-Fluorobiphenyl 61.7 22.0-127 05/09/2020 10:51 WG1472915
(5)p-Terphenyl-d14 72.6 29.0-141 05/09/202010:51 WG1472915
(S)PhenoLd5 25.6 8.00-424 05/09/202010:51 WG1472915
(S)2-Fluorophenol 38.9 10.0-120 05/09/202010:51 WG1472915
(5)2,4,6-Tribromophenol 65.0 10.0-153 05/09/2020 10:51 WG1472915

VVVI'tIGIJI LitVHL1I I L.LiIV 1 I-CVL JVIVIIVIHK T l.JINGL/-\c.rvHIIJi'VVIIJC. 4111117.
/olatlle Organic Compounds (GC/MS) by Method 624.1 L1215360-01
Method Blank (MB)
MB)R3525651-2 05/07/20 13:07
MB Result MB Qualifier MB MDL MB RDL
\nalyte mg/I mg/I mg/I Tc
icrolein U 0.00254 0.0500
lcrylonitrlle U 0.000671 0.0100 3 SS
3enzene U 0.0000941 0.00100
3romodichloromethane U 0.000136 0.00100 4
3romoform U 0.000129 0.00100 Cn
3romomethane U 0.000605 0.00500
2arbon tetrachloride U 0.000128 0.00100 'Sr
2hlorabenzene U 0.000116 0.00100
2hlorodibromomethane U 0.000140 0.00100 6
Thloroethane U 0.000192 0.00500 Qc
2-Chloroethyl vinyl ether U 0.000575 0.0500
2hloroform U 0.000111 0.00500 /GI
:hloromethane U 0.000960 0.00250
1,2-Dichlorobenzene U 0.000107 0.00100
1,3-Dichlorobenzene U 0.000110 0.00100 Al
l,4-Dlchlorobenzene U 0.000120 0.00100
)ichlorodifluoromethane U 0.000374 0.00500 Sc„
1,1-Dichloroethane U 0.000100 0.00100
1,2-Dichloroethane U 0.0000819 0.00100
1,1-Dichloroethene U 0.000188 0.00100
trans-1,2-Dichloroethene U 0.000149 0.00100
1,2-Dichloropropane U 0.000149 0.00100
cis-1,3-Dichloropropene U 0.000111 0.00100
trans-1,3-Dichloropropene U 0.000118 0.00100
Ethylbenzene U 0.000137 0.00100
Methylene Chloride U 0.000430 0.00500
Methyl tert-butyl ether U 0.000101 0.00100
Naphthalene U 0.00100 0.00500
1,1,2,2-Tetrachloroethane U 0.000133 0.00100
Tetrachloroethene U 0.000300 0.00100
Toluene U 0.000278 0.00100
1,1,1-Trichloroethane U 0.000149 0.00100
1,1,2-Trichloroethane U 0.000158 0.00100
Trichloroethene U 0.000190 0.00100
Trichlorofluoromethane U 0.000160 0.00500
Vinyl chloride U 0.000234 0.00100
(S)Toluene-d8 112 80.0-120
(S)4-Bromof1uorobenzene 107 80.0-120
(S)1,2-Dichloroethane-d4 101 70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

rvvr-ricr.:./ r htUHLI I T IrVIV I KVL JVI II I
VIVk LAC.INA I IVIVVVIUk.
'olatile Organic Compounds (GC/MS) by Method 624.1 L1215360-01
.aboratory Control Sample (LCS)
-CS)R3525651-1 05/07/2012:28AI
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
nalyte mg/I mg/I % % Tc
crolein 0.0250 0.0156 62.4 60.0-140
crylonitrile 0.0250 0.0222 88.8 60.0-140 3SS
enzene 0.00500 0.00523 105 65.0-135
romodichloromethane 0.00500 0.00470 94.0 70.0-135 4
romoform 0.00500 0.00453 90.6 70.0-130 Cn
romomethane 0.00500 0.00305 61.0 15.0-185 '
arbon tetrachloride 0.00500 0.00573 115 70.0-130 4S1-
hlorobenzene 0.00500 0.00541 108 65.0-135
hlorodibromomethane 0.00500 0.00499 99.8 70.0-135 6
:hloroethane 0.00500 0.00524 105 40.0-160 QC
-Chloroethyl vinyl ether 0.0250 0.0227 90.8 0.100-225
:hloroform 0.00500 0.00481 96.2 70.0-135 z GI
:hloromethane 0.00500 0.00426 85.2 0.100-205
,2-Dlchlorobenzene 0.00500 0.00545 109 65.0-135
,3-Dichlorobenzene 0.00500 0.00532 106 70.0-130 Al
,4-Dlchlorobenzene 0.00500 0.00529 106 65.0-135
lichlorodifluoromethane 0.00500 0.00801 160 49.0-155 .J4 9
SC
,1-Dichloroethane 0.00500 0.00520 104 70.0-130
,2-Dichloroethane 0.00500 0.00501 100 70.0-130
,1-Dichloroethene 0.00500 0.00614 123 50.0-150
pans-1,2-Dichloroethene 0.00500 0.00565 113 70.0-130
,2-Dichloropropane 0.00500 0.00494 98.8 35.0-165
is-1,3-Dichloropropene 0.00500 0.00496 99.2 25.0-175
raps-1,3-Dichloropropene 0.00500 0.00491 98.2 50.0-150
thylbenzene 0.00500 0.00573 115 60.0-140
Aethylene Chloride 0.00500 0.00515 103 60.0-140
Aethyl tert-butyl ether 0.00500 0.00503 101 64.0-123
laphthalene 0.00500 0.00431 86.2 62.0-128
,1,2,2-Tetrachloroethane 0.00500 0.00504 101 60.0-140
-etrachloroethene 0.00500 0.00533 107 70,0-130
oluene 0.00500 0.00516 103 70.0-130
1,1-Trichloroethane 0.00500 0.00570 114 70.0-130
,1,2-Trichloroethane 0.00500 0.00566 113 70.0-130
'richloroethene 0.00500 0.00544 109 65.0-135
'richlorofluoromethane 0.00500 0.00605 121 50.0-150
tinyl chloride 0.00500 0.00532 106 5.00-195
(S)Toluene-d8 113 80.0-120
(S)4-Bromofluorobenzene 109 80.0-120
(S)1,2-Dichloroethane-d4 102 70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

V v r-I'i I J`t J Vt V H L l I I 1.Li I V I I'c V L .)U IVI IVI/-1 fC T
LJIVG LHG.IVH I IUIVVVIUt. ilk
esticides (GC) by Method EPA 608.3 L1215360-01
Method Blank (MB)
CD
AB)R3525889-1 05/08/20 00:14
MB Result MB Qualifier MB MDL MB RDL
2
nalyte mg/I mg/I mg/I TC
Idrin U 0.0000198 0.0000500
Ipha BHC U 0.0000172 0.0000500 3
SS
eta BHC U 0.0000208 0.0000500
elta BHC U 0.0000150 0.0000500 4
amma BHC U 0.0000209 0.0000500 Cn
,4-DDD U 0.0000177 0.0000500
,4-DDE U 0.0000154 0.0000500 5
Sr
.4-DDT U 0.0000198 0.0000500
ieldrin U 0.0000162 0.0000500 5
ndosulfan I U 0.0000160 0.0000500 QC
ndosulfan II U 0.0000164 0.0000500
ndosulfan sulfate U 0.0000217 0.0000500 'GI
ndrin U 0.0000161 0.0000500
ndrin aldehyde U 0.0000237 0.0000500
ndrin ketone U 0.0000219 0.0000500 Al
leptachlor U 0.0000148 0.0000500
leptachlor epoxide U 0.0000183 0.0000500 0
SC
Iexachlorobenzene U 0.0000176 0.0000500
lethoxychlor U 0.0000193 0.0000500
:hlordane U 0.0000198 0.00500
oxaphene U 0.000168 0.000500
(S)Decachlorobiphenyl 75.7 10.0-144
(S)Tetrachloro-m-xylene 93.3 10.0-135
-aboraltory Control Sample (LCS)
_CS)R3525889-2 05/08/20 00:26
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
,nalyte mg/I mg/I % %
,Idrin 0.00100 0.000688 68.8 42.0-140
,Ipha BHC 0.00100 0.000972 97.2 37.0-140
:eta BHC 0.00100 0.000936 93.6 17.0-147
lelta BHC 0.00100 0.00101 101 19.0-140
;amma BHC 0.00100 0.000993 99.3 32.0-140
,4-DDD 0.00100 0.000968 96.8 31.0-141
,4-DDE 0.00100 0.000936 93.6 30.0-145
,4-DDT 0.00100 0.00101 101 25.0-160
lieldrin 0.00100 0.000957 95.7 36.0-146
:ndosulfan I 0.00100 0.000981 98.1 45.0-153
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

V t7 l•t/ IJYJ i lJ/-k LI I 1 L.Li IN I KLJL .D LJ IVI IVI f-1 i- T UIVt LP.G.NM I IUNVVILit. 41r.
?sticides (GC) by Method EPA 608.3 L1215360-01
9boratory Control Sample (LCS) F
3S)83525889-2 05/08/20 00:26 1 '-,1..
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
lalyte mg/I mg/I % % Tc
dosulfan II 0.00100 0.000990 99.0 1.00-202
,dosulfan sulfate 0.00100 0.000931 93.1 26.0-144 3SS
idrin 0.00100 0.000955 95.5 30.0-147
idrin aldehyde 0.00100 0.000964 96.4 56.0-128 4
idrin ketone 0.00100 0.000947 94.7 54.0-142 Cn
?ptachlor 0.00100 0.000727 72.7 34.0-140
?.ptachlor epoxide 0.00100 0.000952 95.2 37.0-142 5
Sr
txachlorobenzene 0.00100 0.000837 83.7 35.0-120
athoxychlor 0.00100 0.000976 97.6 44.0-160 6
(S)Decochlorobiphenyl 85.1 10.0-144 Qc
(S)Tetrochloro-m-xylene 96.2 10.0-135
GI
1214940-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
)S)L1214940-02 05/08/20 02:18•(MS)R3525889-3 05/08/20 02:31•(MSD)R3525889-4 05/08/20 02:43 Al
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
ialyte mg/I mg/I mg/I mg/I % % % % % SC
drin 0.00100 U 0.000846 0.000759 84.6 75.9 1 42.0-140 10.8 35
pha BHC 0.00100 U 0.000890 0.000929 89.0 92.9 1 37.0-140 4.29 36
sta BHC 0.00100 U 0.000695 0.000912 69.5 91.2 1 17.0-147 27.0 44
elta BHC 0.00100 U 0.000982 0.000971 98.2 97.1 1 19.0-140 1.13 52
smma BHC 0.00100 U 0.000909 0.000950 90.9 95.0 1 32.0-140 4.41 39
4-DDD 0.00100 U 0.00102 0.000986 102 98.6 1 31.0-141 3.39 39
4-DDE 0.00100 U 0.000971 0.000950 97.1 95.0 1 30.0-145 2.19 35
4-DDT 0.00100 U 0.00101 0.00103 101 103 1 25.0-160 1.96 42
ieldrin 0.00100 U 0.000924 0.000890 92.4 89.0 1 36.0-146 3.75 49
idosulfan I 0.00100 U 0.000826 0.000885 82.6 88.5 1 45.0-153 6.90 28
idosulfan II 0.00100 U 0.000944 0.000966 94.4 96.6 1 1.00-202 2.30 53
ldosulfan sulfate 0.00100 U 0.000556 0.000894 55.6 89.4 1 26.0-144 J3 46.6 38
idrin 0.00100 U 0.000998 0.000986 99.8 98.6 1 30.0-147 1.21 48
idrin aldehyde 0.00100 U 0.000892 0.000928 89.2 92.8 1 56.0-128 3.96 20
Kdrin ketone 0.00100 U 0.000588 0.000676 58.8 67.6 1 54.0-142 13.9 20
eptachlor 0.00100 U 0.000885 0.000789 88.5 78.9 1 34.0-140 11.5 43
eptachlor epoxide 0.00100 U 0.000886 0.000903 88.6 90.3 1 37.0-142 1.90 26
exachlorobenzene 0.00100 U 0.00127 0.000795 127 79.5 1 35.0-120 J5 J3 46.0 25
:ethoxychlor 0.00100 U 0.00104 0.00103 104 103 1 44.0-160 0.966 22
(S)Decachlarobiphenyl 95.4 88.7 10.0-144
(S)Tetrochloro-m-xylene 86.5 81.9 10.0-135
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

V V I T/ I J T J - V(u H L I I I \--V IN I L
UIVt LAC.NA IUIVVVIUt. ipt
,lychlorinated Blphenyls (GC) by Method EPA-608.3 11215360-01
ethod Blank (MB) c--
B)R3525990-1 05/07/20 16:44 ICI,
MB Result MB Qualifier MB MDL M8 RDL
2
alyte mg/I mg/I mg/I Tc
B 1260 U 0.000173 0.000500
81016 U 0.000270 0.000500 3 SS
B 1221 U 0.000270 0.000500
8 1232 U 0.000270 0.000500
B 1242 U 0.000270 0.000500 a C n
8 1248 U 0.000173 0.000500
81254 U 0.000173 0.000500 5
Sr
tal PCBs U 0.000173 0.000500
(S)Decochlorobiphenyl 82.2 10.0-144
(S)Tetrochtoro-m-xylene 84.7 10.0-135 6 Qc
3boratory Control Sample (LCS) 7GI
2S)R3525990-2 05/07/20 16:58 L
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Al
alyte mg/I mg/I % %
19 1260 0.00250 0.00258 103 8.00-140 SC
:13 1016 0.00250 0.00214 85.6 50.0-140
(S)Decochlorobiphenyl 93.8 10.0-144
(S)Tetrochloro-m-xylene 90.3 10.0-135
1214940-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
IS)L1214940-02 05/07/20 17:12•(MS)R3525990-3 05/07/20 17:26•(MSD)R3525990-4 05/07/20 17:40
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
lalyte mg/I mg/I mg/I mg/I % % % %
31260 0.00250 U 0.00188 0.00247 75.2 98.8 1 8.00-140 271 38
;13 1016 0.00250 U 0.00740 i 0.00254 296 102 1 50.0-140 .15 P J3 97.8 36
(S)Decochlorobiphenyl 85.5 103 10.0-144
(S)Tetrochloro-m-xy/ene 79.3 96.2 10.0-135
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

!VI'-t/ LJIJ l,(UHLI I T I.VIV I KVL JUIVIIVIHK
VIVO LNG.IVN I IIJIVVVILJt.
mi Volatile Organic Compounds (GC/MS) by Method 625.1 L1215360-01
ethod Blank (MB) (-----
,
B)93526229-2 05/09/20 06:04
MB Result MB Qualifier MB MDL MB RDL
alyte mg/I mg/I mg/I TC
?naphthene U 0.0000886 0.00100
=.naphthyIene U 0.0000921 0.00100 Ss
thracene U 0.0000804 0.00100
)benzene U 0.000105 0.0100 4
nzidine U 0.00374 0.0100 Cn
nzo(a)anthracene U 0.000199 0.00100
nzo(b)fluoranthene U 0.000130 0.00100
'Sr
nzo(k)fluoranthene U 0.000120 0.00100
nzo(g,h,i)perylene U 0.000121 0.00100 6
nzo(a)pyrene U 0.0000381 0.000200 QC
(2-chlorethoxy)methane U 0.000116 0.0100
.(2-chloroethyl)ether U 0.000137 0.0100 7 GI
!-Oxybis(1-Chloropropane) U 0.000210 0.0100
iromophenyl-phenylether U 0.0000877 0.0100
:hloronaphthalene U 0.0000648 0.00100 AI
;hlorophenyl-phenylether U 0.0000926 0.0100
rysene U 0.000130 0.00100 "SC
penz(a,h)anthracene U 0.0000644 0.000200
3-Dichlorobenzidine U 0.000212 0.0100
i-Dinitrotoluene U 0.0000983 0.0100
i-Dinitrotoluene U 0.000250 0.0100
Ioranthene U 0.000102 0.00100
Iorene U 0.0000844 0.00100
!xachlorobenzene U . 0.0000755 0.00100
!xachloro-1,3-butadiene U 0.0000968 0.0100
+xachlorocyclopentadlene U 0.0000598 0.0100
•xachloroethane U 0.000127 0.0100
Jeno(1,2,3-cd)pyrene U 0.000279 0.00100
>phorone U 0.000143 0.0100
Iphthalene U 0.000159 0.00100
trobenzene U 0.000297 0.0100
Vitrosodlmethylamine U 0.000998 0.0100
Vitrosodiphenylamine U 0.00237 0.0100
iitrosodi-n-propylamine U 0,000261 0.0100
,enanthrene U 0.000112 0.00100
mzylbutyl phthalate U 0.000765 0.00300
s(2-ethylhexyl)phthalate U 0.000895 0.00300
-n-butyl phthalate U 0.000453 0.00300
ethyl phthalate U 0.000287 0.00300
methyl phthalate U 0.000260 0.00300
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

V 1't/ L/ I:) h1 V/-k L I I I L.U I V I 1-<U L J U IVI IVI/H K Y UNt LAC.NA I IUNVVIUt. Ar
mi Volatile Organic Compounds (GC/MS) by Method 625.1 L1215360-01
ethod Blank (MB)
3)R3526229-2 05/09/20 06:04 JJ
L..-�
MB Result MB Qualifier MB MDL MB RDL
rlyte mg/I mg/I mg/I Tc
i-octyl phthalate U 0.000932 0.00300
ene U 0.000107 0.00100 3
SS
4-Trichlorobenzene U 0.0000698 0.0100
hloro-3-methylphenol U 0.000131 0.0100 4
.hlorophenol U 0.000133 0.0100 Cn
-Dichlorophenol U 0.000102 0.0100
-Dimethylphenol U 0.0000636 0.0100 tiS•
I
-Dinitro-2-methylphenol U 0.00112 0.0100
-Dinitrophenol U 0.00593 0.0100 6
litrophenol U 0.000117 0.0100 QC
litrophenol U 0.000143 0.0100
itachlorophenol U 0.000313 0.0100 'GI
anol U 0.00433 0.0100
,6-Trichlorophenol U 0.000100 0.0100
S Nitrobenzene-d5 61.0 15.0-314 Al
S)2-Fluorobiphenyl 69.0 22.0-127
5)p-Terphenyl-d14 69.0 29.0-141 `SC
5)Phenol-d5 23.1 8.00-424
S)2-Fluorophenol 37.2 10.0-120
5)2,4,6-Trlbromophenol 70.0 10.0-153
lboratory Control Sample (LCS)
:S)R3526229-1 05/09/20 05:44
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
alyte mg/I mg/I % %
nnaphthene 0.0500 0.0322 64.4 47.0-145
!-Oxybls(1-Chloropropane) 0.0500 0.0296 59.2 36.0-166
nnaphthylene 0.0500 0.0351 70.2 33.0-145
thracene 0.0500 0.0338 67.6 27.0-133
Dbenzene 0.0500 0.0365 73.0 37.0-125
nzidine 0.100 0.0246 24.6 1.00-120
nzo(a)anthracene 0.0500 0.0352 70.4 33.0-143
nzo(b)fluoranthene 0.0500 0.0343 68.6 24.0-159
nzo(k)fluoranthene 0.0500 0.0327 65.4 11.0-162
nzo(g,h,i)perylene 0.0500 0.0308 61.6 1.00-219
nzo(a)pyrene 0.0500 0.0333 66.6- 17.0-163
,(2-chlorethoxy)methane 0.0500 0.0282 56.4 1.00-219
;(2-chloroethyl)ether 0.0500 0.0305 61.0 33.0-185
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

v171•-t/ LJIJ h1VHLI I T I..VIV I KUL
VIVt-LP,G.NH I KJIVVVIUC. • fit,
emi Volatile Organic Compounds (GC/MS).by Method 625.1 L1215360-01
aboratory Control Sample (LCS) `
CS)R3526229-1 05/09/20 05:44 I GIB
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
ialyte mg/I mg/I % % 2Tc
8romophenyi-phenylether 0.0500 0.0341 68.2 53.0-127
•Chloronaphthalene 0.0500 0.0317 63.4 60.0-120 3SS
Chlorophenyl-phenylether 0.0500 0.0347 69.4 25.0-158
nrysene 0.0500 0.0318 63.6 17.0-168 4
ibenz(a,h)anthracene 0.0500 0.0323 64.6 1.00-227 Cn
3-Dichlorobenzidine 0.100 0.0662 66.2 1.00-262
.4-Dinitrotoluene 0.0500 0.0378 75.6 39.0-139 ''Sr
.6-Dinitrotoluene 0.0500 0.0348 69.6 50.0-158
uoranthene 0.0500 0.0353 70.6 26.0-137 6
uorene 0.0500 0.0345 69.0 59.0-121 QC
exachlorobenzene 0.0500 0.0329 65.8 1.00-152
exachloro-1,3-butadlene 0.0500 0.0298 59.6 24.0-120 GI
exachlorocyclopentadiene 0.0500 0.0227 45.4 10.0-120
exachloroethane 0.0500 0.0298 59.6 40.0-120
ideno(1,2,3-cd)pyrene 0.0500 0.0318 63.6 1.00-171 Al
.ophorone 0.0500 0.0277 55.4 21.0-196
aphthalene ;0.0500 0.0276 55.2 21.0-133 9SC
itrobenzene 0.0500 0.0268 53.6 35.0-180
-Nitrosodimethylamine 0.0500 0.0171 34.2 10.0-120 •
-Nitrosodiphenylamine 0.0500 0.0319 63.8 44.0-120
-Nltrosodl-n-propylamine 0.0500 0.0291 58.2 1.00-230
henanthrene 0.0500 0.0318 63.6 54.0-120
enzylbutyl phthalate 0.0500 0.0346 69.2 1.00-152
.is(2-ethylhexyl)phthalate 0.0500 0.0352 70.4 8.00-158
II-n-butyl phthalate 0.0500 0.0379 75.8 1.00-120
iiethyl phthalate 0.0500 0.0367 73.4 1.00-120
ilmethyl phthalate 0.0500 0.0341 68.2 1.00-120 •
ii-n-octyl phthalate 0.0500 0.0355 71.0 4.00-146
yrene 0.0500 0.0313 62.6 - 52.0-120
,2,4-Trichlorobenzene 0.0500 0.0286 57.2 44.0-142
-Chioro-3-methylphenol 0.0500 0.0279 55.8 22.0-147
•-Chlorophenol 0.0500 0.0275 55.0 23.0-134
:,4-Dichlorophenol • 0.0500 0.0286 57.2 39.0-135
:,4-Dimethylphenol 0.0500 0.0273 54.6 32.0-120
,6-Dinitro-2-methylphenol 0.0500 0.0352 70.4 1.00-181
,4-Dinitrophenol 0.0500 0.0382 76.4 1.00-191
:-Nitrophenol 0.0500 0.0304 60.8 29.0-182.
r-Nltrophenol 0.0500 0.0172 34.4 1.00-132
'entachlorophenol 0.0500 0.0346 69.2 14.0-176
'henol 0.0500 0.0133 26.6 5.00-120
ACCOUNT: PROJECT:' SDG: • DATE/TIME: PAGE:

,, v ,-r• „ ,v V1V/-1L1 I I C. JIN I r\.JL JVIVIIVI/- T VIVt LAM.NAIIONWIL)t. iiK
,emi Volatile Organic Compounds (GC/MS) by Method 625.1 L12.15360-01
.aboratory Control Sample (LCS) __..._
_CS)R3526229-1 05/09/20 05:44 ---P
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
naiyte mg/I mg/I % % 1.2
Tc
,4,6-Trichiorophenol 0.0500 0.0334 66.8 37.0-144
(S)Nitrobenzene-d5 52.5 15.0-314 s
(S)2-Fluoroblpheny/ 66.4 22.0-127 SS
(S)p-Terphenyl-d14 63.8 29.0-141
4
(S):Phenol-d5
23.6 8.00-424 Cn
(S)2-Fluorophenol 37.9 10.0-120
(S)2,4,6-1'ribromopheno! 64.5 10.0-153
s
Sr
_1215360-01 Original Sample (OS) • Matrix Spike (MS) 6Qc
DS)L1215360-01 05/09/20 10:51•(MS)R3526229-3 05/09/20 11:11
Spike Amount Original Result MS Result MS Rec. Dilution Rec.Limits MS Qualifier GI
naiyte mg/I mg/i mg/I % %
,2-0xybis(1-Chloropropane) 0.0500 ND 0.0262 52.4 1
36.0-166 f
cenaphthene 0.0500 ND 0.0285 57.0 1 47.0445 Al
cenaphthylene 0.0500 ND 0.0310 62.0 1 33.0-145
nthracene 0.0500 ND 0.0299 59.8 1 27.0-133 9SSC
enzldine 0.100 ND ND 0.000 1 1.00-120 Jt5
enzo(a)anthracene 0.0500 ND 0.0307 61.4 1 33.0-143
enzo(b)fluoranthene 0.0500 ND 0.0297 59.4 1 24.0-159
enzo(k)fluoranthene 0.0500 ND 0.0284 56.8 ' 1 11.0-162
enzo(g,h,i)peryiene 0.0500 ND 0.0296 59.2 1 1.00-219
enzo(a)pyrene 0.0500 ND 0.0290 58.0 1 17.0-163
is(2-chlorethoxy)methane 0.0500 ND 0.0257 51.4 1 33.0-184
is(2-chloroethyl)ether 0,0500 ND 0.0203 40.6 1 12.0-158
-Bromophenyi-phenylether 0.0500 ND 0.0314 62.8 1 53.0-127
-Chiaronaphthalene 0.0500 ND 0.0275 55.0 1 60.0-120 J6
-Chlorophenyl-phenylether 0.0500 ND 0.0311 62.2 1 25.0-158
2-Diphenyihydrazine 0.0500 ND 0.0324 64.8 1 18.0-156
hrysene 0.0500 ND 0.0276 55.2 1 17.0-168
ibenz(a;h)anthraeene 0.0500 ND 0.0297 59.4 1 1.00-227
,3-Dichlorobenzidine 0.100 ND 0.0434 43.4 1 1.00-262
4-Dinitrotoluene 0.0500 ND 0.0331 66.2 1 39.0-139
,6-Dinitrotoluene 0.0500 ND 0.0311 62.2 1 50.0-158
luoranthene 0.0500 ND 0.0274 54.8 1 26.0-137 •
luorene 0.0500 ND 0.0308 61.6 1 59.0-121
exachlorobenzene 0.0500 ND 0.0301 60.2 1 1.00-152
exachioro-1,3-butadiene 0.0500 ND 0.0275 55.0 1 24.0-120
exachlorocyclopentadiene 0.0500 ND 0.0213 42.6 1 10.0-146
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

VVI'-1-/ Gz' 1J La/UHLI I l-. JIN I KVL JUIVIIVI/-kNT I.JINtLHO..IVHIItJIWVIVt. 411r,
>mi Volatile Organic Compounds (GC/MS) by Method 625.1 L1215360-01
1215360-01 Original Sample (OS) • Matrix Spike (MS)
S)L1215360-01 05/09/20 10:51•(MS)R3526229-3 05/09/20 11:11 ' ..,1.,
Spike Amount Original Result MS Result MS Rec. Dilution Rec.Limits MS Qualifier alyte mg/I mg/I mg/I % % TC
rxachloroethane 0.0500 ND 0.0261 52.2 1 40.0-120
ieno(1,2,3-cd)pyrene 0.0500 ND 0.0299 59.8 1 1.00-171 ,SS
Iphorone 0.0500 ND 0.0246 49.2 1 21.0-196
Iphthalene 0.0500 ND 0.0245 49.0 1 21.0-133 4
trobenzene 0.0500 ND 0.0241 48.2 1 35.0-180 Cn
Nitrosodimethylamine 0.0500 ND 0.0153 30.6 1 10.0-120
Nitrosodiphenylamine 0.0500 ND 0.0288 57.6 1 16.0-160 Srl
Nitrosodi-n-propylamine 0.0500 ND 0.0255 51.0 1 1.00-230
lenanthrene 0.0500 ND 0.0281 56.2 1 54.0-120 6
?nzylbutyl phthalate 0.0500 ND 0.0345 69.0 1 1.00-152 Qc
s(2-ethylhexyl)phthalate 0.0500 ND 0.0341 68.2 1 8.00-158
-n-butyl phthalate 0.0500 ND 0.0335 67.0 1 1.00-120 'GI
ethyl phthalate 0.0500 ND 0.0320 64.0 1 1.00-120
methyl phthalate 0.0500 ND 0.0307 61.4 1 1.00-120
-n-octyl phthalate 0.0500 ND 0.0308 61.6 1 4.00-146 Al
'rene 0.0500 ND 0.0326 65.2 1 52.0-120
>-,4-Trichlorobenzene 0.0500 ND 0.0256 51.2 1 44.0-142 Sc'
Chloro-3-methylphenol 0.0500 ND 0.0256 51.2 1 22.0-147
Chlorophenol 0.0500 ND 0.0244 48.8 1 23.0-134
4-Dlchlorophenol 0.0500 ND 0.0270 54.0 1 39.0-135
4-Dimethylphenol 0.0500 ND 0.0252 50.4 1 32.0-120
6-Dinitro-2-methylphenol 0.0500 ND 0.0298 59.6 1 1.00-181
4-Dinitrophenol 0.0500 ND 0.0326 65.2 1 1.00-191
Nitrophenol 0.0500 ND 0.0284 56.8 1 29.0-182
Nitrophenol 0.0500 ND 0.0135 27.0 1 1.00-132
tntachlorophenol 0.0500 ND 0.0288 57.6 1 14.0-176
tenol 0.0500 ND 0.0112 22.4 1 5.00-120
4,6-Trichlorophenal 0.0500 ND 0.0310 62.0 1 37.0-144
(S)Nitrobenzene-d5 46.8 15.0-314
(S)2-Fluorobiphenyl 60.3 22.0-127
(S)p-Terphenyl-d14 71.1 29.0-141
(S)Phenol-d5 28.2 8.00-424
(S)2-Fluorophenol 34.0 10.0-120
(S)2,4,6-Tribromophenol 65.0 10.0-153
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

GLOSSARY OF TERMS ONE LAB.NATIONWIDE .k
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation,and if you have additional questions please contact your project representative.
Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, Ti
Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and
Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received.
Abbreviations and Definitions Ss
MDL Method Detection Limit.
4
ND Not detected at the Reporting Limit(or MDL where applicable). Cn
RDL Reported Detection Limit.
Rec. Recovery. •
Sr
RPD Relative Percent Difference.
SDG Sample Delivery Group.`
Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control Sample/Duplicate and JQc
(S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit(or MDL where applicable). 111
Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the A
Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used In this field,the
result reported has already been corrected for this factor. 9
These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal 5C
Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control
sample.The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was
no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL"
Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL
(Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results,including a discussion of any non-conformances to protocol
Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary Control
analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not
being performed on your samples typically,but on laboratory generated material.
This is the document created in the field when your samples were initially collected.This is used to verify the time and
Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This
Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis:
This section of your report will provide the results of all testing performed on your samples.These results are provided
Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and
times of preparation and/or analysis.
Qualifier Description
J3 The associated batch QC was outside the established quality control range for precision.
J4 • The associated batch QC was outside the established quality control range-for accuracy. -
J5 The sample matrix interfered with the ability to make any accurate determination;spike value is high.
J6 The sample matrix interfered with the ability to make any accurate determination;spike value is low.
P RPD between the primary and confirmatory analysis exceeded 40%.
. ..... _... ..__....._.. .. . ..

ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE. *
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other lab is as
accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry.The most significant benefit to our one location design is the design of our laboratory campus.The model is conducive to accelerated productivity,decreasing
turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. L_,
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
'Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. _
Tc
State Accreditations
Alabama 40660 Nebraska NE-OS-15-05 SS
Alaska 17-026 Nevada TN-03-2002-3
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey—NELAP TN002 C n
California 2932 New Mexico' n'a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Er:375 c
Florida E87487 North Carolina' DC121704
Georgia ___... NELAP North Carolina' c' --
Georgia' 923 North Dakota R-140 ,
Idaho TN00003 Ohio—VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002 ,---
Iowa 364 Pennsylvania 68-02979
Kansas E 10277 Rhode Island LA000356
Kentucky 16 90010 South Carolina 84004 a
Kentucky' 16 South Dakota n/a
Louisiana A130792 Tennessee" 2006
Texas
.. .. Sc
Louisiana' LA180010 T T10470424518 15 9SC
Maine TN0002 Texas LA80152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Third Party Federal Accredi-tations
A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 _, ......................._.....
A2LA—ISO 17025 5 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
'Drinking Water 'Underground Storage Tanks 'Aquatic Toxicity 6 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies.If you would like assistance from one of our support offices,please contact
our main office.Pace National performs all testing at our central laboratory.
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(Billing Information:,, Analysis/Contar• r)Preservative — --.-.s,.., -
TBL Environmental
Laboratory , Inc.
2401 W. 5th St E .
Lumberton, NC 28358 AePorito: 1
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(910) 738- 19 0 , . ti_ �._.__
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{ Same Day 200% 5'PS-- '-'0. No.
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Two Day.. 50% FAX? No Yes of { , `�u 1 Immediately racked an Ice N ` Three Dee _ 25°I° — q� Shipped Via:
Cntrs
Sample ID Comp/Grab tvlatcle Depth Date • Time _ W Remarks/Contaminant Sample#(lab only}
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Reline fished : Signe re) �i Date: Time:. 7 Received b gnat're) •MOI-eS re.turned via:0 UPS Condition: -(lab use only)
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Pace Analytical National Center for Testing & Innovation
• Cooler Receipt Form
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Received By: Sandy Yossef
r�'��ix,.� t"f
r
Sig' nature. t n(1 _i s
AS 5
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COC Seal Present/ Intact?
COcSigned'/Accurate?
Bottles arrive intact?
Correct bottles used?
Sufficient volume sent?
i{��9, 1.� ,3 m. �s�.s��5'.�'�'95z:at4x r'v.�.L.6a"M.:� �ilh�e� •.. �'`r:�. � �`t'..v w..�xa,€ xt',�ni� �4w��es1�� '.�.>E.. a .� � ,. �rr..�.,.
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