WQ0005910_Monitoring - 03-2020_20200428 (2)

GW-59A COMPLIANCE REPORT FORM Permit #_�&QQDQGew)
(Suhrrrit one each monitoring period with GFV 59 forms.)
s
1
Enter date monitoring results were due. O Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
` /
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)" If the answer is "Fes ", contact the Regional 0jrice for guidance,
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section B.
if the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrations)
exceeding standards in the space provided below:
mto 4 - N11—
VWW
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question '5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
w 5 —-COS
31�q�tg - coSS 'i►�altK- U% 1
6M41%A- %-A.1y
\/
'�I�al�q- ►0.5 1�0— io4�
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE iMMEDIATELYFOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is 'YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days • an evaluation may be
re uired to determine the impact the waste disposal system Is havina at the review and compliance
boundaries surrounding this faciiity Fallure to do so may sublect the permittee to a Notice of Volatlon,
fines, and/or penalties. ` A G
n
X12�2� APR
MAC 2 8 2020
D'i" J-N
8
The person completing this portion (GW-59A) of the monitoring rep'©rl'Sliould sign belaw.! d submit this
form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form.
Irhereby;acknowiedge.that ttia`aIgdve information wars evafu6ted and the Informat(an�subm Wn hiseport(CompliariceReport,G,1!V,59Aa;,is
true and complete to the�bst of hiJChowfa,�, �
LA-21-202J
Signature of Pe Date
M

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Awn(cA LLC
Permit Name (if different):
Facility Address: V "
cvV �A'II (Sireev Nc. Z.14S-7 County-- Qark.e.
(Chy) (Slalc) (zip) p 2%7- 4
Contact Person: Tele hone #: t2-; 133
Well Location/ Site Name: No. of Wells to be Sampled:,. 6 "
Well Identification Number (from Permit): Mom- `� For Groundwater Treatment Systems
Well Depth: —2-N ft. Well D' meter: 2 in. Check One: ❑ Influent (98)
Screened Interval: is ft. to ft. ❑ Effluent (99)
Depth to Water Level: it. below measuring point.
Measuring Point (M.P.) Ti— ft. above land surfac Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: Date sample collected: _SZ_2
Field analysis: pH , Specific Conductance uMhos
Temp. °C, Odor WDvl e- Appearance C Vouv-
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH. NC 27699-1636 Phone: [phone]:
PERMIT #: . EXPIRATION DATE
Non -Discharge" Ooo5910 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample analyzed: 313\ _ 1Aj(p j ;kO
Laboratory Name: Ery ►1cQV'nvyne,n
Certification No. ko
PARAMETERS (Samples for metals were collected unfiltered_V YES
NO and field acidified
COD
mg/I
Nitrite (NO2) as N
mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
0.05 mg/I
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 30'6 mg/I
Orthophosphate
AI - Aluminum
mg/I
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC e• \ , o O
mg/I
Ca - Calcium
mg/I
Chloride 2y
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia < ©.O
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
YES NO)
4
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes (1) No (0)
VOC : method # =
method # =
method if =

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Pto(a LLC,
Permit Name (if different):
Facility Address: 9)t'11 Avoca FaI-m Road
cvv %AltI ISl,eeq N(.. 2-I4S7 County 1
(cav) �e�,n Co e ' (zip) Telephone #: 2S2 4�2-�133 Contact Person: _
Well Location/ Site Name:
No. of Wells to be Sampled:
Well Identification Number (from Permit): tAW - 5 For Groundwater Treatment Systems
Well Depth: 2k,71 ft. Well Diameter: 2 in. Check One: ❑ Influent (98)
Screened Interval: i�� ft. to 22- ft. ❑ Effluent (99)
Depth to Water Level: 9.3 ft. below measuring point.
Measuring Point (M.P.) is: 2- ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: 5 Date sample collected: 3' u--z
Field analysis: pH41511— , Specific Conductance uMhos
Temp.'12•`4 -C, Odor ZI-1e- Appearance C,\�av
PARAMETERS (Samples for metals were collected unfiltered
COD mg/I Nitri
Coliform: MF Fecal /100ml Nitr
Coliform: MF Total /100ml Pho
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total 519 mg/I
pH (when analyzed)
units
TOC 3.3 (o
mg/I
Chloride 32
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia SD -OH
mg/I
TKN as N
mg/I
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
PERMIT #: • EXPIRATION DATE:
Non -Discharge W Q 000591 O UIC
IINIU *-.I
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample analyzed: 3131 - 4 j Co 2 D
Laboratory Name: Etnv ►ern nVV11. .k 3•
Certification No. ro
YES NO and field acidified
to (NO2) as N mg/I
ate (NO3) as N 0.0 mg/I
sphorus: Total as P O. 05 mg/I
Orthophosphate mg/I
Al - Aluminum mg/I
Ba - Barium mg/I
Ca - Calcium 35.01 mg/I
Cd - Cadmium mg/I
Chromium: Total mg/I
Cu - Copper mg/I
Fe - Iron mg/I
Hg - Mercury mg/I
K - Potassium mg/I
Mg - Magnesium mg/I
Mn - Manganese mg/I
YES NO)
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes (1) No (0)
VOC : method # =
method If =
method If =

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: N4j)C_u PLC
Permit Name (if different):
Facility Address: fr "
vv K'll (St,eeq Wc- 2-14S7 County 1 ek%e-
(tac "� Co�e�' (zip) Telephone #: 2S2-'-1�2-� 133
Contact Person: _
Well Location/ Site Name:
No. of Wells to be Sampled:
Well Identification Number (from Permit): illy- For Groundwater Treatment Systems
Well Depth: k% ft. Well Diameter: Z in. Check One: ❑ Influent (98)
Screened Interval: 3 ft. to l— ft. ❑ Effluent (99)
Depth to Water Level: (v- k ft. below measuring point.
Measuring Point (M.P.) is: 2 ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: r Date sample collected: 3'30-20
Field analysis: pH(0-2-4 , Specific Conductance uMhos
Temp. 21- S IC,Odor 0vv- Appearance 1,eclx�e'
PARAMETERS (Samples for metals were collected unfiltered
COD mg/I Nitri
Coliform: MF Fecal /100ml Nitr
Coliform: MF Total /100ml Pho
(Note: Use MPN method for highly turbid am les)
Dissolved Solids: Total 13�
mg/I
pH (when analyzed
units
TOC 3. S
mg/I
Chloride —1
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance uMhos
Total Ammonia C O.O
mg/I
TKN as N
mg/I
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
PERMIT #: • EXPIRATION DATE: 10 31 20 y
Non-DischargeWQ000591Q UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedialion: Infiltration Gallery
Spray Field Remedialion:
Rotary Distributor Land Application of Sludge
Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample analyzed:
Laboratory Name: Ery Certification No. No. to
_YES NO and field acidified
to (NO2) as N mg/I
ate (NO3) as N 5.39 mg/I
sphorus: Total as P 0.12 mg/I
Orthophosphate mg/I
Al - Aluminum mg/I
Ba - Barium mg/I
Ca - Calcium 14,44 mg/I
Cd - Cadmium mg/I
Chromium: Total mg/I
Cu - Copper mg/I
Fe - Iron mg/I
Hg - Mercury mg/I
K - Potassium mg/I
Mg - Magnesium mg/I
Mn - Manganese mg/I
YES NO)
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes (1) No (0)
VOC method # =
method # =
method # =

SUBMIT FORM ON YELLOW PAPER ONLY
Mail Original, DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
COMPLIANCE REPORT FORM RALEIGH. NC 27699-1636 Phone: [phone]
FACILITY INFORMATION
Facility Name: Nt)(a LLC-
Permit Name (if different):
Facility Address: AVOCU FaI-m Road
tvv " tl (Street) NL Z-4S-7
(City) (Stale) (zip)
Contact Person:
Well Location/ Site Name:
Please Print Clearly or Type
County SOYA �0e-
Telephone
No. of Wells to be Sampled:
Well Identification Number (from Permit): iy1W' `6 For Groundwater Treatment Systems
Well Depth: Ift. Well Diameter: Z in. Check One: ❑ Influent (98)
Screened Interval: —6 ft. to 1i b ft. ❑ Effluent (99)
Depth to Water Level: 1.4 it. below measuring point.
Measuring Point (M.P.) is: Z— ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: 'S Date sample collected: 3"30'2t
Field analysis: pF , Specific Conductance uMhos
Temp. 20�2 °C, Odor NQ-,0_ Appearance �' .\tea✓
PARAMETERS (Samples for metals were collected unfilt
COD mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total wa'4 mg/I
pH (when analyzed)
units
TOC 3%.%
mg/I
Chloride 2
mg/I
Arsenic
mg/I
Grease and Oils
mg/1
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia O • su
mg/I
TKN as N
mg/I
PERMIT #: , EXPIRATION DATE: iSetg
Non -Discharge w Q 000541 O UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample analyzed: > I31 " y 1 bI 20
Laboratory Name: Etf1v ►xco nv, eni -3_
Certification No. `o
YES NO and field acidified V YES NO)
Nitrite (NO2) as N mg/I
Nitrate (NO3) as N G O. 00 9 mg/I
Phosphorus: Total as P 0. (a5 mg/I
Orthophosphate
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium 35,1
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes (1) No (0)
VOC : method # =
method # =
method if =

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Please Print Clearly or Type
Facility Name:Awo(u LLC-
Permit Name (if different):
Facility Address: "
, 1F
�.V V �• t, IStree9 Nf`. Z_IQS�
L
County
(City) �F1J1 (dale) (zip)
Contact Person: CQv�r,e�
•2S,Z y -- t
Telephone #:
Well Location/ Site Name:
No. of Wells to be Sampled:
(from Permit)
Well Identification Number (from Permit): 'M
For Groundwater Treatment Systems
Well Depth: 22•00 __ ft. Well Diameter: ?-
in.
Check One: ❑ Influent (98)
Screened Interval: 10 ft. to Z3 ft.
Depth to Water Level:ft. below measuring
❑ Effluent (99)
point.
Measuring Point (M.P.) is: 2 ft. above land surface.
Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: S
Date sample collected:3-310-20
Field analysis: pH 5.5 0 , Specific Conductance
uMhos
Temp. Zt•2- °C, Odor N'Qv"kZ
Appearance ���✓
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH. NC 27699-1636 Phone: [phone]:
PERMIT #: , EXPIRATION DATE
Non-DischargeWQ0005910 UIC
NPDES
9
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample analyzed: 3 31— 4 l0 2O
Laboratory Name: Ery' CC)r%v+n¢,n�k
Certification No. 10
PARAMETERS (Samples for metals were collected unfiltered `' YES NO and field acidified
COD
mg/I
Nitrite (NO2) as N
mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N 1.Oq
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P -23
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
mg/I
Al - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC 1,2(o
mg/I
Ca - Calcium •35
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia t O.Ot-}
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
YES NO)
Ni - Nickel mg/I
Pb - Lean mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method If. Attach lab report.)
Report Attached? Yes (1) No (0)
VOC : method # =
method If =
method If =

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Facility Name: AwoCa L.LC
Please Print Clearly or Type
Permit Name (if different):
Facility Address: F l-
CvV ",,II (Street) AIC.
riffs-7 County - I �4"e,
(city) (State)
Contact Person:
(zip) ZSZ y
Telephone #: �2-�►33
Well Location/ Site Name:
No. of Wells to be Sampled:
Well Identification Number (from Permit): MW —1 Q For Groundwater Treatment Systems
Well Depth: 20 _ft. Well Diameter: Z in. Check One: ❑ Influent (98)
Screened Interval: 3 ft. to 2-0 ft. ❑ Effluent (99)
Depth to Water Level: 119 ft. below measuring point.
Measuring Point (M.P.) is: 2 ft. above land surface. Relative M.P. Elevation in ft.:
Gallons of water pumped/bailed before sampling: S Date sample collected: 3 ISO 12,0
Field analysis: pH LA -'I I , Specific Conductance uMhos
Temp. 4-G °C, Odor �jO"w Appearance Lk Co✓
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
WATER QUALITY DIVISION, GROUNDWATER SECTION
1636 MAIL SERVICE CENTER
RALEIGH. NC 27699-1636 Phone: [phone]:
PERMIT #: • EXPIRATION DATE: 1O
Non -Discharge W Q 00059 k c) UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sludge
Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample analyzed: 3131— Lk p120
Laboratory Name: E-r%j 'Cj0trnv+neA-N 3-
Certification No. k0
PARAMETERS (Samples for metals were collected unfiltered V YES NO and field acidified
COD
mg/I
Nitrite (NO2) as N
mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total `-t10
mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
mg/I
Ca - Calcium 23,9(o
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia < D • 0 y
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
YES NO)
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes (1) No (0)
VOC :method # _
method # =
method # =

Wastewater ID i 10
,=,
114 OAKMONT DRIVE PHONE (252j 756-6208
uREENVILL.E, N.C. 27858 FAX [phone]
AVOCA, LLC (WASTEWATER)
MR. BRIAN CONKER
P.O. BOX 129
MERRY HILL ,NC 27957
Effluent
PARAMETERS
BOD, mg/l
2180
Total Suspended Residue, ing/I
120
Ammonia Nitrogen as N, mg/I
4.26
Total Kjeldahl Nitrogen as N,mg/I
50.52
Nitrate -Nitrite as N, mg/I (calc)
0.24
Nitrate Nitrogen as N, mg/i
<0.04
Nitrite Nitrogen as N, mg/i
0.24
Total Phosphorus as P, mg/l
46.00
Total Organic Carbon, mg/l
Chloride, mg/I
47
Total Dissolved Residue, mg/I
2280
Total Dissolved Residue, mg/l
Calcium, ug/I
19647
Magnesium, ug/l
4021
Sodium, ug/l
116518
Sodium Adsorption Ratio (cafe)
6.3
Total Nitrogen, mg/1 (calc)
50.76
ID#: 132
DATE COLLECTED: 03/30/20
DATE REPORTED : 04/21/20
REVIEWED BY:
Well N4 Well #5 Well N7 Well #8 Analysis Method
Date Analyst Code
04/01/20
TMR
521OB-11
04/01/20
JMS
2540D-11
< 0.04
< 0.04
< 0.04
0.56
04/01/20
AKS
350.1 R2-93
04/03/20
AKS
351.2 112-93
353.2 R2-93
10.60
0.09
5.39
<0.04
03/31/20
DTL
353.2 112-93
04/01/20
DTL
353.2 R2-93
0.05
0.05
0.12
0.65
04/03/20
TLH
365.4-74
< 1.00
3.36
3.35
38.80
04/02/20
SEJ
531OC-11
24
32
7
21
04/06/20
MAR
4500CLB-11
04/06/20
GNB
254OC-11
308
579
137
464
04/02/20
GNB
254OC-11
61291
35013
14442
35192
04/02/20
LFJ
EPA200.7
04/02/20
LFJ
EPA200.7
04/02/20
LFJ
EPA200.7

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27658
AVOCA, LLC (WASTEWATER)
MR. BRIAN CONNER
P.O. BOX 129
MERRY HILL ,NC 27957
Ivell N9 well N 10
PARAMETERS
PHONE [phone]
FAX [phone]
ID#: 132
DATE COLLECTED: 03/30/20
DATE REPORTED : 04/21/20
REVIEWED BY:
Analysis Method
Date Analyst Code
Ammonia Nitrogen as N, mg/1
<0.04
<0.04
04/01/20
AKS
350.1 R2-93
Nitrate Nitrogen as N, mg/l
1.09
8.59
03/31/20
DTL
353.2 R2-93
Total Phosphorus as P, mg/1
0.23
0.04
04/03/20
TLH
365.4-74
Total Organic Carbon, mg/1
1.26
1.44
04/02/20
SEJ
5310C-II
Chloride, mg/l
27
82
04/06/20
MAR
45000,11-11
Total Dissolved Residne, mg/1
267
410
04/02/20
GNB
2540C-11
Calcium, ug/1
42350
23969
04/02/20
LFJ
EPA200.7

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P%J-T515X7095, 114 Oakmont Dr. Pa,2e ot`
Greenville. NC 27858
environment I inc.com
DISINFECTION
Phone [phone] - Fax [phone]
I
I
I
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CHLORINE NEUTRALIZED AT COLLECTION
CHLORINE
011,
pH CHECK (LAB)
CLIENT: 132 Week: 15
UV
P
P
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P
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P
P
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CONTAINER TYPE, P/G
,VOCA, LLC (WASTEWATER)
NONE
1R. BRIAN CONNER
,.0. BOX 129
1ERRY HILL NC 27957
FA
A
A
C
C
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CHEMICAL PRESERVATION
A - NONE D - NAOH
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SOLID WASTE SECTION
Well #8
1-3020
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330-20
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CHAIN OF CUSTODY (SEAL) MAINTAINED
DURING SHIPMENT/DELIVERY
N
SAMPLES COUrtTED BY:
Phnt)
r&--Owl
SAMPLES RECEIVED IN LAB AT U C
RELINQUISHED BY (SIG.) (SAMPLER)
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DATETME
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RELINQUISHED BY (SIG.)
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RELINQUISHED BY (SIG.)
DATETIME
RECEIVED BY (SIG.)
DATE11ME
I PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a T" for composite sample or a "G" for
FORM #5 Grab sample in the blocks above for each parameter requested. N2 372073

Laboratories i i_c
a member of The GEL Group INC.
April 16, 2020
Ms. Deedee Woolard
Environment One, Inc.
114 Oakmont Drive
Greenville, North Carolina 27858
Re: Routine Analytical - North Carolina
Work Order: 508725
Dear Ms. Woolard:
U
P080"0712 Chadestnn,S029417
2040 Savage (load Chadeston,SC 29407
P 845.556.8171
F 843.756.1178
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on April 02, 2020, This original data report has been prepared and reviewed in accordance
with GEL's standard operating procedures,
Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards,
with any exceptions noted. The results reported relate only to the items tested and to the sample as received by
the laboratory. These results may not be reproduced except as full reports without approval by the laboratory.
Copies of GEL's accreditations and certifications can be found on our website at www.gel.com.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4707.
Sincerely,
49W
Samuel Hogan for
Katelyn Gray
Project Manager
Purchase Order: PO BJ 13203312020
Enclosures
Page 1 of 15 SDG: 508725
problem solved
gel.com

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
for
ENV0001 Environment One, Inc,
Client SDG: 508725 GEL Work Order: 508725
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
J See case narrative for an explanation
J Value is estimated
U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Katelyn Gray.
M
Reviewed by
Page 2 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www,gel.com
Certificate of Analysis
Company: Environment One, Inc.
Address : 114 Oakmont Drive
Greenville, North Carolina 27858
Contact:
Ms. Deedee Woolard
Project:
Routine Analytical - North Carolina
Client Sample ID:
Well #4
Sample ID:
508725001
Matrix:
Ground Water
Collect Date:
30-MAR-2013:30
Receive Date:
02-APR-20
Collector:
Client
Report Date: April 16, 2020
Project: ENV000101
Client ID: ENV0001
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Ion Chromatography
EPA300.0 Bromide Liquid "As Received"
Bromide U 0.000 0.0670 0.200 mg/t. 1 LXA2 04/02120 2335 1986963 1
The following Analytical Methods were performed: T
Method_ _ Description _ _ Analyst Comments
1 EPA 300.0
Notes:
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level
DL: Detection Limit PF: Prep Factor
MDA: Minimum Detectable Activity RL: Reporting Limit
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 3 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www,gel.com
Certificate of Analysis
Company: Environment One, Inc.
Address : 114 Oakmont Drive
Contact:
Project:
Greenville, North Carolina 27858
Ms. Deedee Woolard
Routine Analytical - North Carolina
Client Sample ID:
Well #5
Sample ID:
508725002
Matrix:
Ground Water
Collect Date:
30-MAR-20 14:05
Receive Date:
02-APR-20
Collector:
Client
Report Date: April 16, 2020
Project: ENVO00101
Client ID: ENVO001
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Ion Chromatography
EPA300.0 Bromide Liquid "As Received"
Bromide 4.98 0.134 0.400 mg/L 2 CH5 04/03/20 0323 1986653 t
The following Analytical Methods were performed:
Method Description �• Analyst Comments
1 EPA 300.0
Notes:
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level
DL: Detection Limit PF: Prep Factor
MDA: Minimum Detectable Activity RL: Reporting Limit
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 4 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company :
Environment One, Inc.
Address :
114 Oakmont Drive
Greenville, North Carolina 27858
Contact:
Ms. Deedee Woolard
Project:
Routine Analytical - North Carolina
Client Sample ID:
Well #7 — - - -
Sample ID:
508725003
Matrix:
Ground Water
Collect Date:
30-MAR-2014:30
Receive Date:
02-APR-20
Collector:
Client
Rcport Date: April 16, 2020
Project: ENV000101
Client ID: ENV0001
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Ion Chromatography
EPA300.0 Bromide Liquid "As Received"
Bromide 4.68 0.134 0.400 mg/L 2 CH5 04/03/20 0350 1986653 1
The following Analytical Methods were performed:
Method Description -_ _ _ Analyst Comments __
I EPA 300.0
Notes:
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level
DL: Detection Limit PF: Prep Factor
MDA: Minimum Detectable Activity RL: Reporting Limit
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 5 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.corn
Certificate of Analysis
Report Date: April 16, 2020
Company : Environment One, Inc.
Address: 114 Oakmont Drive
Greenville, North Carolina 27858
Contact: Ms. Deedee Woolard
Project: Routine Analytical - North Carolina
Client Sample ID:
Well #8 Project: ENV000101
Sample ID:
508725004 Client ID: ENV0001
Matrix:
Ground Water
Collect Date:
30-MAR-20 14:55
Receive Date:
02-APR-20
Collector:
Client
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Ion Chromatography
EPA300.0 Bromide Liquid "As Received"
Bromide 11.9 0.670 2.00 mg/L 10 LXA2 04/03/20 1253 1986863 1
The following Analytical Methods were performed:
Method Description _._ Analyst Comments _
1 EPA 300.0
Notes:
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level
DL: Detection Limit PF: Prep Factor
MDA: Minimum Detectable Activity RL: Reporting Limit
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 6 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Environment One, Inc.
Address :
114 Oakmont Drive
Greenville, North Carolina 27858
Contact:
Ms. Deedee Woolard
Project:
Routine Analytical - North Carolina
Client Sample ID:
Well #9
Sample ID:
508725005
Matrix:
Ground Water
Collect Date:
30-MAR-20 14:15
Receive Date:
02-APR-20
Collector:
Client
Report Date: April 16, 2020
Project: ENV000101
Client ID: ENV0001
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Ion Chromatography
EPA300.0 Bromide Liquid "As Received"
Bromide U 0.000 0.0670 0.200 MIA 1 LXA2 04/03/20 0123 1986863 1
The following Analytical Methods were performed:__
Method Description Analyst Comments
l EPA 300.0 -
Notes:
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level
DL: Detection Limit PF: Prep Factor
MDA: Minimum Detectable Activity RL: Reporting Limit
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 7 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company: Environment One, Inc.
Address : 114 Oakmont Drive
Contact:
Project:
Greenville, North Carolina 27858
Ms. Deedee Woolard
Routine Analytical - North Carolina
Client Sample ID:
Well #10
Sample ID:
508725006
Matrix:
Ground Water
Collect Date:
30-MAR-20 14:40
Receive Date:
02-APR-20
Collector:
Client
Report Date: April 16, 2020
Project: ENVO00101
Client ID: ENV0001
Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method
Ion Chromatography --___..--..--.- —_ -.--•_
EPA300.0 Bromide Liquid "As Received"
Bromide 0.470 0.0670 0.200 mg/L 1 LXA2 04/03/20 0150 I996863 1
The following Analytical Methods were performed:
Method Description Angst Comments
1 EPA 300.0
Notes:
Column headers are defined as follows:
DF: Dilution Factor Lc/LC: Critical Level
DL: Detection Limit PF: Prep Factor
MDA: Minimum Detectable Activity RL: Reporting Limit
MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit
Page 8 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage
Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Report Date: April 16, 2020
Environment One, Inc.
Page I of 2
114 Oakmont Drive
Greenville, North Carolina
Contact: Ms. Deedee Woolard
Workorder: 508725
Parmname NOM
Sample Qual. QC Units RPD%
REC%
Range Anlst
Date Time
lon Chromatography
Batch 1986653 - —
- .._.. _- - -
-
- --
---------
QC1204539087 508721001 DUP
Bromide
0.335 0.346 mg/L 3.08
^
(+/-0.200) CH5
04/02/20 21:58
QC1204539086 LCS
Bromide I.25
1.19 mg/L
95.1
(90%-110%)
04/02/20 21:31
QC1204539085 MB
Bromide
U 0.000 mg/L
04/02/20 21:04
QC1204539088 508721001 PS
Bromide 1.25
0.335 1.52 mg/L
95.1
(90%-110%)
04/02/20 22:25
Batch 1986963- --- ._.._—
-_-
QC1204539430 508710008 DUP
Bromide
2.74 2.69 mg/L 1.74
(0%-20%) LXA2
04/03/2011:32
QC1204539429 LCS
Bromide 1.25
1.25 mg/L
100
(90%-110%)
04/02/20 20:26
QC1204539428 MB
Bromide
U 0.000 mg/L
04/02/2019:56
QC1204539431 508710008 PS
Bromide 1.25
1.37 2.65 mg/L
102
(90%-110%)
04/03/2011:59
Notes:
The Qualifiers in this report are defined as follows:
< Result is less than value reported
> Result is greater than value reported
B The target analyte was detected in the associated
blank.
E General Chemistry --Concentration of the target
analyte exceeds the instrument calibration range
Page 9 of 15 SDG: 508725

GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
Workorder: 508725
Parmname NOM
H
Analytical holding time was exceeded
J
See case narrative for an explanation
J
Value is estimated
N/A
RPD or %Recovery limits do not apply,
N1
See case narrative
QC Summary
Page 2 of 2
- -- - -
Sam Ip a Quai QC Units.._ RPD% _ ,.RRC% Range Anlst Date Time
ND Analyte concentration is not detected above the detection limit
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
R Per section 9.3.4.1 of Method 1664 Revision B, due to matrix spike recovery issues, this result may not be reported or used for regulatory compliance
purposes.
R Sample results are rejected
U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Z Paint Filter Test --Particulates passed through the filter, however no free liquids were observed.
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
d 5-day BOD--The 2:1 depletion requirement was not met for this sample
e 5-day BOD--Test replicates show more than 30% difference between high and low values. The data is qualified per the method and can be used for
reporting purposes
h Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone, by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of+/- the
RL is used to evaluate the DUP result.
k Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 10 of 15 SDG: 508725

General Chemistry
Technical Case Narrative
Environment One, Inc.
SDG #: 508725
Product: Ion Chromatography
Analytical Method: EPA 300.0
Analytical Procedure: GL-GC-E-086 REV# 27
Analytical Batch: 1986653
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID#
Client Sample Identification
508725002
Well #5
508725003
Well #7
1204539085
Method Blank (MB)
1204539086
Laboratory Control Sample (LCS)
1204539087
50872 100 1 (NonSDG) Sample Duplicate (DUP)
1204539088
508721001(NonSDG) Post Spike (PS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary
All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.
Technical Information
Sample Dilutions
The following samples 1204539087 (Non SDG 50872100 1 DUP), 1204539088 (Non SDG 508721001PS),
508725002 (Well #5) and 508725003 (Well #7) were diluted because target analyte concentrations exceeded the
calibration range. Dilutions may be required for many reasons, including to minimize matrix interferences or to
bring over range target analyte concentrations into the linear calibration range.
548725
Anafyle
oo: aoa
Bromide 2X 2X
Product: Ion Chromatography
Analytical Method: EPA 300.0
Analytical Procedure: GL-GC-E-086 REV# 27
Analytical Batch: 1996863
The following samples were analyzed using the above methods and analytical procedure(s).
GEL Sample ID#
508725001
508725004
508725005
Page 11 of 15 SDG: 508725
Client SamVIg Identification
Well #4
Well #8
Well #9

508725006 Well #10
1204539428 Method Blank (MB)
1204539429 Laboratory Control Sample (LCS)
1204539430 508710008(NonSDG) Sample Duplicate (DUP)
1204539431 508710008(NonSDG) Post Spike (PS)
The samples in this SDG were analyzed on an "as received" basis.
Data Summary:
All sample data provided in this report met the acceptance criteria specified in the analytical methods and
procedures for initial calibration, continuing calibration, instrument controls and process controls where
applicable, with the following exceptions.
Technical Information
Sample Dilutions
The following sample 508725004 (Well #8) was diluted because target analyte concentrations exceeded the
calibration range. The following samples 1204539430 (Non SDG 508710008DUP) and 1204539431 (Non SDG
508710008PS) in this sample group were diluted due to matrix interference. Dilutions may be required for many
reasons, including to minimize matrix interferences or to bring over range target analyte concentrations into the
linear calibration range.
508725
Analyte
004
Bromide IOX
Certification Statement
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless otherwise noted in the analytical case narrative.
Page 12 of 15 SDG: 508725

IV
gvironment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oakmont Dr.
+ __..:n_ Mr ��0<0
Page 1 of
.iWG1l VlI1G, lYV L/VJu
.ironment I inc.com
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Plume [phone] • Fax [phone]
CHLORINE
41ENT: 132 Week: 15
pH CHECK (LAB)
❑ UV
P
VOCA, LLC (WASTEWATER)
NONE
P
P
P
P
P
P
P
P
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CONTAINER TYPE, PIG
01J�BRIAN CONNER
BOX 129
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FORM ns Grab sample in the blocks above for each parameter requested. n{0 '1 7 7 (i 71

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o
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Gi-CHL•SR-OD1 Rev&
Page 14 of 15 SDG: 508725

Dist of current GEL Certifications as of 16 April 2020
State
Certification
Alaska
17-018
Alaska Drinking Water
SCO0012
Arkansas
88-0651
CLIA
42DO904046
California
2940
Colorado
SCO0012
Connecticut
PH-0169
DoD FLAP/ ISO17025 A2LA
2567.01
Florida NELAP
E87156
Foreign Soils Permit
P330-15-00283, P330-15-00253
Georgia
SCO0012
Georgia SDWA
967
Hawaii
SCO0012
Idaho
SCO0012
Illinois NELAP
200029
Indiana
C—SC-01
Kansas NELAP
E-10332
Kentucky SDWA
90129
Kentucky Wastewater
90129
Louisiana Drinking Water
LA024
Louisiana NELAP
03046 (AI33904)
Maine
2019020
Maryland
270
Massachusetts
M—SCO 12
Massachusetts PFAS Approv
Letter
Michigan
9976
Mississippi
SCO0012
Nebraska
NE—OS-26-13
Nevada
SC000122020-1
New Hampshire NELAP
2054
New Jersey NELAP
SCO02
New Mexico
SCO0012
New York NELAP
11501
North Carolina
233
North Carolina SDWA
45709
North Dakota
R-158
Oklahoma
2019-165
Pennsylvania NELAP
68-00485
Puerto Rico
SCO0012
S. Carolina Radiochem
10120002
Sanitation Districts of L
9255651
South Carolina Chemistry
10120001
Tennessee
TN 02934
Texas NELAP
T 104704235-20-16
Utah NELAP
SCO00122020-32
Vermont
VT87156
Virginia NELAP
460202
Washington
C780
Page 15 of 15 SDG: 508725