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HomeMy WebLinkAboutNCG030027_DMR_20200213 F , N• Scott K. Bailey Plant Director (336) 503-6536 (phone) (336) 503-6562 (fax) scottkbaileyeaton.com R , D February 24, 2020 MtA o$0.0Z0 CENT L FILES Division of Water Quality D1�VR SEC10N 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attn: DWQ Central Files RE: February 2020 Monthly Tier III Discharge Monitoring Report Attached are the analytical results and associated chain of custody for the February 13, 2020 monthly Tier Ill stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility. Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North Carolina Division of Water Quality (NCDWQ). I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with the system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or other persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Sincerely, Scott K. Bailey Plant Director Attachments Stormwater Discharge Monitoring Report for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000 Date submitted 02/24/2020 CERTIFICATE OF COVERAGE NO. NCGO3 0 0 2 7 SAMPLE COLLECTION YEAR 2020 FACILITY NAME Eaton Corporation SAMPLE PERIOD 0 Jan-June 0 July-Dec COUNTY Person County or ® Monthly' (month) PERSON COLLECTING SAMPLES Colin Betchan DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout _PNA LABORATORY Pace National Lab Cert.# ENV375/DW21704/BI0041 ❑Zero-flow ❑Water Supply nSA Comments on sample collection or analysis: *Other ws-ill;NSW `�' %C I ,1 D PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Part A: Stormwater Benchmarks and Monitoring Results MAR 0 3 2020 i RAL- - No discharge this period?2 :WR Ste' + , Non-Polar O&G/ Date Sample 24-hour rainfall pH, Total Toxic Outfall No. Collected) amount, Total Suspended Solids Standard units Total Copper Total Lead Total Zinc Total Petroleum Organics (mo/dd/yr) Inches3 Hydrocarbons Benchmarks - - 100 mg/L or 50 mg/L4 6.0—9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141 Pond (001) 02/13/2020 0.60 12.3 6.0 0.00700 0.00200 0.0711 0.906 0.03410 Tool Room Trench(005) 02/13/2020 0.60 13.2 6.0 0.00700 0.00200 0.0237 0.873 0.03325 1 Monthly sampling(instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here. 'The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit,Section B,Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies. 'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals,or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11;for semiconductor manufacture use the definition as found in 40 CFR 469.12;for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver,the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Scott K. Bailey Name(Print name) Plant Director Title(Prin itle) LA AA,L- Signature Date Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL,<PQL, Non-detect, ND, or other similar non-numerical format. When results are below the applicable limits,they must be reported in the format, "<XX mg/L",where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month. No discharge this period?2 Outfall No. Date Sample Collected' 24-hour rainfall amount, New Motor Oil or Non-Polar O&G/Total Total Suspended (mo/dd/yr) Inches' Hydraulic Oil Usage Petroleum Hydrocarbons Solids Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4 Parameter Code - 46529 NCOIL 00552 C0530 Footnotes from Part A also apply to Part B Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 2 of 3 FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES El NO E IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO E REGIONAL OFFICE CONTACT NAME: Danny Smith Mail an original copy of this DMR, including all"No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period in the case of"No Discharge"reports)to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate, and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." "O? Signature of Permittee Date Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018 Page 3 of 3 aceAnalytical® A \ A L Y T I C A L R S O R T , National Center for Testing&Innovation February 20, 2 02 0 p I 2 Tc 3Ss Eaton Corporation 4 Sample Delivery Group: L1189390 Cn Samples Received: 02/14/2020 5Sr Project Number: 28091-R 6 Description: Eaton Corp Monthly Stormwater Qc Site: ROXBORO, NC 7 GI Report To: Dustin LaClair 2564 Durham Road &Al Roxboro, NC 27573 9 Sc Entire Report Reviewed By: Heather J Wagner .,. Project Manager Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the information provided, and as the samples are received. r c't 'r,i a y xr x i s e 4 u a ^tv "� ^fie 4 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 14:13 1 of 28 imummimmiummmommilmommumummommoimmie TABLE OF CONTENTS ONE LAB.NATIONWIDE. iik Cp:Cover Page 1 1 Cp Tc:Table of Contents 2 Ss:Sample Summary 3 Tc Cn:Case Narrative 4 3 Sr:Sample Results 5 Ss 2020-02-13-001 L1189390-01 5 4 Cn 2020-02-13-005 L1189390-02 9 Oc:Quality Control Summary 12 5Sr Gravimetric Analysis by Method 2540 D-2011 12 6 Wet Chemistry by Method 1664B 13 Qc Metals(ICP)by Method 200.7 14 7 GI Volatile Organic Compounds(GC/MS)by Method 624.1 15 Pesticides(GC)by Method EPA 608.3 18 JAI Polychlorinated Biphenyls(GC)by Method EPA-608.3 20 y Semi Volatile Organic Compounds (GC/MS)by Method 625.1 21 Sc GI:Glossary of Terms 26 AI:Accreditations& Locations 27 Sc: Sample Chain of Custody 28 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 2 of 28 SAMPLE SUMMARY ONE LAB.NATIONWIDE. AO Collected by Collected date/time Received date/time 2020-02-13-001 L1189390-01 WW 02/13/2009:52 02/14/2008:45 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time 2 �� Tc Gravimetric Analysis by Method 2540 D-2011 � WG1428711 1 02/15/20 22:57 02/16/20 00:55 TH Mt.Juliet,TN Wet Chemistry by Method 1664B WG1430093 1 02/18/20 08:42 02/18/20 22:07 MBP Mt.Juliet,TN 3 Metals(ICP)by Method 200.7 WG1428157 1 02/15/2011:24 02/16/2013:49 CCE Mt.Juliet,TN Ss Volatile Organic Compounds(GC/MS)by Method 624.1 WG1428464 1 02/15/2013:41 02/15/2013:41 ADM Mt.Juliet,TN Volatile Organic Compounds(GC/MS)by Method 624.1 WG1428553 1 02/15/2015:28 02/15/2015:28 BMB Mt.Juliet,TN ° Cn Pesticides(GC)by Method EPA 608.3 WG1428898 1 02/16/2016:38 02/18/20 20:08 HMH Mt.Juliet,TN Polychlorinated Biphenyls(GC)by Method EPA-608.3 WG1428898 1 02/16/2016:38 02/17/2010:11 SSH Mt.Juliet,TN s Semi Volatile Organic Compounds (GC/MS)by Method 625.1 WG1429926 1 02/19/20 15:05 02/19/20 23:34 AO Mt.Juliet,TN Sr 6 Collected by Collected date/time Received date/time QC 2020-02-13-005 L1189390-02 WW 02/13/2009:34 02/14/20 08:45 7 Method Batch Dilution Preparation Analysis Analyst Location GI dateRime date/time Gravimetric Analysis by Method 2540 D-2011 WG1428711 1 02/15/20 22:57 02/16/20 00:55 TH Mt.Juliet,TN -AI Wet Chemistry by Method 1664E WG1430093 1 02/18/20 08:42 02/18/20 22:07 MBP Mt.Juliet,TN Metals(ICP)by Method 200.7 WG1428157 1 02/15/2011:24 02/16/20 13:52 CCE Mt.Juliet,TN Volatile Organic Compounds(GC/MS)by Method 624.1 WG1428464 1 02/15/2014:01 02/15/2014:01 ADM Mt.Juliet,TN SC Pesticides(GC)by Method EPA 608.3 WG1428898 1 02/16/2016:38 02/18/20 20:21 HMH Mt.Juliet,TN Polychlorinated Biphenyls(GC)by Method EPA-608.3 WG1428898 1 02/16/2016:38 02/17/2010:25 SSH Mt.Juliet,TN Semi Volatile Organic Compounds(GC/MS)by Method 625.1 WG1429926 1 02/19/2015:05 02/19/20 23:54 AO Mt.Juliet,TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 3 of 28 CASE NARRATIVE ONE LAB.NATIONWIDE. AA Cp All sample aliquots were received at the correct temperature,in the proper containers,with the appropriate preservatives,and within method specified holding times,unless qualified or notated within the report. Where applicable,all MDL(LOD)and RDL(LOQ)values reported for environmental samples Tc have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative,a non-conformance form 3 or properly qualified within the sample results.By my digital signature below, I affirm to the best of my Ss knowledge,all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory,and no information or data have been knowingly withheld that would affect the quality of the data. Cn 5 Sr Qc GI Heather J Wagner Project Manager Al Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 4 of 28 2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. Si Collected date/time: 02/13/20 09:52 L1189390 Additional Information , Result Units Cp Analyte 2 pH(On Site) 6 su Tc Temperature(on-site) 12.1 Deg C 3 Ss Gravimetric Analysis by Method 2540 D-2011 Result Qualifier MDL RDL Dilution Analysis Batch 4 Analyte mg/I mg/I mg/I date/time Cn Suspended Solids 12.3 0.368 2.63 1 02/16/2020 00:55 WG1428711 Sr Wet Chemistry by Method 1664E 6 Result Qualifier MDL RDL Dilution Analysis Batch Qc Analyte mg/I mg/I mg/I date/time TPH-Oil&Grease U 0.906 6.25 1 02/18/2020 22:07 WG1430093 7GI Metals (ICP) by Method 200.7 C Result Qualifier MDL RDL Dilution Analysis Batch Al Analyte mg/I mg/I mg/I date/time 9 Copper U 0.00700 0.0100 1 02/16/202013:49 WG1428157 SC Lead U 0.00200 0.00500 1 02/16/202013:49 WG1428157 Zinc 0.0711 0.00340 0.0500 1 02/16/202013:49 WG1428157 Volatile Organic Compounds (GC/MS) by Method 624.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/ mg/I mg/I date/time Acrolein U 0.00887 0.0500 1 02/15/2020 13:41 WG1428464 Acrylonitrile U 0.00187 0.0100 1 02/15/2020 13:41 WG1428464 Benzene U 0.000331 0.00100 1 02/15/2020 13:41 WG1428464 Bromodichloromethane U 0.000380 0.00100 1 02/15/202013:41 WG1428464 Bromoform U 0.000469 0.00100 1 02/15/202013:41 WG1428464 Bromomethane U 0.000866 0.00500 1 02/15/202013:41 WG1428464 Carbon tetrachloride U 0.000379 0.00100 1 02/15/202013:41 WG1428464 Chlorobenzene U 0.000348 0.00100 1 02/15/202013:41 WG1428464 Chlorodibromomethane U 0.000327 0.00100 1 02/15/202013:41 WG1428464 Chloroethane U 0.000453 0.00500 1 02/15/202013:41 WG1428464 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 02/15/202013:41 WG1428464 Chloroform U 0.000324 0.00500 1 02/15/202013:41 WG1428464 Chloromethane U 0.000276 0.00250 1 02/15/202013:41 WG1428464 1,2-Dichlorobenzene U 0.000349 0.00100 1 02/15/202013:41 WG1428464 1,3-Dichlorobenzene U 0.000220 0.00100 1 02/15/202013:41 WG1428464 1,4-Dichlorobenzene U 0.000274 0.00100 1 02/15/202013:41 WG1428464 Dichlorodifluoromethane U 0.000551 0.00500 1 02/15/202013:41 WG1428464 1,1-Dichloroethane U 0.000259 0.00100 1 02/15/202013:41 WG1428464 1,2-Dichloroethane U 0.000361 0.00100 1 02/15/202013:41 WG1428464 1,1-Dichloroethene U 0.000398 0.00100 1 02/15/202013:41 WG1428464 trans-1,2-Dichloroethene U 0.000396 0.00100 1 02/15/202013:41 WG1428464 1,2-Dichloropropane U 0.000306 0.00100 1 02/15/202013:41 WG1428464 cis-1,3-Dichloropropene U 0.000418 0.00100 1 02/15/202013:41 WG1428464 trans-1,3-Dichloropropene U 0.000419 0.00100 1 02/15/202013:41 WG1428464 Ethylbenzene U 0.000384 0.00100 1 02/15/202013:41 WG1428464 Methylene Chloride U 0.00100 0.00500 1 02/15/202013:41 WG1428464 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 02/15/202013:41 WG1428464 Tetrachloroethene 0.000648 J 0.000372 0.00100 1 02/15/202015:28 WG1428553 Toluene U 0.000412 0.00100 1 02/15/202013:41 WG1428464 1,1,1-Trichloroethane U 0.000319 0.00100 1 02/15/202013:41 WG1428464 1,1,2-Trichloroethane U 0.000383 0.00100 1 02/15/202013:41 WG1428464 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 5 of 28 2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. * Collected date/time: 02/13/20 09:52 L1189390 Volatile Organic Compounds(GC/MS) by Method 624.1 , Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/I mg/I mg/I date/time Trichlaroethene U 0.000398 0.00100 1 02/15/2020 13:41 WG1428464 z Tc Trichlorofuoromethane U 0.00120 0.00500 1 02/15/2020 13:41 WG1428464 Vinyl chloride U 0.000259 0.00100 1 02/15/2020 13:41 WG1428464 3 (S)Toluene-d8 103 80.0-120 02/15/2020 13:41 WG1428464 Ss (S)Toluene-d8 109 80.0-120 02/15/202015:28 WG1428553 (S 4-Bromofluorobenzene 99.3 80.0-120 02/15/2020 13:41 WG1428464 4 Cn (S 4-Bromofluorobenzene 88.5 80.0-120 02/15/2020 15:28 WG1428553 (S)1,2-Dichloroethane-d4 99.3 70.0-130 02/15/202013:41 WG1428464 (S)1,2-Dichloroethane-d4 102 70.0-130 02/15/202015:28 WG1428553 Sr Pesticides (GC) by Method EPA 608.3 60c Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 7G1 Aldrin U 0.00000813 0.0000500 1 02/18/2020 20:08 WG1428898 Alpha BHC U 0.0000166 0.0000500 1 02/18/2020 20:08 WG1428898 c Beta BHC U 0.0000184 0.0000500 1 02/18/2020 20:08 WG1428898 Al Delta BHC U 0.0000197 0.0000500 1 02/18/2020 20:08 WG1428898 Gamma BHC U 0.0000176 0.0000500 1 02/18/2020 20:08 WG1428898 9SC Chlordane U 0.0000977 0.000500 1 02/18/2020 20:08 WG1428898 4,4-DDD U 0.0000170 0.0000500 1 02/18/2020 20:08 WG1428898 4,4-DDE U 0.0000164 0.0000500 1 02/18/2020 20:08 WG1428898 4,4-DDT U 0.0000177 0.0000500 1 02/18/2020 20:08 WG1428898 Dieldrin U 0.00000751 0.0000500 1 02/18/2020 20:08 WG1428898 Endosulfan I U 0.0000179 0.0000500 1 02/18/2020 20:08 WG1428898 Endosulfan II U 0.0000176 0.0000500 1 02/18/2020 20:08 WG1428898 Endosulfan sulfate U 0.0000196 0.0000500 1 02/18/2020 20:08 WG1428898 Endrin U 0.0000189 0.0000500 1 02/18/2020 20:08 WG1428898 Endrin aldehyde U 0.0000142 0.0000500 1 02/18/2020 20:08 WG1428898 Endrin ketone U 0.0000170 0.0000500 1 02/18/2020 20:08 WG1428898 Heptachlor U 0.0000108 0.0000500 1 02/18/2020 20:08 WG1428898 Heptachlor epoxide U 0.0000175 0.0000500 1 02/18/2020 20:08 WG1428898 Hexachlorobenzene U 0.0000134 0.0000500 1 02/18/2020 20:08 WG1428898 Methoxychlor U 0.0000193 0.0000500 1 02/18/2020 20:08 WG1428898 Toxaphene U 0.000168 0.000500 1 02/18/2020 20:08 WG1428898 (S Decachlorobipheny/ 107 10.0-144 02/18/2020 20:08 WG1428898 (S)Tetrachloro-m-xylene 87.2 10.0-135 02/18/2020 20:08 WG1428898 Polychlorinated Biphenyls (GC) by Method EPA-608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time PCB 1016 U 0.000100 0.000500 1 02/17/2020 10:11 WG1428898 PCB 1221 U 0.0000730 0.000500 1 02/17/202010:11 WG1428898 PCB 1232 U 0.0000420 0.000500 1 02/17/2020 10:11 WG1428898 PCB 1242 U 0.0000470 0.000500 1 02/17/2020 10:11 WG1428898 PCB 1248 U 0.0000860 0.000500 1 02/17/2020 10:11 WG1428898 PCB 1254 U 0.0000470 0.000500 1 02/17/2020 10:11 WG1428898 PCB 1260 U 0.000120 0.000500 1 02/17/2020 10:11 WG1428898 (S)Decachlorobiphenyl 103 10.0-144 02/17/2020 10:11 WG1428898 (S Tetrachloro-m-xylene 98.1 10.0-135 02/17/2020 10:11 WG1428898 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 6 of 28 imimmimmummummeimmommillmmmimmil 2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. .t Collected date/time: 02/13/20 09:52 L1189390 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 , Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/I mg/I mg/I date/time Acenaphthene U 0.000316 0.00100 1 02/19/2020 23:34 WG1429926 2TC Acenaphthylene U 0.000309 0.00100 1 02/19/2020 23:34 WG1429926 Anthracene U 0.000291 0.00100 1 02/19/2020 23:34 WG1429926 3 Benzidine U 0.00432 0.0100 1 02/19/2020 23:34 WG1429926 Ss Benzo(a)anthracene U 0.0000975 0.00100 1 02/19/2020 23:34 WG1429926 Benzo(b)fluoranthene U 0.0000896 0.00100 1 02/19/2020 23:34 WG1429926 4 Cn Benzo(k)fluoranthene U 0.000355 0.00100 1 02/19/2020 23:34 WG1429926 Benzo(g,h,i)perylene U 0.000161 0.00100 1 02/19/2020 23:34 WG1429926 Benzo(a)pyrene U 0.000340 0.00100 1 02/19/2020 23:34 WG1429926 SI Bis(2-chlorethoxy)methane U 0.000329 0.0100 1 02/19/2020 23:34 WG1429926 Bis(2-chloroethyl)ether U 0.00162 0.0100 1 02/19/2020 23:34 WG1429926 6 Oc 2,2-Oxybis(1-Chloropropane) U 0.000445 0.0100 1 02/19/2020 23:34 WG1429926 4-Bromophenyl-phenylether U 0.000335 0.0100 1 02/19/2020 23:34 WG1429926 7 2-Chloronaphthalene U 0.000330 0.00100 1 02/19/2020 23:34 WG1429926 GI 4-Chlorophenyl-phenylether U 0.000303 0.0100 1 02/19/2020 23:34 WG1429926 Chrysene U 0.000332 0.00100 1 02/19/2020 23:34 WG1429926 s Al Dibenz(a,h)anthracene U 0.000279 0.00100 1 02/19/2020 23:34 WG1429926 3,3-Dichlorobenzidine U 0.00202 0.0100 1 02/19/2020 23:34 WG1429926 2,4-Dinitrotoluene U 0.00165 0.0100 1 02/19/2020 23:34 WG1429926 SC 2,6-Dinitrotoluene U 0.000279 0.0100 1 02/19/2020 23:34 WG1429926 1,2-Diphenylhydrazine U 0.000318 0.0100 1 02/19/2020 23:34 WG1429926 Fluoranthene U 0.000310 0.00100 1 02/19/2020 23:34 WG1429926 Fluorene U 0.000323 0.00100 1 02/19/2020 23:34 WG1429926 Hexachlorobenzene U 0.000341 0.00100 1 02/19/2020 23:34 WG1429926 Hexachloro-1,3-butadiene U 0.000329 0.0100 1 02/19/2020 23:34 WG1429926 Hexachlorocyclopentadiene U 0.00233 0.0100 1 02/19/2020 23:34 WG1429926 Hexachloroethane U 0.000365 0.0100 1 02/19/2020 23:34 WG1429926 , Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 02/19/2020 23:34 WG1429926 Isophorone U 0.000272 0.0100 1 02/19/2020 23:34 WG1429926 Naphthalene U 0.000372 0.00100 1 02/19/2020 23:34 WG1429926 Nitrobenzene U 0.000367 0.0100 1 02/19/2020 23:34 WG1429926 n-Nitrosodimethylamine U 0.00126 0.0100 1 02/19/2020 23:34 WG1429926 n-Nitrosodiphenylamine U 0.00119 0.0100 1 02/19/2020 23:34 WG1429926 n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 02/19/2020 23:34 WG1429926 Phenanthrene U 0.000366 0.00100 1 02/19/2020 23:34 WG1429926 Benzylbutyl phthalate U 0.000275 0.00300 1 02/19/2020 23:34 WG1429926 Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 1 02/19/2020 23:34 WG1429926 Di-n-butyl phthalate 0.000360 J 0.000266 0.00300 1 02/19/2020 23:34 WG1429926 Diethyl phthalate U 0.000282 0.00300 1 02/19/2020 23:34 WG1429926 Dimethyl phthalate U 0.000283 0.00300 1 02/19/2020 23:34 WG1429926 Di-n-octyl phthalate U 0.000278 0.00300 1 02/19/2020 23:34 WG1429926 Pyrene U 0.000330 0.00100 1 02/19/2020 23:34 WG1429926 1,2,4-Trichlorobenzene U 0.000355 0.0100 1 02/19/2020 23:34 WG1429926 4-Chloro-3-methylphenol U 0.000263 0.0100 1 02/19/2020 23:34 WG1429926 2-Chlorophenol U 0.000283 0.0100 1 02/19/2020 23:34 WG1429926 2,4-Dichlorophenol U 0.000284 0.0100 1 02/19/2020 23:34 WG1429926 2,4-Dimethylphenol U 0.000624 0.0100 1 02/19/2020 23:34 WG1429926 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 02/19/2020 23:34 WG1429926 2,4-Dinitrophenol U 0.00325 0.0100 1 02/19/2020 23:34 WG1429926 2-Nitrophenol U 0.000320 0.0100 1 02/19/2020 23:34 WG1429926 4-Nitrophenol U 0.00201 0.0100 1 02/19/2020 23:34 WG1429926 Pentachlorophenol U 0.000313 0.0100 1 02/19/2020 23:34 WG1429926 Phenol 0.00199 J 0.000334 0.0100 1 02/19/2020 23:34 WG1429926 2,4,6-Trichlorophenol U 0.000297 0.0100 1 02/19/2020 23:34 WG1429926 (5)2-Fluoropheno/ 38.6 10.0-120 02/19/2020 23:34 WG1429926 (S)Phenol-d5 27.3 8.00-424 02/19/2020 23:34 WG1429926 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 7 of 28 2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. 10 Collected date/time: 02/13/20 09:52 L1189390 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/I mg/I mg/I date/time (S Nitrobenzene-d5 61.9 15.0-314 02/19/2020 23:34 WG1429926 2 Tc (S 2-Fluorobiphenyl 72.7 22.0-127 02/19/2020 23:34 WG1429926 (S)2,4,6-Tribromophenol 89.0 10.0-153 02/19/2020 23:34 WG1429926 3 (S)p-Terphenyl-d14 83.4 29.0-141 02/19/2020 23:34 WG1429926 SS 4 Cn Si 6 Qc 7 GI 8 Al 5 Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 8 of 28 o 2020-02-13-005 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE. 10 Collected date/time: 02/13/20 09:34 L1189390 Additional Information , Result Units Cp Analyte 2 pH(On Site) 6 su Tc Temperature(on-site) 12.5 Deg C 3 Ss Gravimetric Analysis by Method 2540 D-2011 Result Qualifier MDL RDL Dilution Analysis Batch 4 Analyte mg/I mg/I mg/I date/time Cn Suspended Solids 13.2 0.350 2.50 1 02/16/2020 00:55 WG1428711 SL Wet Chemistry by Method 1664B 6 Result Qualifier MDL RDL Dilution Analysis Batch Qc Analyte mg/I mg/I mg/I date/time TPH-Oil&Grease U 0.873 6.02 1 02/18/2020 22:07 WG1430093 7 GI Metals(ICP) by Method 200.7 8 Result Qualifier MDL RDL Dilution Analysis Batch Al Analyte mg/I mg/I mg/I date/time 5 Copper U 0.00700 0.0100 1 02/16/2020 13:52 WG1428157 SC Lead U 0.00200 0.00500 1 02/16/2020 13:52 WG1428157 Zinc 0.0237 J 0.00340 0.0500 1 02/16/2020 13:52 WG1428157 Volatile Organic Compounds (GC/MS) by Method 624.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Acrolein U 0.00887 0.0500 1 02/15/2020 14:01 WG1428464 Acrylonitrile U 0.00187 0.0100 1 02/15/2020 14:01 WG1428464 Benzene U 0.000331 0.00100 1 02/15/2020 14:01 WG1428464 Bromodichloromethane U 0.000380 0.00100 1 02/15/2020 14:01 WG1428464 Bromoform U 0.000469 0.00100 1 02/15/2020 14:01 WG1428464 Bromomethane U 0.000866 0.00500 1 02/15/202014:01 WG1428464 Carbon tetrachloride U 0.000379 0.00100 1 02/15/202014:01 WG1428464 Chlorobenzene U 0.000348 0.00100 1 02/15/2020 14:01 WG1428464 Chlorodibromomethane U 0.000327 0.00100 1 02/15/202014:01 WG1428464 Chloroethane U 0.000453 0.00500 1 02/15/202014:01 WG1428464 2-Chloroethyl vinyl ether U 0.00301 0.0500 1 02/15/202014:01 WG1428464 Chloroform U 0.000324 0.00500 1 02/15/202014:01 WG1428464 Chloromethane U 0.000276 0.00250 1 02/15/202014:01 WG1428464 1,2-Dichlorobenzene U 0.000349 0.00100 1 02/15/2020 14:01 WG1428464 1,3-Dichlorobenzene U 0.000220 0.00100 1 02/15/2020 14:01 WG1428464 1,4-Dichlorobenzene U 0.000274 0.00100 1 02/15/2020 14:01 WG1428464 Dichlorodifluoromethane U 0.000551 0.00500 1 02/15/2020 14:01 WG1428464 1,1-Dichloroethane U 0.000259 0.00100 1 02/15/2020 14:01 WG1428464 1,2-Dichloroethane U 0.000361 0.00100 1 02/15/2020 14:01 WG1428464 1,1-Dichloroethene U 0.000398 0.00100 1 02/15/2020 14:01 WG1428464 trans-1,2-Dichloroethene U 0.000396 0.00100 1 02/15/2020 14:01 WG1428464 1,2-Dichloropropane U 0.000306 0.00100 1 02/15/2020 14:01 WG1428464 cis-1,3-Dichloropropene U 0.000418 0.00100 1 02/15/2020 14:01 WG1428464 trans-1,3-Dichloropropene U 0.000419 0.00100 1 02/15/2020 14:01 WG1428464 Ethylbenzene U 0.000384 0.00100 1 02/15/2020 14:01 WG1428464 Methylene Chloride U 0.00100 0.00500 1 02/15/2020 14:01 WG1428464 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 02/15/2020 14:01 WG1428464 Tetrachloroethene U J4 0.000372 0.00100 1 02/15/2020 14:01 WG1428464 Toluene U 0.000412 0.00100 1 02/15/202014:01 WG1428464 1,1,1-Trichloroethane U 0.000319 0.00100 1 02/15/202014:01 WG1428464 1,1,2-Trichloroethane U 0.000383 0.00100 1 02/15/202014:01 WG1428464 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 9 of 28 2020-02-13-005 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE. I. Collected date/time: 02/13/20 09:34 L1189390 Volatile Organic Compounds (GC/MS) by Method 624.1 , Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/I mg/I mg/I date/time Trichloroethene U 0.000398 0.00100 1 02/15/2020 14:01 WG1428464 2Tc Trichlorofluoromethane U 0.00120 0.00500 1 02/15/2020 14:01 WG1428464 Vinyl chloride U 0.000259 0.00100 1 02/15/2020 14:01 WG1428464 3 (S)Toluene-d8 103 80.0-120 02/15/202014:01 WG1428464 Ss (S)4-Bromofluorobenzene 101 80.0-120 02/15/2020 14:01 WG1428464 (S)1,2-Dichloroethane-d4 100 70.0-130 02/15/2020 14:01 WG1428464 4 Cn Pesticides (GC) by Method EPA 608.3 St Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 6 Aldrin U 0.00000813 0.0000500 1 02/18/2020 20:21 WG1428898 QC Alpha BHC U 0.0000166 0.0000500 1 02/18/2020 20:21 WG1428898 Beta BHC U 0.0000184 0.0000500 1 02/18/2020 20:21 WG1428898 7G1 Delta BHC U 0.0000197 0.0000500 1 02/18/2020 20:21 WG1428898 Gamma BHC U 0.0000176 0.0000500 1 02/18/2020 20:21 WG1428898 Chlordane U 0.0000977 0.000500 1 02/18/2020 20:21 WG1428898 Al 4,4-DDD U 0.0000170 0.0000500 1 02/18/2020 20:21 WG1428898 4,4-DDE U 0.0000164 0.0000500 1 02/18/2020 20:21 WG1428898 9SC 4,4-DDT U 0.0000177 0.0000500 1 02/18/2020 20:21 WG1428898 Dieldrin U 0.00000751 0.0000500 1 02/18/2020 20:21 WG1428898 Endosulfan I U 0.0000179 0.0000500 1 02/18/2020 20:21 WG1428898 Endosulfan II U 0.0000176 0.0000500 1 02/18/2020 20:21 WG1428898 Endosulfan sulfate U 0.0000196 0.0000500 1 02/18/2020 20:21 WG1428898 Endrin U 0.0000189 0.0000500 1 02/18/2020 20:21 WG1428898 Endrin aldehyde U 0.0000142 0.0000500 1 02/18/2020 20:21 WG1428898 Endrin ketone U 0.0000170 0.0000500 1 02/18/2020 20:21 WG1428898 Heptachlor U 0.0000108 0.0000500 1 02/18/2020 20:21 WG1428898 Heptachlor epoxide U 0.0000175 0.0000500 1 02/18/2020 20:21 WG1428898 Hexachlorobenzene U 0.0000134 0.0000500 1 02/18/2020 20:21 WG1428898 Methoxychlor U 0.0000193 0.0000500 1 02/18/2020 20:21 WG1428898 Toxaphene U 0.000168 0.000500 1 02/18/2020 20:21 WG1428898 (S)Decachlorobiphenyl 108 10.0-144 02/18/2020 20:21 WG1428898 (S)Tetrachloro-m-xylene 79.5 10.0-135 02/18/2020 20:21 WG1428898 Polychlorinated Biphenyls (GC) by Method EPA-608.3 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time PCB 1016 U 0.000100 0.000500 1 02/17/2020 10:25 WG1428898 PCB 1221 U 0.0000730 0.000500 1 02/17/2020 10:25 WG1428898 PCB 1232 U 0.0000420 0.000500 1 02/17/2020 10:25 WG1428898 PCB 1242 U 0.0000470 0.000500 1 02/17/2020 10:25 WG1428898 PCB 1248 U 0.0000860 0.000500 1 02/17/2020 10:25 WG1428898 PCB 1254 U 0.0000470 0.000500 1 02/17/2020 10:25 WG1428898 PCB 1260 U 0.000120 0.000500 1 02/17/2020 10:25 WG1428898 (S)Decachlorobiphenyl 105 10.0-144 02/17/2020 10:25 WG1428898 (S)Tetrachloro-m-xylene 108 10.0-135 02/17/2020 10:25 WG1428898 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Acenaphthene U 0.000316 0.00100 1 02/19/2020 23:54 WG1429926 Acenaphthylene U 0.000309 0.00100 1 02/19/2020 23:54 WG1429926 Anthracene U 0.000291 0.00100 1 02/19/2020 23:54 WG1429926 8enzidine U 0.00432 0.0100 1 02/19/2020 23:54 WG1429926 Benzo(a)anthracene U 0.0000975 0.00100 1 02/19/2020 23:54 WG1429926 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 10 of 28 mnimmimimmmommmommmmimmmmmimimmmimmimsmmommsmu 2020-02-13-005 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE. .4111 Collected date/time: 02/13/20 09:34 L1189390 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/I mg/I mg/I date/time Benzo(b)fluoranthene U 0.0000896 0.00100 1 02/19/2020 23:54 WG1429926 z Tc Benzo(k)fluoranthene U 0.000355 0.00100 1 02/19/2020 23:54 WG1429926 Benzo(g,h,i)perylene U 0.000161 0.00100 1 02/19/2020 23:54 WG1429926 3 Benzo(a)pyrene U 0.000340 0.00100 1 02/19/2020 23:54 WG1429926 Ss Bis(2-chlorethoxy)methane U 0.000329 0.0100 1 02/19/2020 23:54 WG1429926 Bis(2-chloroethyl)ether U 0.00162 0.0100 1 02/19/2020 23:54 WG1429926 4 Cn 2,2-0xybis(1-Chloropropane) U 0.000445 0.0100 1 02/19/2020 23:54 WG1429926 4-Bromophenyl-phenylether U 0.000335 0.0100 1 02/19/2020 23:54 WG1429926 2-Chloronaphthalene U 0.000330 0.00100 1 02/19/2020 23:54 WG1429926 Si" 4-Chlorophenyl-phenylether U 0.000303 0.0100 1 02/19/2020 23:54 WG1429926 Chrysene U 0.000332 0.00100 1 02/19/2020 23:54 WG1429926 6 Oc Dibenz(a,h)anthracene U 0.000279 0.00100 1 02/19/2020 23:54 WG1429926 3,3-Dichlorobenzidine U 0.00202 0.0100 1 02/19/2020 23:54 WG1429926 7 2,4-Dinitrotoluene U 0.00165 0.0100 1 02/19/2020 23:54 WG1429926 GI 2,6-Dinitrotoluene U 0.000279 0.0100 1 02/19/2020 23:54 WG1429926 1,2-Diphenylhydrazine U 0.000318 0.0100 1 02/19/2020 23:54 WG1429926 &AI Fluoranthene U 0.000310 0.00100 1 02/19/2020 23:54 WG1429926 Fluorene U 0.000323 0.00100 1 02/19/2020 23:54 WG1429926 9 Hexachlorobenzene U 0.000341 0.00100 1 02/19/2020 23:54 WG1429926 SC Hexachloro-1,3-butadiene U 0.000329 0.0100 1 02/19/2020 23:54 WG1429926 Hexachlorocyclopentadiene U 0.00233 0.0100 1 02/19/2020 23:54 WG1429926 Hexachloroethane U 0.000365 0.0100 1 02/19/2020 23:54 WG1429926 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 02/19/2020 23:54 W61429926 Isophorone U 0.000272 0.0100 1 02/19/2020 23:54 WG1429926 Naphthalene U 0.000372 0.00100 1 02/19/2020 23:54 WG1429926 Nitrobenzene U 0.000367 0.0100 1 02/19/2020 23:54 WG1429926 n-Nitrosodimethylamine U 0.00126 0.0100 1 02/19/2020 23:54 WG1429926 n-Nitrosodiphenylamine U 0.00119 0.0100 1 02/19/2020 23:54 WG1429926 n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 02/19/2020 23:54 WG1429926 Phenanthrene U 0.000366 0.00100 1 02/19/2020 23:54 WG1429926 Benzylbutyl phthalate U 0.000275 0.00300 1 02/19/2020 23:54 WG1429926 Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 1 02/19/2020 23:54 WG1429926 Di-n-butyl phthalate 0.000461 J 0.000266 0.00300 1 02/19/2020 23:54 WG1429926 Diethyl phthalate U 0.000282 0.00300 1 02/19/2020 23:54 WG1429926 Dimethyl phthalate U 0.000283 0.00300 1 02/19/2020 23:54 WG1429926 Di-n-octyl phthalate U 0.000278 0.00300 1 02/19/2020 23:54 WG1429926 Pyrene U 0.000330 0.00100 1 02/19/2020 23:54 WG1429926 1,2,4-Trichlorobenzene U 0.000355 0.0100 1 02/19/2020 23:54 WG1429926 4-Chloro-3-methylphenol U 0.000263 0.0100 1 02/19/2020 23:54 WG1429926 2-Chlorophenol U 0.000283 0.0100 1 02/19/2020 23:54 WG1429926 2,4-Dichlorophenol U 0.000284 0.0100 1 02/19/2020 23:54 WG1429926 2,4-Dimethylphenol U 0.000624 0.0100 1 02/19/2020 23:54 WG1429926 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 02/19/2020 23:54 WG1429926 2,4-Dinitrophenol U 0.00325 0.0100 1 02/19/2020 23:54 WG1429926 2-Nitrophenol U 0.000320 0.0100 1 02/19/2020 23:54 WG1429926 4-Nitrophenol U 0.00201 0.0100 1 02/19/2020 23:54 WG1429926 Pentachlorophenol U 0.000313 0.0100 1 02/19/2020 23:54 WG1429926 Phenol 0.00122 J 0.000334 0.0100 1 02/19/2020 23:54 WG1429926 2,4,6-Trichlorophenol U 0.000297 0.0100 1 02/19/2020 23:54 W61429926 (S)2-Fluorophenol 34.1 10.0-120 02/19/2020 23:54 WG1429926 (S)Phenol-d5 24.7 8.00-424 02/19/2020 23:54 WG1429926 (S)Nitrobenzene-d5 58.9 15.0-314 02/19/2020 23:54 WG1429926 (S)2-Fluorobiphenyl 67.3 22.0-127 02/19/2020 23:54 WG1429926 (S)2,4,6-Tribromophenol 81.4 10.0-153 02/19/2020 23.54 WG1429926 (S)p-Terphenyl-d14 82.6 29.0-141 02/19/2020 23:54 WG1429926 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 11 of 28 WG1428711 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. sk Gravimetric Analysis by Method 2540 D-2011 U189390.01,02 Method Blank(MB) Cp R3500203-1 02/16/20 00:55 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc Suspended Solids U 0.350 2.50 'Ss L1189293-01 Original Sample(OS)•Duplicate(DUP) J (OS)L1189293-01 02/16/20 00:55-(DUP)R3500203-3 02/16/20 00:55 - Cn Original Result DUP Result Dilution DUP RPD DUP QualifierDUP RPD Limits Sr, Analyte mg/1 mg/1 % % Suspended Solids 97.6 94.4 1 3.33 5 6 Qc L1189350-01 Original Sample(OS)•Duplicate(DUP) 'GI (OS)L1189350-01 02/16/20 00:55•(DUP)R3500203-4 02/16/20 00:55 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD a Lim is Al Analyte mgA mg4 % % Suspended Solids 37.2 41.6 1 11.2 P1 5 `Sc Laboratory Control Sample(LCS) (LCS)R3500203-2 02/16/20 00:55 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg4 mg/1 % % Suspended Solids 773 816 106 85.0-115 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 14:13 12 of 28 WG1430093 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .10 Wet Chemistry by Method 16648 L1189390.01,02 Method Blank(MB) (MB)R3500945-1 02/18/20 22:07 'Cp MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mgA mgA Tc TPH-Oil&Grease U 0.725 5.00 113 Laboratory Control Sample(LCS)•Laboratory Control Sample Duplicate(LCSD) (LCS)R3500945.2 02/18/20 22:07.(LCSD)R3500945-3 02/18/20 22:07 Cn 1 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/I mgA mgA % % % % % ell TPH-Oil&Grease 20.0 18.0 17.7 90.0 88.5 64.0-132 1.68 34 12 III Al • el ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 1473 13 of 28 WG1428157 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. ik Metals(ICP)by Method 200.7 L118 9 3 90-0L02 Method Blank(MB) • (MB)R3500314-1 02/16/2013:14 Cp MB Result MB Qualifier MB MDL MB RDL Analyte mg/l mgA mgA •Tc Copper U 0.00700 0.0100 Lead U 0.00200 0.00500 3 SS Zinc U 0.00340 0.0500 4Cn Laboratory Control Sample(LCS) (LCS)R3500314-2 02/16/2013:17 ,Sr Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mgA mgA % % Copper 1.00 0.919 91.9 85.0-115 1111 Lead 1.00 0.930 93.0 85.0-115 7 Zinc 1.00 0.934 93.4 85.0-115 GI • L1189408-01 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) Al (OS)L1189408-01 02/16/2013:20•(MS)R3500314-4 02/16/20 13:25•(MSD)R3500314-5 02/16/20 13:28 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits SC Analyte mgA mgA mg/I mg/1 % % % % % Copper 1.00 ND 0.951 0.950 95.1 95.0 1 70.0-130 0.0250 20 Lead 1.00 ND 0.988 0.991 98.8 99.1 1 70.0-130 0.312 20 Zinc 1.00 ND 0.975 0.986 97.5 98.6 1 70.0-130 1.02 20 L1189615-02 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) (OS)L1189615-02 02/16/20 13:30•(MS)R3500314-6 02/16/20 13:33•(MSD)R3500314-7 02/16/20 13:35 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSO Qualifier RPD RPD Limits Analyte mgA mg/1 mg/1 mgA % % % % % Copper 1.00 0.0392 0.973 0.999 93.4 96.0 1 70.0-130 2.68 20 Lead 1.00 ND 0.976 1.07 97.4 100 1 70.0-130 3.07 20 Zinc 1.00 0.115 1.09 1.12 97.4 100 1 70.0-130 2.38 20 ACCOUNT: PROJECT: SDG: DATE/rIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 1413 14 of 28 WG1428464 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. JO Volatile Organic Compounds(GC/MS)by Method 624.1 L118 9 3 90-01,02 Method Blank(MB) (MB)R3500111-2 02/15/2011:19 Cp MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/I mg/I mg/I Tc Acrolein U 0.00887 0.0500 Acrylonitrile U 0.00187 0.0100 3SS Benzene U 0.000331 0.00100 Bromodlchloromethane U 0.000380 0.00100 4 Bromoform U 0.000469 0.00100 Cn Bromomethane U 0.000866 0.00500 Carbon tetrachloride U 0.000379 0.00100 5Sr Chlorobenzene U 0.000348 0.00100 Chlorodibromomethane U 0.000327 0.00100 Chloroethane U 0.000453 0.00500111 2-Chloroethyl vinyl ether U 0.00301 0.0500 Chloroform U 0.000324 0.00500 7Gl Chloromethane U 0.000276 0.00250 1,2-Dichlorobenzene U 0.000349 0.00100 3 1,3-Dichlorobenzene U 0.000220 0.00100 Al 1,4-Dichlorobenzene U 0.000274 0.00100 Dichlorodifluoromethane U 0.000551 0.00500 °SC 1,1-Dichloroethane U 0.000259 0.00100 1,2-Dichloroethane U 0.000361 0.00100 1,1-Dichloroethene U 0.000398 0.00100 trans-1,2-Dichloroethene U 0.000396 0.00100 1,2-Dichloropropane U 0.000306 0.00100 cis-1,3-Dichloropropene U 0.000418 0.00100 trans-1,3-Dichloropropene U 0.000419 0.00100 Ethylbenzene U 0.000384 0.00100 Methylene Chloride U 0.00100 0.00500 1,1,2,2-Tetrachloroethane U 0.000130 0.00100 Tetrachloroethene U 0.000372 0.00100 Toluene U 0.000412 0.00100 1,1,1-Trichloroethane U 0.000319 0.00100 1,1,2-Trichloroethane U 0.000383 0.00100 Trichloroethene U 0.000398 0.00100 Trichlorofluoromethane U 0.00120 0.00500 Vinyl chloride U 0.000259 0.00100 (S)Toluene-d8 104 80.0-120 (S)4-Bromofluorabenzene 98.6 80.0-120 (S)1,2-Dichloroethane-d4 96.4 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/201413 15 of 28 WG1428464 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE All Volatile Organic Compounds(GC/MS)by Method 624.1 L1189390-01,02 Laboratory Control Sample(LCS) (LCS)03500111-1 02/15/2010:17 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg/I mg/ % % TC Acroleln 0.0250 0.0198 79.2 60.0-140 Acrylonitrile 0.0250 0.0249 99.6 60.0-140 'SS Benzene 0.00500 0.00555 111 65.0-135 Bromodichloromethane 0.00500 0.00543 109 70.0-135 a Bromoform 0.00500 0.00556 111 70.0-130 Cn Bromomethane 0.00500 0.00530 106 15.0-185 Carbon tetrachloride 0.00500 0.00604 121 70.0-130 Sr Chlorobenzene 0.00500 0.00577 115 65.0-135 Chlorodibromomethane 0.00500 0.00535 107 70.0-135 ^Chloroethane 0.00500 0.00416 83.2 40.0-160 QC 2-Chloroethyl vinyl ether 0.0250 0.0262 105 0.100-225 Chloroform 0.00500 0.00608 122 70.0-135 7G' Chloromethane 0.00500 0.00446 89.2 0.100-205 1,2-Dichlorobenzene 0.00500 0.00571 114 65.0-135 8 1,3-Dichlorobenzene 0.00500 0.00556 111 70.0-130 Al 1,4-Dichlorobenzene 0.00500 0.00548 110 65.0-135 Dichlorodlfuoromethane 0.00500 0.00492 98.4 49.0-155 9SC Ll-Dichloroethane 0.00500 0.00524 105 70.0-130 1.2-Dichloroethane 0.00500 0.00525 105 70.0-130 1,1-Dichloroethene 0.00500 0.00621 124 50.0-150 trans-1,2-Dichloroethene 0.00500 0.00575 115 70.0-130 1,2-Dichloropropane 0.00500 0.00539 108 35.0-165 cis-1.3-Dichloropropene 0.00500 0.00548 110 25.0-175 trans-1,3-Dichloropropene 0.00500 0.00543 109 50.0-150 Ethylbenzene 0.00500 0.00583 117 60.0-140 Methylene Chloride 0.00500 0.00565 113 60.0-140 1,1,2.2-Tetrachloroethane 0.00500 0.00540 108 60.0-140 Tetrachloroethene 0.00500 0.00664 133 70.0-130 J4 Toluene 0.00500 0.00575 115 70.0-130 1,1,1-Trichloroethane 0.00500 0.00593 119 70.0-130 1,1,2-Trichloroethane 0.00500 0.00566 113 70.0-130 Trichloroethene 0.00500 0.00573 115 65.0-135 Trichlorofluoromethane 0.00500 0.00569 114 50.0-150 Vinyl chloride 0.00500 0.00467 93.4 5.00-195 (5)Toluene-d8 103 80.0-120 (5)4-Bromolluorobenzene 101 80.0-120 (5)1,2-Dichloroethane-d4 9Z7 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 14:13 16 of 28 WG1428553 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. 10 Volatile Organic Compounds(GC/MS)by Method 624.1 11189390.01 Method Blank(MB) (MB)03500170-2 02/15/2013:59 Cp MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/1 mgfl mg/1 Tc Tetrachloroethene U 0.000372 0.00100 (S)Toluene-d8 110 80.0-120 111 (5)4-BromoBuorobenzene 90.7 80.0-120 (S)1,2-Dichloroethane-d4 102 70.0-130 El Laboratory Control Sample(LCS) 5Sr (LCS)R3500170-1 02/15/20 12:59 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Ell Analyte mgA mg/1 % % Tetrachloroethene 0.00500 0.00510 102 70.0-130 7 (S)Toluene-d8 111 80.0-120 GI (S)4-Bromofuorobenzene 90.6 80.0-120 (S)1,1-Dlchloroethane-d4 102 70.0-130 sAl SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 17 of 28 WG1428898 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. At Pesticides(GC)by Method EPA 608.3 L1189390.01,02 Method Blank(MB) Cp R3501000-1 02/18/20 18:17 MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/1 mg/1 mg/i Tc Aldrin U 0.00000813 0.0000500 Alpha BHC U 0.0000166 0.0000500 3 SS Beta BHC U 0.0000184 0.0000500 Delta BHC U 0.0000197 0.0000500 4 Gamma BHC U 0.0000176 0.0000500 Cn 4,4-ODD U 0.0000170 0.0000500 4,4-ODE U 0.0000164 0.0000500 'Sr 4,4-DDT U 0.0000177 0.0000500 Dleldrin U 0.00000751 0.0000500 Endosulfan I U 0.0000179 0.0000500III Endosulfan II U 0.0000176 0.0000500 Endosulfan sulfate U 0.0000196 0.0000500 CI Endrin U 0.0000189 0.0000500 Endrin aldehyde U 0.0000142 0.0000500 a Endrin ketone U 0.0000170 0.0000500 Al Heptachlor U 0.0000108 0.0000500 Heptachlor epoxide U 0.0000175 0.0000500 Hexachlorobenzene U 0.0000134 0.0000500 el Methoxychlor U 0.0000193 0.0000500 Chlordane U 0.0000977 0.000500 Toxaphene U 0.000168 0.000500 (S)Decachlorobiphenyl 87.0 10.0-144 (5)Tetrochloro-m-xyylene 86.5 10.0-135 Laboratory Control Sample(LCS) (LCS)R3501000-2 02/18/20 18:29 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg/1 mg/I % % Aldrin 0.00100 0.000654 65.4 42.0-140 Alpha BHC 0.00100 0.000797 79.7 37.0-140 Beta BHC 0.00100 0.000845 84.5 17.0-147 Delta BHC 0.00100 0.000817 81.7 19.0-140 Gamma BHC 0.00100 0.000818 81.8 32.0-140 4,4-0DD 0.00100 0.0007E19 78.9 31.0-141 4,4-ODE 0.00100 0.000741 74.1 30.0-145 4,4-DDT 0.00100 0.000772 77.2 25.0-160 Dieklrin 0.00100 0.000811 81.1 36.0-146 Endosulfan I 0.00100 0.000858 85.8 45.0-153 ACCOUNT: PROJECT: SOD: DATE/ONE: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 18 of 28 WG1428898 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Ilk Pesticides(GC)by Method EPA 608.3 L1189390-01,02 Laboratory Control Sample(LCS) (LCS)R3501000-2 02/18/20 18:29 Cp Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 2 Analyte mgA mgA % % Tc Endosulfan II 0.00100 0.000'842 84.2 1.00-202 Endosulfan sulfate 0.00100 0.000789 78.9 26.0-144 el Endrin 0.00100 0.000791 79.1 30.0-147 Endrin aldehyde 0.00100 0.000716 71.6 56.0-128 Endrin ketone 0.00100 0.000848 84.8 54.0-142El Heptachlor 0.00100 0.000668 66.8 34.0-140 Heptachlor epoxide 0.00100 0.000836 83.6 37.0-142 s Sr Hexachlorobenzene 0.00100 0.000718 71.8 35.0-120 Methoxychlor 0.00100 0.000706 70.6 44.0-160 (S)Decachbrobiphenyl 89.5 10.0-144III (S)Tel rochloro-m-xylene 76.6 10.0-135 7 GI L1189247-01 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) 3 (OS)L1189247-01 02/18/2018:54•(MS)03501000-3 02/18/2019:06•(MSD)83501000-4 02/18/2019:19 Al Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits ' Analyte mgA mgA mgA mgA % % % % % SC Aldrin 0.00100 ND 0.000786 0.000807 78.6 80.7 1 42.0-140 2.64 35 Alpha BAC 0.00100 ND 0.000870 0.000902 87.0 90.2 1 37.0-140 3.61 36 Beta BHC 0.00100 ND 0.000918 0.000955 91.8 95.5 1 17.0-147 3.95 44 Delta BHC 0.00100 ND 0.000825 0.000868 82.5 86.8 1 19.0-140 5.08 52 Gamma BHC 0.00100 ND 0.000861 0.000925 86.1 92.5 1 32.0-140 7.17 39 4,4-0DD 0.00100 ND 0.000829 0.000908 82.9 90.8 1 31.0-141 9.10 39 4,4-DDE 0.00100 ND 0.000754 0.000825 75.4 82.5 1 30.0-145 8.99 35 4,4-001 0.00100 ND 0.000896 0.000949 89.6 94.9 1 25.0-160 5.75 42 Dleldrin 0.00100 ND 0.000855 0.000893 85.5 89.3 1 36.0-146 4.35 49 Endosulfan I 0.00100 ND 0.000986 0.00104 98.6 104 1 45.0-153 5.33 28 Endosulfan II 0.00100 ND 0.000873 0.000908 87.3 90.8 1 1.00-202 3.93 53 Endosulfan sulfate 0.00100 ND 0.000840 0.000938 84.0 93.8 1 26.0-144 11.0 38 Endrin 0.00100 ND 0.000891 0.000952 89.1 95.2 1 30.0-147 6.62 48 Endrin aldehyde 0.00100 ND 0.000745 0.000793 74.5 79.3 1 56.0-128 6.24 20 Endrin ketone 0.00100 ND 0.000930 0.000967 93.0 96.7 1 54.0-142 3.90 20 Heptachlor 0.00100 ND 0.000829 0.000840 82.9 84.0 1 34.0-140 1.32 43 Heptachlor epoxide 0.00100 ND 0.000879 0.000900 87.9 90.0 1 37.0-142 2.36 26 Hexachlorobenzene 0.00100 ND 0.000821 0.000916 82.1 91.6 1 35.0-120 '10.9 25 Methoxychlor 0.00100 ND 0.000851 0.00121 85.1 121 1 44.0-160 J3 34.8 22 (5)Decochlorob/phenyl 76.2 8Z5 10.0-144 (5)Tetrochbro-m-xylene 80.9 84.2 10.0-135 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 19 of 28 WG1428898 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE. SI Polychlorinated Biphenyls(GC)by Method EPA-608.3 Ltt89390.01,02 Method Blank(MB) (MB)R3500482-2 02/17/20 07:09 Cp MB Result MB Qualifier MB MDL MB RDL Analyte mgA mg/1 mg/I TC PCB 1260 U 0.000120 0.000500 PCB 1016 U 0.000100 0.000500 3 SS PCB 1221 U 0.0000730 0.000500 PCB 1232 U 0.0000420 0.000500 4 PCB 1242 U 0.0000470 0.000500 Cn PCB 1248 U 0.0000860 0.000500 PCB 1254 U 0.0000470 0.000500 SrS (S)Decochloroblphenyl 86.2 10.0-144 (5)Telrachloro-m-xylene 103 10.0-135 III Laboratory Control Sample(LCS) 7GI (LCS)R3500482-1 02/17/20 06:55 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Al_ Analyte mgA mg4 % % PCB 1260 0.00250 0.00247 98.8 8.00-140 • PCB 1016 0.00250 0.00315 126 50.0-140 SC (5)Decachloroblphenyl 69.2 10.0-144 (5)Telrochloro-m-xylene 94.0 10.0-135 L1189247-01 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) (OS)L1189247-01 02/17/20 08:33•(MS)R3500482-3 02/17/20 08:47•(MSD)R3500482-4 02/17/20 09:01 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/1 mg/1 mgA mg/1 % % % % % PCB 1260 0.00250 ND. 0.00282 0.00321 113 128 1 8.00-140 12.9 38 PCB 1016 0.00250 ND 0.00564 0.00630 226 252 1 50.0-140 J5 P J5 P 11.1 36 (5)Decachloroblphenyl 815 79.5 10.0-144 (5)Tetrachloro-m-xylene 109 104 10.0-135 ACCOUNT: PROJECT: SOS: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 14:13 20 of 28 WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. It Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L118 9 3 90-01,02 Method Blank(MB) (MB)R3501438-2 02/19/20 23:46 Cp MB Result MB Qualifier MB MDL MB RDL 2 Analyte mg/1 mg/I mg/1 Tc Acenaphthene U 0.000316 0.00100 Acenaphthylene U 0.000309 0.00100 3 SS Anthracene U 0.000291 0.00100 Benzldine U 0.00432 0.0100 4 Benzo(ajanthracene U 0.0000975 0.00100 Cn 8enzo(b)fluoranthene U 0.0000896 0.00100 Benzo(k)fluoranthene U 0.000355 0.00100 5Sr Benzo(g,h,i)perylene U 0.000161 0.00100 Benzo(ajpyrene U 0.000340 0.00100 • 81s(2-chlorethoxy)methane U 0.000329 0.0100IIII Bis(2-chloroethyl)ether U 0.00162 0.0100 2,2-0xybis(1-Chloropropane) U 0.000445 0.0100 GI 4-Bromophenyl-phenylether U 0.000335 0.0100 2-Chloronaphthalene U 0.000330 0.00100 , 4-Chlorophenyl-phenylether U 0.000303 0.0100 Al Chrysene U 0.000332 0.00100 Dibenz(a,h)anthracene U 0.000279 0.00100 SC 3,3-Dichlorobenzidine U 0.00202 0.0100 2.4-Dinitrotoluene U 0.00165 0.0100 2,6-Dinitrotoluene U 0.000279 0.0100 Fluoranthene U 0.000310 0.00100 Fluorene U 0.000323 0.00100 Hexachlorobenzene U 0.000341 0.00100 Hexachloro-1,3-butadiene U 0.000329 0.0100 Hexachlorocyclopentadiene U 0.00233 0.0100 Hexachloroethane U 0.000365 0.0100 Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 Isophorone U 0.000272 0.0100 Naphthalene U 0.000372 0.00100 Nitrobenzene U 0.000367 0.0100 n-Nitrosodimethylamine U 0.00126 0.0100 n-Nitrosodiphenylamine U 0.00119 0.0100 n-Nitrosodi-n-propylamine U 0.000403 0.0100 Phenanthrene U 0.000366 0.00100 Benzylbutyl phthalate U 0.000275 0.00300 Bis)2ethylhexyl)phthalate U 0.000709 0.00300 Dl-n-butyl phthalate U 0.000266 0.00300 Diethyl phthalate U 0.000282 0.00300 Dimethyl phthalate U 0.000283 0.00300 Di-n-octyl phthalate U 0.000278 0.00300 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 21 of 28 WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. ilk Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L118 9 3 90-01,02 Method Blank(MB) (MB)R3501438-2 02/19/20 23:46 Cp MB Result MB Qualifier MB MDL MB RDL Analyte mgA mgA mg/1 2Tc Pyrene U 0.000330 0.00100 1,2.4-Trichlorobenzene U 0.000355 0.0100 3Ss 4-Chloro-3-methylphenol U 0.000263 0.0100 2-Chorophenol U 0.000283 0.0100 4 2,4-Dichlorophenol U 0.000284 0.0100 Cn 2,4-Dimethylphenol U 0.000624 0.0100 4,6-Dinitro-2-methylphenol U 0.00262 0.0100 5 Sr 2,4-Dinitrophenol U 0.00325 0.0100 2-Nitrophenol U 0.000320 0.0100 4-Nitrophenol U 0.00201 0.0100IIII Pentachlorophenol U 0.000313 0.0100 Phenol U 0.000334 0.0100 7G1 2,4,6-Trlchlorophenol U 0.000297 0.0100 Azobenzene U 0.000318 0.0100 3 (5)2-Fluorophenol 42.1 10.0-120 Al (5)Phenol-d5 26.6 8.00-424 (5)Nitro benzene-d5 60.9 15.0-314 Sc9 (5)2-Fluorobiphenyl 70.6 22.0-127 (5)24,6-Tribromophenol 685 10.0-153 (S)p-Terphenyl-d14 83.1 29.0-141 Laboratory Control Sample(LCS) (LCS)83501438-1 02/19/20 23:26 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mgA mg/ % % Acenaphthene 0.0500 0.0382 76.4 47.0-145 Acenaphthylene 0.0500 0.0406 81.2 33.0-145 Anthracene 0.0500 0.0391 78.2 27.0-133 Benzldine 0.100 0.0244 24.4 1.00-120 Benzo(a)anthracene 0.0500 0.0413 82.6 33.0-143 Benzo(b)fluoranthene 0.0500 0.0439 87.8 24.0-159 Benzo(k)Buoranthene 0.0500 0.0408 81.6 11.0-162 Benzo(g,h,i)perylene 0.0500 0.0390 78.0 1.00-219 Benzo(a)pyrene 0.0500 0.0433 86.6 17.0-163 Bis(2-chlorethoxy)methane 0.0500 0.0335 67.0 1.00-219 Bis(2-chloroethyl)ether 0.0500 0.0381 76.2 33.0-185 2,2-0lrybis(1-Chloropropane) 0.0500 0.0358 71.6 36.0-166 4-Bromophenyl-phenylether 0.0500 0.0398 79.6 53.0-127 ACCOUNT: PROJECT: MG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 14:13 22 of 28 WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Semi Volatile Organic Compounds (GC/MS)by Method 625.1 12189390-01,02 Laboratory Control Sample(LCS) (LCS)93501438-1 02/19/20 23:26 Cp Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 2 Analyte mgA mgA % % Tc 2-Chloronaphthalene 0.0500 0.0369 73.8 60.0-120 4-Chlorophenyl-phenylether 0.0500 0.0405 81.0 25.0-158 'SS Chrysene 0.0500 0.0395 79.0 17.0-168 Dibenz(a,h)anthracene 0.0500 0.0411 82.2 1.00-227 3,3-Dichlorobenzidine 0.100 0.0800 80.0 1.00-262111 2.4-Dinitrotoluene 0.0500 0.0436 87.2 39.0-139 2,6-Dlnitrotoluene 0.0500 0.0420 84.0 50.0-158 5Sr Fluoranthene 0.0500 0.0421 84.2 26.0-137 Fluorene 0.0500 0.0402 80.4 59.0-121 Hexachlorobenzene 0.0500 0.0398 79.6 1.00-152III Hexachloro-1,3-butadiene 0.0500 0.0323 64.6 24.0-120 Hexachlorocyclopentadlene 0.0500 0.0275 55.0 10.0-120 2Gl Hexachloroethane 0.0500 0.0335 67.0 40.0-120 Indeno(1,2,3-cd)pyrene 0.0500 0.0403 80.6 1.00-171 a Isophorone 0.0500 0.0358 71.6 21.0-196 Al Naphthalene 0.0500 0,0330 66.0 21.0-133 Nitrobenzene 0.0500 0.0332 66.4 35.0-180 9 SC n-Nitrosodimethylamine 0.0500 0.0252 50.4 10.0-120 n-Nitrosodiphenylamine 0.0500 0.0392 78.4 44.0-120 n-Nitrosodi-n-propylamine 0.0500 0.0401 80.2 1.00-230 Phenanthrene 0.0500 0.0396 79.2 54.0-120 Benzylbutyl phthalate 0.0500 0.0438 87.6 1.00-152 Bis(2ethylhexyl)phthalate 0.0500 0.0430 86.0 8.00-158 Di-n-butyl phthalate 0.0500 0.0439 87.8 1.00-120 Diethyl phthalate 0.0500 0.0432 86.4 1.00-120 Dimethyl phthalate 0.0500 0.0412 82.4 1.00-120 Di-n-octyl phthalate 0.0500 0.0425 85.0 4.00-146 Pyrene 0.0500 0.0418 83.6 52.0-120 1,2,4-Trlchlorobenzene 0.0500 0.0323 64.6 44.0-142 4-Chloro-3-methylphenol 0.0500 0.0341 68.2 22.0-147 2-Chlorophenol 0.0500 0.0334 66.8 23.0-134 14-Dichlorophenol 0.0500 0.0343 68.6 39.0-135 2,4-Dlmethylphenol 0.0500 0.0349 69.8 32.0-120 4,6-Dinitro-2-methylphenol 0.0500 0.0428 85.6 1.00-181 2.4-Dinitrophenol 0.0500 0.0436 87.2 1.00-191 2-Nitrophenol 0.0500 0.0354 70.8 29.0-182 4-Nitrophenol 0.0500 0.0170 34.0 1.00-132 Pentachlorophenol 0.0500 0.0491 98.2 14.0-176 Phenol 0.0500 0.0152 30.4 5.00-120 2,4,6-Trichlorophenol 0.0500 0.0382 76.4 37.0-144 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/201413 23 of 28 WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Ilk Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L1189390-01,02 Laboratory Control Sample(LCS) (LCS)R3501438-1 02/19/20 23:26 Cp Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Analyte mg/1 mg/I % % �Tc Azobenzene 0.0500 0.0412 82.4 37.0-125 (5)2-Fluorophenol 46.3 10.0-120 SS (S)Phenol-d5 29.3 8.00-424 (S)Nitrobenzene-d5 569 15.0-314 4 (5)2-Fluorobiphenyl 76.3 22.0-127 Cn (5)2,4,6-Tribromophenol 78.0 10.0-153 (S)p-Terphenyl-d14 84.6 29.0-141 Sr L1189427-05 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) 11111 (OS)L1189427-05 02/20/20 00:47•(MS)R3501438-3 02/20/20 01:08•(MSD)R3501438-4 02/20/20 01:28 7 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits GI Analyte mg/I mg/I mg/I mg/I % % % % % Acenaphthene 0.0500 ND 0.0355 0.0382 71.0 76.4 1 47.0-145 7.33 48 JAI Acenaphthylene 0.0500 ND 0.0381 0.0413 76.2 82.6 1 33.0-145 8.06 74 Anthracene 0.0500 ND 0.0384 0.0397 76.8 79.4 1 27.0-133 3.33 66 8enzidine 0.100 ND 0.0597 0.0224 59.7 22.4 1 1.00-120 J3 90.9 40 -SC Benzo(a)anthracene 0.0500 ND 0.0406 0.0424 81.2 84.8 1 33.0-143 4.34 53 Benzo(b)Buoranthene 0.0500 ND 0.0423 0.0428 84.6 85.6 1 24.0-159 1.18 71 Benzo(k)Buoranthene 0.0500 ND 0.0394 0.0411 78.8 82.2 1 11.0-162 4.22 63 Benzo(g.h,i)perylene 0.0500 ND 0.0380 0.0399 76.0 79.8 1 1.00-219 4.88 97 Benzo(a)pyrene 0.0500 ND 0.0422 0.0436 84.4 87.2 1 17.0-163 3.26 72 Bis(2-chlorethox)r)methane 0.0500 ND 0.0314 0.0331 62.8 66.2 1 33.0-184 5.27 54 Bis(2-chloroethyl)ether 0.0500 ND 0.0353 0.0366 70.6 73.2 1 12.0-158 3.62 108 2,2-Oxybis(1-Chloropropane) 0.0500 ND 0.0334 0.0343 66.8 68.6 1 36.0-166 2.66 76 4-Bromophenyl-phenylether 0.0500 ND 0.0385 0.0398 77.0 79.6 1 53.0-127 3.32 43 2-Chloronaphthalene 0.0500 ND 0.0348 0.0385 69.6 77.0 1 60.0-120 10.1 24 4-Chlorophenyl-phenylether 0.0500 ND 0.0375 0.0407 75.0 81.4 1 25.0-158 8.18 61 Chrysene 0.0500 ND 0.0379 0.0398 75.8 79.6 1 17.0-168 4.89 87 Dibenz(a,h)anthracene 0.0500 ND 0.0394 0.0418 78.8 83.6 1 1.00-227 5.91 126 3,3-Dichlorobenzidine 0.100 ND 0.0792 0.0813 79.2 81.3 1 1.00-262 2.62 108 2.4-Dinitrotoluene 0.0500 ND 0.0416 0.0448 83.2 89.6 1 39.0-139 7.41 42 2,6-Dinitrotoluene 0.0500 ND 0.0394 0.0424 78.8 84.8 1 50.0-158 7.33 48 1,2-Diphenylhydrazine 0.0500 ND 0.0392 0.0413 78.4 82.6 1 18.0-156 5.22 34 Fluoranthene 0.0500 ND 0.0415 0.0428 83.0 85.6 1 26.0-137 3.08 66 Fluorene 0.0500 ND 0.0376 0.0409 75.2 81.8 1 59.0-121 8.41 38 Hexachlorobenzene 0.0500 ND 0.0382 0.0400 76.4 80.0 1 1.00-152 4.60 55 Hexachloro-1,3-butadiene 0.0500 ND 0.0322 0.0339 64.4 67.8 1 24.0-120 5.14 62 Hexachlorocyclopentadiene 0.0500 ND 0.0277 0.0301 55.4 60.2 1 10.0-146 8.30 34 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 14:13 24 of 28 WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .110 Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L1189390.01,02 L1189427-05 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) (OS)L1189427-05 02/20/20 00:47•(MS)R3501438-3 02/20/20 01:08•(MSD)R3501438-4 02/20/20 01:28 Cp Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits .Analyte mgll mgll mg/1 mg9 % % % % % Tc Hexachloroethane 0.0500 ND 0.0335 0.0345 67.0 69.0 1 40.0-120 2.94 52 Indeno(1,2,3-cd)pyrene 0.0500 ND 0.0391 0.0407 78.2 81.4 1 1.00-171 4.01 99 3 SS Isophorone 0.0500 ND 0.0334 0.0353 66.8 70.6 1 21.0-196 5.53 93 Naphthalene 0.0500 ND 0.0313 0.0331 62.6 66.2 1 21.0-133 5.59 65 4 Nitrobenzene 0.0500 ND 0.0319 0.0337 63.8 67.4 1 35.0-180 5.49 62 Cn n-Nltrosodimethylamine 0.0500 ND 0.0256 0.0260 51.2 52.0 1 10.0-120 1.55 40 n-Nltrosodiphenylamine 0.0500 ND 0.0378 0.0391 75.6 78.2 1 16.0-160 3.38 28 s Sr n-Nitrosodi-n-propylamine 0.0500 ND 0.0360 0.0382 72.0 76.4 1 1.00-230 5.93 87 Phenanthrene 0.0500 ND 0.0392 0.0403 78.4 80.6 1 54.0-120 2.77 39 Benzylbutyl phthalate 0.0500 ND 0.0422 0.0434 84.4 86.8 1 1.00-152 2.80 60Fl Bis(2-ethylhexy)phthalate 0.0500 ND 0.0408 0.0420 81.6 84.0 1 8.00-158 2.90 82 Dl-n-butyl phthalate 0.0500 ND 0.0428 0.0433 85.6 86.6 1 1.00-120 1.16 47 Diethyl phthalate 0.0500 ND 0.0405 0.0426 81.0 85.2 1 1.00-120 5.05 100 CI Dimethyl phthalate 0.0500 ND 0.0391 0.0410 78.2 82.0 1 1.00-120 4.74 183 a Di-n-octyl phthalate 0.0500 ND 0.0406 0.0425 81.2 85.0 1 4.00-146 4.57 69 Al Pyrene 0.0500 ND 0.0406 0.0412 81.2 82.4 1 52.0-120 1.47 49 1,2,4-Trlchlorobenzene 0.0500 ND 0.0316 0.0329 63.2 65.8 1 44.0-142 4.03 50 9Sc 4-Chloro-3-methylphenol 0.0500 ND 0.0322 0.0337 64.4 67.4 1 22.0-147 4.55 73 2-Chlorophenol 0.0500 ND 0.0326 0.0343 65.2 68.6 1 23.0-134 5.08 61 2,4-Dichlorophenol 0.0500 ND 0.0326 0.0344 65.2 68.8 1 39.0-135 5.37 50 2,4-Dimethylphenol 0.0500 ND 0.0334 0.0360 66.8 72.0 1 32.0-120 7.49 58 4,6-Dinitro-2-methylphenol 0.0500 ND 0.0423 0.0442 84.6 88.4 1 1.00-181 4.39 203 2.4-Dinitrophenol 0.0500 ND 0.0423 0.0455 84.6 91.0 1 1.00-191 7.29 132 2-N6rophenol 0.0500 ND 0.0334 0.0353 66.8 70.6 1 29.0-182 5.53 55 4-Nltrophenol 0.0500 ND 0.0178 0.0187 35.6 37.4 1 1.00-132 4.93 131 Pentachlorophenol 0.0500 ND 0.0476 0.0494 95.2 98.8 1 14.0-176 3.71 86 Phenol 0.0500 ND 0.0154 0.0162 30.8 32.4 1 5.00-120 5.06 64 2,4,6-Trichlorophenol 0.0500 ND 0.0368 0.0401 73.6 80.2 1 37.0-144 8.58 58 (S)2-Fluorophenol 45.7 49.4 10.0-120 (5)Phenol-d5 30.0 315 8.00-424 (5)Nitrobenzene-6 53.1 56.7 15.0-314 (S)2-Fluorobipheny/ 712 78.1 22.0-127 (5)2,4,6-Tribromophenol 76.5 81.0 10.0-153 (S)p-Terphenyl-d14 82.6 83.5 29.0-141 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/20 14:73 25 of 28 GLOSSARY OF TERMS ONE LAB.NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not Cp intended as a comprehensive explanation,and if you have additional questions please contact your project representative. z Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, TC Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received. 3 Abbreviations and Definitions Ss MDL Method Detection Limit. 4 ND Not detected at the Reporting Limit(or MDL where applicable). Cn RDL Reported Detection Limit. Rec. Recovery. - Sr RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control Sample/Duplicate and Qc (S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit(or MDL where applicable). GI Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the Al Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the result reported has already been corrected for this factor. These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal SC Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control sample.The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL" Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL (Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty Confidence level of 2 sigma. (Radiochemistry) A brief discussion about the included sample results,including a discussion of any non-conformances to protocol Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. • This section of the report includes the results of the laboratory quality control analyses required by procedure or Quality Control Summary(Qc) analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not being performed on your samples typically,but on laboratory generated material. This is the document created in the field when your samples were initially collected.This is used to verify the time and Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples.These results are provided Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable;the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J5 The sample matrix interfered with the ability to make any accurate determination;spike value is high. P RPD between the primary and confirmatory analysis exceeded 40%. P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 26 of 28 ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE. 40 Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other lab is as accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the network 1 laboratories in our industry.The most significant benefit to our one location design is the design of our laboratory campus.The model is conducive to accelerated productivity,decreasing C p turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. "Not all certifications held by the laboratory are applicable to the results reported in the attached report. •Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. 2 Tc State Accreditations 3 Alabama 40660 Nebraska NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZ0612 New Hampshire 2975 4 Arkansas 88-0469 New Jersey—NELAP TN002 Cn California 2932 New Mexico' n/a Colorado TN00003 New York 11742 5 Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 6 Georgia' 923 North Dakota R-140 Qc Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 7 Indiana C-TN-01 Oregon TN200002 GI Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky'6 90010 South Carolina 84004 Al Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee'` 2006 l Louisiana' LA180010 Texas T10 47 0 4 2 4 5-18-15 SC Maine TN0002 Texas LAB0152 Maryland 324 Utah TN00003 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2LA Third Party Federal Accreditations A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA—ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 'Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity `Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies.If you would like assistance from one of our support offices,please contact our main office.Pace National performs all testing at our central laboratory. MT ND POP OR Ir. ." f ID SD VVY IMP NE 1i. OH 42pr t CA co KS MO alaild* �rVA� T • N / TdP NM OK 11 AR 4114 TX GA a.o - 141‘ ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Eaton Corporation 28091-R L1189390 02/20/2014:13 27 of 28 Billing Information. 7lnaivss f CooLiirter I Cr,er,tt�'v.�, Chain of Cuotody rare of NA financial Services Center-1009 Prey Eaton Corporation rte Chi N' aeAnaVical. PO Box 818024 2564 Durham Road Cleveland,ON 44181-8024 Roxboro,NC 27573 i 1 �� tFous W..,Ra fa - 0 Enia To Mount lutrti.tw 3Tt1I Report dustintadairEaeaton.com,cohnwbetchangdeatos co v pmone:ctstsa-test .. DustintaClair y :eoa-Tbssasa 'A Please Cade- --- v r t,6007679 Qf.. �, Coy/State �ot MT CT ET `'r. Project Collected. `� r D<,.scr;pt;on:Eaton Corp Monthly Stonmwat Lab Pro,eet a 1,1 j � ` SDs a { (Lent Project p t �.J_,,,-� Phone 28091-R EATONRNC-28091SW — L11 ` J Ci0 34i w ti X s o 0 Fax Site/Facility IDO P.0-N a. ,p fl y o r� �� Acc.ii...,�-_.-. 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