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WQ0023181_Monitoring - 03-2020_20200420
CAW-59A COMPLIANCE REPORT FARM Permit # (.Sulunit one each monitoring period with GW-59 fornis.) 1 Enter date monitoring results were due. ((Yi ,reac ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? X 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? if the answer is "Yes", contact the Regional Office for guidance. V 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. cD If the answer to question 5 is "YES", list in the space provided belo4ro -eagh we11 w constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each ocettrretor the last two years). O LL Cy C13 L, o 0 Q 6 Are the monitoring wells listed in section 5 located at or beyondffM review bo6dary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility, Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. /iv ace A4,vi: /V� Signature rermittee (or Autho ' d Agent) Date GW-59A 1218t2003 INTERNATIONAL@ PAPER Global Sourcing — Fiber Supply PO Box 710 865 John L Riegel Road Riegelwood NC 28456 910 362 3329 (Office) 910 342- 2869 (Fax) April 10, 2020 NC Department of Environmental and Natural Resources Division of Water Quality — Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Dear Sir/Madam, Enclosed are the completed original and one copy of report #GW59, GW59A, and the lab report used to complete GW59. Regards, A Ben Burger Fiber Specialist SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print i Facility Name: j7A t-e-, /V, r ,,)e r ' JZ; Permit Name (if different): Facility Address: AJ.9 r i or Type t(/ Countyrre- Contact Person: Telephone#: /,�7 h O y- U j/ p Well Location/Site Name: No. of wells to be sampled:411A DEPARTMENT OF ENVIRONMENTAL QUALITY - DIY. OF WATER RESOURCES INFORMA71ON PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Pha16: 919-807.6306 PERMIT Number: `CV'3 31(1 Expiration Date: Non -Discharge UIC NPDES "Ve-G :-,')C;00 lr9 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump P Other: f2ec/c Ltd E - (,^ f`e- WELL ID NUMBER : P from Permit): �^ ( ) D ate sample collected: FIELD ANALYSES: If WELL Well Depth: q /j� ft. WAS Depth to Water level e2sas:'zVJ..- ft. below measuring point Well Diameter: in. Screened Interval: ft. to pH ooaoo: units Temp. 000lo: °C DRY at time of Measuring Point is fWft—above land surfs _ft. Relative M.P. Elevation: �,Q- ft. Spec. Cond. 0ooe4: µMhos Odor 000as: sampling, Volume of water pumped/bailed before sampling: P 9� /� , gallons Appearance check Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO here.❑ LABORATORY INFORMATION Date sample analyzed: 3 Q aG Laboratory Name: /L/t✓a Certification No. � PARAMETERS NOTE: Values hpul reflect dissolved and colloidal concentrations. COD 00335 �� mg/L Nitrite (NO2) as N oosls mg/L Pb - Lead o1o51 Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L ug/L Zn - Zinc 01092 Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L mg/L (Note: Use MPN mettod for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 , 0 units Ba - Barium 01007 ug/L TOC oosao mg/L Ca - Calcium oogls mg/L Chloride oogao a, ! mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ( c) 3 it ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) specific Conductance 000gs µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia ooslo mg/L Ammonia (Ammonia Nitrogen; NH, as N, Nitrogen, Total) Mg - Magnesium 00927 mg/L g , method # Mn - Manganese oloss ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.807-6306 FACILITY INFORMATION � Please Print Clearly or Type ,Z PERMIT Number:/��(Gc � 3/�j Expiration Date: �? 3G 3 Facility Name: - A to l i A-�J 16,4- 'y�('%\ /� � lC-�'11�1 �111 (/ Non -Discharge UIC Permit Name (if different): NPDES ly_ > 91-) 0 Other Facility Address: r'o S )Cti 6' TYPE OF PERMITTED OPERATION BEING MONITORED Al') r,'/1�. /U l County t, r"e-Y1 ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: Contact Person: % f1 % " Telephone#: 0//0 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: ❑ Water Source Heat Pump �] Other:02e C le ,1 from Permd SAMPLING INFORMATION WELL ID NUMBER (from Permit): -{/ I Date sample collected: f :' FIELD ANALYSES: If WELL WAS Well Depth: J,� ft. Well Diameter: in. pH ooaoo: units Temp. 00010: °C DRY at Depth to Water Level 82546: ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is —L ft. above land surface, Relative M.P. Elevation: /,//, ft. Odor 00085 A 14 check Volume of water pumped/bailed before sampling: _gallons` Appearance here: Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION 3 G1 / �� , l /1 /vl�-f-� ALsy d- ,` �j)q Date sample analyzed: ©� Laboratory Name: Certification No. PARAMETERS NOTE: Values h Id reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 1,60 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 + 0 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940, 7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 I.tMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. NH3asN, Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% \. ENCO Laboratmies 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, March 31, 2020 International Paper, Inc. (IN019) Attn: Jim Fretz SR 1102, 247 CR Collins Road Norlina, NC 27563 RE: Laboratory Results for Project Number: [none], Project Name/Desc: NPDES ENCO Workorder(s): CD04658 Dear Jim Fretz, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, March 19, 2020. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, 04XV'6XLC.---�A Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 8 IAI� www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Wet Yard Pond Lab ID: CD04658-01 Sampled: 03/18/20 10:04 Received: 03/19/20 10:00 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/TimcW EPA 420.1 Same 04/15/20 03/30/20 10:00 03/31/20 13:00 Field NO PREP 03/18/20 10:18 03/18/20 10:04 03/18/20 10:04 SM 254OC-2011 NO PREP 03/25/20 03/22/20 15:03 03/22/20 15:03 SM 4500CIE-2011 NO PREP 04/15/20 03/23/20 15:16 03/23/20 17:20 SM 5220D-2011 Same 04/15/20 03/20/20 10:37 03/20/20 19:00 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 8 (� G www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: Wet Yard Pond Lab ID: CD04658-01 Analvte Results Flaa MDL P L Units Method Notes Chemical Oxygen Demand 48 10 10 mg/L SM 5220D-2011 Chloride 2.7 3 1.9 5.0 mg/L SM 4500CI E-2011 pH 8.0 0.0 0.0 pH Units Field Temperature 10.07 0 0 °C Field Total Dissolved Solids 96 50 50 mg/L SM 254OC-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 8 ce�=l 6,00) www.encolabs.com ANALYTICAL RESULTS Description: Wet Yard Pond Lab Sample ID:CDO4658-01 Received: 03/19/20 10:00 Matrix: Surface Water Sampled:03/18/20 10:04 Work Order: CD04658 Project: NPDES Sampled By:3im Hays lClassical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results fin Units PE MDL POL Batch Method Analyzed iy Notes Chemical Oxygen Demand^ 48 mg/L 1 10 10 OC20008 SM 5220D-2011 03/20/20 19:00 10C Chloride [16887-00-6]A 2.7 J mg/L 1 1.9 5.0 OC23027 SM 4500CI E-2011 03/23/20 17:20 AKF Total Dissolved Solids^ 96 mg/L 1 50 50 OC22001 SM 254OC-2011 03/22/20 15:03 10C Field Parameters Analyte [CAS Numberl Results Flag UnM DF MDL POL Batch Method Analyzed By Notes PH 8.0 pH Units 1 0.0 0.0 OC20002 Field 03/18/20 10:04 JH Temperature 10.07 oC 1 0 0 OC20002 Field 03/18/2010:04 JH Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results IFag Units P-E MDL M Batch Method Analyzed Ay Notes Phenolics^ 0.034 U mg/L 1 0.034 0.050 OC27031 EPA 420.1 03/31/20 13:00 JSS FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 8 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OC20008 - Same Blank (OC20008-BLK1) Prepared: 03/20/2020 10:37 Analyzed: 03/20/2020 19:00 Spike Source %REC RPD Analvte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (OC20008-BS1) Prepared: 03/20/2020 10:37 Analyzed: 03/20/2020 19:00 Spike Source %REC RPD Analvte Result Flag P_QL Units Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 510 10 mg/L 500 101 90-110 Matrix Spike (OC20008-MS1) Prepared: 03/20/2020 10:37 Analyzed: 03/20/2020 19:00 Source: CD00122-01 Spike Source %REC RPD Analvte Result Flaa P L m Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 750 10 mg/L 526 220 99 90-110 Matrix Spike Dup (OC20008-MSD1) Prepared: 03/20/2020 10:37 Analyzed: 03/20/2020 19:00 Source: CD00122-01 Spike Source o/aREC RPD Analvte Result Rau RQL Units Level Result %REC Limits RPD limit Notes Chemical Oxygen Demand 730 10 mg/L 526 220 96 90-110 2 5 Batch OC22001 - NO PREP Blank (OC22001-BLK1) Prepared & Analyzed: 03/22/2020 15:03 Spike Source %REC RPD Anal vte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L LCS (OC22001-BS1) Prepared & Analyzed: 03/22/2020 15:03 Spike Source %REC RPD Analvte Result Flag MI. Units Level Result o/aREC Limits RPD Limit Notes Total Dissolved Solids 970 50 mg/L 1000 97 80-120 Duplicate (OC22001-DUPl) Prepared & Analyzed: 03/22/2020 15:03 Source: CD01620-01 Spike Source %REC RPD Analvte Resul[ Flag PQL knits Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 180 50 mg/L 180 3 20 Duplicate (OC22001-DUP2) Prepared & Analyzed: 03/22/2020 15:03 Source: CD01620-02 Spike Source %REC RPD Analyte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 230 50 mg/L 230 0 20 Batch OC23027 - NO PREP Blank (OC23027-BLK1) Prepared: 03/23/2020 15:16 Analyzed: 03/23/2020 17:09 Spike Source %REC RPD Analvte Result Flag PQL Units Level Result %REC Limits RPD Limit Notes Chloride 1.9 U 5.0 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 8 (�Cs N 0 70) www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch OC23027 - NO PREP - Continued LCS (OC23027-BS1) Prepared: 03/23/2020 15:16 Analyzed: 03/23/2020 17:10 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Chloride 100 5.0 mg/L 100 100 80-120 Duplicate (OC23027-DUPl) Prepared: 03/23/2020 15:16 Analyzed: 03/23/2020 17:13 Source: CD04195-03 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD L[Mft Notes Chloride 740 D 50 mg/L 730 0.6 10 Matrix Spike (OC23027-MS1) Prepared: 03/23/2020 15:16 Analyzed: 03/23/2020 17:11 Source: CD04195-02 Spike Source %REC RPD Analvte Result Flaq Q m Level Result %REC Limits RPD Limit Notes Chloride 740 25 mg/L 200 580 79 80-120 QM-07 Matrix Spike Dup (OC23027-MSD1) Prepared: 03/23/2020 15:16 Analyzed: 03/23/2020 17:12 Source: CD04195-02 Spike Source %REC RPD Analvte Result Flag POL Units Level Result %REC Limits RPD Limit Notes Chloride 730 25 mg/L 200 580 75 80-120 1 25 QM-07 Classical Chemistry Parameters - Quality Control Batch OC27031 - NO PREP Blank (OC27031-BLK1) Prepared: 03/30/2020 10:00 Analyzed: 03/31/2020 13:00 Spike Source %REC RPD Analvte Result Flag P41 Units Level Result %REC Limits RPD Limi Notes Phenolics 0.034 U 0.050 mg/L LCS (OC27031-BS3) Prepared: 03/30/2020 10:00 Analyzed: 03/31/2020 13:00 Spike Source %REC RPD Aral Cte Result Flag POL Units Level Result %REC Limits RPD umft Notes Phenolics 0.53 0.050 mg/L 0.500 106 90-110 Matrix Spike (OC27031-MS1) Prepared: 03/30/2020 10:00 Analyzed: 03/31/2020 13:00 Source: CD04658-01 Spike Source %REC RPD Analvte Result Flag PM Units Level Result %REC Limits RPD ilm[t Notes Phenolics 0.48 0.050 mg/L 0.500 0.034 U 96 90-110 Matrix Spike Dup (OC27031-MSD1) Prepared: 03/30/2020 10:00 Analyzed: 03/31/2020 13:00 Source: CD04658-01 Analvte Phenolics Spike Source %REC Result Flaa Q m Level Result %REC Limits RPD 0.53 0.050 mg/L 0.500 0.034 U 105 90-110 9 RPD kinia Notes 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 8 � �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 8 ENVIRONMENTAL CONSERVATION LABORATORIES CHAIN -OF -CUSTODY RECORD www.encolabs.com cans centrat Pori or, 4810 Ex—OCUtive Park Court, Suite 111 102-A Woodwinds industrial Ct. Orlando, FL 32824 Jacksonwile, Ft. 32216-6M Caryk NC 27511 CSAW=WN�G 6) (40n 626-6314 (904)-1qP-3,nj7 Fax (9XA)2196,6210 M91467-30W Fax (919)467-3515 Page _ of Cl;ant Mina Pr4ed Number Requested Analyses Requested Turnaround International Paper, Inc- QN019) tronel 0 Times I Address . . .... Project Name/Desc —i Note :Hush requeM subjed to SR 1102,247 CR Collims Road NPOES LU accwtance by the lautity C4/8Tqv PO 01 Billing lrft C6 Ndrkna, NC 275M S Standard Fait C4 Tel (252)456-25% Ro�rrecltz 0 Expedited Samplai4s Name.Ani orlon (Pnm Ming trJ to w 75 Due C) sarivie.ff Si nature Site Location I 'rime Zone 0 La orkerder GDOD4605 Preservation (See Codes) (Combine as necituary) Col or Malt ix Total of e Commenis Sortioe to (Flold Idenillt, .,,,nl Collection Date G ac C taine'e, Sampl. .. . ..... .. . ..... .... ........ . ...... . .... . ......... rd $w Point! X I X ...... .. . . . -- - - - ------ - --- UINNUI ..... . ... . . . ....... .... .... . .... ... ... . . ..... . . ........ ... . ... .... .. ............ ..... . .... . . .... . ..... .. . ..... - - - --------- ------------ - --- - - - - - - - - -------------- ..... ..... . ... . ...... . . .. ....... .......... .. . ....... . . - ---- - ------ ---- - - --------- - ----- - - -------- --- ...... . .... . ..... ------ --- - - - - - ---------- . ............ .. Tow # of Containers .Sampta KltPtepared i neiinquished By D l i�? D Comment Reporting Requirements swinii'T By 'Mi Received By Relinquished By DatoMme Received By Datemnie Cooler t's It Temps on Receipt Condition upon Frompt t"�p I -Zr tAc"/ Acceptable Unacceptable Mativix: GW.Groundwatef SO -Soil DW-DrinWmg Water SE-Sedimard SW.Surlaco Water WW-Wastewater A -Air "ther (oetall in comments) Pwiwrvatlon: Poo WHO N-HNO3 S-H2SO4 NO-Na0H "ther (detail in cornmOrtift) Note. All samples submitted to ENCO Labs are in accordance with the terms and conditions listed an the reverse of this lbrm, unless prior written agreements exist Sample Preservation Verification ENCO Cary - Work Order: CD04658 Project-, NPIDES Client: International Paper, Inc. (IN019) Project (none) Logged In: 19-Mar-20 10:25 Logged By: Rachel Ann Y nish Preservation Check Performed By: )I Date[Time: 17D �C):-)C� CD04658-01 Cont T�pe Pres (PH) Requirement PH Checked 1: in Control : PH Adjusted QateMme, Adjusted Reagent, Used(Cornments A 250rnLA+H2SO4 <2 N I •NA Y 6�p/ NA D 250mLP+H2SO4 <2 N I NA Y � NZ' NA Reagent Name ID 11 1 21 1 pH Strip IC PH StriPs COA0898 ' - C:kelmnt\P; '__1 , covi vation Check. rpt Reagent Name ID 3 4 Reagent Name ID 6 Page 1 of I