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HomeMy WebLinkAboutWQ0001817_Monitoring - 03-2020_20200424t GW-59A COMPLIANCE REPORT FORM Permit # Mzo od j !Y f 7 (Submit one each monitoring period with GW-59 forms.) 761 j Enter date monitoring results were due. ( - 3i ,ts Will this monitoring report (GW-59 and GW-59A) YES be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW-#- 1,t0 Mw 0-3- ID �" s3 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the lasttwo years). j4CAc�cc Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation maybe➢ required to determine the impact the waste disposal system " having at the review and com boundaries surroundina this facil' ure to do so may s -'ect the ermittee to a t►" fines, and/or penalties. 'L 2020 a 71 uNk n ;'rcce sirs APR 2 9 2024 m 7 Unit In{crrnatio D\N Section � � On, o 8 The person completing this portion (GW--59A) of the monit g regik slip-tld sign below and submit this form with GW-59 forms for required wells to the address p� ided at the- of the current GW-59 form. I hereby acknowledge that the above information was evaltr-3ted and the information submitted in this report (Compli a Report GW-59A) is true and complete to the best of my knoiA ledge. 4 'm Sign of Flermiftee (or ipthorized Agent) Date GW-59A 12/8/2003 ap PA N - 71ct _ �qq S�- 6 - Lf `� olara o� ?, a oII M to 4:tj Ll _=(o9 z-ow`?N-1-1(o-i9 my �r� ` 3� dy 4cl _ r _S> 3 — 7r(p `l t/ f 1- C�.D7 '7 7 •C 11 l�s Lo I m w- 9 AAv W VV _._. M VV4 pv\ vv Lrz5 -<-; P/4 S = 5, g� (o ' S.Y� T Ds Mw - &-A TO s /'4 w - (,;, -s"6 1 �o► > oo TfD S-�:- Nt ui SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Comapany Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island RD TYPE OF PERMITTED OPERATION BEING MONITORED Hertford N.0 27944 County Perqimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: North of Holding Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: trap Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -1-A Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 5.99 units Temp. 000lo: 15.7 °C DRY at Depth to Water Level 82546: 10.8 ft. below measuring point Screened Interval: -5 ft. to -20 ft. Spec. Cond. 000sa: µMhos time ofsampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan Tint here: Samples for metals were collected unfiltered: ❑ YES 0 NO and field acidified: ❑YES ®NO LABORATORY INFORMATION Date sample analyzed:03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.18 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 rng/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 330 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 5.99 units Ba - Barium 01007 ug/L TOC 00680 4•7 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 17 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron olo45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L voc Removal io Shayne Byrum Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Kev. Ub-U/-LUltf SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ElRotary Distributor ElLand Application of Sludge Well Location/Site Name: East of Baffle Lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 A Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH oo400: 5.44 units Temp. 000lo: 14.6 oC DRY at Depth to Water Level 82546: 2.3 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µ time ofMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 5•0 gallons Appearance Yellowlran here: El Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environment Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 rng/L Nitrite (NO2) as N 00615 0.06 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 23 colonies /100mL Nitrate (1403) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 158 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 5.44 units Ba - Barium 01007 ug/L TOC oo68o 30.4 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 17 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type (or GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • . 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South East of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 3 - A Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.39 units Temp. 000lo: 14.5 oC DRY at Depth to Water Level 82546: 3.4 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µ time ofMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: Sulfur check Volume of water pumped/bailed before sampling: 3 gallons Appearance Tan/Turbid here: El Samples for metals were collected unfiltered: ❑ YES A NO and field acidified: ❑ YES 0 NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.08 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 600 coloniess /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 760 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.39 units Ba - Barium 01007 ug/L TOC 00680 19•2 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.436 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type (or AgWrized Agent) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 4- A Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 6.48 units Temp. 00010: 14.0 -C DRY at Depth to Water Level 82546: 3.2 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Slight Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Brown here: El Samples for metals were collected unfiltered: ❑ YES A NO and field acidified: ❑ YES A NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.11 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 800 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 203 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.48 units Ba - Barium 01007 ug/L TOC 00680 33.4 mg/L Ca - Calcium 00916 mg/L Chloride oo94o <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.29 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Pennittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South West of Sprayfield No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 5-A Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.44 units Temp. 000lo: 14.5 oC DRY at Depth to Water Level 82546: 4.9 ft. below measuring point Screened Interval: 12 ft. to 2 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Non check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Brown here:❑ Samples for metals were collected unfiltered: ❑ YES A NO and field acidified: ❑ YES A NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 358 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.44 units Ba - Barium 01007 ug/L TOC 00680 11.5 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 57 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Agent) Name and Title - Please print or type Agent) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY • DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West Of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 6-A Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.91 units Temp. 000io: 14.4 oC DRY at Depth to Water Level 82546: 7.2 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5•0 gallons Appearance Tan/Brown here:❑ Samples for metals were collected unfiltered: ❑ YES A NO and field acidified: ❑ YES NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 653 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 5.91 units Ba - Barium 01007 ug/L TOC 00680 5.6 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 199 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oio45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Secretary - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery N Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West of Baffle lagoon No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 7 Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 16.9 ft. Well Diameter: 2 in. pH 00400: 6.43 units Temp. 00010: 14.3 -C DRY at Depth to Water Level 82546: 2.7 ft. below measuring point Screened Interval: 11.9 ft. to 16.9 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2•5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance ReddishfTan here:❑ Samples for metals were collected unfiltered: ❑ YES 0 NO and field acidified: ❑ YES 0 NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 389 mg/L All - Aluminum oilo5 mg/L pH (Lab) 00403 6.43 units Ba - Barium 01007 ug/L TOC oo68o 32.4 mg/L Ca - Calcium 00916 mg/L Chloride 00940 39 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total oio34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.475 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese oio55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%a Shayne Byrum - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ■❑ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: East of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 8 Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 5.88 units Temp. 000lo: 14.9 aC DRY at Depth to Water Level 82546: 3.2 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan here: Samples for metals were collected unfiltered: ❑ YES 0 NO and field acidified: ❑ YES NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 2700 colonies /100mL Nitrate (NO3) as N 00620 0.09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 307 mg/L All - Aluminum oil o5 mg/L pH (Lab) 00403 5.88 units Ba - Barium 01007 ug/L TOC 00680 4•7 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 98 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oto45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 < 0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secetary Permittee (or Authorized Agent) Name and Title - Please print or type (or Agent) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Te►ephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 9 Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.31 units Temp. 000lo: 15.5 oC DRY at Depth to Water Level 82546: 4.4 ft. below measuring point Screened Interval: 4 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000s5: Slight Sulfur check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan/Brown here:❑ Samples for metals were collected unfiltered: ❑ YES 2 NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 47 colonies /100mL Nitrate (NO3) as N 00620 0.22 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 88 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.31 units Ba - Barium 01007 ug/L TOC 00680 6.8 mg/L Ca - Calcium 00916 mg/L Chloride oo94o <5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permiftee (or Authorized Aqent) Name and Title - Please print or type Agent) GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford N.C. 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 03-26-2020 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.20 units Temp. 000lo: 15.4 oC DRY at Depth to Water Level 82546: 4.9 ft. below measuring point Screened Interval: 5 ft. to 14 ft. Spec. Cond. 00094: µM time ofhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/tan here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES A NO LABORATORY INFORMATION Date sample analyzed: 03-26-2020 / 04-08-2020 Laboratory Name: Environmental Chemists„ Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 6 colonies /100mL Nitrate (NO3) as N 00620 0.24 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 79 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 6•20 units Ba - Barium 01007 ug/L TOC 00680 1.1 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oio45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese oio55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum Corporate Secretary Perrnittee (or Authorized Agent) Name and Title - Please print or type Agent) GW-59 Rev.06-07-2018 a' sus! ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Lab ID Sample ID: 20-12564 Site: MW-1 Test Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 liowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, INC 28540 • 910.347.5843 Lab/Fax info(cvenvironmentalchemists.com Date of Report: Apr 14, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-05097 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 3/26/2020 10:40 AM Water Jay Baker Method Color Depth to Water, Ft. EPA 350.1 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 B SM 4500 Cl E SM 4500 H B SM 5310 B SM 9222D MF EPA 353.2 EPA 353.2 Subtraction Method Results Date Analyzed Tan Tint 03/26/2020 10.8 feet 03/26/2020 <200 pg/L 04/09/2020 5.0 gallons 03/26/2020 Sulfur 03/26/2020 330 mg/L 03/27/2020 15.7 C 03/26/2020 17 mg/L 04/06/2020 5.99 units 03/26/2020 4.7 mg/L 03/26/2020 <1 Colonies/100ml- 03/26/2020 0.18 mg/L 03/27/2020 0.11 mg/L 04/06/2020 <0.02 mg/L 04/08/2020 Report #: 2020-05097 Page 1 of 10 LL envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 25.5-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax i,nfo(4.environmentalchemists.com Albemarle Utility Date of Report: Apr 14, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-05097 Project ID: Monitoring Wells Lab ID Sample ID: 20-12565 Site: MW-2 Test Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Calc) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Collect Date/Time Matrix Sampled by 3/26/2020 10:53 AM Water Jay Baker Method Color Depth to Water, Ft. EPA 350.1 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 B SM 4500 Ct E SM 4500 H B SM 5310 B SM 9222D MF EPA 353.2 EPA 353,2 Subtraction Method Results Date Analyzed Yellow/Tan 03/26/2020 2.3 feet 03/26/2020 <200 pg/L 04/09/2020 5.Ogallons 03/26/2020 Sulfur 03/26/2020 158 mg/L 03/27/2020 14.6 C 03/26/2020 17 mg/L 04/06/2020 5.44 units 03/26/2020 30.4 mg/L 03/26/2020 23 Colonies/100mL 03/26/2020 0.06 mg/L 03/27/2020 < 0.02 mg/L 04/06/2020 <0.02 mg/L 04/08/2020 Report M: 2020-05097 Page 2 of 10 • envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 I..ab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax in fo(ci?env i ronmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Apr 14, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-05097 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12566 Site: MW-3 3/26/2020 11:44 AM Water Jay Baker Test Method Results Date Analyzed Color color Tan/Turbid 03/26/2020 Depth to water, ft. Depth to Water, Ft. 3.4 feet 03/26/2020 Ammonia Nitrogen EPA 350.1 436 pg/L 04/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 3 (dry) gallons 03/26/2020 Odor Qualitative Sulfur 03/26/2020 Total Dissolved Solids (TDS) SM 2540 c 760 mg/L 03/27/2020 Temperature SM 2550 B 14.5 C 03/26/2020 Chloride SM 4500 Cl E 7 mg/L 04/06/2020 pH SM 4500 H e 6.39 units 03/26/2020 Total Organic Carbon (TOC) SM 5310 B 19.2 mg/L 04/01 /2020 Fecal Coliform SM 9222D MF 600 Colonies/100mL 03/26/2020 Nitrate Nitrogen (Cale{ Nitrite Nitrogen EPA 353.2 0.08 mg/L 03/27/2020 Nitrate+Nitrite-Nitrogen EPA 3532 0.03 mg/L 04/06/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/08/2020 Report #:: 2020-05097 Page 3 of 10 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, ,NC 28405 e 910.392.0223 Lab e 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, ;NC 28540 e 910.347.5843 Lab/Fax info(i�environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Apr 14, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-05097 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12567 Site: MW-4 3/26/2020 11:31 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Brown 03/26/2020 Depth to water, ft. Depth to Water, Ft. 3.2 feet 03/26/2020 Ammonia Nitrogen EPA 350.1 290 pg/L 04/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2020 Odor Qualitative Slight Sulfur 03/26/2020 Total Dissolved Solids (TDS) SM 2540 C 203 mg/L 03/27/2020 Temperature SM 2550 B 14.0 C 03/26/2020 Chloride SM 4500 Cl E < 5 mg/L 04/06/2020 pH SM 4500 H B 6.48 units 03/26/2020 Total Organic Carbon (TOC) SM 5310 B 33.4 mg/L 04/01 /2020 Fecal Coliform SM 9222D MF 800 Colon ies/1 00ml- 03/26/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2 0.11 mg/L 03/27/2020 Nitrate+ N itrite-Nitrogen EPA 353.2 < 0.02 mg/L 04/06/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/08/2020 Report #:: 2020-05097 Page 4 of 10 s , s �SM7 ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Lab ID Sample ID: 20-12568 Site: MW-5 Test Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+Nitrite-Nitrogen Nitrate Nitrogen Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(cuenvi ron men talchemists. com Date of Report: Apr 14, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-05097 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 3/26/2020 11:19 AM Water Jay Baker Method Color Depth to Water, Ft. EPA 350.1 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 B SM 4500 Cl E SM 4500 H B SM 5310 B SM 9222D MF Results Date Analyzed Tan/Brown 03/26/2020 4.9 feet 03/26/2020 <200 pg/L 04/09/2020 5.0 gallons 03/26/2020 None 03/26/2020 358 mg/L 03/27/2020 14.5 C 03/26/2020 57 mg/L 04/06/2020 6.44 units 03/26/2020 11.5 mg/L 03/26/2020 <1 Colonies/100mL 03/26/2020 EPA 353.2 < 0.02 mg/L 03/27/2020 EPA 353.2 < 0.02 mg/L 04/06/2020 Subtraction Method <0.02 mg/L 04/08/2020 Report #: 2020-05097 Page 5 of 10 Environmental Chemists, Inc. sne; ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way, Wilmington, NC 25405 • 910.392.0223 Lab • 91.0.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(4environmentatchemists.eom Albemarle Utility Date of Report: Apr 14, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-05097 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12569 Site: MW-6 3/26/2020 11:06 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Brown 03/26/2020 Depth to water, ft. Depth to Water, Ft. 7.2 feet 03/26/2020 Ammonia Nitrogen EPA 350.1 <200 pg/L 04/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2020 Odor qualitative Sulfur 03/26/2020 Total Dissolved Solids (TDS) SM 2540 C 653 mg/L 03/27/2020 Temperature SM 2550 B 14.4 C 03/26/2020 Chloride SM 4500 Cl E 199 mg/L 04/06/2020 pH SM 4500 H B 5.91 units 03/26/2020 Total Organic Carbon (TOC) SM 6310 B 5.6 mg/L 03/26/2020 Fecal Coliform SM 9222D MF <1 Colonies/100m1. 03/26/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.05 mg/L 03/27/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 04/06/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/08/2020 Report #:: 2020-05097 Page 6 of 10 Irenvirochem] ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392,4424 Fax 710 I3owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wjilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infio(a)environmentalchemists.com Albemarle Utility Date of Report: Apr 14, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-05097 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12570 Site: MW-7 3/26/2020 10:25 AM Water Jay Baker Test Method Results Date Analyzed Color Color Reddish/Tan 03/26/2020 Depth to water, ft. Depth to water, Ft. 2.7 feet 03/26/2020 Ammonia Nitrogen EPA 350.1 475 pg/L 04/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2020 Odor Qualitative Sulfur 03/26/2020 Total Dissolved Solids (TDS) SM 2540 C 389 mg/L 03/27/2020 Temperature SM 2550 B 14.3 C 03/26/2020 Chloride SM 4500 Cl E 39 mg/L 04/06/2020 pH SM 4500 H B 6.43 units 03/26/2020 Total Organic Carbon (TOC) SM 5310 B 32.4 mg/L 04/01/2020 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 03/26/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 03/27/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 04/06/2020 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/08/2020 Report #:: 2020-05097 Page 7 of 10 Environmental Chemists, Inc. ANALYTICAL & CONSULTING CHEMISTS 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax i nfoCa?environmen talchemists. com Albemarle Utility Date of Report: Apr 14, 2020 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2020-05097 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-12571 Site: MW-8 3/26/2020 12:15 PM Water Jay Baker Test Method Results Date Analyzed Color Color Tan 03/26/2020 Depth to water, ft. Depth to water, Ft. 3.2 feet 03/26/2020 Ammonia Nitrogen EPA 350.1 <200 pg/L 04/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2020 Odor Qualitative Sulfur 03/26/2020 Total Dissolved Solids (TDS) SM 2540 C 307 mg/L 03/27/2020 Temperature SM 2550 B 14.9 C 03/26/2020 Chloride SM 4500 Cl E 98 mg/L 04/06/2020 pH SM 4500 H B 5.88 units 03/26/2020 Total Organic Carbon (TOC) SM 5310 B 4.7 mg/L 04/01 /2020 Fecal Coliform SM 9222D MF 2700 Colon ies/100mL 03/26/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 03/27/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.09 mg/L 04/06/2020 Nitrate Nitrogen Subtraction Method 0.09 mg/L 04/08/2020 Report * 2020-05097 Page 8 of 10 �sni) ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Lab ID Sample ID: 20-12572 Site: MW-9 Test Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate+ Nitrite -Nitrogen Nitrate Nitrogen Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(aenvironmentalchemists. com Date of Report: Apr 14, 2020 Customer PO #: Customer ID: 09110024 Report #: 2020-05097 Project ID: Monitoring Wells Collect Date/Time Matrix Sampled by 3/26/2020 12:02 PM Water Jay Baker Method Color Depth to Water, Ft. EPA 350.1 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 B SM 4500 Cl E SM 4500 H B SM 5310 B SM 9222D MF EPA 353.2 EPA 353.2 Subtraction Method Results Date Analyzed Tan/Brown 03/26/2020 4.4 feet 03/26/2020 <200 pg/L 04/09/2020 5.0 gallons 03/26/2020 Slight Sulfur 03/26/2020 88 mg/L 03/27/2020 15.5 C 03/26/2020 < 5 mg/L 04/06/2020 6.31 units 03/26/2020 6.8 mg/L 04/01 /2020 47 Colonies/100mL 03/26/2020 < 0.02 mg/L 03/27/2020 0.06 mg/L 04/06/2020 0.06 mg/L 04/08/2020 Report M: 2020-05097 Page 9 of 10 lre7nvirochem ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info(denvii•onmentalchemists.com Date of Report: Apr 14, 2020 Customer PO # Customer ID: 09110024 Report #: 2020-05097 Project ID: Monitoring Wells Lab ID Sample ID: 20-12573 Site: MW-10 Test Collect Date/Time 3/26/2020 12:29 PM Method Matrix Sampled by Water Jay Baker Results Date Analyzed Color color Clear/Tan 03/26/2020 Depth to water, ft. Depth to Water, Ft. 4.9 feet 03/26/2020 Ammonia Nitrogen EPA 350.1 <200 pg/L 04/09/2020 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/26/2020 Odor Qualitative None 03126/2020 Total Dissolved Solids (TDS) SM 2540 C 79 mg/L 03/27/2020 Temperature SM 2550 B 15A C 03/26/2020 Chloride SM 4500 Cl E 7 mg/L 04/06/2020 pH SM 4500 rt B 6.20 units 03/26/2020 Total Organic Carbon (TOC) SM 5310 B 1.1 mg/L 04/01 /2020 Fecal Coliform SM 9222D MF 6 Colonies/100ml- 03/26/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 03/27/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.24 mg/L 04/06/2020 Nitrate Nitrogen Subtraction Method 0.24 mg/L 04/08/2020 Comment: Reviewed by: Report #:: 2020-05097 Page 10 of 10 Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 ^0% ■ r&-'Ir ^L1 Awtn i-UA1Ai n= !`I ICT(%nV 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 VVLLG\+ 1 IV!\ /'u�Y Vr■■� v■ www . CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Danny Perry, ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: danny.porry@albemarleplantation.com Sampled By: $ y SAMPLE r n o o cn TYPE: a _ o o d I = Influent, o ae a t = X m g Z ttnuent, PRESERVATION vv = weu, at - auCal If, '1., - �..■■, ..� - .,.....n.., -- ANALYSIS REQUESTED Sample Identification Collection i = N "' $ x o F w at Time Temp Well: �S^• C P _ t Chloride, TDS G G K Depth to water. 8 4 C P U T Nitrate, TOC, NH3 G G C P H field : Q Fecal G G Gallons Bailed: C P VOC's November G ffG P 1 Color: / k r "{' ` G C P Field odor: G G C P G G C P G G RV— G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: Accepted: effected: Resample equested. Delivered By: Received By. L - � °--� Date: �� Time: Comments: TURNAROUND: ENVIRONMENTAL CHEMISTS, INC 602Wi d illWa0Wilmington, NC2FAX 8 5 OFFICAnalytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Danny Perry, ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: danny.perry@albemarleplantation.com Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m ma E F w o` U : C V' �o V e C r o �+ W 9 W mQ PRESERVATION ANALYSIS REQUESTED Date- Time Temp z $ c $ o m O Well: "i 3 , z .► /A s'3 / C P � � � Chloride, TDS G G ., Depth to water: L C P GR Nitrate, TOC, NH3 G G H (field): 5% q Y C P jXr Fecal G G Gallons Bailed: C P VOC's November G G Color: Y4,/4L/ C P G G Field odor: f„ Ifr✓ C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relin wished B : Date/Time Received By- Date/Time 1. 2. Temperature when Received: �5-� "i,... Accepted: ✓ sec ed: _Resample Requested: _ Delivered By: Received By.�� Dater Time - Comments: ( C� T ` TURNAROUND: ENVIRONMENTAL CHEMISTS, I N C 602 Windmill i d ill Way Wilmington,23 FAX NC 28405 8 5 -4424 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: Cj ADDRESS: CONTACT NAME: Danny Perry, ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: dann er abemarle lantation.com Sampled Bv: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection ECL w E `o m _ `o o a40 " ` m r E " ,� m 3 z PRESERVATION ANALYSIS REQUESTED t Time Temp z _ _ ^ c " g w o Well: 3 N C P Chloride, TDS G G Depth to water: 9"1 C P y °� Nitrate, TOC, NH3 G G H (field): 3 9 C P Fecal G G / Gallons Bailed: ` r� C P VOC's November G G Color: rw 7�'l -`l C P G G Field odor: C P G G C P G G C P G G C P G G Total of 10 welts due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received;y - Accepted:, R jected: Resample Requested:_ _ Delivered By: Received B iL. �C.� -• Date: -L Time: ' -} Comments: TURNAROUND: • ► � t is e Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Danny Perry, ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: danny.perry@albemarlepla tation.com SarnDled Bv: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m r a a o o 0 U = o a U -- t£ U w g Z PRESERVATION ANALYSIS REQUESTED Pate Time Temp Zo 2 0< S x z o w C Well: Ulu, !�/ t C P k AS �( 1' Chloride, TDS G G Depth to water: 3i Nitrate, TOC, NH3 G G H (field): -10 C P Fecal G G Gallons Bailed: C P VOC's November G G // Color: C P G G Field odor: S . 4� C P G G So�{rJ C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: dL Accepted: --Z ` Rejoed: Resample Requested: _ Delivered By: Received By: - _ . �' - �= Date: ZO_Time: Comments: TURNAR UND: 602 ill Way �.� ENVIRONMENTAL CHEMISTS, INC OFFICE: 110-392-0223F'AX910-392-"24 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Danny Perry, ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: danny.perry@albemarleplantation.com Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection m® 2 0 a E o v m _ C j _ `o v a C J = E U O W g i PRESERVATION ANALYSIS REQUESTED Date Time Temp i °z x 0 = x a z 2 o Well: .-9 %//9 /y > t C P Chloride, TDS G G Depth to water:' T' at C P r> �" � Nitrate, TOC, NH3 G G r H (field): C P r Fecal G G Gallons Bailed: i C P VOC's November G G Color: 0-4 Ar� ^' N C P G G Field odor: A,,C C P G G C P G G C P G I G C P G G Total of 10 wells due In March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. Z. Temperature when Received:; `` `' Accepted: ✓ Delivered By: Received By: Comments: pie Requested: e:Time: lc C"i TURNAROUND: Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 CLIENT: Albemarle Plantation PROJECT NAME: MonitoringWells REPORT NO: , - C'{ ADDRESS: CONTACT NAME: Danny Perry, ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: danny.perry@albemarleplantation.com Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection E F a E o` m ct9 `o c-, c .r ow O° PRESERVATION ANALYSIS REQUESTED to Time Temp i , CA c z c o w Well: w oC 140' V C P , Chloride, TDS G G r, Depth to water: VIL C P �' ' - �` Nitrate, TOC, NH3 G G H field . C P r {� Fecal G G r Gallons Bailed: 5 C P VOC's November G G Color: � 14 t�+�° C P G G Field odor: s C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. i entperature wnen Keceivea: cx Accepted: Delivered By: Received By:_ C�% _ Date: t> Time: —! Comments: TURNAROUND: Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 rnI I FrTInN1 Alvin rWAIKI AC f 11QTf%nv 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Danny Per , ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: dann er abemarle lantation.com Sampled Bv: SAMPLE TYPE- 1 - Influent_ F o Fffluarnf W = Walt CT a Q*ranm Qn = Q^il Qi = Ql..A-- rl#k . Sample Identification P Collection m a a a E `o 0 c a ,�- r `o r o f " m _ z PRESERVATION ANALYSIS REQUESTED D to Time Tempo z _ _" i _ c = o Well: 4- > l e- C P 1 513 Chloride, TDS G G •r Depth to water: z' C P r^ "� Nitrate, TOC, NH3 G G H field : ' C P Fecal G G Gallons Bailed: C P VOC's November G G Color: rcj-.,,k C P G G Field odor: C P G G C P G G C P G G C P PG G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 2. I JeC Delivered By: Received /MBy: 1-1�7 Comments: rt:esample Requested: _Date: - z Time: TURNAROUND: 113 ! er Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-3924424 CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Danny Per , ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: danny.perry@albemarleplantation.com Sampled By: SAMPLE TYPE: 1= Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection w v `o o .CE g= PRESERVATION ANALYSIS REQUESTED Date Time TempZ z _ i 2 c 0 Well: « C P _ y Chloride, TDS G G Depth to water: 1 . C P { Nitrate, TOC, NH3 G G+` H (field). 'f �� C P Fecal G G Gallons Bailed: C P VOC's November G G Color: �rt C P G G Field odor: jo C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: ` - Accepted:_ / jected: Resample Requested: Delivered By: Received By:-`; 2 Time: 1, Comments: TURNAROUND: s Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 CC)[_ t FCTION Amn rNAIN nF rl ISTnnv 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO:� ADDRESS: CONTACT NAME: Danny Perry, ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: dann er abemarle lantation.cdm Sampled Bv: AAMPI F TYPF• I = Inflnan+ F = Fffl..an+ W = Wall CT = C+.ems... CA - 0-11 401 - Ct...4 - Sample Identification Collection_ r w a g P E a U c° U J °� V E W 0° °° g z PRESERVATION ANALYSIS REQUESTED t Time Temp W i = � = o i 0 o _ W o / Well: 3 Cc y riot 4 C P J t(� Chloride, TDS G G n Depth to water: �-3 C P Nitrate, TOC, NH3 G G H field C P Fecal G G r' Gallons Bailed: S C P VOC's November G G Color: ���/ ��°""' C P G G Field odor: 3s^ C P G G c /err C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Delivered By: Received By Comments: 3tea: 2t-) Time: t.. ' )b --- 3UND: Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 rnl I FCTlnKl Anln r'untst nc r+l10'rnnv 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Danny Per , ORC PO NO: REPORT TO: PHONE/FAX: 252.339.6557 COPY TO: email: danny.perry@albemarleplantation.com bamnletl HV: 0AIL1n1 C Sample Identification Collection to c o a U c a " r E " c g a Z PRESERVATION OL- � Jtuage, vzner: ANALYSIS REQUESTED to Time Tem o z � � _" i _ o 1 o w o Well: P ! S' C P ju I r", Chloride, TDS / LL S G G Depth to water: -Cl ~ C P L% ys 'j � Nit;ate, TOC, NH3 G G H (field): 6. 0 P Fecal G G Gallons Bailed: S C P VOC's November G G Color: e, /,-,j All,J C P G G Field odor: JL.., C P G G C P G G C P G G C P TT G G Total of 10 wells due in March, July, November. - Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Tamnar!afi.r . u.1- O.a.a.a:...a.,t. .- - - - --- --- - .�.,..t:N.Qa• -I J Kel czea: Resample Requested: Delivered By; Received Time: C Comments: