WQ0000957_Monitoring - 03-2020_20200428

ily� -
VAI_J..EY PROTEINS, INC.
April 20, 2020
Department of Environment & Natural Resources
Division of Water Resources — Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Valley Proteins, Inc. — Wadesboro Division,
Permit #WQ0000957
Enclosed please find the Quarterly Monitoring Wells Report for our Wadesboro, North
Carolina Division.
If you require any additional information or wish to discuss the information in this report,
please feel free to call me at [phone].
Sincerely,
VaRK
General Manager
APR 2 5 2020
DV"dr, S`e s �a
I; lf>vIaD4Ti0Pl PItUE.SSiNO t11di
656 Littie [?uncan Road
%Nladesboro, NC 25170
0 940.8'%"?590
Mzikiilg ci 4LI.St- linable E)1f ,rE nce 0 04.n?4.o145
valleyproteim wits

SUBMIT FORM ON YELLOW PAPER ONLY
.
. . ,
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
NPDES Other
Permit Name (if different):
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
91 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind field #9
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from
Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#1
Date sample collected: 3/24/20
FIELD ANALYSES:
WAS
Well Depth: 33 ft.
Well Diameter: 2 in.
pH 7.2 units Temp. 15.1 °C
DRY at
Depth to Water Level: 10.16 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 1726 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
1 1.1 gallons
Appearance Clear
here:
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ElYES ❑ NO
— f
LABORATORY INFORMATION
Date sample analyzed: 3/24/20 - 4/2/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
me/I
Pb - Lead mg/I
Coliform MF Fecal N/D /100ml
Nitrate (NO3) as N
14 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.084 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 938 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7.2 units
Ba - Barium
mg/I
TOC 2 mg/I
Ca - Calcium
mg/I
Chloride 358 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 32.2 mg/I
Hg - Mercury
mg/1
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/1
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager) Z�
ermittee (or Authorized Agent) Name and Title - Please print or type orized Agent) (Date) t
GW-59 Rev. 1/2007

aceAnalytical
www.pacelabs.com
f
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92470734
Sample: MW-1 Lab ID: 92470734001 Collected: 03/24/20 09:40 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/JDS
1
03/24/20 09:40
Collected Date
03/24/20
1
03/24/20 09:40
Collected Time
09:40
1
03/24/20 09:40
pH
7.2 Std. Units
1
03/24/20 09:40
Temperature
15.1 deg C
1
03/24/20 09:40
Static Water Level
10.16 feet
1
03/24/20 09:40
Specific Conductance
1726 umhos/cm
1
03/24/20 09:40
Total Well Depth
33.05 feet
1
03/24/20 09:40
Odor
None
1
03/24/20 09:40
Appearance
Clear
1
03/24/20 09:40
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/24/20 15:08 03/25/20 14:22
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
938 mg/L 50.0
1
03/25/20 15:44
MW
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.2 Std. Units 0.10
1
03/29/20 11:41
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
32.2 mg/L 1.0
1
03/26/2018:40
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/01/20 13:14
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate
14.0 mg/L 0.20
5
03/25/20 13:02
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.084 mg/L 0.050
1
03/25/20 19:03 03/26/20 22:04
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
358 mg/L 25.0
25
03/26/2019:04
16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/02/2020 05:10 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 48

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-1 Lab ID: 92470734001 Collected: 03/24/20 09:40 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310E TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon 2.0 mg/L 1.0 1 04/02/20 06:30 7440-44-0
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 48

Document Natne; Field data Sheet
Date Issued: March 8, 2019pa
$CBArk7ditW y
e: 1 of
Document lxlumbir. F•CAR-CAR-001-tev.03
Issuing Authority: Pace Huntersville Quality-
Office .
Field Data Sheet • :)rT *,,I h e.l9/
Climf: 11f:�j PI-6 ► c� Location: k1j A- D VS r-4 0) 4c- Project #:_ Y Ord \
Name and Affiliation (Sampler(s):_ �� SPS -PfK.E FieldData Sheet Review:
Nme- and Affiliation (inspector): nli �S
Well Inforrnatian
Well ID: k.W -1 WellLocked: YE / NO / Flushmount )
Well Diameter: t i _ Construction: QV-V-C/Steel/Stainiess Steel)
Total Well Depth: 73 3 ft Multi Factor*: 2? -16 3� [*(Radius/12)2 x 3.14 is 7.49).
Static Water Level: 'ft Casing Volume: Iq gallons.
Height of Water Column: 38 ft Cal. 3 Volumes: 1 i i gallons
Pump Intake: #j) (t
Purge Infartnatiort
Date Purged: D3' / � ./ao Start: '0.; Finish 10s_ Purge Rate:
Purging Method: A �^' Total Volume'Purged: 1 allo 1111s/L)
Sainvline Information
Date Collected: f-L-/24/ B-0 Time Collected: �� Q pm)
Sampling Bquiprnent Used: 3 . Instrurnent ID:_ y J S
Bottle Type Preservation Analysis Required
3; q Vol
t—S�? sn�
— Ia / Hasp All 7"�hoj
IpK,4, 5� 1 1Nj
�. - : ., _ _ �.En <'�� c;�:xt�ritsl�.il;,. r �4soati� ,_ � � .. _ _ ,, .. •. _ _
Sample Teinp' (0q: 15.1 Time:
oR q o Turbidity (ntu):
Time: -
Digs Oxy (mgf L): •---- Time:
Fe 2+ mg/L.
Specific Cond. (uS): ace Time:
6WO Res. Cl (mg/L)/(µg/L):
Time:.
Sample pH (s.u.): 7-Time: _M46 Od"or:_ . _ N0 01
Time: 0L7C0
ReDox (qN): "--- Time.
"-' 'Appearance: dt'4 '
Time: 0940
ReDox (EH va1ue):YSI ProPlus +2Q0mV
-- Other:
Time:
General/4V aher Observations:. MAJ---)
.
:,(sunnk&*rainy) Temp. 2? (°F) Wind jO- (mph)
Sampler Signature
Stabilization 'test
Time
Purged
Temp.
(dC)
Dlss Oxy.
(mg/L)
Spec'
(S>
PH (s.u,)
ReDox
(mV
Turbidity
(ntu)
oume
r ' ved
ns 1nls/
Water
. level (ft)
Other
Page 41 of 48 i

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
[VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT- -
COMPLIANCE REPORT FORM
•
•
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
NPDES Other
Permit Name (if different):
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
1 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind field #4
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#2
Date sample collected: 3/24/20
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 7 units Temp. 14 °C
DRY at
Depth to Water Level: 5.49 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 1991 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
13.5 gallons
Appearance Murky
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/24/20 - 4/2/20
LaboratoryName: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
9.3 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.064 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 1200 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7.1 units
Ba - Barium
mg/I
TOC 1.1 mg/I
Ca - Calcium
mg/I
Chloride 437 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 11.5 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007
Agent)

Pace Analytical Services, LLC
2225 Riverside
aceAnalytical
Asheville, NC 2880404
www.pacelabs.com [phone]
I
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Sample: MW-2 Lab ID: 92470734002 Collected: 03/24/20 09:25 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JDS
1
03/24/20 09:25
Collected Date
03/24/20
1
03/24/20 09:25
Collected Time
09:25
1
03/24/20 09:25
pH
7.0 Std. Units
1
03/24/20 09:25
Temperature
14.0 deg C
1
03/24/20 09:25
Static Water Level
5.49 feet
1
03/24/20 09:25
Specific Conductance
1991 umhos/cm
1
03/24/20 09:25
Total Well Depth
33.02 feet
1
03/24/20 09:25
Odor
NONE
1
03/24/20 09:25
Appearance
Murky
1
03/24/20 09:25
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method: SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/24/20 14:45 03/25/20 14:18
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
1200 mg/L 125
1
03/25/20 15:44
MW
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.1 Std. Units 0.10
1
03/29/20 11:35
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
11.5 mg/L 1.0
1
03/26/2018:54
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/01/20 13:16
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
9.3 mg/L 0.20
5
03/25/20 13:01
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.064 mg/L 0.050
1
03/25/20 19:03 03/26/20 22:04
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
437 mg/L 25.0
25
03/26/2019:05
16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/02/2020 05:10 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 48

aceAnalytical
www.pacclabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-2 Lab ID: 92470734002 Collected: 03/24/20 09:25 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon 1.1 mg/L 1.0 1 04/02/20 07:50 7440-44-0
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 48

Document Name: Field data Sheet
Date Issued: Marc 8,2019
llagc 1 of
Document Number. F-CAR-FLD-001-rev.03
issuing Authority: Pace Huntersvilte Qualit .. -
--ace-Anal3weie
office
Field Data Sheet
Cli,!,f.- Vall-c-w 0-0.4_14"5 Location: W0,dZSJ!>or0,A.)C_ Pt9jeCt#
Name and MILtion Field' Data Sheet Review/
�v- cc_
Name- and Affiliiatiort (Inspectcr):A)lk Date: al l aC By:
Well Information
Well ID: Well .Locked: %�_MT NO / Flushinount)
Well Diameter: Construction: �,(�teel/Stairdess Steel)
Total Well Depth: 1(2. � ft Multi Factor-; r(Fadius/12)2 x 3.14 7.181.
Static Water Level: ..S-qi.__ ft CasingYalume: gallons.
Height of Water Qofurnn:_22. 53it Cal, 3 Volumes.: 1 o c 6 gallons
PumpIntake: (t
turge Information
Date Purged -Ali 3 -980 Start: Finish: 10!11- Purge Rate: I)Pr
Puiging Method:_( 30, f _Toied Volume* Purged:
Sampling Information
Date ColleAe d:9_3L_/aY/ D-02 Time Collected.—CSP �—am pm)
616 *3
Sampling Equipment Used: .__lnstruiftent.lD: Sr
Bottle Type, Preserv3t..0 Analysis Required
=0
QL
260
7- K'a
sw (n L_� L.Orr A_IZ5n,L_ t, Y -'kSo 14
f L STic—
&a,nple Tefftp- (0c): i Time Turbidity (ntu): Time:'•
Digs OxY (Jng/L)- Time: Fe2+.mg/L:
Specific Cond, Tim&. Res. 0(Tg/L)&g/L).-_=_Time:.
SarftPle PH (S.11.): Time: Odor: Nc�L Time:
ReDox (m'V): 17— Time: 'Appearance: rn Time:
ReDox (PH value):YSI PToPlus +200j1iV_�_� Other: Time:
GeneraYWeather Observations-. Vv�
(surthyAclo /r Iny) Temp. (OF) Wind ?�/(mph)
Sampler Signature
Stabilization Test
5-z-oze
Time
Purged
Temp.
('lq�
D16s Oxy.
(mg/L)
Spec.
ndPH
t
(s.u,)
ReDox
(MV)
Turbidity
(ntu)
Volume
i6roved
���inls/
Ll
Water
level (ft)S)
Other
101M -
1G. 1.
1
5
I 5.,q
10,11
1LA'
-3

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: Valley Proteins
Permit Name (if different):
Facility Address: 656 Little Duncan Road
Wadesboro NC 28170
act Person: Matt Hanks
Location/Site Name: Behind field #1
County Anson
Telephone#: [phone]
No. of wells to be sampled: 8
)EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
:)IViSiON OF WATER QUALITY -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number:
Expiration Date: 06/30/2023
Non -Discharge W00000957
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
K❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
:LL ID NUMBER (from Permit): MW#3 Date sample collected: 3/24/20
.11 Depth: 29.2 ft. Well Diameter: 4 in.
pth to Water Level: 13.4 ft. below measuring point Screened Interval: ft. to ft.
asuring Point is ft. above land surface Relative M.P. Elevation: ft.
lume of water pumped/bailed before sampling: 13.5 gallons
moles for metals were collected unfiltered: EYES ❑ NO and field acidified: ❑ YES ❑ NO
Date sample analyzed: 3/24/20 - 4/2/20 Laboratory Name: PACE Analytical
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NOZ) as N
mg/I
Coliform: MF Fecal
N/D /100ml
Nitrate (NO3) as N
5.3 mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
ND mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
1110 mg/I
Al - Aluminum
mg/I
pH (when analyzed)
7.3 units
Ba - Barium
mg/I
TOC
1.3 mg/I
Ca - Calcium
mg/I
Chloride
372 mg/I
Cd - Cadmium
mg/1
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
185 mg/I
Hg - Mercury
mg/I
Specific Conductance
µMhos
K - Potassium
mg/I
Total Ammonia
ND mg/I
Mg - Magnesium
mg/I
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
TKN as N
mg/I
Ni - Nickel
mg/1
❑ Water Source Heat Pump ❑ Other
FIELD ANALYSES:
pH 7.2 units
Spec. Cond.
Odor None
Appearance Clear
Temp. 15.8 °C
1895 uMhos
Certification No. #12
Pb - Lead mg/I
Zn - Zinc mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager) Z,
Permittee (or Authorized Agent) Name and Title - Please print or type ee (or Authorized Agent) (Datt
GW-59 Rev.1/2007
IriTlMIXIIII
ZY at
ie of
mpling,
0

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92470734
Sample: MW-3 Lab ID: 92470734003 Collected: 03/24/20 10:00 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/JDS
1
03/24/20 10:00
Collected Date
03/24/20
1
03/24/20 10:00
Collected Time
10:00
1
03/24/20 10:00
pH
7.2 Std. Units
1
03/24/20 10:00
Temperature
15.8 deg C
1
03/24/20 10:00
Static Water Level
13.41 feet
1
03/24/20 10:00
Specific Conductance
1895 umhos/cm
1
03/24/20 10:00
Total Well Depth
27.24 feet
1
03/24/20 10:00
Odor
None
1
03/24/20 10:00
Appearance
Clear
1
03/24/20 10:00
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method: SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/24/20 15:08 03/25/20 14:22
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
1110 mg/L 125
1
03/27/20 16:23
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.3 Std. Units 0.10
1
03/29/20 11:46
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
185 mg/L 4.0
4
03/27/2017:26
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/01/20 13:17
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
5.3 mg/L 0.080
2
03/25/20 13:03
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
ND mg/L 0.050
1
03/25/20 19:03 03/26/20 22:05
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
372 mg/L 25.0
25
03/26/2019:06
16887-00-6
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 48

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-3 Lab ID: 92470734003 Collected: 03/24/20 10:00 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon 1.3 mg/L 1.0 1 04/02/20 08:26 7440-44-0
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 48

`J 8C@ fjit>E y
Document Name: Field data Sheet
Date Issued: Match 8, 2019
Page: 1 of
Document Number. P-CAR-FLD-001-rev.03
Issuing Authority: Pare untenville Quality,
Office .
Location:
Name. amd Affiliation (Sampler(s): -\� CD,.' J t�,
Name -and Affiliation (Inspector): A� R
Well In'forrnati(in
Well ID: t',3 Well Locked:
Well Diameter: t �Consttuction:
Po ra)L Project #:3'C�
Field Data Sheet Review:
Date: 0 3 __,Zq_;_0
0 / Flushmount )
t�teel/Stainless Steel)
Total Well Depth: � �� _ft Multi Factor*, C�' ['(Radius/12)2 x3.14> 7.481.
Static Water Level: ISCII Q ft Casing Volume: 3 - gallons.
Height of Water Column: Cal, 3 Volumes: • �q gallons
Pump Intake: 1i (t
�_L ?mo
By:�
'Purge Information. f
Date Purged: 0 3 /!Z3/Start : � Finish: (I C7 Purge Rate: A)A-
Purging Method: �aa Total Volume'Purged: allon mis/L)
Samvlina Information 150,L/
Date Collected:yLa/2i�/0_4�0 Time Collected: 1 V
Sampling $quipment Used: ZaLkL _Instrument ID:_ '3 —
Bottle Type Pre"servafic n Analysis Required
3-�r n 1- i,lal. a °S re1 i�
- oth nnii t Z So rn L - z g,,� /Ud �r'�.� G �. �i � :b�. S�, I /V �f,�'a � /✓ �7 L��
AS
Sample Teatp (oq: 15'• s Time: CO as Turbidity (ntu): Time:1
Dins Oxy (mg/L) Time: Fe 2+ mg/L: ~' Time; r
Specific Cond. (6): 1 3 `/ � Time: 1000 Res. C1(rpg/ L)/(µg/L): — Time:.
Sample pH (s.u.): Time: Odor:. Nd n e- Time: /000
ReDox(gM: Time: Appearance: -tQatr Time: 1000
ReDox (EH value):YSI ProPlus +290=V Other: —7— ' Time:
General/WeatherObservations: i.v\W � I.)a_S N +-oto
_,(surtnyr,ou airy) Temp.-M) (°F) wind_ n t Q(mph)
Sampler Signature
Stabilization Vest
'
Time
Purged
. g
Temp.
C
i°)
Digs Oxy.
m L
( $/)
Spec.
Cond.
(US)
pH (s.u.)
ReDox
( �i
Turbidity
ntu
( )
oume
removed
0 is
� /
Water
-level (ft}
Outer
I"
t S'
r
ZoZ'3
---
--
--
c
b
q
Page 43 of 48

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF. WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
X❑ Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Pond #1
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#5
Date sample collected: 3/24/20
FIELD ANALYSES:
WAS
Well Depth: 29.2 ft.
Well Diameter: 2 in.
pH 6.7 units Temp. 13.8 °C
DRY at
Depth to Water Level: 6.46 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 2378 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
11.4 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/24/20 - 4/2/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
ND mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.074 mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 1380 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.8 units
Ba - Barium
mg/I
TOC 2.1 mg/I
Ca - Calcium
mg/I
Chloride 374 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 35.9 mg/I
Hg - Mercury
mg/1
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager) '
Permittee (or Authorized Aqent) Name and Title - Please print or type gq r Authorized Agent)
GW-59 Rev. 112007

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-5 Lab ID: 92470734004 Collected: 03/24/20 09:05 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/JDS
1
03/24/20 09:05
Collected Date
03/24/20
1
03/24/20 09:05
Collected Time
09:05
1
03/24/20 09:05
pH
6.7 Std. Units
1
03/24/20 09:05
Temperature
13.8 deg C
1
03/24/20 09:05
Static Water Level
6.46 feet
1
03/24/20 09:05
Specific Conductance
2378 umhos/cm
1
03/24/20 09:05
Total Well Depth
29.62 feet
1
03/24/20 09:05
Odor
None
1
03/24/20 09:05
Appearance
Clear
1
03/24/20 09:05
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/24/20 14:45 03/25/20 14:18
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
1380 mg/L 25.0
1
03/27/20 16:23
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
6.8 Std. Units 0.10
1
03/29/20 11:23
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
35.9 mg/L 1.0
1
03/26/2019:23
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/01/2013:19
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
03/25/20 12:46
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.074 mg/L 0,050
1
03/25/20 19:03 03/26/20 22:06
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
374 mg/L 25.0
25
03/26/2019:07
16887-00-6
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
D6, H3
Page 11 of 48

aceAnalytical
www.pacolabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-5 Lab ID: 92470734004 Collected: 03/24/20 09:05 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310E TOC Analytical Method: SM 531OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon 2.1 mg/L 1.0 1 04/02/20 08:50 7440-44-0
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 48

W Alert '
Document Name: Field data Sheet
Date Issued: March A, 2019
Pa e: l of I
Document Numb8r. F-CAR-FLD-001-rev.03
isnung Authority: Pare Huntersville Quality„-
Office
�.�
Field Data Sheet
��t�1 Locatiopt, c 1����5 BO`�; jr Project#; YViArG 2t+2i�
Name and AffiTia'tion (Sampler(s): d LXd / dMag f cr,,, held Data Sheet Review:
Name and Affiliation Jnspector).Date: ol
-
Well Information
Well tD: V' . — s Well Locked: YE / NO / Fluslunount )
Well Diameter: a I I Consttuction: (S�SteeI/Stainless Steel)
Total Well Depth: a4.b ?✓ ft
Static Water Level: re. 4 G ft
Height of Water Column: : � �ft
Multi Factor*: 0.03 3 I (Radius/12)20.14 x 7.481
Casing Volume: gallons.
Cal. 3 Volumes: gallons
Pump Intake:_ NIA {t
By: 11J
Purge Information
Date Purged: D .3 J Z ./C Start : D . '2- Finish:�S! Purge Rate:
Purging Method: 1�a J A- Total VoIume'Purged: aIlons misx)
Sampling Information
Date Collected:// l Time Collected:�Dm)
Sampling Equipment Used: t IL I _Instrurnent lD:_ YS?✓ 3 '/ (p
Bottle Type, Preservati¢n Analysis [required
f --a s�►�, _ . Nor s v �J� t awl
AfY-3
5t,14* A lj
!ff" LI}►�^� --. .. ..... . _. -
Sample Te iIp (°C): 131-3 Time: 0 ?Q Turbidity (ntu); Time:` - ~�
Dias Oxy (mg/L) ..� Time: Fe 2+ mg/1✓ �` Time;
.Specific C'.ond. (uS): g 3 _4-e Time:. 0 l OS- Res. 0 (mg/L)/(µg/L): """ Time:.
Sajtple pH (s.u.): 4a Time: 070 Od'or: _ . /I)0.4-( - Time 0 �� 5
ReDox (mV): `— Time: ---� ' Appearance: Llea r- Time: 0 S
ReDox'(EH value):YSI ProPlus +200n1V Other: --^ Time: — -
General/Weather Observations:
Sampler Signature
Stabilization Test
(sunny clou /rainy) Temp,_13� (OF) Wind . E$/o (mph)
/an
Time
Purged
Temp.
d
(C)
Digs Oxy.
(mg/L}
Spec.
Cond.
(US)
pH (s.u.)
ReDox
(mV)
Turbidity
(ntu)%mis/
o ume
meinoved
Water
.level (ft)
Other
,,cf 0
Page 44 of 48

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
(VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
61. MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
NPDES Other
Permit Name (if different):
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
a 1 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #20
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from
Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#6
Date sample collected: 3/24/20
FIELD ANALYSES:
WAS
Well Depth: 45 ft.
Well Diameter: 2 in.
pH 6.6 units Temp. 13.7 °C
DRY at
Depth to Water Level: 3.76 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 159.2 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
11 gallons
Appearance Murky
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/24/20 - 4/2/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
ND mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.27 mg/I
(Note Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 193 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.6 units
Ba - Barium
mg/I
TOC ND mg/I
Ca - Calcium
mg/I
Chloride 14.6 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 6.6 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen. NH3as N: Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.1/2007
Aqent)

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-6 Lab ID: 92470734005 Collected: 03/24/20 10:55 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua)
Monitoring Well Data
Collected By
Collected Date
Collected Time
pH
Temperature
Static Water Level
Specific Conductance
Total Well Depth
Odor
Appearance
MBIO 9222D Fecal Coliform CHT
Fecal Coliforms
2540C Total Dissolved Solids
Total Dissolved Solids
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
365.1 Phosphorus, Total
Phosphorus
4500 Chloride
Chloride
Date: 04/02/2020 05:10 PM
Analytical Method:
Pace Analytical Services - Charlotte
JJQ/JDS
1
03/24/20 10:55
03/24/20
1
03/24/20 10:55
10:55
1
03/24/20 10:55
6.6 Std. Units
1
03/24/20 10:55
13.7 deg C
1
03/24/20 10:55
3.76 feet
1
03/24/20 10:55
159.2 umhos/cm
1
03/24/20 10:55
44.90 feet
1
03/24/20 10:55
None
1
03/24/20 10:55
Murky
1
03/24/20 10:55
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
ND CFU/100 mL 1.0
1
03/24/20 15:08 03/25/20 14:22
Analytical Method: SM 2540C-2011
Pace Analytical Services -Asheville
193 mg/L 25.0
1
03/27/2016:23
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
6.6 Std. Units 0.10
1
03/29/20 12:09
H3
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
6.6 mg/L 1.0
1
03/26/2019:38
14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.10
1
04/01/2013:20
7664-41-7
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/L 0.040
1
03/25/2012:58
14797-55-8
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
0.27 mg/L 0.050
1
03/25/20 19:03 03/26/20 22:08
7723-14-0
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
14.6 mg/L 1.0
1
03/26/2019:08
16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 48

JceAnalXical"
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-6 Lab ID: 92470734005 Collected: 03/24/20 10:55 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon ND mg/L 1.0 1 04/02/20 09:26 7440-44-0
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 48

J. aceArjaldltTeal�
Document Name: Field data Sheet
Date Issued: March 8, M19
Page: 1 of I
Document I�Jumbpr. F-CAR-FLD-001-rev.03
Issuing Authority; Pace Huntenville Quality.-
Office .
PC
rieja Data Sheet
lJe.o%-i for ra
Name and Affiliation (Sarnpler(s):_ -
Name and Affiliation (inspector):- . ✓1�/� �--�
Well Information
Well ID: _ . 6 Well Locked:
Well Diameter: I" Construction: G
✓� project #: S ��
:ld Data Sheet Review:
Date: 03 - �4-ab
ATO / Flushmount )
eel/Stainless Steel)
Total WeIlDepth: `I�f,` o ft Multi Firctor*:©.�� r(Radius/12)2x3.14x7481.
Static Water Level: �•-..`ft Casing Volume: gallons.
Height of Water Column: QL % it . Cal. 3 Voluines: -gallons
Pump Intake: 0/-)- ft
By: V
Varge Information.
Date Pur'ged.4 • / -/ .,Z Start •�_ Finish.- 1 �•�� Purge!rater
PuxgingMethod:�� ! 2 Total Volume'Purged: H - gallons s/L)
Samplinglnformation
Date Collected:31_±/ 20 Time Collected: � � an`pm) '
Sampling $quipmentUsed: ?iAAty' _Instrument ID:- L6
Bottle Type Preservafien Analysis Required
-2 /UO/1 P . Tp c 1 sly!
"+`--x1&rIIC�',ri':�ieiE�uli"'lialYtSJ F��.�iy"�3.~x ..-:...,..... :+•. �. », rw.,.. .:5,:. s:,.,, -
Sampleemp (°C): 13 Time: /O: y Turbidity (ntu): Time: —�
Dim Oxy (mg/L): Time: Fe 2+ mg/L:-
edp
Specific Cond. Time �0 :` Res. Cl (mg/L)/(µg/L): Time:.
�o
Sample pH (s. afro e: /O: Odor:.-jS�41✓� Time:
ReDox (mV): Time: Appearance: ) 1 GtY- k Time:
ReDox (EH value):YSI ProPlus +200mV Other: Time:
General/Weather Observations: - c
Sampler Signature
Stabilization Test
/ oudy rainy) Temp. 5a (OF) WindS-210 (mph)
tw 3 l."-q ):2.0 .
Time
Purged
Temp.
CC)
Digs Oky.
(mg/L)
Spy'
Cond.
pH (s.u.)
ReDox
(nnV)
Turbidity
(ntu)
oume
reinoved
ons 1s/
Water '
Other
(US)
.level (ft)
r
+
Page 45 of 48

SUBMIT FORM ON YELLOW_ PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
��15117
MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 <Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
1 Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #19
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#7
Date sample collected: 3/24/20
FIELD ANALYSES:
WAS
Well Depth: 52 ft.
Well Diameter: 2 in.
pH 7.3 units Temp. 16.8 °C
DRY at
Depth to Water Level: 17.63 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 539.9 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling:
10 gallons
Appearance Clear
here:
El
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/24/20 - 4/2/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NOZ) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
.19 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100m1
Phosphorus: Total as P
ND mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 539.9 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7.3 units
Ba - Barium
mg/I
TOC ND mg/I
Ca - Calcium
mg/I
Chloride 33 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 17.1 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Agent) Name and Title - Please print or type
Aqent)
GW-59 Rev. 1/2007

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-7 Lab ID: 92470734006 Collected: 03/24/20 10:40 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/JDS
1
03/24/20 10:40
Collected Date
03/24/20
1
03/24/20 10:40
Collected Time
10:40
1
03/24/20 10:40
pH
7.3 Std. Units
1
03/24/20 10:40
Temperature
16.8 deg C
1
03/24/20 10:40
Static Water Level
17.63 feet
1
03/24/20 10:40
Specific Conductance
539.9 umhos/cm
1
03/24/20 10:40
Total Well Depth
53.30 feet
1
03/24/20 10:40
Odor
None
1
03/24/20 10:40
Appearance
Clear
1
03/24/20 10:40
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/24/20 15:08 03/25/20 14:22
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Pace Analytical Services -Asheville
Total Dissolved Solids
505 mg/L 25.0
1
03/27/20 16:23
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services -Asheville
pH at 25 Degrees C
7.3 Std. Units 0.10
1
03/29/20 12:04
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
17.1 mg/L 1.0
1
03/26/2019:52
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/01/20 13:24
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.19 mg/L 0.040
1
03/25/20 12:57
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050
1
03/25/20 19:03 03/26/20 22:09
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
33.0 mg/L 1.0
1
03/26/2019:09
16887-00-6
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
H3
Page 15 of 48

aceAnalytical
www.pacelabs.eom
f
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-7 Lab ID: 92470734006 Collected: 03/24/20 10:40 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services - Asheville
Total Organic Carbon ND mg/L 1.0 1 04/02/20 11:03 7440-44-0
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, -LC.
Page 16 of 48

%=
i
Document Name; Field data Sheet
Date Issued: March 8, 2019
Page: 1 of
Document M1umb2r. F-CAR-FLD-001-cev.03
Issuing Authority: Pare Huntersville Quality+
dire
Name alid Affiliation
Name and Affiliation (Inspector):_ A11A
Well Information
Well YD: f�'i jii�. - . Well Locked:
Well Diameter:' a Construction:
Total Well Depth; 53. O ft
Static Water Level: ft
Height of Water Column: 3 ft
ii�eet - di�^uft 26ap
Mip NG Project
Field Data Sheet Review:
Date; 0 'ILA 1110 By:
<[9$/ NO / Flushmount )
V� Steel/Stainless Steel)
Multi Factor'`:_ r(Radius/12)2 x ,14 z 7.48].
Casing Volume:I gallons.
Cal, 3 Voluines: i '--f , gallons
Pump Intake: �j' /t it
V,urge Information.
Date Purged: 03 / P. 3 ./ .2-LQ Start : i? q Y Finish Purge Rate: A',k
Pur'gingMethod: &t� TotslVolume'Purged: U Eo�n
mISA)
Ur�SainvlingL,Information "
Date Collected: f}_22'/Q8/_RQ_ Tfine Collected: (am/PM)
SampUTLg Equipment Used: o AA".. Instrutitent jD:_ t/`;:,
Bottle Type Preservafi4n Analysis Required
-St�pr�Q i. aSrJ►sLT�iaS� A[a�1 I ,{oYit So 1 )AJlkt .
_ Lt
w.._.,.
oeutslt,�beiva><Isaiss.:....
� r�
Sample TejAp, (°C): _(0 _Time._ Turbidity (ntu): Time
Dias Oxy (mg/�L�L
Time: Fe 2+ mg/L..
�% biuF1•iv
Specific Cond. Time: �0Res. Cl (mg/L)/(µg/L): Time:.
Saiiipl� pH (s.u,): Time: Odox: �J��i Time•
ReDox (mV): - — Time: -Appearance: LI f u Y' Time:_
ReDox (EH value):YSI ProPlus +200mV ' Other: Time.
GeneraMeather Observations: ) W ::9— .
(sunny/ oud rainy) Ternp. _D (°F) Wind �(mph)
Sampler Signature
Stabilization Test
Time
Purged
8e
Temp.
CC)
( )
Diss Ozy.
m /L
{ g )
Spec.
Cand.
(US)
pH (s,u,)
ReDox
{ m
Turbidity
niu
{ }
oume
r ' ved
o mis
{ /
Water
level (ft)
Other
1
Page 46 of 48

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
IVISIONOFWATER QUALITY4NFOR ATIONPROCESSINGUNIT
COMPLIANCE REPORT FORM
617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print
Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
X❑ Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #16
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#8
Date sample collected: 3/24/20
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 6.9 units Temp. 14.5 °C
DRY at
Depth to Water Level: 1.41 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 801 µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
check
Volume of water pumped/bailed before sampling: 11.70 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: 3/24/20 - 4/2/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
ND mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.088 mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 324 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 7 units
Ba - Barium
mg/I
TOC ND mg/I
Ca - Calcium
mg/I
Chloride 149 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 11.7 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
Aqent)
z
GW-59 Rev.1/2007

;I�Wce Analytical "
www.pacelabs.eom
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92470734
Sample: MW-8
Lab ID: 92470734007 Collected: 03/24/20 10:30
Received: 03/24/20 12:30 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Collected By
JJQ/JDS
1
03/24/20 10:30
Collected Date
03/24/20
1
03/24/20 10:30
Collected Time
10:30
1
03/24/20 10:30
pH
6.9 Std. Units
1
03/24/20 10:30
Temperature
14.5 deg C
1
03/24/20 10:30
Static Water Level
1.41 feet
1
03/24/20 10:30
Specific Conductance
801 umhos/cm
1
03/24/20 10:30
Total Well Depth
29.60 feet
1
03/24/20 10:30
Odor
None
1
03/24/20 10:30
Appearance
Clear
1
03/24/20 10:30
MBIO 9222D Fecal Coliform CHT
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
03/24/20 15:32 03/25/20 14:28
2540C Total Dissolved Solids
Analytical Method: SM 254OC-2011
Pace Analytical Services - Asheville
Total Dissolved Solids
324 mg/L 25.0
1
03/27/20 16:23
4500H+ pH, Electrometric
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
pH at 25 Degrees C
7.0 Std. Units 0.10
1
03/29/20 11:58
H3
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
11.7 mg/L 1.0
1
03/26/20 20:07
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
04/01/2013:26
7664-41-7
353.2 Nitrogen, N021NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
ND mg/L 0.040
1
03/25/20 12:56
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Phosphorus
0.088 mg/L 0.050
1
03/25/20 19:03 03/26/20 22:09
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
Chloride
149 mg/L 5.0
5
03/27/2018:48
16887-00-6
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 48

aceAnalXical
www.pacelabs.com
ANALYTICAL RESULTS
Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-8 Lab ID: 92470734007 Collected: 03/24/20 10:30 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 531 OB-2011
Pace Analytical Services -Asheville
Total Organic Carbon ND mg/L 1.0 1 04/02/20 11:27 7440-44-0
Date: 04/02/2020 05:10 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 48

Document Name; Field data Sheet
Date issued: Mur A, 2019
,ay•
Page. lof_j
Document Number. F•CAR-CAR-001-rev.03
Issuing Authority; Pace Huntersville Quality-
Office .
Clii'nf:�
Name aitd
r MN%, -
Name and Affiliation (Inspector): A
Well Information
Well ID: -AU) - 12 . Welt Locked: ' NO / Flushmount )
Consttuction: teel/Stainless Steel)
Multi Factor*: [(Radius/12)2 x 3.14 x 2.48J.
Casing Volume: �� - b� gallons.
Cal. 3 Volumes: G gallons
Well Diameter: a It
Total Well Depth: �.R'. ft
Static Water Level: (, A--'.ft
Height of Wafter Column:ft
,ld Data Sheet Review:
Date: By: 0
Pump Intake:_ . V_T ��ft
Purge Iitfoiination.
Date Purged; " PC Stan: 71 Finish 2l 3 1 . Purge hate:
ISurgingMethod:Tot alVolume'Purged: �af�II'on`s'�mis/L)
+ DKy
Sairtipling Information
Date Collecfe 0_4/_; Time Collected: ©3z' pm)
Sampling Equipment Used: • Instrurztent ID:_ .3 S k _
Bottle Type- Preservati n Analysis Required
NO
VIA 5+' c
.., ....-.�.. V,6,1.�:i^s�ff�"Jd:"YI:R"$'S`l:ilt'J�c�Qfi��YV6f't.'�.??�•....... .......,_ ..�., _. �..r✓:....__a:is:_.�--..� � c -.. w.._.., .... _ -..-. .-._.._ , .. _ .-,�..Y ...... ...�......, ...
Sample Temp- (°C): 1'�, `� Time: / b 3Z Turbidity (ntu): Time: T
Digs Oxy (rng/L): r=-- Time: Fe 2+ mg/L: Time:. -
Specific Cond. (uS): t) Time 3 0 Res. Cl (mg/L)/(µg/L): ---Time:.
Sample, pH (s.u.): Time: D 3 Odor: A/0YI C _ Time:
ReDox (mV): "Jr Time: Appearance: j �a ✓ Time: / 0 3 (7
ReDox {EH value):YSI ProPlus +200rtzV r Other: Time:
GeneraV6Veather Observations: 1yj ' 1IN
Sampler Signature
Stabilization Test
/rainy) Temp ,1�(OF) Wind a+o_(mph)
I'-4 l
Time
Purged
Temp.
Cq
Digs Ogy.
(mg/L)
Spy'
(S) .
pK (s.w)
ReDox
(mV)
Turbidity
(ntu)
oume
r owed
( oils Is/
Water `
level (ft)
Other
r
y
T
�y
-I
..��
'DV a
Page 47 of 48

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL: RESOURCES
GROUNDWATER QUALITY MONITORING:
m-e`
VISION OP WATER QUALITY4NFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
17 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 06/30/2023
Facility Name: Valley Proteins
Non -Discharge W00000957 UIC
Permit Name (if different):
NPDES Other
Facility Address: 656 Little Duncan Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Wadesboro NC 28170 County Anson
K❑ Spray Field ❑ Remediation:
Contact Person: Matt Hanks
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Behind Field #14
No. of wells to be sampled: 8
❑ Water Source Heat Pump ❑ Other:
from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#9
Date sample collected: 3/24/20
FIELD ANALYSES:
WAS
Well Depth: 30 ft.
Well Diameter: 2 in.
pH 6.9 units Temp. 14.7 °C
DRY at
Depth to Water Level: 8.72 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. 1841 µMhos
time of
sampling,check
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor None
Volume of water pumped/bailed before sampling:
9.9 gallons
Appearance Clear
here: ❑
Samples for metals were collected unfiltered: El YES
❑ NO and field acidified: ❑ YES El NO
LABORATORY INFORMATION
Date sample analyzed: 3/24/20 - 4/2/20
Laboratory Name: PACE Analytical
Certification No. #12
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal N/D /100ml
Nitrate (NO3) as N
.82 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
.081 mg/I
(Note. Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 1841 mg/I
Al - Aluminum
mg/I
pH (when analyzed) 6.9 units
Ba - Barium
mg/I
TOC ND mg/I
Ca - Calcium
mg/I
Chloride 421 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 29.1 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia ND mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen, NH,as N, Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Matt Hanks (General Manager)
Permittee (or Authorized Aqent) Name and Title - Please print or type
Aqent)
Z
GW-59 Rev.1/2007

aceAnalytical
www.pacelabs.com
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Project: Sprayfield Wells
Pace Project No.: 92470734
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW-9 Lab ID: 92470734008 Collected: 03/24/20 10:15 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data
Collected By
Collected Date
Collected Time
pH
Temperature
Static Water Level
Specific Conductance
Total Well Depth
Odor
Appearance
MBIO 9222D Fecal Coliform CHT
Fecal Coliforms
2540C Total Dissolved Solids
Total Dissolved Solids
4500H+ pH, Electrometric
pH at 25 Degrees C
300.0 IC Anions 28 Days
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
365.1 Phosphorus, Total
Phosphorus
4500 Chloride
Chloride
Date: 04/02/2020 05:10 PM
Analytical Method:
Pace Analytical Services - Charlotte
JJQ/JDS
1
03/24/20 10:15
03/24/20
1
03/24/20 10:15
10:15
1
03/24/20 10:15
6.9 Std. Units
1
03/24/20 10:15
14.7 deg C
1
03/24/20 10:15
8.72 feet
1
03/24/20 10:15
1841 umhos/cm
1
03/24/20 10:15
29.23 feet
1
03/24/20 10:15
None
1
03/24/20 10:15
Clear
1
03/24/20 10:15
Analytical Method: SM 9222D-2006 Preparation
Method:
SM 9222D-2006
Pace Analytical Services - Charlotte
ND CFU/100 mL 1.0
1
03/24/20 14:45 03/25/20 14:18
Analytical Method: SM 2540C-2011
Pace Analytical Services - Asheville
710 mg/L 125
1
03/27/2016:23
Analytical Method: SM 4500-H+B-2011
Pace Analytical Services - Asheville
7.0 Std. Units 0.10
1
03/29/20 11:52
H3
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
29.1 mg/L 1.0
1
03/26/20 20:21
14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/L 0.10
1
04/01/2013:30
7664-41-7
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services - Asheville
0.82 mg/L 0.040
1
03/25/2012:55
14797-55-8
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services - Asheville
0.081 mg/L 0.050
1
03/25/20 19:03 03/26/20 22:10
7723-14-0
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services - Asheville
421 mg/L 20.0
20
03/27/2018:51
16887-00-6 M6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 48

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Sprayfield Wells
Pace Project No.: 92470734
Sample: MW-9 Lab ID: 92470734008 Collected: 03/24/20 10:15 Received: 03/24/20 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC
Total Organic Carbon
Date: 04/02/2020 05:10 PM
Analytical Method: SM 531 OB-2011
Pace Analytical Services -Asheville
ND mg/L 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
04/02/2011:57 7440-44-0
Page 20 of 48

i eAn.?fyffc&'
Document Name: Field data Sheet
Date Issued: March 8, 2019
Page: 1 oi_If
Document Number. FCAR-CAR-001-rev.03
Issuing Authority: Pace Huntersville Quality,.
Office .
rlelcl Data Sheet
Clienf• PCl7S P,f +1S Location:4C f0ject
Name and Affiliation (Sampler(s)._ %Sb5 - !c C- Field' Data SheetReview:
Name and Affiliation (Inspector): N/A
Well Infozrrlation Date: 0 3.7-4' ZO
Well ID: " ��_ _ Well Locked: T�K / NO / Flushmount )
Well Diameter: tj Construction: VbSteel/Stainless Steel)
Total Well Depth: '2(7 -it
Static Water Level: 9 ZZ2 ft
Height of Water Column: RCI5
Multi Factor*:0-16�0) l*(Radius/12)2 x 3.14 x 7.48].
Casing Volume: 73 gallons.
Cal. 3 Volumes: gallons
Pump Intake: AIJA- ft
By:17ps
Purge Inforaeatl'on
Date Purged: a � / �AD Siam j Finish: ram! Purge Rate:
Purging Method: + +-mil Total Volume'Purged: �'� E9mlsl L)
Sampling Information
Date Collected:. �3/ ` act Tirtte Collected:_ C2 pm)
Sampling Equipment Used: 61t [ jzL Instrument ID:_ V S L ei / lol
Bottle Type Pre-servati¢n Analysis Required
j 40 •ram %l o4 Y�jq 0S j� c,t ID
-_ I'� ��,.,� �zzz•s:rttis/f)bservattoats . .. . _ --;: __., .:�.,w. --- •;• -.-< ,�• :: ;...., ;; - ..:.,.. ::. -. - - _ _ ., ... r �...,. _ . �...;
Sample Teihp• (°C-1: _�L_Time:_ Turbidity (ntu): Time:"
Digs Oxy (mgjQ: Time: Fe 2+.rag/L: - Timer
Specific Cond. (us): —141 Time: Q1 5 -Res. Cl (mg/L)/(µg/L): = Time:.
Sadtple pH (s.u.): (01 2 - Tine: . 10,15-. Od'or:_ 'r) Time:
ReDox (rnV .- """ Time: `—' Appearance: CleGv^ Time: /p
ReDox (EH value):YSI ProPlus +200=V - Other: `—^' Time:
General/Weather Observations: iv1
(sunny ou rainy) Temp.11� (°F) Wind at Q (mph)
Sampler Signature
Stabilization Test
Time
Purged
Temp.
(C)
Digs Oxy.
(mg/L)
Spec.
Cond.
(US)
PH (s.u.)
ReDox
Turbidity
(ntu)
a ume
owed
ons mis/
Water
.level (ft)
Other
o
4,0
J M
Dup..--
Page 48 of 48

GW-59A COMPLIANCE REPORT FORM Permit #
(Submit one each monitoring period with GW_59 forms.)
W00000957
1
Enter date monitoring results were due. ( 4/30/2020 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
N
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)?f the answer is "YES", contact to Regional Office for guidance
4
Are any monitoring constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES'list the affected wells individually with constituents(s) and concentration(s)
exceeding standards in the space provided below:
MW# 1, 2, 3, 5, 7 and 9 exceed ground water standards for Total Dissolved Solids.
MW# 1, 2, 3, and 5 exceed for chlorides.
MW#1 exceeds for nitrate.
5
For the same constituents identified in question 4 above, have standards been exceeded previously for the
YE:S
NO
same constituents s in the same wells s in the last two ears?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES"Dist in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
See Report enclosed.
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
:YES
NO
If the answer is "YES", a groundwater quality problem may be occuring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO'tontact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permitteee to a Notice of Violation
fines, and/or penalties.
Piezometers were placed in the irrigation fields to determine water quality .
Total Dissolved Solids and Chlorides are naturally high in this area.
Sprinkler heads were purposely capped off near monitoring well #1 as instructed by Jim Barber (Regional Engineer)
to see If the nitrate level will change in the well.
8
The Person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true an complete to the best of my knowledge.
S' eoa (or Authorized Agent) D o
GW-59