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HomeMy WebLinkAboutNCG120064_DMR_20200807M, July 29, 2020 Chambers Development of NC, Inc. and Waste Connections of the Carolinas, Inc. Anson Waste Management Facility 375 Dozer Road Polkton, NC 28135 Attention: Mr. Tyler Fitzgerald Reference: Monthly Stormwater Monitoring Anson Waste Management Facility Polkton, North Carolina S&ME Project No. 4140-15-007 Dear Mr. Fitzgerald: S&ME, Inc. (S&ME) is pleased to submit this report detailing the results of the July 2020 stormwater monitoring activities conducted at the Anson Waste Management Facility (AWMF) in Polkton, North Carolina. This work was completed in accordance with our Master Services Agreement dated January 2, 2017, and in accordance with Task 2 in S&ME Proposal No. 41-1600394 (Rev. 1) dated August 8, 2016. This letter summarizes results of sampling efforts conducted by facility personnel. ® Background Stormwater sampling is required on a semi-annual basis as defined by the National Pollutant Discharge Elimination System (NPDES) General Permit for Landfills NCG120000 for the facility outfalls. The following outfalls are identified at the facility: Outfall 1, Outfall 2, Outfall 3, Outfall 4, Borrow Area North Outfall, and Borrow Area West Outfall. Outfall 2 was eliminated in August 2018 by the expansion of Sediment Basin 3 and, therefore, is no longer sampled. Monthly sampling has been initiated following December 2019 results at Outfall 3 and Outfall 4, in response to Tier 2 and Tier 3 response actions at the facility. Parameters for quantitative analysis include chemical oxygen demand (COD) per Standard Method (SM) 2540D, fecal coliform per SM 9222D, and total suspended solids (TSS) utilizing SM 2540D. In addition to the previously listed parameters, Outfall 1 and Outfall 3 are also sampled for chemical parameters associated with vehicle maintenance which include total petroleum hydrocarbons (TPH) per Environmental Protection Agency (EPA) Method 1664E and pH utilizing SM 4500. ® Stormwater Sampling and Quantitative Analyses AWMF personnel collected the July stormwater samples at two (2) designated outfall locations on July 21, 2020. The total rainfall for the July 21, 2020 storm event was reported as approximately 2.03 inches in 24 hours. Sampling was performed during that storm event. S&ME, Inc. 1 644 Eastern Star Road I Kingsport, TN 37663 1 p 423.349.2800 1 www.smeinc.com iv Monthly Stormwater Monitoring Anson Waste Management Facility S&ME Project No. 4140-15-007 Quantitative chemical laboratory results for the monitoring event are compared to benchmark values as established by your NPDES permit on the attached Discharge Monitoring Report (DMR). Parameter exceedances of benchmark values, if any were documented through field and laboratory analyses, are summarized in bold type below for your reference. Benchmark 120 100 1000 15 6-9 Outfall 3 Sed Basin 3 <25.0 29.2 800 <6.7 6.01 Outfall 4 Sed Basin 4 <25.0 17.2 420 ANR 6.94 ANR = Analvte not reauested and not reouired by the NPDES Permit mg/l= milligrams per liter CFU/ml= colony -forming units per milliliter The DMR is included with this letter as Attachment I for your signature and submittal to the North Carolina Department of Environmental Quality (NCDEQ), Division of Water Quality. The Laboratory Data Report for this sampling event is included as Attachment II for your records. ® Closure S&ME appreciates this opportunity to be of service to you and Waste Connections. We trust this information is responsive to your needs at this time. If you have any questions, please contact us at your convenience. Sincerely, S&ME, Inc. Lindsey O. Harris James R. Bruce Project Manager Senior Reviewer Attachments: Discharge Monitoring Report Laboratory Data Report Site SWPPP Map cc: Mike Lawyer, Fayetteville Regional Office Lana Brown, Waste Connections Nelson Breeden, Waste Connections of the Carolinas, Inc. Page 2 Attachments Attachment I Discharge Monitoring Report .E O 0� 7-- Z� a ❑ ++ = CL o � 0 ❑3 3❑ u a! � 9 35❑3 _ o N ❑ O 3 o t N a, 12 d ++ 0NO ❑❑❑ w LU 7 -, as+ c O N O ❑Q LU O Z 12 OED °- oaC CL a N N � 'IT co 01 01 U J O c Z 3 LLIU �0 W > N O� U Q C LL WWC O W G Q ZQ mZ U aO U. 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The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services- Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, C " Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 u ceAnalyiical www.pacelabs.com CERTIFICATIONS Project: Anson LF Stormwater Pace Project No.: 92487109 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 ceAnalyiical www.pocelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater Pace Project No.: 92487109 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92487109001 Outfall 3 92487109002 Outfall4 92487109003 Outfall1 PASI-A = Pace Analytical Services -Asheville PASI-C = Pace Analytical Services - Charlotte EPA 1664E HH 1 SM 9222D-2006 KDF 1 SM 254OD-2011 JNS 1 SM 5220D-2011 LMS1 1 SM 9222D-2006 KDF 1 SM 2540D-2011 JNS 1 SM 5220D-2011 LMS1 1 EPA1664B HH 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. PASI-C PASI-C PASI-A PASI-A PASI-C PASI-A PASI-A PASI-C Page 3 of 14 ,s oD aceAnalytical www.picelabs.com SUMMARY OF DETECTION Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater Pace Project No.: 92487109 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92487109001 Outfall 3 SM 9222D-2006 Fecal Coliforms 800 CFU/100 mL 1.0 07/22/20 13:07 SM 254OD-2011 Total Suspended Solids 29.2 mg/L 5.0 07/24/20 12:53 92487109002 Outfall 4 SM 9222D-2006 Fecal Coliforms 420 CFU/100 mL SM 2540D-2011 Total Suspended Solids 17.2 mg/L REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 1.0 07/2212013:07 3.8 07/24/2012:53 Page 4 of 14 laneAnalytical" www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater Pace Project No.: 92487109 Sample: Outfall 3 Lab ID: 92487109001 Collected: 07/21/20 08:19 Received: 07/21/20 09:54 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 6.7 1 07/25/20 10:36 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 800 CFU/100 mL 1.0 1 07/21/20 14:21 07/22/20 13:07 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 29.2 mg/L 5.0 1 07/24/20 12:53 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand ND mg/L 25.0 1 07/23/20 17:10 07/24/20 15:36 Sample: Outfall 4 Lab ID: 92487109002 Collected: 07/21/20 07:40 Received: 07/21/20 09:54 Matrix: Water LE Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Pace Analytical Services - Charlotte Fecal Coliforms 420 CFU/100 mL 1.0 1 07/21/20 14:21 07/22/20 13:07 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Pace Analytical Services -Asheville Total Suspended Solids 17.2 mg/L 3.8 1 07/24/20 12:53 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Pace Analytical Services -Asheville Chemical Oxygen Demand ND mg/L 25.0 1 07/23/20 17:10 07/24/20 15:36 Sample: Outfall 1 Lab ID: 92487109003 Collected: 07/21/20 08:33 Received: 07/21/20 09:54 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 10.0 1 07/25/20 10:36 Date: 07/27/2020 12:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 14 ?�IaceAnalj&al" www.pacelabs.com Project: Anson LF Stormwater Pace Project No.: 92487109 QC Batch: 555814 QC Batch Method: EPA 1664B Associated Lab Samples: 92487109001, 92487109003 METHOD BLANK: 2951873 Associated Lab Samples: 92487109001, 92487109003 Parameter Units Total Petroleum Hydrocarbons mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 07/25/2010:25 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2951874 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 15.1 76 64-132 MATRIX SPIKE SAMPLE: 2951875 92487109001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 26.7 ND 8 64-132 M1 Results presented on this page are In the units Indicated by the "Units'' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2020 12:30 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 �h arceAnalytical www.pecolobs.com Project: Anson LF Stormwater Pace Project No.: 92487109 QC Batch: 554797 QC Batch Method: SM 9222D-2006 Associated Lab Samples: 92487109001, 92487109002 QUALITY CONTROL DATA Analysis Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte METHOD BLANK: 2947221 Matrix: Water Associated Lab Samples: 92487109001, 92487109002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/22/20 13:07 SAMPLE DUPLICATE: 2947222 92487062003 Parameter Units Result Fecal Coliforms CFU/100 ml- 29.0 Dup Result RPD Qualifiers 100 110 D6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2020 12:30 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical www.pacefabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater Pace Project No.: 92487109 QC Batch: 555587 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92487109001, 92487109002 METHOD BLANK: 2950625 Matrix: Water Associated Lab Samples: 92487109001, 92487109002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 07/24/20 12:51 LABORATORY CONTROL SAMPLE & LCSD: 2950626 2950627 Spike LCS LCSD LCS LCSD % Rec Parameter Units Conc. Result Result % Rec % Rec Limits Total Suspended Solids mg/L 251 256 242 102 96 90-110 SAMPLE DUPLICATE: 2950628 92487406001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 194 200 3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Max RPD RPD Qualifiers 6 25 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2020 12:30 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 leAnalytical www.pacolabs.com QUALITY CONTROL DATA Project: Anson LF Stormwater Pace Project No.: 92487109 QC Batch: 555408 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92487109001, 92487109002 METHOD BLANK: 2950012 Matrix: Water Associated Lab Samples: 92487109001, 92487109002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L NO 25.0 07/24/20 15:32 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2950013 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 758 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2950014 2950015 MS MSD 92487100002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 114 121 97 104 90-110 6 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2950016 2950017 MS MSD 92487100003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 114 107 108 101 90-110 6 R1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2020 12:30 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 A aceAnaIXical www.pacelabs.com QUALIFIERS Project: Anson LF Stormwater Pace Project No.: 92487109 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2020 12:30 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 aceAnalytical 1 www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Anson LF Stormwater Pace Project No.: 92487109 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92487109001 Outfall 3 EPA 1664B 555814 92487109003 Outfall 1 EPA 1664E 555814 92487109001 Outfall 3 SM 9222D-2006 554797 SM 9222D-2006 554798 92487109002 Outfall 4 SM 9222D-2006 554797 SM 9222D-2006 554798 92487109001 Outfall 3 SM 2540D-2011 555587 92487109002 Outfall 4 SM 2540D-2011 555587 92487109001 Outfall 3 SM 5220D-2011 555408 SM 5220D-2011 555712 92487109002 Outfall4 SM 5220D-2011 555408 SM 5220D-2011 555712 Date: 07/27/2020 12:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 11 'A Document Name: Document Revised: February 7, 2019 aceAnalytical Sample Condition Upon Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority. F-CAR-CS•033•Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Aehouillo n Fdenn CUPentnto,oud n Htrntpreuille RaleiehD MechanicsyilleQ SamPle Conditi6n Client Name: Project H:WO# : 924871 09 • S 4-/Ht rwc . 'TIV Courier: ❑Fed Ex QUPS ❑USPS ❑Client ❑ Commercial [336ce []Other: 1111111111111111111111 92467209 _ ( Date/InitlalsPerson Examining Contents: i S( ��J Packing Material: Bubble Wrap u8ubble Bags ❑None ❑ Other Biological Tissue. FF9zen? Thermometer:. 92T061 Type of ice: wet []Blue [)None ❑Yes • ❑No 96/A b � R Gun 10: Cooler Temp (*Cl: 0, Ll Correction Factor: Add/Subtract ('C) 0.0 �. Temp should be above freezing to VC Cooler Temp Corrected (°C): — --f— ❑Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil (Z/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally, rive. f-lrun Including Hawaii and Puerto Rico)? Elves []NO Comments/Dlscrepancyi Chain of Custody Present? of, ON. ❑N/A 1. Samples Arrived within Hold Time? [ayes CINO ❑N/A 2. Short Hold Time Analysis (02 hr.)? Yes o N/A 3. Rush Turn Around Time Requested? Y/�es • No N/A 4. Sufficient Volume?�.,Y/ es []NO❑N/A 5. Correct Containers Used? [IN.❑N/A 6• -Pace Containers Used? es ONO EINIA Containers Intact? Yes ON. ❑N/A 7. Dissolved analysis: Samples Field Filtered? []yes l o ❑N/A 8. Sample Labels Match COC? Yes ❑No ❑N/A 9. -Includes Date/Time/ID/Analysis Matrix: VVr Headspace in VOA Vials (>S-6mm)? []Yes []No N/ 10. Trip Blank Present? []Yes []No ®/A 11. Trip Blank Custody Seals Present? Yes []No N/A COMMENTS/SAMPLE DISCREPANCY r Field Date Required? ❑Yes []No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: I'-1nYY 1 Project Manager SRF Review: f J1� %A — Date/Time: Date: —YrLP Date: Page 12 of 14 fit a �' 1C8AR8lytICc7J Document Name: Sample Condition Upon Recel t(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS•033-Rev.06 Issuing Authority: Pace Carolinas Quality Office *Check rnavir tap half of boat If H and/or dechlorination Is Project it 1 In fi Q2 A R71 fig verified and within the acceptance range for preservation samples. PM: AMB Due Date: 07/28/20 Exceptions: VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, UH8 CLIENT: 92-S&ME TN **Bottom half of box is to list number of bottle N bl a C CI E J E pO 8 ? Z C ► c J E N A L L v n 7 E J of Q S m a C 7 6. J E OQ. m v v n c 6 J E in N , 6 m v a c 7 1 J E o u1 d m d a n. C d P: _ r1 CL m a N = G. J E 6 m a O z = C' J E N 6 m O 4 m w `� 2 N K J E 6 m N a _ 2 v (L J E '`� 6 m Ey1 nc o = `� �j 5 EI� W. v_ 3 Z c 7 a Q •� 7 V' v n u i apy V ri U' z Gl m a - E J E o N i7 N n N S �Q l7 N V ° O s a4Cj J o N l7 ? v Z °10 E < -� o .. "Qi U' Z V a O J E 4 O� y`ia+i m 0 rv�vi N a O J E 4 l7 z a C ¢ O J E q Z a 1. m a J E q 6 p� o>> 2 M o u� m a ' Q \ Z X = a ,V .ii a Y D a y u vi v+ A Q \ N a N d E o N u, n V N x U _ a E 0 N m 1 Z 2 2 i� 3 4 S 6 7 6 9F7 F 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservition adjusted Amount of Preservative added Lot It ..( Nd. f— oral ho um to rhp Nnrth [aralina 0FHNR Certification Office (I.e. Note: Whenever there is a discrepancy attecung Nortn Carolina carnpu ILC o =Vrr Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 13 of 14 m$ m� 5 A o m g I CO Cc ./ m (n A' W tV A ITEM # c � 9 if 0 ?v z 0 r�0 0 m A W d w p f+ 7 o 'e m f+ "3 w m o ]CO) a D0 I N N 0 , a � J j .- m � c' r r � ap C a l 2 o o IL W O MATRI%GOOF (sea Valid codes to left) � � 2 SAMPLETYPE (G=GRAB C=COMP) ' t r m y Db rA o o 8 r Ell Z 3 m m m m 3 S� m � SAMPLE TEMP AT COLLECTION M re C # OF CONTAINERS �• lid - 3 v Unprosarved yH2SO4 IFm u p HNO3 m HCI M m NaOH / Na28203 M an Methanol m Other Anetyses7pM YIN s' $ m x x COD = ¢ { z 8 x x Fecal Cali (8 Hr Hold) m N �) 3 x X I TPH Oil and Grease by 166 x x TSS n ,S w TEMP in C A Residual Chlorine (YIN) Z n S d Received on Ice b I Z us e y Sealed Cooler YIN' j W 0 Samples Intact (Y/N) � n Page 14 of 14 Attachment III — Site SWPPP Map IF �1 W Z 0O 2S u U C) Z Z Q Ui �Q! z eliLn !Q Z<t w Q —+ Z¢ Y W Z M�wli1 4Lil UW� U 0 '3 W ~)� �� Wz O� WMY V) aLLi La V Q Li. w V U » fx m QQ' { } .f IN �, `' � it � � �. 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