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HomeMy WebLinkAboutWQ0016247_More Information (Received)_20200717APPLICATION MAP LEGEND APPLICATION AREA UNSUITABLE AREA — — — — — — PRIVATE ROAD W O WATER — STREAM ONSITE HOUSE — DRAIN OFFSITE HOUSE - -X X FENCE OUTBUILDING PROPERTY LINE 0' SOIL BORING 0 WELL The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 1 " = 660' 660' 0 660' N C- I R-20 Field 4 APPLICATION MAP z. LEGEND APPLICATION AREA - — — — — - PRIVATE ROAD O — - - — STREAM — - — DRAIN . X X M FENCE PROPERTY LINE 0 s �KF,A ty r }Ty K f s • S � UNSUITABLE AREA WATER ONSITE HOUSE OFFSITE HOUSE OUTBUILDING WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 660' 0 660' � 6 NC-AL-13 Field 6 APPLICATION MAP ® REDMON RD El A7 F- S � ac . r p0 O � LEGEND APPLICATION AREA UNSUITABLE AREA — — PRIVATE ROAD W O WATER — — — — STREAM . ONSITE HOUSE — DRAIN OFFSITE HOUSE -- FENCE OUTBUILDING PROPERTY LINE 0 WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 1 " = 660' 660' 0 660' NC-RA-05 Fields 1-2 AF'I='I-.IC,A TION MAP LEGEND APPLICATION AREA - — — — — - PRIVATE ROAD O - -- - - — STREAM — - — DRAIN . X x X FENCE PROPERTY LINE (� UNSUITABLE AREA WATER ONSITE HOUSE OFFSITE HOUSE OUTBUILDING WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever Is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 660' 0 660' NC-AL-13 Fields 4-5 APPLICATION MAP z. LEGEND APPLICATION AREA - — — — — - PRIVATE ROAD O — - - — STREAM — - — DRAIN . X X M FENCE PROPERTY LINE 0 s �KF,A ty r }Ty K f s • S � UNSUITABLE AREA WATER ONSITE HOUSE OFFSITE HOUSE OUTBUILDING WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE 660' 0 660' � 6 NC-AL-13 Field 6 SOIL SURVEY GRAPHIC SCALE ssoo sso The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-AL-13 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundaryand the perimeter of the residuals application area. All locations are approximate. Fields 4.5 SOIL SURVEY GRAPHIC SCALE ssoo sso The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-AL-13 9 Am ■lrJnF0 TOPOGRAPHIC MAP GRAPHIC SCALE 1"=660' ssoo sso The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-AL' 13 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Field 6 TOPOGRAPHIC MAP cPR % -- �ti GRAPHIC SCALE 800' 0 800' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C'AL-1 3 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 4-5 VICINITY MAP GRAPHIC SCALE 4,000, 0 4,000' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-AL-13 Fields 4-6 APPLICATION AREA - — — — — - PRIVATE ROAD — - - — STREAM - — DRAIN X x X FENCE PROPERTY LINE APPLICATION MAP UNSUITABLE AREA O WATER ® ONSITE HOUSE . OFFSITE HOUSE OUTBUILDING (� WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the properly boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. t, GRAPHIC SCALE sso o sso' SOIL SURVEY GRAPHIC SCALE ssoo sso The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-AL-15 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1.3 r, TOPOGRAPHIC MAP L� }'JON C.Jmf. . GRAPHIC SCALE The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. i NC-AL-15 Fields 1-3 VICINITY MAP \� U le IF— IF mi U y t C'IF lJ o k IF IL C / t Fj v _de AP I aF \ IC IF IF IF C - L �( -IF - ' r mil/ 1 IF IF IF GRAPHIC SCALE a,000, o 41000' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1-3 APPLICATION MAP dm r, r P' i rnrnin APPLICATION AREA � UNSUITABLE AREA — — — — — — PRIVATE ROAD O WATER — — — — STREAM ONSITE HOUSE GRAPHIC SCALE — — DRAIN . OFFSITE HOUSE 1" = 660' sso' o sao' X X X FENCE OUTBUILDING PROPERTY LINE ( WELL Q SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-AL-16 Field 1 SOIL SURVEY Q Z Un GRAPHIC SCALE The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-AL-1 6 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Field 1 TOPOGRAPHIC MAP GRAPHIC SCALE 1"=800' 800' e 800' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-AL-16 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. I Field 1 ® VICINITY MAP I(- d,I V Cr L J r11 lIV „ ✓ohs �! )1to .- C"._ `V Q 'IV do o r,Ad V �_ _i•— �,'��J ZI riV C 3 ' twl �7 �Voodoo I or IV IV too dj V do Lto) . Lso aVI P�� —� do -_ do do I It VV Ir r �. D r IV IV cli ded / IL IVIVIVIVI do rVVII:Z do OP / k _� I 'S L (� 1:^ -- 1. GRAPHIC SCALE a,a00, 0 41000' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C'AL-1 6 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance houndary and the perimeter of the residuals application area. All locations are approximate. Field 1 APPLICATION MAP LEGEND APPLICATION AREA — — — — — — PRNATE ROAD - - — STREAM — — DRAIN -,r x X FENCE PROPERTY LINE O 0 UNSUITABLE AREA WATER ONSITE HOUSE GRAPHIC SCALE OFFSITE HOUSE sso, o ssa OUTBUILDING WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CD-03 Fields 2-3 -_F&B2 FaC2.yyuC FaC2 WOB t I B FaC2 ALI WOt• 1 w won llwF HwF NwF' WaC yr �. LL�} ma it 1 .. �r_1 At .��. .Wo6..FmC - 2: it PI I AL " woc r.,, FeC2 APPLICATION MAP I�YV y\I�l APPLICATION AREA � UNSUITABLE AREA -- n� PRIVATE ROAD �W WATER — - - — STREAM ONSITE HOUSE GRAPHIC SCALE — - — DRAIN . OFFSITE HOUSE 1" = 660' sso, o eso' x FENCE OUTBUILDING PROPERTY LINE WELL SOIL BORING The compliance boundary is established either 250 it from the residuals application area or 50 feet within N C—C D-03 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields &7 ■1f� iFTZ 00* TaB2 t.Fnnz f/ �- ,� I FaB2 FaD2 FaD2 WoC �+♦- ..1 ; r444 it �-FdD2r. y AT N a z ul APPLICATION MAP I 1=r_�nln APPLICATION AREA � UNSUITABLE AREA — — — — — — PRIVATE ROAD OW WATER — — — — STREAM ONSITE HOUSE — — DRAIN . OFFSITE HOUSE GRAPHIC SCALE 1"=660' X x X FENCE OUTBUILDING sso' o sso' PROPERTY LINE WELL (� SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CD=03 Field 9 0 Q Z Ul SOIL SURVEY GRAPHIC SCALE sso o sso The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CD-03 Fields 9 5I) TOPOGRAPHIC MAP ^r I (mv rz 17 t 'moo r 0 All GRAPHIC SCALE 1 1,000' 11000, 0 11000, rr rr The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C=C D m03 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 2.3, 10 TOPOGRAPHIC MAP GRAPHIC SCALE aooo aoo The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-C D-03 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Field 9 TOPOGRAPHIC MAP IX Q Z Ln GRAPHIC SCALE The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-CD-03 in the property Boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Field 9 VICINITY MAP ,�. �%L ALL Lt Of �.r Fter, / % it LL,f l r U' ti a. IL It 5 LJ c p M1 ^� IF JAL k v, eL 41, - -� _ 4 v� GRAPHIC SCALE a,000• o a,000 rr The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review houndary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-CD-03 Fields 2-3,6,7,9,10 APPLICATION MAP APPLICATION AREA � UNSUITABLE AREA — PRIVATE ROAD OW WATER — — — — STREAM ONSITE HOUSE GRAPHIC SCALE — — — DRAIN ■ OFFSITE HOUSE 1" = 660' x FENCE OUTBUILDING eso, o 660' PROPERTY LINE WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-IR-36 Fields 1-2 APPLICATION MAP LEGEND AnAPPLICATION AREA M UNSUITABLE AREA AMA PRIVATE ROAD OW WATER STREAM ONSITE HOUSE GRAPHIC SCALE - - DRAIN . OFFSITE HOUSE 1" = 660' sso' o sso' x FENCE OUTBUILDING PROPERTY LINE WELL Q SOIL BORING The compliance boundary is established either 250 Arom the residuals application area or 50 feet within in the properly boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. N C-I R-36 Fields 3-4 APPLICATION MAP Ov Q z V) I C!'CAlrl APPLICATION AREA � UNSUITABLE AREA — — — — — — PRIVATE ROAD OW WATER — — — — STREAM ONSITE HOUSE — — — DRAIN ■ OFFSITE HOUSE GRAPHIC SCALE 1" = 660' x X FENCE OUTBUILDING sso' a sso PROPERTY LINE WELL 0 SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-IR-36 Field 5 SOIL SURVEY ry Q Z GRAPHIC SCALE ssoo sso The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC -I R-36 Fields 1-2 SOIL SURVEY ry Q Z GRAPHIC SCALE The compliance boundary is established either 250 (t from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 3-4 TOPOGRAPHIC MAP /// JfVl L>' 4 GRAPHIC SCALE sooo aoo The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-IR-36 Fields 1-2 ® TOPOGRAPHIC MAP L Far , /f Ln Ll ` IF � 11 \ 0gaff If �. Q ,L If Y'1 �.i I . ~ J • �j ���- VO /� I OJIF / { GRAPHIC SCALE 1"=1,000, 11000, 0 15000, The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C- I R-36 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 3-5 0 Q Z Ul VICINITY MAP GRAPHIC SCALE a,000o a,000 rr rr The compliance boundary is established either 250 fl from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. NC-IR-36 Fields 1-5 Z Ul PPLIO,ATION MAP I t=rt=nln APPLICATION AREA � UNSUITABLE AREA — — — — — — PRIVATE ROAD WATER GRAPHIC SCALE - - - - STREAM . 1" = 660' ONSITE HOUSE — — DRAIN 669 0 660 OFFSITE HOUSE X X X— FENCE OUTBUILDING PROPERTY LINE WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C—RA-05 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1-2 LEGENDMIMI - - - - - - PRIVATE ROAD - - - STREAM - - - DRAIN x�X FENCE PROPERTY LINE i 1• UNSUITABLE AREA O WATER GRAPHIC SCALE . ONSITE HOUSE 1" = 660' 660' 0 660' . OFFSITE HOUSE " .m OUTBUILDING WELL The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundaI and the perimeter of the residuals application area. All locations are approximate. NC-RA-05 Fields 2-3 EnC. r if t / MuC2 f fESC Eac MaD2 2� DeD - �I WIiB WaA DoB TOPOGRAPHIC MAP �7 1 !1 �1748 � •- !! '�' '1 - all 1 1 ( ,t all ,!aal L) 4. V� " FF all Nab alas o_� \, --� - t -row 2 ` --. ". / .all GRAPHIC SCALE 1"=1,000' 1,000' 0 11000, The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N & RA-05 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1.3 VICINITY MAP GRAPHIC SCALE 4,000' 0 4,D00' rr rr ' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C- RA-05 in the property boundary, whichever is closest to the application area. The review boundary is estahlishetl midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields 1.3 APPLICATION MAP LEGEND APPLICATION AREA PRIVATE ROAD — - - — STREAM — — — DRAIN X x FENCE PROPERTY LINE O ❑{ 0 UNSUITABLE AREA WATER ONSITE HOUSE OFFSITE HOUSE OUTBUILDING WELL SOIL BORING The compliance boundary is established either 250 ft from the residuals application area or 50 feet within in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. GRAPHIC SCALE ssc' s sso' NC-RA-53 Fields 1-2 Pbc Po6 0 ChA z 1;�7 PrE a TOPOGRAPHIC MAP GRAPHIC SCALE 1,000' 0 1,000' rr �r The compliance boundary is established either 250 ft from the residuals application area or 5o feet within N C-RA-53 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundaryand the perimeter of the residuals application area. All locations are approximate. Fields 1.2 ® VICINITY MAP ;t -= IV r� YI _r If GRAPHIC SCALE a,000, 0 41000' The compliance boundary is established either 250 ft from the residuals application area or 50 feet within N C-RA-53 in the property boundary, whichever is closest to the application area. The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area. All locations are approximate. Fields ii State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documcntation listed below. A. Land Application Site Certification (FORM: LASC 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit the requested information for all land application sites. ® For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. B. Land Application Site Information: ® The status of the land application site with respect to this residuals land application program must be provided in table I. The status categories and their corresponding codes are as follows: ♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D) ® Attach the following in accordance with each status code: Status Code Required Item N R T M ✓ County Board Notification.doc +' I . Land Owner Agreement (If applicable) I A I' V V/ V/ V/ Setback Waiver Agreement An updated vicinity/setback map in accordance with the "Map Guidance for Residuals Land Application Permits" ✓ ✓ ✓ A soils and agronomic evaluation in accordance with the "Soil Scientist Evaluation Policy" ✓ INSTRUCTIONS FOR FORM: LASC 06-16 Page 1 of 3 An updated accounting of the land application site's cumulative pollutant loading rates (CPLRs) Required Item Status Code N7 R T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly ✓ indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation Policy" Acknowledgement of field transfer from Land Owner (Fields may not be permitted to multiple Permittees over the same time period) * This item may be required for land application site with a status code "M", please contact the Division if you need assistant in determining attachment requirements. ® Crop Type should include the most likely crop types for the life of the permit (five years). ® Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ® For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ® New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. ® Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: • Address Matching (ADD) • Aerial Photography with Ground Control (AER) • Cadastral Survey (SUR) • Conversion from Coordinate Plane (CP) • Conversion from Township -Section -Range (TSR) • Conversion from Universal Trans Merc (UTM) • Map Interpretation by Digital or Manual Extraction (MAP) • Digital or Raw Photo Extraction (EXT) • Geodetic Quality GPS Survey (GEO) • LORAN-C Navigation Device (LOR) • Navigation Quality GPS (GPS) • Remote Sensing (RS) • Zip Code Centroid (ZIP) C. Waterbody and Classifications Information: (new sites only) ® Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ® Surface water body classifications information may be found at: http://deq.nc.gov/about/divisions/water- resources/planning/classification-standards/classifications ® Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ® A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: http://deq.nc.gov/contact/regional-offices ® General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream name" as the waterbody name. 3. Open the link http:Hdeg.nc.gov/about/divisions/water-resources/planning/classification-standards/classifications. ® Stream Classification Process: One of the options below may be used depending on the known initial project information. ® KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15ANCAC 02B .0301(i). ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Basin And Savannah River Drainage Area Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified "B Tr." French Broad River Basin Streams entering Tennessee will be classified "B." Watauga River Basin Streams entering the State of Tennessee are classified "C." Broad River Basin Streams entering South Carolina are classified "C." New River Basin Streams entering the State of Tennessee are classified "C." Catawba River Basin Streams entering South Carolina are classified "C." Yadkin -Pee Dee River Basin Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Roanoke River Basin Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River Basin All drainage canals not noted in the schedule are classified "C Sw." except the main drainage canals to Pamlico Sound and its bays which shall be classified "Sc." Pasquotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 LAND APPLICATION SITE CERTIFICATION Applicant's name: Synagro Western Piedmont Land application sites currently certified: 813.6 net acres and Total to be certified: 1,315.5 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Codes Site/Field ID Landowners �) Lessees or Operator(s) �) Net Acres County s Crop(s) p�) Predominant Soil Series Name' Mapping Unit or Rep. Slope' N IR-36-1 Chris Cartner 52.6 Iredell Corn, Wheat N IR-36-2 Chris Cartner 19.4 Iredell Corn, Wheat N IR-36-3 Chris Cartner 21.9 Iredell Corn, Wheat N IR-36-4 Chris Cartner 41.5 Iredell Corn, Wheat N IR-36-5 Chris Cartner 23.8 Iredell Corn, Wheat N RA-05-1 Allen Livegood 17.6 Rowan Fescue Pasture ■ N RA-05-2 Allen Livegood 44.8 Rowan Fescue Pasture N RA-05-3 Allen Livegood 18.5 Rowan Fescue Pasture N RA-53-1 ALLO l.l.c (Janet Tevepaugh) Rowan Fescue Hay N RA-53-2 Mark Tevepaugh 19.1 Rowan Fescue Hay N AL-13-4 Danny Millispas 8.5 Alexander Fescue Pasture N AL-13-5 Danny Millispas 15.9 Alexander Fescue Pasture N AL-13-5 Danny Millispas 19.2 Alexander Fescue Hay N AL-15-1 Mary Ann Icenhour Ray Icenhour 1-a Alexander ijorn, Wheat, Soybeans N AL-15-2 Mary Ann Icenhour Ray Icenhour 26.8 Alexander ,orn, Wheat, Soybeans N AL-15-3 Mary Ann Icenhour Ray Icenhour 10.2 Alexander torn, Wheat, Soybeans N AL-16-1 Kevin Daniels 20.8 Alexander Fescue Pasture N CD-03-2 Patrick Starnes 17.8 1aldwell Fescue Hay N CD-03-3 Patrick Starnes 8.5 Caldwell at, Soybeans N CD-03-6 Patrick Starnes 4.2 Caldwell Corn, Wheat, Soybeans N CD-03-7 Patrick Starnes 3.5 Caldwell Corn, Wheat, Soybeans N CD-03-9 Mark Douglas Patrick Starnes 21.4 Caldwell Fescue Hay FORM: LASC 06-16 Page 1 LAND APPLICATION SITE CERTIFICATION M IR-20-4A Dennis Phillips 42.3 Iredell Fescue Hay a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) b Soil Series Name (i.e. Appling, Cecil, etc.) Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed P Class IR-36-1 35.47.21.87 80.47.37.64 NAD 83 MAP Nearest Second 12-108-20 C C IR-36-2 35.47.5.64 -80.47.18.7 NAD 83 MAP Nearest Second 12-108-20 C C IR-36-3 35.51.7.51 -80.46.58.71 NAD 83 MAP Nearest Second 12-108-13 C C IR-36-4 35.51.10.76 -80.47.5.53 NAD 83 MAP Nearest Second 12-108-13 C C IR-36-5 35.50.55.1 -80.47.45.84 NAD 83 MAP Nearest Second 12-108-13 C C RA-05-1 35.42.45.35 -80.39.37.18 NAD 83 MAP Nearest Second 12-108-21-3 C C RA-05-2 35.42.20.19 -80.39.40.59 NAD 83 MAP Nearest Second 12-108-21-3 C C RA-05-3 35.42.8.74 -80.39.33.62 NAD 83 MAP Nearest Second 12-108-21-3 C C RA-53-1 95.45.20.16 -80.38.41.28 NAD 83 MAP Nearest Second 12-108-20-4 C C RA-53-2 35.12.38.11 -80.16.52.05 NAD 83 MAP Nearest Second 12-108-20-4 C C AL-13-4 35.53.37.63 -81.9.56.89 NAD 83 MAP Nearest Second 11-69-7-(0.7) WS-IV WS-IV AL-13-5 35.53.46.43 -81.9.51.11 NAD 83 MAP Nearest Second 11-69-7-(0.7) WS-IV WS-IV AL-13-6 35.52.45.14 -81.7.50.82 NAD 83 MAP Nearest Second 11-69-7-1-1 WS-IV WS-IV AL-15-1 35.58.8.27 -81.10.41.3 NAD 83 MAP Nearest Second 11-69-4 C , FORM: LASC 06-16 Page 2 LAND APPLICATION SITE CERTIFICATION AL-15-2 15.58.20.63 -81.10.48.17 NAD 83 MAP Nearest Second C C AL-15-3 15.58.22.64 -81.10.53.15 NAD 83 MAP Nearest Second C C AL-16-1 35.58.44 -81.11.7.8 NAD 83 MAP Nearest Second r■ CD-03-2 35.50.56.76 -81.20.47.40 NAD 83 MAP Nearest Second 11-59-(1) CD-03-3 35.50.51 -81.20.40.56 NAD 83 MAP Nearest Second 11-59-(1) CD-03-6 35.51.22.46 -81.22.41.69 NAD 83 MAP Nearest Second 11-58-(5.5) WS-IV WS-IV CD-03-7 35.51.27.36 -81.22.28.92 NAD 83 MAP Nearest Second 11-58-(5.5) WS-IV WS-IV CD-03-9 35.48.18.36 -81.21.14.76 NAD 83 MAP Nearest Second 11-57-(2) WS-IV;CA WS-IV;CA Note: Please keep the site information (L) and waterbody information (II.) of the same field on the same page. FORM: LASC 06-16 Pagc 3 SYNAGR®, WESTERN PIEDMONT CLASS B PERMIT WQ 0016247 SOIL SCIENTIST CERTIFICATION This is to certify that soil profile evaluations were conducted on the proposed application sites for the Western Piedmont project by Piedmont Environmental Associates, P.A. on behalf of Synagro Central, LLC. The evaluations consisted of hand auger borings and descriptions of the soils on the application sites. All hand auger borings included in this package were either performed by me or under my direct supervision. All other work performed for this permit application was conducted by Synagro Central, LLC. sort NOM*A G. Christopher Murray, L.S.S. No. 1284 Synagro, Western Piedmont WWTP Project, Various Fields L2 lMiseld FJ� ZssaulmogS Z OWE �Z� 000ualsls u M>w d W s 3dAl eajn;onjlS CL3ZIS - aan;onilS 34b'aJ - am;one;g � a�n;xa1 N T d � o N sn;e;S ain;slow O N U a Urn N f1 T N N U a Q .� '' ad/'o U) o azlS aglow O U v eouepungy al;;ow C7 o E 0 LL s iolo0 alllow o� N � N N mZ o` 4) V V m a m to Joloo xU;ew ) E N O (n � LL m W U N o ul FL sagoul l aG a 4a O nL v uonpop a o y rn� N w aai E E 0 0 E E N N mm M � o v o � Q m N C N O N E m E O N - w U v m E �w ow> > a L > > U N y O a 9 N U O C U _ 9 O N C m j N m C� y � E m E O E O T E m u 0 O T T U ID E TTa'o _T N N U U N NN N N J ;low FJi ssaullal;c i Z OWN iZ� oua;sL ��u M>w d W s 3dAl aainpnj;c or3ZIS - a.Ln;ona;c 30b21J - am;one;c Of N T a °o a 3 0 sn;e;S ajn;sloN N O 0 o U O m r LL U r d N Q > N m .w a01'ou00 xopaZ U3 o o OZl$ alAoN a cn 0 U aouepungy aµ;ol CY o E i s �olo3 ala7oN w LL t m N � @ N �w z� O N m �_ zT ~ N m '� oloo XIJ;eU j, @ N O O (n ZE LE M W U @ a N N = � N LL sagou! 4; a( o � a� a O O U uozuof a a n n C N N N N N N C N N N N N a a a a E E E E 3 E 3 N U U N N N U o 0 o E E E E O W m m V LO N N N M IMO O m V � CJ nR cm N c N � N N E @ E > > O N - 2 (D w E o w> w> a � U N T O a y 9 N U O @ . n rn a a N E 0 m @O c C a m o @ 3 E n m U ` y E N 3 m E O E O T E @ U @ O T T U a E ° a _ @ N J J llo FJ< zF e ssaul�nl;c Zz' < ua;slsuo0;sloN W_Cau o 7 C M dWe 3dAl - ajn;onj;c CL3ZIS - ain;oni;c 34tl21J - a�n;one;c am;xa� N sn;e;g ain}slop o m `o U Z m v LL C7 LL a ri F a s o o m @ ,� aa/Rou00 xopaj U v U ) U e o azIS 0I110Y U) C O U V eouepungV aI1;oV Cl 0 STJoloo aB1oV aLL N w n m � Z rn rn cro Joloo xp;ep m �aao� U a N 73 o U E m sayaul y; aj l U N N E m E N £ G N a 'S "_ 45 a) m m a o o a a) o U 2Y 3 E w E m E 0 o E E W U o T T V m E 0 T Ta m - w .NN m m _T tN /1 O U U N N N � a] N J ;�o7C �;$elc F � � ZF s ssaw�{al;c OWw 0 p oua;Si o WPMo iiWe 3dAl - aan;ona;c CL3ZIS - ain;oni;c 34`dLIcJ - am;one;c a � o a N a sn;e;S ain;sp m : o o U I LL N O > a)W o ) o m m .a) ad/'O U v 0 o'o o OZIS 0I1100 c 0 � U v eouepungy al;1oN O 0 0 S l loo aI11ov d LL N a > @ > z� o � Joloo xu;em w oLI: spa p " m .- o LL sagoul q1 a( 'M o U uozijof c m ' O a N N N C Y Y .� .O N N EEE O O O E E E U U U N N N N I <rvv }} co°'v V Hamm U N N V1 N N E @ E > > O N .g - U 2 @ E E o w > c > �� E L5 0 m a N 0 0 � m o 3 E m (7 U L Y E N 3 E O E O E m m a E c H N � FJ� Zf s ssaul>Iol;c OWM Y Wu We ,o M � 3dAl - am;oni;c 3ZIS - ain;ona;c �oua;s� •suoo;slom 30tl21J - am;any;c w ain;xa� N T Cn m � N a sn;e;S ajn;sloN tv m O 0 0 U r v � U U a) O T a N vcoo a4� a�o� xopa� U) o azIS alaloN U) O � U v aouepungy ap;olA C! 0 Es aolo3 allloN aLL N N Q �=4 Z o �oef loo xu;eNi c f) m m �noiiMm U N a N o � LL m sayaul y; aQ oM O o Q U uozuoH � I � a a N N N N , C G Y Y I rnrnaa N N m a) 0 aa) E E E E 0 a a a 0 0 0 0 E E E E N N U U E .2 .E .E v v�a0 au v 4 am�y Q¢mm v N � N 4) o E m E 3 o a) - U 2 Z E m w E o> w> a g V-- E w '5 V- > U >`oa N O C m (6 3 N .> U C T 2 m uEl OU L5l f1 Q m N N E � E N m c a 6 a a m o 0 3 E N C7 m U ` Y E � 3 N in o E E 0 0— @ m O T T U E a� N0 N N N U U y N N N J ;1a7 I;selc O �;, ; 3 Z I S s a sa a n u l i a� n a a l a; cc FzWZauaaSiWSoM de 3dAl - ainjani;06 c 34b 2 1 J - a m ; a n � a c MwrvrddUaciUNN@NA OUaY�LL`vOONG@N UUaIaatT0Nl omMmMa 3aN0 a � n a x a � snials ajn;sloN U. (D LL a ' a0/ateUEU) az'S alalolA 0)aauepunyyop1oN 0E TsTJO�100014101A LLmZ 0 0 1010J XI;eN oC,) E sayaul y; ac a Mo UOZIOF J Q c U N � � N N E @ E N a)LI E E N o w > > -o g E k S �> U T O U � U � N O C C N 2 m E E a� m a� m Y C a o 0 3 E w m U 2 3 E ` N � E @ E O E O T E @ N @ O T T U TI E = - @ @ N@ N N U U N N In a� N N N U U N N V�1 N J ;I� iseld :�oMe s s a u l �l O ! a c ZmpQoOua;si W3dA1- am;Ona;c CL3ZIS-aan;3na;c 34b21J - a m ; O n g ; c ��v�<cNuamNmNo '.N�rMNC n a � n ; x a � O_ sn;e;S ain;slolAQ cU O r L r) UID aQlOuoo xopat(Do azlS aplON O D aOuepungtl aIRoN 30aE TSTJO�IOOGIPOLA LL O U) olooxu;ev naLEtsoLloup y; aci. o_ O N10 to U uO P% J G II � c N N � N N v l m E > > O N - a U Z N c N N � w E a � E w w U U � N E rn fl.n am m N'E N m `m c N a o 6 m O m U ` y 3 E w .. m � 0 m m o > N— U1 N U U N N 'Ul X - N N N U U d J ;Ion FJ14 ZF ssoulNol;C OWM 0 oua;slsuoo ISION u WPM 3dAl - aan;ona;S CL3ZIS - aan;oni;5 34tl21J - am;oni;5 � aan;xa1 (a 'o sn;e;g ISIOA o `o U O vLL a) a D N 0 rcl ea/'a o azlS aN1oN a U) O � U V aouepungy aR7olA d 0 aE E s aolo0 aB3olA ` o_ LL m N � Z O ca m a m rr aoloo xu;eIA OD co d LL M W o FL m sayoul 41 aC O cuoZIJOF .n c c N N N N N C C N `ol Y Y rn 9 9 � N N a a a a E ElE a a a a o O o o , E E E E U U U U N N N E E E E ro ao ro V � N r N m � N M am �-UK Q Q m m U U N � E 6 E > > o a) - U E c m w E o > > `5 5 U U 9 al U C F U al ' N @ U E a N M D m 9 m N 2 m UU N N N E m a a fl m m N E m m m m m a c 0 a O o 3 E w U m U y E N 3 m E O E T O E m O m O > > U m a E w X 0 N N U U y N N a c m v~ — N N N U U N N a�l N J J Im { x f e ssauhlal;c owo Zouo;sisuoo;slolp W&o M dWe 3dAl - aan;one;c CL3ZIS ain;oni;c 34V21J - am;any;c N am;xa� N N c- a `0 3 sn;e;S ain;sloU LV LL (.`J .-- N O > N w 0 a o .� a0l'oa UOO xopaj o az'S oplov a U) 0 v U eouepungy al;;op C� 0 `m s aoloo olllov a LL 0 �@ z� Y m ° Joloo xij;eU m �amc? cno_i��w U N a N o U) u= m sagoul q; of a1 o 0 C v uozliof J Q fl_ N N N C N N E E E a o 0 Y E E 3 N U U .E.E V o�w vvv I}yy N N M W p W N Q fl_ N N N C N N E E E a o 0 Y E E 3 N U U .E.E V o�w vvv I}yy N N M W p W N N C N_ N N in N E m E > > O 0 _ U c ro w E o w> w> o g w L > > (D U N T 0 .O 9 N U O � .0 N U C > ~ N N m c a o �3 Ern C� U ` Y EN cn3 E m E O O N E 6 U O 0 O > > U N 1p N U U N N U1 �a) a� N — N N U U N d N N J ;MISLIC FJ[ xf e ssaul�ol;c �E: Z oua;si W&a N ILZ 3dAl - alnpna;c 3ZIS - ain;ona;c 3CItliI°J - a�n;one;c N � � sn;e;S ajn;sioN 0 m 1 LL U LL N > N N n o 0 m m .°� aCl/" U U o o az!S aR1oN U) O r U v aouepungtl aFriov C7 0 0 `m s JOIOO aB3oIN LL LL N d) N N G Z OL m ro M JOIOO xlJ;eN a T 0 N UJ LL LL M aD o LL saoul a 4 4a C L o C 0 44 ° J ° U uozuoE �-naa N C N C N N Y Y o� N N a a-oa E E E O O o Y E E E 3 u1 U U N N N N o E E E E v v m m d <O V <} W N r M ¢¢mm U N pCj � N � E m E > > O N .: - 2 (D 0 E > w > a 2E ` w 4,;; > U ° C (6 ' m rn `m rn > = E U E E E N m m m a o ° m 3 E N c� U ` Y N o E N O E m U m r m m v� - N N N U U N G�l N N J ;IOC FJe zF e ssaul�Oi;c OW,; a _ 044 aua;Si7ISUOO ISION �u WPM dWs 3dA L - aJn;OnJ;c CL3ZIS - aJn;OnJ;c 30b21°J - aJn;OnJ;c � aJn;xa1 n o c �J .o Sn;e;S aJn;sioN O LL � N d T a)N v a4/'O�o XOpab m o azlS aR3OlA 0) O U v aauepungy aµ;oN C7 0 S J E oloo olllom N @ 0_ LL N c @ Z o Y V � .c> a n m 10I00 XIJ;eN' u1)d iLLmm VON o N LL m sayaul 43 a0 LL a U uozuoh a a a c N N N N N C C C Y Y � a a-o a-o E E E E E O O O Y Y E E E 3 3 N ((1 .E.E.E.E U1 � 1/1 vvmmco vcOvvv Ln N N N o � ch ro co a m U U Q Q m m N_ C N U! N N E m E J ? O Ul w U E > m w E o>4.3 4 a g N m m` m o 3 E N c� J U Y 3 E m N E 0 m m E N U E T Ta a N N U U y N NN N J IIOl;selc FJs ZF ; ssaUn{ol;c O W u Qo' oUa;slsuOO;sloN u W>� d W s 3dld - ain;ona;c or 3ZIS - am;onj3c 34tli1°J - am;ani;c 5 m a O y sn;e;g am;s{oU O c O 0 o U m M�(Dvo N 0 >. N aQiOUoo xopa� ci o co v0 aziS amou C O U eouepungtl ap;op C1 c 0 v s AOloo a17;ou N n. Z O` (NO d a �olo� xu;ep U) 0 l M OD o U) E m sayoul q; a{ a O O v uozlio{ a Q Q N C N N �ww Y Y O N �U1 EEE O O Y E 3 N U U IA N N E E E I I I M W AO M V N I N >1 � M W � 1 0 � r M {Qmm U N N in N N m E E E o >w E `��� Y U O � C ~ U `m c rn > E> 3 a E N u16 N m U O. O. IO NN E E N m `m rn Y C O O O N 3 E w C� U 2 3 E ` N � E `6 E O N o E A wo E w U N w O > 7 U E a N til N U U N N N a� U U N N N J 107 I;selc F"cs ZH ; ssauhl3l;c O w N Di Z OUa;si71 suoO;slOV i` u W�� dWs 3dAl. w ein;3nJ;c, 3ZIS - einl3nJ;c 34V21J - am;3nJ;c 11 aJn;xa� � T 3 N 3 sn;e;s aJn;slop N N 00 o `oU° nI LL (D 4r N O > N apt 3uo0 xopa2 U m o �n o az!S al;lop C O t U a3uepungy alllop C1 c 0 s JOIOo ag;Op N Z O V W N N N co m Joloo XU;ej (D U) aOm LL o�� w ° m sa Oul ; al t�� a O U UO2UOl n a a C ww� � m EEE O 3 E 3 U N U N N 0 I E E E I I I I M O] OD M CD I N r r r a) a l C6 M I¢mm N m `m rn o 3 E m c� E O E NO E m U B 3 t0 O >, T °> ��� NI N O 'N 'N U U UI fq N C yl- N ___ (q N U U_ y _ N � N J ;PPS2lc FJs = F ; ssauhlal;c 0w� QIx1004 au01Slsu00;slON u Id 0 &Zm 3dkL - aln;onJ;c CL3ZIS - ampnJ;c 30tla°J - aln;anJ;c v am;xa J N T @ @ a o No c sn;e;S ain;slop N E 0 o Urn O M LL CD V F N 0 > N N 0 0 m m °' ad/'auoo xopa� NU ID� a` U o azlS alajop C U) O U N aauepungtl ap;op Ci 0 S J010J 01;;00 a N Z O O I� M JO O XIJ e M m I� 3 6 U j U N a N U) '� N saOul o LL � 4 4l al 0- a 0 U uozlloli a n C N Y N aai aai E E O E 3 U — N 0 E E I' I' 1� J' (D M � N M � o M Qm U N � UJ N N E @ E - v ` m M E > in 'c E 'o » > > E N m O N @ O U m U 2 3 E ` N � `6 E 0 E o T E E u ° v� LA - Ilo f .J49 Z H ; ssaul8o!aS Z OWE �Z` aua;si� ,suoO;SIOR ��u o ILZ 3dA L - ejn nj3S or 3ZIS - am;onj;S 34 V21J - am;one;g N T N � Nc sn;e;S ain;sloN M LL U` V F- N d T N W Uo a0l83uog xopa dl o U _ � o az!S al3;oN c U 0 U aouepungtl alAoN c� 0 s Jolo0 01110IA Ul Z `o `r v m TOIOO xlJ;e[A m CO o ro r ( AD LO LO o LL M 00 U (D (D ` N 60 LE c sagaul ga aC a v O U uozuoE �-a n N C N N L Y Y N N EEE E 3 E 3 — U U a o .E.E M M LO LO N V u]co V o � m M Q m m U N_ N U1 N N E C N E 2 U @ E �w E o�> > as 2 — E w 5� > U O � C F � w rn > U C T E E N to O m O_ O_ U (0 O N E m a. aam W E m m 4 m Y C 0 O NN 3 E w U ` Y 3 E N E m E O l0 E E U O T (0 O TTU ma E 0>1Co T�a,, w CEO N 0 N N U U N N G N J ;low I;seld c FJ �1 F ; ssaul�al;g OWW 0 04 oua;sL u W>� azWo 3dA1- ajn;3nj15 Or RZIS - am;onj15 s 34b'b°J - am;an�1S N a�n;xa1 N T (0 � 4 o sn;e;g ajn;slo 0 N 0 0 0 m o 0 LL CD N a T N N vm '' adl•o co o OZIS aI11oN U) O r U v aauepungy al;;oiA O 0 v s �olo3 ag;oN m a N > Z rn ro 10100 xli;eN m m-ow� m sa auI a u d a O 0 v oZuoF N a C N Y m 9 N E E 3 � N U N f/1 .E � M N Yv o � Q m N C N N N N m E m E O N - L U Z .L Z, Na � m E E ow > > w E ` U U C l6 N G @ E LP N 2 0 9 w'u E �`o�aa0m E UI m v m Y G �o 0 0 a0 3 E N C� U ` Y E a E o E o m E m u 0 O T T U u U N Uil/1 N N N U U N � N N J State of North Carolina DWR Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION Divislon of water Resources INSTRUCTIONS FOR FORM: RSC 0616 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted the Applicant shall submit one on final and two co ies of the a lication and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 1145, FORM: DCAR 11-15, or FORM: SDR 1145). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. ti]I C. Page I of 1 INSTRUCTIONS FOR FORM: RSC 06-16 State of North Carolina Department of Environmental Quality DWR Division of Water Resources RESIDUALS SOURCE CERTIFICATION Division of Water Resources FORM: RSC 0646 L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction BJ: 1. Facility Name: Killian Creek WWTP 2. Facility permit holder is: ❑ Federal, O State, ® Local Government, or Private. Facility permit issued by: Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: 3. Facility contact person and title: Tim Simmons Lake Killian W WTP Superintendent Complete mailing address: 7085 Old Plank Rd, City: Stanley State: Zip: 28164 Telephone number: 704 749-2226 E-mail address: tsimmons@lincolncounty.org 4. Facility physical address: 7085 Old Plank Rd City: Staple State:' Zip: 8164- Coordinates: Latitude: 35o 25' 22" Longitude: 810 Ol' S6" Datum: NAD 84 Level of accuracy:ee Method of measurement: t 5. Purpose of the facility: ® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: '_ % industrial and F. % domestic) ❑ other (explain: ). Yes ❑ No 6. Does the facility have an approved pretreatment program: 7. Facility permitted/design flow: 2.5 MGD and facility average daily flow: 1_1 MGD 8. Average amount of residuals being generated at this facility Est.'1125 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 2 digestors totaling, 1.05 million gallons Type and volume of residuals storage (i.e., outside of residuals treatment on 255K gallon sludge holding tank RESIDUALS QUALITY INFORMATION (See instruction C.): 1. specify if residuals are regulated under: M 40 CFR Part503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257, 2. Specify if residuals are defined under 15A NCAC 02T 1102(6) as: Biological ❑ Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing ter� or the biological teerasutilizes biological processesincluding lagoons, activated sludge systems, extended aeration systems, and fixed film systems). Page 1 of 5 FORM: RSC 06-16 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under completed for facilities that are less than 0.5 MGD in design flow that treat RCRA: (Note -this item does not have to be 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: d yes no. if yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ Yes N ho, f the latest toxicity characteristic leaching procedure (TCLP) analysis as Fill in the following tables with the results o well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 2/14/2020 Passed corrosivity test: yes ❑ no. pH: s.u. (2 < pH < 12.5) . Flashpoint: >200 °F (> 140°F) Passed ignitability test: ®Ye5 no. P Passed reactivity test: ®yes ❑no. HCN: ND mg/kg (<250) & HiS: ND mg/kg (<500 ) TCLP Parameter Limit Result TCLP Parameter Limit Result (mg/1) (mg/i) (Mg/0 (S ) Arsenic 5.0 ND Hexachlorobenzene 0,13 ND Barium 100,0 ND Hexachloro-1,3-Butadiene 0.5 ND 0.5 ND Hexachloroethane 3.0 ND Benzene ND l.0 ND Lead 5.0 Cadmium Lindane 0A ND ( Carbon Tetrachloride 0.5 ND 0 2 ND Chlordane 0,03 ND Mercury Chlorobenzene 100.0 ND Methoxychlor 10.0 ND ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND ridine 5.0 ND o-Cresol 200:0 ND P Y p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-13 10.0 ND Tetrachloroethylene 03 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND ND Trichloroethylene 0.5 ND 1,2-Dichloroethane 0.5 ND 2,4,5-Trichlorophenol 400.0 1,1-Dichloroethylene 09 ND 2,4-Dinitrotoluene 0.13 ND ND 2,4,6-Trichlorophenol 2.0 Endrin ND 0.02 ND 2,4,5-TP (Silvex) Lo Vin 1 Chloride 0.2 ND Heptachlor and its Hydroxide 0.008 ND Y Page 2 of 5 FARM: RSC 06-16 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waydoint Analytical and Date of analysis: 6/17/2020 Parameter Ceiling Monthly Average Result Concentration Limits Concentration Limits (ClassA & ClassB) (Class A Only) (mg1kg) (mg/kg) (mg/kg) Arsenic 75 41 <19.2 Cadmium 85 39 <3.85 Copper 4,300 1,500 286 Lead 840 300 14.4 Mercury 57 17 1.03 Molybdenum 75 n/a 10.8 Nickel 420 420 46.5 Selenium too 100 <19.2 1 Zinc 72500 2,800 727 b. For Surface Disposal Unit (lanrlfll/): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: L- and Date of analysis: aw Distance from Disposal Arsenic Chromium Nickel Unit to Boundary to Closest Property Line k (mglkg) (mg/kg) (meters, check one) (mg1 g) ❑ > 0 but <25 30 200 210 > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) Page 3 of 5 FOKM: RSC 06-16 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 2.61 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis:6/17/2020 Parameter Result (nag/kg) Aluminum 1 Q600 Ammonia -Nitrogen 31,000 Calcium 13,700 Magnesium 3,550 Nitrate -Nitrite Nitrogen 229 PH (Standard Unit) 73 Phosphorus 203900 Potassium 55080 Sodium 36,300 Total Kjeldahl Nitrogen 88,500 c. Using the results listed in Item II, 5b. above, calculate the sodium adsorption ration (SAR): ll_55 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: [}0 %. This rate is a (check one): ® default value, or N actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (15t) Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (ing/kg) Surface 325979 443197 Injection/Incorporation 48,479 5%697 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 5 7. Pathoeen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. ForDistribidiae/LmtdAppticattonofClpssAorEnaivnlent: Li A fecal coliform density that is demonstrated to be less than 1,000 WIN per gram of total dry solids, or 0 A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] - Time/Temperature Compliance. ® Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. rNI Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ® Alternative 4 [15A NCAC 02T.1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Hchninth Ova. Alternative 5 [15A NCAC 02T.I l06(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, % heat drying, R71 heat treatment, ❑ thermophilic aerobic digestion, beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Laud Application of Class B: ® Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.1 106(c)Q1 -Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, K air drying, ❑ anaerobic digestion, ❑ composting, or ITJI lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II.7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item It. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item I1.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC' 02T.7107, specify how residuals will meet the VAR requirements: Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38%Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Alternative 4 [15A NCAC 02T.1 ] 07(a)(4)] -Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes, Z Alternative 6 [15A NCAC 02T.1107(a)(6)] -Alkaline Stabilization. Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals. Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I107(b)(2)]. Not Applicable -Non-Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or I may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 KILLIAN CREEK WWTP QUANTITATIVE JUSTIFICATION FOR RESIDUALS PRODUCTION RATE The following is a record of the annual land application volume for Killian Creek wastewater treatment plant: Year Dry Tons Land Annliell 2018 68.51 2019 30.41 The proposed permitted volume (250 dry tons per year) is greater than the anticipated need for the coming years. Over the 2 years shown above the average number of dry tons land applied were 49.46 however future plans for maintenance cleanouts and application of backlogged material are expected to require the requested 250 dry tons per year requested. Residuals Sampling Plan Synagro Residuals Land Application WQ0016247 Killian Creek WWTP Nutrients and Metals Analysis • Sampling Point: Sludge Holding Tank • Sampling Frequency: Annually • Sample Type: Composite • Lab: Pace Analytical Pathogen Reduction (Fecal Coliform Density Demonstration) • Sampling Point: Sludge Holding Tank • Sampling Frequency: Annually • Sample Type: Grab ( • Lab: Statesville Analytical Vector Attraction Reduction (38% VSR) • Sampling Point: Digester TCLP Sampling Frequency: Annually • Sample Type: Composite • Lab: Meritech • Sampling Point: Sludge Holding Tank • Sampling Frequency: Once/permit Sample Type: Composite • Lab: Summit Environmental Technologies, Inc VICINITY MAP SYNAGR® �c rra / Hilh Me O�qA i .o / 5 ° �WastewaterTreatment Mini Smart Car Finder v oy JJ ' Sennebogen oiOr Earnhardt Grading, Inc 0 T Ari�L� J r LKN Boat Lifts Q °rh; kcr Rock Hill United Methodist Church P o"Plank Rd x eQa\\\o9� l GNp�Pnn yr OWNER s Lincoln Co: Killian Creek Wastewater COUNTY: Lincoln ��' Treatment Plant aceAnalytical Ir„ .Flcfllht February 24, 2020 Crystal Little Statesville Analytical, Inc. 122 Court Street PO Box 228 Statesville, NC 28667 RE: Projeck LC Pace Project No.: 92463883 Pace Analytical so"icea, LlC BB08 IOnwyAva. sa8c 100 nunterawle. NC 28078 1704)878 8082 Dear Crystal Little: Enclosed are the analytical results for samples) received by the laboratory n this report. Results reporteedd herein conform o February 05, 2020. The results relate only to the samples included Itthe nd the whereurrent, appliun cable TNI/NEise n tadLAC ndardsIn body of the reportlaboratory's Quality Assurance Manual, most applic ble, If you have any questions concerning this report, please feel free to confect me. Sincerely, Tyriek Nooks tyriek.hooks@pace) abs.com (704)876-9092 Project Manager Enclosures Page 1 8127 PO Box 228 •Statesville, NC 28687 • 704/872/4697 Page 1 f of 37 aceAnalytical' ywgecerlLeem Project: LC Pam Project No.: 92463883 peas Analyllaal Servlees Pennsylvania 1638 Roseylown Rd Sultea 21364, Greensburg, PA 15601 ANA6 DOD -FLAP Red Aceredilalion #: 124'17 Mabama Certification #: 41690 Arizona Codification #: AZO134 Arkansas Cedlficalmn California Codification #: 04222CA Colorado Codification No PA01541 Connecticut Codification M PH 0804 Delaware Codification EPA Region 4 DW Ratl FladdarTNI Codification #: E87683 Georgia Codification N: C040 Florida: Cod E871140 SEK5 WET Guam Codification Hawail Cedl9calion Idaho Codification Illinois Codification Indiana Codification Iowa Codification M 391 KansasRNI Certification #: E-10355 Kentucky Certification #: KY90133 KY WW Permit #: KY0008221 KY WW Permit 4: KY0000221 Louisiana DHHRNI Certification #: LA180012 Louisiana DEG7TNI Codification #: 4086 Maine Certification #: 2017020 Maryland Codification #: 300 Massachusetts Cedifioelion #: M-PA7457 MichigaNPADEP Codification M 9991 Pace Analytical Services National 12065 Lebanon Raad, MI. 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NC 28078 (704)075.9092 CERTIFICATIONS Missouri CeNOcellon q: 235 Mou tons Certification #: Car10082 make Corllgea0on #: NE-OS-29•M Nevada Codification #: PA014572018-1 New HampshlreRNI Codification #: 297617 New Jersoy7TNl CenlOcallon #: PA051 New Mexico Cedifcea8on #: PA01457 New YorkJTNI Codification #: 10080 NOall Carolina Cenlgcati at N: 42106 North Dakota Codification #: R-190 Ohio EPA Ratl Approval: )[41249 OregonRNl Cenllicallon #: PA200002-010 PonnsylvaniarrNI Codification #: 65-00282 Puerto Rico Con ficallon M PA01457 Rhode Island Certification #: 65.00282 South Dakota Codification Teamasses Cer igoallan #: 02867 TexaslTNI Cadificalion #: T104704188.17J UIahfTNI Corlillcalion #: PA014572017.9 USDA Sol[ Permit #: P330.17-00091 Vermont Dept. of Health: ID# VT-0282 Virgin IslendlPADEP Certification VirglnleMELAP Certification #: 9526 Washington Codification #: C668 Weal Virginia DEP Codification #: 143 West Virginia DHHR Certification #: 9964C Wisconsin Approve List for Rod Wyoming Certification #: STMS-L N:I- Kentucky Codigcailan #: 90010 Louialne Certification#: 2 Laul9lane DW Cargill #: LA100010 Maine Cen[Bcatlon #: TNM02 Maryland Codification #: 324 Massachuselts Codifeallan #: M-TNO03 Michigan Codification #: 9958 Minmacro Conificalion #: 047-999.395 Mississippi Certification 9: TN00003 Mlssoud Cedgcation #: 340 Montana Codification 0: CERT0086 Nebreaks Codification #: NE-0845-D5 Nevada Codification #: TN-03-2002-34 New Hampshire CergOoollon #. 2975 New Jersey Certification M TNO02 Now Maxim DW Cedificmlon New Yolk Cedifkatiorl ll: 11742 Nadh Carolina Aqualic Toxicity Codification #: 41 North Carolina Drinking Water Certification It: 21704 Nanh Carolina Environmental Cedigcare #: 376 REPORT OF LA60RATORY ANALY313 1Ne report anon del ba mpmaaaaa. axeepun Iwl. v411wul the written consent of Pace Analygcal6arvicas. LLC. Page 2 of 27 PO Box 228 •Statesville, NC 28587 • 704/872/4097 Page 12 of 37 aceAnalytical• YIM4.plta1r11.aen ProleG: LC Pecs Prated No.: 92463883 Paee Analy9ca19ervlces National North Dakota Certification M R440 Ohio VAP CeN6callon #: CL0069 Oklahoma Certification #: 9916 Oregon Codification #: TN200002 Pennsylvania Cerlificallon M 68,02979 Rhode Island Codification #: LA000366 South Carolina Codification #: 84004 South Dakota Codification Tennessee DWIChenVMicro Codification 2006 Texas Codification #: T 104704246-17-14 Texas Maid Comeaallon #: LAB0152 USDA Soil Permit #: P330.15.00234 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersvilla, NC 28078 LovislenalNELAP CeNficallon # LAW0026 North Caroline Drinking Water CerllOcaft n 0:37706 North Carolina Field Services Cedilkefir n #: 5342 Nodh Carolina Wasiewalercartlficallon #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 20904 FloddsINELAP Certificetlon #: E87048 Mossachueolk Codification #: M-NC030 North Carolina Drinking Water Codification #: 37712 Paco Analytical Services, LLC 600otuitoy Avo. Sidle 100 HunlersWllo, NC 28078 17041075r9092 CERTIFICATIONS Uleht.of#:TN00003 Vermoontnt Deptof Health: ID# VT-2006 Virginto Codification #: VT2006 Wginla Codification #: 460132 Wa thinglan CedlOcalion #: C841 at Virginia Cediflcation #: 233 Wisconsin Cedificatlan M 9980039910 Wyoming UST Codification #: via A21A 2926,01 A21A-18017026 Certification #: 1461.01 A2LA-ISO 17D26 certineo6on #: 1461.02 AIHA-LAP/LLC EMLAP Cedification#:100789 South Carolina CediOcallon #: 89006001 Fbrlda7NELAP Codification #: E87627 Kenlucky UST Codification #: 84 VlrglnIoNELAP Codification It. 460221 1. Nodh Carolina Wastewater CertiOcellon #: 40 South Carolina CedlOcalion #: 99030001 Vi(glnIaNELAP Ce tificaboo #: 460222 REPORT OF LABORATORY ANALYSIS Tnls report shell not he reproeuce4, except In Nn, Pa00 3 of 27 out the written consent or Paw Anelyliwl 6eNlces. LLC. PO Box 228 •Statesville, NC 28687 • 704/872/4fi97 Page 13 Of 37 aceAnalytica axW.7anlM.soa ProfeCL• LC Pace Project No.: 92463683 Lab ID Sample lD 92463663001 200204,49,01 LC. Pace Anolyllcal so" Coal LLC eo00 KomyAve. Suite 100 HunleraWle. NC 26070 t1a41916.9092 SAMPLE ANALYTE COUNT gnalytas Analysis Reported Laboratory Method _ 3 PAN 8ISIA EPA 51A 9 PASI-C EPABOSIB GEM GEM SEM 8 PASI-C EPABOB2A EPA6082A GEM 8 PAS6C Sill 7 PASLA EPAMOD EPA7470A Soo 1 PASI-A SPJ 18 PASt-C EPA827OF EPA826OD SAS 14 PASI-C SMK 1 PASI•A EPA101OA SMK 1 PASI-A EPA0046D EPA90958 SMK 1 PASI-A PAS 1 PASWA EPA9014 SM 450082E-2011 PAS 1 PASI-PA REPORT OF LA80RATORY ANALYSIS Thta repwl shalt nal be repretlucetl, except In lull, w11hoW the wrltton consent of Paco Analytiwl6ervitesI LIC. PaOe 4 of 27 PO Box 228 • Statesville, NC 28687 • 704/$72/4697 Page 14 of 37 aceAnapifcal ` Mw Pnvlll.tw ANALYTICAL RESULTS pace Analytical Services, LLC 9000KInceyAva. Sue0100 Humemule. NO 26018 (7041D16,9092 Pcoleci: LC Pace Project No: 92463083 Semple: 200204.49.g1 I.C. Lab ID: 92463883001 Collected: 0210412012:26 RacelVad: 02/05f2013:08 Matdx: Water Results Units Report Limit OF Prepared Analyzed CAS No. _Dual Resu Parameters --.- Chlorinated Herb,(OC) 6151A Analytical Method: EPA 6151A Pfepatallon Melhod:8161A Leachata MelhodlDate:1311; D2liif3014:58. Initial pH:7.04; Final pH:4.00 No mglL 0,00200 1 02/1212019:28 021W20 00:17 93.72.1 2,4.5-TP(Sllvex) ND 8tL 0.00200 1 02112f2019:26 0211412000:17 94-76.7 2,4.0 Surrogates 69.8 % 14.0-156 1 001212.019'28 021102000:17 19719.20.9 2.4•DCAA(3) 8081 TCLP Pesticides FIVE Analytical Method: EPA 8081E Preparation Method: EPA 3610C Leachele MalhodlDate: EPA 1311; 0211312017:17 initial pH: 5.93; Final PR NO vile. 0.50 1 0211412013:29 02115P2009:57 68-09-9 gamma•BHC (Lindens) NO ulik. 3.0 1 0211412013:29 0211512009.57 57-14-9 CNordane(Technical) NO �� 0.50 1 0211412013:20 0211512009:57 72-208 Endrin 0.50 i 0211412013:29 0211512009:67 70-44.8 Heptachlor NO ug1L NO ug1L 0.60 1 02I1412013,29 02115/2009:57 1024.57.3 1leplechlor spoxIds NO ugll- 1000 7 02H412013.29 0211512000:57 72-43.5 Melhoxychlor NO uglL 3.0 1 0211412013:29 0211512009:57 8001-35-2 Toxaphene Surrogates % 10435 1 ON1a1'2013:20 02IJ612009:57 2061.24-3 43 Decachlorobiphaml(5) 44 % 10.110 1 02,14,2013:29 0211512009:57 677-09.8 Tebechloro-m-xylene(8) BD02 005 PCB RVE Analyllcsl Method: E PA 6082A Preparation Method; EPA 35100 802 G 16 PC8 for 1018) NO uglL 6.56 1 02t11/2010:39 02 IWI)16:18 12674.11-2 PC8ND uelL 0.50 1 0211112010.39 0211212016:18 11104.28-2 PCB•1221 (Aoclor 1221) NO u911 0.60 1 02/1112010,39 02/12/20 Wig 11141.16-5 PCB.1232(Aroclor 1232) ND uglL 0,50 1 02/1112010:39 02M21201618 53469.2t-9 PC5•1242(Aroclor 1242) NO uglL 0.59 1 02Ht/2010:39 02M2120%ifl 12672,22.6 PCB•1248(Procter 1248) ND uglL 0.50 1 021111201003l 02JI 212016:18 11097.69.1 PCB-1254 (Aloolor 1254) ND u91L 0.50 1 oM11120 10:39 0211212016:18 11006 82-5 PCB.1260 (Aroclor 1260) Surrogates 38 % 10-130 1 02111120 100 021t2120 18:18 2051.24-3 Decacnloroblphenyl(8) Analytical 8052 TCLP PCBs RVE Leachh)Melhotl:ate:Ep 2APleperacf2 Me1110tl:EPA3516D Leechele MelhatllDeie: EPA 1311; 02/13I201T.17 Initial pH: 5.93: Final pH: PCB•1018 (Arocbr 1016) NO ug/L loco 1 0211412013:29 02/15/20 14:05 12674.11-2 PCB-1221 (Aroclor 1010) ND u91L 100D 1 02M4/20 13:29 02115120 14'95 11104.28-2 PCB-1232 (Arocbr 12211 ND ug/L 1000 1 02114/2013.29 02115120 14:05 11141-186 PCB•1242 (Aroclor 1232) NO ug1L 1009 1 0211412013:29 02115/2014o5 53469-21.9 PCB•1248 (Amster 1242) NO ug/L loco 1 02/1412013:29 0211512014:D5 12672,29.8 PCBA254 (Aroclor 1246) NO uglL loco 1 0211412013:29 02/15/2o 14:05 11097.69-1 PCBA280 (Aroclor 1250) NO ug/L 1000 1 0211412013:29 OV1512014:05 11096'82-5 Surrogates 59 % 10-132 1 02114120 13:29 02/15/20 14.05 7051.2403 Decacht=11113h8nyl (3) 6010 MET ICP1 TCLP Analytical Method: ate: EP 1 preparation:02IJ312Me100tli EPA3010A Leachele MalhodlDale: EPA 1371; 02/13I2o 17:00 Initial pH: 7.74; Final pH: 4.6 0.050 1 02/14120 11:12 02/15120 01110 7440.38.2 Arsenic ND millL 0.25 1 0211412011:12 0211512001:10 7440.39-3 Barium ONO mgR 0.0050 1 02114120102 0211517001:10 7440.43.9 Cadmium REPORT OF LABORATORY ANALYSIS TBIs rapo4 sbell not b0 repiO4uced. 0xcepl In lull. page 5 0( 27 Data: 021241202006:09 PM viboullhewrillenwnsenlol Pace Analytkal SOlMices,LLC. PO Box 228 •Statesville, NC 28687 • 704/872J4697 Page 15 Df 37 Pace Molyucal Sonflaos, LLC 98o0Kocoy AVo. Buile 100 HunlersOlile. NG 2BO78 awnalytical • (7041876 9092 .pagkbuc4m ANALYTICAL RESULTS Proleci: LC Pace Plolecl No.: 92453803 Semple, 200204.49.01 LC, Lab 10: 92468083001 Cclloct¢d: 0210412012:28 Received: 02106/20 13:08 Malrtx: Water Results units Report Limit OF Prepared Analyzed CAS No. Duel parameters - 6010 MET ICP, TCLP Analytical Method: EPA60100 Preparation Method: EPA3010A LBschste MelhodiD8la: EPA 1311; 02113/20 17:00 Initial pH: 7.74; Final pH: 4.6 0.05D 1 0211412OW12 02115I2001:10 7440-47-3 Chromium NO MIL nip MOp 0,025 1 0211412011:12 021151200110 7439.92-1 Lead NO MOIL 0.10 1 02M41201112 0211612001.10 778249.2 Selenium NO MOIL 0.025 1 0211412011:12 0211812001:10 7440-22.4 Silver MaMethod: 7470APrap13M00dEPA 7470A 7470MOrGury,TCLP LeaahaleMBlhotlloUrEPA1311; 02,1312017:00 Initial pill: 7.74; Final pH: 4.5 NO MOIL 0,00020 1 0211412Q 16:31 0211720 10:59 7439-97-6 Mercury 8270E MSSV TCLP Bap Funnel Analytical Molhod: EPA 8270E Preparation Method: EPA35100 NO ugIL 60.0 1 021J420 10:27 02M4120 16:24 1O6.464 1,4.01chloroberf NO ugll. 50.0 1 02M4120 10:21 02/14120 16:24 121.14-2 2,4-DInilfotoMsne 14D ugIL 600 1 02M412010:27 02114120 16 24 07.603 Hexaohlofo-1,3-buladlene ND MOIL solo 1 0211412010:27 0217412016:24 118.74-1 Hexachombenzene NO ugIL solo 1 0211412010:21 O2f1412016:24 67-72-1 Hexachloroethane NO ugll. 60.0 1 02/14120 10:27 07J14120 16:24 95-48.7 2•Melhylphenol(a-Cre601) NO ug)L 69.0 1 02A412010:21 02/14/20 %24 16831-10.4 384-Methylphenol(m8p Cms01) NO ugIL 50.0 1 02114120 10:27 02114120 16:24 98-95-3 Nitrobenzene ND ugIL 100 1 02/14/20 f0:27 02)1412016:24 87-B6.5 PentachlomPhenOl NO ugIL 50.0 1 02JI4120 10.27 02114120 16:24 110-86-1 Pyridine NO uglL 50.0 1 02M412010.27 02IJ412016:24 95-95-4 2,4,5.Trichlorophenol 14D ug1L 60.0 1 02f14IZO 10:27 0211412016:24 88.06-2 21416-TdchunDithenol Surrogates fib % 12-102 1 0211412010:27 02114120 16:24 4165.60.0 Nitrobenzene-0(S) 65 % 13.107 1 02M4120 JO:27 0211412016:24 321-60-8 2-FluorobiPhenYl(5) 96 % 21-132 1 0211412070:27 02/1412016,24 1718-51-0 Telphenyl-d14(S) 22 % 10-110 1 0211412010:27 0211412016:24 13127.883 Phenobde(S) 32 10-110 1 021141201o:27 02014120 16:24 36T.12.4 2-FluomPI1MAol(9) 91 % 27-ioe 1 0211412010:27 0211412016:24 11B.79-6 2.4,e-Tribromaphenol(8) 8260D MSV TCLP Analytical Method: EPA 8260D 02IJ412016:68 71-43-2 u IL too 20 Benzene ND O 200 20 0211412016:58 78.93.3 2-Bulanon0(MEK) NO ug& 100 20 0711412076:58 56.23.5 Carbon tetrachloride NO ugIL 100 20 OW1412018:58 108-90-7 NO ugl ChloraDenzene L 100 20 0211412018:58 67•663 Chloroform NO upt. 100 20 02M4I2016:58 JOI)AB.7 1,4-01chlarobenzene ND MOIL 100 20 02H4120 16:66 107.06-2 1,2.01Ghlomethane NO ugIL 02IJ420 10:55 75.35.4 NO uglL 100 20 Telrac ImOulheng NO ugIL 100 20 0211420 1858 727-1-0 Trioldola lhormne NO uOL 100 20 0211412018:68 75.01-0 Tflc1110melhane NO V98. f00 20 02114/2018:58 75.01-4 L1 Vinyl chloride surrogates 105 % 70-130 20 02114120 18:68 2037.26m5 L2-Dlchloembane-d4(5) 106 % 67-135 20 02114120 %18:68 20OmOO-4 Toluene-d8(8) 103 % 70.130 20 02114120 18:58 480.00-4 4-Bromonuorobenzeno(S) REPORT OF LABORATORY ANALYSIS TNs repon shoe not Da repiOauNa, except N Intl, page 6 of 27 pate: 02124202005:09 PM Athoul the written eonsant of Pace Anarylinalfi0rvicas.LLC. PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 16 Dt 37 Pace Analytical Services, LLC 98o0 Kincay Ave. Salle too Huntenv918• NC 2BO78 1weAnalytical • (704)676 9092 MMwAardlErFM ANALYTICAL RESULTS Protect: LC ON) Project No.: 92483883 Semple: 200204.49.01 LC. lab I0: 92460860001 Collected: 02104i2012'26 Received: 02105/20 13:00 Matrix: Water ad Analyzed CAS No. Qual Parameters Results Units Report Limit OF Prepar 1010 Flashpoln6Closed Cup Analytical Method: EPA 1010A 02118/20 15:28 lg >200 deg F 70.0 1 FlashDolnl 2046 PH Sell Analytical Method: EPAnits 0.10 7.0 Sid. Units 02M7120 15:41 H3 pH at 25 Degrees C 1 9095 Paint Filler Liquid Test Analytical Method: EPA 90950all 1'0 02118f20 10:54 Free Liquids F1 7330 S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-046 0.2 1.0 i 02110122110/2016:55 0211t/2017:19 Cyanide, Reactive No mglk9 7345 Reactive Sulfide Analytical Method: SM 450DS2F.2011 Preparation Method: SW-6467,3.4.2 Sulfide, Raacirve NO mgm9 10 1 02I1012016465 0211012016:67 REPORT OF LA80RATORY ANALYSIS T81s report snptl not be repraduceq ezcopt in lull. page 7 o12T Date: 02124/2020 W09 PM without t5e wroton consent of Pace Analytical SOMces, Llc. PO Box 228 •Statesville, NC 28687 • 704/872/4697 Page 77 of 37 8?6Analpical• Wwa.IreNslr.em Paco AnalyOcal Services, LL9 9a00 Kincey Ave. Suite 100 F rrsrsville, NC 28078 (7041875-SM2 QUALITY CONTROL DATA Prolaci: LC Pace Poled Na.: 92463883 QC Belek 1428765 Analysts Method: EPA8161A QC Balch Method: 8151A Analysis 06SUIPIRM: Chlorinated Herb. (QC) 8151A Associated Lob Samples: 92403883001 METHOD BLANK: R3498818-i Aescalated Lab Samples: 92463883001 Parameter Units 214-D rrlglL 2,4,5-TP(311vex) m82 2,4-OCAA (S) % LABORATDRY CONTROL SAMPLE: R369ge18-2 Parameter Units 2,4-D m911, 2,4,5-TP(Sllvex) mgiL 2,4.DCAA (S) % Matrix: 6olitl Blank Reporting Result Limit Analyzetl QualiOals ND 0.00200 0211312012;05 ND 0.00Y00 0211312012:05 67.2 14.0.158 0211312012:05 Spike LCS LCS % Rea Cone. Result % Rea Limits Qualifiers 0.0360 72.0 60.0. 120 0.0500 0,0500 0,0372 74.4 60.0.125 71.0 14.0.168 MATRIX SPIKE B.MAiftIx SPIKE DUPLICATE: R34906183 R3498618A MS MSD L1188836.02 Spike Spike MS MSD MS MSD % Roo Parameter Units Result Cana. Cone. Rosati Result % Rea %Rea Limits RPD Qua] 214•D mg/L ND OB600 0,0500 0.0360 0,0324 72.0 64,8 50.0,120 10,5^- 2,4,5.TP(Silvex) mglL NO 0.0500 0.0600 0.0374 0.0330 74,8 66.0 60.0-125 12.5 0/0 81.8 SBA 14.0-158 2,4•DGAA(S) n.mr. nraa.m,een wla a.e..,• m m. emu macma av m. •omi: • caamn «o.pteker. an aurnau amw pracm.am m. nam an6a r.rou. REPORT OF LABORATORY ANALYSIS TMs rapod abnll nM be reprotlu<etl, aaaepl In full, Oate: 021241202005:09 PM vnlhoullbe%vattemmnsenl or Pace Analylical9arvlwsI LLF Page 8 d 27 PO Box 228 • StatesvHle, NC 28687 • 704/872/4697 Page 18 D137 i aceAnaVicale - rlww.Psedrhl.een ProJecc LC Pace project No.: 92463583 DG Belch: 525220 DC Belch Method: EPA7470A Associated Lab Samples: 92463063001 METHOD BLANK: 2600050 Associated Lob Samples: 92463883001 Parameter Merwry QUALITY CONTROL OA7A Analysis Method: `�'a ��� Malysls DBSGIP0011: 7470 Mercury TGLP -- Maldx: Water Blank Repotting Analyzed qualifiers Units Result Limit qualifiers mg2 ND 0.00020 0211712016:40 Paco Analyleal SBrvleea. LLC 9600 Klncey AVe. Sells 100 Hunlarse la. NC 28078 (7041878.9092 LABORATORY CONTROL SAMPLE: 2807381 Spike LCS LGS %Rec Parameter Vnlls Conc. Result %Ron Limits Duallfmrs 80-120 Mercuryry moil 0.0025 0.0028 114 2807362 2007363 MA7ft1%SPIKE SMATRI%SPIKE DUPLICATE; MS MSD 92463414001 Spike Spike MS MSD MS MSD %Rec Units Result emu. Conc. Result Result %Rec %Reo Limits RPD Duel Parameter 95 112 75-125 16 J— mail ND 0.0025 0.0025 0.0024 0.0028 Mercury PeeVlla presented onlFla papa ere In the voila Ntllasiedby the"Unlr�' <olvm" ex<ePtwaera ee elle�nels unit la psese"letl la the rI9M11 e1 iFe mull. REPORT OF LABORATORY ANALYSIS This report ehail not be reproduced. except In lull. page 9 of 27 Oare: 021241202005:09 PM wilhoul the unite" consent of Pew Analylieal Services, U.C. ( PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page ig of 97 aceAnaVicalo ww.prrdrespala QUALITY CONTROL DATA Project: LC Pace project No.: 92463883 CC Belch: 626225 Analysis Method: EPA6010D Analysis Description: 6010 MET TCLP QC Botch Method: EPA301DA Associated Lab Samples: 92463883001 Matdz: Water METHOD BLANK: 2006056 Associated Lab Samples: 92463883001 Blank Reporting Parameter Units Result Limit Analyzed NO 0.050 02/1612000:22 Arsenic mg1L NO 0.25 021162000:22 Barium Mon. NO 0.0050 0211612000:22 Cadmium MSNO 0.050 0211612000:22 Chrmolum M9�L NO 0-025 0211512000:22 Lead NO 0.10 0211512000:22 Selenium MOIL NO 0,025 021151200022 Silver METHOD BLANK: 2806716 Associated Lab 3amplea: 82463803001 Parameter Unlls Arsenic mg/l milli. Barium IL Cadmium OIL MOIL Chromium M91L Lead MOIL Selenium Mali. Silver Matllx'. Weler qusli0ers Blank Reponing Analyzed QualiOen Resell Llmil NO 0.050 0211612000:28 NO 0.25 021162000:28 NO 0.0050 0211612000.28 NO 0.050 021162000:28 NO 0.025 02)1512000:26 NO 0.10 021152000:2B NO 0,025 021151200028 Pavo Analyllcal Shortens, LLC Ha00looney Ave. Suite 100 Hunlersvllle, NC 28MB (70e)815-9092 LABORATORY CONTROL SAMPLE: 2807346 spike LCS LCS %Roc Conc. Result %Rec Llmils Qualieere Parameter MOIL _ 2.5 2.5 f00 80-120 Arsenic M91L 2.6 2.5 102 80,120 Barium MgIL IL 2.5 2.6 100 80-120 Cadmium mgg8 BOA20 Chromium MOItLL 2.5 2.5 98 60.120 mglL 26 205 107 RO.120 Lead In9ll 2.5 2.7 Selenium MOIL 1 2 1,2 97 80-120 Silver LABORATORY CONTROL SAMPLE: 2807341 Spike LCS LCS %Rec Ungg Conc. Rhsull %Rec Limits OuallOers Perameler 101 80-120 15 2.5 Armerdo M� 26 2.6 104 00-120 Barium assess Presented no Ibis pasaan In the bolts Indtoatea by aw"undo" wlrmn sentP, ,bars an alternate unit Is presented to the fight of reaull. REPORT OF LABORATORY ANALYSIS This ropod area nal be reproduced, exceN in lug' page 10 of 27 Dale: 02242020 05:09 PM wlihvel Me written mnsenl of Pace Analytical Sbrvless. LLC. PO Box 228 •Statesville, NC 28687 • 704/872J4697 page 20 of 37 a ceA�nalytical• QUALITY CONTROL DATA Project: LC Pace Pooled No.: 92463083 LABORATORY CONTROLSAMPLE: 2801347 LCS Spike LCS Conn. Result % Rec ParameterUnits mg1L 2.5 2.6 Cadmium mgIL 2'5 26 Chromium mull. 2.5 2.6 Lead mglL 2.5 2.0 Selenium mglL 5.2 1.3 Silver Pace Analyllcel Services, LLC BB00 Rlacey AYe, Sure 100 Hunleravule, NC 20018 (704)915.9062 Rec Limits Qualifiers 04 80,120 01 60-120 103 60.120 111 BO 120 01 80A20 2807350 MATRIX SPIXE BMATRIX SPINE bUPLICATE: 2807349 MS MSD 92464791005 Spike Spike MS MSD MS MSD Parameter Units Result Cone. Cone. Result Result % Rac %Rec --_ mull. NO 2.6 2.5 2.3 2.3 93 90 Arsenio mglL O,NO 2.6 2.5 2.6 2.5 95 91 eadmI mglL 0.29 2.5 2.5 2.8 2.7 09 95 Cadmium mull 78.2 2.5 2.6 76.0 74.4 .11 -76 Chromium lL 1.1 2.5 2.5 3A 3.3 94 91 Seed mgiL silverum m9r. NO 1.5 2.5 1.2 2.4 197 97 Silvef mull. 0.0039J 1.2. 1.2 5.2 1.2 97 94 %Rec Limits RPD Qu01 75-126 3 75-125 4 75-125 3 75-125 2 M5 75-125 2 75-125 5 75.125 4 aevulle psvfemetl on Ibis pees are In the antis lntllcatetl sy lM1e'0Nu"column va4eplwM1vra en ellernela anti le preeenlealo the r19F1 p11Fv result. REPORT OF LABORATORY ANALYSIS mla repo4 sneu not 6a ragcavwa, except m mn, Date: 0212412020 08:00 PM without thewGllpn consanl of Pace Malylipnl8eniws.LLC. Pegs 11 0127 PO Box 228 • Stetesvllle, NC 28687 • 704/872/4697 Page 21 Qf 37 aceAnapical• — „w.we.h4naprl gUAIITY CONTROL DATA Paso Anablleal fiaMeos, LLC 9800lancey Ave. SuilelUO Rudenville, NC 26078 (7041875-9092 Protect: Lc —_ Pace Profecl No.: 92463883 EpA 82600 526288 Analysis Malhod: QC Batch: Analysis Description: 82800 MSV TCLP QC Balch Method: EPA 82800 Associated Lob SemPlae: 92403883001 McMz:. Water METHOD BLANK: 2WI866 Associated Lab $amples: 92453883001 Blank Reporting Result Unist Analyzed Castigate Parameter Units U9A NO &0 02M4/2016:64 1,1-Dichlomethene ugIL NO 6.0 02114120 16:54 1,2-DlcMarcelheno UgIL NO 5.0 02M412016:54 1,4-Djohloommizene UgfL NO 10.0 0211020 16:54 2-Bujimme(MEK) UgIL NO 5.0 0211412016:54 Benzene uglL NO 5.0 02/14120 16:54 Carbon leUechlodde ugll NO 5.0 0211412D 16:54 Chlorobenzene UgIL NET 5.0 02/1412016:54 Chloroform 1L NO 5.0 02M412016:54 Totmchlotoethug ene ug)L NO 5.0 02/1412016:64 Trichloloalhene NO 5.0 WIND 18:54 ugfl- Vinyl chlalde % 103 70.530 02fW2056:64 1,2-Dlchloroelltene-d4 (S) % gg 70130 02/1412016:54 4-Bromo9aorobenzene(S) % 105 67135 0211412016:54 Toluene-d8(S) LABORATORY CONTROL SAMPLE: 2807055 Spike LCS LCS %Rea Parameter Units Cane. Result %Rao Limits Qualifiers Ugh 50 59,8 118 70-130 1,1-Dlcietorcelhene n. 50 $0.6 lot 70-T70.130 1,2-Dlchlohmmane UgfL 476 95 BeIA30 Ug4 50 1,4-Dichtorobanzene 100 113 119 84-136. 2-eutanone(MEK) UgIL 55.0 TV 70.530 50 109 Benzene °Bg- 647 70.100 uglL 50 gg 10-130 Carbon tetrachloride ugh 50 49.4 Chlorobanzeng dust. 60 57.3 115 70.190 Chloroform 60 48.9 98 69A30 TatrachloroeU)L 60 thene Uq537 107 10,130 0- bg 68.9 134 70.131 L1 Trlchloroethene ugh Vbylc Irde % g7 10.13o 1,2-DlchloroelharmA4 (S) Y 100 07A36 4•BromuOuorobenzone(S) % 100 87.135 Tolusno-d8(3) 2507858 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2807857 MS MSO MSD MS MSD %Rec 92463993001 Spike Spike MS Parameter Unite Result Cane, Cone. Result Result %Rec Ye Roe Limits RPD Cued �— ugh NO 400 400 536 537 134 134 70-154 0 1,1-Dichloroerhena Recoils pros Pines on this page are In the Vion redlaeUd by REPORT wlumneaceptwhne an arterials unit is PTO aenhtlto the IIpM of Ihs IeNI. REPORT OF LA130RATORY ANALYSIS This rePodaSell not be reproduced, except In lull page 12 of 21 Dale: 021241202005:00 PM wkhma the written corsair of Pecs Marylkal servicos,LLD. PO Box 228 •Statesville, NC 28687 • 704/872/4697 Page 22 D137 Pace Analytical SOMIC03L LLC 90o0Kerney Ave. Suite 100 Hunlersvllle, NC 26078 aceftlytical • p941eTasoa2 y reJelr.rM QUALITY CONTROL DATA Project LC Pecs project No.: 92463083 2807858 MATRIX SPIKE 6 MATRIX SPIKE DUPLICATE: 2801857 MS MSD 92463993001 Spike Spike MS MSD MS MSD % Roe %ftec Limits RPD Quel Parameter Units Result Conc. Conn. Result Result %Rec 1,2•Dichleroelhene uglL ND 400 400 448 452 112 f99 70.133 1 1,4.Dlchlorobeozens ug8. ND 400 400 406 39B 121 99 60.139 2 2-Butanone(MEK) ugf. ND 800 000 969 913 121 116 60-161 6 Benzene ug1L ND 400 400 464 465 116 116 70.151 0 Carbon lelrechlodde ugll. ND 400 400 452 456 113 114 70-143 1 Carbon snzehl ug8. ND 400 400 429 423 107 1% 10-138 1 uglL ND 400 400 494 470 123 117 70-139 5 Chlorolorm NO 400 400 494 470 98 103 59-143 5 Tetrachloroelhena ugIL ND 400 400 448 447 112 112 ]0 147 0 Trichloroslhene uB�LL ND 400 400 660 649 140 137 70-166 2 Vinyl chloride 9 96 99 70-130 1,2•01chlomelhane-d4(S) % 105 102 70,130 4-DromoOuorobenzene(S) % 10f 100 67-135 Toluene-d8(8) a..ml. P e ,m.a an me pa4.,r. m m. emi. mmcnea by u,o °untie• emomnexc.plwnve an num,l. anti 1. pncmleatom. naht m rm,e,ml. REPORT OF LABORATORY ANALYSIS This repen dull not be repreanced. except In full. page 13 of 27 Date: 021241202005:09 PM without the wntlen consent of Pace Analytical Services,LLC. PO Box 228 •Statesville, NC 28687 • 704/872/4697 Pege 23 of 37 aceAnalytical ( I xw.pacdes7.9e12 QUALITY CONTROL DATA Pro)bcl; LC pace Project No.: 92463863 QC Balch: 625242 Analysts Method: EPA 6061E Analysts Description: 8081 TCLP Pesticides RV QC Batch Method; EPA3510C Associated Lab Samples: 92463883001 METHOD BLANK: 2806013 Matrix: Water Associated Lab Samples: 92463883001 Blank Reporting Parameter Units Result Limit Analyzed QualiOers ug1L NO 3.D 0211512010:55 Chkadzno(Technical) uglL Np 0.50 02115t2010:55 Enddn U91L NO 0.50 02/15/20 10:66 gamma-SHC (Undone)U91L NO 0.50 021151'10 V155 Heptachlor lL NO O.SD 0211512010:65 Hug eplachlor epoxide U91L NO 1000 02/15/2010;65 Mathoxyug1L NO 3.0 02M5120 10:55 Toxaphene % 59 ioA36 02/15120 10:55 Decachll(S) % 61 10-110 02115120 10:55 7etrachlor0rom-m.xyle-xylene (S) Pace Malyucal SeMces, I,LC 9e00 KlnceyAve. 6011e too Huntersullle, NC 28078 (704)075-9002 1ABORATORY CONTROLSAMPLE: 2007438 Spike LC9 LGS Ye Rac Parameter Units Cone. Result ARec LiIn Quallfers ug/L 1.2 0.89 66 2D-134 Enddn 2 0.74 60 20-110 gamma -RHO (Undone) �a2 1 1 2 016 60 20-142 Heptachlor U91L 12 0.76 61 22.133 Heptachiids uglL 3.6 2 5J OB 44.150 MalhoxychI0T hlor % 60 10.138 Decochicroblphenyl(S) % 81 10-110 Tahachlorem.xylens (8) 2867440 MATRIX SPIKE 6 MATRIX SPIKE DUPLICATE: 2RO7439 MS MSD 92463883001 Spike Spike MS MSD MS MSD %Rac Parameter Units Result Cone. Cane. Result Resell %Rae %Rao Limits RPD Qual Enddn ugA NO 1.2 �1.2 0.71 0.63 57 50 21-733 12 ugll NO 12 1.2 0,71 0.69 62 55 24-119 11 gamma-BHC (Undone) NO 1,2 1.2 0.71 0.67 6C 59 i6-12B 5 HeplaI uglL NO 12 12 075 0.66 60 53 50-160 13 Heplachlar opoxide ugIL 61 50-150 Melhoxychlor ug1L NO 3.6 3.8 2AJ 2.3J 03 46 42 10,138 pecachloroblphenN(5) % 56 55 10.110 Tstrachlar0-MI (S) % neemu p uemea oa Inls aeaa en m me amh mamma ay mrow.•.am•n e.aealwh..e.n di.ma. ami 1. a.•+•m.a m m. a9m mlm...mi. REPORT OF LABORATORY ANALYSIS This rayon shad nol be eeprodueed, amepl In lull. Page'14 0127 Date: 0212412D2005:09 PM without the Wron consent of Pace Analylieal SSNKa6, 1.1.0. p0 BOX 228 a Statesville, NC 28687 • 70A/872/4697 Page 24 of 37 �. ace Analytical .1seJsll.s4n ProJecl; LC Page Project No.: 924B3883 QC 0atch: 624373 qC Oatch Method: EPA3510C Associated Lab SOMP1e5: 92463883001 METHOD BLANK: 2803157 Associated Lab Samples: 92463883001 Parameter Units PCB -1016 (Arocbr 1016) CB-1221(Aredor 1221) PCB-1232 (Aroclor 1232) PCB4242 (Amolor 1242) PC8-1248 (ArOCIOr 1248) P08-1254(Amolor 1254) PCB.1260 (Avocior 1260) Decachlombiphenyl (8) troll. vgIL ug1L ug/L troll. uglL ug1L % gUA41TY GONTROL DATA Analysis Descrfpllan: BOB2 GCS PCB Maldx: Water Limit Blank Reg RasUll Limit Analyzetl Qualifiers NO 0.60 02112/2010:47 ND 0.50 02M212010:47 NO 0.50 021212016:47 NO 0,60 02112/2016:47 NO 0,60 021212016:47 NO 0.60 02/12020 10:47 ND 0,50 02112120 16:47 92 10430 021121201 .47 Face Ansly(TUISO C iLLC 9aDa wnauy Ave. aWle 100 Hunlersvllle, NO 25070 (704)675 9002 LABORATORY CONTROL SAMPLE: 2803158 Splke LCS LCS %Rec Perameter Units Came, Result %Rec Limits Qualifiers 2.7 54 41-130 PCB-1016 (Arodor 1015) u9IL 5 4.2 65 42.130 PCB-1260 (ArOCIOr 1260) ugll. 6 77 10.130 Oecachloroblphenyl(S) MATRIX SPIKE SAMPLE: 2803159 92464777001 Spike MS MS %Rec Parameter Units Result Cone. Result %Rae Limits Qualifiers No 5 2A 49 W30 PCB-1018 (AfeCIO11016) troll. PCB4260(Aroclor 1260) vi NO 6 4.0 80 10-130 % 02 0-130 Docadlloroblphenyl (3) SAMPLE DUPLICATE: 2803160 Parameter Face Ansly(TUISO C iLLC 9aDa wnauy Ave. aWle 100 Hunlersvllle, NO 25070 (704)675 9002 LABORATORY CONTROL SAMPLE: 2803158 Splke LCS LCS %Rec Perameter Units Came, Result %Rec Limits Qualifiers 2.7 54 41-130 PCB-1016 (Arodor 1015) u9IL 5 4.2 65 42.130 PCB-1260 (ArOCIOr 1260) ugll. 6 77 10.130 Oecachloroblphenyl(S) MATRIX SPIKE SAMPLE: 2803159 92464777001 Spike MS MS %Rec Parameter Units Result Cone. Result %Rae Limits Qualifiers No 5 2A 49 W30 PCB-1018 (AfeCIO11016) troll. PCB4260(Aroclor 1260) vi NO 6 4.0 80 10-130 % 02 0-130 Docadlloroblphenyl (3) SAMPLE DUPLICATE: 2803160 Parameter Units 9246429-0001 Resell Dup Rosull RPD QualiOars PC54016(Arodor 10164 UgIL NO NO ND PCSA221 (Aroclor 1221) troll. ND N N PCR,1232(Arodor 1232) coil. NO NO PCB.1242 (Arocior 1242) uglL NO N PCB-1248(Aracbr 1248) ug/L NDO NO PCS,1264(Arocbr 1254) uglL No ND PCB-1260(Amster 1260) uglL Decachlorobiphenyl(S) % 84 85 Rosvlln pie enle4 onlhn DeBe ere In the coil. rn4lcatea by Ue "UBII>"column exe<prwFere en eeemare uNlll plesemee to the sIBM of Inc swell. REPORT OF LABORATORY ANALYSIS TFle repod shall Mlle raproJucetl, exceplin Nll. pa 150f 7.7 Dab: 02124/202005:09 PM without the wriam consent 0(Pace Analyllcal serviseeI LlC. 9e PO BoX 228 • Statesvlll8, NC 28687 • 704/872/4697 Page 25 of 37 aceAnalytical• rw.vlaweteea QUALITY CONTROL DATA Pro)ecl: LC Pace Project No.: 92463883 OC Belch: 526243 Anelysls Method: EPA 8082A QC Batch Method: EPA3510C Analysis Description: 0002 TCLP PCB RV Associated Lob Samples: 92463883001 METHOD BLANK: 2800013 Matrix: Water Associated Lab Samples: 92463883001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB•1016 (AlOclar 1018) ugll- ND 1000 02/15/2015:03 1000 02116/20 15:03 PCB-1221 (Aroclor 1221) ugh. NO PC8-1232(Aroclor 1232) uglL NO 1000 02115Y2015:03 PCB•1242 (Aroclor 1242) US& NO 1000 02/1512016.03 PCB•124B(Aroclar 1248) ug0- NO 1000 02116/2015:03 PCB4264(Araclar 1264) ug/I. NO 1000 0211512016:03 PCB-1260(AfOctOr 1260) ug/L NO 1000 02JI6120 15:03 Dawchlorgbiphenyl(8) % 50 10.132 02/16/20 15:03 peas Analytical Sorylcas, LLC 90 in Kaxey Ave. suits 100 HunlersvNa, NC 28078 (704)875 9092 LABORATORY CONTROL SAMPLE: 2807441 Spike LCB LCB % ftec Parameter units Conc. Result %Rec Limits Qualifiers PCB-1016(Aroclor 1015) uglL 25 NO 66 38-t13 PCBA260 (ArOclol 12110) uglL 25 NO 48 35.120 Oacachloroblphenyl (Sj % 49 10-132 MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2807442 2807443 MS MSO 92463883001 Spike Spike MS MSD MS IVIED %Rec Parameter Units Result Cone. Conc, Result Result %Rec Y, Roo Limits RPD Qua, PCB-1016 (Aroclor 1016) u91L NO 25 25 NO NO 79 50 19-142 PCB-1260 (Aroclor 1260) ug1L NO 25 25 NO NO 60 4a 10-132 oocachloroblphenyl(8) % numl pyamaaa„mup=seen In m. umta memmasrma^wna^<•wmn.xuPiwmre+n nwaae aanuPraom.ela m, nem.nn.l..ap. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In lull. pale: 0212412020 OS:Og PM without Ne writlan cement of Pace Analytical 3awices, LLC. Page III g127 PO Box 228 •Statesville, NC 28687 • 704/872/A697 Page 26 0137 aceAnalytical • annrgtolnr.s4n QUALITY CONTROL DATA Protect: LC Pace Project No.: 92463883 OC Balch: 525179 Analysts Method: EPA 0270E OC Balch Method: EPA3510C Analysis DeswiplCHI: 9270E TCLP MSSV Associated Lab Samples; 924638830D1 METH00 BLANK: T806813 Maulx: Wafer Assoclelad Lob SemPIGS: 92463883001 Blank Reporting Parameter Units Result Limit Analyzed Du9118e7s i,4-Dlchlorobenzene UgIL NO 60.0 02/14/20 74:38 2145-TAc1110rophenal ugg- NO 50.0 02114/20 14:36 2,4,6.Tdchtorophonol UgIL NO 60.0 02114120 14:36 2,4-Dinthritoluens unit- NO 60.0 0211412014:36 2-Methylphre ol(o-Creaol) UgIL NO 60.0 02114/2014:36 384-Melhylphen0l(rn8p Cresol) ug/L NO 60.0 02114/20 14:36 Hexachloro-1,3•buladlene ug)L NO 60.0 02/14120 14:36 Haxachlorobenzena uglL NO 50-0 07/14/20 14:36 Hexechloroathane uglL NO 50.0 02114120 14:36 Nitrobenzene uglL NO 50.0 0211412014:30 Penlachlorophenol ugA. NO 100 02/14120 14:36 Pyridlee UgIL NO 50.0 02114/2014:36 2,4,6-Trlbromaphen0l(S) % 68 27AD0 02/14/20 %36 2•Fluarablphenyl(S) % 48 13.707 02M412014:36 2-Fluamphenal(5) % 25 10.11g 02M412614`:36 Nillobanzene-tl5 (S) % 51 12.102 02114120 14:36 Phen0bd6(S) % 16 10AID 02M412014:36 Terphanyl-d74(8) % 104. 21.132 02M4120 74:36 LABORATORY CONTROL SAMPLE: 2607146 Parameter tA-Dlchlorobanzene 2.4,6Tdchl0rophend 2,4,6•Tdchlor0phenol 2,4-Dinurololuenu 2.Malhylpherol(u-Cresol) 384-Melhl4phenol(m6p Cresol) Hexachloro-1,3-buladlene HexachlDrebenZane Hexechlorcelhene Nitrobenzene Penlachlomphenal Pydalne 2,4,6•TrlbmmoPhDno4 (S) 2•Fluorobiphenyl(S) 2•Fluorophenol(8) Nilrobenzeoe-tl6(S) Phenobd6(8) Terphanyl-dt4(3) Repulls q,erennd on lhn pepo pre lnlM unite lndlcalee by lM1e "Unga"column evca0l wha,p an dlamela volt is lne r4eull. pnppnlee la lM1e �IpM1l pr Units Pace Anaboopl scorlces, LLC BBODKincey Ave. Suite 1a0 HunleravilOp NC 28018 (704)876.9092 % Rec LMils OUaliOars ug/L UgIL atilt- uti1L atilt UgIL UgIL UgIL UgIL ug/L atilt. ug1L % % Spike Conc, LCS Result LCS %Rea _ 500 205 41 Boo 212 04 600 266 63 600 50(1 100 500 173 35 500 158 32 500 192 38 Soo 465 93 Soo 196 39 Soo 241 48 1000 1020 102 600 116 24 719 46 26 50 17 105 REPORT OF LABORATORY ANALYSIS This report snail nut he mprotluced eawpl In Nll. Date: 02/24/2020 05:09 PM wilhatt Me mitten consent of Pace Analyeral services.LLC. 10.110 39.108 40.104 0.2.109 31.7f0 30.110 0.110 39.121 0.110 32-101 8-108 0 110 2r-t08 so 3-t07 0-11D 2-102 a-110 21-t32 Pe90 17 0127 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 27 of 37 aceAnalytical• lrxw.)ttthht.epa QUALITY CONTROL DATA Protect; LC Pace Project No.: 92463083 QC Batch: 526621 Analysis Mel hod: EPA 1010A QC 6alch Method: EPA1010A Analysis Description: 1010 Plash Paint, Closed Cup Associated Lab SamPle6: 92463083001 SAMPLE DUPLICATE: 2809465 Parameter Units Flashpoinl deg F Result 01 Result Rasull Resell RPD QUO Were >200 >200 Peca Anahllcal arm so LLC 99001(Incey Ave. 6U11e 100 Hunlcrsvlge, Nc U078 (704197&9092 RvwlltP rtnlvtl an lM ie inlhe Unlle MtlletUa bYlnv UNIe"column tavtPtwM,e to ellnrnvly p,dlly pre.enled to lM ne for lM1e reaull. t p.eva REPORT OF LABORATORY ANALYSIS ims repodsnan nUl fie repro6acea, oetPpun nm. Date: 021241262005:09 PM v411wut the vailten consl al Pece Analytical SPrviwe.LLC. Page 1 a c127 PO Box 228 •Statesville, NC 28687 • 704/872/4697 Page 28 of 37 MAnalyticai• vw.parellNxan QUALITY CONTROL DATA Paee analytical 6mvlces, LLo 9000 Kincey Ave. guile 100 Humelselle, NO 20070 /7041070 9092 Project: LG Pace Project No.: 92463D03 —� QC Batch: 525376 Analysis Method: EPA9045D QC Balch Melhod: EPA9045D Analysis Description: gD45 PH Associated Lab Samples: 9Z163603001 SAMPLE DUPLICATE: 2808235 92465153001 Dup Parameter Units Result Result RPD Qualinera pH e125 Degrees G Sid, Units 0.8 6.9 1 H3 SAMPLE DUPLICATE: 2808236 82d63701010 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Sid. Units 5A 6.0 1 H3 Rve Ile preeenletl on mh peps are In Invanee indlulee ay Ina"Untie" eoNmn exeeplwM1ore en ellernele un1l le vreeenlee Io Ina .lent of me residr, REPORT OF LABORATORY ANALYSIS This ropad wall nal ea reprotluceQ except in lull, p0 e19 of 27 Date: 021241202005:09 PM wrnou thewrilloncunsoreol Pace Analytical6ervlcesI LLC. 9 PO 8Dx 228 •Statesville, NC 28687 • 704/872/4697 Page 29 of 37 IAnialyticarce Nxx.)lcllllv.cxe Prolem LC Pace Project No.: 92463883 QC Balch: 625378 QC Batch Methe0: EPA0095B Associated Lab Samples: 92463883001 QUALITY CONTROL DATA Malysis Description: 9085 PAINT FILTER LIQUID TEST SAMPLE DUPLICATE: 2000241 92403877001 Dup Parameter Units Result Result RPD Queli ers Free Liquids Fell Fall pace AnalyllCxl SoNICes, LLC 4800KIncey Ave. Suite tO0 Hunletsvllle, NC 20078 17041875-9092 Recalls prevenNtl on Nn papa are to the unite Intllrelea by IM1a"Unlit" column eeecptwM1ara en atunele unit if preelnlea to IM1r rlehl al IM1e result. REPORT OF LABORATORY ANALYSIS This report shall nolbe reprotlucM, except In Ir10, Date: 02124/202005:00 PM v4thout the rvriuen ronaenf of Pars Analytical Services. LLC. Pape 20 0127 p0 Box 228 •Statesville, NG 28687. 7OA/872/4697 Page 30 0137 ace Analytical" tll M QUALITY CONTROL DATA Pro)acl: LC Pace Project Ni 92463833 WC Batch: 382926 Analysis Malhod: EPA9014 QC Batch Method: SW-8487-3.3.2 Analysis Description: 733C Reactive Cyanide Associated Lob Samples: 92463883001 METHOD BLANK: 1856706 Mabin; Solid Associated! Lob Samples: 92463883001 Blank Rep0ning Parameter Units Result LTmil Analyzed Qualifiers Cyanide, RaecBve mglkg ND 1.0 02111/20 17:11 Pace AnelyBcal sawkes, LLC 9800 Klncey Ave. Suite lea Humersville. NO 2W78 (704)975.9092 lAeORATORV CONTROL SAMPLE: Parameter 1$56797 Units Spike LCS LCS Conn. Result %Roc %Roc Limits Qualifiers Cyanlda, Reactive mglk9 [ODNO 0 0.8 SAMPLE OUPLICATE: 1858957 Parameter Units 30349063001 OUP Result Result RPO .Qualifiers Cyanide, Reactive m91](1) NO NO aasuln PreeenNd an Ilile Peee are In the prJla lndlpelea by IFe "Unite" cplmm� escePlwhem an slNmels poll le plesenlea to IM ripN al IFe reaull. REPORT OF LABORATORY ANALYSIS Tms reppn sM1011 not be reproduced, axoopl In lull, Oata: 021241202006700 PM wki Na written consent of Paco Analytical 6ervlces,LLC. Page 21 0127 PO Box 228 a Statesville, NC 28687 e 700./872/4697 Page 31 0(37 aceMalytical• npwee.epm QUALfTY CONTROL DATA Pro(ed: LC Pace Pmject No.: 92463883 OC Batch: 3B2925 Analysts Mothed: SM 4500S2F-2011 QC Dutch Method; SW-840 7.3.4.2 Analysis Description: 734S Reactive Sulfide Associated Lab Samples: 02463883001 METHOD BLANK: 1855792 Matrix: Solid Associated Lab Samples: 02463883001 Blank Reporting. Parameter Units Result Limit Analyzed Qualifiers Sulfide, Reactive mglkg ND 10.0 02y1072018:57 PaaO Analnlcal service:, LLC eea0 Klncey Ave. Suite led Runtersvuie. NC 28078 (704)876.9092 LADORATORV CONTROL SAMPLE: 7865793 Spike LCS LCS %Rec Parameter Units Cone. Result %Rea Limits Qualifiers Sulfide, Reactive mgikg 200 36.0 18 0.52 SAMPLE DUPLICATE: 1856951 30348053001 Dup Parameter Units Result Result RPD Qualifiers sulfide. Reactive mglkg NO No Paauaa praeanntl on INa Papa Grain IM voila Inalealea OY lee "unite' eolumn saeprwMre en elnrnaN volt la proxMea to Ina rIBM of IM1e result. REPORT OF LABORATORY ANALYSIS This report snail not be reproduce:, except in full, Date: 021241202005:09 PM whiroi4tbe written consent orvace Analylicalserv¢eeI LLC, Page 22 0127 PO Box 228 •Statesville, NC 28687. 704/872/4697 Page 32 of 37 Pace A nali?Mal 50Nices, LLC 9Baekincey Ave. Suite too ace Analytical " 28078 (104)0759092 c92 vw,rpardab[.[an QUALIFIERS Pralecb LC Pace Project No.: 92453883 OEFINITION3 DF - Dilution Factor, It reposed, reprosems the factor applied to the reported data due to dilution of the sample aliquot. NO - Not Detected at or above adjusted reporting limit. TNTC -Tao Numerous To Count J - Estimated conconlralion above the adjusted method detection limit and below the adjusted reporting limit. MOL- Adjusted Method Detection Limit. PQL - Practical Quantitalion Limit. Ra ioing Li anal Thlowest e a specific mmrlxon value that meats project requirements for quantitative data with known precision and bias sp ecific y e S-Surrogate 1,2-Dlphenylhydrozlne decomposes to and cannot be separated f[om Azabenzene using Method 8270. The result for each acolyte is combined concentration. Consistent with EPAguldetines, unrounded data are displayed and have been used to calculate % recovery and RPO values. LCS(D) - Laboratory Conlml Semple (Duplicate) MS(D) - Matrix Splice (Duplicate) OUP - SamPle DUPilcate RPD - Relative Percent Difference NC - Not Calculable. SG, Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroelhylvinyl ether. A separate vial Preserved to a PH of 4-5 Is recommended In SW846 Chapter for the analysis of Acrolein end Acrylonliale by EPA Method 8260. Neenecombinedcopo !l lion.mcannot be separated from Olphenylamine using Method 8270. The result reported to each r Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analyles, TNI - The NELAC Institute. LABORATORIES pAN Pece Analytical National PAST -A PecriAnolylical Services -Asheville PAST-C PaceAnalylical Services - Charlotte PASI-PA Pace Analytical Services - Greensburg ANALYTE QUALIFIERS 1g Sample bailed over at 200F H3 Sample was received at, analysis requested beyond the recognized method holding lime. L1 Anelyle recovery in the laboratory control sample (LCS) Was above QC limits. Results lorlhls anaiyla In associated samples may be closed high. pled based on laboratory Contra[ sample ILCS ) recovery. MI Matrix spike recoveryexceeded OC limits. perch acts so Surrogate recavery outside laboratory control limits. REPORT DF LABORATORY ANALYSIS rnia r°Pon anon col 5s reweauseo, exnePt In rmt Date: 021241202005:00 PM witaca[he writien consent of Pace A CSY1 al SaMceS.LLC. Page 23 of 27 PO Box 228 •Statesville, NC 28687 • 704/872/4697 Page 33 of 37 aceAnalyticai• ( wvtrdleuan QUALITY CONTROL DATA CROSS REFERENCE TABLE Protect: LC Pace Project No.: 92463003 Lab ID Sample lD 92463883001 200204,49,01 LC, 92463883001 200204,49,01 LC, 92463083001 200204.49.01 LC. 92463BO3001 200204,49,01 LC. 82463883001 200204.48.01 LC, 92463883001 200204.49,01 I.C. 92463883001 200204.49.01 LC, 82463883001 200204,49.01 LC. 92403883001 200204.49.01 LC, 92403883001 200204.49.01 LC, 92463883001 200204,49,01 LC. 92463883001 200204.49.01 I.C. 924038830D1 200204.49,01 LC, Oale: 0212412020 05:09 PM pace AnalyllCal Satvlces, LLC 9800 aiuey AvO. Suite IN IWnlersvllle. NC 28WO (700075.9092 CC Batch Method QC Balch Analytical Method Analyllcal Batch 8161A 1426755 EPA0151A 1426765 EPA3510C 526242 EPA80818 525346 EPA3510C 524373 EPA8082A 524604 EPA 351DC 626243 EPA8082A 526347 EPA 3010A 525225 EPA60100 525233 EPA 7470A 525226 EPA7470A 625474 EPA 3510C 526179 EPA 8270E 525364 EPA 82601:11 525208 EPq 1010A 826621 EPA 9046D 525376 EPA9095B 525378 SW8467.3.3.2 382926 EPA9014 383218 SW-8467.3A.2 382925 SM 4500S2F.2011 383217 REPORT OF LABORATORY ANALYSIS This repa6 snail apt ee lepmducetl, except In lull. wilnW I Ins w411en consent cl Pdce AnalyUcatOervices,LLO. page 24 0127 PO 80x 228 •Statesville, NC 28687 • 704/872/4697 Page 34 of 37 L€10 99 060d L69V/ZL8/VOL • L898Z A `allhsaje38 . 8ZZ x09 Od �Y' t4. U t-. z § r s t A � N eta l It i gg 9f 't�+�-��� � �5 �v8 � '. i4. �ri.�tf as�� 3 qfx •� a>r k�,-:-'may. VI Ir f y EG 'y1 a In it �e ,a (�C F a % $ 6°Yd h CD - am ua--- ' L£ lO 9£ 060d L69b/ZL91VOL a L899Z JN 'apJASale1S 0 SZZ X08 Od /,Z IB az e6ed Laboratory receiving samples: Asheville ❑ fden0 Greenwood ❑ Huntersvllle Holelghu MechenlcBvllle� 3 Client Name: ,a prp)Bcl Wl �`�•' • 9246388 PKI TIH• Rut, D►t►t 02/19/20 Causles; F,Id E. pUPS USPs Cnp^r CUENTI 92wStst►►vst [ICommercial a a,,,/y/ Other:_ / Custody Seal Prasen[7 QYes kyPlo Seals lnlacli ,[..]LY/as n(r7/ 0ale(minaIs PeNan examinees Con Packing Materiel: [Bubble Wrap []Bubble gags 6NO,a Olhel Blolagltal Thsue [AOlen7 Qyes [No 91A Thermometer: �����������yy Type Of Ice: Wel ❑Blue I]None 13IAsnnlD;-92Taaaa— CaoineTempi'C)1 I�' Correction Factor: Add/Subtract IT) O.O•C Tempi uld be above Creating to 64C Cookie Tlmp COIIltUd l'qr ll.� amples out at lamp uInfla. Samples on lee, cooling placili hasbegun _ USDA_ftegulaled 4oII IQ N/A, witerlamplel — —'--' DM I it I I quaranllne ron0 wllFln lheUnlled SUler CP NV aISC ltheeNmaps)1 IlldudIag Htarlgm° °�lnleamsionany,^— fimp e Indu►n Nmal and Pu¢rlo 0.k0)7 ❑Yet QNo Yes No comments aucre an¢ Chain of Cuslod Present Y s No N/A Sam lea Anthers within Hold Time? ON NA Short Hold Here Anal sit477 LOT,)? Yn INNp E3% Rush Turn Around Time Be 'nettedi ❑Np Sufficient Vplumai Y No N/A Correct Containers Used? ❑No ❑N/A 6. .Pace Containers Used? y NoN A Containel Wait? yes L3no Z 7. Dissolved irsaisis: Samref field Fillemdi Sample labels Match COCI Yes [4]Yes n4 No N/A ❑w/A B. 9. SQjl',?1 15 �^���.stnq on coe .Includes Date/lime/lD/Anal fls Matrla: flea she ace in VOA ViaisaS,6mm7 No A 10, Trip Blank Present? ❑Yo ONo U. Trip Blankfurtod Seals Present? No /A fpMMFNTd/dPMPIE DISCREPANCY ?told Pala R<ealcedl VY¢s WNo �— lot 10 of spilt containers: CIIENT NOTIFICATION/RESOSUTION Person contacted: DAIe/Time: Project Menagar SCURF Review: Date: Project Manegor SRF Review; r Dow , .— LC 10 LC aged L69b/ZL8iv0L a L898Z :)N 'allIASOJOIS a SZZ X08 dd LZ to LZ eaud DOcument Name: Da[umenl Ppvlsed: Febluaty ], ]O1B cpAna JCAI Sample Condition U ne Recolot(SCURI Pate ]of F Document No.: lasulmr Authority: F•CAgdS6D33•acyas Pace Oasalinas Quality Office 'Check mark tap hall of boX If pH end/or dechlorinatlon Is verlfled and within the acceptance range for preservation samples. Eacrmuow VOAj Calllorm, TOC, oil and Greater 000/80151Waled DDC, LLNa e•nottom half of bog Is to list number of bottle Protect N w0# a 924658$3 TDu• D�lol 92/19/20 PM, IN C41ENT1 92-SRdovll ago on ISO a Is M so 14 on aon ■ 8 on ai pH Adjustment Log for Preserved Sample: Sample lD Type of Ple[trVellve PN UPan fetelpl Bala Pieaervallpn adlufled Tlma praaprveilon atlhntd Amaunl alPrnefvaltve added leltl Nate: Whenever there If a tllsct¢pancy ane[Ilna Nalmcafpxna comDllanae fampias, a aavv e, urn m„v •„n Dul of hold, incorrect prasarvnave, out olkmp, rmarretl <anNlnera. ointV® W��-ANALYTICAL 6/19/2020 Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC, 28fi69 Ref: Analytical Testing Report Number: 20-164-0005 Project Description: Lincoln Co 7621 Whitepine Road, Richmond, VA 23237 Mafn 804-743-9401 °Fax 804-271-6446 www.way po i nta Holy ti ca I.co m Dear Dennis Key: Waypoint Analytical Virginia, Inc. received samples) on 6112I2020 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method. Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, P� ray Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 7 �n 7621 Whitepine Road, Richmond, VA 23237 Waypoi■ ■�. MaIn 804-743-9401°Pax 804-271-6446 ANALYTICAL www.waypolntanalytical.com Sample Summary Table Report Number: 20-164-0005 Client Project Description: Lincoln Co Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 SM-4600-NH3C WP MTN 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 9046D WP MTN 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 4500NO3F-2011 WP MTN 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 6010D WP MTN 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 SW-7471B WP MTN 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 SM-4500-NH3C-TKN WP MTN 72625 Lincoln Co Solids 06/10/2020 12:30 06/12/2020 SM-2540G WP MTN WP MTN -Memphis, TN: Waypoint Analytical -TN, Memphis, TN Page 2 of 7 ffrr�� �i�iT 7621 Whitepine Road, Richmond, VA 23237 WaypOl ■ ■ fir. Main 804-743-9401 °Fax 804-271-6446 ANALYTICAL www.waypointanalyHcal.com 46381 Southern Soil Builders Project Lincoln Co Report Date : 06/19/2020 Dennis Key Received : 06/12/2020 958 Hoots Road Information Roaring River , NC 28669 P��o m` GPe"'� Pauric McGroary Report Number :20-164-0005 REPORT OFANALYSIS Agronomist Matrix: Solids Lab No : 72625 Sampled: 6/10/202012:30 Sample ID :Lincoln Co Results Units MQL DF Date /Time By Analytical Test Analyzed Method Moisture 97.4 � 0.010 1 06/17/2017:27 ADM SM-2540G Results Units MDL DF Date I Time By Analytical Test Analyzed Me[hod ( 33000 mg/Kg-dry 962 1 06/19/2011:30 JP] SM-4500-NH3C Ammonia Nitrogen Nitrate+Nitrite-N 229 mg/Kg-dry 185 1 06/18/2015:47 2BD 4500NO3F-2011 Organic N 57700 mg/Kg-dry 9620 1 06/19/2010:00 CALCULATION 7 3 s u. 1 06/1$/20 06:05 JSL 9045D pH % 0.010 1 06/17/20 17:27 ADM SM-2540G Total Solids 2.61 Total Kjeldahl Nitrogen BB500 mg/Kg -dry 9620 1 06/19/20 10:00 ]P] iM-4500-NH3C TKP Phosphorus 20900 mg/Kg -dry 192 1 06/17/20 17:50 T]S 6010D Aluminum 10600 mg/Kg -dry 192 1 06/17/20 17:50 T]S 6010D Arsenic <19.2 mg/Kg -dry 19.2 1 06/17/20 17:50 TJS 6010D Calcium 13700 mg/Kg -dry 1920 1 O6/17/20 17:50 TJS 6010D Cadmium <3.85 mg/Kg -dry 3.85 1 06/17/20 17;50 T]S 6010D Chromium 24.1 mg/Kg -dry 9.62 1 06/18/20 22:29 JIR 6010D Copper 286 mg/Kg -dry 19.2 1 06/18/20 22:29 ]TR 6010D Iron 16100 mg/Kg -dry 385 1 06/17/20 17:50 T]S 6010D Lead 14.4 mg/Kg -dry 11.5 1 06/17/20 17:50 TJS 6010D Magnesium 3550 mg/Kg -dry 192 1 06/17/20 17:50 Tl5 6010D Manganese 442 mg/Kg -dry 19.2 1 06/18/20 22:29 JTR 6030D L Limit Exceeded Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 3 of 7 Waypoint. ANALYTICAL 46381 Southern Soil Builders Project Lincoln Co Dennis Key 958 Hoots Road Informa0on Roaring River , NC 28669 Report Number :20-164-0005 Lab No: 72625 Sample ID :Lincoln Co Test Mercury Molybdenum Nickel Potassium Selenium Sodium Zinc Sulfur 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypo i n to n a lyfi cal.com REPORT OFANALYSIS Results Uniis MOL Report Date: 06/19/2020 Received : 06/12/2020 P m` ��"� Pauric McGroary Agronomist Matrix: Solids Sampled: 6/ SO/2020 12:30 DF Date/Time ey Analytical Analyzed Method 1.03 mg/Kg -dry 0.592 1 06/18/20 11:57 DDB SW-74718 10.8 mg)Kg -dry 9.62 1 06/17/20 17:50 T]S 6010D 46.5 mg/Kg -dry 9.62 1 06/17/20 17:50 T]S 6010D 5080 mg/Kg -dry 385 1 06/17/20 17:50 TJS 6010D <19.2 mg/Kg -dry 19.2 1 06/17/20 i7:50 Tl5 6010D 36300 mg/Kg -dry 962 1 06/17/20 17:50 TJS 6010D 727 mg/Kg -dry 48.1 1 06/17/20 17:50 TJS 6010D 9920 mg/Kg -dry 385 I 06/17/20 17:50 T]5 6010D Qualifiers) DF Dilution Factor Definitions MQL Method Quantitation Limit L Limit Exceeded Page 4 of 7 Wa oint�® Y-ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.way p o i nta n a lyti ca l.com Client: Southern Soil Builders CASE NARRATIVE Project: Lincoln Co Lab Report Number: 20-164-0005 Date: 6/19l2020 Metals Analysis Method 6010D Sample 72652 Analyte: Aluminum QC Batch No: L497167 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Calcium QC Batch No: L497167 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Analyte: Iron QC Batch No: L497236 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Potassium QC Batch No: L497167 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Sulfur QC Batch No: L497167 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 7 Waypoint ANALYTICAL 7621 Whltepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypotnta na lytical.com Shipment Receipt Form Customer Number:46381 Customer Name: Southern Soil Builders Report Number: 20-164-0005 Shipping Method Fed Ex � US Postal !� Lab � Other (� UPS � Client [� Courier Thermometer ID: Shipping container/cooler uncompromised? � Yes !� No Number of coolers/boxes received Custody seals intact on shipping container/cooler? (� Yes � No � Not Present Custody seals intact on sample battles? Q Yes (� No � Not Present Chain of Custody (COC) present? � Yes (� No COC agrees with sample label(s)? � Yes (� No COC properly completed � Yes � No Samples in proper containers? � Yes (� No Sample containers intact? � Yes � No Sufficient sample volume for indicated test(s)? � Yes � No All samples received within holding time? � Yes (� No Cooler temperature in compliance? !� Yes � No CoolerfSamples arrived at the laboratory on ice. � Yes � No Samples were considered acceptable as cooling process had begun. Water -Sample containers properly preserved � Yes � No � N/A Water -VOA vials free of headspace !� Yes � No � N/A Trip Blanks received with VOAs � Yes � No � N/A Soil VOA method 5035 —compliance criteria met � Yes (� No � N/A High concentration container (48 hr) � Low concentration Encore samplers (48 hr) � High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? � Yes � No Comments: Signature: Brandi Watson Date &Time: 8/12/2020 12:07:04 Page 6 of 7 \\ , < g 00 as_\ \ \)\ uj 5 a ®a = ) \ / o \ / e = ! 7! §" ® § G# §k! !©! co ) a_ / 0 ) § ; �( a » / / {) � ° r �� .5) ) �! / / ) 2£ �]@ • - -- �\/ \ \\ / aa\ e 0.9 !g — o ) z m t \ \ / _ e / ) u ; - }ED M \ k u \ } paa / < cri) to c ) f - Z ca \ ) )ti e - «\ «! 77 j/1lu L) ƒ!S � Analytical Results Southern Soil Builders 958 Hoots Road 40 Roaring River, NC 28669 Receive Date: 02/04/2020 Reported: 02/05/2020 For: Lincoln County Comments: Geometric Mean: 317,638 MPN/g Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 20020448-01 Fecal Coliforms 1 >642570 MPN/g SM92210E-2006 02/04/2020 WC 200204-48-01 Percent Solids 1 2.49 % SM2640B-2011 02104/2020 WC 200204.4M2 Fecal Coliforms 2 209205 MPN/g SMN210E-2006 02104/2020 WC 200204-48-02 Percent Solids 2 2,39 / SM25408-2011 02/04/2020 WC 200204.48-03 Fecal Coliforms 3 214592 MPN/g SM92210E-2006 02104/2020 WC 200204-48-03 Percent Solids 3 2,33 % SM254OB-2011 02/04/2020 WC 200204-48-04 Fecal Coliforms 4 394737 MPN/g sm"21cE-2006 02/04/2020 WC 200204-48-04 Percent Solids 4 2.28 % SM25400-2011 02/04/2020 WC 200204-48-05 Fecal Coliforms 5 355731 MPN/g SM92210E.2096 02/04/2020 WC 200204-48-06 Percent Solids 5 2.53 / SM26406.2011 02/0412020 WC 200204-48-06 Fecal Coliforms 6 218341 MPN/g SM92210E-2006 02104/2020 WC 200204-48-06 Percent Solids 6 2.29 /a SM26400-2011 02104/2020 WC 200204-48-07 Fecal Coliforms 7 368852 MPN/g SM9221cE-2006 02104/2020 WC 200204-48.07 Percent Solids 7 2.44 % SM25408-2011 02/04/2020 WC Respectfully submitted, tlw '/(A..11)7 �(a. Dena Myers NC Cert #440, NCDW Cart #37755, EPA #NC00909 PO Box 228 •Statesville, NC 28687 • 704/872/4697 Pege 1 ot4 Condition of Receipt Sample Number 200204-48-01 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfale Received on Ice Sample Number 200204-48-02 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfale Received on Ice Sample Number 200204-48-03 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 20020448-04 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received an Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200204-48.05 Temp on Arrival: 3.2 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfale Received on Ice Sample Number 200204-48-06 Temp on Arrival: 3.2 PO Box 228 •Statesville, NC 28687 • 704/872/4697 Page 2 o14 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 200204-48-07 Temp on Arrival; 3.2 Paramoter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice PO Box 228 •Statesville, NC 28687 • 704/872/4697 Page 3 of 4 m ,9BEd 69t7/ZLf?/VU ,L89r ON 'DIIIASOIRIS . m XOS a - ))§);}re / �AL\ - ®°#° ) - ¥ \ C. 2 { \ ) w } } As ! ! } !lz /G I I `|®�» ( k ■ ( ! ** � ,z»mow \ / ƒ ƒ / #; ! # M6� E E k E a fr;0 « a j j\ ) / \ ) a w ;e 7 431 f : c w 0 / ! J 2 j{J 0 f } } R } / / / PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS SM 2540 B-2011 B_A x I,000,000 = mglL TSS C B_D x 11000,000 = mg/L VSS V3S x 100= %VSS C TSS (550°C) \ REPC/)tTED BY: IGNITIONmg/I. i. ais4 DA E ANA YSTI SAMPLE ml Used PAN N TARE WT. DRY WT TSS Rpp'�'sso 4°6 VSS"1.0% REPORTED BY: (550°C) DATE ANALYST SAMPLE ml Used PAN q TARE PVT. DRY WT TSS m (550°C) IGNITION WT. (g) VSS mglL REPORTED BY: (550°C) IGNITION WT. (g) VSS mg/L REPORTED BY: (550°C) IGNITION WT. (g) VSS mg/L REPORTED BY: x` > O Y o � a O n o = U a n N E o _ = an o z 9 k a IL JNi vv�� O V N c m for f N N 9 7 K� N L d xc _ cr .. .. G x .3 10 0LI a 1. G w O =if tool O v m o C = _ 4 .. O ry .. ll 1p • W Z `" E o a a p y H m m u q m m u O m ) L{ u Efj ,pQs •CL o WZ ` o o t r N = W �A O s u W .a + o °C o z E i � v W v 0 G W a D ca c U � f`f @ C. J i IJ- m yl I: is 10 Z c E a }E'- v v c � `o v eu `� o w y. 4 ( % Volatile Solids (Am C) x 100 = 3.88 A _ B 0,0487 WAS Tare Wt. ( B) 1.2655 Dry Wt. (A) 1.3142 Ignition WT. (C) 1.2754 %Volatile Solids A - B 0.2317 SHT Tare Wt. (B) 1.2542 Dry Wt. (A) 1.4859 Ignition WT. (C) 1.3886 Volatile Solids Reduction ( (in -out) x 100 = 37.7 in - (in x out) 0.46 79.1 % 42.0 SL5