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WQ0016247_Modification_20200805 (2)
Initial Review Reviewer Thornburg, Nathaniel Is this submittal an application? (Excluding additional information.)* r Yes r No Permit Number (IR)* WQ0016247 Applicant/Permittee Synagro Central, LLC Applicant/Permittee Address 284 Boger Rd Mocksville, INC 27028 Is the owner in BIMS? r Yes r No Is the facility in BIMS? r Yes r No Owner Type Organization Facility Name Synagro Western Piedmont RLAP County Alexander Fee Category Major Is this a complete application?* r Yes r No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Does this need review bythe hydrogeologist?* r Yes r No Regional Office CO Reviewer Admin Reviewer Fee Amount 395 Complete App Date 08/05/2020 Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Kendall Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Rease provide information on the person to be contacted by N B Staff regarding electibnittal, confirmation of receipt, other .......................................................... electronic surece, aner correspondence. _ - Name * Chris Wynne Email Address* cwynne@synagro.com Project Information ........ ......... ....................................................................................................................................... . Application/Document Type* r New (Fee Req ui red) c Modification - Major (Fee Required) r Renewal with Major Modification (Fee Required) r Annual Report r Additional Information r Other Phone Number* 3369098627 O Modification - Minor C Renewal C GW-59, NDMR, NDMLR, NDAR-1, NDAR-2 r Residual Annual Report r Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* r Wastewater Irrigation r High -Rate Infiltration r Other Wastewater r Reclaimed Water r Closed -Loop Recycle r Residuals r Single -Family Residence Wastewater r Other Irrigation Permit Number:* WQ0016247 Fbs Current Existing permt number Applicant/Permittee* Synagro Central, LLC Applicant/Permittee Address* 284 Boger Rd Mocksville, NC 27028 Facility Name * Synagro Western Piedmont RLAP Please provide comments/notes on your current submittal below. Modification of Synagro's Class B permit. Find all additional information in submittal. Thanks! At this time, paper copies are no longer required. If you have any questions about what is required, please contact Tessa Monday at tessa.monday@ncdenr.gov or (919) 707-3660. Please attach all information required or requested for this submittal to be reviewed here.* (Application Form Engineering Rans, Spec'rfications, Calculations, Rc.) Synagro Class B mod ification_Final_07242020.pdf 49.12MB upload only 1 RCF docurrent (less than 250 M3). Mitiple documents nest be corrbined into one RJF file unless file is larger than upload limit. * W By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature * 6 w Submission Date Is filled in automatically once submitted. SYNAGRO July 2411, 2020 N.C. Department of Environment and Natural Resources Division of Water Resources Water Quality Permitting Section -- Class B Residuals Permit 1617 Mail Service Center Raleigh, NC 27699-1617 ATTENTION: Mr. Nathaniel Thornburg REFERENCE: APPLICATION FOR MODIFICATION of Permit #WQ0016247 Synagro Western Piedmont, LLC Dear Mr. Thornburg: Synagro Western Piedmont, LLC is submitting this application to modify the referenced residuals land application permit. It is requested that 15 fields and 3 sources be added to the referenced permit. The new fields and sources are as follows: CH-78, Fields 1,2,3, and 5 CH-73, Field 10 HA-47, Fields 1, 2, 3, and 4 RC-49, Fields 1-6 City of Mayodan WWTP Town of Siler City WWTP Harnett County Regional North Plant Enclosed is a check for $395.00 to cover the fee associated with a major permit modification. This application package should contain all information necessary to complete the requested modification of Synagro's land application permit. However, if you require additional information or have further questions, please contact me at (336) 909-8627 or cwynne@synagro.com. Thank you in advance for the timely and efficient review of the application. Sincerely 4- Christopher C. Wynne Technical Services Specialist 284 Boger Road, Mocksville, NC 27028 • Phone: (336) 790-1610 • Fax: (443) 489-9182 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 —RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T . l 100, Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): ® Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer, ® The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15ti NCAC 02T .0I06(b). ® If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). FFacility Classification New Permit F_Major Modification r Major (land are permitted for > 300 acres) $1,310 $395 Minor (land are permitted for < 300 acres) $810 $245 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (May be Required — See 15A NCAC IC .0300) ® Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 06-16 Pagel of3 E. Operation and Maintenance Plan (New and Renewal Application Packages) ® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T. I 1 10 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipment calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following infonmation; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requu-ements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. F. Program Determination ❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T .1102(12). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: ❑ Any land application site certified f'or the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. ❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary i nportance. ❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. ❑ Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information ❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. ❑ Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) ❑ Submit three (3) sets of standard size plans and two (2) sets of 1 1" by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modifications) only. ❑ Plans must include the following minimum items: ❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. ❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). ❑ Delineation of the review and compliance boundaries ❑ Setbacks as required by 15 A NCAC 02T ,1108 ❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s), ❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. ❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate thatthey are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 I. Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) ❑ Submit a project evaluation and receiversite management plan (ifapplicable)with recommendationsconcemingeovercrops and their ability to accept theproposedapplication rates. J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the totaldesign capacity) ❑ Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1 104(d)(4) and current Division Policy available at: htt //www.newater.oi'Rules_Policieseand_Regulationg/. The document shall be silted, sealed and dated by a qualified prof essiona I. K. Engineering Design Documents (All New or Modification Application Packages with fixed hiigation facilities or irrigation facilities fed through fixed supply system) ❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15ANCAC 02T .1 104(d)(2). For Modif ications, submit a n updated site map specific to the modification(s) only. ❑ The design documents must include the following minunum items: ❑ Engineering plans for the facility and equipmentexceptthose p reviou sly permitted unless they are directly tied into thenew units or are critical tothe understandingofthe complete process; ❑ Specifications describing m aterials to be used, method of construction, and means forensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for eachpump,and irrigation design. ❑ Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) ❑ Submitacompleted and accurate water balance unaccordancewith 15ANCAC 02T2T.1IQ4(d)(5)and current Division Policy availableat: httt)://www.newater.orRules Policies and Re ulations/. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/orrelocatedt'eatment or irrigation components) ❑ Property ownership documentation shall consist ofone ofthe following: ❑ Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or El Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or ❑ An easement running with the land specifica lly indicating the intended use of the property and meeting the requirements of 15A NCAC 02L .0107(f), or ❑ A written notarized lease agreement signed by both parties, indicating the intended use of theproperty, as well as a pla t or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Cou lerLSpecial Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 —RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Synagro Central, LLC Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ❑ Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Robert N. Roth Title: Technical Services Manager Applicant's mailing address: 284 Boger Rd City: Mocksville_ State: NC Zip: 27028 Telephone number:(336) 790-1610 Email Address: rroth?a synagro,com 2. Consultant's name: Chris Wynne License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: Synagro LLC ) Consultant's mailing address: 284 Boger Rd. City: Mocksville State: NC Zip: 27028- Telephone number: (336) 909-8627 Email Address: cwvnne@synawo.com 3. Agronomist's name: License Number: Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: _) Agronomist's mailing address: City: State: Zip: - Telephone number: (_)= Email Address: 4. Soil Scientist's name: Christopher Mum X License Number: 1284 Affiliation: ❑ N/A ❑ On Staff ® Retained (Firm: N/A) Soil Scientist's mailing address: 5401 Thacker Dairy Rd City: Greensboro State: NC Zip: 27406 Telephone number. (336) 215-8820 Email Address: chris@13iedrnontsoil.com 5. Fee submitted: $395.00 (See Instruction B) U. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number. WQ0016247 Date of most -recently issued permit: 11/17/2017 Date of most -recently certified Attachment A (if different than the permit): Date of most -recently certified Attachment B (if different than the permit): FORM: RLAP 06-16 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: Source specific City: State: Zip: - Coordinates: Latitude: ° "' Longitude: Datum: NAD 84 Level of accuracy: Second Method of measurement: MAP, 2. County where residuals land application program is headquartered: Source specific 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs f'or the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Robert N. Roth Synagro 1001672 Back -Up ORC Adam Brigman Synagro 1006653 Additional Back -Up ORCs if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Sannnarp: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 3 140 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 32.36 36.63 101,612 115,004 Five -Year Maximum Adjusted 49.38 53.64 155,051 168,443 b. LandA iplicativn Site UseSununarl : Summarize information regarding the land application sites as currently ceitifed and proposed f'or certification with this application: Category Use Acres Comments Crops Forest or Plantation 0 Row Crops 54.8 Hay 436.9 Pasture 699.5 Total: 1191.2 Methods Surface 1191.2 Incorporation or Injection 0 Total: 1191.2 FORM: RLAP 06-16 Page 2 of 5 Assumed Acres Required Using Acres Required Using Application Rate First -Year PAN Concentrations Five -Year Maximum Adjusted PAN (lbs PAN/nc _ i) Concentrations Surface Incorporation or Surface Incorporation or Injection Injection 2032.2 2300.1 3101.0 3368.9 so 100 1016.1 1150.0 1550.5 1684.4 150 677.4 766.7 1033.7 1123.0 200 508.1 575.0 775.3 842.2 6. If applicable, provide a plananda schedule to resolve anyknown issues thatwould prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enougli storage,not enough land, vector reduction practices not in place, etc.): 7. Specify typeof residuals program (See Instruction F): ® Non-dedicatcd ❑ Dedicated IfDedicA-tc-d, specify the following (clieck all that apply): ❑ Residuals program contains any land application sitc(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land applicationsite(s) that is used primarily forresiduals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed u-igation facilities or irrigation facilities fed through a fixed supply system, explain, IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals SourceCe•trficalion and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Land Application Siite Certification. doc FORM: RLAP 06-16 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: ❑ Spray ❑ Drip 2. Disposal system is: ❑ existing ❑ proposed. 3. Minimum depth to mean seasonal high watertable (SHWT)within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules l 5ANCAC 02T.0505(u)requires at least one -foot vcrticalseparation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? ❑ Yes or ❑ No If Yes, please explain if the soil scientist reportaddresses artificial structures andplea seindicate if structures are to be maintained or modified: 5. Loading r'atesrecommended bythe Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate (in/hr) Recommended Loading Rate (in/yr) 6. Design loading rates are equal or less thanth eloading rates recommended bySoil Scientist? ❑ Yes or❑ No IfNo, explain why 15ANCAC 02T.0505(n) is notmet. 7. Non -dedicated System Design (fill in the appropriate inforniation foreither a spray ordrip irrigation system): Field / Zone Design Area ft2) Number of Nozzles Maximum Application Rate gallons/hr) Design Annual Loading Rate (allons/yr) Total Spray Irrigation Design Element Plan Sheet Number Specification Page Number Wetted diameterofnozzles ft Wetted area of nozzles ft2 Nozzle capacity gpm Nozzle manufacturer/ model / Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes ❑ No, Explain; T-,&e, a 0 , Rvti-, r"WC-C i- (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for :m !y h %'JrV L C (Facility Nanic) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: Date: 7— ' Z o 2_ o FORM: RLAP 06-16 Page 5 of 5 OPERATIONS AND MAINTENANCE PLAN SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0016247 (Synagro Western Piedmont Class B) Inspection Plan Inspections for the land application of residuals will be conducted on a weekly basis at the land application site during the land application activities of this project. The inspection frequency is based on the time frame that it is going to take to complete the project and the amount of dry tons to be land applied from this facility. The inspections will consist of inspecting a current field that is being applied as well as inspecting random fields that have been completed. These inspections will consist of: 1. Verifying that the Pre -Operations Check List has been completed and signed by both Operations and Technical staff. 2. Checking the calculated loads to ensure the correct amount of residuals are being land applied. 3. Ensure that all manned equipment has a copy of the spill control plan, the permit, and the operations and maintenance plan. 4. Ensure that the field has been flagged properly and that all buffers are being adhered to. 5. Ensure that the Crop and Landowner Verification form has been filled out. 6. Verifying that thecorrect numberof samples of the residuals has beentaken and that it meetsthe criteria for land application. 7. The records will be kept in the project files in the respective office for the project. 8. The Permittee or Inspector shall report by telephone to the Fayetteville Regional Office by Telephone at 910-433-3300 as soon as possible but no later than 24 hours after or the next working day following the occurrence or the first knowledge of the occurrence of the following. • Any occurrence with the distribution program resulting in the land application of significant amounts of material that is abnormal in quantity or characteristics. • Any failure of the distribution system that results in the release to surface waters. • Any time that self -monitoring indicates that the facility has gone out of compliance with the permit. • Any process failure that results in the system not adequately treating the residuals. • Any spill or discharge from a vehicle or piping system during residuals transportation. • Any release that requires immediate reporting outside of normal business hours shall be called in to DENR at 1- 800-662-7956,1-800-858-0368, or 1-919-733-3300. These numbers are to be called in the event of a release to surface waters, imminent failure of a storage system when the event occurs outside of normal business hours. • Within 5days of the first notice of on occurrence a written response in the form of a letter shall be sent to DENR outlining the actions taken or purposed actions taken to ensure that the problem does not recur. Persons responsible for inspections on this project are as follows: Chris Wynne, Technical Services Specialist (336) 909-8627 OPERATIONS AND MAINTENANCE PLAN SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0016247 Sampling Plan Sampling for this project consists of sampling the residuals prior to or during the time that land applicationis occurring. This will result in one round of sampling to occur before land application commences inorder to ensure that the residuals are suitable for land application. Based on the dry tonnage of this plant this will be four samples for all parameters peryear with the exception of the TCLP. The residuals shall be sampled annually for the following: (Regulatory level in milligrams per liter in parentheses.) Arsenic (5.0) 1, 4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1, 2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1, 1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2, 4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13 Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008)Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachlorethane (3.0) 2,4,5-Trichlorophenol (400.0) M-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5 TP ( Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl Chloride (0.2) Cresol(200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) The residuals will also be sampled based on the chart below for the following constituents Dry Tons Generated (short tons per year) Monitoring Frequency (Established in 40 CFR 503 and 15A NCAC 02T.1111) <319 1 time per year =>319-<1,650 1 per Quarter (4 times per year) =>1,650-<16,500 1 every 60 days (6 times per year) =>16,500 1 every month (12 times per year) Aluminum Ammonia -Nitrogen Arsenic Cadmium Calcium Copper Lead Sodium Adsorption Ratio (SAR) Magnesium Mercury Molybdenum Nickel Nitrate -Nitrite Nitrogen Phosphorous Potassium pH Plant Available Nitrogen (calculation) Selenium Sodium % Total Solids Total Kjeldahl Nitrogen Zinc In order to meet pathogen requirements the material will be sampled to meet the fecal coliform density requirement. The grab samples will be pulled from the pad, basin, or lagoon for either plant that are currently holding the residuals. Other samples that will be pulled are a TCLP and a nutrient and metals sample to prove that the material is suitable for land application. The nutrient and metal and TCLP sample will be collected randomly and consist of at least 10 individual samples mixed together in order to get the composite sample for these parameters. The following people are responsible for sampling: Chris Wynne, Technical Services Specialist (336)909-8627 OPERATIONS AND MAINTENANCE PLAN SYNAGRO RESIDUALS LAND APPLICATION FOR WQ0016247 (Synagro Western Piedmont) Operational Functions The operation function ofthis project is going to involve mixing the lagoon with lagoon mixersto achieve a well mixed and consistent material thatwill be spread as a liquid for land application. It is goingto be spread at agronomic rates that are determined bythe nutrient and metal samplethat is currentforthat monitoring period. It is goingto be spread with a liquid applicator that will use pressure to spread the material in such a wayto achieve a consistent spread pattern. The material is goingto be land applied on fields that are in normal agricultural row crop production or grass land. Safety Measures Synagro believes in operating in a safety conscious manner and has all employees participate in quarterly online safety course that are designed to help its employees recognize safety issues and take steps to prevent accidents from occurring. In addition all Synagro employees have the authority to stop operations if they think any aspect of the operation is going to cause environmental or personal harm. Maintenance Schedule Synagro will follow the maintenance schedule asrecommended bythe Synagrofleet managerforthe equipment iecessaryto complete thejob. SPILL RESPONSE PLAN PROJECT: SYNAGRO WESTERN PIEDMONT PERMIT W00016247 IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTIONS SHALL BE TAKEN IMMEDIATELY: 1. MANAGEMENT OF SPILL CLEAN-UP ACTIVITIES: The Synagro Operations Manager shall take immediate charge and initiate clean-up activities. Synagro labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the NC Department of Transportation, and other private contractors as necessary. 2. HALT THE SOURCE OF THE SPILL: Such as a ruptured container or damaged transport unit. 3. CONTAIN THE SPILL: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Synagro Operations Manager or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean- up operation, i.e., local farmers, fails supply centers, nurseries, etc. 4. CLEAN-UP: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw- and sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. 5. FINAL CLEAN-UP: Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the spill area to its original condition if possible. 6. NOTIFICATION: As soon as possible after the spill occurs, the Synagro Operations Manager or assistant will notify the Synagro Central office, and they will then be responsible for notifying other key Synagro personnel. 7. REPORTING: Synagro Central personnel will notify the Winston-Salem Regional office at (336) 776-9800 as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The Operations Manager shall provide a written report within 48 hours of the spill to the Technical Services Director. The report shall list all relative information and actions taken. Synagro Central personnel will file a written report to the Winston-Salem Regional office of the NCDENR within 5 days of the occurrence. For after hours reporting the Division's emergency number shall be called to report all incidences (1-800-858-0368) or (919-733-3300). Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a cheeldist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation Formorehilbi-mrlion,visillheH,alerQualilyPermiuingSec lion'sNon-Dischar ePei-mittinz g Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1 100. Do notsubmit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supportingdocunlentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 1 1-15) form. Please do not make any unauthorized content changes to thisfonn. Ifnecessary for clarity ordue to space restrictions, attachmentsto the application may be made, as long asthe a ttachments are numbered to correspond to the section and item to which they refer. ® For new or renewed_ perm its, submit a separate certification for each source facility. ® Formodifedpennits,submitaseparatecertificationforonlythosefacilitiesthatareaffectedbytheproposedmodification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For eachsource facility, attach the following: ®Vicinity map -A vicinity map that shows the location ofthefacility and meetsall ofthe criteria in the "MalmGuidance for Residuals Land Application Pemmits". ® Process flowdiagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are tobe generated, treated, processed, andstored attlmefacility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8. Ensure that the amountofresiduals listed isthe maxvnunm amount expected to be generated by the facility forthe life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the pla n deta ils how the facility and/or the residuals are monitored for any applicable pa thogen reduction a n d vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/ordisposed. C. Residuals Quality Information: ® For eachsource facility, attach the following: ® Laboratory analytical reports and operationaldata -reports for alllaboratory analyses used tocomplete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ® For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility alongwith the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page I of I RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: S_ Yna�,,ro Western Piedmont. LLC Status Codea Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current" Proposed N Harnett County Utilities North Harnett Regional WWTP Harnett NCO021636 0 1500 N Town of Mayodan Mayodan WWTP Rockingham NCO021873 0 315 N Town of Siler City Siler City WWTP Chatham NCO026441 0 1325 I a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Dlvlslon of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: North HamettReyional WWTP 2. Facility permit holder is: ❑ Federal, El State, ®, Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Envii•onmentalHealth, or Da Other (explain: ). 3. Facility contactperson and title: Billy Thomas, Plant ORS: Complete mailing address: 607 Edwards Brothers Dr City:LiIlington State: NC Zip: -27546 Telephone number: (910) 893-2424 E-mail address: bthomas( hatnett.org 4. Facility physical address: 607 Edwards Brothers Dr City: Lillie on State: NC Zip: 27546- Coordinates: Latitude:35°23'45'� Longitude:78°48'04" Datum: NAD 84 Level of a ccuracy: Second Method of measurement: MAP 5. Purpose of the facility: ® treatmentofmunicipalwastewater, ❑ treatmentof 100%domesticwastewater, Q treatmentofpotablewater, ❑ treatment of 100% industrial wastewater, 0, treatmentof industrial wastewatermixed with domesticwastewater, (approximate percentages: 1 1% industrial and _ % domestic) ❑ other (explaui: ). 6. Does the facility have an approvedpretreatment program: ® Yes No 7. Facility petinitted/design flow: 77.5 MGD and facility average daily flow: 4_4 MGD 8, Average amountof residuals being generated at this facility 572.2 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volumeofresiduals treatment: Aerobic Digestion with 2-1 million gallon basins Type and volume of residuals storage (i.e., outside ofresiduals treatmentunits): 5 acre, 26 million gallon facultative lagoon H. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ® 40 CFR Pail 503 or Q 40 CFR Pail 257, Note: Only residua Is that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under40 CFR Part 257. 2, Specify if residuals are defined under 15A NCAC 02T.1 102(61as: ® B iological Q Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, anunal processutg wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -mu n icipa 1, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes Z no. If yes, list the number(s): f b. Specify whether or notthe residuals exhibit any ofthe characteristics defined by40 CFR §261.21- 261.24: P yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well a s thosef orcorrosivity, ignitability, and reactivity: Laboratory: Pace Ana] ticaIServices LLC and Date of analysis:3/18/2020 Passed corrosivity test: ® yes ❑ no. pH: sm. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint:>140 OF(> 140°F) Passed reactivity test: 19ycs 0 no, HCN: ND nig/kg (<250) & H2S: 180 nig/kg (<500) TCLP Parameter Limit (1119/1) Result (rng/1) TCLP Parameter Limit ()Itg/1) Result (mg/U Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 0.4 Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hcxachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND ni-Cresol 200.0 ND Pent achlorophenol 100.0 ND ' o-Cresol 200.0 ND Pyridine I 5.0 I ND p-Cresol 200.0 ND Selenium I 1.0 I ND Cresol 200.0 ND Silver 5.0 I ND 2,4-D I U ND Tetrachloroethylene l 0.7 I ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 I ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 2,4,5-Trichloroplienol ` 400.0 I ND 2,4-Dinitrotoluene 0.13 ND 2,4,6-Trichlorophenol I 2.0 I ND ' Endrin 0.02 ND 2,4,5-TP (Silvex) I 1.0 I ND Heptachlorand its Hydroxide 0.008 ND Vinyl Chloride I 0.2 I ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e,, as applicable) to demonstrate that the residuals do not violate the ceiling concentration form eta lsregulated under 15A NCAC 02T .1 105. a. For D1slribntiOnlLand Application: Fill in the following table with the results of the latest analyses (i.e., o n a dry weight basis) for the following meta 1parameteis: Laboratoiy: Pace Ana 1 byicalServices, LLC and Date of analysis: 05/01 /2020 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A On )) (nig/kg) Result (nrg/kg) Arsenic 75 41 4.8 Cadmium 85 39 1.1 Copper 4,300 1,500 220 Lead 840 300 16 Mercury 57 17 ND Molybdenum 75 n/a ND Nickel 420 420 11 Selenium 100 100 ND Zinc 7,500 2,800 670 b. For Snnfuce Dispolul Unit (Lind ilh Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the follownig metal parameters: Laboratory: andDateofanalysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, checkone) Arsenic (,ng/kg) Chromium 019/1T) Nickel (rng/kg) ❑' > 0 but< 25 30 200 210 ❑ > 25 but< 50 34 220 240 ❑ >_ 50 but< 75 39 260 270 ❑ >_75 but< 100 46 300 320 ❑ > 100 but< 125 53 360 390 ❑ >_125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Totalsolids: 2.19 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratoiy: Pace AnalyticalSeryices, LLC and Date of analysis:05/01/2020 Parameter Result (rig/kg) Aluminum 38000 Ammonia -Nitrogen 3300 Ca Icium 15000 Magnesium 3800 Nitrate -Nitrite Nitrogen 112 pH (Standard Unit) 7.0 Phosphorus 14000 Potassium 1800 Sodium 2300 TotalKjeldahl Nitrogen 30000 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0:64 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc,), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): ® defaultvalue,or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected defaultvaluc is appropriate to be applied to these residuals: ,I l e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill theresults in the following table: Application Method First (151) Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (nrg/kg) Surf'a ce 9772 14981 Injection/Incorporation 14981 16631 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N/A FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction; Per 15A NCAC 02T.1 106,specify how residuals will meet the pathogen reduction requirements: a. For Distribution/L,nd Application of0as.s A or Equivalent: []' A fecalcolifonn density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or [], A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of tot a ldry solids. AND one of the followings (except fornon-biological residuals): ❑ Alternative 1 [15A NCAC 02T.]106(b)(3)(A)] -Time/TemperatureComplianee. Alternative [15A NCAC 02T.1106(b)(3)(B)] -Alkaline Treatment. Q1 Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] -Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.]106(b)(3)(D)] - No Prior Testing for Enteric Vn•us/Viable Helminth Ova. ❑! Alternative 5 [15A NCAC 02T.1106 (3)(E)-(K)1 - Process to Further Reduce Pathogens (PFRP). Specify one: Elcomposting, 8I heatdrying, ❑ Ircattreatrnent, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gain marayirradiation, or ❑ pasteurization. b. Fo►•LtnrdA )lic�rtioato ClassB: Ej Alternative 1 [15A NCAC 02T.1106(c)(1)]-Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobiedigestion, ❑; composting, or ❑ lime stabilization. c. For Srrt face Dlslrasrrl: 0, Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II.7a. above. Q Select One of the Class B or Equivalent Pathogen Reduction Alternatives in item 1I.7b. above. ❑I Exempt -If Daily Cover Alternative is chosen in Item II.9. below[ 15A NCAC 02T.1 106(a)(2)]. ❑' Not Applicable - Non-Biologicai Residuals with NO Domestic WastewaterContribution. 8, Vector Attraction Reduction (VAR): Per 15ANCAC 02T.1 107,specify howresiduals will meetthe VAR requirements: ® Alternative 1 [15A NCAC 02T.1107(a)(1)] - 39%Volatile Solids Reduct ion (Aerobic/Ana erobic Digestion). ❑' Alternative 2 [15A NCAC 02T.1 107(a)(2)] - 40-DayBench Scale Test (Anaerobic Digestion). ® Alternative 3 [15A NCAC 02T.1 107(a)(3)] - 30-DayBcnelr Scale Test (Aerobic Digestion). ® Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.1 107(a)(5)] - 14-Day Aerobic Processes. ® Altemative 6 [15A NCAC 02T.1107(a)(6)] -Alkaline Stabilization. ❑: Alternative 7 [15A NCAC 02T.1 ]07(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.1 107(a)(9)] -Drying ofUnstabilized Residuals. ® Alternative 9 [15A NCAC 02T.] 107(a)(9)] - Injection. Alternative 10 [ 15A NCAC 02T.1 1 07(a)(I 0)]- Incorporation. Eli Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.1 107(b)(2)]. ❑j Not Applicable - Non -Biological Residuals with NO Domestic WastewaterContribution. Note: For annnalprocessi ig residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 Iowz) fudom.,umm) 1jamwu 'Y'd 'HaININ v ONVIZAvm Au% qVKOIDn Avn fu-.Li qm"m all WHOIDn Avn6na-li aw"" E I I 41 Zky pi Vill E� .1,Z2 "IN �Ojlqyl 7 MAIL L- J T it 0*9ZI 'A313 0001A 'HA 001 :310N VICINITY MAP Harnett Lillington 7 Regional Qf:jv,,.Waste Water SYNAGRO COUNTY: Harnett OWNER(S): North Harnett Regional WWTP f 1 i C 1 1 aplip YAIRIk.ME'A' Fix Aarrcna+ a Grsa- AFC i `1 , ILl� � -16 � ' i ettmcfiosau�arnte i 1{"', r= `��•-' � Mwer4'r.-'- .�.—.�• . � �1��T r—._ems—x—._.._. e� � e .-8—. —�- Residuals Sampling Plan Synagro Residuals Land Application for WQ0016247 Harnett County Regional North Treatment Plant Nutrients and Metals Analysis Sampling Point: Lagoon Sampling Frequency: Based on Diy Tons Sample Type: Composite Lab: Pace Analytical Services, LLC Pathogen (Fecal Coliform Density Demonstration) Sampling Point: Lagoon Sampling Frequency: Based on Dry Tons Sample Type: 7 Grab samples Lab: Cameron Testing Vector (38% VSR) TCLP Sampling Point: Lagoon Sampling Frequency: Based on Diy Tons Sample Type: Composite Lab: Cameron Testing Sampling Point: Lagoon Sampling Frequency: Annually Sample Type: Composite Lab: Sununit Environmental Technologies, Inc Quantitative Justification for Residuals Production Rate F acility: Harnett County Utilities /North Harnett Regional WWTP Requested Permitted Rate: Current: Requested Justification: 1500 Diy Tons/year 1500 Diy Tons/year Based off the past 3 years diy tonnage: 2019: 787.7 Dry Tons 2018: 374.6 Dry Tons 2017: 554.3 Dry Tons Calculations: Average: 572.2 Dry Tons Based on the average daily flows of 4,400,000 gallons per d ay, 1500 dry tons per year should be sufficient for any increase in volumes. Total Dry Tons = gallons of residuals x % solids x 8.34 lbs/gallon 2,000 lbs/ton = 4,400,000 Lrallons x_ 0.0219 x 8.34 Ilion 2,000 lbs/ton = 402 dry tons Chris Wynne, Technical Services Specialist aceAnalytical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Nate Roth Project Name: North Harnett WWTP Lot Number:VC03022 Date Completed:03/18/2020 M 03/18/2020 2:35 PM Approved and released by: Lab Director - Greenville: Lucas Odom AdM- AASI Falrortal arnedArENn 6oa+? 4B ACC F1 E D I T E 0 7ESTMOUWRATONv The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc,) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page l of 10 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VC03022 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative, The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP Due to low percent solids sample -001 was weighed out at 3 times the normal weight. The LOQ has been elevated to reflect the dilution. Nitrate The following sample was diluted due to the nature of the sample matrix: VC03022-002. The LOQ has been elevated to reflect the dilution. Paint Filter Sample -001 has been qualified with an "H", however, there is not a method defined hold time for this parameter. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 10 Guent:aynagro Laooraiory 11J:vL:U3ULL-UU'I Description: NH 20 Matrix: Solid Date Sampled:0212812020 1300 % Solids: 5.05 03/03/2020 2237 Date Received:0310312020 Inorganic non-metals Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch (% Solids) SM 2540G 1 03/03/2020 2237 MDD 46788 1 (Ignitability) 1010A 1 03/09/2020 1716 SLC 47298 1 (Paint Filter) 9095B 1 03/10/2020 1443 SLC 1 (Reactive Cya) 7.3.3 1 03/10/2020 0000 KFE 03/10/2020 1046 1 (Reactive Sul) 7.3.4 1 03/10/2020 1925 HET 03/10/2020 1046 1 (Soil pH meas) 9045D 1 03/05/2020 2211 SRB 47065 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 5.05 % 1 Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 0 ° F 1 Paint Filter Test 9095B Fail H` passifail 1 Reactive Cyanide 7.3.3 ND 50 50 mg/kg 1 Reactive Sulfide 7.3.4 180 50 50 mg/kg 1 Soil pH measured in water @ 20.9 ° C 9045D 7.4 su 1 TCLP Volatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311t503OB 8260D 10 03/13/2020 0445 JTH 47756 03/11/2020 2110 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 8260D ND 0.050 0,0040 mg/L 1 2-Butanone (MEK) 78-93-3 8260D ND 0.10 0,020 mg/L 1 Carbon tetrachloride 56-23-5 8260D ND 0,050 0,0040 mg/L 1 xobenzene 108-90-7 8260D ND 0.050 0.0040 mg/L 1 L.nloroform 67-66-3 8260D ND 0,050 0,0040 mg/L 1 1,2-Dichloroethane 107-06-2 8260D ND 0.050 0.0040 mg/L 1 1,1-Dichloroethene 75-35-4 8260D ND 0.050 0.0040 mg/L 1 Tetrachloroethene 127-18-4 8260D ND 0.050 0.0040 mg/L 1 Trichloroethene 79-01-6 8260D ND 0.050 0.0040 mg/L 1 Vinyl chloride 75-01-4 8260D ND 0.010 0.0040 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 99 70-130 1,2-Dichloroethane-d4 97 70-130 Toluene-d8 104 70-130 TCLP Semivolatiles Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270E 1 03/12/2020 1657 SCD 03/10/2020 1710 47402 03/08/2020 2357 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run LOQ Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range OL —Detection Limit N D = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL �il of holding time W = Reported on wetweightbasis Fo..a Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791.9700 Fax (803) 791.9111 www.pacelabs.com Page 3 of 10 t.uem:bynagro Description: NH 20 Date Sampled:02/28/2020 1300 Date Received:03/03/2020 TCLP Semivolatiles Laooraiory lu: vt.usuzZ-uu'l Matrix: Solid %Solids: 5.05 03/03/2020 2237 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1311/3520C 8270E 1 03/12/2020 1657 SCD 03/10/2020 1710 47402 03/08/2020 2357 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dichlorobenzene 106-46-7 8270E ND 0.040 0.0050 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270E ND 0.080 0.0050 mg/L 1 Hexachlorobenzene 118-74-1 8270E ND 0.040 0.0050 mg/L 1 Hexachiorobutadiene 87-68-3 8270E ND 0.040 0.0050 mg/L 1 Hexachloroethane 67-72-1 8270E ND 0.040 0.010 mg/L 1 2-Methylphenol 95-48-7 8270E ND 0.040 0.010 mg/L 1 3+4-Methylphenol 106-44-5 8270E ND 0.040 0.015 mg/L 1 Nitrobenzene 98-95-3 8270E ND 0.040 0.015 mg/L I Pentachlorophenol 87-86-5 8270E ND 0.20 0.020 mg/L 1 Pyridine 110-86-1 8270E ND 0.040 0.0050 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270E ND 0.040 0.0050 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270E ND 0.040 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 68 37-129 2-Fluorophenol 50 24-127 Nitrobenzene-d5 74 38-127 Phenol-d5 79 28-128 Terphenyl-d 14 84 10-148 2,4,6-Tribromophenol 69 41-144 TCLP Herbicides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 03/16/20201847 JJG 03/12/2020 1747 47726 03/08/2020 2357 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 2,4-D 94-75-7 8151A ND 0.020 0.0050 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 0.0013 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 74 50-112 TCLP Pesticides Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 03/13/20201621 DAL1 03/11/2020 1452 47527 03/08/2020 2357 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 0.00017 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantilation of compound exceeded the calibration range DL = Detection Limit N D = Not detected at orabove The DL N = Recovery is out of criteria P = The RPO between two GC columns exceeds 40% J = Estimated result < LOQ and > DL rt of holding time W = Reported on wet weightbasis P—e Analytical Services, LLC (formeiiy Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,pacelabs.com Page 4 of 10 Lment: oynagro Description: NH 20 Date Sampled:02/28/2020 1300 Date Received:03/03/2020 TCL.P Pesticides i-aooratory lu: VL:usuGL-uui Matrix: Solid % Solids: 5.05 03/03/2020 2237 i Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date i 1311/3520C 8081B 1 03/13/2020 1621 DAL1 03/11/2020 1452 47527 03/08/2020 2357 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Chlordane 57-74-9 8081B ND 0.0040 0.0015 mg/L 1 Endrin 72-20-8 8081B ND 0,00040 0.00015 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 0.00015 mg/L 1 Heptachlor epoxide 1024-57-3 8081B ND 0.00040 0,00016 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0016 0.00021 mg/L 1 Toxaphene 8001-35-2 8081B ND 0.0080 0.0030 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 88 20-131 Tetrachloro-m-xyiene 87 26-132 TCLP Metals Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3010A 6010D 1 03/10/2020 1033 LLL 03/09/2020 2018 47306 03/08/2020 2357 1 1311/7470A 7470A 1 03/10/2020 1522 KSH2 03/10/2020 0941 47316 03/08/2020 2357 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Arsenic 7440-38-2 6010D ND 0.15 0.025 mg/L 1 Barium 7440-39-3 6010D 0.40 0.25 0.031 mg/L 1 r'gdmium 7440-43-9 6010D ND 0.050 0.0060 mg/L 1 omium 7440-47-3 6010D ND 0.10 0.013 mg/L 1 Lead 7439-92-1 6010D ND 0.10 0.047 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 0.00091 mg/L 1 Selenium 7782-49-2 6010D ND 0.20 0.085 mg/L 1 Silver 7440-22-4 6010D ND 0.10 0.021 mg/L 1 Footnote(s): 'Paint Filter: 5mL collected; LOQ - Limit of Quanlilation B - Detected in the method blank E = Quanlitalion of compound exceeded the calibration range DL Detection Limit ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOD and> DL it of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 10 ument:aynagro Description: N H 1 Date Sampled:0212812020 1300 Date Received:0310312020 Laooratory iu:vuuauzz-uue Matrix: Solid % Solids: 1.97 0310312020 2237 Inorganic non-metals 7 1 t Prep Method Analytical Method Dilution Analysis Date Analyst _ Prep Date Batch 1 (% Solids) SM 254OG 1 03/03/2020 2237 MDD 46788 1 350.1 (Ammonia - N ) 350.1 5 03/09/2020 1336 SLC 46871 2 (Nitrate - N) 9056A 5 03/17/2020 1253 AMR 48204 1 (Nitrite - N) 9056A 5 03/11/2020 1836 AMR 47697 1 (Phosphorus) 365.1 10 03/06/2020 1358 DMA 03/06/2020 0937 47087 1 (Soil pH meas) 9045D 1 03/05/2020 2215 SRB 47065 1 351.4 (TKN) 351.2 1 03/04/2020 1544 DMA 03/04/2020 1002 46808 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 1.97 % 1 Ammonia - N (gas diffusion) 350.1 6500 250 130 mg/kg 1 Nitrate - N (soluble) 9056A 210 130 6.2 mg/kg 2 Nitrite - N (soluble) 9056A 36 J 51 4.9 mg/kg 1 Phosphorus 7723-14.0 365.1 15000 2500 510 mg/kg 1 Soil pH measured in water@ 21 ° C 9045D 7.3 su 1 TKN 351.2 77000 1300 1300 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 7471E 7471B 1 03/04/2020 1642 KSH2 03/04/2020 1230 46714 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run mercury 7439-97-6 7471E ND 3.8 0.91 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 03/09/2020 1946 LLL 03/06/2020 1452 46709 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429.90.5 601OD 6700 330 120 mg/kg 1 Arsenic 7440-38-2 6010D ND 12 4.1 mg/kg 1 Cadmium 7440.43-9 6010D 1.6 J 4.1 1.0 mg/kg 1 Calcium 7440-70.2 6010D 7000 4100 510 mg/kg 1 Chromium 7440-47-3 6010D 7.1 J 8.2 2.0 mg/kg 1 Copper 7440-50-8 6010D 77 8.2 3.7 mg/kg 1 Iron 7439-89-6 6010D 5600 82 37 mg/kg 1 Lead 7439.92.1 6010D 4.9 J 8.2 3.7 mg/kg 1 Magnesium 7439-95-4 6010D 650 J 4100 510 mg/kg 1 Manganese 7439-96-5 6010D 380 12 4.8 mg/kg 1 Molybdenum 7439-98-7 6010D ND 33 8.2 mg/kg 1 Nickel 7440-02-0 6010D ND 33 8.6 mg/kg 1 LOD =Limit of Quantitation B - Detected in the method blank E - Quantitaticn of compound exceeded the calibration range DL = Detection Limit ND = Not detected at or above the DL N - Recovery is out of criteria P -The RPD between two GC columns exceeds 40% J = Estimated result a LOD and > DL it of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 10 unem: aynagro Laooratory iu: vcusu«-uuz Description: NH 1 Matrix: Solid Date Sampled:02/28/2020 1300 % Solids: 1.97 03/03/2020 2237 Date Received:03/03/2020 ICP-AES _ i Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 03/09/2020 1946 LLL 03/06/2020 1452 46709 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Potassium 7440.09-7 6010D 2800 J 4100 510 mg/kg 1 Selenium 7782-49-2 6010D ND 16 6.6 mg/kg 1 Sodium 7440-23-5 6010D 3700 J 4100 510 mg/kg 1 Zinc 7440.66-6 6010D 240 41 10 mg/kg 1 LOO = Limit of Quanlitation 0 = Detecled in the method blank E = Quantltation of compound exceeded the calihratlon range DL = Detection Limit N D = Not detected a t or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds40% J = Estimated result < LOQ and> DL it of holding time W - Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 10 Chain of Custody and Miscellaneous Documents Pace Analytical Seivices, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 9 of 10 PACE ANALYTICAL SERVICES, LLC Sheet1 Shaaly Environmental 3arvlcos, Inc. 1t)f: Vinlago Point Drive ti arrla' Chaim cd Cusfody Racc rd Wed coluntle, South Care[ine 20172 Number 4, 1Mpph«le Na. (803) 791-97CO Fax Vo. (BL5)79i-B11S p trl -1YheAro I R.!Dod to Gonteet ` )`rU�J��rnitrtfr'ti.Vcti"n > amFb+(krHao limit) 1 �lIuj+ I1,It Y'wYl:il Nil ) '4l1 r 1 NN�ItIj u '�:hktt7 i j 2�a 3aaer R4, l H{lntre Nu tfs+r �L:, /Eami ' " My Slakr klreks-Alta t4C 25pCLbs 's7R?.E FrvcarVai.v I.Vl*re3, d;HNOj 7,O&OH �, NaQN�ns i. Hr7. r 3 W2®UE 8. Wa . ht:.. A rt a ! a 1 1 ♦ r�IUU1 j �i C0302 j �' L.10 — NG ies�il Pahl ells TLC014 CCE (rato 7-1 IV Gre981 Ralb l 1plape[Ne Te i =u1 Pe Lc W�hr, I t PH PCB S7rS1 M l Nrnhe P.ONlMlaer �` r i Me1rSx '3w UN Wier S one- [ Sampetofa7rzcri on 1 tecrltail %li;rewiearrOmt'rbp"'oi4d j tnaleOne) DOW Trims 'cam o I �; x x x x f 1� r Ia j : �� G ✓ �1:m,Vcuna-"5Ael WrMarre6rwUNMr%,HtawftmY^ gt . dvd rl tRWSh ptezld "!IM 7dvx por_uc, Lr'G"Vler slit'Dlepuadl OI Renia Cr ini � G` pa.1w Lab it ; Gtrtfimfirn ic6dhke b.ieiimlk zziri r4ar*azajd, FlmrneKe F � +tn H 4l1Wnc?ei i, Reimilo Dzta 2 T-nn q 1. AKRNll V cote Z POArr.W "I b7 CQte Time 2. NaoEhlea W oe e I Winquarral by C'l.Y dire 1Rettmw w Date ,1 n ��V1 � / 4 'llingt.�ch u1 CY ff \ �'1 e, 1 tl rr Tjfnr2 � M 4 a 3 Nate; All Samples aro rat iinad for six woeke hrorn Waiipt unless other arrangements are LABLS2 CKY mado R 4iccicnxrlCh�elQ yd' Q vcPeck y-t:'� 3 Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive Wes[ Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 9 of 10 PACE ANALYTICAL SERVICES LLC Slwbkv m¢uneryInc laps t 911 D<,jftnrl NeroLkt-MCOW:-4 LnNtI) etBrl_lk S4>t>ni><ple Receipt Checklist (STIC') Client: Synagro eta° / 07ff1;in-o20 L,or;ft 1;C03022 cans ofrecelpi. SES1 FI C i:nl ❑ (IP5 ❑ Yes ®Hu 1. Were custody seals ove,4v tt un the owl er7 Ycs N:- NA 2. if custoe. seibb wean rusenr, were th" inlael turd unhrvtken'l pl-I Strip IlY NA C)dnrine Sl-ip ID: NA Tested by -,NA _ Original tamNretnr'a upon receipt Dcrived (CotreGtod) :eu» pe:a:ure upon Teceiht 'Molid Snap -Cup ill: 14-2113 5.2 /5.). `C NA /,NA �(, \'A ;NA AC NA INA aL tvtexhod: �Tert�para{uro Mani: QAgpainst Bottles IR (itm 1D: 6 IR Gun Corrcation hactot: °C Mrthr,d of coo:nnt: ® We, ice ❑ :ca Packs ❑ 13 ice ❑ None ❑ Yes ❑ No NA _ 3. ]:fern rulurc of airy cnoler cxr.eeded 6,t3°C, was Project Manager Notified" PM wsc Nu',if cd by: phnne l ornail I fucerlu-fucc (circle one). ® Yes ❑'Na ❑ NA 4, is tite Commercial courier's packing slip attached to this falrm'j 5. Wuxi prt>per custody ptu=rlurta (mlinquishe i/Teaeived) rollowcd'? 0 yes ❑ NO j4 Ycs Nt7 6. Ware satuple IDs listed on the CCQC_' Yes ❑ Nn _ 7, 1:1ere sample Ms listed oil (Ili slim le cnnininnrs? Ycs ❑ No S. lrlas eollvc'ion Me A time listed on ilia COO? ❑ Yes MP 9, Was collewon date& time listed on all swilple coutainers'-r_ 10. Did all oorrtAll r'Label ialanrmlion (10, date, tfr io) agree with lttu t:C U'. ® YuS ❑ o Wj YeS 11. W(ro tests to:w Wrfonued lima on tie COC? 12, Did all sxntples arrive in the prop:tr Luntilincrs for each lest and/or itt Aoot: condition n No l Yes El No (anhroken, lids on, cti;J1 13. Was adcquate sample valtnne availnldc? Yes ❑ No _ ❑ Yes VI No 1,1. Were all s. nlplt�-Cccived within is the holdiag limo or4K hnitr5, wi icliever cwnvs f<rst'1 Yes ONO 15. Werc any sam leS containers missingimcess oim"a one) stunpirs 4ot.listed on COC7 ❑ Yes ❑ No O n A Id. Pot VDA and RSK• 17S samples. were bubbics pvcseni ?"ne:: size" ('A"or 6mm in diameter) in mlly of Hie VOA vials? ❑ YCS "No Q.'%io NA 17- WerC ul1 1�1C(�linet�:Srtnlliier]t s;llilplCy re{~Cil'ed }11..r [rH t7f 7 I8. Werc all cyanlde samples trmivA nt a Ill1 - 12 and sulfide xnmpl_Y received fit a p1: = 9? ❑ YaF ®i~1A 71Ycs ❑ No 19. Were M applic Ic dH ! I'KN{t yanldap tens 625 (,z 0,5TnWL.) same es n ee ofr>r.-6 nl 0 NA clsltirin�7 ❑ Yrxa ❑ No ®NA 20. 'ti um c:i{ntT mnarks,hvcquests fi_e, roquestec dilutions. MSAvlSrl drs'gnatfoa&, etc...; er,rrct:l;ran y transcribed frurn the CDC Into the couuneul SCCdon in I .IIv1S? ❑ Yes No 121. Was the goulc ntrrrther kiell on the cojiWner label's If C5, Quote r NA4 �aaulple l'rt Serration Miusr be eouipleted for any sar:lple(s) incomeclly preserved or with hoadspaot;,) 'ample(s) NA were reccivcd incorrectly praser% xW 4111d were adjusted accordir-gly in sample rcceivi_rtg with. NA_nll,of circle ono: HM)4, ITNG3, .Hel, NuOH using SR * NAfirm pfnzesen�tlen NA If Mom, than one pirmmpnhwti is neetkd, picese t101e itt 1111113 GOn11TI MS bc: % SwIlple(s) NA Nvele YeCCjVW with bubblcs: 6 marl 41 diameter" Sairiplcs(s) NA were mccived )with TRC: > 0.5 mg.2 (117619 is rru) rind were adjusted eccotdingly in siimple receiving wills-widilan tniosuffatc (Na,S2()3) with Shealy 11): NA hR barcode l4bcl3 applied by; 13MG _ Didr: (00312020 Comnlcins: Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,pacelabs.com Page 10 of 10 aceAnalytical Report of Analysis Synagro 12701 Lancaster Hwy Pineville, NC 28134 Attention: Nate Roth Project Name: Harnett Lot Number:VD23025 Date Completed:05/01/2020 05/04/2020 11:44 AM Approved and released by: Lab Director - Greenville: Lucas Odom `Q`PCCRFp� � ANSI Nali"jlArwd fahaa &j1d 'Q e ACC REDIY ED TFSTINGLASMATONY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC, Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page l of PACE ANALYTICAL SERVICES, LLC SCDHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Synagro Lot Number: VD23025 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time. Metals by ICP Due to low percent solids the samples were weighed out 3 times the normal amount. The LOQ has been elevated to reflect the dilution. Nitrate The following sample was diluted due to the nature of the sample matrix: VD23025-001. The LOQ has been elevated to reflect the dilution. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of Uienr:bynagro Laooraiory iu: vuzsuto-uui Description: Harnett WWTP Matrix: Solid Date Sampled:04121/2020 1115 % Solids: 2.19 0412312020 2207 Date Received:0412312020 Inorganic non-metals _ Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch .I (% Solids) SM 254OG 1 04/23/2020 2207 HET 51982 1 350.1 (Ammonia - N) 350.1 2 04/28/2020 1528 SLC 52271 2 (Nitrate - N) 9056A 5 05/01/2020 0920 AMR 52669 1 (Nitrite - N) 9056A 1 04/26/2020 0148 HKL 52211 1 (Phosphorus) 365.1 10 04/28/2020 1639 DMA 04/28/2020 1146 52263 1 (Soil pH meas) 9045D 1 04/23/2020 1927 SRB 51981 1 351.4 (TKN) 351.2 1 04/29/2020 1508 DMA 04/29/2020 0934 52375 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run % Solids SM 254OG 2.19 % 1 Ammonia - N (gas diffusion) 350.1 3300 91 47 mg/kg 1 Nitrate - N (soluble) 9056A 97 J 110 5.6 mg/kg 2 Nitrite - N (soluble) 9056A 15 9.1 0.88 mg/kg 1 Phosphorus 7723-14.0 365.1 14000 2300 460 mg/kg 1 Soil pH measured in water @ 18.2 ° C 9045D 7.0 su 1 TKN 351.2 30000 1100 1100 mg/kg 1 CVAA Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7471B 7471B 1 04/27/2020 2333 JMH 04/27/2020 0317 51971 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run NAgrcury 7439-97-6 7471B ND 3.7 0.88 mg/kg 1 ICP-AES Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 04/27/2020 2003 LLL 04125120201414 51966 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Aluminum 7429.90-5 6010D 38000 300 110 mg/kg 1 Arsenic 7440-38-2 6010D 4.8 J 11 3.8 mg/kg 1 Cadmium 7440.43-9 6010D 1.1 J 3.8 0.95 mg/kg 1 Calcium 7440-70-2 6010D 15000 3800 470 mg/kg 1 Chromium 7440-47-3 6010D 20 7.6 1.9 mg/kg 1 Copper 7440-50.8 6010D 220 7.6 3.4 mg/kg 1 Iron 7439-89-6 6010D 19000 76 34 mg/kg 1 Lead 7439.92-1 6010D 16 7.6 3.4 mg/kg 1 Magnesium 7439-95-4 6010D 1200 J 3800 470 mg/kg 1 Manganese 7439.96-5 6010D 1200 11 4.5 mg/kg 1 Molybdenum 7439-98-7 6010D ND 30 7.6 mg/kg 1 Nickel 7440-02-0 6010D 11 J 30 7.9 mg/kg 1 LOQ - Limit of Quantilation B - Detected in the method blank E - Quanlitalion of compound exceeded the calibration range DL = Detection Limit ND -Not defected at or above the DL N = Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL it of holding time W-Reportedonwetwelghtbasis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 7 Uienubynagro Description: Harnett WWTP Date Sampled:04121/2020 1115 Date Received:04/23/2020 ICP-AES Laooraiory lu: vuzsu1a-uu3 Matrix: Solid % Solids: 2.19 04/23/2020 2207 i Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 04/27/2020 2003 LLL 04/25/2020 1414 51966 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Potassium 7440-09-7 6010D 1800 J 3800 470 mg/kg 1 Selenium 7782-49-2 6010D ND 15 6.1 mg/kg 1 Sodium 7440-23.5 6010D 2300 J 3800 470 mg/kg 1 Zinc 7440-66-6 6010D 670 38 9.5 mg/kg 1 LOD= Limit of0uantitation 8= Detected inthemethod blank E=Ouanlilatlonofcompound exceeded the calibration range DL=DetecrlonLimit ND = Not detected at or above the DL N - Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result < LOD and > DL ul of holding lime W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of Chain of Custody �1T1 Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 7 PACE ANALYTICAL SERVICES LLC 6 R L� 'L 'C W .� eg O `�" Q q o �—` k7 ti R- IF t� iE t m.S. �c 4111titIJTi �� 91 p�' OLD 001. 0 W 1- o aas rjp PUG I10 •i 0U ❑ Auliij w$i;d Tt a (iEWI's ! 1LJ tes9:� ON, n 5 r t•Ia'v w6vurS a v lad ri xoltsad �l�J Ilh� m S [f "f?:{?f{•:�S.L,k,.((7,,��,}1};;,r ':14: I .: G1; 4.1iw7�fr••.'+.RT�{ : SI911ruv r ;yy'(( Lik= gR:vy' legjs rrJ�; 7}_�,. '.t��k:. Sa: F`.f.,i4ti� ar'i,i �. .i• � � ����,,An rr11 •_11M � V c �4 �� ti d rS {A r F 6D l�L o La o ~ 14 ❑ Eday y L..J a4j 60 � x :4 v) CL T ,nr X rtl F a � r• t _ y �3r C ,JS m .S y d rL •r. K v� �.s� N r r + v � � ➢ Id MI ,`u '� F 10FC hT• ' 4 � v C � .� cS 1�1 I� L � d h 'd kc/• r �.. IV w LI pp�p Ill .r t{ •1 } Gam! fi .� .� fi .� G? tr diC� r.. cc c Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (B03) 791-9700 Fax (803) 791-9111 www.pacelabs,com "age 6 of 7 PACE ANALYTICAL SERVICES LLC Stcn;s Cnvironrr-nial Som z _y, ]r PnNr i Or: rtxuir .td Numbar_ htCOot "f? O'T.r ve nim 4.213418 SAmp1C Receipt Cbeeldist (,SRC:) Client .Synkoi Cooler Inspomd byl4we: dMG ; 04123212020 Lot lh 1'IM13.25 Mc.U1s ol'eet U4 t: ❑ S1781 ❑ C[ienl 0 tIPS tnjfFedU OHter: - — Yas 6fl No � I. %V= custodY scats p_�seat ua the cooler; Ycs Na NA 2, lfcnkt,ld r seals w:n re}e:st were they intout anil ttnbml.erl? rIl Strip I1); NA Chlorine Strip 11); _:CIA Tested by:N'.1 _ Original ternpernture upon roceipt 1 Derived (Corrected) temperature upon receipt %Solid Snap-Cu1> :13: 1' -2043 5,$ /5_8 oL NA /N'A oC NA 'NA °C ONA °C Medlud: 0'1'emperatwe Bl:uik OAnainsl Mottles Ifs t inn lit; 6 TR Gun l:orrect[on Facto:' Meth.cdofecwlunt:_ 0 Wet lac ❑ Tee lacks ❑ixy icc ❑ None ❑ Y El No NA 3. If temperntw)a Of any Gooier ex rreded 6,0°C, wrs Project Manager Notified'? I'M wns Notified by: phone I cmaa / fac"u-face (circls one). ® Yes ❑ N o 0 NA 4, Is the commen cial eo3Ticr's packing slip a:tuuluxl to this lorm? Yes ❑ No 15. wort proper wsrody prul,'t:(illr't:s { L'IIY tliSlnPl Ct'C{ i4'C{3) IUIIaIVCII? aj Yes Nip 16. Were sample IDy listed on the COC'? � Yw ❑ Nn ?. Wen; sumple 10s listed oo ell sample ennt,tiness? Yes ❑ No 8. was sollcadon date R time :issed on the COC I ❑ Yes ®�lo _ 9. Wag colim-lion dale & time listed On ah sairrp]e containers? ® Yas ❑ No 10, Did a][ container label information (ID, dale, tit)ie) arrt;e with iL• e. COC? ® Yes ❑ No I I. v4'tsn, faststo be In:rlbintied 101tid as The COC_I ® Yes ❑ Na 12. Did all samples arrive in the prOFar containers for eadi lc.l andlor n good condilior. (utsbrf,,ken, ]ids on, ctc.)? J j Vss ©No 13_ W&K adequw-, santplu volume available? _0 Yvs O'Nol 114. Wao all samples teeeivi:d within',4 the holding(imc or •IR hours, whicliuv r come.; first? Yas O No 15_ )l'r:re atny sr:mpics conuincrs naissnt < i:xcess ci,mle one) rainplC: Igor I`srcd on COC'? 16, For VOA find RSA,-17 s smuiplus, Were bubbles present >"pea --size" (:4"Dr 61nm in diameter) [] YGs ❑ No 0 NA in any of the VOA vials? ❑ Ycs ❑ No NA 17- Wint all DRO.I netalshlutnew sainpius received at a pH of < 2? Yes Igo ®it'A 18. Wert; all 'cyanide som les reLyivcd at a aT > 12 find sulfide samples received ut n p1I > 9? 0 Yes O Na DNA l4. Wcre all app ioa leNHa,r17CN.Icylirti elp nriatt!677 (<:0 yn ps ) sornplcs tree ot'rCstcua c111orine7 _ 20. Wait Anent rouiarks;4cqucs1s (i,G. raquemd dilutions, 'MYNISCn dusignationt;, etc...) d Yg ❑ No 0 NA correctly trisn cribed C."ii the COC into tic cunlmctnt sPr.rloa hi LIMS? CJ `t'cc No LI. Was tine + sA,, number 11.4'Nrl on this container label? If i:s, quote it NA Sample Prrmwva lion (Must he cnnlplatt d Cor tiny santplc(s) incum.� ily preserved or �vilit ht�t¢elnaGe,) Sampte(s) NA wit: rcccived incorrectly pl sorvix! and were aaluhted accordingly in sample receivi,rg wits? NA a L of circic one: H2SO4. I M, 01, BCI, NLOH using Sk. ft NA I' 1'itrleofp+vsavuiicm TA Tfgore than one preservative is neWvti, plea.5e;1o(+) inn die+:ummen-.5 ht.-low, rnple(s) NA were r=`ved with 1xibbles>b run:in diameter': npleS(s) ItA- Fl were rccoived sviih'I'RC ,> 0.5 ni,%'L (Tf 419 is pin) and ivcra usted uccordingly in. somplc-mcciving with sodium lhsosul'.ttc Ni a,%C( ) with slicilly 1D: NA SR barcc:rt labels applied by: 131fo i T>,_to; D4/23/2020 - 1 Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 WvM.pacelabs.com Page 7 or7 Cameron Testing Services, Inc, Laboratory Report MC DENR*654 NC PHHS #37799 US EPA#NC01918 Client: Synagro CTS Projt. 2002-215 Project,. Harnett WWTP Requlatary Yes Sample Information 4ample'l M. Boyd D Oto 02127120 RoCOWGO: J. Cameron Rat® 02/27/20 Analyses and Results . thods R16(pronce i 2002-215 1 3ildgla C;f Peo-Coliform-S; <134000 MI/a I54800 02/28120 RL 0222D - MF 2 <35400 cruig 35400 3 <38400 CM9 38400 4 <43400 OFLY9 43400 5 <29600 M/9 29600 6 <68400 GFUN SU400 7 <48500 CFUtJ) 48500 Gownean <48800 2002-215 01 1 31wdDt Gr TS 0,745% 0-01 02e27120 RL 2540 G JS 2 3 2.61% % 0,01 4 2,31% u 0.01 5 3,38% 0.01 6 1.71% 1s 0.01 7 2,06% % 0,01 Report Review /) L � ell ac Lab Diroctor Date 219 S. Steele Sit. 919-208-11140 5anfiird NC 27330 Chris 8% Report Project Synagro Client: Hamett WWTP 38% Volatiles Reduction (EPA 625/R-921013, Appendix D) CTS Proj. Regulatory -2002-216 Sampled Received i Ref. Methods Std_ Meth. 1931 ed ar M_ Boyd Irate 02127120 By J_ Cameron Darn 02/27/20 RequesteAnalysis Analy As 2540 G - TS 2540 G - VS Type I Grab Matrix � Sludge Sample ID tabib TS N � V8 (,�j A.� Ctalyf�rs Analyst in out -0B 0.38% -09 1.27% 74.4% 45 57.5% -09 FVSR (VK) 53.5% ERp 'Pass> 38W Lab Director Notes: Pare i 1 ' Date: 219 S Stee.'e Str. Sanford, NC 22;33 Phone, 919-20a-4240 Cameron Testing Services, Inc. NC W&JOW Cori: #654 NC PHHS Corr 9 37799 US EPA NC01919 Chain of Custody Page of COi ny, Synagro E,nall: mOcyd*synagrc.ccr CTS lab use onty Con1 ?Melinda Boyd phone- 336-W9-a627 SN"?� �� Ai ddrress (City, 284 Boger Rd. I"ax tca (YIN) sute,Z" Mocksville. NC 27028 Noon: Pear& (VI j?1 ojec1_I I J :"'7 I T' lMelinda Rash i1f1N} bue: Coosctba Nsme: Boy S�rtatu�: r!�W�, -L��� Sample lnforinaticM Number c►fb6tfles Requested Ana"is Sample I D _� � x 6 z_ } $ o n z � < Preservaliti�s_ fujrt +ved. t�(o?I. IFl2 SP4. H(N)03, (Na)Th:�May. Na(0)K CTS Lab ci' M ° ° qtrie� {x), jrrdicste e `/�' I I — - -- - - Relin Dish tf: Received- DatelTime /�J��/� C50 /f /�jJ' j V Rash wo> v e ll ,requae prior approval. Addit anal charges will apply DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one orip-inaI and two conies of the application and supl)ortin2 documentation For more information, visit the Water Quality Permitting Section's Na7-Dischcitge Peruri11ii7g�Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification, ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed naiz-ative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ® For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page l of 1 RESIDLALS SOURCE FACILITY SUN MARY Applicant's name: 'Synagro Western Piedmont, LLC Status Code Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed N Harnett County Utilities North H�trtP Regional Harnett NCO021636 0 1500 315 N Town ofMayodan MayodanWWTP Rockingham NCO021873 0 N Town of Siler City Siler City WWTP Chatham NCO026441 0 1325 3 Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Town of Ma odan WWTP 2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Nadine Blackwell, Suez Area Manage` Complete mailing address: 2625 Neudorf Road City: Clemmoni State: NC Zip: `7012- Telephone number: (336) 766-0270 E-mail address: nadine.hlackwell(2suez.com 4. Facility physical address: Cardwell Rd (end of road, South). City: Mayodan State: NC Zip: s 7027 Coordinates: Latitude: 36' 23' 58" Longitude: 79' 57' 23_I" Datum: NAD 84, Level of accuracy: Second Method of measurement: MAP 5. Purpose of the facility: ® treatnent of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ® Yes ❑ No 7. Facility permitted/design flow: 3.0 MGD and facility average daily flow: 1.028 MGD 8. Average amount of residuals being generated at this facility Est.1100 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility; Type and volume of residuals treatment: Extended Aeration treatment with 4.5 million gallon capacity. Type and volume of residuals storage (i.e., outside of residuals treatment units): Digestor and aeration basins estimated 4.9 million capacity II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ® 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1 102(61 as: ® Biological ❑ Non -Biological FORM: RSC 06-16 Page] of5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Environmental Chemist, Inc. and Date of analysis: 5/6/2020 Passed corrosivity test: ® yes ❑ no. pH: sm, (2 <pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >206, OF (> 140°F) Passed reactivity test: ® yes ❑no. HCN: 0.084 mg/kg (<250) & HzS: <0.5 mg/kg (<500) TCLP Parameter Limit (mgN) Result (mg/1) TCLP Parameter Limit (raga) Result (mg/1) Arsenic 5.0 <1.0 Hexachlorobenzene 0.13 <0.05 Barium 100.0 <1.0 Hexachloro-1,3-Butadiene 0.5 <0.05 Benzene 0.5 <0.01 Hexachloroethane 3.0 <0.05 Cadmium 1.0 <1.0 Lead 5.0 <1.0 Carbon Tetrachloride 0.5 <0.01 Lindane 0.4 <0.0005 Chlordane 0.03 <0.02 Mercury 0.2 <0.0002 Chlorobenzene 100.0 <0.01 Methoxychlor 10.0 <0.0005 Chlorofonn 6.0 <0.01 Methyl Ethyl Ketone 200.0 <0.05 Chromium 5.0 < 1.0 Nitrobenzene 2.0 <0.05 m-Cresol 200.0 <0.05 Pentachlorophenol 100.0 <0.25 o-Cresol 200.0 <0.05 Pyridine 5.0 <0.05 p-Cresol 200.0 <0.05 Selenium 1.0 <1.0 Cresol 200.0 <0.05 Silver 5.0 <1.0 2,4-D 10.0 <1.0 Tetrachloroethylene 0.7 <0.01 1,4-Dichlorobenzene 7.5 <0.003 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.05 Trichloroethylene 0.5 <0.01 1, 1 -Dichloroethylene 0.7 <0.01 2,4,5-Trichlorophenol 400.0 <0.05 2,4-Dinitrotoluene 0.13 <0.05 2,4,6-Trichlorophenol 2.0 <0.05 Endrin 0.02 <.0005 2,4,5-TP (Silvex) 1.0 <0.0003 Heptachlor and its Hydroxide 0.008 <.0005 Vinyl Chloride 0.2 <0.01 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Dish•ihttliwr/LrtttrlApplicatiott: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Environment I, Inc and Date of analysis: 5/07/2020 Parameter Ceiling Concentration Limits (C1assA & ClassB) Ong/kg) Monthly Average Concentration Limits (Class A Only) (mg4g) Result (mg/kg) Arsenic 75 41 <2.5 Cadmium 85 39 IA Copper 4,300 1,500 625 Lead 840 300 131 Mercury 57 17 I 0.96 Molybdenum 75 n/a 7 Nickel 420 420 17 Selenium 100 100 I <5.0 Zinc 7,500 2,800 642 b. ForSttrfitce Disposal Unil j andfill : Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: L and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 1.69 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and mrcronutrrent parameters: Laboratory: Environment I, Inc. and Date of analysis: 5/07/2020 Parameter Result (mg/kg) Aluminum 9979 Ammonia -Nitrogen 1736 Calcium 9664 Magnesium 3141 Nitrate -Nitrite Nitrogen 2795 pl-1 (Standard Unit) 4.7 Phosphorus 3239 Potassium 4054 Sodium 5.6 Total Kjeldahl Nitrogen 55590 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.73 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth], d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 90 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a diy weight basis) and fill the results in the following table: Application Method First (I") Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 19,819 30,325 Injection/Incorporation 20,687 31,193 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1 106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal colifor7n density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [ 15A NCAC 02T. 1106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [ 15A NCAC 02T.1 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T. 1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [ 15A NCAC 02T.1 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ therrnophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irTadiation, or ❑ pasteurization. b. For Land Application of Clarss B: ® Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposarl: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a, above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt- if Daily Cover Alternative is chosen in Item II.8. below [ 15A NCAC 02T.1 106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T,1 107, specify how residuals will meet the VAR requirements: ® Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ® Alternative 3 [15A NCAC 02T.1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ® Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion), ❑ Altemative 5 [15A NCAC 02T.1 107(a)(5)] - 14-Day Aerobic Processes. ® Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization. ❑ Altemative 7 [15A NCAC 02T.1 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals. ® Alternative 9 [15A NCAC 02T.1 107(a)(9)] - Injection. ® Alternative 10 [ 15A NCAC 02T.1 107(a)(I 0)] - Incoiporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1 107(b)(2)]. C] Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC O6-16 Page 5 of 5 VICINITY MAP SYNAGRO a a 4� Z� Sturm, Ruger & Co, Inc 4 r r �4 o° Y171 �ahPcl n TWOAGNEG P Nubian Goats COUNTY: Rockingham OWNER(S): Mayodan WWTP Town of Mayodan PROCESS DESCRIPTION NPDCS Permit NCO021873 The Town of Mayodan Wastewater Treatment Plant is a 3.0 MGD design capacity facility. The annual average discharge volume in 2019 was 1.028 MGD. The facility treats a combination of domestic, industrial and commercial wastewaters. The treatment scheme includes an influent lift station, influent bar screens, an influent sampler, influent splitter box, aeration basins and secondary clarifiers. The treated effluent is disinfected by chlorination (Sodium Hypochorite) followed by dechlorination (Sodium Bisulfite) and flows through a flow measuring device, prior to discharge to the Mayo River. Excess biological sludge is thickened in one of two gravity thickeners and subsequently digested in an aerobic digester. The stabilized sludge is then land applied (on permitted sites) as a liquid directly from the digester or other approved disposal sites. The volumetric capacities are noted on the flow schematic. I nfl vent T- --. Inftuen# Bar Slow ------- 6om Unifi P Plant In uent Pump Chlorins Contact #1 FLOW SCHEMATIC TOWN OF MAYODAN WWTP *- Aeration Basin - Aeratio i Basin ; 1.75 MGD E Aeration Basin 1.25 M D Total, 1.5 MGD Hypochlorite Liquid Control ; Bleach Building r , r , ¢i Waste Sludge_._-•-- --'-•--•-- --�-- -- __ __.�...-- -••• - -_ _- -- -_ Return Sludge --------=-------------- --------- Sludge st❑�g� Clarifier Pumping Loadin 0.143 M ��ding Clarifier Digestor 0.143 MG t ' - 0-400 MG _ _ uump i d n Clarifier Clarifier r - ` 0.400 MG 0.400 MG Digestor ` Li uid i + 0.400 MG q Sludge � Sodium �------------------ ------ v Cl Thickener; Bisulifte Idg 502 Waste Sludge Flow Meter Chlorine Chlorine Contact # 2 Contact # 3 Residuals Sampling Plan Synagro Residuals Land Application for WQ0016247 Mayodan WWTP Nutrients and Metals Analysis • Sampling Point: Digestor • Sampling Frequency: Annually • Sample Type: Composite • Lab: Pace Analytical Pathogen Reduction (Fecal Colif'orm Density Demonstration) • Sampling Point: Digestor • Sampling Frequency: Annually • Sample Type: Grab • Lab: Environment 1, Inc. Vector Attraction Reduction (Specific Oxygen Uptake Rate Test) TCLP • Sampling Point: Digestor • Sampling Frequency: Annually 0 Sample Type: Grab • Lab: In-house • Sampling Point: Digestor • Sampling Frequency: Once per permit • Sample Type: Composite • Lab: Summit Environmental Technologies, Inc MAYODAN WWTP QUANTITATIVE JUSTIFICATION FOR RESIDUALS Due to the lack of recent residuals removal and fluctuating plant operations the quantity of residuals is a function of historical data and plant capacities. -Estimated maximum of 3.75 million gallons -2.0% solids -8.34 lbs/gal (3,750,000 X 8.34 X 2.0%) / 2000 = 315 Dry Tons Given the lack of recent historical land application data, it is requested that Mayodan WWTP be permitted for 315 di tons/vr. F77 :77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 910.392.0223 Lab 910.392,4424 Fax �} 710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax 255-A WiLmin tun i�ighlvay, Jacksonville, NC 285,40 • 910.347,5843 Lab/Fay ANALYTICAL & CONSULTING CHEMISTS info(a,)environmentalchenlists.com Environment - 1 Post Office Box 7085 Greenville NC 27858 Attention: Lab ID Sample ID: 20-17717 Site: Sludge Sample Test Date of Report: May 20, 2020 Customer PO #: Customer ID: 08100051 Report #: 2020-07200 Project ID: Suez Water (Mayodan WWTP) Collect Date/Time Matrix Sampled by 4/29/2020 9:00 AM Solid/Sludge Client Method Results Date Analyzed Chlordane (TCLP) SW 846 Method 808113I3510 <0.02 mg/L 05/06/2020 Endrin (TCLP) SW 846 Method 8081B13510 <0.0005 mg/L 05/06/2020 Heptachlor (TCLP) SW 846Metliod 80811313510 <0.0005 mg/L 05/06/2020 Heptachlor epoxide (TCLP) SW 846 Method 808113I3510 <0.0005 mg/L 05/06/2020 Lindane (TCLP) SW 846 Method 8081 BI3510 <0.0005 mg/L 05/06/2020 Methoxychlor (TCLP) SW 846 Method 808113I3510 <0.0005 mg/L 05/06/2020 Toxaphene (TCLP) SW 646Method 80811313510 <0.05 mg/L 05/06/2020 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/05/2020 2,4,5-Trichlorophenol (TCLP) SW 846 method 6270/3510 <0.050 mg/L 05/05/2020 2,4,6-Trichlorophenol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/05/2020 2,4-Dinitrotoluene (TCLP) SW 846 method 82708510 <0.050 mg/L 05/05/2020 Cresol (TCLP) SW 846 method 82708510 <0.050 mg/L 05/05/2020 Hexachloro-1,3-butadiene (TCLP) SW 846 method 82708510 <0,050 mg/L 05/05/2020 Hexachlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/05/2020 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/05/2020 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/05/2020 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/05/2020 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 05/05/2020 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 05/05/2020 Pyridine (TCLP) SW 846 method 827013510 <0.050 mg/L 05/05/2020 2,4,5-TP (TCLP) SW846 Method 8151A <0.003 mg/L 05/09/2020 2,4.0 (TCLP) SW846 Method 8151A <0.003 mg/L 05/09/2020 1,1-Dichloroethylene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 05/13/2020 1,2-Dichloroethane (TCLP) SW846 Method 8260/5030 <0.01 mg/L 05/13/2020 Benzene (TCLP) SW846 Method 8260/5030 <0.01 mg/L 05/13/2020 Carbon Tetrachloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 05/13/2020 Report#:: 2020-07200 Page 1 of2 • • rs�ni ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inca 6602 Windmill Wily, Wilmington, NC 28405 • 910.392.0223Lab « 910,392.4424 Fax 710 Bowsertown Read, Mantco, NC 27954 ® 252,473,5702 Lab/Fax 2-95-A Wilmington I lighway, Jacksonville, NC 2£540 e 910.347.5843 Lab/Fax in ft)riisenviroaunentalcheniists,com Environment - 1 Date of Report: May 20, 2020 Post Office Box 7085 Customer PO #: Greenville NC 27858 Customer ID: 08100051 Attention: Report #: 2020-07200 Project ID: Suez Water (Mayodan WWTP) Chlorobenzene (TCLP) SW846 Method 826015030 <0.01 mg/L 05/13/2020 Chloroform (TCLP) SW846 Method 826015030 <0.01 mg/L 05/13/2020 Methyl ethyl ketone (TCLP) SW846Method 826015030 <0,05 mg/L 05/13/2020 Tetrachloroethylene (TCLP) SW846Method 8260/5030 <0.01 mg/L 05/13/2020 Trichloroethylene (TCLP) SW846 Method 826015030 <0.01 mg/L 05/13/2020 Vinyl Chloride (TCLP) SW846 Method 8260/5030 <0.01 mg/L 05/13/2020 RCI Cyanide EPA 335A 0.084 mg/kg 05/08/2020 Sulfide SM450OSD <0.50 mg/kg 05/11/2020 Reporting limit elevated due to matrix interference. Ignitability SW 846 method 1010 >190 °F 05/20/2020 pH S W 846 Method 90450 5.51 units 05/11/2020 TCLP Metals Arsenic EPA 200.7 <'I ,0 mg/L 05/06/2020 Barium EPA 200.7 <1.0 mg/L 05/06/2020 Cadmium EPA 200.7 <1.0 mg/L 05/06/2020 Chromium EPA 200.7 <1.0 mg/L 05/06/2020 Lead EPA 200.7 <1.0 mg/L 05/06/2020 Selenium EPA 200.7 <1.0 mg/L 05106/2020 Silver EPA 200.7 <1.0 mg/L 05/08/2020 Mercury EPA 245.1 <0,0002 mg/L 05/08/2020 Comment: Reviewed by: Report tt:: 2020-07200 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client: _..,.__Date: I -jam Report Number:�j�—[:�_j�� f Receipt of sample: Delivered UPS D FeclEx ❑ Other D D YES D NO N/A 1. Were custody seals present on the cooler? J� ❑ YES I ❑ NO N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt T) C. Corrected temperature upon receipt °Ci How temperature taken: Cl Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0 D YES ❑ NO 13. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? X YES ❑ NO 1 4. Were proper custody procedures (relinquished/received) followed? 21t YES ❑ NO 5. Were sample ID's listed on the COO �) YES ❑ NO 16. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COO YES D NO 8. Were tests to be performed listed on the COO I{ YES D NO 9. Did samples arrive in proper containers for each test? YES 10 NO 10. Did samples arrive in good condition for each test? YES D NO 11. Was adequate sample volume availableT JJK YES D NO 12. Were samples received within proper holding time for requested tests? D YES D NO 13. Were acid preserved samples received at a pH of <2? �D YES D NO 14. Were cyanide samples received at a pH >12? D YES I ❑ NO 15. Were sulfide samples received at a pH >9? D YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** D YES ❑ NO 117. Were Sulfide/Cyanide received at a chlorine residual of <O.S m/L? D YES 10 NO 1 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked attime of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) __ were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 x Z O 0 U p z LU Q oQ l o Z Q O W Q o mQ LLJ N Ur O U Z Q Z S N Z 'Lu U Q 3 (lj w CIJ w m Ir a U) cn c! Z ¢ O O ULLJ O ul 0c U W ¢ ¢ U ¢ m U 171 � O w w O U y w U' l� Z C] ri U a oU U y 2 5 '" �J 2 (NJ S1S31i��fJ.3Wf/}Jt1d v "� n 1 Q V 1r� 6 F^ Z W U d ejaxa d'i0L g O C U d slulaw d-17,1. V— d sappiyaH d 101 L" L Lu U d saps !McI C11,31 ->^ o U d ]OAS/IDA dliol, I n d ,U!Rquaru2j a z SHJNIV1N0030N '^ C4 LU n m m' N01103i100.1V > O 0.:'3Nll1VEi3dW33.1 m' o ram. 7 U Z ui N0110]1�001V 1/hn d0 C] ui 0 I/bw'3N180lHOlVl01 a c z c3 0Lu M Q W i F 4 a ` U Z O y — U7Orl T—W-0j. ao CN m N. (" 7 OI z CU a) o � nn n E cn m n rn = � U � N O � d O j U O O c9 to U U c9 O L N N L O G 1� Nmw'Hw@mE@M TA hcupumbd 114 OAKMONT DRIVE GREENVII LE N,C. 27858 L+TATJ,LAlS; BLACKWELL P.O. BOY 7.279 CLENIZ•SONS , NC, 27012 VN' I'Judls Ftllalluiusll-nt ((]L'y WL 1:zsis), mg/1rg Arm* (dry ;wt. vuasis), -ng/1rg :si.cduar� (cloy ,ir,. C,'nsds), 961E/t(g Co.,lrnhim (dry : 1. basis), mg/I(g Copper (du';/ %%'L Q:a;is), fng/!rg �11rc,upldasu �, i , (Airy w1v La,`s),ralg/s(g L vkj (dry ,ieigl l b"IsiS), rng/1tg 1-4aguasitum (dr/ -:v3, basis), Ing/I(g f6enury (dfi-;/ lq#e:tm0 (ch'y vvl. Iiastsl, o-ugl;rg• Fo nsf'50"a (du',v 114. bmi's), toghtg Seiun llrm !airy 10, basis), n1glt(g SG'lium (dry M. basis): mg/l(g ?Mm (dory wt. bQ515), aq/1cg Sc(Wirn A;11504'@IUOT) RR'tio (aslc) T olal Solidv, w, 1'KH (r:lury ,g'i,), rng/ (g F 7 a�uaP,e t 1 dirogEm (dEa y wl� ),tuag/l'.g F,l3tsypl`Drwr.m, T. (dry ;aft.), o'ng/QcE I'Twale-1,10 $ie (r10/ 'Pl.), -jug/kg Piao1 Avadlmb a Mgrrogelz, Ir►g/icg Moiybdeour;rm (dry ;it, bpsls), mg/1(g sln(ige /luaAlysts Metbod ^oampie r3ele. Amlyst Carle 4.7 05/01/2C JP/j:, 40):Mll 8879 05/07/26 LFJ E7'0,200.7 <2.5 05/13/20 krt'i Me. 311311-04 M4 05/07/20 it,6 IEIPA290.7 1.4 O5/G8124E M Ti'Nf ,;130-c-4 625 05/07/20 IL?, 'PUPP,;200.7 22 05/07/20 C•IA'1 ZlibAMM 51 MR/29 i`iThA 3iiw, lM4 31.4E 05/07/20 L!Y' I2Yk20,7 0.96 OS/04/20 tNiTf/d U474713 17 '85/08/20 F3 UA200.7 4054 05/08/20 i:.L,,1• FU`4200.7 <S-0 05/14/20 MTI/; 3113B.04 2489 05/08/20 US C,'PA200,7 642 05/07/20 LFJ R FA2010 5.6 1.68 04/30/20 1W1v:R 254W-L 1 e 55592 05/07/20 'l'l H 351.2 R2-93 c 17 115/01PIO '4'011 35U—1 !U-5,3 a 32S 95/0-7120 J:"i'L, NM-7/ 2795 05/05/29 T LVJ 71,S3.2 U2-93 15819 O5/lt3/20 8RA 7 05/07/20 LCU 1Sc A209.7 PHONE (252) 756 6208 FAX (252) 756-0633 U11 990 DATE COLLECTEDs 0;/29/20 DATE, REPORTED z 05/l 8/20 RF'vzmg3V BY, 1,7Z 0 uncert!kSee, dat- . OWR doeo not orCor non,nqueoua CaYtification Pot 4iia aralYVICa1 procedure. r- 0 o u _. w r\ Q z ¢ �i �3 � J Ilk and 12 FjX'-j' d ltJ tr`Lil (..) Q QQ p W QQQ� 3 v, � _ o I! -is Fs -3ljSWA(NVUVd S f.. I I II i I I I I I Il I Ck V Ck rk l SI:A: De � Ems, II z o SH3NiVIMO3O H G O w - m NOIDT"OO B Ga,'3U()tVU33w31 — f� I, Q 17171 171 rFOI�a3'rroo IV use, ao 'aNILiOlhla I� lAiul IV.LUJ. . Lu CS 0 .� Z a m tla z A. U L: to N LO m 0l Z a Qj v cu 'A •D N O Q) 0) � En a(ni O n o E a, O U O � tb f11 U N U � f11 n C � 0) n a� cu E cn c7 .N Cf N C`f 0 E I Ln Wwi&prinkLrjq Water Iti: 1771, Wastewater FAi 10 14 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27858 FAX (252) 756-0633 SUEZ WATER (MAYODAN WWTP-SLUDGE) NADXNE BLACKWELL P.O. BOX 1279 CLEMMONS ,NC 27012 PARAMETERS Total Residue, mg/I Fecal Colirorm (MPN), /grain Solids Sample Sample Sample #1 #2 #3 17360 17260 17200 45000 46000 76000 ZD#: 990 B DATE COLLECTED: 04/29/20 DATE REPORTED : 05/04/20 REVIEWED BY: Sample Sample Analysis Method #4 #5 Daly Analyst Cade 17360 17460 04/30/20 MAR 2540B-11 45000 200000 04/29/20 MAR 9221E-06 14 OAKMONT DRIVE GREENVILLE, N.C. 27858 SUEZ WATER (MAYODAN WWTP-SLUDGE) NADINE BLACKWELL P.O. BOX 1279 CLEMMONS ,NC 27012 wtirF_ka„r•._,, DrinkSn8 Water TA Waateua t er ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 990 B DATE COLLECTED: 04/29/20 DATE REPORTED : 05/04/20 REVIEWED BY: Semple Sample Analysis Method PARAMETERS N6 N7 Date Analyst Code Total Residue, mg/1 16720 17220 04/30/20 MAR 2540E-11 Fecal Colif'orm (MPH /gram Solids 47000 52000 04/29/20 MAR 9221E-06 Environment , .ac. CHAIN OF CUSI —oDY RECORD P.O. Box 7085, 114 Oakmont Dr. Page I of 1 Greenville, NC 27858 environment) inc.com DISINFECTION CHLORINE NEUIRALIZED AT CO-LECTION Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE o pH CHECK (LAB) CLIENT: 990 B Week: s UV P P CONTAINER TYPE, PIG SUEZ WATER (MAYODAN WWTP-SLUDGE) NADINE BLACKWELL NONE { P.O. BOX 1279 CLENIINONS NC 27012 A A CHEMICAL PRESERVATION A -NONE D -NAOH E o (336) 766-0270 z w �3 ¢ „ LU B HNC, E HCL J Cc 0 Er LU z a us C HZSO; F - ZINC ACETATE/NAOH COLLECTION cc:a LU o a o c� G NATHIOSLLFATE SAMPLE LOCATION DATE 1IME Sample #1 �� 2 s = s# �a CLASSIFICAT ON: Sample I!2 2 WASTPNATER(NPDES) Sample II3 2 tray. r DRINKINGWATER R Sample #4 2 DWRIGW Sam le#5 P 2 x !� � LSample I!6 I% �' 2j _I I I I I I I I I [ I [ I SOLID WASTE SECTION Sample #7 �� � J� f 2 ��?� � ':"a* CHAIN OF CUSTODY (SEAL) MAINTAINED DURING S.ENT/DELIVERY I Y N € SAMPLES COLLECTED BY: (Plea?,l Z f [ [ I I [ I l f l[ I[ l l l[[ 1 1 1 II � SAMPLESRECE 1NLABAT--[---d -C R ISHED BY (SIG.) (SAMPLER) D TPTIME RECEIVED BY (SIG.) DATEITIME COMMENTS: T — UISH SIG.} DATEIiIME R1 CEN {SIG.) DA ME QUISHI±DBY(Sl3.) DATEtTIME 1 RECEIVED BY (SIG.) ATFITIME 1 FSE READ Instructions for completing this form on the reverse side. Sampler must place a"C" for composite sample or a "G" for FORM as Grab sample in the blocks above for each parameter requested. N ,75214 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 0 M Slope: Intercept: Correlation Coefficient: own or ma oaan V00002672 5/13/2020 15.1 /13/2020 / 11:00 am iary Moore /13/2020 / 11:05 am 'ary Moore milliliters 1.68 % Dry Solids 15.1 degrees Celsius 15.1 [degrees Celsius 0.0 10.1 1.D Oxygen Uptake Rate: 2.54 mg Oxygen/L/Hr Ambient Specific Oxygen Uptake Rate: 0.151 mg Oxygen/hr/g Average Temperature: 15 degrees Celsius Temperature Correction Factor: 1,402551731 Temperature Corrected Specific Oxygen Uptake Rate:l: 0.210'mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Oxygen Uptake Rate Chart 10.2 -- 10 I I 9.8 --� y = -0.042 .X + 10-1 M %.6 0 o _ /A /A q9.4 9.2 9 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 Time (minutes) Sample Location: Mayodan Digester Sample Date: 5/13/2020 Sample Time: 11:00 AM Analysis Date: 5/13/2020 Analysis Time: 11:05AM State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise rioted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Pl ater Qualioi Pewnitting Section's Non -Discharge Permiltln Unit General This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1 100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessaiy for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate ceitification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities, B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® Foreach source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ® For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page I of I RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: a.3Tagro Western Piedmont, LLC Status Codea Facility Permit Holder Facility Name County Permit Number Maximum DryTons Per Year Current Proposed N Hamett County Utilities North Hamett Regional egional Hamett NCO021636 0 1500 N Town of Mayodan Mayodan WWTP Rockingham NCO021873 0 315 N Town of Siler City Siler City WWTP Chatham NCO026441 0 1325 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): . Facility Name: Siler City WWTP 2. Facility permit holder is: ❑ Federal, ❑ State, ® Local Government, or ❑ Private. Facility pennit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Brittany York, WW Su Rerinten nt Complete mailing address: 370 Waste Treatment Plant Rd. City: Siler City State: NC Zip: 27344 Telephone number: (919) 742-4581 E-mail address: byork a,silereity.org 4. Facility physical address: 370 Waste Treatment Plant Rd City: Siler City State: NC Zip: 27344-___j Coordinates: Latitude: 350 43' 44" Longitude: 790 25' 39" Datum: NAD 84', Level of accuracy: ]Second Method of measurement: MAP 5. Purpose of the facility: ® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater in ixed with domestic wastewater, (approximate percentages: % industrial and % domestic) ❑ other (explain: ' ). 6. Does the facility have an approved pretreatment program: ❑ Yes ❑ No 7. Facility permitted/design flow: 4_0 MGD and facility average daily flow: 1_8 MGD 8. Average amount of residuals being generated at this facility Est. 425 dry tons per year. 9. Specify the fbllowing regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 1.8 MG Oxidation Ditches Type and volume of residuals storage (i.e., outside of residuals treatment units): 1 MG Sludge Thickening Basin RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: Z 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, othemise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1 102(6) as: ® Biological ❑ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, anunal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed fihn systems). FORM: RSC06-16 Page 1 of r 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): F b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Summit Environmental and Date of analysis: 2/4/2020 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: nonflammable °F (> 140°F) Passed reactivity test: Eyes ❑no. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500) TCLP Parameter Limit (mg/!) Result (mg//) TCLP Parameter Limit (mg/l) Result (mg/l) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND in -Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1, 1 -Dichloroethylene 0.7 ND 2,4,5-Trichlorophenol 400.0 ND 2,4-Dinit•otoluene 0.13 ND 2,4,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under _15A NCAC 02T .1 105. a. For Dlstr•ilontionlLand Application Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratoiy: Waypoint Analytical and Date of analysis: 4/08/2020 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 < 18.5 Cadmium 85 39 <3.7 Copper 4,300 1,500 270 Lead 840 300 <11.1 Mercury 57 17 <0.548 Molybdenum 75 n/a <9.26 Nickel 420 420 21.3 Selenium 100 100 <18.5 Zinc 7,500 2,800 485 b. For Surface Disttnsrrl Urril (laud ll). Fill in the following table with the results of the latest analyses (i.e., on a dhy weight basis) for the following metal parameters: Laboratoiy: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ >_ 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nut rient/Micronutrient Determination: Complete the following: a. Total solids: 2.66 %. b. Fill in the following table with the results of the latest analyses (i.e., on a diy weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waxpoint Analytical and Date of analysis: 4/08/2020 Parameter Result (mg/kg) Aluminum 51,500 Ammonia -Nitrogen 5,960 Calcium 11,300 Magnesium 1,570 Nitrate -Nitrite Nitrogen 1,490 pH (Standard Unit) 6.4 Phosphorus 17,500 Potassium 3,460 Sodium 4,960 Total lejeldahl Nitrogen 66,300 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.89 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treahnent of municipal or domestic wastewater, cxpkiin or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (I") Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 22,572 34,344 Injection/Incorporation 25,552 37,324 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: N/A FORM: RSC 06-16 Page 4 of 5 7. P.itho[Zen Reduction: Per 15A NCAC 02T.1 106, specify how residuals will meet the pathogen reduction requirements: a. For Dislribrrliorr/L(ind Applieallorr of'Class A or E2niyalew: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.1 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [ 15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [ 15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing f'or Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [ 15A NCAC 02T.1 I O6(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [ 15A NCAC 02T.1 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thennophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Lar1d Applicrrfiorr ofiCla.Vs B: ® Alternative I [I5A NCAC 02T.1 106(c)(I )] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP), Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. ForSrrfireeD4osa ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item I1. 7b. above. ❑ Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [ 15A NCAC 02T. 1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction VAR): Per 15A NCAC 02T.1 107, specify how residuals will meet the VAR requirements: ® Alternative 1 [15A NCAC 02T.1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T. 1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ® Alternative 3 [15A NCAC 02T.1 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ® Alternative 4 [15A NCAC 02T. 1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.1 107(a)(5)] - 14-Day Aerobic Processes. ® Altemative 6 [15A NCAC 02T.1 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.1 107(a)(7)] - Dzying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.1 107(a)(8)] - Diying of Unstabilized Residuals, ® Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ® Alternative 10 [15A NCAC 02T.1 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.I 107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 VICINITY MAP SYNAGRO �mnimeia s V Murphy USA Ea Chlckc_n 'N BrarBQ T jaragles az� San Eellpo Mcmlram Walmart Supercenter ro Waste Management - Sanford Transfer Station azi " °Ves Creek ai WASTE WATER Y1 TREATMENT PLAT az 1 COUNTY: Chatham OWNER(S): Ski- City Wastewater Treatment Plant TOWN OF SILER CITY PERMIT RENEWAL QUANTITATIVE JUSTIFICATION FOR RESIDUALS PRODUCTION RATE The following is a record of the annual land application volume for the Town of Siler City's wastewater treatment plant: Year Dt' Tons Lanz! A > >lierl 2016 336.55 2017 450.59 2018 301.29 2019 340.72 The proposed permitted volume (1,325 diy tons per year) is greater than the anticipated need for the coming years. Over the 5 years shown above the average number of dry tons land applied were 357.28, which is well within reason of the permitted dry tonnage. Looking forward the volume of material is expected to increase due to returning industries. Residuals Sampling Plan Synagro Residuals Land Application WQ0016247 Town of Siler City NC WWTP Nutrients and Metals Analysis • Sampling Point: Basin • Sampling Frequency: 4/yr • Sample Type: Composite • Lab: Waypoint Analytical Pathogen Reduction (Fecal Coliform Density Demonstration) • Sampling Point: Basin • Sampling Frequency: 4/yr • Sample Type: Grab 0 Lab: Meritech Inc. Environmental Lab Vector Attraction Reduction (SOUR Test) TCLP • Sampling Point: Digester • Sampling Frequency: 4/yr • Sample Type: Composite • Lab: In house • Sampling Point: Basin • Sampling Frequency: Annually • Sample Type: Composite • Lab: Summit Environmental Technologies, Inc ,6 - >— J U Q F— Z W W a WO F� W LLJ J � 3Q Q 3 U W J A 1 A AY.i+ln�-ii K1{ yy Sg400dr��i ry pry n nnrf r qq ri vvI� i H vn nri y{n v J I ySpf .o-nn�ea.. oR&fyRniCS6R19AR=Ff r�� sr rv. w gAyYa �w .r w w wu-r�bMwVtwtil+ mw a �awan �ws Process Flow • Flow comes into the Plant, Travels through the Bar screen where it removes bigger items (rags, gloves, sticks, feminine products) • Then it flows into the Grit Collector where the majority of the grit and sand is removed via the Grit auger, which dumps into a dumpster and is removed twice a week. • Flow then travels to the Influent pump station where the flow is pumped up the hill to the Oxidation Ditches • Then it proceeds to the Clarifiers thru the splitter box where the Lime and Alum is added • From the Clarifier the water travels to the Filters by way of the junction box where Chlorine is added • From the Tertiary filters the water travels to the contact chamber, S02 is added and • Then down the cascade aerator and out to the creek. • From the clarifiers the sludge will either be returned to the Oxidation Ditches or wasted to the Digesters • Where it then goes to the Thicken Sludge Basin and out to the farms. SUMMIT E[��IR;7A1fd�fd7AL��CNk�fSL+��33�5, iti�` J1n�lyticat �ab�ra[nN�s February 13,2020 Ryan Copeland Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Dear Ryan Copeland: Suninrit Emviroumental Technologies, hrc. 3310 TVin St. Cigahoga Falls, Olrio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489 TVebsite: h11n:/Annj,.se[1ek.conl Order No.: 20011551 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/24/2020 fbr the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NF1,AC E87688, Georgia E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Matyland 339, Minnesota 409711, New Hampshire 2996, New Jersey OH006, Now York 11777, NorthCarorura 39705 and 631, NotthDakota R-201, Ohio DW, Oltio VAP CL0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas TI 04704466-11-5, Utah OH00923201 1-1, VirginJa VELAP 9456, Washington C891 Page 1 of 32 �1T S,mm,tfEurlroua,enta,Technologies, Inc. Case Narrative S3310 R in St. ENVU10A ENTAL TVCIIN01.oG1rqS, INC: Cuyahoga Falls, Ohio 44223 WO#: 20011551 Analyflcal taboralar)ev TEL: (330) 253-8211 FAX (330) 253-4489 tVebslfe: a1r ://Wwiv.setlekeoul Date: 2/13/2020 CLIENT: Synagro Project: WorkOrder Narrative: 2001 1551: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summaty Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program Analytes Repotl" for accredited analytes list. The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Prep Sample QC Comments: 2001 1590-001 A 507180: Prep Comments for MtlPrep_TCLP(3010A), Sample 20011590-001 A: Sample filtered after digestion. Analytical Sequence Sample Notes: 2001 1551-001A TCLP-SVOC-CPEST(808 I B): Bracketing CCVs failed high for some analytes. Samples in batch 41806 were non -detect for all analytes. 2001 1551-001A TCLP-SVOC-CPEST(8081 B): LCS exhibited high recovery for several analytes; Sample is ND 2001 1551-001 A TCLP-SVOC-HERB_NPW(8321 B): Sample exhibited high recovery of Surrogate: DCAA; Sample is non -detect for all analytes of interest. Original Page 2 of 32 SUMMIT S,mnnil Environmental Technologies, Inc. Case Narrative 3310 6Vin S!. ENVIII01JPsi LWAL'tGCIMMOGWS, Wr. Cuyahoga Falls, Ohio 44223 WO#: 20011551 Analytical Loborarorw 7EL: (330) 253-8211 FAX: (330) 253-4489 6Vebsife: htty:/hi�rw.seuek.cor,, Date: 2/13/2020 CLIENT: Synagro Project: Analytical Sequence QC Notes: CCV-108861 VOC-MSTR_NPW(8260): The VOC CCV (Batch R 108861) exhibited high recovery for Vinyl Chloride; All samples were ND. Original Page 3 of 32 SUMMj0t Srnnrrrit Lrrnirorrrrrerrtnl 3310 Teclufl, in /n Qualifiers and Acronyms 33/0 V ENVInOWADOTAL 1ECIfN01,t1( jFC;' Pmr Cuyahoga Falls, Ohio442� WO##: 20011551 tlnatVrlcal Laboralarlas TEL: (330) 253-821I FAX: (330) 253-44d Website: Irtty:/in°mu.sellek.co Date: 2/13/2020 These commonly used Qualifiers and Acronyms may or may not be present in this report, Qualifiers T The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. m Manual integration was used to determine the area response. cl Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25%difference. C The result has been confirmed by GUMS. N The result was not confirmed when GC/MS Analysis was perlormed. B/NIB+ The analyte was detected in the associated blank, C The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QNI-/+ The MS or MSD recovery failed low (-) or high (+), QNIR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits, Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting I..imit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ I..evel OfQuantilation LCSD I..aboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegU l Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CIF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting, Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 4 of 32 SUMMIMF Sraniirii Gnriroiriireirial Technologies,1,ic. Workorder 3310 6Vin Sr. E6WHIONfill Cuyahoga Falls, Ohio 44223 Sample Summary AsmlyVci t L dbOral0 ve TEL: (330) 253-821 / PAX: (330) 253-4489 WO#l: 20011551 Websire: hrrn://ma,r.seuek.conr 13-Feb-20 CLIENT: Synagro Project: Lab SamplelD Client Sample LD 20011551-001 SilerCity WWTP Tag No Date Collcetcd 1/22/2020 1:15:00 PM Date Received Matrix 1/24/2020 10:20:00 AM Sludge Page 5 of 32 SUMMIT nnN„.;,v;rn,,s•,narTacl,u310 n.0 DATES REPORT 33f0IVinS7. ENVIiIOtLAEt7TAt 1711kn14gIFR.tNC Qi,oho, lYAls Ohio 44223 Annlptleaf tabOratorlla 7EL: (330) 253.8211 EAK (330) 253-4489 WON: 20011551 IYehVile: hIt r.'v u�r..re!lekernn 13-Feh-20 Client: Synagro Project: Sample 11) Client Sample in Collection Date Matrix TestNnme Leachate Date Prep Date Analysis Date 20011551-OOIA SilerCilyNV\VTP V22/20201:15.00PM Sludge IgnitabilityoPSolids(SW-846t 1030) 2/3/20201:00:00PM PH (SW9045D) V2912020 12:15:53 PM Reactive Cyanide (9014/7.3.3.2)-Solid 216/20203t36:001'M Reactive Sulfide (9034)/7.3.4.2 2/16/2020 1:15:00 PM 'TCLP Heibicides by EPA 83218 1/31/2020 5.00.00 PM 2/7/2020 829:00 AM TCLP Mercury Analysis (S W I311/747 V31/2020 5:00:00 PM 2/4/2020 9 00:00 AM 2/4/2020 2:16:00 PM TCLP Metals Analysis (SW 1311/60101131/2020 5:00:00 PM 2/3/2020 I 1:35:00 AM 2/4/2020 1:41.20 PM TCLP Pesticides Analysis (SW1311/8(1731/20205,0O:OOPM 2/3/202010:45:00AM 2/6/202012:27:00AM TCLP Semi-Volatiles Analysis 1/31/2020 5:00:00 PM 2/3/2020 10:3Q00 AM 2/4/2020 k24:00PM (SW 1311/8270) TCLP Volmiles Analysis 1/31/20205:00-OOPM 2/3/20207:58:OOPM Original Page 6 of 32 Summit Envir•onmewal Technologies, hrc' Analytical Report u mm i ss 33/0 4Vhr Sr. ENVIIIONIACNiALTt:OIINOt.O€;Itln, Mr, Criyahoga Falls, oleo 44223 (base report) Analytica/ Labaralarlm 7EL: (330) 253-8211 FAX: (330) 253-4489 WO#: 20011551 6Vebsile: lrlrr2-/A nr.serrek.cOm Date Rcported: 2/13/2020 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/22/2020 1:15:00 PM Lab ID: 20011551-OOIA Project: Client Sample ID Siler City WWTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: MJM TCLP MERCURY ANALYSIS (SW1311 /7470) TCLP Mercury ND 0.00200 mg/L 1 2/4/2020 2:16:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: EAM TCLP METALS ANALYSIS (SW1311/6010) TCLPArsenic(As) ND 0.500 mg/L 1 21412020 1:41:20 PM TCLP Barium(Ba) ND 5.00 mg/L 1 2/4/2020 1:41:20 PM TCLP Cadmium(Ccl) ND 0.100 mg/L 1 2/4/2020 1:41:20 PM TCLP Chromium(Cr) ND 0.200 mg/L 1 2/4/2020 1:41:20 PM TCLP Lead(Pb) ND 0.500 mg/L 1 2/4/2020 1:41:20 PM TCLP Selenium(Se) ND 0.0500 mg/L 1 2/4/2020 1:41:20 PM TCLP Silver(Ag) ND 0.500 mg/L 1 2/4/2020 1:41:20 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270 SW3510C Analyst: SFG TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270) 1,4-Dichlorobenzene ND 0.200 mg/L 2 2/4/2020 7:24:00 PM 2,4,5-Trichlorophenol ND 0.500 mg/L 2 2/4/2020 7:24:00 PM 2,4,6-Trichlorophenol ND 0.500 mg/L 2 2/4/2020 7:24:00 PM 2,4-Dinitrotoluene ND 0.100 mg/L 2 2/4/2020 7:24:00 PM Cresols, Total ND 10.0 mg/L 2 2/4/2020 7:24:00 PM Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 2/4/2020 7:24:00 PM Hexachlorobenzene ND 0.100 mg/L 2 2/4/2020 7:24:00 PM Hexachloro ethane ND 0.200 mg/L 2 2/4/2020 7:24:00 PM Nitrobenzene ND 0.200 mg/L 2 2/4/2020 7:24:00 PM Pentachlorophenol ND 0,500 mg/L 2 2/4/2020 7:24:00 PM Pyridine ND 0.500 mg/L 2 2/4/2020 7:24:00 PM Surr: 2-Fluorophenol 53.6 10 - 109 %Rec 2 2/4/2020 7:24:00 PM Surr: Phenol-d6 52.4 10 - 109 %Rec 2 2/4/2020 7:24:00 PM Surr: Nitrobenzene-d5 62.5 19 - 120 %Rec 2 2/4/2020 7:24:00 PM Surr: 2,4,6-Tribromophenol 74.2 10 - 120 %Rec 2 2/4/2020 7:24:00 PM Surr: 2-Fluorobiphenyl 60.3 22 - 117 %Rec 2 2/4/2020 7:24:00 PM Surr: p-Terpheny1-d14 90.0 34 - 116 %Rec 2 2/4/2020 7:24:00 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response / MC Value is below Minimum Compound Limit, N Tentatively identified compounds l ND Not Detected P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Original RL Reporting Detection Limit U Samples with CalcVal < MDL Page 7 of 32 Snmmir Environmental Technologies, Inc, S U Eqn MM I i 3310 fVie St. faVllttlNlnCM7AL"ti iiNr71.[7CIC",, tNr Cuyahoga Falls, Ohio 44223 Armiytical toboreroni, TEL: (330) 253-8211 FAX. (330) 253-4489 fVebsiie: Lrtm:/RviU=11ek.com Analytical Report (base report) WO#: 20011551 Datc Reported: 2/13/2020 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/22/2020 1:15:00 PM Lab ID: 20011551-OOIA Project: Client Sample ID Siler City WWTP Analyses Result RL Qua[ Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP PESTICIDES ANALYSIS (SW1311/8081) Chlordane, total ND Toxaphene ND Endrin ND gamma-BHC ND Heptachlor ND Heptachlor epoxide ND Methoxychlor ND Surr: TCMX 14A Surr. DCB 18.4 TCLP HERBICIDES BY EPA 8321 B 2,4-D ND 2,4,5-TP ND Surr: 2,4-Dichlorophenylacetic aci 149 SW8081 SW3510C Analyst: SEK 0.125 mg/L 5 2/6/2020 12:27:00 AM 0.250 mg/L 5 2/6/2020 12:27:00 AM 0.0125 dQL+ mg/L 5 2/6/2020 12:27:00 AM 0.0125 dQC+ mg/L 5 2/6/2020 12:27:00 AM 0.0125iQC+QL+mg/L 5 2/6/2020 12:27:00 AM 0.0125iQC+QL+mg/L 5 2/6/2020 12:27:00 AM 0.0125iQC+QLimg/L 5 2/6/2020 12:27:00 AM 10 -1 19 %Rec 5 2/6/2020 12:27:00 AM 10 - 119 %Rec 5 2/6/2020 12:27:00 AM SW8321A SW1311M Analyst: BJH 0.500 mg/L 50 2/7/2020 8:29:00 AM 0.500 mg/L 50 2/7/2020 8:29:00 AM 70 - 130 S %Rec 50 2/7/2020 8:29:00 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260 SW1311M Analyst: RMT TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 0.500 mg/L 100 2/3/2020 7:58:00 PM 1,2-Dichloroethane ND 0.500 mg/L 100 2/3/2020 7:58:00 PM MEK ND 10.0 mg/L 100 2/3/2020 7:58:00 PM Benzene ND 0.500 mg/L 100 2/3/2020 7:58:00 PM Carbon tetrachloride ND 0.500 mg/L 100 2/3/2020 7:58:00 PM Chlorobenzene ND 5.00 mg/L 100 2/3/2020 7:58:00 PM Chloroform ND 0.500 mg/L 100 2/3/2020 7:58:00 PM Tetra chloroethene ND 0.500 mg/L 100 2/3/2020 7:58:00 PM Trichloroethene ND 0.500 mg/L 100 2/3/2020 7:58:00 PM Vinyl chloride ND 0.200 QC+ mg/L 100 2/3/2020 7:58:00 PM Surr: 4-Bromofluorobenzene 98.2 70 - 130 %Rec 100 2/3/2020 7:58:00 PM Surr: Dibromofluoromethane 106 70 - 130 %Rec 100 2/3/2020 7:58:00 PM Surr: Toluene-d8 103 70 - 130 %Rec 100 2/3/2020 7:58:00 PM Qualifiers: B Anaiyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation oranalysis exceeded M Manual Integration used to detenninearea response MC Value is below Minimum Compound Limit, N Tentatively identified compounds ND Not Detected P Second column confirmation exceeds PI. Pennit Limit R RPD outside accepted recovery lim its Original RL Reporting Detection Limit U Samples with CalcVal < MDL Page 8of32 1 SUMM111- Summit Environmental Technologies, Inc. 33/0 6Vin St. Analytical Report ENVIItL11JIAENTAt TTCIINr1LOCIFS, mr.. Cuyahoga Falls, Ohfo 44223 (base report) AnalytIcal Lattoratoner TEL- (330) 253-8211 FAX. (330) 253-4489 WOM 20011551 6f ebsite: httn;/Ariviv.sellek.cO1 t Date Reported: 2/13/2020 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/22/2020 1:15:00 PM Lab ID: 20011551-OOIA Project: Client Sample ID Siler City WWTP Analyses Result RL Qual Units DF Date Analyzed RCI-SOLID-Wl IGNITABILITY1030 SW9014 Analyst: CXS REACTIVE CYANIDE (901417.3.3.2)-SOLID Cyanide, Reactive ND 12.1 mg/Kg I 2/6/2020 3:36:00 PM RCI-SOLID-Wl IGNITABILITY1030 SW1030 Analyst: AJT IGNITABILITY OF SOLIDS (SW-846: 1030) Ignitability non-flammable mm/sec 1 2/3/2020 1:00:00 PM RCI-SOLID-Wl IGNITABILITY1030 SW9045D Analyst: VVK PH (SW9045D) PH 6.8 s.u.@20.9C 1 1/29/2020 12:15:53 PM RCI-SOLID-WI IGNITABILITY1030 SW9034 Analyst: CXS REACTIVE SULFIDE (9034)17.3.4.2 Sulfide, Reactive ND 25.0 mg/Kg 1 2/16/2020 1:15:00 PM Qualifiers: B Analyte detected in the associated Method Blank G Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response i MC Value is below Minimum Compound Limit. N Tentatively identified compowids l ND Not Detected P Second column confirmation exceeds PL Permit Limit R RPD outside accepted recovery limits Original R.I_ Reporting Detection Limit U Samples with CalcVal < MDL Page 9 of 32 UMM,T Summit EnNirorrulerrinlTechrrologies, lnc. Accreditation Program 3310 Rin St. Anal tes Report 514VInONWENTAL 1'E(:HNO[ OMF ;, WC Cuyahoga Falls, Ohio 44223 Y I' Amlykal Leboraloilte 78L: (330) 253-8211 rAX: (330) 253-4489 WOM 20011551 Websire. 13-Feb-20 Client: Synagro State: NW Project: Program Name: NC WW SCM Sample 1D Matrix Test Name Analyte Status 200115 51-001 A Sludge Ignitability of Solids (SW-846'. 1030) Ignitability A Sludge pH (SW9045D) Hydrogen ton (pH) A Sludge Reactive Cyanide (9014/7.3.3.2)-Solid Cyanide, Reactive U Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U Sludge TCLP Herbicides by EPA 8321 B 2,4,5-TP A Sludge TCLP Herbicides by EPA 8321 B 2,4-D A Sludge TCLP Mercury Analysis (SW 1311/7470) Mercwy A Sludge TCLP Metals Analysis (S W 131 1/6010) Arsenic A Sludge TCLP Metals Analysis (SW1311/6010) Barium A Sludge TCLP Metals Analysis (SW1311/6010) Cadmium A Sludge TCLP Metals Analysis (S W 1311/6010) Chromium A Sludge TCLP Metals Analysis (SW1311/6010) Lead A Sludge TCLP Metals Analysis(SW1311/6010) Selenium A Sludge TCLP Metals Analysis (SW1311/6010) Silver A Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A Sludge TCLP Pesticides Analysis (S W 1311/8081) Endrin A Sludge TCLP Pesticides Analysis (SW 1311 /8081) gamma-BHC A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Sludge TCLP Pesticides Analysis (SW131 1/8081) Heptachlor epoxide A Sludge TCLP Pesticides Analysis (S W 1311/8081) Methoxychlor A Sludge TCLP Pesticides Analysis (S W 131 1 /8081) Toxaphene A Sludge TCLP Semi-Volatiles Analysis (SW1311/8270) 1,4-Dichlorobenzene A Sludge TCLP Semi-Volaliles Analysis (S W1311/8270) 2,4,5-Trichlorophenol A Sludge TCLP Semi-Volatiles Analysis (SW 1311/8270) 2,4,6-Trichlorophenol A Sludge TCLPSemi-Volaliles Analysis (SW1311/8270) 2,4-Dinitrotoluene A Sludge TCLP Semi-Volaliles Analysis (S W 131 1 /8270) Cresols, Total A Sludge TCLP Semi-Volaliles Analysis (SW 131 1/8270) I-lexachlorobenzene A Sludge TCLP Semi-Volaliles Analysis (SW131 1/8270) Hexachlorobrdadicne A Sludge TCLP Semi-Volaliles Analysis (S W 131 1/8270) I-lexachloroelhane A Sludge TCLP Semi-Volaliles Analysis (S W 1311/8270) Nitrobenzene A Sludge TCLP Semi-Volaliles Analysis (SW1311/8270) Pentachlorophenol A Sludge TCLP Semi-Volaliles Analysis (SW 1311/8270) Pyridine A Original # 1 Page 10 of 32 Sunni! Environmental Technologies, hrc, Accreditation Program UM'Nt 331nwrnS` Anal tes Report Y EN0110}J6ACNTAL T�CNN01 001r£., Mr Cuyahoga Falls, Ohio 44223 AfwVflcal Laborator)& TEL: (330) 253-8211 FAY: (330) 253-4489 WO#: 20011551 Websife: lit fr.//u srsr.selfekconr 13-Feb-20 Client: Synagro State: NW Project: Program Name: NC_WW SCM Sample ID Matrix Test [tame Analyte Status 20011551-001A Sludge TCLP Volatiles Arialysis Ll-Dichloroethene A Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A Sludge TCLP Volatiles Analysis 2-Butanone A Sludge TCLP Volatiles Analysis Benzene A Sludge TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volatiles Analysis Chlorobenzcne A Sludge TCLP Volatiles Analysis Chlorolorm A Sludge TCLP Volatiles Analysis Tetrachlorocthene A Sludge TCLP Volatiles Analysis Trichloroclhene A Sludge TCLP Volatiles Analysis Vinyl chloride A Original # I Page 11 of 32 SwInnitbrirmiu,e,rinl7 chnologies, Inc. SQC SUMMARY REPORT ,u M M' IVinr SI. EN%gMONMENTAL T[f.HHOrOOri ;, Wr Ctq'ahogn Fo!!s3310 Ohio 14223 AnMytfrnf Ln6nrntnlraP 76L: f330) 253-82 11 1,;4X: (330) 253-1189 W011: 20011551 Wehrire: h11u mvsv.serrek vain 13-Peb-20 Client: Synagro Project: 13atch[D: 41775 iamplelD: MB•41775 SampType: MBLK TestCode: TCLP-VOC-M Units: mglL Prep Date: 113112020 RunNo: 108884 '.Bent ID: PBS Batch ID: 41775 TestNo: SW8260 SW1311M Analysis Date: 21412020 SegNo: 2603620 \nalyte Result PQL SPKvalue SPK Ref Val %REC Lowt-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1-Dichloroethene ND 0.0500 1,2-Dichloroethane ND 0,0500 MEK ND 1.00 Benzene ND 0.0500 Carbon tetrachloride ND 0.0500 Chlorobenzene ND 0.500 Chloroform ND 0.0500 Tetrachloroethene ND 0.0500 Trichforoethene ND 0.0500 Vinyl chloride ND 0.0200 Surr:4-Bromofluorobenzene 492 Sure: Dibromofluoromethane 520 Surr: Toluene d8 517 Qnnliriers: B Analyte defected in the associated Method Blank I Analytedctaledbeloevquanlitationfimits ND Not Detected R RYD outside accepted recovery limits 500.0 98.4 70 130 500.0 104 70 130 500.0 103 70 130 E Value above quantitation range M Manual lntegation used to determine area response P Second column confirmation exceeds I(L Reporting Detection Limit Page 12 of 32 H Holding times for preparalion or anai) MC Value is beloev Minimum Compound Pt, Permit Limit S Spike Recovery outside accepted reco Q C+ Original 91SUMM111- 3310JYilr S1- Sunnuil himuiroroneulrrl7echns,bu- QC SUMMARY REPORT 33l0 l Ei�VIat3MAEN1'pL tCC nNdl.dRlFS, INt' Cbyalugo l"ollr, Ohio 44223 WOtt: 20011551 Annfyliral Lpbnralnlleo 7EL: (330) 253-A2111,AK (330) 2534469 Websile. ham-llmutre.sellek.ivmr 13-Feh-20 Client: Synagro Project: Batch ID: 41795 Sample ID- MB-41795 SampType: M13LK TestCode: Mti-TCLP•7(6 Units: mg/L Prep Date: 213/2020 RunNo: 108891 Client ID: PBS Balch ID: 41795 TestNo: SW6010D SW3010A Analysis Date: 214/2020 SegNo: 2604322 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit High✓_imil RPD Ref Val %RPD RPDLimil Qual TCLP Arsenic(As) ND 0.500 TCLP Barium(Ba) ND 5.00 TCLP Cadmium(Cd) ND 0.100 TCLPChromium(Cr) ND 0200 TCLP Lead(Pb) ND 0.500 TCLP Selenium(Se) ND 0.0500 TCLP Silver(Ag) ND 0.500 Sample ID: LCS-41795 SampType: LCS TestCode: Mtl-TCLP-7(6 Units: mglL Prep Date: 2/3/2020 RunNo: 108891 Client ID: LCSS Batch ID: 41795 TestNo: SW6010D SW3010A Analysis Dale: 2/4/2020 SegNo: 2604323 Analyle Result PQL SPKvalue SPKRefVal %REC Lowl-imit Hightlmit RPDRefVal %RPD RPDLimit Qual TCLP Arsenic(As) 1.97 0.500 2.000 0 98.3 80 120 TCLP Barium(Ba) ND 5.00 2.000 0 104 80 120 TCLPCadmium(Cd) 2.20 0.100 2.000 0 110 80 120 TCLP Chromium(Cr) 2.06 0.200 2.000 0 103 80 120 TCLP Lead(PW 2.17 0.500 2,000 0 108 80 120 TCLP Selemum(Se) 2.18 0.0500 2.000 0 109 80 120 TCLP Silver(Ag) 2.19 0.500 2.000 0 i09 80 120 Qunlifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times far preparation or anal) f Analyte detected below quantitation limits M Mammal Integration used to determine area response MC Value is belmv Minimum Compound ND Not Detected P Second column continuation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RI, Repating Detection Limit S Spike Recovery outside accepted reco Page 13 of 32 iuMM111,,»,»ac,,,itrn,,,e»i�larr,,3310rinSi. QC SUMMARY REPORT 33/0 WinSi. ENWROWNUTAL=iIHOLOW-S.IHC 01,io44223 AahlytfCnl tRbnrefarlFS TEL (330) 25382// FAX: (330) 253-4489 W09: 20011551 IYebsire: heu./Av,rsv..cei7ektour 13-f'eh-10 Client: Synagro Project: Kateh[D: 41814 ;ample ID: MB-41814 SampType: MBLK TeslCode: SVOC•BNA_T Units: mg/L Prep Dale: 21312020 RunNw 108857 aient ID: PBS Balch ID: 41814 TesiNo: SW8270 SW3510C Analysis Dale: 2/412020 SegNo: 2604887 knalyte Result POL SPKvalue SPKRefVal %REC Lowl-imil Hight-imil RPDRefVal %RPD RPDLimil Oual 1,4-Dichlorobenzene ND 0.100 2,4,5-Trichlorophenol ND 0.250 2,4,6Trichlorophenol ND 0.250 2,4-Dlnilrololuene ND 0-0500 o-Cresol ND 0,250 Cresols, Total ND 5.00 Hexachloro-1,3-buladiene ND 0,0200 Hexachlorobenzene ND 0,0500 Hexachloroethane ND 0A00 Nitrobenzene ND 0.100 Pentachlorophenol ND 0.250 Pyridine ND 0.250 Surr: 2-Fluorophenol 0,450 Surr- Phenol-d6 0-488 Surr: Nitrobenzene-d5 0.471 Surr: 2, 4,6-Tri bromophenol 0-812 Surr: 2-Fluorobiphenyl 0.474 Surr: p-Terphenyl-d14 0,861 Qualifiers: B .4ualyte detected in the associated Method Blank I Analyte detected below quantitatioa limits ND Not Detected R RPD outside accepted recovery limits 1.000 45.0 10 109 1.000 48.8 10 109 1.000 471 19 120 1-000 81.2 10 120 1.000 47.4 22 117 1.000 86A 34 116 E Value above quantitatiourange M Manual integration used to determine area response P Second column confirmation exceeds RL Reporting Detection Limit Page 14 of 32 H Holding times for preparation or anal) MC Value is belowMnimum Compound PL Pem,it Limit Original S Spike Recovery outside accepted reco { SUMMII Samr, r Gmirn,rrneninl Techn33ogles, h t. 33I0 IVin SY, , I(-xynhogn Fa!!s, Ohio a4223 A rMfyHOBl Labprefarle8 TIil: (330) 253,7211 FAX(330) 253409 IVebsire: hrtn:, rruerr.yeiiekrnnr QC SUMMARY REPORT W09: 20011551 13-Feb-27l Client: Synagro Project: BatchED: 41814 Sample ID: LCS-41814 SampType: LCS TestCode: SVOC-BNA_T Units: mg/L Prep Date: 21312020 RunNo: 108857 Client ID: LCSS BalchlD: 41814 TestNo: SW8270 SW3510C Analysis Date: 2/412020 SegNo: 2604888 Analyte Result PQL SPKvalue SPK Ref Val %REC LowLimit Hight-imit RPD Ref Val %RPD RPDLimit Qual 1,4-Dichlorobenzens 0.373 0A00 0.8000 0 46.6 36.4 130 2,4,5-Trichlorophenol 0,757 0.250 0.8000 0 94.7 31.7 132 2,4,6-Trichlorophenol 0727 0,250 0,8000 0 90-9 31-1 133 2,4-Dinitrotoluene 0.893 0.0500 0.8000 0 112 43.3 130 o-Cresol 0-584 0.250 0.8000 0 730 32.9 130 Cresols, Total ND 5.00 1.600 0 74-5 31-7 130 Hexachloro-1,3•buladiene 0.388 0.0200 0.8000 0 48.5 31-4 130 Hexachlorobenzene 0.688 0.0500 0.8000 0 86.0 43.1 130 Hexachloreelhane 0.335 0.100 0.8000 0 41.9 36.5 130 Nitrobenzene 0.540 0A00 0.8000 0 67.5 39-5 130 Penlachlorophanol 0.812 0.250 0.8000 0 102 34 130 Pyn'dine 0.269 0.250 0.8000 0 33.6 10 130 Surr: 2-5luorophenol 0.631 1.000 63.1 17.1 130 Surr: Phenol-d6 0.647 1,000 64.7 10 130 Surr: Nitrobenzene-d5 0.626 1.000 62.6 32.6 130 Surr: 2,4,6-Tribromophenol 1.01 1,000 101 4.43 130 Surr:2-Fluorobiphenyl 0.639 1.000 63.9 41-8 130 Surr: p-Terphenyl-d14 0.937 1.000 93.7 36.4 130 Qualifiers: B Annlyte detected in the associated Method Blank E Value above quantitation range H Holding times tot preparation oranalS ] Annlyte detected below quantitation limits M Manual Integration used todctcmiinc area response MC Value is below Minimum Compound ND Not Detected P Second column contimiation exceeds PL Pcnnit Limit Original R RPD outside accepted recovery limits RI, Reporting Detection Limit S Spike Recovery outside accepted reco Page 16 of 32 S umm'll .Srmmmil Inc. 3310 I rein S!. ftJ 01VIR0111.t[i/TALIWIM01.(:1f3.1111 CnJWWgorn/Ls,01dodd223 Malyllenl Lebereferfe- Trla (330) 253.8211 FAY, (330)753-4189 Wehshe. hap:/hvuvir.seflek.com QC SUMMARY REPORT W09: 20011551 13-Feb-20 Client: Synagro Project: BatchID: 41814 ample to: 20011447�001AMS SampType: MS TestCode: SVOC-BNA T Units: mg1L Prep Date: 213/2020 RunNo: 108857 lien 1D: Batch QC Batch ID: 41814 TestNo: SW8270 SW3510C Analysis Date: 21412020 SegNo: 2606452 ,nalyte Result POL SPK value SPK Ref Val %REC LowLimit HighLimil RPD Ref Val ° RPD RPDLimit Qual 1,4-Dichlorobenzene 0.342 0.200 0.8000 0 42.7 33.8 126 2,4,5-Trichlorophenol 0.782 0.500 0.8000 0 97.8 28.7 144 2,4,6-Trichlorophenol 0.850 0.500 0-8000 0 106 12.8 153 2,4-Dinitrotoluene 0.729 0A00 0.8000 0 91A 20.4 155 0-Cresol 0.666 0.500 0,8000 0 83.2 10 148 Cresols, Total ND 10.0 1,600 0 85.8 10 148 Hexachloro-1,3-butadiene 0.368 0.0400 0,8000 0 46.0 29 126 Hexachlorobenzene 0.679 0.100 0.8000 0 84.9 33.7 134 Hexachloroethane 0-323 0.200 0.8000 0 40.4 32.8 132 Nilrobenzene 0-562 0.200 0.8000 0 702 20 158 Pentachlorophenol 0-937 0.500 0.8000 0 117 10 176 Pyridine ND 0500 0.8000 0 44.3 10 130 Surr:2-Fluorophenol 0 1,000 0 3.39 130 Surr: Phenol-d6 0.732 1.000 73.2 5 130 Surr: Nitrobenzene-d5 0-648 1.000 64.8 14-5 154 Surr. 2,4.6-Tribromophenol 0.998 1.000 99.8 19-5 130 Surr:2-Fluorobiphenyl 0313 1,000 71.3 34.4 130 Surr: p-Terphenyl-d14 0.901 1.000 90.1 8-86 156 Qunliriers: R Analytedetected inthe associated Method Blank 3 Analyte detected below quantitalion l imits ND Not Detected R RPD outside accepted recovery limits E Value above quantitaii on range M Manual Integration used to dctennine area response P Second column confirmation exceeds RL Reporting Detection Limit Page 16 of 32 In Sd H Holding times for preparation or anall MC Value is below Minimum Compound PL Pennit Limit Original S Spike Recovery outside accepted reco SUMMIT-s,,,r nE,rr;,,urneunlTeelnw310JrinSi. QC SUMMARY REPORT 3310 IYin.Sl. UAIIIIONMEWAL TECIMM-0( r., INC (7nyahognNnHs. Ohio 44223 Anfll yth al Labotalorim ML: (330) 253,1211 FfUi (330) 253-1489 WOk: 20011551 IVehsile: 1rlrn:/.5rmrr.reruerxrr 13-Feh-20 Client: Synagro Project: BatchED: 4I814 ;ample ID: 20011447.001AMSD SampType: MSD TeslCode: SVOC-i3NA_T Units: mg1L Prep Dale: 21312020 Run No: 108857 :lien( ID: 6atchQC Balch ID: 41814 TestNo: SW8270 SW3510C Analysis Dale: 21412020 SegNo: 2606453 malyle Result PQL SPK Value SPK RefVal %REC Low17mi1 HighLimil RPD Ref Val %RPD RPDLimil Qual 1,4-Dichlorobenzene 0.302 0.200 0.8000 0 37.8 33.8 126 0.3416 12.2 30 2,4,5-Ti'ichlorophenol 0.715 0,500 0.8000 0 89,4 28.7 144 0,7820 8.98 30 2,4,6-Trichlorophenol 0.804 0.500 0.8000 0 101 12.8 153 0.8504 5,56 30 2,4-Diniltololuene 0.729 0100 0.8000 0 91.2 20.4 155 0.7288 0.0549 30 o-Cresol 0,641 0.500 0.8000 0 80.2 10 148 0.6656 3.73 30 Cresols, Total ND 10.0 1-600 0 81.5 10 148 0 0 30 Hexachloro-1,3-buladiene 0.360 0.0400 0.8000 0 45.0 29 126 0.3680 2.20 30 Hexachlorobenzene 0.632 0,100 0.8000 0 79.0 33.7 134 0.6792 7.20 30 Hexachloroelhane 0,274 0.200 0.8000 0 34.3 32.8 132 03228 16.4 30 Nitrobenzene 0.539 0,200 0,8000 0 67.4 20 158 0.5620 4.22 30 Penlachlorophenol 0.909 0,500 08000 0 114 10 176 0.9372 3.03 30 Pyridine ND 0,500 0.8000 0 44.8 10 130 0 0 30 In Sure 2-Ruorophenol 0 1 000 0 3,39 130 0 Sd Surr Phenol-c16 0,667 1.000 66.7 10 130 0 Surr:: Nitrobenzene.c15 0.632 1.000 63.2 14.5 154 0 Surr. 2,4,6-Tribromophenol 0.957 1.000 95.7 19.5 130 0 Surr.2-Fluorobiphenyl 0700 1.000 70.0 34.4 130 0 Surr: p-Terphenyl-d14 0.847 1.000 843 8-86 156 0 Qunlirierst B Analyte detected in the associated Method Blank E Value above quanlitation range H Holding times for preparation or anal} J Analyte detected below quanti tationrunits M Manual Integration usediodeiemrine area response MC Value is below Minimum Compound Original ND Not Detected P Second column confirmation exceeds PL PemritLimit R RPD outside accepted recovery limits RI. Reporting Detection Limit S Spike Recovery outside accepted rcco Page 17 of 32 Srnuuth h'nPirumnewal Achuologies, Ijk. SUMMIT. 3310IrwSt. QC SUMMARY REPORT ENVIRON AN TAL IU1,nN01 amr. r, Mr. CupnhogrPnlJc 01do 44223 AnnfyflrnJ / nbaretari�� y✓OH: 20011551 77s•L: 030) 253,1211 FA,\: (330) 253.4489 IVebs&,: G!!n:/ iru•u seUak.eoui 13.Feh-20 Client: Synagro Project: BatchED: 41818 Sample ID: MB-41818 SampType: MBLK TestCode: HG TCLP(74 Units: PPM Prep Date: 214/2020 RunNo: 108886 Client ID: PBS Batch 10: 41818 TeslNo: SW7470A SW7470A Analysis Date: 214/2020 SegNo: 2603657 Analyte Result PQL SPK value SPK Ref Val %REC Lawl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury ND 0,00200 Sample ID: LCS-41818 SampType: LCS TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/412020 RunNo: 108886 Client ID: LCSS Batch ID: 41818 TestNo: SW7470A SW7470A Analysis Date: 21412020 SegNo: 2603658 Analyte Resuit PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00402 0.00200 0.00400 0 101 80 120 Sample ID: 20011609.001AMS SampType: MS TestCode: HG_TCLPJ74 Units: PPM Prep Date: 214/2020 RunNo: 108886 ClientlD: BalchQC Balch ID: 41818 TestNo: SW7470A SW7470A Analysis Dale: 214/2020 SegNo: 2603668 Analyle Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury 0.00424 0.00200 000400 0 106 75 125 Sample ID: 20011609.001AMSD SampType: MSD TestCode: HG_TCLP(74 Units: PPM Prep Date: 2/412020 RunNo: 108886 Client ID: BalchQC Batch 10: 41818 TestNo: SW7470A SW7470A Analysis Date: 2/412020 SegNo: 2603669 Analyte Result PQL SPKvalue SPKRefVal %REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Qual TCLP Mercury 0-00436 0.00200 0.00400 0 109 75 125 0,00424 2.79 20 Qualifiers: li Analytedeiected in the associated Method Blank E Vaiue above quantitation range H holding times for preparation or anal) 1 Analyte detected below quantitation limits M Manual Integration used todetemiine area response MC Vaiue isbelow Minimum Compound Original IVD Not Detected P Second column confirmation exceeds Pl. Permit Limit R RPD outside accepted recovery limits ILL Repotting Detection Limit S Spikc Recovery outside accepted reco Page 18 of 32 S V M1� ' nirEn, I,urnror Trcrn3310 411st. QC SUMMARY REPORT 33ID SS';a S1. ENV11100 14TALTECIINOLOGW3,INC Clr}'nrwgnFull."Ohio44223 Annlytlenf Laborefanes TEL: (330) 253-8211 FAA. (330) 253-4489 WON: 20011551 IVeAs;le; h+rn:nv,eu..venek.roru 13-Feh-10 Client: Synagro Project: Batchl& 41818 Sample ID: 20011609.001AMSD SampType: MSD TestCode: HG_TCLPJ74 Units: PPM Prep Date: 21412020 RunNo: 108886 Client ID: BatchQC Batch ID: 41818 TestNo: SW7470A SW7470A Analysis Date: 214r2020 SegNo: 2603669 Analyle Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sampte ID: M62-41818 SampType: MBLK TestCode: HG_TCLP(74 Units: PPM Prep Date: 2)412020 RunNo: 108886 Client lD: PBS Batch ID: 41818 TestNo: SW7470A SW7470A Analysis Date: 21412020 SegNo: 2603670 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDL-unit Qual TCLP Mercury ND 0.00200 Sample 10: TCLP BLANK 2-3-20 SampType: MBLK TestCode: HG TCLP(74 Units: PPM Prep Date: 21412020 RunNo: 108886 Client ID: PBS Batch ID: 41818 TestNo: SW7470A SW7470A Analysis Date: 21412020 SegNo: 2603678 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual TCLP Mercury ND 0.00200 Qualifiers: B Analyte detected 1n the associated Method Blank 3 Analyte detected below quantitalion limits 1VD Not Detected R RPD outride accepted recovery limits E Value above quantilation range H Holding limes for preparation or anal) M Manual integration used todetermine area response MC Value is below Minimum Compound P Second column confirmation exceeds FL Permit LimitOriginal RL Reporh ng Detection Limit S Spike Recovery outside accepted reco Page 19 of 32 Swunth Enwro„r„rmal fMn„ kgles. Inc. QC SUMMARY REPORT u m m, � 3310 irurS1. BNvlt[OtiInENTAi tEf.7if10LO;;iFS, INC Grl+olx gn hb1Ls Ohio 44??3 Annfytioai Ln6olafoNes TEL (330) 253-8211 FAX (330) 253-I4B9 W09: 20011551 Illebsile: r77r.! r.vellr,(.con 13-Feb-20 Client: Synagro Project: Batchm: R108624 Sample ID: LCS-R108624 SampType: LCS TeslCode: pH_Oil(90450 Units: s.u.@20.9C Prep Date: RunNo: 108624 Client 10: LCSW Batch ID: R108624 TestNo: SW90450 Analysis Date: 1/29/2020 SegNo: 2592160 Analyte Result POL SPKvalue SPKRefVal %REC LcwUmit HighLimit RPDRefVal ° RPD RPDLimit Oual pH 7.0 7.0 0 999 90 110 Sample ID: CHECK 7 SampType: LCS TestCode: pH_Oil(9045D Units: s.u.@21.1C Prep Date: RunNo: 108624 Client 10: LCSW Batch ID: R108624 TeslNo: SW90450 Analysis Dale: 112912020 SegNo: 2592362 Analyte Result PQL SPKvalue SPKRefVal %REC LowLimit HighLimit RPD Ref Val ° RPD RPDLimit Oual pH 7.0 To 0 99.9 90 110 SampleID: CHECK 7 SampType: LCS TestCode: pH_Olf(9045D Units: s.u.@21.3C Prep Date: RunNo: 108624 Client 1D: LCSW BatchlD: R108624 TeslNe: SW90450 Analysis Dale: 1/29/2020 SegNo: 2594509 Analyte Result POL SPKvalue SPKRefVal %REC Lcwt-imit HighLimit RPDRefVal ° RPD RPDLimit Oual pH 7-0 7.0 0 100 90 110 Qualifiers: B Anatytedetected inthe associaledMethodBlank E Value above quanlitationrange li molding times for preparation or anal) 7 Analyte detected below quantitation limits M MaoualIntegration used todetemtinearea response MC Value is below MinimumCompotmd ND NotDelecled P Second column confionati on exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 20 of 32 SUMMIT- Tec,,n33111IsMSLQC SUMMARY REPORT 3310 lfri» SL, C,»Tnhnga,�irllr, 0111a 44223 Malylleal Lnbareforips TEL: (330) 233-8211Tff. 1330) 253-4489 WOk: 20011551 iyebsile: hrNI.,hu-reu%serlek.cn»r 13-F'eh_20 Client: Synagro Project: BatchlD: RI08624 ;ample SD: 20010820.001ADUP SampType: DUP TestCode: pH_NPW(450 Units: s.u.@20.2C Prep Date: RunNo: 108624 Ilient ID: BatchQC Batch ID: R108624 TestNo: SW90450 Analysis Date: 1/29/2020 SagNo: 2592172 lnalyte Result PQL SPK value SPK Rat Val %REC Lowl-imit Hight-imil RPD Ref Vat %RPD RPDLimit Qual pH 6,8 NOTES: pH is an EPA field recommended parameter. Per 40 CFR 136.3, hold time is 15 minutes from collection. Qunlificrs: B Analyte detected in the associated Method Blank 1 Analytedetected below quantitation limits ND Not Detected R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to detenninearea response P Second column confirmation exceeds RI. Reporting Detection Limit Page 21 of 32 6.8 0.3 5 H H Holding times for preparation or anal) MC Value is belmv Minimum Compound PL Permit Limit Original S Spike Recovery outside accepted rcco Summit &mwhaaorental Pech,tologles, hrc. S.UMM17- 3310INnSI. QC SUMMARY REPORT ENWITONM94TAI-TGGHNn4f11irr,.%, mC C'nyahogaFalls, Ohio 44223 An tlyflrel Lxhorataller' WOk: 20011551 ITL: (330) 233 Y2111 !,t': (330) 233-4489 Weh.We: hRn:/Mw u seDe k.c'anr 13-Feh-20 Client: Synagro Project: BatchED: R108839 Sample ID: LCS•R108839 SampType: LCS TestCode: Ignitabllity_S Units: mmisec Prep Date: RunNo: 108839 Client to: LCSS Batch ID: R108839 TestNo: SW1030 Analysis Date: 21312020 SegNo: 2601828 Analyte Result PQL SPKvalue SPK Ref Vat %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitabilily 8.29 7.240 0 115 70 130 Sample ID: 20010917-001ADUP SampType: DUP TestCode: Ignitability_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BatchQC Batch ID! R108839 TestNo: SW1030 Analysis Date: 2/312020 SegNo: 2601830 Analyte Result PQL SPKvalue SPKRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD RPDLimit Qual Igmtabilfty non-flammable 0 0 20 Sample ID: 20011093-001ADUP SampType: DUP TestCode: Ignitabillty_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BatchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 213/2020 SegNo: 2601832 Analyte Result PQL SPKvalue SPK Ref Vat %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability non-flammable 0 0 20 Sample ID: 20011093.002ADUP SampType: DUP TestCode: Ignitabllity_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BatchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 2/312020 SegNo: 2601834 Analyte Result PQL SPKvalue SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability non-flammable 0 0 20 Qualifiers: 8 Analyte detected in the associated Method Blank E Value above quantitatior range H Holding times for preparation or anal) J Analyte detected below quanti tation limits ND Not Detected M Manual Integration used to determine area response P Second column confirmation exceeds MC Pt. Value is below Minimum Compound Permit Limit Original R RPD outside accepted recovay limits RL Reporting Detection Limit S Spike Recovery outside accepted rem Page 22 of 32 s� �+* J'»»„»,iGai.�„me»larleetn310Win St QC SUMMARY REPORT 331 U {Vi» JY. ENVI1100,104TALTEGNHnLrlGtr;,lr,a Ca3ahogalitRa:Ohio 44223 Anm/Ptten/ Ltrbonsforl" TL•L (330) 233 4211 F/LY.. (.330) 233-4489 WON: 2001 I551 We/,site: .501facorn 13-Feh-20 Client: Synagro Project: 13atchED: R108839 Sample ID, 20011093-002ADUP SampType: DUP TestCode: tgnitablllty_S Units: mmisec Prep Date: Runblo: 108839 Client ID: BatchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 213/2020 SegNo: 2601834 Analyte Result PQL SPK value SPK Ret Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] Sample ID: 20011324-001ADUP SampType: DUP TestCode: Ignitability_S Units: mmisec Prep Date: Runblo: 108839 Client ID: BatchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 213/2020 SegNo: 2601836 Analyte Result PQL SPKvalue SPKRefVal O/oREC Lowl.imit Hight-imil RPDRefVal %RPD RPDLimit Qua] Ignitability non-flammable 0 0 20 Sample ID: 20011551-001ADUP SampType: DUP TestCode: tgnitability_S Units: mm/sec Prep Date: RunNo: 108839 Client ID: Sitar City WWTP Batch tD: R108839 TestNo: SW1030 Analysis Date: 2/3/2020 SegNo: 2601838 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitability non-flammable 0 0 20 Sample ID: 20011552-001ADUP SampType: DUP TestCode: Ignitability_S Units: mm/sec Prep Date: RunNo: 108839 Client ID: BatchQC Batch to: R106639 TestNo: SW1030 Analysis Date: 21312020 SegNo: 2601840 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref VaI %RPD RPDLimit Qual Ignitability non-flammable Qualifilers: B Analytc detected in the associated Method Blank 3 Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits 0 0 20 E Value above quantitation range It Holding times for preparation or anal3 M Manual Integration used to determine area response MC Value is below Minimum Compound P Second column confirmation exceeds PL Pemtit Limit RL Reporting Detection Limit S Spike Recovety outsideaccepted mco Page 23 of 32 Original SUMMIffSfunnri! Gwiromuenlal 3310 Teclmahrc. lU Iv8'ins7. ENYInUNM8H1'AL ti?CII1rfILQGif ;. trrr. C.r(tnhoxa l cells. Ohio 44223 AnafyAtal Lnbarnto^Ire TEL: (330) 2534211T U17. (330) 253-4489 1VeDsile. lrrin:IA"e tnr.serlek.cnor QC SUMMARY REPORT WOk: 20011551 13-Feh-20 Client: Synagro Project: BatchlD: R108839 Sample ID: 20011553-001ADUP SampType: DUP TestCode: Ignilabilily_S Units: mm/sec Prep Date: RunNo: 108839 Client ID: BaIchQC Batch ID: R108839 TestNo: SW1030 Analysis Dale: 213/2020 SegNo: 2601842 Analyle Result PQL SPKvalue SPK Ref Val %REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Qual Ignitability non-flammable 0 0 20 Sample ID: 20011412.001ADUP SampType: DUP TeslCode: Ignilabllity_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BaIchQC Balch ID: R108839 TestNo: SW1030 Analysis Date: 2/3/2020 SegNo: 2601844 Analyte Result PQL SPKvalue SPKRefVal %REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Qual Ignitability non flammable 0 0 20 Sample ID: 20011412.001ATRIP SampType: DUP TestCode: Ignitabillty_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BaIchQC BatchlD: R108839 TestNo: SW1030 Analysis Date: 213/2020 SegNo: 2601845 Analyte Result PQL SPKvalue SPKRefVal %REC LowUmit HighLimit RPDRefVal %RPD RPDLimit Qual Ignitability non flammable 0 0 20 Sample ID: 20011412.002ADUP SampType: DUP TestCode:Ignitabillty_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BaIchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 21312020 SegNo: 2601847 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Ignitabilily 0.450 0.4100 9.30 20 Qualiliers: B Analyte devetedinthe associated Method Blank E Value abovcquantitation range H Holding times for preparation or anal) I Analyte detected below quantitation limits M Manual Integration used to detemiine area response MC Value is below Minimum Compound ND Not Detected P Second column eonlimiation"ceeds PL permit Limit Original R RPD outside accepted recovery limits RL Repotting Detection Limit S Spike Recovery outside accepted reco Page 24 of 32 czm"SUMMIT Summitldmirnrrnmrrinl Technologies, Inc. 3310 na v.. ENVISQNI.11INTAl-MIiNOILDOWS,M CrytrhnbmF'alls,01rioda123 Me}yflral Lnbararerlec TEL: (330) 253.8211 FAX: (330) 253-4489 Nehi He: lelln:/lxnnr..cerlek.com QC SUMMARY REPORT WOO: 20011551 FJ_Feb-20 Client: Synagro Project: RatchlD: R108839 Sample ID: 20011412-002ADUP SampType: DUP TestCode: lgnitability_S Units: mm/sec Prep Date: RunNo: 108839 Client ID: BatchQC Batch 10: R108839 TestNo: SW1030 Analysis Date: 21312020 SegNo: 2601847 Analyte Result PUL SPKvalue SPKRefVal °/aREC Lowl.imit HighLimit RPD Ref Val %RPD RPOLimit Qua[ Sample ID: 20011412-002ATRIP SampType: DUP TestCode: Ignilablllty_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BatchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 213/2020 SegNo: 2601848 Analyte Result PUL SPKvalue SPKRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimil Uual Ignitability 0.430 0.4100 4.76 20 Sample ID: 20011412.003ADUP SampType: DUP TestCode: Ignitabllity_S Units: mmisec Prep Date: RunNo: 108839 ClientlD: BatchQC BatchlM R108839 TeslNo: SW1030 Analysis Date: 213/2020 SegNo: 2601850 Analyte Result PUL SPKvalue SPKRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimil Uual Ignitability non-flammable 0 0 20 Sample ID: 20011412.004ADUP SampType: DUP TestCode: Ignitabllky_S Units: mmisec Prep Date: RunNo: 108839 Client ID: BatchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 213/2020 SegNo: 2601852 Analyte Result PUL SPKvalue SPKRefVal %REC Lowlimit HighLimit RPDRefVal %RPD RPDLimil Uual Ignitability non-flammable 0 0 20 ....-.+-_--•-------._..,--..-.---._..-.....-_ ..- ..--"----..--a•--.-'----------......... -----_�_.__ ..._._...---__................ ND Not Detected P Second column confirmat(on exceeds PL Pennit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S SpikeRecavery outside accepted reco Page 26 of 32 Summit EnWrnonterrtalTechanlogies.11ttt SUMMIT- iV 331001. QC SUMMARY REPORT ENVIIIBNhteNTALWMINfn6fIYS,IN(- Croynhogn7•hll. Ohm44223 Annly+lCnf LFlbnratarlr 7ZL: (330) 253 8211 GiIX: (330) 253-444I WOt+: 20011551 Website: rnek.cwtt 13-Feh-10 Client: Synagro Project: BatchID: R108839 Sample iD: 20011412-005ADUP SampType: DUP TestCode: Ignitabilily_S Units: mm/sec Prep Date: RunNo: 108839 lienl ID: BalchQC Batch ID: R108839 TestNo: SW1030 Analysis Date: 2/312020 SegNo: 2601854 4nalyte Result PoL SPK value SPK Ref Val %REC LowLimit Kght imit RPD Ref Val %RPD RPDLimit oust Ignitability non-flammable Qunlifiers: A Analytc detected in the associated Method Blank J Analyte detected below quantitation limits ND Not Detected R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area response P Second column conlinnadon exceeds RL Reporting Detection limit Page 26 of 32 0 0 20 11 Holding times for preparation or anal3 MC Value is below Minimum Compound PL Permit Limit S Spike Recovery atttside accepted reco Original summur .Summit Eurirnrma!ulal Teclrr3310 Wvi &. 3310 i{'dr 17. 0IOh'a 44223 Aonlylkn11nbareforlor TEL: (330) 253-8211 FAX (330) 2534489 Wchvile. hllo:/.irn'trsellek.rarn QC SUMMARY REPORT WOtk 20011551 13_Feb-20 Client: Synagro Project: BatchED: B109221 Sample ID: MB-R109221 SampType: MBLK TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 109221 Client ID: PBS Batch10: R109221 TestNo: SW9014 Analysis Date: 216/2020 SegNo: 2620714 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight.imil RPD Ref Val %RPD RPDLimit Dual Cyanide, Reactive NO 10.7 Sample ID: LCS-R109221 SampType: LCS TestCode: Cyanlde,Rea Units: mg/Kg Prep Date: RunNo: 109221 Client ID: LCSS Batch I0: R109221 TestNo: SW9014 Analysis Date: 2/6/2020 SegNo: 2620715 Analyte Result PQL SPK value SPK RefVal %REC Lowlimil HighLimit RPD Ref Val %RPD RPDLimit Qual Cyanide, Reactive NO 12.5 10.00 0 96.9 85 110 Sample ID: RLC-R109221 SampType: RLC TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 109221 Client ID: BatchQC Batch ID: R109221 TestNo: SW9014 Analysis Date: 2/612020 SegNo: 2620717 Analyte Result PQL SPK value SPK RefVal %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Dual Cyanide, Reactive NO 12.1 05000 0 125 50 150 Sample ID: 20011287-OOBAMS SampType: MS TestCode: Cyanide,Rea Units: mg/Kg Prep Date: RunNo: 109221 Client ID: BatchQC Batch 10: R109221 TestNo: SW9014 Analysis Date: 216/2020 SegNo: 2620724 Analyle Result PQL SPKvalue SPKRefVal %REC LowLimit HighLimit RPDRefVal %RPD RPDLimit Dual le, Reactive NO 12.1 10,00 0 95.3 81.6 122 Qualifiiers: B Analyte detected in the associated Method Blank E Value above quantitati on range H Holding times for preparation or anall J Anal ytedetected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound NO Not Detected P Second column cordirmati on exceeds PL Original Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 27 of 32 -� � �, � Srrnmdl f�3rrrcnnr.rrenlnl Technologies. Inc. 3310 IViu St. ENVI110M.1 4TAL trCIM01.01.1., trtc Cuyahoga Falls, Ohio 44223 Anntyllent tnbonnfaHrf TEL: (330) 253-8211 FAY, (330) 253-4489 1f'ehcile: hllec �irarm..eellekram QC SUMMARY REPORT W09: 20011551 13-Feb-20 Client: Synagro Project: 111tchlD: R109221 Sample ID: 20011287.008AMS SampType: MS TeslCode: Cyanide,Rea Units: mglKg Prep Date: RunNo: 109221 Client ID: BatchQC Batch ID: R109221 Tes1No: SW9014 Analysis Dale: 216/2020 SegNo: 2620724 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highlimit RPD Ref Val %RPD RPDLimit Qua] Sample ID: 20011287-008AMSD SampType: MSD TestCode: Cyanlde,Rea Units: mglKg Prep Date: RunNo: 109221 Client ID: BalchQC Batch ID: R109221 TestNo: SW9014 Analysis Date: 21612020 SegNo: 2620725 Ana(yte Result PQL SPK value SPK Ref Val %REC Lowl imit Highlimit RPD Ref Va( %RPD RPDLimil Qual Cyanide, Reactive ND 12.1 10.00 0 96.2 81.6 122 0 0 5 Qualifiierc 8 Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anall I Analyte detected below quantitation limits M Manual lntebaaton used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column co�mcati.on exceeds Pi. Pennit Limit Original R RPD outside accepted recovery limits RL Repotting Detection Limit S Spike B.ccovery outside accepted rem Page 28 of 32 5uM10111 SuuurNrlrwlrnsurrntnlTecblrologier/rrc. E3310 IVb R.. BNVI8Ur0aYNTALTftTiroot.UAIG7,iNC CutwhogaFW4 ON,, 44223 Art,tfyfleal Laboreforlep TEI.: (330) 253.82111 €X: (330) 253-4189 IlreOsih^ blro:/iu�rnr.xelrck-error QC SUMMARY REPORT Wolff: 20011551 13-Feb-2f! Client: Synagro Project: BatchlD: R109223 Sample ID: 20011287.008AMS SampType: MS TestCcde: Suffide,React Units: mg/Kg Prep Date: Run No: 109223 Client ID: BatchQC Batch ID: R109223 TestNo: SW9034 Analysis Date: 211612020 SegNo: 2620766 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD RefVal %RPD RPDLimit Quai Sulfide, Reactive 4580 25.0 4800 0 95.4 80 120 H Sample ID: 20011287-008AMSD SampType: MSD TestCode: Sulfide,React Units: mg/Kg Prep Date: RunNo: 109223 Client ID: BatchQC Balch 10: R109223 TestNo: SW9034 Analysis Date: 211612020 SegNo: 2620767 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive 4540 25.0 4800 0 94.6 80 120 4580 0.877 30 H Qunlifilers: 8 Analyte detected in the associated Method Blank L Vaiuc above quantitation range H Holding times for preparation or anal) 3 Analyte detected below quantitation limits M Manual Integration used to determine area response MC value is bdmv Minimum Compound ND Not Detected P Second column confirmation exceeds Pl. Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco Page 29 of 32 S V MMI't Srunuril Lm7mmnerrtnl TerAno310W, iu Sf. irm. 33101YQC SUMMARY REPORT ffIENblllUNMLNiAi tecMxataCrT-3, INCCn3nlragn Fn1G; Olrio 44223 WOtt: 20011551 Annly0cal Loborednrlps TFJ,- (330) 253-8211 FiLY. (330) 253-4489 Webslle: hNn:. •Irmsellek.cmn 13-Pe&20 Client: Synagro Project: liatclill): R109223 Sample ID: MB-R109223 SampType: MBLK TestCode: Sulfide,React Units: mg1L Prep Date: RunNo: 109223 Client ID: PBW Match ID: R109223 Tes1No- SW9034 Analysis Date: 2116/2020 SegNo: 2620758 Analyte Result POL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Sulfide, Reactive ND 25.0 Sample ID: LCS-R109223 SampType: LCS TestCede: Sulfide,Reac1 Units- rngJL Prep pate: RunNo: 109223 Client ID: LCSW Match ID: R109223 TestNo: SW9034 Analysis Date- 211612020 SegNo: 2620759 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val ° RPD RPDLimit Qual Sulfide, Reactive 4560 25-0 4800 0 95.0 85 115 Qualifiers: 11 Analyte detected in the associated Method Blank E Value above quantitation range H I lolding times for preparation or anal? 1 Analyte detected belocvquantitation limits M Manual Lttcgration used to determine area response MC Value is below Minimum Compound ND Not Detected P Second column continuation exceeds Pt, Permit Limit Original R JLPD outside accepted recovery limits RL ReponingDetection limit S Spikettecovezy outside accepted reco Page 30 of 32 SaO��f�� S�G[�fySa� f� uOultguo7 3o iagtunH aAljHAddBdJ� �a14N aul�R=Ma'+IV�V `aBPnIS�'iS 00-0 'PMbjj-1 'PIIoS-q -.Yljleku i�isadwo� 1 G C--p k z d]] d J i/) '" v 0 u c� E m r age 31 of 32 SUMMIT Summit Environmental Technologies, Inc. 3310 Win Sr. ENVIIT0fll 0J1`AL TCL`NN01,11CIES. Mr Cuyahoga Falls, Ohio 44223 Sample Log -in Check List AnolVNcal Lalioratbrhs TEL: (330) 253-8211 1,A : (330) 253-4469 01ebsite: hum,iinviv.sellek.com Client Name: SYN-NC-27028 Work Order Number: 20011551 RcptNo: 1 Logged by: John A.Semenik Completed By: John A.Semenik Reviewed By: Jennifer Woolf 1/24/2020 10:20:00 AM 1/24/2020 3:16:26 PM 1/31/2020 3:26:00 PM Chain of CustodU 1. Is Chain of Custody complete? Yes ❑ No ❑ Not Present ❑ 2, How was the sample delivered? UPS Log In 3, Coolers are present? Yes ❑ No ❑ NA ❑ 4, Shipping container/cooler in good condition? Yes ❑ No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present❑ No. Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes d❑ No ❑ NA ❑ 6. Were all samples received at a temperature of >0° C to 6.0°C Yes d❑ No ❑ NA ❑ 7. Sample(s) in proper container(s)? Yes d❑ No ❑ 8. Sufficient sample volume for indicated test(s)? Yes d❑ No ❑ g, Are samples (except VOA and ONG) properly preserved? Yes d❑ No ❑ 10. Was preservative added to bottles? Yes ❑ No d❑ NA ❑ 11, Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials❑ 12, Were any sample containers received broken? Yes ❑ No d❑ 13, Does paperwork match bottle labels? Yes d❑ No ❑ (Note discrepancies on chain of custody) 14, Are matrices correctly identified on Chain of Custody? Yes No ❑ 15. Is it clear what analyses were requested? Yes ❑ No ❑ 16, Were all holding times able to be met? Yes ❑ No ❑ (If no, notify customer for authorization.) Special Handling (if applicable) 17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA d❑ Person Notified: Date: By Whom: Via: ❑ eMaii ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 18. Additional remarks: Cooler Information Not Pre: Seal No Page 32 of 32 Waypoint.. ANALYTICAL 4/15/2020 Synagro Central LLC/ Siler City Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 20-097-0001 Project Description: Siler City 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 4/6/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method, Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method, Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated, This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, PM• or 607- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratoty's option, repeating the analysis in question at laboratoty's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 Waypoint-(D ANALYTICAL Report Number: 20-097-0001 Client Project Description: Siler City 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 SM-4S00-NH3C WP MTN 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 9045D WP MTN 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 4500NO3F-2011 WP MTN 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 6010D WP MTN 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 SW-7471B WP MTN 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 SM-4500-NH3C-TKN WP MTN 70952 Siler City Solids 04/02/2020 10:05 04/06/2020 SM-2540G WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 6 0 Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46490 Synagro Central LLC/ Siler City Ryan Copeland Mary Brewer Project Slier City Report Date 04/1S/2020 284 Boger Road Information Received : 04/06/2020 Mocksville , NC 27028 Submitted By : Ryan Copeland Report Number : 20-097-0001 REPORTOF ANALYSIS Agronomist mistMcGiy Agronomist Lab No : 70952 Matrix: Solids Sample ID : Siler City Sampled: 4/2/2020 10:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 97.3 % 0.010 1 04/07/201615 ADM SM-2S40G Test Results Units MQL DF Date / Time By Analytical Analyzed Method Ammonia Nitrogen 5960 mg/Kg - dry 3700 1 04/1S/20 14:00 JPJ SM-4S00-NH3C Nitrate +Nitrite-N 1490 mg/Kg - diy 178 1 04/13/20 14:01 ZBD 4SOONO3F-2011 Organic N 60400 mg/Kg - dry 9260 1 04/13/20 14:00 CALCULATION pH 6.4 S.U. 1 04/13/20 OS;39 JSL 904SD Total Solids 2.66 % 0.010 1 04/07/20 HAS ADM SM-2S40G Total Kjeldahl Nitrogen 66300 mg/Kg - dry 9260 1 04/13/20 14:00 JPJ oM-4S00-NH3C-TKlN Phosphorus 17500 mg/Kg - diy 18S 1 04/08/20 20:46 TJS 6010D Aluminum 51500 mg/Kg - dry 18S 1 04/08/20 20:46 TJS 6010D Arsenic <18.5 mg/Kg - dry 18.5 1 04/08/20 20:46 TJS 6010D Calcium 11300 mg/Kg - diy 926 1 04/08/20 20:46 TJS 6010D Cadmium <3,70 mg/Kg - dry 3.70 1 04/08/20 20:46 TJS 6010D Chromium 16.3 mg/Kg - dry 9,26 1 04/08/20 20:46 TJS 6010D Copper 270 mg/Kg - diy 9.26 1 04/08/20 20:46 TJS 6010D Iron 34000 mg/Kg - dry 18S 1 04/08/20 20:46 TJS 6010D Lead <11.1 mg/Kg - dry 11.1 1 04/08/20 20:46 TJS 6010D Magnesium 1570 mg/Kg - dry 18S 1 04/08/20 20:46 TJS 6010D Manganese 1050 mg/Kg - dry 18.5 1 04/08/20 20:46 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 6 Waypointo ANALYTICAL 46490 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Synagro Central LLC/ Siler City Ryan Copeland Mary Brewer Project Siler City Report Date : 04/15/2020 284 Boger Road Information : Received : 04/06/2020 Mocksville , NC 27028 Submitted By ; Ryan Copeland Pauric McGroary Report Number :20-097-0001 REPORTOFANALYSIS Agronomist Lab No : 70952 Matrix: Solids Sample ID : Slier City Sampled: 4/2/2020 10:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury <0.548 mg/Kg - dry 0.548 1 04/08/20 11:45 DDB SW-7471B Molybdenum <9.26 mg/Kg - dry 9.26 1 04/08/20 20:46 TJS 6010D Nickel 21.3 mg/Kg - dry 9.26 t 04/08/20 20:46 TJS 6010D Potassium 3460 mg/Kg - dry 185 1 04/08/20 20:46 TJS 6010D Selenium <18.5 mg/Kg - dry 18.5 1 04/08/20 20:46 TJS 6010D Sodium 4960 mg/Kg - dry 926 1 04/08/20 20:46 TJS 6010D Zinc 485 mg/Kg - dry 46.3 1 04/08/20 20:46 TJS 6010D Sulfur 6040 mg/Kg - dry 185 1 04/08/20 20:46 TJS 6010D Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 6 (D WayplRint 7621 Whltepine Road, Richmond, VA23237 Main 804-743-9401 ° Fax 804-271-6446 AYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 46490 Customer Name: Synagro Central LLC/ Siler City Report Number: 20-097-0001 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other: is UPS 0 Client 0 Courier Thermometer ID: Shipping container/cooler uncompromised? I* Yes 0 No Number of coolers/boxes received IT-1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Yes 0 No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions Included? 0 Yes No Comments: — Signature: 113randi Watson Date & Time: 04/0612020 10:29:38 Page 5 of 6 SAMPLING LOG # PROJECT MANAGER: - Phone: ( 336 ) 60 ` " �N Svnaaro Central LLC: Sifer ON Siler city 20-097-0001 Aso CHAIN OF CUSTODY 04062020 10:27:20 RECORD & ANALYSIS RECORD i attest mat me proper field sampling procedures were used daring fFre caif1wdon of (hose samples y� CQPWWVD A do L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAB # SA19PLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED Relinquished by Sampler. Date Time Redeved by: REMARKS: Rft COPIELA00 045 Relinquished by: Time Re leved by: W-5 Relinquished by. Time M SPECIAL INSTRUCTIONS: -r"" PO#: J 0� For ' " C., monitoring purposes, ESIAl SAMPLE ANALYSIS REQUEST l'D' SL1 SL2 I NHS! NO,N IJr�anl Cd + CP NI Pb As Hg I Se pH C.8� �� Mo Cl NOQ-N SL1: Total Solids (Molst n), Total l9eldahl Nitrogen, Phosphorus, and Potawfurn SL2: Basic Test SLi plus Sulfur, Calcium, Magnesium, Sodium, Iron, Alurninum, Manganese, Copper and Zinc T Ns, 0 ro Contact: Ryan Copeland Client: Synagro 284 Boger Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Report Date: 4/14/2020 Project: Siler City Date Sample Rcvd: 4/3/2020 Meritech Work Order # 04032031 Sample: Siler City 1 Grab 4/3/20 Parameters Results Analysis Date Reporting Limit Method % Total Solids 1.65 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 6,061 col/gdrywt 4/3/20 130 col/g dry wt SM 9222D Meritech Work Order # 04032032 Sample: Siler City 2 Grab 4/3/20 Parameters Results Analysis Date Reporting Limit Method %Total Solids 2.04 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 8,467 col/g dry wt 4/3/20 130 col/g dry wt SM 9222D Meritech Work Order # 04032033 Sample: Siler City 3 Grab 4/3/20 Parameters Results Analysis Date ReportingRpporting Limit Method % Total Solids 2.25 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 6,869 col/gdry wt 4/3/20 130 col/gdrywt SM 9222D Meritech Work Order # 04032034 Sample: Siler City 4 Grab 4/3/20 Parameters Results Analysis Date Rep-o Method % Total Solids 3.25 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 4,755 col/g drywt 4/3/20 130 col/g dry wt SM 9222D Meritech Work Order # 04032035 Sample: Siler City 5 Grab 4/3/20 Parameters Results Analysis Date Reporting Limit Method % Total Solids 3.30 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 6,061 col/gdrywt 4/3/20 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 LIN"41 Contact: Ryan Copeland Client: Synagro 284 Boger Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 2 Report Date: 4/14/2020 Project: Siler City Date Sample Rcvd: 4/3/2020 Meritech Work Order # 04032036 Sample: Siler City 6 Grab 4/3/20 Parameters Results Analysis Date RW. orting Limit Method %Total Solids 3.26 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 5,020 col/gdry wt 4/3/20 130 col/g drywt SM 9222D Meritech Work Order # 04032037 Sample: Siler City 7 Grab 4/3/20 Parameters Results Analysis Date Reporting Limit Method %Total Solids 3.26 % 4/7/20 0-100 % SM 2540B Fecal Coliform (Sludge) 6,414 col/g dry wt 4/3/20 130 col/g drywt SM 9222D 1 hereby certify that (have reviewed and approve these data. "Mk U-k-' Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 5-9-201b Chain of Custody Record (COC) _ NPDES#: Client: 57��f�-Phone: � dv� AddFax: L� �ck5vi�-�- IJC- Email: �C'-PcuwCc SV'tp7z'o [ oM Project: 1L&L C,y pp P.O.#: Attention: (,Cc-,ANO Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply: mail preferred), Fax, Mail Std 10 s) 5�ai{s 24 � M E R ITECH, INC.� V' ENVIRONMENTAL LABORATORIES 642TamcoRd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechlabs.com Sample Location and/or 1 D # Sampling Dates & Times Person Taking Sample (Sign/Print): Nfo 0ceLAAnLab�Use Only � Start End Comp? Grab? # of Cont. Test (s) Required On Ice? s / No pH OK? CI OK? Date Time _ Date Time 3 3> F7 s r 3s F7.................. '-TT. ................ 7 37 I Temperature Upon Receipt: �r Method of Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.*** Shipment: Comments: Compositor # J UPS IJug# U /Fed Ex Are these results f or regulatory purposes? Yes No ❑ Report results in: mg/L ❑ mg/kg ❑ ug/L Ll Hand Delivery Relinquished by: 6� /' _ rc- Lq� Date: 1 /3/Zo Time: 13 ZU v (� 1 Received by: Date: Time: U Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Rec ' ed by Lab i �� ��lC Date: Time: 1 snerCity wastetreatmentPiantLab. SPECIFIC OXYGEN UPTAKE RATE (SOUR) Date Sample Taken .7y Analysis Done By 94 Time Taken ;::;2 ; 10 AM f Aerated from AM/PM to AM/PM By Whom 4314 Aeration Time — (Must be < 2 hrs.) Temperature When Taken 20 °C Analysis Start Time e9:-q0 Location of Sample : (Circle One) Digester A or D' ester B r road) NOTE: Temperature should be between 10°C and 30°C Aeration required if DO is < 5 % Total Solids Place 25 gms. to 50 gms. of sample for % total solids @ 30 mis. SAMPLE #1 Dish # mis. 3l� Wt. of Dish,g } . a t4 6 Q) Wt.of Wet sample +Dish,g _^3:3 .1J.` j Wt. of Dried Residue + Dish,g 72 r 3 S g U SAMPLE #2 Dish # mis. 3� Wt. ofDish,g /, 9 ,,�te15, Wt.of Wet sample+Dish,g Wt. of Dried Residue + Dish,g Placed in 103-105 degrees C oven @ _ I: - Taken out of oven @ Drying time hrs. min, Placed In dessicator & weighed . % TOTAL SOLIDS = Wt, of Dried residue + dish --Wt. of Dish . x 1000 (x 100 ) Wt. of Wet sample +dish,g. -Wt. of Dish,g. x 1000 Sample #1 %Total Solids= Sample #2 % Total Solids= R,:3.�VO-- 2,;?^ &511 - /.,s �..: 5 r3 � •— lr�� le � �� 4�'fcC •— 149�� 30r.001-1 3 ores i �IOCiJ )t� SilercityWastetreatmentPlant Lab. SPECIFIC OXYGEN UPTAKE RATE (SOUR) Date Sample Taken _ q- 2 - 2 0 Analysis Done By 84 Time Taken _ _ Q: oci A M ' Aerated from --- AM/PM to -- AMIPM By Whom i3if _ Aeration Time (Must he < 2 hrs.) Temperature When Taken ;2 i il °C Analysis Start Time ? : C 5- rM Location of Sample : (Circle One) ester ' r Digester B(near road) NOTE: Temperature should be between 10°C and 30°C Aeration required if DO is < 5 TEMP.°C TIME(min) <>=< DOReading(mpnl % Total Solids Start=20. 0 '7.5 Place 25 gms. to 50 gms. of sample 1 7.Y3 for % total solids @ 30 mis. 2 Le 3 SAMPLE #1 4 ] , j Dish # j 5 7. C 41 mis. 3y 6 Mid.=,r'O.di 7 Cr.�tJ Wt. ofDish,gi is $ .73 Wt.of Wet sample +Dish,g 31. y93 Wt. of Dried Residue + Dlsh,g• �d 10 11 ,14 SAMPLE #2 12 Dish # ;2 13 ZZ mis.� ...........14 . ; End= 7Q.' 15 i Wt, of Dlsh,g Wt.of Wet sample +Dish,g ._31, 5 e 13 _ Wt. of Dried Residue + Dlsh,g 7 Placed in 103-105 degrees C oven @ .; /0 Taken out of oven @ nrr-, Drying time F�Lhrs. D min. Placed in dessicator & weighed . (o TOTAL SOLIDS = Wt. of Dried residue + dish - Wt, of Dish . x 1000 ( x 100 ) Wt. of Wet sample +dish,g. -Wt. of Dish,g. x 1000 Sample #1 %Total Solids= 1 3! 1 ,31,q�5'�- 1,�.3iI Sample #2 % Total Solids= , - 5 0j :3 - �, s' '.j j d-.5- 71 Q'9" 4�y 1I9go sflerCity wastetreatmentPlant Leb. SPECIFIC OXYGEN UPTAKE RATE (SOUR) Date Sample Taken `f ? 7'V) Analysis Done By 3,14 Time Taken :'? :1�5- A Aerated from AM/PM to AM/PM By Whom Aeration Time (Must he < 2 hrs.) Temperature When Taken — °C _ Analysis Start Time Location of Sample ; (Circle One) Digester A or(ti ester B n> road) NOTE: Temperature should be between 10°C and 30°C Aeration required if DO is < 5 % Total Solids Place 25 gms. to 50 gms. of sample for % total solids @ 30 mis. SAMPLE #1 Dish # mis. 3G Wt. of Dish,g '. ; P, ' [1� _ Wt.of Wet sample +Dish,g 3,2. Wt. of Dried Residue+ Dish,g,J:� SAMPLE #2 Dish # mis. 30 Wt, of Dish,g 9- u q :!� Wt.of Wet sample +Dish,g 3�� f G :5 5 Wt. of Dn'ed Residue + Dish,9 Lo .11 f7 Placed in 103-105 degrees C oven @ Taken out of oven @ Drying time hrs.— Placed in dessicator & weighed . % TOTAL SOLIDS = Wt. of Dried residue + dish,g - Wt. of Dish,q. x 1000 x 100 ) Wt. of Wet sample +dish,g. -Wt. of Dish,g, x 1000 Sample #1 %Total Solids= Sample #2 % Total Solids= 193 -- 2. ���P 1 .3b,19g5- ?,C��?�O .�.a4z5 Y d57S5- /� = �` sflercitywastetreatment Piantl.ab. SPECIFIC OXYGEN UPTAKE RATE (SOUR) Date Sample Taken '"t"it.-.aD Analysis Done By Time Taken � . AM,-W Aerated from AMI o 'I -1, AMO!0 By Whom b- Aeration Time 6; 4-- (Must be < 2 hrs.) Temperature When Taken a1" _°C Analysis Start Time Location of Sample : (Circle One) cEigester r Digester B(near road) NOTE: Temperature should be between 10°C and 30°C Aeration required if DO is < 5 % Total Solids Place 25 gms. to 50 gms. of sample for % total solids @ 30 mis. SAMPLE #1 Dish # mis. '3 0 Wt. of Dish,g 1 .1 S 4 L) Wt.of Wet sample +Dish,g . '3 a : y t�� ,L' 3 '7 Wt. of Dried Residue + Dish,g 12. 7.3 k SAMPLE #2 Dish # mis. 2 10 Wt. of Dish,g / . $ J Wt.of Wet sample +Dish,g G 3 3 Wt. of Dried Residue + Dish,g _ 2,YL 6 b Placed in 103-105 degrees C oven @ '3"'4 Taken out of ove (— Drying timers. min. Placed in dessicator & weighed . Yo TOTAL SOLIDS = Wt. of Dried residue + dish,g- Wt. of Dish.q x 1000 (x 100 ) Wt. of Wet sample +dish,g. -Wt. of Dish,g. x 1000 Sample #1 %Total Solids= 36.611 9 Sample #2 % Total Solids= lkj 1. q 90 m*,City w�°�m��Plant Lab. SPECIFIC OXYGEN UPTAKE RATE '\ Date Sample Taken _ �� Ana�o�Done By ~�; Time Taken l AM&Aerated from '�T By Whom Aeration Time uutbe<2hro.) Temperature When Taken 20 CIC Analysis Start Time � Location ofSample : (Circle One) Digester omrroad) NOTE: Temperature should be bobmoon 1O,C and 30"C Aeration required if DO is < 5 96 Total Solids TEMP.00 TIME(min) Reading (rng�) Place 25gmo.ho5Ogmo.ofsample for 96 \nbe| solids @3O m|o. 3 SAMPLE#1 Dioh# m|o. Wt. o[nISn.9 Wt.of Wet nample+oish.0 Wt. n/Dried Residue +oish.g 2. 10 SAMPLE#2 �12 Dish # 13 MIS. 14 15 Wt. mDish u 7-777 �L rNw�num�e+0d`g w/,vrDried Residue +oinh.0 Placed in 103'105degr Taken out nf opn @ 'Zhm. Drying time 0min. Placed in deooicatnr&weighed . % TOTAL SOLIDS = Wt. of Dried residue + dish, Wt. of Dish,( � Sample #1 %T�o Sn�o 2��� '�- i^2~k» S '�66 q1 Sample hQ96Total SnUdo= 63.11 ,~"�� �� /°�_ -- `---~—�-- ^`°v � --------~'--^ /�^/^7 AV /~°/ '» SilerCllyWasletreatmentPlant Lab. SPECIFIC OXYGEN UPTAKE RATE (SOUR) Date Sample Taken tI ' Zq A'' Analysis Done By Time Taken i o .. 10 wpm Aerated from AM/PM to AM/PM By Whom 6!4�? Aeration Time — (Must be < 2 hrs.) Temperature When Taken 7,0 °C Analysis Start Time 10!114!}m Location of Sample : (Circle One) Digester A o k�oica ear road) NOTE: Temperature should be between 10' Aeration required if DO is < 5 % Total Solids Place 25 gms, to 50 gms. of sample for % total solids @ 30 mis. SAMPLE #1 Dish # 1 mis. _ .�t Wt. of Dlsh,g t. S x (a 7 Wt.of Wet sample +Dish,g .31 el 9 U Wt. of Dried Resldu e + Dish,g `Z .20:3 SAMPLE #2 Dish # .2, mis. '30 r" Wt. of Dish,g 1 c I q.13 Wt.of Wet sample +Dish,g .3i j r 64) 1 2� Wt. of Dried Residue + Dish,g a 316% 1 Placed in 103-105 degrees C oven @ 0 Ai►Z Taken out of oven @ y `,2G ?rA Drying time 4 hrs. 45 min. Placed in dessicator & weighed . % TOTAL SOLIDS = Wt. of Dried residue + dlsh,g - Wt. of Dish,g. x 1000 (x 100 ) Wt. of Wet sample +dish,g. -Wt. of Dish,g. x 1000 Sample #1 %Total Solids= 2' y Z a s +' g 2 (o S 31, eIclo1 - I . g %-_ D.6gW ---.4 (1 oov) 3o.1bIto Sample #2 % Total Solids-- -1W 29114`1 j1g1'`/0 AV ),91x Slier City Wastetreatment Plant Lob. SPECIFIC OXYGEN UPTAKE RATE (SOUR) Date Sample Taken 7 - I -7-0 Analysis Done By 6 Time Taken C? !� AM M Aarated from AM/PM to AM/PM By Whom 16.5Aeration Time -- (Must be < 2 hrs.) Temperature When Taken _ Iri °C Analysis Start Time GI : Hy Am Location of Sample : (Circle One) Digester A o Di ester B ear road) NOTE: Temperature should be between 10"C and 30°C Aeration required if DO is < 5 % Total Solids Place 25 gms. to 50 gms. of sample for % total solids @ 30 mis. SAMPLE #1 Dish # _ mis. 130 Wt. of Dish,g Wt.of Wet sample +Dish,g Wt. of Dried Residue + Dish,g -21 SAMPLE #2 Dish # mis. -30 Wt. of Dish,g I ' % Z(a Wt.of Wet sample +Dish,g 3 i , 5Z09 Wt. of Dried Residue + Dish,g .2,Y36 Cyr Placed In 103-105 degrees C oven @ _Jp : GyA01 Taken out of oven @ ly, 10 Pm Drying time .6—_hrs. /O min. Placed in desslcator & weighed . Xo TOTAL SOLIDS = Wt. of Dried residue + dishg - Wt. of Dish . x 1000 (x 100 ) Wt. of Wet sample +dish,g. -Wt. of Dish,g. x 1000 Sample #1 %Total Solids= Sample #2 % Total Solids- �i�S�v9- fr9ya � d, r �� G C� OT, 7ra q 7 5 ciao -vz f, N, c,,793 .I)*,,, .© V. State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checldist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one or•ieinal and two copies of the application and suoporting documentation For more inrormation, visit the Water Quality Permitting Section 'sNon-Dischar gY� aft;g Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted,the Applicant shall submit one original and two copies oftlre application and supportingdocuincntation listed below. A. Land Application Site Certification (FORM: LASC 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) fort". Please do not make any unauthorized content changes to this f orrn. If necessary for clarity or due to space restrictions, attachment s to the application may be rnade,a s long as the a tta chrnents are numbered to correspond to the section and itern to which they refer. ® For new or renewed pennits, submit therequcsted inf6rmationforall landapplication sites. ® For modified pennits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification, B. Land Application Site information: ® The status of the land application site with respect to this residuals land application program must be provided in table I. The status categories and their corresponding codes areas follows: ♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D) ® Attach the following in accordance with each status code: Status Code Required Item N R T M County Board Notifica tion. doc Land Owner Agreernent (If applicable) r_v,'- ✓ ✓ ✓ ✓ Setback Waiver Agreement An upda ted vicinity/setback ma p in a ccordance with the "Mao Guidance ✓ ✓ ✓ for Residuals Land Anylication_Permits" A soils and agronomic evaluation in accordance with the "Soil Scientist ✓ Evaluation Policy" INSTRUCTIONS FOR FORM: LASC 06-16 Page l of 3 updated accounting of the land application site's cumulative pollutant loadinAn rates CPLRs) Status Code Required Item N R T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly ✓ indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation Policy" Acknowledgement of field transfer from Land Owner (Fields may not ✓ be permitted to multiple Pcrmittccs over the same tune criod) This item may be required for land application site with a status code "NI", please contact the Division if you need assistant in determining; attachment requirements. ® Crop Type should include the most likely crop types for the life of the periit (five years). ® Predominant Soils Series Name must be either the name of the soil indicated in Attachment "B" of the existing pennit, or nameofthesoil series asprovidedbythe licensed soil scientist. ® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of cacti site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mappnrgunit. If a representative slope is provided, it must be determined accordingly: ® For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides infornation on both the soil series name a nd the slope of the soil), the Applicant may detenninc the represents tive slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have representative slope of 6%. ® New Sites to be permitted must havcslopes determined as pa►t of the soils report prepared bya licensed soil scientist. ® Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their cor,esponding codes are as follows: • Address Matching(ADD) • Aeria 1 Photography with Ground Control (AER) • Ca dastralSmvey(SUR) • Digital or Raw Photo Extraction (EXT) • Geodetic Quality GPS Survey (GEO) • LORAN-C Navigation Device (LOR) • Conversion from Coordinate Plane (CP) • Navigation Quality GPS (GPS) • Conversion fi-om Township -Section -Range (TSR) • Remote Sensing (RS) • Conversion from Universal Trans Merc (UTM) • Zip Code Centroid (ZIP) • Map Interpretation by Digita 1 or Manual Extraction (MAP) C. Waterbody and Classifications hrformation: (new sites only) ® Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, theidentificd location, and be of clear and reproducible qua ity. ® Surface water body classifications information may be found at: lrttp://deq.nc.p-ov/about/divisions/watcr- tesaurceslnlamnine/classification standards/classifications ® Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ® A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: htt :/n /deq,nc,gov/contact/re6onaj-offices ® General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodieswith assigned subba sins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 1 1-inch sheet showingthe project area should be submitted with the permit application regardless of whethera Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to sh•eam rrame" as the waterbody name. 3. Open the link httR:/Ideg.ne.g ov/about/divisions/water-resources/planninyJclassificat ion-standards/classifications. ® Stream Classification Process: One of the optionsbelow may be used depending on the known initial project information. ® KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically a s this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 2. Locate then a in e of the identified waterbody(from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The tenn "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classificationsapplicable to the project. ® KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county,hydrologically report. 2.Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same watcrbody name in the report, select and verify the location description. The terin "source" in the description means the beginning of the wa terbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ® UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clicka ble basin map to hydrologically soiled list report. 2. Click on the approximate project location to bring tip the hydrologically soiled list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the reporl, select and verify the location description. The teen "source" in the description means the beginning of the wa terbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ® Notes on index number and unnamed streams: Unnamed Streams 15ANCAC 0213.0301 i . N Any stream which is not named in the schedule of stream classifications canies the same classification as tha t assigned to the stream seginent to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaterstributary to tidalsaltwaters will be classified "C"; or (C) a fter November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" finless case -by -case reclassification proceedings are conducted. N The following river basins have different policies for unnamed streams entering other states or forspecific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassce River Basin Streams entering Georgia or Tennessee shall be classificd "C Tr." Little Tennesse River Basin And Savannah River Drainage Area Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified "B Tr." French Broad River Basin Streams entering Tennessee will be classified "B." Watauga River Basin Streams entering the Statcof Tennessee are classified "C." Broad River Basin Streams entering South Carolina arc classified "C." New River Basin Strca ms entering the State ofTennessee are classified "C." Catawba RiverBasin Streamsentering South Carolina arc classified "C." Yadkin -Pee Dee River Basin Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Roanoke River Basin Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River Basin All drainage canals not noted in the schedule are classified "C Sw." except the main drainage I canalstoPain licoSound and itsbayswhich shall be classified "SC." Pas uotankRiverBasin I All drainage canalsnotnoted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 LAND APPLICATION SITE CERTIFICATION Applicant's name: Synatrro Western Piedmont RLAP Land application sites currently certified: 813.6 net acres and Total to be certified: 377.6 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Code' Site/Field ID Landowners O Lessees or Operator(s) O Net Acres Count y Crop(s) s pO Predominant Soil Series Name y Mapping Unit or Rep. Slope, N RC-49-01 Ann Purgason 21.2 Rockingham Pasture Clifford CgB2 N RC-49-02 Bennett Farms LLC 10.7 Rockingham Row Crop Clifford CgB2 N RC-49-03 Bennett Farms LLC 7.4 Rockingham Hay Clifford CgB2 N RC-49-04 Bennett Farms LLC 10.7 Rockingham Hay Clifford CgB2 N RC-49-05 Bennett Farms LLC 8.7 Rockingham Row Crop Clifford CgB2 N RC-49-06 Bennett Farms LLC 5.8 Rockingham Hay Clifford CgB2 N HA-47-1 James W. Pope 19.2 Harnett Pasture Aycock AyA N HA-47-2 James W. Pope 9.9 Harnett Pasture Aycock AyA N HA-47-3 James W. Pope 11.0 Harnett Pasture Aycock AyB N HA-47-4 James W. Pope 4.3 Harnett Pasture Aycock AyB N CH-78-1 Bobby Branch 66.4 Chatham Pasture Cid-Lignum CmB N CH-78-2 Bobby Branch 40.7 Chatham Pasture Cid-Lignum CmB N CH-78-3 Bobby Branch 57.6 Chatham Pasture Cid-Lignum Cm.B N CH-78-5 Bobby Branch 65.5 Chatham Pasture Georgeville GeB2 N CH-73-10 Doug Ellis 38.5 Chatham Hay Georgeville GeB2 N N N N N Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) C Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) FORM: LASC 06-16 Page 1 LAND APPLICATION SITE CERTIFICATION H. WATCRBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed P Class RC-49-01 36° 17' 22" 79° 57' 26" NAD 83 ADD Nearest Second Little Hogans Creek, 22-3 1-1 C C RC-49-02 36° 17' 22.4" 79° 57' 67' NAD 83 ADD Nearest Second Little Hogans Creek, 22-3 1-1 C C RC-49-03 36° 17' 22.3" 790 56' 54.4" NAD 83 ADD Nearest Second Little Hogans Creek, 22-3 1-1 C C RC-49-04 360 17' 17.8" 790 56' 53.9" NAD 83 ADD Nearest Second Little Hogans Creek, 22-3 1-1 C C RC-49-05 360 17' 12.5" 7Q0 57' 6.2" NAD 83 ADD Nearest Second Little Hogans Creek, 22-3 1-1 C C RC-49-06 360 17' 23" 790 57' 12.7" NAD 83 ADD Nearest Second Little Holans Creek, 22-3 1-1 C C HA-47-1 350 34' 41" 780 74' 88" NAD 83 ADD Nearest Second Second Silver Run, 18-20-33-1 WS-Iv WS-Iv HA-47-2 350 20' 52" 780 44' 55" NAD 83 ADD Nearest Second Second Silver Run, 18-20-33-1 WS-Iv WS-Iv HA-47-3 350 34' 97" 78° 74' 70" NAD 83 ADD Nearest Second Cape Fear River, 18-(16.7) WS-Iv WS-Iv HA-47-4 350 35' 22" 780 74' 67" NAD 83 ADD Nearest Second Cape Fear River, 18-(16.7) WS-Iv WS-Iv CH-78-1 350 37' 13.5" 790 21' 46.7" NAD 83 ADD Nearest Second Sandy Branch, 17-43-16-1 C C CH-78-2 350 36' 53.3" 790 22' 21.7" NAD 83 ADD Nearest Second Sandy Branch, 17-43-16-1 C C CH-78-3 350 37' 11.9" 790 22' 7" NAD 83 ADD Nearest Second Sandy Branch, 17-43-16-1 C C CH-78-5 350 40' 27.9" 790 22' 18.4" NAD 83 ADD Nearest Second Tick Creek, 17-43-13 C C CH-73-10 350 40' 77" 790 27' 50.2" NAD 83 ADD Nearest Second Tick Creek, 17-43-13 C ° , " Note: Please keep the site information (I.) and waterbody information (II.) of the same field on the same page. FORM: LASC 06-16 Pacre 2 GRAPHIC SCALE 1" = 4,000` 4,000' 0 4,000' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. N C-RC-49 Fields 1-6 APPLICATION MAP LEGEND APPLICATION AREA UNSUITABLE AREA — —�— — — PRIVATE ROAD OW WATER STREAM ONSITE HOUSE GRAPHIC SCALE DRAIN OFFSITE HOUSE "_ FENCE OUTBUILDING 660' 0 660' PROPERTY LINE WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-RC`49 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area, All locations are approximate. Fields 1-6 1 l 5 l f TOPOGRAPHIC MAP GRAPHIC SCALE 1"=800' 800, 0 800, j 5 � 1I a i � J i f'— The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area, The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NO 04 Fields 1-6 SOIL SURVEY GRAPHIC SCALE 1" = 660` sso' 0 sso' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area, The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area, All locations are approximate. N C- RC-49 Fields 1-6 nWg State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a cliecklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will lielp produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for (lie permit application. Unless otherwise noted, the Applicant sliall submit one original and two copies of the application and supporting documentation FO;- lore inf))rmalion, visit the Water Qarctlily Permitting Section's Non-Dischmye Permitting Unit. General — This document is an agreement between (he Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T •1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA O6.16): Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. (�] Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. [� A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's came: !IMrkCV-o We�T icz hereinafter referred referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (Yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) e ToLs e- AjA Fe-eek The landowner or his representative receives, in consideration, Rill use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement sliall remain in effect for the length of the Division's permit for the residuals land application program and sliall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 1, STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2, Should the landowner or his representative lease or otherwise pernut the use of the land application sitc(s) to a third ptu•ty, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4, Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification firom the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application sitc(s). 6, The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pit of the land application sitc(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application sitc(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. II. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application sitc(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application sitc(s) for a 30-day period following a residuals land application event. Land application sites that tu'e to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be hauvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14- month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface f'or four months or longer prior to incorporation into the soil. 6. Food craps with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals arc applied shall not be harvested for a 12-month period following a residuals land application event. IILALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; AA re -defined compliance boundary is needed for field(s) 1D: T-C-46i - 1 (Please include the rationale for the requested re -location of the compliance bounday and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the ficld(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FOW: LOA 06- I6 Page 2 of 3 Landowners Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another Municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: ' !' A/ Al Address:: _ j5 '� �u -p(6 City: ZJ TEf ��5 CJtti4) '� State: rl% '� —Zip: 9,7-3.s Phone: 3 - Q),% 70 SKI ,p y7 E-mail address: Signature: _ �/ (l!y DaLc: —A 9 04w NORTH CAROLINA,l _ COUNTY I, the undersigned Notary Public do hereby certify that �in_Y Cif Sdy'1 personally appeared before Me this day and acknowledged the due rexecution of the forgoing instrument. WITNESS My hand and official seal this the �h day of �V'IWfh , 20 20 Signature and seal: ,WUfJ f ROBERT N. ROTH My commission expires: Del- NOTARY PUBLIC GUILFORD COUNTY STATE OF NORTH CAROLINA, Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name Address: City: Phone: Signature: Permittee's Certification: State: Zip: E-mail Date: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: T h� / /jv Y ,kQ-6� Signature: Date: d FORM: I.OA 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting( nit. General This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with , SA NCAC 02T . I IOU. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his repree1sentative hereby permits: Applicant's name: -Ur tr:�c�Yo (jCS ��L y e-J+nnn hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field W Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) -c-a�-2..� I r�� � roc, kv}Mid Fce-J- � -- 4 cl — 3 . if, G A/0 NAV I'A 1Mij Fa;� f The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page] of3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. f Landowner name: Address: / [ City: ! ! y�State: _ �� _ _ _ _ _ _ Zip: '7 5 _ Phone: Y3 E-mail address: e ►^ Y' H�' �-Cca?!01 Signature: tf/ Date:T/ NORTH CAROLINA, . tci„L� L, yCOUNTY I, the undersigned Notary Public do hereby certify that �' �161 CUtin (SJV JMVJ-� personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the co t h day of , 20 2 fJ Signature and seal: Kelly Dillon Noiary Public My commission expires: ' � am , Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: _ _ _ _ State: _ Phone: E-mail Signature: Permittee's Certification: Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: Signature: _ 'lop— 2� _ _ _ _ Date: — 6LZ (4 /ZQ FORM: LOA 06-16 Page 3 of 3 SOIL DESCRIPTION SFIE, ET SYNAGRO Project: %/i`'r� (� )I L�=��+'10i•Landowner: Site:kr _ Field: Sample #: Slope: Acres (gross): Acres (net): Crop: G r SOIL PROFILE DESCRIPTIONS Horizon Depth PROFILE A 4 • ,�, Texture ;. • Color Structure Mottles l ram_ ✓I Depth to SHWT: Depth & type of restrictive layer: S oil Series: Horizon Depth Texture Color Structure Mottles PROFILE B i Depth to SHWT: Depth & type of restrictive layer: Soil Series: Notes: 14,t h,&JG Described By: Legend Texture Structure Grade s Sand 1 Weak I Loam 2 Moderate si Silt 3 Strong c Clay Date: Structure Tvoe gr Granular abk pl Platy sbk pr Prismatic sg cpr Columnar m Angular Blocky Subangular Blocky Single Grained Massive SHEET SYNAGRO SOIL DESCRIPTION SH n 1,fJ7 Project: 4142E Fow ndowner:' > r Site: A___-- Field: Sample #: Slope: Acres (gross): Acres (net): Crop: 6t ; SOIL PROFILE DESCRIPTIONS Horizon Depth Texture Color Structure PROFILE A A _r --7 r-L I r Depth to SHWT: ')q Depth & type of restrictive layer: y Soil Series: Mottles Horizon Depth Texture Color Structure es _ PROFILE B �G -U o d �1 1► 1 l Depth to SHWT: Depth & type of restrictive layer:•q' 1238 r Soil Series: �' �� Notes: Described By: Date: D� Leciend Texture Structure Grade Structure Type s Sand 1 Weak gr Granular abk Angular Blocky I Loam 2 Moderate pl Platy sbk Subangular Blocky si Silt 3 Strong pr Prismatic sg Single Grained c Clay cpr Columnar m Massive SOIL DESCRIPTION SHEET1401 AGRO e ,o Project: Landowner: ,��✓ A,�:fL Site: L Field: Sample #: Slope: Acres (gross): Acres (net): Crop: j4sea- SOIL PROFILE DESCRIPTIONS Horizon Depth Texture Color Structure Mottles PROFILE A l9• r '�fe ---UA f•k �� �_ Ile C� Depth to SHWT: t Depth & type of restrictive layer: Soil Series: Horizon Depth Texture Color PROFILE B Structure Mottles � ran The u w Depth to SHWT: Depth & type of restrictive layer: Soil Series: 1238 Notes: ?L,Z Described By: r Date: `� Le end Texture Structure Grade Structure Tvpe s Sand 1 Weak gr Granular abk Angular Blocky I Loam 2 Moderate pl Platy sbk Subangular Blocky si Silt 3 Strong pr Prismatic sg Single Grained c Clay cpr Columnar m Massive NAGRO SOIL DESCRIPTION SHEET Project: d Landowner: d�h1ca1�'_ Site: _ _ Field: Sample #: Slope: Acres (gross): Acres (net): Crop: SOIL PROFILE DESCRIPTIONS Horizon Depth Texture Color Structure Mottles PROFILE A I PROFILE B Depth to SHWT: Depth & type of restrictive la yer: Soil Series: Horizon Depth Texture Color Structure Mottles Depth to SHWT: Depth & type of restrictive layer: Described By: Date: v Ado 4 0 Legend Texture Structure Grade Structure Type s Sand 1 Weak gr Granular abk Angular Blocky I Loam 2 Moderate p1 Platy sbk Subangular Blocky si Silt 3 Strong pr Prismatic sg Single Grained c Clay cpr Columnar m Massive SOIL DESCRIPTION SHEET NAGRO f Project: &N n I'A.0 4 °� , A ' ''Y"J",t � ' Landowner: � I� � 1,4— , Site: Field: 9 Sample #: Slope: Acres (gross): Acres (net): Crop: - Ark SOIL PROFILE DESCRIPTIONS Horniz�on Depth Texture Color Structure PROFILE A ��T �� sc 8� Ili elf q Mottles Depth to SHWT: Depth & type of restrictive layer: � Soil Series: rr -,l'°tv?ofi�T Horizon Depth Texture Color Structure r' " PROFILE B De th to SHWT: Depth & type of restrictive layer: Soil Series: Q_AtntlytA Notes; Described By: Date: Le end Texture Structure Grade Structure Type s Sand 1 Weak gr Granular abk Angular Blocky I Loam 2 Moderate pl Platy sbk Subangular Blocky si Silt 3 Strong pr Prismatic sg Single Grained c Clay cpr Columnar m Massive SOIL DESCRIPTION SHEET Project: " BO-A 96Y Site: r t Field: 4— Acres (gross): Acres (net): SYNAGR0 Landowner: 44- a-� — Sample #: Slope: , 3 c Crop. SOIL PROFILE DESCRIPTIONS Horizon Depth Texture Color Structure PROFILE A At? 15.4, 7. 4v. w - 1L. 1+ �. PROFILE B Notes: Legend Mottles Depth to SHWT: - � Depth & type of restrictive layer: +� Soil Series: 6,14b,424 Z94,2 4 ,. 1: , �Ew�eJ1.f Horizon Depth Texture Depth to SHWT: Depth & type of restrictive layer: Soil Series: Described By: Color Structure Mottles Date:1W � Texture Structure Grade Structure jpe s Sand 1 Weak gr Granular abk Angular Blocky I Loam 2 Moderate pl Platy sbk Subangular Blocky si Silt 3 Strong pr Prismatic sg Single Grained c Clay cpr Columnar m Massive NCDA&CS Agronomic Division Phone: (919) 733.2655 Website: www.ncagr.govlagronomi/ Report No. FY20-SLO31178 v I r 14 g, Client: Jim Goodwin Advisor: Nate Roth y, , r Heavy Metals 156 Jess Lane Synagro - PALS Account Stokesdale, NC 27357 284 Boger Rd Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Sampled County : Rockingham LinkstoHW�flInformation Client ID: 508595 Advisor ID: 425354 Sampled: 04/10/2020 Recelved: 05/21/2020 compleied: 05/27/2020 Farm: RL-49 Agronomist's Comments: This report contains both routinesoiliesi information as well as heavy metals datain a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a soil test extraciani, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead (Pb)- 4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007). Note elevated lead (Pb) in samples 49.02 and 49-04. Although the above metals here are not believed to pose a concern for plant growth, continue to monitor these and note where elevated above background levels. Note any lime and fertilizer recommendations. Ja athi Kamalakanihan, Agronomist, 512712020 Sample ID: 49-01 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/rim, M 0.0 120-200 140 20 0 0 0 $ 0 0 Note 12 Note: 2- 0.0 Test Results (units - WN In g/cm3; CEC and Na In meg1100 cm' ; NO3-N In mgldnr3): Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N 0.09 0.93 3.8 77 0.9 5.8 4 64 49 20 270 80 65 25 25 27 0.1 3 Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.3 Chromium, 0.5 Lead, 4.7 Selenium, 0.1 Sample ID: 49-02 Recommendations: Lime Nutrients (16lacre) More Crop (tonslacre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.4 0 140 10 0 0 0 6 2 0 Note: 3 2- 0.0 Test Results (units - WN in g1cm3; CEC and Na in meq/100 cm3; NO3•N In mgldnr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3.N 0.04 0,95 5.1 78 1.1 5.6 4 70 40 31 496 32 29 8 8 20 0.1 2 Heavy Metals (parts per million): Arsenic, 0.2 Cadmium, 0.0 Nickel, 0.1 Chromium, 0.3 Lead, 9.6 Selenium, 0.1 North Carolina Tk*ULO Trwt tvndCommi»Mon Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the Noah Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxier, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733.2666 Website: www.ncagr.gov/agronomll Report No. FY20-SLO31178 Jim Goodwin Page 2 of 4 Sample ID: 49-03 Recommendations: Lime Nutrients (Iblacre) More Crop (tonslacre) N P205 K20 Mg S Mn 2n Cu B Information Lime History: 1 -Fescue/OGrassfTim, M 0.0 120-200 140 110 0 0 0 $ 0 0 Note: 12 Note. 2- 0.0 Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N In mgldnf ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 2n.I 2n-AI Cu-I Na ESP SS-1 NO3-N 0.13 0.92 4.9 84 0.8 6.2 3 14 46 36 79 30 32 15 15 36 0.1 2 Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.2 Chromium, 0.2 Lead, 4.3 Selenium, 0.1 Sample ID: 49-04 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn 2n Cu B Information Lime History: 1 -Fescue/OGrassfTim, M 0.5 120-200 140 100 0 0 0 $ $ 0 Note: 12 Note: 2- 0.0 Test Results [units - WN in g1cm3; CEC and Na in meg1100 cm3; NO3-N In mgldm3jr Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 2n-I 2n-AI Cu4 Na ESP SS-1 NO3-N 0.13 0.88 4.0 71 1.2 5.5 2 21 37 30 387 15 26 20 20 25 0.1 3 Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.2 Chromium, 0.3 Lead, 7.7 Selenium, 0.1 Sample ID: 49.05 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P205 K20 Mg S Mn 2n Cu B Information Lime History: 1-Soybean 0.6 0 90 20 0 0 0 0 2 0 Note: 3 2- 0.0 Test Results [units - WN in g1cm3; CEC and Na In meg1100 cm3; NO3-N in mgldm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 2n-I 2n-AI Cu-I Na ESP SS -I NO3-N 0.18 0.93 4.6 73 1.2 5.5 20 69 44 22 445 34 30 50 50 25 0.1 2 Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.2 Chromium, 0.3 Lead, 3.8 Selenium, 0.1 NCDA&CS Agronomic Division Phone: (919) 733.2655 Webslte: www.ncagr.gov/agronomit Report No. FY20-SL031178 Jim Goodwin Page 3 of 4 Sample ID: 49-06 Recommendations: Lime Nutrients (Iblacre) More Crop (tonstacre) N P2O5 K2O Mg S Mn Zn Cu H Information Lime History: 1 -Fescue/OGrasslrim, M 0.0 120-200 150 110 0 0 $ $ $ 0 Note: 12Note: 2 - 0.0 Test Results [units -WN In g1cm3; CEC and Na In megf100 cm3; NO3•N in mgldm3J: Soil Class: Mineral HM% WN CEC HS% Ac pH P.l K-1 Ca% Mg% S-1 Mn-I Mn-Ali Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.04 0.85 3.7 98 0.1 6.4 1 17 73 22 296 8 15 6 6 22 0.1 3 Heavy Metals (pails per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.1 Chromium, 0.3 Lead, 5.1 Selenium, 0.0 NCDA&CS Agronomic Division Phone: (919) 733-2655 Webslte: www.ncagr.goviagronomil Report No, FY20-SLO31178 Jim Goodwin Page 4 o f 4 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low forthe crop(s) indicated, a lime recommendation will be given in units of either 8 boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting- BS % % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at on( Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM % percent humic matter Recommendations for field crops or other large areas are listed separately foreach nutrient to be added (in units of K-1 potassium index lb/ac(e unless otherwise specified). Recommendations for N (and sometimes for 8) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index forcfop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index armers and other commercial producers should pay special attention to micronutrient levels. If$, pH$, $pH, C or Z M-O mineral -organic soil class notations appear on the soil report, refer to Oofe: Secondary Nutrients and Micr+onutnents In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.govlagronomitpubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit-m",,i.ncagrgoy/avroncn*obuad4.htmflf nd information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowners Guide to Fertilizer P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume The first seven values [soil class, HM%, W/V, CEC, 8S%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-1, Ca%, Mg%, Mn-I, Mn-Al 1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S4, SS -I, Na, ESP, SS-1, NO3-N (not routinely Zn-I zinc index available)) indicate levels of plant nutrients or other fertility measurement. Visit r+�+w•ncaar.gov/agronomi/wrst.hfm Waypointe) ANALYTICAL 6/12/2020 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Ref: Analytical Testing Report Number: 20-160-0005 Project Description: Jim Goodwin RC-49 Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 6/8/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and N ELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, ?, K. Xcry Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 10 Q) Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-160-0005 Client Project Description: Jim Goodwin RC-49 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 72587 01 Solids 06/08/2020 SW-7471B WP MTN 72588 02 Solids 06/08/2020 SW-7471B WP MTN 72589 03 Solids 06/08/2020 SW-7471B WP MTN 72590 04 Solids 06/08/2020 SW-7471B WP MTN 72591 05 Solids 06/08/2020 SW-7471B WP MTN 72592 06 Solids 06/08/2020 SW-7471B WP MTN WP MTN - Memphis, TN; Waypoint Analytical - TN, Memphis, TN Page 2 of 10 Waypointo ANALYTICAL 46622 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypolntanalytical.com Synagro Central LLC/ Technical Nate Roth Mary Brewer Project Jim Goodwin Report Date : 06/12/2020 284 Boger Road Information : RC-49 Received : 06/08/2020 Mocksville , NC 27028 Submitted By : Nate Roth Report Number:20-160-000S REPORTOFANALYSIS Agronomist Pauric ry Lab No : 72587 Matrix: Solids Sample ID : 01 Sampled: Test Results Units MQL Mercury 0.0404 mg/Kg 0.0151 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit DF Date/Time By Analytical Analyzed Method 1 06/11/2010:37 DDB SW-7471B L Limit Exceeded Page 3 of 10 Waypointo ANALYTICAL 46622 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Synagro Central LLC/Technical Nate Roth Mary Brewer Project Jim Goodwin Report Date 06/12/2020 284 Boger Road Information : RC-49 Received 06/08/2020 Mocksville , NC 27028 mG G�N� Submitted By : Nate Roth Report Number : 20-160-0005 REPORTOFANALYSIS Agronomist ry Lab No : 72588 Matrix: Solids Sample ID : 02 Sampled: Test Results Units MQL DF Date /Time By Analytical Analyzed Method Mercury 0.0549 mg/Kg 0.0141 1 06/11/2010:39 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of. 10 0 7621 Whltepine Road, Richmond, VA 23237 Waypoint, Main 804-743-9401 ° Fax 804-271.6446 ANALYTICAL www.waypointanalytical.com 46622 Synagro Central LLC/ Technical Nate Roth Mary Brewer Project Jim Goodwin Report Date : 06/12/2020 284 Boger Road Information ; RC-49 Received 06/08/2020 Mocksville , NC 27028 XF Submitted By : Nate Roth Pauric McGroary Report Number: 20-160-0005 REPORT OFANALYSIS Agronomist Lab No ; 72589 Matrix: Solids Sample ID: 03 Sampled: Test Results Units MQL DF Date ITime By Analytical Analyzed Method Mercury 0.0644 mg/Kg 0.0141 1 06/11/2010:40 DDB SW-7471B Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 5 of 10 0 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com 46622 Synagro Central LLC/ Technical Nate Roth Mary Brewer Project Jim Goodwin Report Date 06/12/2020 284 Boger Road Information : RC-49 Received : 06/08/2020 Mocksville , NC 27028 mc Submitted By : Nate Roth Pauric McGroary Report Number :20-160-0005 REPORT OFANALlKSIS Agronomist Lab No : 72590 Matrix: Solids Sample ID : 04 Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0430 mg/Kg 0.0159 1 06/11/2010:44 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 6 of 10 Waypointo ANALYTICAL 46622 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Synagro Central LLC/ Technical Nate Roth Mary Brewer Project Jim Goodwin Report Date : 06/12/2020 284 Boger Road Information : RC-49 Received : 06/08/2020 Mocksville , NC 27028 Submitted By : Nate Roth Pauric McGroary Report Number : 20-160-0005 REPORTOFANALYSIS Agronomist Lab No : 72591 Matrix: Solids Sample ID: 05 Sampled: Test Results Units MQL DF Date/Time By Analytical Analyzed Method Mercury 0.0343 mg/Kg 0,0136 1 06/11/2010:45 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 7 of 10 Waypointo ANALYTICAL 46622 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Synagro Central LLC/ Technical Nate Roth Mary Brewer Project Jim Goodwin Report Date 06/12/2020 284 Boger Road Information : RC-49 Received : 06/08/2020 Mocksville , NC 27028 mG G� Submitted By ; Nate Roth Pauric McGroary Report Number : 20-160-0005 REPORTOFANALYSIS Agronomist Lab No : 72592 Matrix; Solids Sample ID: 06 Sampled; Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0603 mg/Kg O.01S6 1 06/11/2010:46 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 8 of 10 Waypigint(DAYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 46622 Customer Name: Synagro Central LLC/Technical Report Number: 20-160-0005 Shipping Method 0 Fed Ex I. US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? I. Yes 0 No Number of coolers/boxes received F-7 i0 Custody seals intact on shipping container/cooler? Yes 0 No I* Not Present Custody seals intact on sample bottles? 0 Yes 0 No I* Not Present Chain of Custody (COC) present? I. Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? ID Yes 0 No Sample containers intact? ID Yes 0 No Sufficient sample volume for indicated test(s)? ID Yes 0 No All samples received within holding time? ID Yes 0 No Cooler temperature in compliance? 0 Yes ID No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes ID No Water - Sample containers properly preserved 0 Yes 0 No ID N/A Water - VOA vials free of headspace 0 Yes 0 No ID N/A Trip Blanks received with VOAs 0 Yes 0 No ID N/A Soil VOA method 5035 —compliance criteria met 0 Yes 0 No ID N/A High concentration container (48 hr) [_ Low concentration Encore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes Comments: I 40 No Signature: Brandi Watson 1 Date & Time: 106/08/2020 09:34:04 Page 9 of 10 OT 3o OZ abad U U O � u C Cl \ I n �J o E > .s E a � U J LL Y U I4k a)o ., a a �v _ u m O in I i N nLn u ti = v a) O I j I` z M m a lii 76 1 % t n. r 1 V � C fV L r f C T l B � � - c� ro . B Q ci CC 4 . 1 n >• ' N C w a C. v — = Q r �n u • V � � � � O n n U N '7 — (n N p C U d7 W10 O ir _ �m 2' i u 0 InU) C) L a°1 (D W — l _ C)_ Z ti %n } L 7 m V .•c- J G� O 0 .v _ a a M. C j N ra t o >- C p O 30 � .. Q. c c •1 � —I a r � ai � x C. y a m crj V) 'In - A a"4THIS BOOK 1576 vac 87Y(2) wr. ,II iIIIIY^IIII Flied Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:17 PM Fee Amt: $26.00 NC Excise Tax: $0.00 LAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMENT TO WAIVE SETBACKS PURSUANT' To 15A NCAC on .Howe) I, JAMES REESE GOODWIN JR , certify that I ani a deeded owner of the property located at: Address: 156 JESS LANE Parcel No,: 163729 City: STOKESDALE State: NC Zip Code: 27357 County: ROCKINGHAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that l do hereby agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following page. af For the parcel identified above, I consent to a reduced setbacIt from 50 feet to o feet, thereby allowing the application of Class B residuals as near as 0 feet rrom my property line. For the parcel identified above, I consent to a reduced setbacIt from 400 feet to 100.feet, thereby allowing the application of Class B residuals as near as no feet from my residence. FORM: NDRMPW-LAS 11-18 CHANGE; OF OWNERSHIP OF ANY PARTIES INVOLVED** ,"..a,. 1,,,.,,11- Date: � 27� � Page 1 ora /v Permittee: Synagro Western Piedmont RI_AP Address: 284 Boger Rd. Mochville NC 27028 Permit No,: W00016247 City: MocicsvilIe State: NC Zip Code:27028_Cou11ty: Davie NORTH CAROLINA, TO&fv COUNTY I, N IZo a Notary Public for&,�County, North Carolina, do hereby certify thatti personally appeared before me this day and acknowledged the due execution of the foregoing instrument. Witness my hand and official seal, this the day of SEAL ROBERT N. ROTH Signature of Notary Public — NOTARY PUBLIC GUILFORD COUNTY �12y eanrnaissiorr e.�pirea _ �'� STATE OF NORTH CAROLINA Once notarized, this form shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the following address: Division of Water Resources Non -Discharge Branch 161.7 Mail Service Center Raleigh, North Carolina 27699-1617 FORM NDRA4PW-1.AS I I-18 Page 2 of i,. aoo. 1576 aara 89 (2) Filed Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:18 PM Fee Amt: $26.00 NC Excise Tax: $0.00 LAUREN B, GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMMNT TO WAIVE SETBACKS PURSUANT TO 15A NCAC 02T .1108(c) I, EDWARD R BAILES__ , certify that I am a deeded owner of the property located at: Address: 541 ALBERT ROAD Parcel No.: 116200 City: STOKESDALE— __ State: NC Zip Code: 27357 County: ROCKINGHAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following page. For the parcel identified above, I consent to a reduced setback from 50.feet to 0 feet, thereby allowing the application of Class B residuals as near as 0 feet froin my propertyline. 6For the parcel identified above, I consent to a reduced setback from 400 feet to 100 feet, thereby allowing the application of Class B residuals as near as 100 feet from my residence. "THIS WAIVER SHALT, BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED" Signature: _aO/�.� Date: FORM: NDRMPW-LAS I1-18 4 k9 Page I oft !n'l o clLs 01 -1f e/ Pexmittee: Synagro Western Piedmont R.LAP Address: 284 Boger Rd. Mocksville NC 27028 _Permit No.: W00016247 Ci y:Mocksyille State: NC Zip Code:27028 County: Davie NOR'I'H CAROLINA, oGJ- VW fjtt.,, COUNTY 1, 1Lol� �3._r�- 1'll , a Notary Public for. Vt+1 Il 1Y& _.. _County, North Carolina, do hereby certify that .., J4,(,/A personally appeared before me this day and acknowledged the due execution of the )foo�regoing instrument. Witness my band and official seal, this the ! I day of ,WA Z(.,Z SEA /J Z ROBERT N. ROTH NOTARY PUBLIC Signature of Notary Public GUILFORD COUNTY STATE OF NORTH CAROLIN My commission expires., Once notarized, this fonn shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the following address: Division of Water Resources Non -Discharge Branch 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDRMPW-1_AS 1 l-18 Page 2 of BOOK 1576 Pn1cc p91 (2) �frr. 5e:300 111111111111111111111111I Filed Rockingham County, NC Benjamin J. Curtis, Register of Deecfs 04/09/2020 01:30:19 PM Fee Amt: $26.00 NC Excise Tax: $0.00 LAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMENT TO WAIVE SETBACKS PURSUANT TO 15A NCAC 021' .1108(c) I, THURMAN EUGENE SMITH , certify that I am a deeded owner of the property located at: Address: 530 ALBERT ROAD Parcel No.: 116201 City: STOKESDALE States NC Zip Code: 27357 County: ROCKINGHAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the Applicant/Penuittee listed on the following page. Foes- the parcel identilied above, I consent to a reduced setback from 50,feet to 0 feet, thereby allowing the application of Class B residuals as near as 0 feet from my propertyline. For the parcel identified above, I consent to a reduced setback froln 400 feet to 100 feet, thereby allowing the application of Class B residuals as near as_100 feet from any residence. "THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED" G Signature: l? per126 FORM: NDRMPW-LAS 1148 7_0 q T0". " Pagel of 2 2�m Zs Perroittee: Synagro Western Piedmont RLAP Address: 284 Bover Rd. Mocksville, NC 27028 _Permit No.: WQ016247 City:Mocksville State: NC Zip Code:27028 County: Davie NO�R�THl_CA_jR_O�LINA, &Lr tM. COUNTY I I, IUD i t & I �1 � � , a Notary Public for kl 1 Po14, County, North Carolina, do hereby certify that_J&( �MkA F"CIU-62a .55Eh personally appeared before me this day and acknowledged the due execution of the foregoing instrument, m Witness y hand and official seal, this the��� day of � "6h Zo Z O_, . T aRTTAFiy N, ROTH Signature of Notary Public LFORD COUNTY OF NO My cot�t►►tissiott expires - STATE NORTH CAITOLINA Once notarized, this form shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the following address: Division of Water Resources Non -Discharge Branch 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDRMPW-LAS 1 l-18 Page 2 of Ma,r, q, KZU IU;53AM No. iyh"1 F. 'i BOOK 1576 PAGE 93 (2 ) 597301 Filed Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:20 PM Fee Amt: $26.00 NC Excise Tax: $0.00 LAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS D RESIDUALS AGREEMENT TO WAIVE SETBACKS PURSUANT TO 15A NCAC 02T ,1108(c) I, PATRICIA A KPIMER , certify that I am a deeded owner of the property located at; Address; 518 ALBERT ROAD_ _ Parcel No.; 116241 City: STOlaSDALE State; NC Zip Code: 27357 County; ROC KIN't: HAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the Applieant/Permittee listod on the following page, For the parcel identified above, Z consent to a reduced setback from 50,feet to 0 feet, thereby allowing the application of Class B residuals as near as_Q Eeet from my propei�tyline. . For the parcel identified above, Z consent to a reduced setback from 400 feet to 10 feet, thereby allowing the application of Class B residuals as near as 100 feet ft-om illy residence. **THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED** Siguat�tre; cl�wc..;--c�� Cr; , 4 FCCZM;XDRIv2W-Ias 11,18 te; 5 ` 0 'O—;) Wt 'Ro,44h 2�(f i3cyc-f ?e. ,/r /t%` Z 2p age 1 of �OG��5cJr � Ma;1, 4. 20U 1 U: AAM No. 3yb2 r, 4 Per:ruttee: S na ro 'Western Piedmont DLLAP Address: 284 Boger U, Mocksville NC 2 028 PerniitNo.: W00016Z 7 City:Mocksville, State: NC Zip Codo:27029 County: avie _ ct�.se_ J I COUNTY T, IiY1 e�i� `� >1� UAl *otary Public for 1_ Cotinty, do hereby certify that i-'UkX \`\60i k V\6 - personally appeared before me this day and acknowledged the due execution of the foregoing instrunieut. Witness xny hand and official seal, this the day of ,SEAL aft ��Ao lit AMELIA DIANE NUNLEY Signature of Notary Pubrl'e NOTARY PUBLIC Comm Reg. eajIh#718 of Virginia Ally eomr2ti.ssion expires Q �U(. A d,�a Reg. A�71f1387?� ' c� My Commission Expires Once notarized, this form shatl be recorded at the Register of Deeds in the county or counties in which the described properties are located. A, copy of the recorded waiver shall be sent to the following address: Division of dater Resources Non-bischaxge Bunch 16171VZO. Service Center Raleigh, North Carolina 27699-1617 FORM: NpRNIPW-LAS 11-19 page 2 of , . +v BOOK 1576 aaGEII 95 (2) p� 597302 IIIIIIYYIA^I Filed Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:21 PM Fee Amt: $26.00 NC Excise Tax: $0.00 LAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMENT TO WAIVE SETBACKS PURSUANT TO 15A NCAC 021' .1108(c) I, ALTON GLENN KING. certify that I am a deeded owner of the property located at: Address: 487 ALBERT ROAD Parcel No.: 116234 City: STOKESDALE_. .State: NC _—Zip Code: 27357 County: ROCKINGHAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following page. For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby allowing the application of Class B residuals as near as 0,1'eet from my property line. [,For the parcel identified above, I consent to a reduced setback from 400 feet to 100 feet, thereby allowing the application of Class B residuals as near as 100 feet from my residence. **THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED* * Signature: f Date: Ir _ FORM: NDRMPW-LAS 11-18 n Page 1 of Adc S ul 11 e I /JL 2Yn 2 8 Permittee: SLnagro Western Piedmont RLAP Address: 284 Boger Rd. Mocksville, NC 27028 _ Permit No.: WQ0016247 City:Mocksville State: NC Zip Code:27028,County: Davie NORTH CAROLINA, o K , COUNTY I, P,f' �- � � �o t` \ , a Notary Public for i o ! County, North Carolina, do hereby certify that Al:b n g leylyt KI nn personally appeared before me this day and acknowledged the due execution of the foregoing instrument. ri Witness my hand and official seal, this the 1_day of wdq _. SEAI. ROBERT N. ROTH Signature ofNvtaq Public GUlOT01y cot ICmX STATE pF COUNTY NORTH CAROLINA My coufmission exhi►es 20Z-1 Once notarized, this form shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the following address: Division of Water Resources Non -Discharge Branch 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDR_NTW-LAS 11-18 Page 2 of A - ak (� BOOK 1576 PAGE 97 (2) '°"° 111 Filed Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:22 PM Fee Amt: $26.00 NC Excise Tax: $0.00 LAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMENT TO WAIVE SETBACKS PURSUANT TO 15A NCAC 02T .1108(c) I, WILLIAM MATTHEW DEREMER , rectify that I am a deeded owner of the property located at: Address: 470 ALBERT ROAD Parcel No.: 116233 City: STOKESDALE State: NC Zip Code: 27357 County: _ROCKINGHAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following page. For the parcel identified above, I consent to a reduced setback from S0.feet to 0 feet, thereby allowing the application of Class B residuals as near as 0 feet from my propertyline. [� For the parcel identified above, I consent to a reduced setback from 400 feet to 100 feet, thereby allowing the application of Class B residuals as near as 100 feet from my residence. "THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED" FORM: NDRMPW-r-AS 11-18 Date: 19 �+ PC' 're-1w(A +a ; NaJL 41-h 2� 4 Page 1 of 2 ^CA suol < / JC 2::i6' 2'? i Permittee: Synag!•o Western Piedmont RLAP Address: 284 Boger Rd. Mocksy lle, NC 27028 PermitNo.: WQ0016247 City:Mocksville State: NC Zip Code:27028 County: Davie NORTH CAROLIN' A, COUNTY 1, T o�l_r �- IV 1� ' , a Notary Public for County, North Carolina, do hereby certify that Wli " t ic4m k4heo_ Aft,-N _peA•sonally appeared bef'or•e me tliis day and acknowledged the due execution of the foregoing instrument. Witness my hand and official seal, this theff day of &Weh _ 2D ZQ SEACED Signature ofNorary Public INA' My corrrrrrissiorr ezpir•es _ ec. zo Z-4 Once notarized, this form shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the fbllowing address; Division of Water Resources Non -Discharge Branch 1617 Mail Service Center Raleigh, Noi-th Carolina 27699-1617 FORM: NDRMPW-LAS 1 l-18 Page 2 of ,A- " BOOK 1576 PAGE 99 (2) "'n. 111111111111111111111 Filed Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:23 PM Fee Amt: $26.00 NC Excise Tax: $0.00 lAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMENTTO WAIVE SETBACKS PURSUANT" I'O 15A NCAC 021' .1108(c) I, WILLIAM M DEREMER__ certify that I am a deeded owner of the property located at: Address: 440 ALBERT ROAD Parcel No.: 116136 City: STOKESDALE _ _ __ Slate: NC Zip Code: 27357 County: ROCKINGI-JAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the ApplicantlPermittee listed on the Following page. W For the parcel identified above, I consent to a reduced setback from 5o_feet to o feet, thereby allowing the application of Class B residuals as near as 0 feet from my propertyline. For the parcel identified above, I consent to a reduced setback from 400 feet to 100 feet, thereby allowing the application of Class B residuals as near as 100 feet from my residence, "`THIS WAIVER SI-JALL BFI TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED** Signature: — — Date: R® Taily V1 in FORM: NDRMPW-LAS 1I-IS 2,0 'I�Uey Page ] of M12,1-,rSur'1r1_ f �Jc 2 020 Permiace: Sytiagro Western Piedmont RLAP Address: 284 BggerR& Mocksville NC 27028 Permit No-: W 00162d7 City:Mocksville State: NC Zip Code:27028 Comity: Davie NORTH CAROLINA, COUNTY 4 I _1P f �. D -,a Notary Public for emi I-FOY(iC County, North Carolina, do herebyeertify that ?�'bafb `ty personally nppeared before me this day and acknowledged the due execution of the foregoing instrument. Witness my hand and official seal, this the day of LA SEA L ROBERT N, ROTH NOTARY PUBLIC GUILrORD COUNTY STATE OF NORTH CAROLINA Signature of Notary Prrblie My Commission expires Once notarized, this form shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the following address: Division of Water Resources Non -Discharge Branch 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NIDRMPW-[.AS 11-7 8 Page 2 of 2 BOOK t576 a,:Ge tOt (2) �, 11111II1IlN61IP1Pl1lil� Filed Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:24 PM Fee Ami: $26.00 NC Excise Tax: $0.00 LAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMENT TO WAIVE SETBACKS PURSUANT TO 15A NCAC 02T .1108(c) I, BOBBY EUGENE EATON JR , certify that I am a deeded owner of the property located at: Address: 449 ALBERT ROAD Parcel No.: 116238 City: STOKESDALE_ State: NC _Zip Code: 27357 County: ROCKINGHAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following page. Vor the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby allowing the application of Class B residuals as near as 01'eet from my propertyline. For the parcel identified above, I consent to a reduced setback from 400 feet to 100 feet, thereby allowing the application of Class B residuals as near as 100.feet from my residence. "THIS WAIVER SHALL BE TERMINATED UPON CHANGE Of OWNERSHIP Or ANY PARTIES INVOLVED" Signature: _Date: FORM: NDRMPW-LAS 11-18 Page 1 of 2 Vq U i N t �J 270 z 9 Permittee: SynaUo Westeni Piedmont RLAP Address: 284 Boger Rd. Mocksville, NC 27028 Permit No.: WQ0016247 _. City:Mocksville State: NC Zip Code:27028 County: Davie NORTH C.ARO,. kLINA, COUNTY I, "Va10,�,f�- N �o' , a Notary Public for ^County, North Carolina, do hereby certify that l +1114 e_ GAyon VV . personally appeared before me this day and acknowledged the due execution of the foregoing instrument. Witness my hand and official seal, this the /V'day of U"lW�y1_ 7Q1(a SEAL ROBERT N. ROTH NOTARY PUBLIC GUILFORD COUNTY STATE OF NORTH CAROLINA Signature of Notary Publie My Commission eehires c Once notarized, this form shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the following address: Division of Water Resources Non -Discharge Branch 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDRMPW-LAS 11-18 Page 2of2 BOOK 1576 PAGE 103 (2 ) 597306 1111111111111111111111 Filed Rockingham County, NC Benjamin J. Curtis, Register of Deeds 04/09/2020 01:30:25 PM Fee Amt: $26.00 NC Excise Tax: $0.00 LAUREN B. GAMMON State of North Carolina Department of Environmental Quality Division of Water Resources NON• -DISCHARGE RESIDUALS MANAGEMENT PROGRAM WAIVER FOR THE APPLICATION OF CLASS B RESIDUALS AGREEMENT TO WAIVE SETBACKS PURSUANT TO 15A NCAC 02T .1108(c) 1, GEORGE ROGER TYSINGER _, certify that I am a deeded owner of the property located at: Address: 175 JESS LANE Parcel No,: 115242 City: STOKESDALE_ State:. NC ___Zip Code: 27357 County: ROCKINGHAM Furthermore, I certify that I am authorized to make decisions regarding this property, and that I do hereby agree that the setback distances cited below be granted to the Applicant/Permittee listed on the following page. [ For the parcel identified above, I consent to a reduced setback from 50 feet to 0 feet, thereby allowing the application of Class B residuals as near as 0 feet from my propertyline. For the parcel identified above, I consent to a reduced setback from 400 feet to 100 feet, thereby allowing the application of Class B residuals as near as 100 feet from my residence. "THIS WAIVER SHALL BE TERMINATED UPON CHANGE OF OWNERSHIP OF ANY PARTIES INVOLVED" Signature:_ Date: / ��f' - Tefwv 1Jce_ FORM: NDRMPW-LAS 1 l-18 Z$4 '�n9'e1 Page 1 of WtoOr—s L) f f f' r— /J�— Z �F-S Permittee, Synagro Western Piedmont RLAP Address: 294 Bogey Rd. Mocksville, NC 27029 Pei-mit No.: WQ0016247 City:Mocksville State: NC Zip Code:27028_County: Davie NORTH CAROLINA 'ZoGV-:\ COUNTY K, a Notary Public for. loc i f �oy !� County, North Carolina, do hereby certify that Ge�)Y�P� �IS4;P_�i personally appeared before me this day NIJ and acknowledged the due execution of the foregoing instrument. Witness my hand and official seal, this the_L Its day of MIA(Gh 'zoZ,Q, S ROBERT N. ROTH NOTARY PUBLIC Signature of Notary Public GUILFORD COUNTY STATE OF NORTH CAROLINA p My commission ewj;ires pe-L, l Once notarized, this form shall be recorded at the Register of Deeds in the county or counties in which the described properties are located. A copy of the recorded waiver shall be sent to the following address: Division of Water Resources Non -Discharge Branch 1617 Mail Seivice Center Raleigh, North Carolina 27699-1617 FORM: NDRMPW-LAS 11-18 Page 2 of VICINITY MAP cc L / ii �.... jr +4061k GRAPHIC SCALE 1" = 4,000' 4.C(1e1 0 n,cca The compliance boundary is established either 250 it from the residuals application area or 50 feet within In the property boundary, whichever is closest to the application area, The review boundary Is established midway between the compliance boundary and the porimetor of the residuals application area. All locations are approximate, 3r' NC-HA-47 Fields 1-4 APPLICATION MAP y Z ; r Lin 10 / ❑* ,S l n✓ e� LLL l j» S 0111 , LEGEND APPLICATION AREA UNSUITABLE AREA — — — — — — PRIVATE ROAD WATER GRAPHIC SCALE STREAM ONSITE HOUSE 1" = 660' eso o 6W DRAIN OFFSITE HOUSE W—.X W— FENCE OUTBUILDING PROPERTY LINE 0 WELL The compliance boundary is established either 250 ft from the residuals application area or 50 feel within I _L1 A_ A47 in the properly boundary, whichever Is closest to the application area. The review boundary Is established NVV flit A midway between the compliance boundary and the perimeter of tho residuals application area. All locations are approximate, Fields 1-4 TOPOGRAPHIC 1MAP C2O 1� III , , it Ce �'rvr % GRAPHIC SCALE V = 1,000' soon 0 11000' The compliance boundary Is established either 250 ft from the residuols application area or 50 feel within A I I V_�L1 AA .4'T in the property boundary, whichever is closest to the application area. The review boundary Is established f V f� midway between the compliance boundary and the perimeter of tho residuals application area. All locations are approximate, Fields 1-4 I(D SOIL SURVEY Cr x Q � ; I� V) k i v-v �I GRAPHIC SCALE 9" = 800' 000, 0 a00' The compliance boundary Is established either 250 ft front the residuals application area or 50 feet within NC- HA-47 In the properly boundary, whichever is closest to the application area. The review boundary Is established midway between the compliance boundary and the porimelor of the residuals application area, All ,1 locations are approximate. Fields 1-4 nwp Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources I SA NCAC 02T .1100— LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a cheeldist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application an supporting documentation Fa•more infjormatron, }visit the WaterQtialityPertnitting Section's Non-Dischai-ze rn ' t Unit. General —This document is an agreementbetwecn the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant orother type residuals) in accordance with _15A NCAC 02T .11 OQ. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otheiivise noted, the Applicant shall submit one original and two copies of the application and supportingdocumentatio n listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) f'oim. Please do not make any unauthorized content changes to this form. if necessary for clarity or due to space restjictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prcpare a separate agreement for cacti set of land application sites that arc owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must beprovided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name; Synayy-o Western Piedmont RLAP hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Laud Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-HA-47-1 N Pasture Grazing NC-HA-47-2 N Pasture Gazing NC-HA-47-3 N Pasture Grazing NC-HA-47-4 N Pasture Grazing The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residua Is. this Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM; LOA 06-16 Page] of3 I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 11) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the Ituid application site(s). 6, The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement ofany residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application sitc(s). 1 1. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement a d schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terns and conditions of the pennit take necessary leachate, surface water, groundwater, or soil samples during the tern of, and 12 months after termination of, this Agreement. iI. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or thelandowner or his representative to control public access to the land application site(s) during active use and for the 12-month period followi g a residuals land application event, Such conln'ols may include the posting of signs that indicate the activities being conducted at the land application sitc(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals laud application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not beharvested for a 14-month period following a residuals land application event. 5. Food amps with harvested parts below the surface of the land shall not be harvested fora 20-month period following a residuals land application event when the residuals remain on the land surface f'or four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested f'or a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. HLALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COWLIANCE BOUNDARY: (please sheets one) 1 SA NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, ISA NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please marls one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale forthe requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) A re -defined compliance boundary is not needed for this site. IV. ACIINOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: . is currently permitted under another residuals land application program; Pennit Number WQ: The land owner hereby acknowledge that by signing this agreement, Ire/shc is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. l certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other perniitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives fbr water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: �w_" ap e, Address: Jr T 1 ' BOSS City: L;14 h State: N G Zip: Phone: _ E-mail address: Signature: Date: NORTH CAROLINA, boo'v-%.L. A— COUNTY 1, the undersigned Notary Public do hereby certify that Toe t_ 2775 personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the day of V "ViAV , 20 GU Signature and seal: �✓ �'� My commission expires: Q Z NOTARY PUBLIC STATE OF NORTH CAROLINA Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: State: Zip: Phone: E-mail address: Signature: -- -- Date: Permittee's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: Q42 Signature: /?�'✓v "� / ! fi r Date: A(��� p SYNAGRO, HARNETT COUNTY UTILITIES CLASS B PERMIT WQ 0014885 SOIL SCIENTIST CERTIFICATION This is to certify that soil profile evaluations were conducted on the proposed application sites for the Harnett County Utilities project by Piedmont Environmental Associates, P.A. on behalf of Synagro Central, LLC. The evaluations consisted of hand auger borings and descriptions of the soils on the application sites. All hand auger borings included in this package were either performed by me or under my direct supervision. All other work performed for this permit application was conducted by Synagro Central, LLC. G. Christopher Murray, L.S.S. No. 1284 Synagro, Harnett County Utilities Project, Various Fields Soil Profile Descriptions in Field Locations Project: Harnett County Utilities (WQ 0014885) % Slope: 2% Site: J.W. Pope Farm Crop: Forage/Pasture PIEDMONT Field: J.W. Pope, Field 1 Conducted By: GC Murray Coordinates: 35"34'41"N Date: 9/10/2019 ENVIRONMENTAL -78'74'88"W Soil Series: Aycock A a o a I w r■ s, •. w. o w W > C a a o v O N 6 N e N O U O U O Q rn U ;v m > > t0 N LhI ?� N O N OI fU C N ate. U u C1 N Y I p m O Gi O' `I S O 5 Ap 0-6 10YR 3/3 moist I sl I mod I med gr fr ns np� E 6-10 10YR 3161 moist I sl I mod I med gr fr ns np Btt 10-30 1 10YR 514 1 moist cl mod med sbk ri s B12 30-48 10YR 514 1 5YR &5, 1oYR 7/3 com. med. C$D moist cl mod med sbk fi s Legend: Texture s sand I loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam sicl silly clay loam Structure Grade Structure Tyne wk weak gr granular m moderate pl platy str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky sg single grained ma massive Structure Size f fine med medium Moist Consistency fr friable vfr very friable fi firm vfi very firm Seasonal High Water Table: Depth (") Type (apparent/parched) 34 1 perched Soil Profile Descriptions in Field Locations Project: Harnett County Utilities (WQ 0014885) % Slope: 2% Site: J.W. Pope Farm Crop: Forage/Pasture , PIEDMONT Field: J.W. Pope, Field 2 Conducted By: GC Murray Coordinates: 35°20'52"N Date: 9/10/2019 ENVIRONMENTAL -78"44'55"W Soil Series: Aycock w a s o a I w r a Z. P. A. m Ci w N d m y U G .O. 7 N CO V) t }a} ti t O O c U U L Q U fn i O N y ( � �' C N ..L+ x O/ Gt N M KI <i O O y� i S S S N 5 10 wI Ap 0-4 10YR 313 moist fsl mod med gr fr I ns np-1 E 4-11 10YR 413 moist sl mod med gr fr ns np Bt1 11-25 10YR 514 - moist cl mod med sbk fi s p Bt2 25-42 10YR 514 - I I moist cl mod med sbk ri s p Bt3 42-48 10YR 514 5YR s15, 10YR 7r2 com. med. C&D moist c wk I med abk I fi s Legend: Texture s sand loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam Sid silty clay loam Structure Grade Structure Type wk weak gr granular m moderate pl platy str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky sg single grained ma massive Structure Size f fine med medium Moist Consistency fr friable vfr veryfriable fi firm vfi very firm Seasonal High Water Table: Depth (") Type (a arentl erched) 45 1 perched Soil Profile Descriptions in Field Locations Project: Harnett County Utilities (WQ 0014885) % Slope: 2% Site: J.W. Pope Farm Crop: Forage/Pasture `; PIEDMONT Field: J.W. Pope, Field 3 Conducted By: GC Murray I Coordinates:35°34'97"N Date:9/10/2019 ENVIRONMENTAL -78°74'69.7"W Soil Series: Aycock w s : o c w r ■ . .. w . N L) n fl Q N W U d N L O C U G U3 N O O L) i> 2 4 Q fJ O en U y 7 7 C a U . N y K N •O Z'i aY Z'i _N C r 7 Z'i U U U C �. 4 .1C N N O T n S S O S O N O � S rY S i+ iA w iA --' O nI 1. S Ap 0-5 10YR 3/3 moist sl mod med gr fr ns n E 5-12 10YR 3/4 - moist fsl mod med gr fr ns np Btl 12-32 10YR 5/4 - moist cl mod med sbk fi s p Bt2 32-48 10YR 5/4 5YR 6/5, 10YR P2 com. med. C&D moist cl wk med abk ft s p Legend: Texture s sand I loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam sicl silty clay loam Structure Grade Structure Type wk weak gr granular m moderate pl platy str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky sg single grained ma massive Structure Size f flne med medium Moist Consistencv fr friable vfr vefyfriable fi firm vfi very firm Seasonal High Water Table: Depth (") Ty a {apparentlperched) 38 perched Soil Profile Descriptions in Field Locations Project: Harnett County Utilities (WQ 0014885) % Slope: 2% Site: J.W. Pope Farm Crop: Forage/Pasture PIEDMONT Field: J.W. Pope, Field 4 Conducted By: GC Murray Coordinates: 35°35'22"N Date: 9/10/2019 FuMrsnuuruTAr -78°74'66.8"W Soil Series: Aycock w ■ s o c I w r > > . P.A. LLIa m o d c } a O O u a O N U ` = N C) W N ` W 0� C N +O+ U U U la 0 O O S O S Ap 0-4 10YR 3/3 moist I sl mod med gr fr ns np E 4-10 10YR 4/3 - moist sl mod med gr fr ns np Bt1 10-34 10YR 5/4 - moist cl mod I med sbk fi s p Bt2 34-48 10YR 5/4 - - moist cl wk med sbk fi s p Legend: Texture s sand I loam si silt sil silt loam c clay cl clay loam sci sandy clay loam sl sandy loam sicl silty clay loam Structure Grade Structure Type wk weak gr granular m moderate pl platy str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky sg single grained ma massive Structure Size f fine med medium Moist Consistency fr friable vfr very friable fi firm vti very firm Seasonal High Water Table: Depth (") Type (apparent/perched) NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govfagronomlr Report No, FY20-SL001678� IIl14ri Client: JWPope Advisor: SYNAGROCenIraILLC *�µl Heavy Metals 5815 Ross Rd One Commerce Square Lillingion, NC 27546 Suite 204 Washington, NC27889 y kr Soil Report o Sampled County : Harnett Sampled Links to tipipfid Information _-- Client ID: 500901 Advisor ID: 400832 sampred: Recewed: 08/01/2019 compreted: 08/12/2019 Farm: Agronomist's Comments: This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals undersoil test lab results. using Mehlich 3 as a soil test extracianl, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic(As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead (Pb)- 4.2 ppm, nickel (Ni)- 0.8 ppm, 8, selenium (Se)- 0.2 ppm (FY2005-2007). Although the above metals here are not believed to pose a concern for plant growth, continue to monitor these and note where elevated above background levels, Note any time and fertilizer recommendations. Where soil test phosphorus (P) is very hi h P-1 > 100 cro s will not respond to additional P applied. David H. Hard , Agronomist, August 12 2019 Sample ID; 01-01 Recommendations: Lime NUinents acre More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Bermuda hay/past., M 0.0 180-220 20 110 0 20 0 0 0 0 Note: 12 2 - Bermuda hay/past., M 0.0 180-220 20 110 0 20 0 0 0 0 Note: 12 Test Results (units - WN in grcm3; CEC and Na in megr100 cm3; NO3-N in mgrdm3]; Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-Al Cu-1 Na ESP SS-1 NO3-N 0.36 1.27 5.2 81 1.0 6.1 55 50 54 22 23 92 71 71 60 60 72 0.1 2 Heavy Metals (parts per million): Arsenic, 0.4 Cadmium, 0.1 Nickel, 0.4 Chromium, 0.3 Lead, 7.5 Selenium, 0.1 Sample ID: 01-02 Recommendations: Lime Nutrients acre More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 - Bermuda hay/past., M 0.5 180-220 20 80 0 0 0 0 0 0 Note: 12 2-Bermuda hay/past, M 0.0 180-220 20 80 0 0 0 0 0 0 Note 12 Test Results (units - WN In g/cm3; CEC and Na in megr100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-Ali Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS -I NO3-N 0.60 1.21 6.7 78 1.5 5.7 51 67 55 18 38 249 166 166 298 298 251 0.1 1 Heavy Metals (parts per million): Arsenic, 0.3 Cadmium, 0.1 Nickel, 0.5 Chromium, 0.3 Lead, 11.8 Selenium, 0.1 North Carolina [Al buur Trud rd6rl CivivoiWon Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler.Commissioner ofApriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronoml/ Report No. FY20-SL001678 JW Pope Page 2 of 3 Sample ID: 01-03 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P305 K20 Mg S Mn 2n Cu B Information Lime History: 1-Bermuda hay/past., M 1.4 180-220 0 100 0 0 0 0 0 0 Note: 12 2-Bermuda hay/past., M 0.0 180-220 0 100 0 0 0 0 0 0 Note: 12 Test Results (units - W N In g/cm3; CEC and Na In meq/100 cm3; NO3-N In mg/dm3j: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 2n-I 2n-Al Cu-I Na ESP SS -I NOa-N 1,31 1.18 5.6 57 2.4 5.1 122 55 40 12 46 64 55 55 89 89 72 0.1 2 Heavy Metals (parts per million)' Arsenic, 0.5 Cadmium, 0A Nickel, 0.4 Chromium, 0.3 Lead, 7.7 Selenium, 0.0 Sample ID: 01-04 Recommendations: Lime Nuir enis ( acre) More Crop (tons/acre) N P205 K20 Mg S Mn 2n Cu B Information Lime History: 1-Bermuda hay/past., M 0.0 180-220 0 0 0 0 pH$ 0 0 0 Note: 12 Note: 2-Bermuda hay/past-, M 0.0 180-220 0 0 0 0 pH$ 0 0 0 Note: 12 Note: Test Results (units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N In mg/dn�]j Soil Class: Mineral HM% WN CEC 13S% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 2n-I 2n-AI Cu-I Na ESP SS -I NO3-N 0.46 0.86 9.8 99 0.1 7.3 195 614 38 30 63 153 88 88 256 256 104 0.1 1 ieavy Metals (parts per million): Arsenic, 0.3 Cadmium, 0.0 Nickel, 0.5 Chromium, 0.2 Lead, 2.8 Selenium, 0.0 NCDA&CS Agronomic Division Phone: (919) 733.2666 Webslte: www.ncagr.govlagronomll Reporl No. FY20-SL001678 JW Pope Page 3 of 3 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is toolow for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one Ca% % CEC occupied by calcium time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate CEC cation exchange capacity is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K2O potash forthe crop being grown, not on soil test results. K-1 and P-1 values are based on testresults and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1Mn-Al2 Mn-availability index for crop 2 Mn-I manganeseindex 3rmers and other commercial producers should pay special attention to micronutrient levels, If $, PH$, $PH, C or Z M-O mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronorriL/pubs.htm. NOa-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot find pH current soil pH the exact fertilizer grade recommended on the report, visit ivww.nca r. v/a mnomi/ob art4_ht Ind information that P-1 phosphorus index may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer. P2O5 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W!V weight per volume The first seven values [soil class, HM%, WfV, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-Al zinc availability index remaining 16 (P-I, K-I, Ca%, Mg%, Mn-1, Mn-Al 1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely Zn-I zinc index available)] indicate levels of plant nutrients or other fertility measurement. Visit ww ncarlaov/anronomi/uyrst.htm Waypointo ANALYTICAL 6/10/2020 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 20-156-0003 Project Description: JW Pope 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 6/4/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report, Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypoint,(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Sample Summary Table Report Number: 20-156-0003 Client Project Description, JW Pope Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 72564 1 Solids 06/04/2020 SW-7471B W P MTN 72565 2 Solids 06/04/2020 SW-7471B WP MTN 72566 3 Solids 06/04/2020 SW-7471B WP MTN 72567 4 Solids 06/04/2020 SW-7471B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 8 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical Mary Brewer Project JW Pope 284 Boger Road Information Mocksville , NC 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Number: 20-156-0003 REPORT OFANAL YSIS Lab No : 72564 Sample ID ; 1 Report Date : 06/10/2020 Received ; 06/04/2020 pot" r 6eb7-01 Pauric McGroaty Agronomist Matrix: Solids Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury <0,0143 mg/Kg 0.0143 1 06/09/2012:38 DDB SW-7471B Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 3 of 8 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical Mary Brewer Project JW Pope 284 Boger Road Information Mocksville , NC 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Number : 20-156-0003 REPORTOFANALYSIS Lab No : 72565 Sample ID: 2 Report Date : 06/10/2020 Received : 06/04/2020 Pauric McGroary Agronomist Matrix: Solids Sampled; Test Results Units MQL DF Date I Time By Analytical Analyzed Method Mercury 0.0189 mg/Kg 0.0146 1 06/09/2012:39 DDB SW-7471B Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 8 0 7621 Whitepine Road, Richmond, VA 23237 Waypoint Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypolntanalytical.com 46622 Synagro Central LLC/ Technical Mary Brewer Project JW Pope Report Date 06/10/2020 284 Boger Road Information Received : 06/04/2020 Mocksville , NC 27028 me GIN Pauric McGroary Report Number :20-156-0003 REPORT OFANAL YSIS Agronomist Lab No : 72566 Matrix; Solids Sample ID : 3 Sampled: Test Results Units MOL DF Date I Time By Analytical Analyzed Method Mercury 0.0477 mg/Kg 0.0151 1 06/09/2012:40 DDB SW-7471B Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 5 of 8 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical Mary Brewer Project JW Pope 284 Boger Road Information Mocksville , NC 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Report Number :20-156-0003 REPORTOFANALYSIS Lab No : 72567 Sample ID: 4 Report Date 06/10/2020 Received 06/04/2020 Pauric McGroary Agronomist Matrix: Solids Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0393 mg/Kg 0.0143 1 06/09/2012:42 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 6 of 8 Waypoeinto ANALYTICAL 7621 Whltepine Road, Richmond, VA23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number:46622 Customer Name: Synagro Central LLC/Technical Report Number: 20-156-0003 Shipping Method 0 Fed Ex 0 US Postal 0 Lab is UPS 0 Client 0 Courier 0 Other: Thermometer ID: Shipping container/cooler uncompromised? le Yes 0 No Number of coolers/boxes received I 3 Custody seals intact on shipping container/cooler? 0 Yes 0 No I. Not Present Custody seals intact on sample bottles? 0 Yes 0 No I. Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? I. Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? I. Yes 0 No Sample containers intact? I. Yes 0 No Sufficient sample volume for indicated test(s)? I. Yes 0 No All samples received within holding time? I. Yes 0 No Cooler temperature in compliance? 0 Yes I. No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes I. No Water - Sample containers properly preserved 0 Yes 0 No I. N/A Water - VOA vials free of headspace 0 Yes 0 No I. N/A Trip Blanks received with VOAs 0 Yes 0 No I. N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No I. N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) [_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes I. No Comments: Signature: lBrandi Watson Date & Time: 106/04/2020 09:41:39 Page 7 of 8 (D WaYPAoint_ NALYTICAL S- - ----- - ---_ 111 IIIV 11 IIIVlllllll Wll IV III II 4662206-04-2020 Swraao Central LLCJ Technical 09:39:56 JW Pope 'M Account # / Grower/Project Information ormation tiubmltted by Charge To -51 va_� Po Farm ID �A - � � Field ID 1gOC k--� v{1[,e, lJ G 2 -70 Credit Card # I CSV Exp. Date: / Phone # .9 3 La 107 rL Z 7 IE-mail address C W IVto e Q f> two • c. tit Crop Into For Recommendations Sample ID Lab Number (Lab Use Only) S1 M 'S2M - Spe6ifyAdditional Tests S3M Soluble Salts Texture NO3-N Additional Tests Intended Crop Yield Goal Alternative Crop Yield Goal Previous Crop B jCujFejMnjNaj S jZn 7 _ Lab# E 72564-1 1 3 Cust: 46622 Synaqro Central LLC/ Technical - Col: Rec: 06/04/2020 00:00 -� 20-156-00o3 Preservation: I I I I I I I r Lab# E 72565-1 2 Cust.-46622 Synaqro Central LLC/ Technical Col: Rec: 06/04/2020 00:00 20-IS6-0003 Preservabon: _ Lab# E 72566-1 3 Cust: 46622 Synaqro Central LLC/ Technical — Col; Rec: 06/04/2020 00:00 20-1564003 Pressration: Lab# E 72567-1 4 Oust:46622 SynagmCentral LLC/Technical Cot 0 : 0003 Rer= 06/04/2020 00:00 Preservation: Mehlich 1117est Packages Special Instructions or Additional Tests SiM - Orgarvc matter. Phosphorus, Potassium, Calcium, Magnesium, pH, Buffer pH Cation Exchange Capacity, and % Base Saturation. S2M -Test S1 M plus any two of the following: Sodium, Sulfur, Boron, Zinc, Manganese, Iron, Copper. Each additional test (above two) cost $2.00. S3M -Test S1M plus Sodium, Sulfur, Boron, Zinc, Manganese, Copper, and Iron. �t4 4- p yt M LO vz o Y GRAPHIC SCALE 1 " = 4,000' 000' o 4,000' i The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. N C-CH-78 Fields 1-3,5 �■ APPLICATION MAP LEGEND APPLICATION AREA — —�— — — PRIVATE ROAD STREAM DRAIN X X x FENCE PROPERTY LINE UNSUITABLE AREA WATER + ONSITE HOUSE 0 OFFSITE HOUSE ❑ OUTBUILDING WELL The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 1 " = 660' 660' 0 660' NC-CH-78 Fields 1,3 APPLICATION MAP LEGEND APPLICATION AREA — —�— — ^ PRIVATE ROAD C STREAM DRAIN . -- FENCE ❑ PROPERTY LINE 0 UNSUITABLE AREA WATER ONSITE HOUSE OFFSITE HOUSE OUTBUILDING WELL The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 1 " = 660' sso' o sso' E NC-CH-78 Field 2 ((� APPLICATION MAP 1 ■ Z ■ 000� ' Q � o i ■ i LEGEND APPLICATION AREA UNSUITABLE AREA PRIVATE ROAD WATER GRAPHIC SCALE STREAM ! ONSITE HOUSE 1 " = 660' DRAIN . sso' o sso' OFFSITE HOUSE FENCE ❑ OUTBUILDING PROPERTY LINE 0 WELL The compliance boundary is established either 250 ftfrom the residuals application area or 50 feet within N C-CH-78 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the locations are approximate. residuals application area. All Field 5 TOPOGRAPHIC MAP s 1 ` ` t if r �. •Jf ! i ., ! GRAPHIC SCALE 1"=1,000' 1,000, 0 1,000, i The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CH-78 Fields 1-3 TOPOGRAPHIC MAP Ln {, 1-1 GRAPHIC SCALE 1" = 1,000' 1,000, 0 1,000- The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CH-78 Field 5 SOIL SURVEY GRAPHIC SCALE 1 " = 800' 800, 0 800, The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. N C-CH-78 Field 1 ref: SOIL SURVEY GRAPHIC SCALE V = 800' 800, 0 800, r r 0 The compliance boundary is established either 250 ft from the residuals application area or 50 feet within NC-CH-78 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area, All locations are approximate. Field 2 SOIL SURVEY GRAPHIC SCALE 1" = 660' 660' 0 660' The compliance boundary is established either 250 ft f rom the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CH-78 Field 3 SOIL SURVEY GRAPHIC SCALE 1" = 660' 660' 0 660' i The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CH-78 Field 5 State of North Carolina Department of Environmental Quality Division of Water Resources Dlvlslon of Water Resources 15A NCA'C 02T .l 100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two conies of the apLlication and supporting documentation For ►nore injor►nation, visit the Water Quality Permitting Section's rt-DischorQe Permitting Unit, General -- This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otheruise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form, If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicants narne: Synagro Western Piedmont RLAP hereinafter referred to as the Permittee, to land apply residuals from the following tacility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease es/no (Y ) Land Use or Cropping Patterns PP g Intended Use of Crops Residuals Source o tional (optional) Special note (no-till/over-seed/ pasture) NC-CH-78-1 N Pasture Grazing NC-CH-78-2 N Pasture Grazing NC-CH-78-3 N Pasture Grazing NC-CH-78-5 N Pasture Grazing The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Pagel of 3 1. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with inf oimation and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pI-I of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lure shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., f61ilizer, unregulated animal waste, etc.) that have been applied to the land application sitc(s). 11, The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative priorto and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. I1. RESTRICTIONS: I. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14- month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil, 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. ULALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the f ollowing; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: , is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transf6Ted into the new program; (Name of the new program) POPA/[- I nA nti_iti PaaP 7 of I Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to la d apply residuals to the land application site(s) as specified herein. Landownername: Address: '(—) 1 City: �Z- �� -�Z State: _�� L Zip: Phone: �� E-mail address: (��c_ S` sl� Signature: Date: NORTH CAROLINA, Ctia�ti�� COUNTY I, the undersigned Notary Public do hereby certify that — personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the 5e-k)e- ee_ e day of r- Signature and seal: L. My commission expires: Lessee's/Operator's Certification: , 20 Z GUILFORD COUNTY STATE OF ]NORTH CAHOLWA I certify that 1 have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail Date: Zip: I certify that 1 have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: Signature: iDate: FORM: LOA 06-16 Page 3 of SYNAGRO, HARNETT COUNTY CLASS B PERMIT WQ 0007066 SOIL SCIENTIST CERTIFICATION This is to certify that soil profile evaluations were conducted on the proposed application sites for the Harnett County project by Piedmont Environmental Associates, P.A. on behalf of Synagro Central, LLC. The evaluations consisted of hand auger borings and descriptions of the soils on the application sites. All hand auger borings included in this package were either performed by me or under my direct supervision. All other work performed for this permit application was conducted by Synagro Central, LLC. G. Christopher Murray, L.S.S, No. 1284 Synagro, Harnett County MTP Project, Various Fields Soil Profile Descriptions in Field Locations Project: Synagro Harnettt Co. (WQ 0007066) % Slope: 3% Site: CH_78 Crop: Forage/Pasture Field: Field 1 Conducted By: GC Murray Coordinates: 35.6220 N Date: 12/6/2019 -79.3619 W Soil Series: Cid/Lignum PIEDMONT ENVIRONMENTAL A S s Oct AT us, P A. BC 1 23-27 12.5YR 4/81 1- - - moist I sicl I mod I med I sbk I fi I s Ip CR 28 - - - - - - - - - - - - - Legend: Texture s sand I loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam sicl silty clay loam Seasonal High Water Table: Structure Grade Structure Type Structure Size Depth (") Type (apparentlperched) wk weak gr granular f fine 20 perched m moderate pl platy med medium str strong pr cpr prismatic columnar SM blocky$~� PHAR OP abk angular sbk subangular blocky Moist Consistency sg single grained fr friable o A. ma massive vfr very friable mf �•� fi firm 1z�Qr ►ems A very firm ' Soil Profrle Descriptions in Field Locations Project: Synagro Harnettt Co. (WQ 0007066) % Slope: 3% Site: CH_78 Crop: Forage/Pasture PIEDMONT Field: Field 2 Conducted By: GC Murray Coordinates: 35.6159 N Date: 12/6/2019 -79.3664 W Soil Series: Cid/Lignu m ASSOCIATE:. P• w. a, a w a ua w a d = V w W N i N H 3 d CCn N 7C d d d 3 7 3 C U t K i i U N p y cC r n S O S O S O a O S fY S n n 0 l0 n S n n Ap 0-5 10YR 3/3 - - - - moist sil mod med gr fr ns n E 5-11 10YR 6/3 - - - - moist sil mod med gr fr ns np Bt 11-25 10YR 5/8 10YR 6/6, 10YR 7/11 few I med I C&D I moist sic I mod I med I sbk I vfi I vs I vp BC 25-32 10YR 5/8 - - - - moist sicl mod med sbk fi s CR 32 - - - - - - - - - - - - - Legend: Texture s sand I loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam sicl silty clay loam Seasonal High Water Table: Structure Grade Structure Type Structure Size Depth (") Type (apparent/perched) wk weak gr granular f fine 19 perched m moderate pl platy med medium str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky Moist Consistency sg single grained fr friable ma massive Or very friable fi firm vfi very firm Soil Profile Descriptions in Field Locations Project: Synagro Harnettt Co. (WQ 0007066) % Slope: 3% Site: CH_78 Crop: Forage/Pasture Field: Field 3 Conducted By: GC Murray Coordinates: 35.6145 N Date: 12/6/2019 -79.3725 W Soil Series: Cid/Lignum O O v O O _ •= U V O X G! T f•1 S S PIEDMONT ASSOCIATES, P. A. = 00 3 W Q OC � W N N d H m h N G! G! O O S S C x O fY O S x ` w fn v fA O +3+ fA = o r O S Ap 1 0-6 1 10YR 3/3 1 moist sil I mod I med gr fr ns n E 1 6-11 1 10YR 6/3 1 - 4 - - - moist I sil ! mod I med I gr I fr ns np Bt 11-19 10YR 5/8 10YR 6/6, 10YR 7/1 few med C&D moist sic mod med sbk fi s p CR 20 - - - - - - - - - - - - - Legend: I loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam sicl silty clay loam Structure Grade Structure Type wk weak gr granular m moderate pl platy str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky sg single grained ma massive Seasonal High Water Table: Structure Size Depth (") Type (apparent/perched) f fine 14 perched med medium soft f Moist Consisten G fr friable a T vfr very friable v� fi firm fi F� 12" AKW"" vfi very firm Soil Proirle Descriptions in Field Locations Project: Synagro Harnettt Co. (WO 0007066) % Slope: 3% Site: CH_78 Crop: Forage/Pasture � PIEDMONT Field: Field 5 Conducted By: GC Murray Coordinates: 35.6768 N Date: 12/6/2019 ENVIRONMENTAL -79.3734 W Soil Series: Georgeville/Tarrus w s so c I w To s. P. A. w C O C) O C) J Q W N fn L O V y I l 1 i 0 O U) _ N w ` G7 O C 3 V V 41 V 41 C V i+ O 07 ca O O O N y 3 N H Ap 0-7 10YR 3/3 - - - - moist sil mod med gr fr ns np AB 7-13 10YR 6/3 - - - - moist sil mod med gr fr ns n Bt I 13-33 12.5YR 5/8I - I - I- I- I moist I c I mod I med ] sbk I fi I s I p ] ] BC I 33-39 12.5YR 5/8I - I - I- I - I moist I sicl I wk I med I sbk I fi I s I p I C 139-48 12.5YR 5/81 - 1 - 1- 1 - I moist I sil I wk I med I sbk I fi I s I p I Legend: Texture s sand I loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam sicl silty clay loam Structure Grade Structure Type Structure Size wk weak gr granular f fine m moderate pl platy med medium str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky Moist Consistency sg single grained fr friable ma massive vfr very friable fi firm vfi very firm Seasonal High Water Table: Depth (") Type (apparent/perched) NCDA&CS f - inomic Division Phone: (919) 733-2655 Website: www,n- ,gr.gov/agronomi/ Report No. Fi _j-SL019874 Client: f,f Heavy Metals Bobby Branch 284 Boger Rd Advisor: Bobby Branch 284 Boger Rd Mocksville, NC 27028 Mocksville, NC 27028 Soil Report Mehlich-3 Extraction Sampled County: Chatham -- - -- - _ Client ID: 505064 Advisor ID: 505064 Sampled: 12/06/2019 Received: 12/19/2019 Completed: 01/03/2020 Farm: CH-78 Agronomist's Comments: This report contains both routine soil test information as well as heavy metalsdata in a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a soil test extractant, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead (Pb)- 4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007). Although the above metals here are not believed to pose a concern for plant growth, continue to monitor these and note where elevated above background levels. Note any lime and fertilizer recommendations. Where soil test phosphorus (P) is very hi h P-I a 100),crops will not respond to additional P applied. Ja athi Kamalakanthan 1 /3/2020 Sample ID: 78-01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/rim, M 0.6 120-200 90 30 0 0 0 0 0 0 Note: 12 2-Fescue/OGrass/rim, M 0.0 120-200 90 30 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS4 NO3-N 0.09 0.91 5.2 77 1.2 5.3 22 57 48 23 48 97 75 75 27 27 76 0.2 4 Heavy Metals (parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.3 Chromium, 0.1 Lead, 2.2 Selenium, 0.0 Sample ID: 78-02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 2.4 120-200 140 100 0 0 0 0 0 0 2- Fescue/OGrass/Tim, M 0.0 120-200 140 100 0 0 0 0 0 0 Test Results [units - WN i n g/cm3; CEC and N a i n meq/100 cm3; NO3-N in mg/dm): Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS4 NO3-N 0.32 0.92 5.2 34 3.4 4.5 4 20 18 14 56 67 57 57 135 135 30 0.3 6 Heavy Metals (parts per million): Arsenic, 0.0 Cadmium, 0.0 Nickel, 0.4 Chromium, 0.1 Lead, 2.0 Selenium, 0.0 North Carolina A Tobxco Trust Find Ctmmmwon Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler• Commissioner of Awiculture NCDA&CS A,,_.momic Division Phone: (919) 733-2655 Website: www.i._-gr.gov/agronomi/ ReportNo. Fl .,,-SL019874 Bobby Branch Page 2 of 3 Sample ID: 78-03 Recommendations: Lime Nutrients (lb/acre) More Crop (Eons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 1.1 120-200 110 110 0 0 0 $ 0 0 Note: 12 Note: 2 -Fescue/OGrass/Tim, M 0.0 120-200 110 110 0 0 0 $ 0 0 Note 12 Note: Test Results [units -WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drn ): Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn,AI Cu-I Na ESP SS4 NO3-N 0.09 0.98 5.3 68 1.7 5.0 13 16 45 22 62 80 65 65 16 16 81 0.4 8 Heavy Metals (parts per million); Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.3 Chromium, 0.1 Lead, 2.9 Selenium, 0.0 Sample ID: 78-0 5 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 50 0 0 0 0 0 0 2- Fescue/OGrass/Tim, M 0.0 120-200 0 50 0 0 0 0 0 0 Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3): Soil Class: Mineral HM% WN CEC BS% Ac pH P4 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS4 NO3-N 0.46 0.75 8.9 87 1.1 6.0 207 46 65 20 39 212 144 144 463 463 571 0.2 2 Heavy Metals (parts per million): Arsenic, 0.2 Cadmium, 0.1 Nickel, 0.4 Chromium, 0.2 Lead, 5.2 Selenium, 0.1 Waypointo ANALYTICAL 6/10/2020 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 20-156-0005 Project Description: Bobby Branch 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 6/4/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated, Ceitain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 4O., [4'�y Pauric McGroary Agronomist Laboratory's liability In any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis In question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-156-0005 Client Project Description: Bobby Branch Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 72569 1 Solids 06/04/2020 SW-7471B WP MTN 72570 2 Solids 06/04/2020 SW-7471B WP MTN 72571 3 Solids 06/04/2020 SW-7471B WP MTN 72572 4 Solids 06/04/2020 SW-7471B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 8 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271.6446 www.waypointanalytical.com Mary Brewer Project Bobby Branch Report Date : 06/10/2020 284 Boger Road Information : Received : 06/04/2020 Mocksville , NC 27028 Report Number: 20-156-0005 REPORTOFANALYS7S Pauric McGroary Agronomist Lab No : 72569 Matrix: Solids Sample ID : 1 Sampled: Test Results Units MQL DF Date t Time By Analytical Analyzed Method Mercury 0.0201 mg/Kg 0.0148 1 06/09/2012:44 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 3 of 8 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Mary Brewer Project Bobby Branch Report Date : 06/10/2020 284 Boger Road Information : Received : 06/04/2020 Mocksville , NC 27028 Report Number: 20-156-0005 REPORT OFANALYSIS Pauric McGroary Agronomist Lab No : 72570 Matrix: Solids Sample ID : 2 Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0279 mg/Kg 0.0156 1 06/09/2012:46 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 4 of 8 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical 7621 White pine Road, Richmond, VA 23237 Main 804-743-9401 1 Fax 804-271.6446 www.waypointanalytical.com Mary Brewer Project Bobby Branch Report Date : 06/10/2020 284 Boger Road Information : Received : 06/04/2020 Mocksville , NC 27028 Report Number : 20-156-0005 REPORT OFANALYS7S Pauric McGroary Agronomist Lab No : 72571 Matrix: Solids Sample ID : 3 Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0187 mg/Kg 0.0156 1 06/09/2012:47 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quantitation Limit Page 5 of 8 Waypointo ANALYTICAL 46622 Synagro Central LLC/ Technical 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Mary Brewer Project Bobby Branch 284 Boger Road Information Mocksville , NC 27028 Report Number: 20-156-0005 Lab No : 72572 Sample ID: A, 5 Test Mercury REPORT OPANAL YUS Results Units 0.0352 mg/Kg MQL 0.0151 Report Date : 06/10/2020 Received ; 06/04/2020 Pauric McGroary Agronomist Matrix: Solids Sampled: DF Date / Time By Analytical Analyzed Method 1 06/09/2012:48 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quandtation Limit Page G of 8 Air WaypNALYTICAL 7621 Whltepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Shipment Receipt Form Customer Number: 46622 Customer Name: Synagro Central LLC/ Technical Report Number: 20.156-0005 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other: is UPS 0 Client 0 Courier Thermometer ID: Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No I. Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes I. No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes I. No Water - Sample containers properly preserved 0 Yes 0 No I. N/A Water - VOA vials free of headspace 0 Yes 0 No I. N/A Trip Blanks received with VOAs 0 Yes 0 No I. N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No I. N/A High concentration container (48 hr) F Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) r Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes No Comments: I Signature: [Brandi Watson 1 Date & Time: 06/04/2020 09:50:09 Page 7 of 8 Waypointo ANALYTICAL Illl►Ilil�llillflll>rlNl�l��ll�llalll�fllulll� Synagro Cenho. j I account Grower/Project Information w_� V iformation 3- c 66 �� �� � SUbrritled By Charge To Farm ID IField ID I r�Ucicc-v €�� OJ C_ Z�0 ZQ Credit Card # CSV I I Exp. Date: / Phone # 3 3 (� �, L% E-mail address C Vj I v'At- cP Sy rna-1 w - C4 Crop Info For Recommendations Sample ID Lab Number 'S2NI - Specify Additional Tests Soluble Additional Intended Yeld Altemative (Lab Use S1M ^^- c 7n S3M Salts Texture NO;-N Tests Crop I Goal Crop Lab# E 72569-1 1 — Lab# E 72571-1 3 Cust: 46622 Synagro Central LLC/ Technical Cot: - Cust: 46622 Synagro Central LLC/ Teclirncal 20-156-0005 Rec: 06/04/2020 00:00 Col: 06/04/2020 00:00 Preservation: _ 20-156-0005 Preservation: I r Lab# E 72570-1 2 — — Lab# E Cust: 46622 Synagro Central LLC/ Technical Cust_u 72572-I 4 465 Col: Rec: 06/04/2020 00:00 Col: SMagro Central LLC/ Te�ni 20-156-0005 Preservation: � — ',56-0005 P aRec:06/pq/2020 i 'bon: 00:00 I Mehlich III Test Packages Special Instructions or .31 Tests Yield Goal Previous Crop Z 5 S1 M - Organic matter, Phosphorus, Potassium, Calcium, Magnesium, pH, Buffer pH Cation Exchange Capacity, and % Base Saturation. S2M - Test S1 M plus any two of the following: Sodium, Sulfur, Boron, Zinc, Manganese, Iron, Copper. Each additional test (above mo) cost S2.00. S3M - Test S1M plus Sodium, Sulfur, Boron, Zinc, Manganese, Copper, and Iron. I _ l _ C r �k e t-( y VICINITY MAP 1�WaAa p "'WHd Z pg4.W1 ('.nwc4 /W �71) � 117d {j h j r I fJzl ,ht111�^Htl 1 ]]: '•k Vgnrpt BgslrptRd ' .r IXdve Ad IWnlee url Bonlee E1 113fi • 1 Lx�S ,1 ]3 1rl 76 , fl„n14L fell n a s VA OI 907 �a x 17,78 nv�ld 100 peo"�'ka CfrurrhlldF K 51 1141 Hear Creek lix lii 7s� ^ GRAPHIC SCALE 111 = 5,000' 5,000' 0 5,000' The compliance boundary is established either 250 R from the residuals application area or 50 feet within N C-C H-73 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Field 10 APPLICATION MAP i P:nrwn APPLICATION AREA — —�— — — — PRIVATE ROAD STREAM DRAIN . FENCE PROPERTY LINE 0 UNSUITABLE AREA WATER ONSITE HOUSE OFFSITE HOUSE OUTBUILDING WELL The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 1"=660' ssoa o sso' NC-CH-73 Field 10 TOPOGRAPHIC MAP A ry z ids i GRAPHIC SCALE 1"=800' 800' 0 800, The compliance boundary is established either 250 ftfrom the residuals application area or 50 feet within N C-CH-73 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area, All locations are approximate, Field 10 Ix I0 4 z SOIL SURVEY N-- GRAPHIC SCALE 1" = 1,000' 1,000- 0 1,000, The compliance boundary Is established either 250 ft from the residuals application area or 50 feetwithin NC-CH-73 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area, All locations are approximate. Field 10 41AIR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 —LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and sporting documentation For more information, visit the Water Quality Permitting Section's Nora -Discharge Permitting Unit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or othertype residuals) in accordance with 15A NCAC 02T .1 100. Do not submit this agreement f'or review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Synagro Western Piedmont RLAP hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Sou rce (optional) Special note (no-till/over-seed/ Pasture) NC-CH-73-10 N Pasture Hay The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page i of 3 I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity fbr the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 11) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDL-NR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Perrnittee must request and obtain a permit modification fi•om the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules fbr typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable fbr the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10, The landowner or his representative will provide the Permittee with in formation regarding the amount and analysis of other sources of nutrients (e.g., fertil izer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13, The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. 11. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and fbr the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites thatare to be used for grazing shall have Fencing that will be used to prevent access duringthese periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested fora 20-month period lollowing a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the landshall not be harvested fora 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. I It. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105 h 7 allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance bounda►y is needed for field(s) ID: (Please include the rationale fbrthe requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. IV, ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the I ield(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) { ()TlNA, T C)A 0A_1(, Dana') nf`3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that l have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein, Landowner name: Address: 43 t✓IN /e'e/ «� City: /Yf 6tr,de, State: N Phone:, -E-mail address:___ Signature: Date: NORTH CAR NA, COUNTY zip: li�7 _;_20 7) �2J I, the undersigned Notary Public do hereby certify that��� personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the . I ALenv k day of Signature and seal: /Z'V'v`L;- My commission expires: L 61 Lessee's/Operator's Certification: ,20Z0 ROBERT N. ROTH GUILFORD COUNTY STATE OF NORTH CAROLINA certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail address: Date: Zip: 1 certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: Q/j 0 1� — _. Signature: / 1 X! / Date: I2�/ FORM: LOA 06-16 Page 3 of 3 SYNAGRO, HARNETT COUNTY CLASS B PERMIT WQ 0007066 SOIL SCIENTIST CERTIFICATION This is to certify that soil profile evaluations were conducted on the proposed application sites for the Harnett County project by Piedmont Environmental Associates, P.A. on behalf of Synagro Central, LLC. The evaluations consisted of hand auger borings and descriptions of the soils on the application sites. All hand auger borings included in this package were either performed by me or under my direct supervision. All other work performed for this permit application was conducted by Synagro Central, LLC. G. Christopher Murray, L.S.S. No. 1284 Synagro, Harnett County WUVTP Project, Various Fields Soil Profile Descriptions in Field Locations Project: Synagro Harnettt Co. (WQ 0007066) % Slope: 2% Site: CH_73 Crop: Forage/Pasture Field: Field 10 Conducted By: GC Murray Coordinates: 35.6669 N Date: 12/6/2019 -79.4648 W Soil Series: Georgeville a� H H o � m v _O O � N _ = O U O U Q 4 N O U y N r+ X w N r T x n F. F.F.S.-N S I ~AT Ass O c I Arcs, P. A. w N } � U H H C N O V 'W ,DUI V V N O Y v A rn rn rn S n n A 0-5 10YR 3/3 - - - - moist sit mod I med r fr ns np AB 5-14 10YR 6/3 - - - - moist sil mod med gr fr ns np Bt 14-48 1 2.5YR 4/81 1- - -1 moist I c I mod med I sbk I fi I s p Legend: I loam si silt sil silt loam c clay cl clay loam scl sandy clay loam sl sandy loam sicl silty clay loam Structure Grade Structure Type wk weak gr granular m moderate pl platy str strong pr prismatic cpr columnar abk angular blocky sbk subangular blocky sg single grained ma massive Seasonal High Water Table: Structure Size. Depth (") Type (apparent/perched) f fine - med medium S014 OP HE Moist Consistency fr friable 0 vfr very friable fi firm y'F vfi very firm NCDA&CS Ay-. nomic Division Phone: (919) 733-2655 Website: www.i._ _gr.gov/agronomi/ Report No. F , _ ,-SL019873 Client: Synagro Advisor: Synagro Heavy Metals Synagro Synagro 284 Boger Rd. 284 Boger Rd. Soil Report Mehlich-3 Extraction Mocksville, NC 27028 Mocksville, NC 27028 :�..41 Sampled County : Chatham Links to Helpful Ir - - - Client ID: 503079 Advisor ID: 503079 Sampled: Received: 12/19/2019 Completed: 01/03/2020 Farm: Agronomist's Comments: This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals under soil test lab results. Using Mehlich 3 as a soil test extractant, background levels of these metals typically seen in NC soils when analyzed are as follows: arsenic (As)- 4.5 ppm, cadmium (Cd)- 0.1 ppm, chromium (Cr)- 0.2 ppm, lead (Pb)- 4.2 ppm, nickel (Ni)- 0.8 ppm, & selenium (Se)- 0.2 ppm (FY2005-2007). Although the above metals here are not believed to pose a concern for plant growth, continue to m nitor these and note where elevated above background levels. Note any lime and fertilizer recommendations. Jagathi Kamalakanthan 1 /3/2020 Sample ID: 73-1.0 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M 0.4 120-200 100 20 0 0 0 0 0 0 2- Fescue/OGrass/Tim, M 0.0 120-200 100 20 0 0 0 0 0 0 Test Results [units - WN i n g/cm3; CEC and N a i n meq/100 cm3; NO3-N i n mg/dm3 : Soil Class: Mineral HM% WN CEC BS% Ac pH Pg K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS4 NO3-N 0.27 0.79 10.6 87 1.4 5.8 16 65 54 29 83 244 163 163 201 201 146 0.1 1 Heavy Metals (parts per million): Arsenic, 0.0 Cadmium, 0.1 Nickel, 0.3 Chromium, 0.1 Lead, 2.1 Selenium, 0.1 North Caro;'..: 71 Reprogramming oft he laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Aprrculture Waypoint ANALYTICAL 6/10/2020 Synagro Central LLC/ Technical Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 20-156-0004 Project Description: Doug Ellis 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 6/4/2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Resultsfor solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist L.aboratay's liablilly in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratay's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 5 Q) Waypoint. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401° Fax 804-271.6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 20-156-0004 Client Project Description: Doug Ellis Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 72568 10 Solids 06/04/2020 SW-74716 WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 5 Waypoint ANALYTICAL 46622 Synagro Central LLC/ Technical 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypoiiitaiialytical.com Mary Brewer Project Doug Ellis Report Date : 06/10/2020 284 Boger Road Information : Received : 06/04/2020 Mocksville , NC 27028 Pam« mG ��►� Report Number :20-156-0004 REPORT OFANAL YSIS Pauric McGroary Agronomist Lab No : 72568 Matrix: Solids Sample ID : 10 Sampled: Test Results Units MQL DF Date / Time By Analytical Analyzed Method Mercury 0.0375 mg/Kg 0.0154 1 06/09/2012:43 DDB SW-7471B Qualifiers/ DF Dilution Factor L Limit Exceeded Definitions MQL Method Quandtation Limit Page 3 0£ 5 Wayppint.0AYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www_waypointanalytical.com Shipment Receipt Form Customer Number: 46622 Customer Name: Synagro Central LLC/ Technical Report Number: 20-156-0004 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other: is UPS 0 Client 0 Courier Thermometer ID: ; Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? is Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 -- compliance criteria met 0 Yes 0 No N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: IBrandi Watson ] Date & Time: 06/04/2020 09:49:22 Page 4 of 5 Waypoeint ANALYTICAL • SOIL ^""" 7E sLLCF Teciu466622 ub�i�w�iwi�wi�wi�iw douo Ent 2020 c9:4s 24 Account # Grower/Project Information on 5ubminea rsy Charge To p�14 s J I �ILr15 �V tiK'r Farm ID GN-� 3 Field ID IJC- 27 D 2- Credit Card # CSV Exp. Date: Phone # 3 (s 11) Z E-mail address I G �.,, i v, c, try 5-1 t q'� C 0 " Crop Info For Recommendations Sample ID Lab Number (Lab Use Only) SW S21VI - Specifjlrl Additional Tests S3M Soluble Salts Texture NO3-N Additional Tests Intended Crop Yield Goal Attemative Crop Yield Goat Previous Crop B Cu Fe Mn Na S Zn I Lab# E 72568-1 10 Cust: 46622 synagro central u.CJ Technical Col: Rec: 06/04/2020 00:00 20-156-0004 Prese^vab°n'. i -- - Mehlich III Test Packages Special Instructions or Additional Tests S1M - Organic matter, Phosphorus, Potassium, Calcium, Magnesium, pH, Buffer pH Cation Exchange Capacity, and % Base Saturation. S2M -Test S1M plus ary two of the follovAng: Sodium, Sulfur, Boron, Zinc, Manganese, Iron, Copper. Each additional test (above two) cost S2.00. S3M - Test S 1 M plus Sodium, Sulfur, Boron, Zinc, Manganese, Copper, and Iron. i l 1 !!! North Carolina Department of Environmental Quality Pat McCrory Donald R. van der Vaart Governor Secretary Date: 5/21/20 To: Name of Chairman to the Board of County Commissioners: MARK{ F. RICHARDSON Complete mailing address: PO Box 101 City: Wentworth State: NC Zip: 27375- County where land application sites are located: Rockingham From: Applicant's name: Synagro Western Piedmont RLAP (on behalf of the Division of Water Resources in accordance with Session Law 2013-340) Contact person and title: Nate Roth, Technical_ Services Manager Complete mailing address: 284 Boger Rd, City: Mocksville State: NC Zip: 27028-" Telephone number: (336) 790-1610 E-mail address: i•roth@syna rg o.com Subject: Notification of residual land application site proposal This is to notify you that the Applicant listed above will be submitting an application to the Division of Water Resources for the land application of residual solids to site(s) located in your county. During this review, the Division will ensure that all federal and state regulations are enforced. Attached to this form is information regarding residuals - generating sources and locations of the proposed land application sites. Please forward this letter and its associated attachments to the appropriate Department within your County (i.e., Health or Environmental Health Department and Planning Department) if applicable. More information of the land application sites included in this application will be available at the following Division of Water Resources Regional Off ice: Name of appropriate regional office: Winston Salem Re ional Office Complete inailing address: 450 West Hanes Mill Road, Suite300 City: Winston Salem State: NC Zip: 27105- Telephone number: 336) 776-9800 Expected date of application submission: 1 Should you desire to comment on this application, please do so no later than 30 calendar days following the expected application submission date. If you have any questions or comments about this notification, or if you would like more information, please contact the appropriate regional office at the telephone number provided above. Thank you in advance for your attention to this matter. Enclosures: Source Facility Summaiy Land Application Site Suininary Maps Non-Dischaige Pennitling Unit 1617 Mall Service Center, Raleigh, Nodh Carolina 27699-1617 Phone; 919-807-64641 Internet: hitpalpooal.ncdenr.ora7webhua An Equal Oppoilunily%AKrmativeAclionEmployer -Made in pail with recycled paper FORM: CBN 06-16 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name_ J'-agr'o'Western Piedmont RLA.P Status Codea Facility Permit holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed N Town of Mayodan Mayodan WWTP Rockingham NC00218ri 0 315 E Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page I LAND APPLICATION SITE CERTIFICATION Applicant's name: Slna_¢ro Western PiedmontRLAP Land application sites currently certified: 813.6 net acres and Total to be certified: 64.5 Mayodan net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Code' Site/Field ID Landowners () Lessee(s)or O s Operator(s) () Net Acres CountyCrop(s ) Predominant Soil b Mapping Unit Series Name or Rep. Slope' N RC-49-01 Ann Purgason Jim Goodwin 21.2 Rockingham Ps'r Clifford CgB2 N Bennett Farms LLC Jim Goodwin :0.7 Rockinghamg Clifford CgB2 N k(fz9-03° Bennett Farms LLC Jim Goodwin 7.4 Rockingham Hay + Clifford CgB2 N RC-49-04 Bennett Farms LLC Jim Goodwin 10.7 Rockingham Hay Clifford CgB2 I N RC-49-05 Bennett Farms LLC Jim Goodwin 8.7 Rockingham Row Crop Clifford CgB2 N RC-49-06 Bennett Farms LLC Jim Goodwin 5.8 Rockingham Hay Clifford CgB2 N E: M N j= l,YAM z Status Code for land application sites are: + N (New) ♦ R (Renewed) + M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) Mapping unit must be consistent with those used in the County Soil Survey (i.e_ fora 2-8% slope Cecil in Anson County the mapping unit is CeB2) II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Location Method Code Location Accuracy Waterbody Subbasin and Current and Proposed Datum Stream index No. 1 Class RC-49-01 §,6A4° 17' 22" 79�� 57' 26" NAD 83 ADD Nearest Second Little Hogans Creek, 22-31-1 C C NO '�l'l 36° 17' 22.42" 79- 57' 6.7" NAD 83 ADD Nearest Second Little Hogans Creek, 22-31-1 C C - ; 3'6- 17'22.3" T9° 56' 54.4" NAD 83 ADD NearestSecond Little Hogans Creek, 22-31-1 C C RC-49-04 36- 17' 17.8" 79° 56' 53.9" NAD 83 ADD Nearest Second I Little Hogans Creek, 22-31-1 C C RC-49-05 36° 17' 12.5" ° 57' 6.2" NAD 83 ADD Nearest Second Little Hogans Creek, 22-31-1 C C RC a9 06 36" 17' 23" 790 57' 12.7 NAD 83 ADD Nearest Second Little Hogans Creek, 22-31-1 C C r NAD $3 ADD Nearest Second NAD 83 ADD Nearest Second OHIO Note: Please keep the site information (I.) and waterbody information (1L) of the same field on the same page_ FORM: LASC 06-16 Page I VICINITY MAP GRAPHIC SCALE 1" ^ 4,000' 4,000' 0 4,000' The complianceboundaty is established either 250 fl from the residuals application area or 50 feelwilhin In the property boundary, whichever Is closest to the appllcatlon area. The review boundary Is established midway between the compliance boundary and the perimeter of the residuals application area, All locations are approximate, N C- RC-49 Fields 1-6 Proof of Delivery Dear Customer, This notice serves as proof of delivery for the shipment listed below, Tracking Number 1Z51F76W0105526616 service UPS Next Day Air®j )elivered On 07/17/2020 10:13 A.M. Delivered To STOKESDALE, NC, US Weight 0.50 LBS Shipped / Billed On 07/16/2020 Left At Front Door Thank you for giving us this opportunity to serve you. Details are only available for shipments delivered ~within the last 120 days. Please print for your records if YOU require this information after 120 days. Sincerely, UPS Tracking results provided by UPS: 07/17/2020 10:54 A.M. EST Print this page North Carolina Department of Environmental Quality Pat McCrory Donald R, van der Vaart Governor Secretary Date: 6/26/2020 To: Name of Chairman to the Board of County Commissioners: Howard L. Penny Complete mailing address: PO Box 736 City: Coats State: NC Zip: 27521- County where land application sites are located: Harnett From: Applicant's name: Synagro Western Piedmont RLAP (on behalf of the Division of Water Resources in accordance with Session Law 2013-340) Contact person and title: Chris Wynne, Technical Services Specialist Complete mailing address: 284 Boger Rd. City: Mocksville State: NC Zip: 27028 Telephone number: 336909-8627 E-mail address: ewynne n,syna rg a.com Subject: Notification of residual land application site proposal This is to notify you that the Applicant listed above will be submitting an application to the Division of Water Resources for the land application of residual solids to site(s) located in your county. During this review, the Division will ensure that all federal and state regulations are enforced. Attached to this forth is infbrmation regarding residuals - generating sources and locations of the proposed land application sites. Please forward this letter and its associated attachments to the appropriate Department within your County (i.e., Health or Environmental Health Department and Planning Department) if applicable. More information of the land application sites included in this application will be available at the following Division of Water Resources Regional Office: Name of appropriate regional office: Fayetteville Regional Office Complete mailing address: 225 Green St, Suite 714 City: Fayetteville State: NC Zip: 28301- Telephone number: (910) 433-3300 Expected date of application submission: 6/26/20 Should you desire to comment on this application, please do so no later than 30 calendar days following the expected application submission date. If you have any questions or comments about this notification, or if you would like more information, please contact the appropriate regional office at the telephone number provided above. Thank you in advance for your attention to this matter. Enclosures: Source Facility Summary Land Application Site Summary Maps Non -Discharge Permitting Unit 1617 Mail Service Center, Raleigh, Nodh Carolina 27699.1617 Phone: 919.807-6464 t Internet: htta:/lrwrtal.ncdenr.oM1weh/wa An Equal Opporlunity t Affirmative Action Employer —Made in pat wilh recycled paper FORM: CBN 06- l6 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Synagro Western Piedmont, LLC Status a Code Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current Proposed N Harnett County Utilities North Harnett Regional WWTP Harnett NCO021636 0 1500 8 Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e. not applicable to new facility). SUMMARY FOR FORM_ RSC 06-16 Page 1 LAND APPLICATION SITE CERTIFICATION Applicant's name: Svnaaro Western Piedmont RLAP Land application sites currently certified: 813.6 net acres and Total to be certified: 44.4 Harnettnet acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Site/Field Code" ID Landowner(s) Lessee(s) or Operator(s) Net Acres County Crop(s) Predominant Soil Series Name Mapping Unit or Rep. Slope` N HA-47-1 James W. Pope James W. Pope 19.2 Harnett Pasture Aycock AyA N HA-47-2 James W. Pope James W. Pope 9.9 Harnett Pasture Aycock AyA N HA-47-3 James W. Pope James W. Pope 11.0 Harnett Pasture Aycock AyB N HA-47-4 James W. Pope James W. Pope 4.3 Harnett Pasture Aycock AyB Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) 'Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed p Class HA-47-1 350 34' 41" 780 74' 88" NAD 83 ADD Nearest Second Second Silver Run, 18-20-33-1 WS-Iv WS-Iv HA-47-2 350 20' 52" 780 44' 55" NAD 83 ADD Nearest Second Second Silver Run 18-20-33-1 WS-Iv WS-Iv HA-47-3 350 34' 97" 780 74' 70" NAD 83 ADD Nearest Second Cape Fear River, 18-(16.7) WS-Iv WS-1v HA-47-4 350 35' 22" 780 74' 67" NAD 83 ADD Nearest Second Cape FearRiver, 18-(16.7) WS-Iv WS-1v Note: Please keep the site information (I.) and waterbody information (11.) of the same field on the same page. FORM: LASC 06-16 Page 1 VICINITY MAP r \"*� f 1a .� V� 1 GRAPHIC SCALE 1" = 4,000' 4,000' 0 4,000' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-HA-47 Fields 1-4 Tracking Number: 70200090000151709551 Status Your item was picked up at the post office at 3:60 pm on @r Delivered July 7, 2020 in COATS, NC 27521. J* 7. 2020 a13.50 pm OeWemed. IrrdiMwl Picked Up st Post Office COATS, NC 2752% Get Updates v Text & Email Updates Tracking History Product Information See Less ^ Delivered Reprove X North Carolina Department of Environmental Quality Pat McCrory Donald R. van der Vaart Governor Secretary Date: 7/6/2020 To: Name of Chairman to the Board of County Commissioners: Karen Howard Complete mailing address: PO Box 1809 City: Pittsboro State: NC Zip: 27312- County where land application sites are located: Chatham From: Applicant's name: Synagro Western Piedmont, LLC (on behalf of the Division of Water Resources in accordance with Session Law 2013-340) Contact person and title: Chris Wynne Complete mailing address: 284 Boer Rd. City: Mocksville State: NC Zip: 27028 Telephone number: 336 909-8627 E-mail address: cwynncta`e,synagro.cotn Subject: Notification of residual land application site proposal This is to notify you that the Applicant listed above will be submitting an application to the Division of Water Resources for the land application of residual solids to site(s) located in your county. During this review, the Division will ensure that all federal and state regulations are enforced. Attached to this form is information regarding residuals - generating sources and locations of the proposed land application sites. Please forward this letter and its associated attachments to the appropriate Department within your County (i.e., Health or Environmental Health Department and Planning Department) if applicable. More information of the land application sites included in this application will be available at the following Division of Water Resources Regional Office: Name of appropriate regional office: Raleigh Regional Office Complete mailing address: 3800 Barrett Drive City: Raleigh State: NC Zip: 27609- Telephone number: (919) 791-4200 Expected date of application submission: 7/13/2020 Should you desire to comment on this application, please do so no later than 30 calendar days following the expected application submission date. If you have any questions or comments about this notification, or if you would like more information, please contact the appropriate regional office at the telephone number provided above. Thank you in advance for your attention to this matter. Enclosures: Source Facility Summary Land Application Site Summary Maps Non -Discharge Permitting Unit 1617 Mall Service Center, Raleigh, North Caiolina 27699-1617 Phone: 919-807.6464 l Internet: http:l/podal._n_cdenr.orglwebAN An Equal Oppodunily k Affirmalive AM n Employer — Made in part with recycled pa per FORM: CBN06-16 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Suynagro Western Piedmont, LLC Status Codes I Facility Permit Holder � Facility Name County Permit Number Maximum Dry Tons Per Year Current n Proposed N Harnett County Utilities North Harnett Regional WWTP Harnett NCO021636 0 1500 N Town of Siler City Siler City WWTP Chatham NCO026441 0 1325 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently pennitted fbr distribution, Iand application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 LAND APPLICATION SITE CERTIFICATION Applicant's name: Synam Western Piedmont RLAP Land application sites currently certified: 813.6 net acres and Total to be certified: 268.7 Chatham net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Code' Site/Field ID Landowners I () Lessees or Operator(s) () Net Acres Count Y Crop(s) s P() Predominant Soil Series Name b Mapping Unit or Rep. Slope° N CH-78-1 Bobby Branch 66.4 Chatham Pasture Cid-Lignum CmB N I CH-78-2 Bobby Branch 40.7 Chatham Pasture Cid-Lignum CmB N I CH-78-3 Bobby Branch 57.6 Chatham Pasture Cid-Lignum CmB N I CH-78-5 Bobby Branch 65.5 Chatham I Pasture Georgeville GeB2 N CH-73-16 Doug Ellis 38.5 Chatham Hay Georgeville GeB2 Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) OM(Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) H. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy L Waterbody Subbasin and Stream Index No. Current and Proposed Class CH-78-1 1 350 37' 13.5" f 79° 21' 46.7" NAD 83 ADD Nearest Second Sandy Branch, 17-43-16-1 C C CH-78-2 350 36' 53.3" 790 22' 21.7" I NAD 83 ADD Nearest Second Sandy Branch, 17-43-16-1 C C CH-78-3 1 350 37' 11.9" 79- 22' 7" NAD 83 ADD Nearest Second Sandy Branch, 17-43-16-1 C C CH-78-5 350 40' 27.9" 790 22' 18.4" ! NAD 83 ADD Nearest Second I Tick Creek, 17-43-13 C C CH-73-10 350 40' 77" 790 27' 50.2" NAD 83 ADD Nearest Second Tick Creek, 17-43-13 C C Note: Please keep the site information (1.) and waterbody infonnation (II_) of the same field on the same page. FORM: LASC 06-16 Page 1 GRAPHIC SCALE T' = 4,000' ON' o a,000- The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CH-78 Fields 1-3,5 ��fCJrXGh i IJ t Jo6kjru�,y,3? $N d A c7� ecrfrr tt.� FIN 0 Vv; Fs CA-Ch4di VICINITY MAP 0 7 {1�FO L�nfreK'� FY�n�r. 11b; m Iva ttrs I Sa1 e r f1d^d. rt f 111 K-BE,n _ ID ' lll9 GRAPHIC SCALE 1" = 5,000' 510001 0 5,000' The compliance boundary is established either250 ft from the residuals application area or 50 feet within NC-CH-73 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Field 10 Tracking Number. 70192280000164349514 Status Your item was delivered at 10:42 am on July 9, 2020 in G Delivered PITTSBORO, NC 27312_ July 9, 2620 at 10:42 am Detrvered PTTTSBOAO. NC 27312 Get Updates v Dalivened Text & Email Updates Tracking History Product Information See Less ^ v v Remove X