Loading...
HomeMy WebLinkAboutWQ0000485_Monitoring - 03-2020_20200428 (2)V=1 April 20, 2020 VALLEY PROTEINS, INC. Division of Water Resources Attn: Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Ground Water Quality Monitoring Report (GWQMR) Valley Proteins Inc. — Rose Hill To whom it may concern, Please find enclosed the Groundwater Quality Monitoring Compliance Report for Surface Irrigation for the month of March 2020 for our Rose Hill Division. Should you require any additional information or wish to discuss this matter, please feel free to contact me at 910.289.2083 x 25119. Sincerely, Toby Schlink District Manager cc: VP Corporate Office Making a Sustainable Difference. APR 2 8 2020 IONI G'.'t:°?'A6TIC?1 PROCESSING UNIT 469 Yellow Cut Road Rose Hill, NC 28458 O 540.877.2590 • 866.558.0994 Transportation • 866.651.8175 valleyproteins.com SUBMIT FORM ON YELLOW PAPER ONLY • • •DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different). NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 12.46 ft. Well Diameter: 2 in. pH4500HB 5.00 units Temp. 000lo: 'b' °C DRY at Depth to Water Level 82546: 1.9 Screened Interval: 12.46 ft. to 2.46 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear checl] Samples for metals were collected unfiltered: X YES El NO and field acidified: X YES M NO here. LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.36 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.16 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 149.00 mg/L Al - Aluminum 01105 mg/L Sodium 6.24 mg/L pH (Lab) 00403 5.00 units Ba - Barium 01007 ug/L TOC oo68o 0.9 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 6 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 74 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N. Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Perrnittee (or Authorized Apent) Name and Title - Please print or Noe GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearty or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field El Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 31.00 ft. Well Diameter: 2 in. pH4500HB 7.40 units Temp. 000lo: 155 °C DRY at Depth to Water Level 82546: 10.3 ft. below measuring point Screened Interval: 30.15 ft. to 20.15 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur sampling, check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance None here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1.0 /100mL Nitrate (NO3) as N 00620 0.06 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.24 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 297.00 mg/L Al - Aluminum 01105 mg/L Sodium 11.1 mg/L pH (Lab) 00403 7.40 units Ba - Barium 01007 ug/L TOC oo68o 1.2 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 7 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH, as N, Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Permittee (or Authorized Accent) Name and Title - Please print or type GW-59 Rev.8/2013 SUBMIT FORM ON YELLOW PAPER ONLY • • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 28.93 ft. Well Diameter: 2 in. pH4500HB 7.60 units Temp. 000lo: 14.8 °C DRY at Depth to Water Level 82546: 3.5 ft. below measuring point Screened Interval: 28.93 ft. to 18.93 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Yellow / Tan Tint here: Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.73 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 217.00 mg/L Al - Aluminum oilo5 mg/L Sodium 8.62 mg/L pH (Lab) 00403 7.60 units Ba - Barium 01007 ug/L TOC 00680 <.5 mg/L Ca - Calcium oo916 mg/L Chloride 00940 <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 <5 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.8/2013 • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-s07-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7A Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.00 units Temp. 000lo: 15J °C DRY at Depth to Water Level 82546: 4.5 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 2.42 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Reddish Brown chec" Samples for metals were collected unfiltered: X YES NO and field acidified: X YES ❑ NO here: LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 0.7 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 173.00 mg/L AI - Aluminum o11o5 mg/L Sodium 17.3 mg/L pH (Lab) 00403 4.00 units Ba - Barium 01007 ug/L TOC oo68o <.5 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 62 mg/L Cd - Cadmium a1027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 20 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? p Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium oo937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 0.5 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Perntittee (or Authorized Agent) Name and Title - Please print or type • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: , • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 9194074306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name Field 5 - damaged by farm equip / to replace No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8A Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.40 units Temp. 000lo: 15.4 °C DRY at Depth to Water Level e2546: 5.1 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: ItMhos time of Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan Tint checlf—� Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO here:µ LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 1.33 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.34 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 78.00 mg/L Al -Aluminum oilo5 mg/L Sodium 2.02 mg/L pH (Lab) 00403 5.40 units Ba - Barium 01007 ug/L TOC 00680 0.60 mg/L Ca - Calcium 00916 mg/L Chloride oo94o <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 26 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 76732: method # SM 6200C Total Ammonia oo610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: Nljas N, Ammonia Nitrogen, Total) Mn - Manganese oio55 uglL , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Permiftee (or Authorized Agent) Name and Title - Please print or type • . • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print CleariyorType PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 13.73 ft. Well Diameter: 2 in. pH450oHB 5.90 units Temp. 0o01o: 13 °C DRY at Depth to Water Level 82546: 6.2 ft. below measuring point Screened Interval: 13.73 ft. to 3.73 ft. Spec. Cond. 00094: ]Mhos time of Measuring Point is 3.50 ft. above land surface Relative M.P. Elevation: ft. Odor 0006s: Sulfur sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Brown Tint checl� Samples for metals were collected unfiltered: X YES NO and field acidified: X YES El NO here:] LABORATORY INFORMATION Date sample analyzed: 3/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 0.04 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 1100mL Nitrate (NO3) as N 00620 <.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.34 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 219.00 mg/L Al - Aluminum 01105 mg/L Sodium 56.1 mg/L pH (Lab) 00403 5.90 units Ba - Barium 01007 ug/L TOC oo68o 53.0 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 9 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 20 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? []Yes (0) ❑ No (0) Specific Conductance 00095 ltMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo6lo 0.5 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NJ as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 1.8 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Toby Schlink - District Manager Pernittee (or Authorized Agent) Name and Title - Please print or type mg/L Effluent Total VOCs: mg/L VOC Removal% DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10A Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH45001­1e 4.90 units Temp. 000lt 13.9 °C DRY at Depth to Water Level 82546: 3.5 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Reddish Brown checlf—� Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0,02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.67 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 659.00 mg/L Al -Aluminum o1105 mg/L Sodium 98.2 mg/L pH (Lab) 00403 4.90 units Ba - Barium 01007 ug/L TOC owao 3.8 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 254 mg/L Cd - Cadmium 01027 ug/L Arsenic oloo2 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 108 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? p Yes (0) ❑ No (0) pecific Conductance 000ss uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 <.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nljas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.60 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Permittee (or Authorized Agent) Name and Title - Please print or type OUNDWATER QUALITY MONITORING: MPLIANCE REPORT FORM LITY INFORMATION Please Print Clearly or Type ty Name: Valley Proteins Inc.- Rose Hill it Name (if different): ty Address: 469 Yellow Cut Rd. Rose Hill, NC 28458 County Duplin act Person: Corey Lanier Telephone#: (910) 660-1173 Location/Site Name No. of wells to be sampled: 11 (from Permit) ION OF WATER RESOURCES - INFORMATION PROCESSING UNIT MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807.6306 on -Discharge UIC PDES Other fPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11A Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH45ooHB 5.10 units Temp. 000ic 15.4 °C DRY at Depth to Water Level 82546: 4.3 Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. Odor00065: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance White/Tan Tint checl� SamDles for metals were collected unfiltered: X YES rl NO and field acidified: X YES I-1 NO here: Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead 01051 Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.07 mg/L Zn - Zinc 01092 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.57 mg/L Certification No. DWQ#94 ug/L mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 492.00 mg/L Al - Aluminum 01105 mg/L Sodium 79.6 mg/L pH (Lab) 00403 5.10 units Ba - Barium 01007 ug/L TOC 00680 2.70 mg/L Ca - Calcium oo916 mg/L Chloride 00940 127 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo94s 167.0 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? p Yes (0) ❑ No (0) >pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia 00610 0.3 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, Ndas N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 0.7 mg/L Ni - Nickel 01067 ug/L method # DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM , • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill _ Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-12B Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB: 5.00 units Temp. 000lo: 16.5 °C DRY at Depth to Water Level 62546: 5.2 ft. below measuring point Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00065: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear checlf-1 Samples for metals were collected unfiltered: X YES M NO and field acidified: X YES M NO Ihere: LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N oo62o <,02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.55 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 797.00 mg/L Al - Aluminum 01105 mg/L Sodium 144 mg/L pH (Lab) 00403 5.00 units Ba - Barium 01007 ug/L TOC 00680 2.80 mg/L Ca - Calcium oo916 mg/L Chloride oog4o 188 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 281 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 <.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nfjas N; Ammonia Nitrogen, Total) Mn - Manganese wo55 ug/L , method # TKN as N 00625 0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Permittee (or Authorized Agent) Name and Tide - Please print or type DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM e , • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-607-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28468 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-13A Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in, pH4500HB 4.90 units Temp. 000lo: 15.9 °C DRY at Depth to Water Level 82546: 4.0 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. 00094: uMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance White/Tan Tint checlt-I Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N omi5 0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P oo665 0.44 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 64.00 mg/L Al - Aluminum 01105 mg/L Sodium 5.57 mg/L pH (Lab) oo4o3 4.90 units Ba - Barium 01007 ug/L TOC oo68o <.5 mg/L Ca - Calcium 00916 mg/L Chloride oog4o <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 12.00 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0) Specific Conductance 00095 uMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia oo610 <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NF`as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N oo625 <0.50 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Pennittee (or Authorized Agent) Name and Title - Please print or type • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: • • • • DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: 919407.6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00000485 Expiration Date: 3/31/2025 Facility Name: Valley Proteins Inc.- Rose Hill Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Rose Hill, NC 28458 County Duplin X Spray Field ❑ Remediation: Contact Person: Corey Lanier Telephone#: (910) 660-1173 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other: (from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-14A Date sample collected: 3/7/2020 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 5.20 units Temp. 000l( 15.3 °C DRY at Depth to Water Level 82546: 3.3 ft. below measuring point Screened Interval: 10 ft. to 2.5 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00065: None sampling, Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Brown Tint checl� Samples for metals were collected unfiltered: X YES NO and field acidified: X YES NO here: LABORATORY INFORMATION Date sample analyzed: 03/07/2020-03/27/2020 Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 1.81 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31MX /100mL Phosphorus: Total as P 00665 0.46 mg/L (Note: Use M PN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7o3oo 1180.00 mg/L Al - Aluminum oilm mg/L Sodium 155 mg/L pH (Lab) 00403 5.20 units Ba - Barium 01007 ug/L TOC oo68o 4.30 mg/L Ca - Calcium 00916 mg/L Chloride oog4o 339 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total wom ug/L Grease and Oils oo552 mg/L Cu - Copper o1042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 342 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: method # SM 6200C Total Ammonia omio <0.20 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; Nijas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 <0.5 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Toby Schlink - District Manager Pennittee (or Authorized Agent) Name and Title - Please print or type GW-59A COMPLIANCE REPOR'I' FORM Permit # W0000048 (Submit one each nrciuitnring perind with GIJ -59 firm.) I Enter date monitoring results were due. (12-31.2019) Will this monitoring report (GW-59 and GW-59A) NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? No IF the answer to question 1 or 2 is "YES', list in the space provided below the well identification numbers) and explain the problems encountered in obtaining the required information. MW-BA was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC, moving the replacement well 10' due North per DEQ direction. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification No plate, area overgrown, etc.)? If the on over is "Yes ". contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 5 For the constituents identified In question 4 above, have standards been exceeded previously for the same YES constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section S. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES problem? If the answer to question 7 is "YES', describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation fines, and/or penalties. Additional monitoring was performed to identify constituents of TOC in MW No.9. The facility has been communicating with Mr. Geoff Kegley in the Wilmington Regional Office. 8 The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form. I hereby acknowledge that the above information was evaluated and the Information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. Signature of P r rizetl Agent) Date ��13'102� Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report TDS 500 10A 12B 14A March-20 659 797 1180 November-19 637 908 1120 July-19 535 799 903 March-19 736 874 1220 November-18 659 621 1160 July-18 713 640 962 March-18 655 1110 988 pH 6.5-8.5 1 7A 8A 9 10A 11A 12B 13A 14A March-20 5 4.00 5.40 5.90 4.90 5.10 5.00 4.90 5.20 November-19 5.29 5.42 4.98 5.03 4.62 5.55 5.39 July-19 5.78 5.33 5.41 4.88 5.93 5.93 March-19 5.6 3.83 5.59 6.17 4.18 4.60 4.21 5.23 4.95 November-18 5.63 4.78 5.25 5.72 4.90 4.78 4.34 5.47 4.90 July-18 6.14 4.81 5.50 5.28 5.00 4.88 5.89 5.03 March-18 5.6 5.15 5.16 4.99 4.99 4.85 5.13 5.19 Chloride 250 10A 14A March-20 254 339 November-19 288 July-19 March-19 286 November-18 291 July-18 March-18 272 286 Sulfate 250 12B 14A March-20 281 342 November-19 289 July-19 322 March-19 302 339 November-18 400 July-18 287 March-18 378 258 Eenv7irochel ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax 710 $owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax info( envifnnnientalchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09538 Site: MW-1 3/7/2020 11:10 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/07/2020 Depth to water, ft. Depth to water, Ft. 1.9 feet 03/07/2020 Sodium EPA200.7 6.24mg/L 03/16/2020 Sulfate EPA 300 0 74 mg/L 03/10/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 03/19/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/07/2020 Odor Qualitative N/D 03/07/2020 Total Dissolved Solids (TDS) SM 2540 C 149 mg/L 03/09/2020 Temperature SM 2550 B 16.1 C 03/07/2020 Chloride SM 4500 Cl E 6 mg/L 03/13/2020 pH SM 4500 H B 5.0 units 03/07/2020 Total Phosphorus SM 4500 P F 0.16 mg/L 03/20/2020 Total Organic Carbon (TOC) SM 5310 B 0.9 mg/L 03/09/2020 Fecal Coliform SM 9222D MF <1 Colonies/100mL 03/07/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 03/09/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.36 mg/L 03/16/2020 Nitrate Nitrogen Subtraction Method 0.36 mg/L 03/18/2020 Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) EPA 351.2 0.5 mg/L 03/26/2020 Total Nitrogen Total Nitrogen 0.9 mg/L 03/27/2020 Report #:: 2020-03927 �� Page 1 of 11 rnvirochem 6�h ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(�Penvironmentalchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09539 Site: MW-2 3/7/2020 11:18 AM Water jcb/envirochem Test Method Results Date Analyzed Color Color Clear 03/07/2020 Depth to water, ft. Depth to water, Ft. 10.3 feet 03/07/2020 Sodium EPA200.7 11.1 mg/L 03/16/2020 Sulfate EPA 300.0 7 mg/L 03/10/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 03/19/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/07/2020 Odor Qualitative N/D 03/07/2020 Total Dissolved Solids (TDS) SM 2540 c 297 mg/L 03/09/2020 Temperature SM 2550 B 15.5 C 03/07/2020 Chloride SM 4500 Cl E 10 mg/L 03/13/2020 pH SM 4500 H B 7.4 units 03/07/2020 Total Phosphorus SM 4500 P F 0.24 mg/L 03/20/2020 Total Organic Carbon (TOC) SM 5310 B 1.2 mg/L 03/09/2020 Fecal Coliform SM 9222D MF <1 Colonies/100mL 03/07/2020 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 03/09/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.06 mg/L 03/16/2020 Nitrate Nitrogen Subtraction Method 0.06 mg/L 03/18/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2 < 0.5 mg/L 03/26/2020 Total Nitrogen Total Nitrogen <0.5 mg/L 03/27/2020 Report # 2020-03927 Page 2 of 11 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 66o2 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab • 910.392.4424 Fax 710 8owsertown Road, Manteo, NC 27954 i 252.473.5702 Lab/ Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(qelivironmentalchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09540 Site: MW-4 3/7/2020 10:45 AM Water jcb/envirochem Test Method Results Date Analyzed Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+ Nitrite-N itrogen Nitrate Nitrogen Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Color Yellow/Tan Tint 03/07/2020 Depth to water, Ft. 3.5 feet 03/07/2020 EPA 200 7 8.62 mg/L 03/16/2020 EPA 300 0 <5 mg/L 03/10/2020 EPA 3501 < 0.2 mg/L 03/19/2020 Gallons Bailed before sampling 5.0 gallons 03/07/2020 Qualitative N/D 03/07/2020 SM 2540 C 217 mg/L 03/09/2020 SM 2550 B 14.8 C 03/07/2020 SM 4500 Cl E < 5 mg/L 03/13/2020 SM 4500 H B 7.6 units 03/07/2020 SM 4500 P F 0.73 mg/L 03/20/2020 SM 5310 B <0.5 mg/L 03/09/2020 SM 9222D MF <1 Colonies/100mL 03/07/2020 EPA 353.2 < 0.02 mg/L 03/09/2020 EPA 353.2 < 0.02 mg/L 03/16/2020 Subtraction Method <0.02 mg/L 03/18/2020 EPA 351.2 Total Nitrogen < 0.5 mg/L 03/26/2020 <0.5 mg/L 03/27/2020 Report #:: 2020-03927 Paqe 3 of 11 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 0 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab; Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843' Lab/ Fax ANALYTICAL & CONSULTING CHEMISTS info(aenvironmentalchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09541 Site: MW-7A 3/7/2020 12:12 PM Water jcb/envirochem Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Method Results Date Analyzed Color Reddish Brown 03/07/2020 Depth to water, Ft. 4.5 feet 03/07/2020 EPA 200.7 17.3 mg/L 03/16/2020 EPA 300.0 20 mg/L 03/10/2020 EPA 350.1 0.5 mg/L 03/19/2020 Gallons Bailed before sampling 5.0 gallons 03/07/2020 Qualitative N/D 03/07/2020 SM 2540 C 173 mg/L 03/09/2020 SM 2650 B 15.7 C 03/07/2020 SM 4500 Cl E 62 mg/L 03/13/2020 SM 4500 H B 4.0 units 03/07/2020 SM 4500 P F 0.70 mg/L 03/20/2020 SM 5310 B <0.5 mg/L 03/09/2020 SM 9222D MF <1 Colonies/100ml- 03/07/2020 EPA 353.2 < 0.02 mg/L 03/09/2020 EPA 353.2 < 0.02 mg/L 03/16/2020 Subtraction Method <0.02 mg/L 03/18/2020 EPA 351.2 Total Nitrogen < 0.5 mg/L 03/26/2020 <0.5 mg/L 03/27/2020 Report # : 2020-03927 Paoe 4 of 11 www- envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347,5843 Lab/Fax info(rti,environmentit lchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09542 Site: MW-8A 3/7/2020 12:00 PM Water jcb/envirochem Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Calc) Total Kjeldahi Nitrogen (TKN) Total Nitrogen Method Results Date Analyzed Color Tan Tint 03/07/2020 Depth to water, Ft. 5.1 feet 03/07/2020 EPA 200.7 2.02 mg/L 03/16/2020 EPA 300.0 26 mg/L 03/10/2020 EPA 350.1 < 0.2 mg/L 03/19/2020 Gallons Bailed before sampling 5.0 gallons 03/07/2020 Qualitative N/D 03/07/2020 SM 2540 C 78 mg/L 03/09/2020 SM 2550 B 15A C 03/07/2020 SM 4500 Cl E < 5 mq/L 03/13/2020 SM 4500 H B 5.4 units 03/07/2020 SM 4500 P F 0.34 mg/L 03/20/2020 SM 5310 B 0.6 mg/L 03/09/2020 SM 9222D MF <1 Colonies/100mL 03/07/2020 EPA 3532 < 0.02 mg/L 03/09/2020 EPA 353.2 1.33 mg/L 03/16/2020 Subtraction Method 1.33 mg/L 03/18/2020 EPA 351.2 Total Nitrogen < 0.5 mg/L 03/26/2020 1.3 mg/L 03/27/2020 Report # 2020-03927 Paqe 5 of i t Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 = 910.392.0223 Lab = 910.392.4424 Fax 710 Bowsertov,-n Road, M.anteo, NC 27954 * 252.473.5702 L.ab/Fax sty 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Pax ANALYTICAL & CONSULTING CHEMISTS info{denvironmentalchetnists.com Valley Proteins - Rose Hill Post Office Box 1026 Rose Hill NC 28458 Attention: Susan Melchor Date of Report: Mar 27, 2020 Customer PO #: Customer ID: 08100027 Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09543 Site: MW-9 317/2020 10:58 AM Water jcb/envirochem Test Method Results Date Analyzed Color color Tan/Brown Tint 03/07/2020 Depth to water, ft. Depth to Water, Ft 3.5 feet 03/07/2020 Sodium EPA 200.7 56.1 mg/L 03/12/2020 Sulfate EPA 300.0 20 mg/L 03/10/2020 Ammonia Nitrogen EPA 350.1 0.5 mg/L 03/19/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/07/2020 Odor Qualitative Sulfur 03/07/2020 Total Dissolved Solids (TDS) SM 2540 C 219 mg/L 03/09/2020 Temperature SM 2550 B 13.0 C 03/07/2020 Chloride SM 4500 Cl E 9 mg/L 03/13/2020 pH SM 4500 H B 5.9 units 03/07/2020 Total Phosphorus SM 4500 P F 0.34 mg/L 03/20/2020 Total Organic Carbon (TOC) SM 5310 B 53.0 mg/L 03/09/2020 Fecal Coliform SM 9222D MF <1 Coloniesl100ml- 03/07/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.04 mg/L 03/09/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 03/16/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 03/18/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA351.2 1.8mg/L 03/26/2020 Total Nitrogen Total Nitrogen 1.8 mg/L 03/27/2020 Report #.: 2020-03927 Paae 6 of 11 6e"n:vj7iriochemn] ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab * 910.392.4424 Fax 710 Uowsertown Road, Manteo, NC 27954 i 252.473.5702 Lab/Fax 25 -A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax it) fo( enviconmentalehemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09544 Site: MW-10A 3/7/2020 12:30 PM Water jcb/envirochem Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Method Results Date Analyzed Colo` Reddish Brown 03/07/2020 Depth to water, Ft. 3.5 feet 03/07/2020 EPA 2007 98.2 mg/L 03/12/2020 EPA 300.0 108 mg/L 03/12/2020 EPA 350.1 < 0.2 mg/L 03/19/2020 Gallons Bailed before sampling 5.0 gallons 03/07/2020 Qualitative N/D 03/07/2020 SM 2540 C 659 mg/L 03/09/2020 SM 2550 B 13.9 C 03/07/2020 SM 4500 Cl E 254 mg/L 03/13/2020 SM 4500 H B 4.9 units 03/07/2020 SM 4500 P F 0.67 mg/L 03/20/2020 SM 5310 B 3.8 mg/L 03/09/2020 SM 9222D MF <1 Colonies/100mL 03/07/2020 EPA 353.2 < 0.02 mg/L 03/09/2020 EPA 353.2 < 0.02 mg/L 03/16/2020 Subtraction Method <0.02 mg/L 03/18/2020 EPA 351.2 Total Nitrogen 0.6 mg/L 03/26/2020 0.6 mg/L 03/27/2020 Report #:, 2020-03927 Paae 7 of 11 Lenvirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 9:10.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 I.,ab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910,347.5843I.ab/Fax info(c%environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09545 Site: MW-11A 3/7/2020 12:44 PM Water jcb/envirochem Test Method Results Date Analyzed Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Color White/Tan Tint 03/07/2020 Depth to water. Ft. 4.3 feet 03/07/2020 EPA 200.7 79.6 mg/L 03/12/2020 EPA 300.0 167 mg/L 03/12/2020 EPA 350.1 0.3 mg/L 03/19/2020 Gallons Bailed before sampling 5.0 gallons 03/07/2020 Qualitative N/D 03/07/2020 SM 2540 C 492 mg/L 03/09/2020 SM 2550 B 15.4 C 03/07/2020 SM 4500 Cl E 127 mg/L 03/16/2020 SM 4500 H B 5.1 units 03/07/2020 SM 4500 P F 0.57 mg/L 03/20/2020 SM 5310 B 2.7 mg/L 03/09/2020 SM 9222D MF <1 Colonies/100mL 03/07/2020 EPA 353.2 < 0.02 mg/L 03/09/2020 EPA 353,2 0.07 mg/L 03/16/2020 Subtraction Method 0.07 mg/L 03/18/2020 EPA 351.2 Total Nitrogen 0.7 mg/L 03/26/2020 0.8 mg/L 03/27/2020 Report #.. 2020-03921 Page 8 of 11 77 F"""_ a 71 Environmental Chemists, Inc. k envirochem 6602 Windmill Way, Wilmington, NC 28405 • 9"10.392.0223 Lab • 9.10.392.4424 Fax 710 Bowser -town Road, Manteo, NC 27954 • 252.473.5702 Lab /Fax ShF 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab 'Fax ANALYTICAL & CONSULTING CHEMISTS info(a�environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09546 Site: MW-12B 3/7/2020 12:56 PM Water jcb/envirochem Test Method Results Date Analyzed Color Color _ Clear 03/07/2020 Depth to water, ft. Depth to water, Ft 5.2 feet 03/07/2020 Sodium EPA200.7 144mg/L 03/12/2020 Sulfate EPA 3000 281 mg/L 03/12/2020 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 03/19/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/07/2020 Odor qualitative N/D 03/07/2020 Total Dissolved Solids (TDS) SM 2540 C 797 mg/L 03/09/2020 Temperature SM 2550 B 16.5 C 03/07/2020 Chloride SM 4500 Cl E 188 mg/L 03/16/2020 pH SM 4500 H B 5.0 units 03/07/2020 Total Phosphorus SM 4500 P F 0.55 mg/L 03/20/2020 Total Organic Carbon (TOC) SM 5310 B 2.8 mg/L 03/09/2020 Fecal Coliform SM 9222D MF <1 Colonies/100mL 03/07/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 < 0.02 mg/L 03/09/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 03/16/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 03/18/2020 Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) EPA 351.2 0.5 mg/L 03/26/2020 Total Nitrogen Total Nitrogen 0.5 mg/L 03/27/2020 Report # 2020-03927 Pace 9 of 11 enviroch• srs� ANALYTICAL & CONSULTING CHEMISTS Valley Proteins - Rose Hill Post Office Box 1026 Rose Hill NC Attention: Susan Melchor Lab ID Sample ID: 20-09547 Site: MW-13A Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(4,environmentalchemists.com Date of Report: Mar 27, 2020 Customer PO #: 28458 Customer ID: 08100027 Report #: 2020-03927 Project ID: March - Monitoring Wells Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Ca1c) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Total Nitrogen (Calc) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Collect Date/Time Matrix Sampled by 3/7/2020 1:09 PM Water jcb/envirochem Method Results Date Analyzed Color White/Tan Tint 03/07/2020 Depth to water, Ft 4.0 feet 03/07/2020 EPA 200.7 5.57 mg/L 03/12/2020 EPA 300.0 12 mg/L 03/12/2020 EPA 350.1 < 0.2 mg/L 03/19/2020 Gallons Bailed before sampling 5.0 gallons 03/07/2020 Qualitative Slight Sulfur 03/07/2020 SM 2540 C 64 mg/L 03/09/2020 SM 2550 B 15.9 C 03/07/2020 SM 4500 Cl E < 5 mg/L 03/16/2020 SM 4500 H B 4.9 units 03/07/2020 SM 4500 P F 0.44 mg/L 03/20/2020 SM 5310 B <0.5 mg/L 03/09/2020 SM 9222D MF <1 Colonies/100mL 03/07/2020 EPA 353.2 0.02 mg/L 03/09/2020 EPA 353.2 0.05 mg/L 03/16/2020 Subtraction Method 0.03 mg/L 03/18/2020 EPA 351.2 < 0.5 mg/L 03/26/2020 Total Nitrogen <0.5 mg/L 03/27/2020 Report #. 2020-03927 Paap 10 of 11 Lenvirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoga;environmentalchemists.com Valley Proteins - Rose Hill Date of Report: Mar 27, 2020 Post Office Box 1026 Customer PO #: Rose Hill NC 28458 Customer ID: 08100027 Attention: Susan Melchor Report #: 2020-03927 Project ID: March - Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-09548 Site: MW-14A 3/7/2020 11A5 AM Water jcb/envirochem Test Color Depth to water, ft. Sodium Sulfate Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+N itrite-N itrogen Nitrate Nitrogen Total Nitrogen (Cale) Total Kjeldahl Nitrogen (TKN) Total Nitrogen Method Results Date Analyzed Color Brown Tint 03/07/2020 Depth to water, Ft 3.3 feet 03/07/2020 EPA 200.7 155 mg/L 03/12/2020 EPA 300 0 342 mg/L 03/12/2020 EPA 350.1 < 0.2 mg/L 03/19/2020 Gallons Bailed before sampling 5.0 gallons 03/07/2020 Qualitative N/D 03/07/2020 SM 2540 C 1180 mg/L 03/09/2020 SM 2550 B 15.3 C 03/07/2020 SM 4500 Cl E 339 mg/L 03/16/2020 SM 4500 H B 5.2 units 03/07/2020 SM 4500 P F 0.46 mg/L 03/20/2020 SM 5310 B 4.3 mg/L 03/09/2020 SM 9222D MF <1 Colonies/100ml- 03/07/2020 EPA 353.2 < 0.02 mg/L 03/09/2020 EPA 353.2 1.81 mg/L 03/16/2020 Subtraction Method 1.81 mg/L 03/18/2020 EPA 351.2 Total Nitrogen Comment: Reviewed by: Rau'd \Ohlwy� < 0.5 mg/L 03/26/2020 1.8 mg/L 03/27/2020 Report # 2020-03927 Page 11 of 11 Environmental Chemist, Inc., Wilmington, NC Lab p94 6602.Windmill Way Wilmington, NC 28405 910,392.0223 Sample Receipt Checklist Client: Date:3 0�0 0 -- � q�7 Report Number.Q O ReceiptES❑ of Sample: Delivered N/Aeyed UPS ❑ Fed Ex ❑ Other E3 ❑ YES ❑ NO 1, were custody seals present on the cooler? Original temperature u N/A 2. If custody seals were present, were they intact/unbroken? pon receipt 4C How temperature taken: 13 Temperature Corrected temperature IR Gun ID: Thomas Traceable S/N 19251 657ture Btank upon receipt Against Bottles ❑ YES ❑ NO 3, if temperature of cooler) exceeded 6'C,CorrectionR Gun was Project M Or, ❑ NO 4. Were proper custody YES ❑ NO g /� notified? YES p dY procedures (relinqutshed/receivedj followed? S. Were sample ID s listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample con YES ❑ NO 7. Were collection date and tainers? time listed on the rs YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containerh YES O NO test? YES ❑ s for eac NO 10. Did samples arrive in good condition for each test? 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples rece YES ived within proper holding time for requested 13 NO 13. Were acid preserved samples received at a PH of <2? • YES ❑ NO tests? ❑ YES 14 Were cyanide samples received at a pH >121 ❑ NO 15. Were sulfide samples received at a YES ❑ NO 16. Were NH31MN/Phenol received a11 t a chlorine residual of c0.5 rn/L? .. ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of < • 0.5 m/L? TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. w� Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any samples) incorrectt Samples) y preserved or with headspace) by adding were received incorrectly preserved and were adjusted accordingly g (circle one): H2SO4 were HCI Time of preservation: NaOH Note: Notify customer If more than one preservative is needed, n service immediately for incorrect Otate in Comm Obtain a new notify the state lab if directed to analyzed by the customer, Who wassna fed, date and Te amP1e or comments below, Volatiles Sample(s) were received with headspace COMMENTS: C. QA.002 oC 2 Windmill on, NC ENVIRONMENTAL CHEMISTS, INC OOFFIC .910-392-02 3'IFAX 91G 4422405 Analytical 8 Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 infoOenvironmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 2-D ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: 11ti SAMPLE TYPE: 1= Influent, E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludge. Other: Sample Identification p Collection K m a y 8 E° c7 _ C° a m z E " ¢ m a J Z PRESERVATION ANALYSIS REQUESTED Date Time Temp z g d _ o _ o w o MW: / t l�C4 X NO2,Chloride,TDS,Sulfate G G . . De th to water: 3 C P X NO3,NH3,Total P, Total N calc G G gallons bailed: C P X P 4- f jNa G G H •field : 3 C P X Fecal Coliform G G odor: '� `^ ` C P X < TOC G G color: C C P X VOC (November only) G G C P G G C P G G C P G G 11 monitoring wells: due march, july, november Transfer Relinquished By: Daterrime Received By: Date/Time 1. 2. 1. eq•_ _Resample R ed: Delivered By:.__ �- C7�'_ _ Received By: Date Time: Comments:--------------_--__ _ __ ___ TUR A OUND: Windmill Way ENVIRONMENTAL CHEMISTS, INC OOFOFICE:91a3 2-02231FAX 9110 2�2405 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 infoOonvironmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: D _ 039 a 7 ADDRESS: CONTACT NAME: PO NO: REPORT TO: Sutaa-Priee- PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well. ST = Stream. SO = Soil. SL = Sludae. Other: Sample Identification Collection E a E o 0 U m o V a m c� t E v Q Qw a �' Z PRESERVATION ANALYSIS REQUESTED ate Time Temp i = y £ c _ o _ '' o MW: Z /s'' C P 1 1 X NO2,Chloride,TDS,Sulfate G G Depth to water: r'L `� C P D ,5 X IN03,NH3,Total P, Total N (caic) G G allans bailed: < C P � X Na G G H (field): '7113 Qi, C P X Fecal Coliform G G odor: A—e C P 3 0 %C < TOC G G color: C P X VOC (November only) G G C P G G C P G G C P G G 11 monitoring wells: due march, july, november Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: Accepted. Rejected: Resampie Requested: _ Delivered By:_ __ C,C�. Received By: I Dater 7QO Time: V_ Comments: _ _ _ TURNAROUND: ndmill Way mington ENVIRONMENTAL CHEMISTS, INC E+ 91a392-02 3'IFAX910-, NC392-44524� Analytical &Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: U— U -] ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: a-%) email: Sampled By: < 14 SAMPLE TYPE: I = Influent, E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae. Other: Sample Identification Collection K a a E o u m C 'o �n m t E U ¢ a 2 _jz PRESERVATION v ANALYSIS REQUESTED Date Time Temp _ i c 0 _ 0 _ o '' w o MW: / i �`� c C P �J � X NO2,Chloride,TDS,Sulfate G G Depth to water: L d C P ,S X 1� NO3,NH3,Total P, Total N talc G G s gallons bailed: C P X Na G G LZ pH (field): �" C P X Fecal Coliform G G odor: ° "` C P q fX < TOC G G color: G�•"'� C P X VOC (November only) G G C P G G C P G G C P G I G 11 monitoring wells: due march, july, november Transfer Relinquished By: Date/Time Received By: Daterrime 1. 2. I emperature when Received:_.. Accepted:_ Rejected: Resample uested: Delivered By: E C iReceived By: E ----Date:3 O Time: Comments:_ _ _ __......... _-------_--`_ TURNAROUND: Windmill Way ENVIRONMENTAL CHEMISTS, INC o; E:910-3 2-0223tFAX910 2�245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info 0 onvironmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: o- 03927 ADDRESS: CONTACT NAME: PO NO: REPORT TO: ' e PHONEIFAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil. SL = Sludge. Other: Sample Identification Collection g 2 o m ^ o a t " ¢ a 'z PRESERVATION ANALYSIS REQUESTED Date Time Temp i U = N i 0 = 4 o Mw: 3 ,., t ►� C P 1 ON X NO2,Chloride,TDS,Sulfate G G Depth to water: S'' + C P .S /' X P NO3,NH3,Total P, Total N calc) G G gallons bailed: S C P X Na G G pH (field): Y ' C P X Fecal Conform G G odor: rr— C P X TOC G G I color: T�d�%tL ��oJ� C P X IVOC(November only) G G C P G G C P G G C I G I G 11 monitoring wells: due march, july, november Transfer Relinquished By: DatelTime Received By: Date/Time 1. 2. I emperature when deceived: Accepted:_ Rejected: Resample uested:___ Delivered By:______ ' --Received By:7�_ — Date 3 h 1,3kri Time: 3 t --- ----- Comments: ____ TURNAROUND: Windmill Way mington C ENVIRONMENTAL CHEMISTS, IN OFF E: 910-392-02231FAX 910-392-44245 NCDENR: DWO CERTIFICATION # 94 NCDHHS: OLS CERTIFICATION # 37729 infoOenvironmentalchemists.com Analytical & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: U- &3Q 7 ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sam led B SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: P Y• Sample Identification Collection a E �, s a E o 0 o _ o ° a " v m t_ v M a _j= PRESERVATION ANALYSIS REQUESTED Date Time Temp _ z y i z o z g iz = o `7 MW: ii / s V` C P � X NO2,Ch1oride,TDS,Sulfate G G t. Depth to water: ` C P �'S X NO3,NH3,Total P, Total N (calc G G gallons bailed: C P X P Na G G pH (field): S • SQ C P I X Fecal Coliform G G odor: C P 14 X TOC G G color: 'f�►N �' ° C P X VOC (November only) G G C P G G C P G G C P G G 11 monitoring wells: due march, july, november Transfer Relinquished By: DatelTime Received By: Datelrime 1. 2. Temperature when Received: 3 Accepted:- Rejected:______Resample uested: Delivered By:_ CC�C Received By: Dater Time:.3' Comments:----..- _ ___ __ TURNAROUND: ill Way ENVIRONMENTAL CHEMISTS, INC �� OFFICE: 2-02 3'IFAX910- 2�8245 NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentaichemists.com Analytical & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 0 ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: M email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification p Collection k F- ! E y z c a c 2 c m a g o a U` m o rn tti E ¢ m M g Z PRESERVATION ANALYSIS REQUESTED a e Time Temp _ o z z _ p a z c 3 W s o MW: °% za fl? ; C P l X NO2,Chloride,TDS,Sulfate G G ., Depth to water: aL C P d { X NO3,NH3,Total P, Total N calc G G s gallons bailed: �, C P X Na G G H (field): S! 19l C P X Fecal Coliform G G odor: µ rt `"f C P 3 l t TOC G G color: Ar"' � C P X VOC (November only) G G .+ C P G G C P G G C P G G 11 monitoring wells: due march, july, november Transfer Relinquished By: DatelTime Received By: Datelrime 1. 2. Temperature when Received:_3 —_Accepted: --- ✓___ __Rejected: _ Resampleed: _ Delivered By:- -- - -- - - -- --- --- -- ----Received By: --------------- ----- —Date: 3y --Time: -3 '-?— Comments: TURNAROUND: on, RN MIR ENVIRONMENTAL CHEMISTS, I N C 6602 E: 910.392-02 3'IFAX 910 2�245 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 into0environmentalchemists.com Analytical & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: U _ 039a7 ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONEIFAX: COPY TO: bazll� email: Samnled Rv: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sam le Identification p Collection F "- E n s m °a o m C _ c C7 `o U a m $ c V E ¢ G W g z PRESERVATION ANALYSIS REQUESTED 14ate Time Temp i i = i p� = o _ g` O MW: 1 /4 7 a �1 X L NO2,Chloride,TDS,Sulfate G G Depth to water: `i� C P <u • X a j� NO3,NH3,Total P, Total N (calc) G G gallons bailed: C P X k} Na G G pH (field): q- C P I X I Fecal Coliform G G odor: /ton. C P �3 t�x ITOC G G color: r.11.5L I,j'J C P X I JVOC (November onl ) G G l C P C P G G C P _17 FF G IG 11 monitoring wells: due march, july, november Transfer Relinquished By: DateMme Received By: Datei7ime 1. 2. Temperature when Received:Accepted: ✓ Delivered By: LCK Comments:----- _----._-._ Received _Rejected:_ Resample uested:_. ar CJIv Date: 3l`l Time: TURNAROUND: Windmill Way ton ENVIRONMENTAL CHEMISTS, I N C o E: 910-392-02231FAX9910-392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: -. ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: '�'t email: Sampled By: q&�:'_ SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection a N o 2 y _ IvC7 c 'o a m �` `o a " e ccPRESERVATION Qw g M = ANALYSIS REQUESTED ate Time Temp i Z = g c p W o MW: /%� C P h� X NO2,Chloride,TDS,Sulfate G G ,. Depth to water: SL C P < X pi 1NO3,NH3,Total P, Total N calc G G allons bailed: C P X P Na G G pH (field): {. aL C P X Fecal Coliform G G odor: N' -`- C P q iCI ITOC G G // color: w�'!' C P X VOC November only) G G C P G G C P G G C P G G 11 monitoring wells: due march, 'ul , november Transfer Relinquished By: Date/Time Received By: DatelTime 1. 2. Temperature when Received:___Accepted: Rejected: Resample quested: Delivered By: Received By:Date 3 Time:3 " 4 1 Comments: TURNAROUND: ton, NC 284 ming ENVIRONMENTAL CHEMISTS, I N C O °F Windmill: 910-392-02231FAX 910-392-442405 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info®environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: Q() — 03 7 ADDRESS: CONTACT NAME: PO NO: REPORT TO: Saeon-Price- PHONE/FAX: COPY TO: S email: Sampled By: 9�$ SAMPLE TYPE: 1= Influent, E = Effluent, W = Well, ST = Stream. SO = Soil. SL = Sludae. Other: Sample Identification Collection 12 d E a a `i a 0 c(7 S o 0a m c o v E a w m 0° Jz PRESERVATION ANALYSIS REQUESTED Date Time Temp W i i �, = x Z = ¢ o MW: I Z n to L > /C S C P X NO2,Ch1oride,TDS,Su1fate G G „ Depth to water: G L C P 0 X NO3,NH3,Total P, Total N (calc) G G gallons bailed: C P I XI lNa G I G pH field): t/_ `i C P X Fecal Coliform G G odor: A' ( C Pj TOC G G color: e_rJ C I P X JVOC (November onl G G C P G G C P G G C P G G 11 monitoring wells: due march, July, november Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: 3 Accepted: Rejected:__Resample a nested: Delivered By: �C Received By:___Date 3 Time: Comments: ____._ TURNAROUND: Analytical 8 Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchomists.com Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: 0 _ o39a7 ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: `9S SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m � s & o F 8 y o a o " E m O° J i PRESERVATION ANALYSIS REQUESTED a Time Temp w Z i = x Z g ~ w o MW: � J �S'9` C P `1 X NO2,Chloride,TDS,Sulfate G G , De th to water: y� C P {D `� X P NO3,NH3,Total P, Total N (calc G G gallons bailed: C P X P Na G G pH(field): `{ $ S C P IX I Fecal Coliform G G odor: Iv fA-/ C P c TOC G G color: W C P X VOC (November only) G G C P G G C P G G C P G G 11 monitoring wells: due march, july, november Transfer Relinquished By: DateRime Received By: DatelTime 1. 2. Temperature when Received:_.S Accepted: i Rejected: Resampie R uested: _ Delivered BReceived By: _ Date:_ _Time: 3 41 Comments: TURNAROUND: MI ENVIRONMENTAL CHEMISTS, I N C 65602 IWindmill in9 m�9 -0223iFAX 9t10-392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Valley Proteins -Rose Hill PROJECT NAME: Monitoring Wells REPORT NO: U _ ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well. ST = Stream. SO = Soil. SL = Sludae. Other: Sample Identification Collection K f E W 6 0 Ca S 8t a cr C O cc a "� z PRESERVATION V ANALYSIS REQUESTED ate Time Temp z z * c o z 2W € o Mw: I Y A /tY f / ` C P ci{c X NO2,Chloride,TDS,Sulfate G G Depth to water: 3 S C P X p NO3,NH3,Total P, Total N (calc) G G allons bailed: S C P X P Na G G pH (field): S •Z C P X Fecal Coliform G G odor: n - C P 1�3 ITOC G G color: 1 r•a •• 'f'. C P I X VOC (November only) G G C P G G C P I G G d C P G G 11 monitoring wells: due march, july, november Transfer Relinquished By: Date/Time Received By: Dateffime 1. 2. � c131NcIOLUI W rnlon r1wL-C1VCG: -.jE Accepiea: 4.-- Hejected: Resamplenested: Delivered By:___,__� Received By: _ Date: 0 Time:3 t{ I Comments: _ ______ _ TURNAROUND: