HomeMy WebLinkAboutNCG030027_DMR_20200213 F , N• Scott K. Bailey
Plant Director
(336) 503-6536 (phone)
(336) 503-6562 (fax)
scottkbaileyeaton.com
R , D
February 24, 2020 MtA o$0.0Z0
CENT L FILES
Division of Water Quality D1�VR SEC10N
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attn: DWQ Central Files
RE: February 2020 Monthly Tier III Discharge Monitoring Report
Attached are the analytical results and associated chain of custody for the February 13, 2020 monthly Tier
Ill stormwater outfall sampling event, submitted in accordance with Section D of the NPDES Stormwater
General Permit No. NCG030000 and Certificate of Coverage No. NCG030027 issued to our facility.
Additionally, attached is the applicable Discharge Monitoring Report (DMR) Form provided by the North
Carolina Division of Water Quality (NCDWQ).
I certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with the system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,
or other persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violations.
Sincerely,
Scott K. Bailey
Plant Director
Attachments
Stormwater Discharge Monitoring Report
for North Carolina Division of Energy, Mineral and Land Resources General Permit No. NCG030000
Date submitted 02/24/2020
CERTIFICATE OF COVERAGE NO. NCGO3 0 0 2 7 SAMPLE COLLECTION YEAR 2020
FACILITY NAME Eaton Corporation SAMPLE PERIOD 0 Jan-June 0 July-Dec
COUNTY Person County or ® Monthly' (month)
PERSON COLLECTING SAMPLES Colin Betchan DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout _PNA
LABORATORY Pace National Lab Cert.# ENV375/DW21704/BI0041 ❑Zero-flow ❑Water Supply nSA
Comments on sample collection or analysis: *Other ws-ill;NSW
`�' %C I ,1 D PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4
Part A: Stormwater Benchmarks and Monitoring Results MAR 0 3 2020
i RAL- - No discharge this period?2
:WR Ste' + ,
Non-Polar O&G/
Date Sample 24-hour rainfall pH, Total Toxic
Outfall No. Collected) amount, Total Suspended Solids Standard units Total Copper Total Lead Total Zinc Total Petroleum Organics
(mo/dd/yr) Inches3 Hydrocarbons
Benchmarks - - 100 mg/L or 50 mg/L4 6.0—9.0 0.010 mg/L 0.075 mg/L 0.126 mg/L 15 mg/L 1 mg/L
Parameter Code - 46529 C0530 00400 01119 01051 01094 00552 78141
Pond (001) 02/13/2020 0.60 12.3 6.0 0.00700 0.00200 0.0711 0.906 0.03410
Tool Room Trench(005) 02/13/2020 0.60 13.2 6.0 0.00700 0.00200 0.0237 0.873 0.03325
1 Monthly sampling(instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall.
2 For sampling periods with no discharge at any single outfall,you must still submit this discharge monitoring report with a checkmark here.
'The total precipitation must be recorded using data from an on-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement.
4 See General Permit,Section B,Table 1 to identify the especially sensitive receiving water classifications where the more protective benchmark applies.
'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture
electronic crystals,or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA
Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11;for semiconductor
manufacture use the definition as found in 40 CFR 469.12;for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray
tube manufacture use the definition found in 40 CFR 469.31).
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 1 of 3
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring
may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General
Permit. For those facilities electing to employ the TTO monitoring waiver,the discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics
(TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or
stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the
solvent management plan included in the Stormwater Pollution Prevention Plan."
Scott K. Bailey
Name(Print name)
Plant Director
Title(Prin itle)
LA AA,L-
Signature Date
Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL,<PQL, Non-detect, ND, or other similar non-numerical
format. When results are below the applicable limits,they must be reported in the format, "<XX mg/L",where XX is the numerical value of the detection
limit, reporting limit, etc. in mg/L.
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging> 55 gal of new oil per month.
No discharge this period?2
Outfall No. Date Sample Collected' 24-hour rainfall amount, New Motor Oil or Non-Polar O&G/Total Total Suspended
(mo/dd/yr) Inches' Hydraulic Oil Usage Petroleum Hydrocarbons Solids
Benchmarks - - - 15 mg/L 100 mg/L or 50 mg/L4
Parameter Code - 46529 NCOIL 00552 C0530
Footnotes from Part A also apply to Part B
Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text.
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 2 of 3
FOR PART A AND PART B MONITORING RESULTS:
• A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B.
• TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES El NO E
IF YES, HAVE YOU CONTACTED THE DEMLR REGIONAL OFFICE? YES Q NO E
REGIONAL OFFICE CONTACT NAME: Danny Smith
Mail an original copy of this DMR, including all"No Discharge"reports, within 30 days of receipt of the lab results(or at end of monitoring period in the
case of"No Discharge"reports)to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED:
"I certify, under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,or
those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate, and complete. I
am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations."
"O?
Signature of Permittee Date
Permit Date: 11/1/2018-05/31/2021 SWU-245, last revised 11/1/2018
Page 3 of 3
aceAnalytical® A \ A L Y T I C A L R S O R T ,
National Center for Testing&Innovation February 20, 2 02 0 p
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Eaton Corporation
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Sample Delivery Group: L1189390 Cn
Samples Received: 02/14/2020 5Sr
Project Number: 28091-R
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Description: Eaton Corp Monthly Stormwater Qc
Site: ROXBORO, NC
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Report To: Dustin LaClair
2564 Durham Road &Al
Roxboro, NC 27573
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Entire Report Reviewed By:
Heather J Wagner
.,. Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values.This test report shall not be
reproduced,except in full,without written approval of the laboratory.Where applicable,sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068.Where sampling conducted by the customer,results relate to the accuracy of the information provided,
and as the samples are received.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 14:13 1 of 28
imummimmiummmommilmommumummommoimmie
TABLE OF CONTENTS ONE LAB.NATIONWIDE. iik
Cp:Cover Page 1 1
Cp
Tc:Table of Contents 2
Ss:Sample Summary 3 Tc
Cn:Case Narrative 4
3
Sr:Sample Results 5 Ss
2020-02-13-001 L1189390-01 5 4
Cn
2020-02-13-005 L1189390-02 9
Oc:Quality Control Summary 12 5Sr
Gravimetric Analysis by Method 2540 D-2011 12
6
Wet Chemistry by Method 1664B 13 Qc
Metals(ICP)by Method 200.7 14 7
GI
Volatile Organic Compounds(GC/MS)by Method 624.1 15
Pesticides(GC)by Method EPA 608.3 18 JAI
Polychlorinated Biphenyls(GC)by Method EPA-608.3 20
y
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 21 Sc
GI:Glossary of Terms 26
AI:Accreditations& Locations 27
Sc: Sample Chain of Custody 28
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 2 of 28
SAMPLE SUMMARY ONE LAB.NATIONWIDE. AO
Collected by Collected date/time Received date/time
2020-02-13-001 L1189390-01 WW 02/13/2009:52 02/14/2008:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time 2
�� Tc
Gravimetric Analysis by Method 2540 D-2011 � WG1428711 1 02/15/20 22:57 02/16/20 00:55 TH Mt.Juliet,TN
Wet Chemistry by Method 1664B WG1430093 1 02/18/20 08:42 02/18/20 22:07 MBP Mt.Juliet,TN 3
Metals(ICP)by Method 200.7 WG1428157 1 02/15/2011:24 02/16/2013:49 CCE Mt.Juliet,TN Ss
Volatile Organic Compounds(GC/MS)by Method 624.1 WG1428464 1 02/15/2013:41 02/15/2013:41 ADM Mt.Juliet,TN
Volatile Organic Compounds(GC/MS)by Method 624.1 WG1428553 1 02/15/2015:28 02/15/2015:28 BMB Mt.Juliet,TN °
Cn
Pesticides(GC)by Method EPA 608.3 WG1428898 1 02/16/2016:38 02/18/20 20:08 HMH Mt.Juliet,TN
Polychlorinated Biphenyls(GC)by Method EPA-608.3 WG1428898 1 02/16/2016:38 02/17/2010:11 SSH Mt.Juliet,TN s
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 WG1429926 1 02/19/20 15:05 02/19/20 23:34 AO Mt.Juliet,TN Sr
6
Collected by Collected date/time Received date/time QC
2020-02-13-005 L1189390-02 WW 02/13/2009:34 02/14/20 08:45
7
Method Batch Dilution Preparation Analysis Analyst Location GI
dateRime date/time
Gravimetric Analysis by Method 2540 D-2011 WG1428711 1 02/15/20 22:57 02/16/20 00:55 TH Mt.Juliet,TN -AI
Wet Chemistry by Method 1664E WG1430093 1 02/18/20 08:42 02/18/20 22:07 MBP Mt.Juliet,TN
Metals(ICP)by Method 200.7 WG1428157 1 02/15/2011:24 02/16/20 13:52 CCE Mt.Juliet,TN
Volatile Organic Compounds(GC/MS)by Method 624.1 WG1428464 1 02/15/2014:01 02/15/2014:01 ADM Mt.Juliet,TN SC
Pesticides(GC)by Method EPA 608.3 WG1428898 1 02/16/2016:38 02/18/20 20:21 HMH Mt.Juliet,TN
Polychlorinated Biphenyls(GC)by Method EPA-608.3 WG1428898 1 02/16/2016:38 02/17/2010:25 SSH Mt.Juliet,TN
Semi Volatile Organic Compounds(GC/MS)by Method 625.1 WG1429926 1 02/19/2015:05 02/19/20 23:54 AO Mt.Juliet,TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 3 of 28
CASE NARRATIVE ONE LAB.NATIONWIDE. AA
Cp
All sample aliquots were received at the correct temperature,in the proper containers,with the
appropriate preservatives,and within method specified holding times,unless qualified or notated within
the report. Where applicable,all MDL(LOD)and RDL(LOQ)values reported for environmental samples Tc
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative,a non-conformance form 3
or properly qualified within the sample results.By my digital signature below, I affirm to the best of my Ss
knowledge,all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory,and no information or data have been
knowingly withheld that would affect the quality of the data. Cn
5
Sr
Qc
GI
Heather J Wagner
Project Manager Al
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 4 of 28
2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. Si
Collected date/time: 02/13/20 09:52 L1189390
Additional Information ,
Result Units Cp
Analyte
2
pH(On Site) 6 su Tc
Temperature(on-site) 12.1 Deg C
3
Ss
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier MDL RDL Dilution Analysis Batch 4
Analyte mg/I mg/I mg/I date/time Cn
Suspended Solids 12.3 0.368 2.63 1 02/16/2020 00:55 WG1428711
Sr
Wet Chemistry by Method 1664E
6
Result Qualifier MDL RDL Dilution Analysis Batch Qc
Analyte mg/I mg/I mg/I date/time
TPH-Oil&Grease U 0.906 6.25 1 02/18/2020 22:07 WG1430093 7GI
Metals (ICP) by Method 200.7 C
Result Qualifier MDL RDL Dilution Analysis Batch Al
Analyte mg/I mg/I mg/I date/time
9
Copper U 0.00700 0.0100 1 02/16/202013:49 WG1428157 SC
Lead U 0.00200 0.00500 1 02/16/202013:49 WG1428157
Zinc 0.0711 0.00340 0.0500 1 02/16/202013:49 WG1428157
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/ mg/I mg/I date/time
Acrolein U 0.00887 0.0500 1 02/15/2020 13:41 WG1428464
Acrylonitrile U 0.00187 0.0100 1 02/15/2020 13:41 WG1428464
Benzene U 0.000331 0.00100 1 02/15/2020 13:41 WG1428464
Bromodichloromethane U 0.000380 0.00100 1 02/15/202013:41 WG1428464
Bromoform U 0.000469 0.00100 1 02/15/202013:41 WG1428464
Bromomethane U 0.000866 0.00500 1 02/15/202013:41 WG1428464
Carbon tetrachloride U 0.000379 0.00100 1 02/15/202013:41 WG1428464
Chlorobenzene U 0.000348 0.00100 1 02/15/202013:41 WG1428464
Chlorodibromomethane U 0.000327 0.00100 1 02/15/202013:41 WG1428464
Chloroethane U 0.000453 0.00500 1 02/15/202013:41 WG1428464
2-Chloroethyl vinyl ether U 0.00301 0.0500 1 02/15/202013:41 WG1428464
Chloroform U 0.000324 0.00500 1 02/15/202013:41 WG1428464
Chloromethane U 0.000276 0.00250 1 02/15/202013:41 WG1428464
1,2-Dichlorobenzene U 0.000349 0.00100 1 02/15/202013:41 WG1428464
1,3-Dichlorobenzene U 0.000220 0.00100 1 02/15/202013:41 WG1428464
1,4-Dichlorobenzene U 0.000274 0.00100 1 02/15/202013:41 WG1428464
Dichlorodifluoromethane U 0.000551 0.00500 1 02/15/202013:41 WG1428464
1,1-Dichloroethane U 0.000259 0.00100 1 02/15/202013:41 WG1428464
1,2-Dichloroethane U 0.000361 0.00100 1 02/15/202013:41 WG1428464
1,1-Dichloroethene U 0.000398 0.00100 1 02/15/202013:41 WG1428464
trans-1,2-Dichloroethene U 0.000396 0.00100 1 02/15/202013:41 WG1428464
1,2-Dichloropropane U 0.000306 0.00100 1 02/15/202013:41 WG1428464
cis-1,3-Dichloropropene U 0.000418 0.00100 1 02/15/202013:41 WG1428464
trans-1,3-Dichloropropene U 0.000419 0.00100 1 02/15/202013:41 WG1428464
Ethylbenzene U 0.000384 0.00100 1 02/15/202013:41 WG1428464
Methylene Chloride U 0.00100 0.00500 1 02/15/202013:41 WG1428464
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 02/15/202013:41 WG1428464
Tetrachloroethene 0.000648 J 0.000372 0.00100 1 02/15/202015:28 WG1428553
Toluene U 0.000412 0.00100 1 02/15/202013:41 WG1428464
1,1,1-Trichloroethane U 0.000319 0.00100 1 02/15/202013:41 WG1428464
1,1,2-Trichloroethane U 0.000383 0.00100 1 02/15/202013:41 WG1428464
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 5 of 28
2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. *
Collected date/time: 02/13/20 09:52 L1189390
Volatile Organic Compounds(GC/MS) by Method 624.1
,
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
Trichlaroethene U 0.000398 0.00100 1 02/15/2020 13:41 WG1428464 z
Tc
Trichlorofuoromethane U 0.00120 0.00500 1 02/15/2020 13:41 WG1428464
Vinyl chloride U 0.000259 0.00100 1 02/15/2020 13:41 WG1428464 3
(S)Toluene-d8 103 80.0-120 02/15/2020 13:41 WG1428464 Ss
(S)Toluene-d8 109 80.0-120 02/15/202015:28 WG1428553
(S 4-Bromofluorobenzene 99.3 80.0-120 02/15/2020 13:41 WG1428464 4
Cn
(S 4-Bromofluorobenzene 88.5 80.0-120 02/15/2020 15:28 WG1428553
(S)1,2-Dichloroethane-d4 99.3 70.0-130 02/15/202013:41 WG1428464
(S)1,2-Dichloroethane-d4 102 70.0-130 02/15/202015:28 WG1428553 Sr
Pesticides (GC) by Method EPA 608.3 60c
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time 7G1
Aldrin U 0.00000813 0.0000500 1 02/18/2020 20:08 WG1428898
Alpha BHC U 0.0000166 0.0000500 1 02/18/2020 20:08 WG1428898 c
Beta BHC U 0.0000184 0.0000500 1 02/18/2020 20:08 WG1428898 Al
Delta BHC U 0.0000197 0.0000500 1 02/18/2020 20:08 WG1428898
Gamma BHC U 0.0000176 0.0000500 1 02/18/2020 20:08 WG1428898 9SC
Chlordane U 0.0000977 0.000500 1 02/18/2020 20:08 WG1428898
4,4-DDD U 0.0000170 0.0000500 1 02/18/2020 20:08 WG1428898
4,4-DDE U 0.0000164 0.0000500 1 02/18/2020 20:08 WG1428898
4,4-DDT U 0.0000177 0.0000500 1 02/18/2020 20:08 WG1428898
Dieldrin U 0.00000751 0.0000500 1 02/18/2020 20:08 WG1428898
Endosulfan I U 0.0000179 0.0000500 1 02/18/2020 20:08 WG1428898
Endosulfan II U 0.0000176 0.0000500 1 02/18/2020 20:08 WG1428898
Endosulfan sulfate U 0.0000196 0.0000500 1 02/18/2020 20:08 WG1428898
Endrin U 0.0000189 0.0000500 1 02/18/2020 20:08 WG1428898
Endrin aldehyde U 0.0000142 0.0000500 1 02/18/2020 20:08 WG1428898
Endrin ketone U 0.0000170 0.0000500 1 02/18/2020 20:08 WG1428898
Heptachlor U 0.0000108 0.0000500 1 02/18/2020 20:08 WG1428898
Heptachlor epoxide U 0.0000175 0.0000500 1 02/18/2020 20:08 WG1428898
Hexachlorobenzene U 0.0000134 0.0000500 1 02/18/2020 20:08 WG1428898
Methoxychlor U 0.0000193 0.0000500 1 02/18/2020 20:08 WG1428898
Toxaphene U 0.000168 0.000500 1 02/18/2020 20:08 WG1428898
(S Decachlorobipheny/ 107 10.0-144 02/18/2020 20:08 WG1428898
(S)Tetrachloro-m-xylene 87.2 10.0-135 02/18/2020 20:08 WG1428898
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
PCB 1016 U 0.000100 0.000500 1 02/17/2020 10:11 WG1428898
PCB 1221 U 0.0000730 0.000500 1 02/17/202010:11 WG1428898
PCB 1232 U 0.0000420 0.000500 1 02/17/2020 10:11 WG1428898
PCB 1242 U 0.0000470 0.000500 1 02/17/2020 10:11 WG1428898
PCB 1248 U 0.0000860 0.000500 1 02/17/2020 10:11 WG1428898
PCB 1254 U 0.0000470 0.000500 1 02/17/2020 10:11 WG1428898
PCB 1260 U 0.000120 0.000500 1 02/17/2020 10:11 WG1428898
(S)Decachlorobiphenyl 103 10.0-144 02/17/2020 10:11 WG1428898
(S Tetrachloro-m-xylene 98.1 10.0-135 02/17/2020 10:11 WG1428898
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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imimmimmummummeimmommillmmmimmil
2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. .t
Collected date/time: 02/13/20 09:52 L1189390
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
,
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
Acenaphthene U 0.000316 0.00100 1 02/19/2020 23:34 WG1429926 2TC
Acenaphthylene U 0.000309 0.00100 1 02/19/2020 23:34 WG1429926
Anthracene U 0.000291 0.00100 1 02/19/2020 23:34 WG1429926 3
Benzidine U 0.00432 0.0100 1 02/19/2020 23:34 WG1429926 Ss
Benzo(a)anthracene U 0.0000975 0.00100 1 02/19/2020 23:34 WG1429926
Benzo(b)fluoranthene U 0.0000896 0.00100 1 02/19/2020 23:34 WG1429926 4
Cn
Benzo(k)fluoranthene U 0.000355 0.00100 1 02/19/2020 23:34 WG1429926
Benzo(g,h,i)perylene U 0.000161 0.00100 1 02/19/2020 23:34 WG1429926
Benzo(a)pyrene U 0.000340 0.00100 1 02/19/2020 23:34 WG1429926 SI
Bis(2-chlorethoxy)methane U 0.000329 0.0100 1 02/19/2020 23:34 WG1429926
Bis(2-chloroethyl)ether U 0.00162 0.0100 1 02/19/2020 23:34 WG1429926 6
Oc
2,2-Oxybis(1-Chloropropane) U 0.000445 0.0100 1 02/19/2020 23:34 WG1429926
4-Bromophenyl-phenylether U 0.000335 0.0100 1 02/19/2020 23:34 WG1429926 7
2-Chloronaphthalene U 0.000330 0.00100 1 02/19/2020 23:34 WG1429926 GI
4-Chlorophenyl-phenylether U 0.000303 0.0100 1 02/19/2020 23:34 WG1429926
Chrysene U 0.000332 0.00100 1 02/19/2020 23:34 WG1429926 s
Al
Dibenz(a,h)anthracene U 0.000279 0.00100 1 02/19/2020 23:34 WG1429926
3,3-Dichlorobenzidine U 0.00202 0.0100 1 02/19/2020 23:34 WG1429926
2,4-Dinitrotoluene U 0.00165 0.0100 1 02/19/2020 23:34 WG1429926 SC
2,6-Dinitrotoluene U 0.000279 0.0100 1 02/19/2020 23:34 WG1429926
1,2-Diphenylhydrazine U 0.000318 0.0100 1 02/19/2020 23:34 WG1429926
Fluoranthene U 0.000310 0.00100 1 02/19/2020 23:34 WG1429926
Fluorene U 0.000323 0.00100 1 02/19/2020 23:34 WG1429926
Hexachlorobenzene U 0.000341 0.00100 1 02/19/2020 23:34 WG1429926
Hexachloro-1,3-butadiene U 0.000329 0.0100 1 02/19/2020 23:34 WG1429926
Hexachlorocyclopentadiene U 0.00233 0.0100 1 02/19/2020 23:34 WG1429926
Hexachloroethane U 0.000365 0.0100 1 02/19/2020 23:34 WG1429926 ,
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 02/19/2020 23:34 WG1429926
Isophorone U 0.000272 0.0100 1 02/19/2020 23:34 WG1429926
Naphthalene U 0.000372 0.00100 1 02/19/2020 23:34 WG1429926
Nitrobenzene U 0.000367 0.0100 1 02/19/2020 23:34 WG1429926
n-Nitrosodimethylamine U 0.00126 0.0100 1 02/19/2020 23:34 WG1429926
n-Nitrosodiphenylamine U 0.00119 0.0100 1 02/19/2020 23:34 WG1429926
n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 02/19/2020 23:34 WG1429926
Phenanthrene U 0.000366 0.00100 1 02/19/2020 23:34 WG1429926
Benzylbutyl phthalate U 0.000275 0.00300 1 02/19/2020 23:34 WG1429926
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 1 02/19/2020 23:34 WG1429926
Di-n-butyl phthalate 0.000360 J 0.000266 0.00300 1 02/19/2020 23:34 WG1429926
Diethyl phthalate U 0.000282 0.00300 1 02/19/2020 23:34 WG1429926
Dimethyl phthalate U 0.000283 0.00300 1 02/19/2020 23:34 WG1429926
Di-n-octyl phthalate U 0.000278 0.00300 1 02/19/2020 23:34 WG1429926
Pyrene U 0.000330 0.00100 1 02/19/2020 23:34 WG1429926
1,2,4-Trichlorobenzene U 0.000355 0.0100 1 02/19/2020 23:34 WG1429926
4-Chloro-3-methylphenol U 0.000263 0.0100 1 02/19/2020 23:34 WG1429926
2-Chlorophenol U 0.000283 0.0100 1 02/19/2020 23:34 WG1429926
2,4-Dichlorophenol U 0.000284 0.0100 1 02/19/2020 23:34 WG1429926
2,4-Dimethylphenol U 0.000624 0.0100 1 02/19/2020 23:34 WG1429926
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 02/19/2020 23:34 WG1429926
2,4-Dinitrophenol U 0.00325 0.0100 1 02/19/2020 23:34 WG1429926
2-Nitrophenol U 0.000320 0.0100 1 02/19/2020 23:34 WG1429926
4-Nitrophenol U 0.00201 0.0100 1 02/19/2020 23:34 WG1429926
Pentachlorophenol U 0.000313 0.0100 1 02/19/2020 23:34 WG1429926
Phenol 0.00199 J 0.000334 0.0100 1 02/19/2020 23:34 WG1429926
2,4,6-Trichlorophenol U 0.000297 0.0100 1 02/19/2020 23:34 WG1429926
(5)2-Fluoropheno/ 38.6 10.0-120 02/19/2020 23:34 WG1429926
(S)Phenol-d5 27.3 8.00-424 02/19/2020 23:34 WG1429926
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 7 of 28
2020-02-13-001 SAMPLE RESULTS - 01 ONE LAB.NATIONWIDE. 10
Collected date/time: 02/13/20 09:52 L1189390
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
(S Nitrobenzene-d5 61.9 15.0-314 02/19/2020 23:34 WG1429926 2
Tc
(S 2-Fluorobiphenyl 72.7 22.0-127 02/19/2020 23:34 WG1429926
(S)2,4,6-Tribromophenol 89.0 10.0-153 02/19/2020 23:34 WG1429926 3
(S)p-Terphenyl-d14 83.4 29.0-141 02/19/2020 23:34 WG1429926 SS
4
Cn
Si
6
Qc
7
GI
8
Al
5
Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 8 of 28
o
2020-02-13-005 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE. 10
Collected date/time: 02/13/20 09:34 L1189390
Additional Information ,
Result Units Cp
Analyte
2
pH(On Site) 6 su Tc
Temperature(on-site) 12.5 Deg C
3
Ss
Gravimetric Analysis by Method 2540 D-2011
Result Qualifier MDL RDL Dilution Analysis Batch 4
Analyte mg/I mg/I mg/I date/time Cn
Suspended Solids 13.2 0.350 2.50 1 02/16/2020 00:55 WG1428711
SL
Wet Chemistry by Method 1664B
6
Result Qualifier MDL RDL Dilution Analysis Batch Qc
Analyte mg/I mg/I mg/I date/time
TPH-Oil&Grease U 0.873 6.02 1 02/18/2020 22:07 WG1430093 7 GI
Metals(ICP) by Method 200.7 8
Result Qualifier MDL RDL Dilution Analysis Batch Al
Analyte mg/I mg/I mg/I date/time
5
Copper U 0.00700 0.0100 1 02/16/2020 13:52 WG1428157 SC
Lead U 0.00200 0.00500 1 02/16/2020 13:52 WG1428157
Zinc 0.0237 J 0.00340 0.0500 1 02/16/2020 13:52 WG1428157
Volatile Organic Compounds (GC/MS) by Method 624.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Acrolein U 0.00887 0.0500 1 02/15/2020 14:01 WG1428464
Acrylonitrile U 0.00187 0.0100 1 02/15/2020 14:01 WG1428464
Benzene U 0.000331 0.00100 1 02/15/2020 14:01 WG1428464
Bromodichloromethane U 0.000380 0.00100 1 02/15/2020 14:01 WG1428464
Bromoform U 0.000469 0.00100 1 02/15/2020 14:01 WG1428464
Bromomethane U 0.000866 0.00500 1 02/15/202014:01 WG1428464
Carbon tetrachloride U 0.000379 0.00100 1 02/15/202014:01 WG1428464
Chlorobenzene U 0.000348 0.00100 1 02/15/2020 14:01 WG1428464
Chlorodibromomethane U 0.000327 0.00100 1 02/15/202014:01 WG1428464
Chloroethane U 0.000453 0.00500 1 02/15/202014:01 WG1428464
2-Chloroethyl vinyl ether U 0.00301 0.0500 1 02/15/202014:01 WG1428464
Chloroform U 0.000324 0.00500 1 02/15/202014:01 WG1428464
Chloromethane U 0.000276 0.00250 1 02/15/202014:01 WG1428464
1,2-Dichlorobenzene U 0.000349 0.00100 1 02/15/2020 14:01 WG1428464
1,3-Dichlorobenzene U 0.000220 0.00100 1 02/15/2020 14:01 WG1428464
1,4-Dichlorobenzene U 0.000274 0.00100 1 02/15/2020 14:01 WG1428464
Dichlorodifluoromethane U 0.000551 0.00500 1 02/15/2020 14:01 WG1428464
1,1-Dichloroethane U 0.000259 0.00100 1 02/15/2020 14:01 WG1428464
1,2-Dichloroethane U 0.000361 0.00100 1 02/15/2020 14:01 WG1428464
1,1-Dichloroethene U 0.000398 0.00100 1 02/15/2020 14:01 WG1428464
trans-1,2-Dichloroethene U 0.000396 0.00100 1 02/15/2020 14:01 WG1428464
1,2-Dichloropropane U 0.000306 0.00100 1 02/15/2020 14:01 WG1428464
cis-1,3-Dichloropropene U 0.000418 0.00100 1 02/15/2020 14:01 WG1428464
trans-1,3-Dichloropropene U 0.000419 0.00100 1 02/15/2020 14:01 WG1428464
Ethylbenzene U 0.000384 0.00100 1 02/15/2020 14:01 WG1428464
Methylene Chloride U 0.00100 0.00500 1 02/15/2020 14:01 WG1428464
1,1,2,2-Tetrachloroethane U 0.000130 0.00100 1 02/15/2020 14:01 WG1428464
Tetrachloroethene U J4 0.000372 0.00100 1 02/15/2020 14:01 WG1428464
Toluene U 0.000412 0.00100 1 02/15/202014:01 WG1428464
1,1,1-Trichloroethane U 0.000319 0.00100 1 02/15/202014:01 WG1428464
1,1,2-Trichloroethane U 0.000383 0.00100 1 02/15/202014:01 WG1428464
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 9 of 28
2020-02-13-005 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE. I.
Collected date/time: 02/13/20 09:34 L1189390
Volatile Organic Compounds (GC/MS) by Method 624.1
,
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
Trichloroethene U 0.000398 0.00100 1 02/15/2020 14:01 WG1428464 2Tc
Trichlorofluoromethane U 0.00120 0.00500 1 02/15/2020 14:01 WG1428464
Vinyl chloride U 0.000259 0.00100 1 02/15/2020 14:01 WG1428464 3
(S)Toluene-d8 103 80.0-120 02/15/202014:01 WG1428464 Ss
(S)4-Bromofluorobenzene 101 80.0-120 02/15/2020 14:01 WG1428464
(S)1,2-Dichloroethane-d4 100 70.0-130 02/15/2020 14:01 WG1428464 4
Cn
Pesticides (GC) by Method EPA 608.3
St
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time 6
Aldrin U 0.00000813 0.0000500 1 02/18/2020 20:21 WG1428898 QC
Alpha BHC U 0.0000166 0.0000500 1 02/18/2020 20:21 WG1428898
Beta BHC U 0.0000184 0.0000500 1 02/18/2020 20:21 WG1428898 7G1
Delta BHC U 0.0000197 0.0000500 1 02/18/2020 20:21 WG1428898
Gamma BHC U 0.0000176 0.0000500 1 02/18/2020 20:21 WG1428898
Chlordane U 0.0000977 0.000500 1 02/18/2020 20:21 WG1428898 Al
4,4-DDD U 0.0000170 0.0000500 1 02/18/2020 20:21 WG1428898
4,4-DDE U 0.0000164 0.0000500 1 02/18/2020 20:21 WG1428898 9SC
4,4-DDT U 0.0000177 0.0000500 1 02/18/2020 20:21 WG1428898
Dieldrin U 0.00000751 0.0000500 1 02/18/2020 20:21 WG1428898
Endosulfan I U 0.0000179 0.0000500 1 02/18/2020 20:21 WG1428898
Endosulfan II U 0.0000176 0.0000500 1 02/18/2020 20:21 WG1428898
Endosulfan sulfate U 0.0000196 0.0000500 1 02/18/2020 20:21 WG1428898
Endrin U 0.0000189 0.0000500 1 02/18/2020 20:21 WG1428898
Endrin aldehyde U 0.0000142 0.0000500 1 02/18/2020 20:21 WG1428898
Endrin ketone U 0.0000170 0.0000500 1 02/18/2020 20:21 WG1428898
Heptachlor U 0.0000108 0.0000500 1 02/18/2020 20:21 WG1428898
Heptachlor epoxide U 0.0000175 0.0000500 1 02/18/2020 20:21 WG1428898
Hexachlorobenzene U 0.0000134 0.0000500 1 02/18/2020 20:21 WG1428898
Methoxychlor U 0.0000193 0.0000500 1 02/18/2020 20:21 WG1428898
Toxaphene U 0.000168 0.000500 1 02/18/2020 20:21 WG1428898
(S)Decachlorobiphenyl 108 10.0-144 02/18/2020 20:21 WG1428898
(S)Tetrachloro-m-xylene 79.5 10.0-135 02/18/2020 20:21 WG1428898
Polychlorinated Biphenyls (GC) by Method EPA-608.3
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
PCB 1016 U 0.000100 0.000500 1 02/17/2020 10:25 WG1428898
PCB 1221 U 0.0000730 0.000500 1 02/17/2020 10:25 WG1428898
PCB 1232 U 0.0000420 0.000500 1 02/17/2020 10:25 WG1428898
PCB 1242 U 0.0000470 0.000500 1 02/17/2020 10:25 WG1428898
PCB 1248 U 0.0000860 0.000500 1 02/17/2020 10:25 WG1428898
PCB 1254 U 0.0000470 0.000500 1 02/17/2020 10:25 WG1428898
PCB 1260 U 0.000120 0.000500 1 02/17/2020 10:25 WG1428898
(S)Decachlorobiphenyl 105 10.0-144 02/17/2020 10:25 WG1428898
(S)Tetrachloro-m-xylene 108 10.0-135 02/17/2020 10:25 WG1428898
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch
Analyte mg/I mg/I mg/I date/time
Acenaphthene U 0.000316 0.00100 1 02/19/2020 23:54 WG1429926
Acenaphthylene U 0.000309 0.00100 1 02/19/2020 23:54 WG1429926
Anthracene U 0.000291 0.00100 1 02/19/2020 23:54 WG1429926
8enzidine U 0.00432 0.0100 1 02/19/2020 23:54 WG1429926
Benzo(a)anthracene U 0.0000975 0.00100 1 02/19/2020 23:54 WG1429926
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 10 of 28
mnimmimimmmommmommmmimmmmmimimmmimmimsmmommsmu
2020-02-13-005 SAMPLE RESULTS - 02 ONE LAB.NATIONWIDE. .4111
Collected date/time: 02/13/20 09:34 L1189390
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier MDL RDL Dilution Analysis Batch Cp
Analyte mg/I mg/I mg/I date/time
Benzo(b)fluoranthene U 0.0000896 0.00100 1 02/19/2020 23:54 WG1429926 z
Tc
Benzo(k)fluoranthene U 0.000355 0.00100 1 02/19/2020 23:54 WG1429926
Benzo(g,h,i)perylene U 0.000161 0.00100 1 02/19/2020 23:54 WG1429926 3
Benzo(a)pyrene U 0.000340 0.00100 1 02/19/2020 23:54 WG1429926 Ss
Bis(2-chlorethoxy)methane U 0.000329 0.0100 1 02/19/2020 23:54 WG1429926
Bis(2-chloroethyl)ether U 0.00162 0.0100 1 02/19/2020 23:54 WG1429926 4
Cn
2,2-0xybis(1-Chloropropane) U 0.000445 0.0100 1 02/19/2020 23:54 WG1429926
4-Bromophenyl-phenylether U 0.000335 0.0100 1 02/19/2020 23:54 WG1429926
2-Chloronaphthalene U 0.000330 0.00100 1 02/19/2020 23:54 WG1429926 Si"
4-Chlorophenyl-phenylether U 0.000303 0.0100 1 02/19/2020 23:54 WG1429926
Chrysene U 0.000332 0.00100 1 02/19/2020 23:54 WG1429926 6
Oc
Dibenz(a,h)anthracene U 0.000279 0.00100 1 02/19/2020 23:54 WG1429926
3,3-Dichlorobenzidine U 0.00202 0.0100 1 02/19/2020 23:54 WG1429926 7
2,4-Dinitrotoluene U 0.00165 0.0100 1 02/19/2020 23:54 WG1429926 GI
2,6-Dinitrotoluene U 0.000279 0.0100 1 02/19/2020 23:54 WG1429926
1,2-Diphenylhydrazine U 0.000318 0.0100 1 02/19/2020 23:54 WG1429926 &AI
Fluoranthene U 0.000310 0.00100 1 02/19/2020 23:54 WG1429926
Fluorene U 0.000323 0.00100 1 02/19/2020 23:54 WG1429926 9
Hexachlorobenzene U 0.000341 0.00100 1 02/19/2020 23:54 WG1429926 SC
Hexachloro-1,3-butadiene U 0.000329 0.0100 1 02/19/2020 23:54 WG1429926
Hexachlorocyclopentadiene U 0.00233 0.0100 1 02/19/2020 23:54 WG1429926
Hexachloroethane U 0.000365 0.0100 1 02/19/2020 23:54 WG1429926
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100 1 02/19/2020 23:54 W61429926
Isophorone U 0.000272 0.0100 1 02/19/2020 23:54 WG1429926
Naphthalene U 0.000372 0.00100 1 02/19/2020 23:54 WG1429926
Nitrobenzene U 0.000367 0.0100 1 02/19/2020 23:54 WG1429926
n-Nitrosodimethylamine U 0.00126 0.0100 1 02/19/2020 23:54 WG1429926
n-Nitrosodiphenylamine U 0.00119 0.0100 1 02/19/2020 23:54 WG1429926
n-Nitrosodi-n-propylamine U 0.000403 0.0100 1 02/19/2020 23:54 WG1429926
Phenanthrene U 0.000366 0.00100 1 02/19/2020 23:54 WG1429926
Benzylbutyl phthalate U 0.000275 0.00300 1 02/19/2020 23:54 WG1429926
Bis(2-ethylhexyl)phthalate U 0.000709 0.00300 1 02/19/2020 23:54 WG1429926
Di-n-butyl phthalate 0.000461 J 0.000266 0.00300 1 02/19/2020 23:54 WG1429926
Diethyl phthalate U 0.000282 0.00300 1 02/19/2020 23:54 WG1429926
Dimethyl phthalate U 0.000283 0.00300 1 02/19/2020 23:54 WG1429926
Di-n-octyl phthalate U 0.000278 0.00300 1 02/19/2020 23:54 WG1429926
Pyrene U 0.000330 0.00100 1 02/19/2020 23:54 WG1429926
1,2,4-Trichlorobenzene U 0.000355 0.0100 1 02/19/2020 23:54 WG1429926
4-Chloro-3-methylphenol U 0.000263 0.0100 1 02/19/2020 23:54 WG1429926
2-Chlorophenol U 0.000283 0.0100 1 02/19/2020 23:54 WG1429926
2,4-Dichlorophenol U 0.000284 0.0100 1 02/19/2020 23:54 WG1429926
2,4-Dimethylphenol U 0.000624 0.0100 1 02/19/2020 23:54 WG1429926
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 1 02/19/2020 23:54 WG1429926
2,4-Dinitrophenol U 0.00325 0.0100 1 02/19/2020 23:54 WG1429926
2-Nitrophenol U 0.000320 0.0100 1 02/19/2020 23:54 WG1429926
4-Nitrophenol U 0.00201 0.0100 1 02/19/2020 23:54 WG1429926
Pentachlorophenol U 0.000313 0.0100 1 02/19/2020 23:54 WG1429926
Phenol 0.00122 J 0.000334 0.0100 1 02/19/2020 23:54 WG1429926
2,4,6-Trichlorophenol U 0.000297 0.0100 1 02/19/2020 23:54 W61429926
(S)2-Fluorophenol 34.1 10.0-120 02/19/2020 23:54 WG1429926
(S)Phenol-d5 24.7 8.00-424 02/19/2020 23:54 WG1429926
(S)Nitrobenzene-d5 58.9 15.0-314 02/19/2020 23:54 WG1429926
(S)2-Fluorobiphenyl 67.3 22.0-127 02/19/2020 23:54 WG1429926
(S)2,4,6-Tribromophenol 81.4 10.0-153 02/19/2020 23.54 WG1429926
(S)p-Terphenyl-d14 82.6 29.0-141 02/19/2020 23:54 WG1429926
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 11 of 28
WG1428711 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. sk
Gravimetric Analysis by Method 2540 D-2011 U189390.01,02
Method Blank(MB) Cp
R3500203-1 02/16/20 00:55
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/I mg/I mg/I Tc
Suspended Solids U 0.350 2.50
'Ss
L1189293-01 Original Sample(OS)•Duplicate(DUP)
J
(OS)L1189293-01 02/16/20 00:55-(DUP)R3500203-3 02/16/20 00:55 - Cn
Original Result DUP Result Dilution DUP RPD DUP QualifierDUP RPD
Limits
Sr,
Analyte mg/1 mg/1 % %
Suspended Solids 97.6 94.4 1 3.33 5 6
Qc
L1189350-01 Original Sample(OS)•Duplicate(DUP) 'GI
(OS)L1189350-01 02/16/20 00:55•(DUP)R3500203-4 02/16/20 00:55
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
a
Lim is Al
Analyte mgA mg4 % %
Suspended Solids 37.2 41.6 1 11.2 P1 5 `Sc
Laboratory Control Sample(LCS)
(LCS)R3500203-2 02/16/20 00:55
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg4 mg/1 % %
Suspended Solids 773 816 106 85.0-115
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 14:13 12 of 28
WG1430093 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .10
Wet Chemistry by Method 16648 L1189390.01,02
Method Blank(MB)
(MB)R3500945-1 02/18/20 22:07 'Cp
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/I mgA mgA Tc
TPH-Oil&Grease U 0.725 5.00
113
Laboratory Control Sample(LCS)•Laboratory Control Sample Duplicate(LCSD)
(LCS)R3500945.2 02/18/20 22:07.(LCSD)R3500945-3 02/18/20 22:07 Cn
1
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mgA mgA % % % % % ell
TPH-Oil&Grease 20.0 18.0 17.7 90.0 88.5 64.0-132 1.68 34
12
III
Al
•
el
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 1473 13 of 28
WG1428157 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. ik
Metals(ICP)by Method 200.7 L118 9 3 90-0L02
Method Blank(MB) •
(MB)R3500314-1 02/16/2013:14 Cp
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/l mgA mgA •Tc
Copper U 0.00700 0.0100
Lead U 0.00200 0.00500 3
SS
Zinc U 0.00340 0.0500
4Cn
Laboratory Control Sample(LCS)
(LCS)R3500314-2 02/16/2013:17 ,Sr
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mgA mgA % %
Copper 1.00 0.919 91.9 85.0-115
1111
Lead 1.00 0.930 93.0 85.0-115
7
Zinc 1.00 0.934 93.4 85.0-115 GI
•
L1189408-01 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) Al
(OS)L1189408-01 02/16/2013:20•(MS)R3500314-4 02/16/20 13:25•(MSD)R3500314-5 02/16/20 13:28 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits SC
Analyte mgA mgA mg/I mg/1 % % % % %
Copper 1.00 ND 0.951 0.950 95.1 95.0 1 70.0-130 0.0250 20
Lead 1.00 ND 0.988 0.991 98.8 99.1 1 70.0-130 0.312 20
Zinc 1.00 ND 0.975 0.986 97.5 98.6 1 70.0-130 1.02 20
L1189615-02 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD)
(OS)L1189615-02 02/16/20 13:30•(MS)R3500314-6 02/16/20 13:33•(MSD)R3500314-7 02/16/20 13:35
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSO Qualifier RPD RPD Limits
Analyte mgA mg/1 mg/1 mgA % % % % %
Copper 1.00 0.0392 0.973 0.999 93.4 96.0 1 70.0-130 2.68 20
Lead 1.00 ND 0.976 1.07 97.4 100 1 70.0-130 3.07 20
Zinc 1.00 0.115 1.09 1.12 97.4 100 1 70.0-130 2.38 20
ACCOUNT: PROJECT: SDG: DATE/rIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 1413 14 of 28
WG1428464 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. JO
Volatile Organic Compounds(GC/MS)by Method 624.1 L118 9 3 90-01,02
Method Blank(MB)
(MB)R3500111-2 02/15/2011:19 Cp
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/I mg/I mg/I Tc
Acrolein U 0.00887 0.0500
Acrylonitrile U 0.00187 0.0100 3SS
Benzene U 0.000331 0.00100
Bromodlchloromethane U 0.000380 0.00100 4
Bromoform U 0.000469 0.00100 Cn
Bromomethane U 0.000866 0.00500
Carbon tetrachloride U 0.000379 0.00100 5Sr
Chlorobenzene U 0.000348 0.00100
Chlorodibromomethane U 0.000327 0.00100
Chloroethane U 0.000453 0.00500111
2-Chloroethyl vinyl ether U 0.00301 0.0500
Chloroform U 0.000324 0.00500 7Gl
Chloromethane U 0.000276 0.00250
1,2-Dichlorobenzene U 0.000349 0.00100 3
1,3-Dichlorobenzene U 0.000220 0.00100 Al
1,4-Dichlorobenzene U 0.000274 0.00100
Dichlorodifluoromethane U 0.000551 0.00500 °SC
1,1-Dichloroethane U 0.000259 0.00100
1,2-Dichloroethane U 0.000361 0.00100
1,1-Dichloroethene U 0.000398 0.00100
trans-1,2-Dichloroethene U 0.000396 0.00100
1,2-Dichloropropane U 0.000306 0.00100
cis-1,3-Dichloropropene U 0.000418 0.00100
trans-1,3-Dichloropropene U 0.000419 0.00100
Ethylbenzene U 0.000384 0.00100
Methylene Chloride U 0.00100 0.00500
1,1,2,2-Tetrachloroethane U 0.000130 0.00100
Tetrachloroethene U 0.000372 0.00100
Toluene U 0.000412 0.00100
1,1,1-Trichloroethane U 0.000319 0.00100
1,1,2-Trichloroethane U 0.000383 0.00100
Trichloroethene U 0.000398 0.00100
Trichlorofluoromethane U 0.00120 0.00500
Vinyl chloride U 0.000259 0.00100
(S)Toluene-d8 104 80.0-120
(S)4-Bromofluorabenzene 98.6 80.0-120
(S)1,2-Dichloroethane-d4 96.4 70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/201413 15 of 28
WG1428464 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE All
Volatile Organic Compounds(GC/MS)by Method 624.1 L1189390-01,02
Laboratory Control Sample(LCS)
(LCS)03500111-1 02/15/2010:17
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/I mg/ % % TC
Acroleln 0.0250 0.0198 79.2 60.0-140
Acrylonitrile 0.0250 0.0249 99.6 60.0-140 'SS
Benzene 0.00500 0.00555 111 65.0-135
Bromodichloromethane 0.00500 0.00543 109 70.0-135 a
Bromoform 0.00500 0.00556 111 70.0-130 Cn
Bromomethane 0.00500 0.00530 106 15.0-185
Carbon tetrachloride 0.00500 0.00604 121 70.0-130 Sr
Chlorobenzene 0.00500 0.00577 115 65.0-135
Chlorodibromomethane 0.00500 0.00535 107 70.0-135
^Chloroethane 0.00500 0.00416 83.2 40.0-160 QC
2-Chloroethyl vinyl ether 0.0250 0.0262 105 0.100-225
Chloroform 0.00500 0.00608 122 70.0-135 7G'
Chloromethane 0.00500 0.00446 89.2 0.100-205
1,2-Dichlorobenzene 0.00500 0.00571 114 65.0-135 8
1,3-Dichlorobenzene 0.00500 0.00556 111 70.0-130 Al
1,4-Dichlorobenzene 0.00500 0.00548 110 65.0-135
Dichlorodlfuoromethane 0.00500 0.00492 98.4 49.0-155 9SC
Ll-Dichloroethane 0.00500 0.00524 105 70.0-130
1.2-Dichloroethane 0.00500 0.00525 105 70.0-130
1,1-Dichloroethene 0.00500 0.00621 124 50.0-150
trans-1,2-Dichloroethene 0.00500 0.00575 115 70.0-130
1,2-Dichloropropane 0.00500 0.00539 108 35.0-165
cis-1.3-Dichloropropene 0.00500 0.00548 110 25.0-175
trans-1,3-Dichloropropene 0.00500 0.00543 109 50.0-150
Ethylbenzene 0.00500 0.00583 117 60.0-140
Methylene Chloride 0.00500 0.00565 113 60.0-140
1,1,2.2-Tetrachloroethane 0.00500 0.00540 108 60.0-140
Tetrachloroethene 0.00500 0.00664 133 70.0-130 J4
Toluene 0.00500 0.00575 115 70.0-130
1,1,1-Trichloroethane 0.00500 0.00593 119 70.0-130
1,1,2-Trichloroethane 0.00500 0.00566 113 70.0-130
Trichloroethene 0.00500 0.00573 115 65.0-135
Trichlorofluoromethane 0.00500 0.00569 114 50.0-150
Vinyl chloride 0.00500 0.00467 93.4 5.00-195
(5)Toluene-d8 103 80.0-120
(5)4-Bromolluorobenzene 101 80.0-120
(5)1,2-Dichloroethane-d4 9Z7 70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 14:13 16 of 28
WG1428553 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. 10
Volatile Organic Compounds(GC/MS)by Method 624.1 11189390.01
Method Blank(MB)
(MB)03500170-2 02/15/2013:59 Cp
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/1 mgfl mg/1 Tc
Tetrachloroethene U 0.000372 0.00100
(S)Toluene-d8 110 80.0-120
111
(5)4-BromoBuorobenzene 90.7 80.0-120
(S)1,2-Dichloroethane-d4 102 70.0-130
El
Laboratory Control Sample(LCS) 5Sr
(LCS)R3500170-1 02/15/20 12:59
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Ell
Analyte mgA mg/1 % %
Tetrachloroethene 0.00500 0.00510 102 70.0-130
7
(S)Toluene-d8 111 80.0-120 GI
(S)4-Bromofuorobenzene 90.6 80.0-120
(S)1,1-Dlchloroethane-d4 102 70.0-130 sAl
SC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 17 of 28
WG1428898 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. At
Pesticides(GC)by Method EPA 608.3 L1189390.01,02
Method Blank(MB)
Cp
R3501000-1 02/18/20 18:17
MB Result MB Qualifier MB MDL MB RDL 2
Analyte mg/1 mg/1 mg/i Tc
Aldrin U 0.00000813 0.0000500
Alpha BHC U 0.0000166 0.0000500 3
SS
Beta BHC U 0.0000184 0.0000500
Delta BHC U 0.0000197 0.0000500 4
Gamma BHC U 0.0000176 0.0000500 Cn
4,4-ODD U 0.0000170 0.0000500
4,4-ODE U 0.0000164 0.0000500 'Sr
4,4-DDT U 0.0000177 0.0000500
Dleldrin U 0.00000751 0.0000500
Endosulfan I U 0.0000179 0.0000500III
Endosulfan II U 0.0000176 0.0000500
Endosulfan sulfate U 0.0000196 0.0000500
CI
Endrin U 0.0000189 0.0000500
Endrin aldehyde U 0.0000142 0.0000500 a
Endrin ketone U 0.0000170 0.0000500 Al
Heptachlor U 0.0000108 0.0000500
Heptachlor epoxide U 0.0000175 0.0000500
Hexachlorobenzene U 0.0000134 0.0000500 el
Methoxychlor U 0.0000193 0.0000500
Chlordane U 0.0000977 0.000500
Toxaphene U 0.000168 0.000500
(S)Decachlorobiphenyl 87.0 10.0-144
(5)Tetrochloro-m-xyylene 86.5 10.0-135
Laboratory Control Sample(LCS)
(LCS)R3501000-2 02/18/20 18:29
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/1 mg/I % %
Aldrin 0.00100 0.000654 65.4 42.0-140
Alpha BHC 0.00100 0.000797 79.7 37.0-140
Beta BHC 0.00100 0.000845 84.5 17.0-147
Delta BHC 0.00100 0.000817 81.7 19.0-140
Gamma BHC 0.00100 0.000818 81.8 32.0-140
4,4-0DD 0.00100 0.0007E19 78.9 31.0-141
4,4-ODE 0.00100 0.000741 74.1 30.0-145
4,4-DDT 0.00100 0.000772 77.2 25.0-160
Dieklrin 0.00100 0.000811 81.1 36.0-146
Endosulfan I 0.00100 0.000858 85.8 45.0-153
ACCOUNT: PROJECT: SOD: DATE/ONE: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 18 of 28
WG1428898 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Ilk
Pesticides(GC)by Method EPA 608.3 L1189390-01,02
Laboratory Control Sample(LCS)
(LCS)R3501000-2 02/18/20 18:29 Cp
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 2
Analyte mgA mgA % % Tc
Endosulfan II 0.00100 0.000'842 84.2 1.00-202
Endosulfan sulfate 0.00100 0.000789 78.9 26.0-144
el
Endrin 0.00100 0.000791 79.1 30.0-147
Endrin aldehyde 0.00100 0.000716 71.6 56.0-128
Endrin ketone 0.00100 0.000848 84.8 54.0-142El
Heptachlor 0.00100 0.000668 66.8 34.0-140
Heptachlor epoxide 0.00100 0.000836 83.6 37.0-142 s
Sr
Hexachlorobenzene 0.00100 0.000718 71.8 35.0-120
Methoxychlor 0.00100 0.000706 70.6 44.0-160
(S)Decachbrobiphenyl 89.5 10.0-144III
(S)Tel rochloro-m-xylene 76.6 10.0-135
7
GI
L1189247-01 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) 3
(OS)L1189247-01 02/18/2018:54•(MS)03501000-3 02/18/2019:06•(MSD)83501000-4 02/18/2019:19 Al
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
'
Analyte mgA mgA mgA mgA % % % % % SC
Aldrin 0.00100 ND 0.000786 0.000807 78.6 80.7 1 42.0-140 2.64 35
Alpha BAC 0.00100 ND 0.000870 0.000902 87.0 90.2 1 37.0-140 3.61 36
Beta BHC 0.00100 ND 0.000918 0.000955 91.8 95.5 1 17.0-147 3.95 44
Delta BHC 0.00100 ND 0.000825 0.000868 82.5 86.8 1 19.0-140 5.08 52
Gamma BHC 0.00100 ND 0.000861 0.000925 86.1 92.5 1 32.0-140 7.17 39
4,4-0DD 0.00100 ND 0.000829 0.000908 82.9 90.8 1 31.0-141 9.10 39
4,4-DDE 0.00100 ND 0.000754 0.000825 75.4 82.5 1 30.0-145 8.99 35
4,4-001 0.00100 ND 0.000896 0.000949 89.6 94.9 1 25.0-160 5.75 42
Dleldrin 0.00100 ND 0.000855 0.000893 85.5 89.3 1 36.0-146 4.35 49
Endosulfan I 0.00100 ND 0.000986 0.00104 98.6 104 1 45.0-153 5.33 28
Endosulfan II 0.00100 ND 0.000873 0.000908 87.3 90.8 1 1.00-202 3.93 53
Endosulfan sulfate 0.00100 ND 0.000840 0.000938 84.0 93.8 1 26.0-144 11.0 38
Endrin 0.00100 ND 0.000891 0.000952 89.1 95.2 1 30.0-147 6.62 48
Endrin aldehyde 0.00100 ND 0.000745 0.000793 74.5 79.3 1 56.0-128 6.24 20
Endrin ketone 0.00100 ND 0.000930 0.000967 93.0 96.7 1 54.0-142 3.90 20
Heptachlor 0.00100 ND 0.000829 0.000840 82.9 84.0 1 34.0-140 1.32 43
Heptachlor epoxide 0.00100 ND 0.000879 0.000900 87.9 90.0 1 37.0-142 2.36 26
Hexachlorobenzene 0.00100 ND 0.000821 0.000916 82.1 91.6 1 35.0-120 '10.9 25
Methoxychlor 0.00100 ND 0.000851 0.00121 85.1 121 1 44.0-160 J3 34.8 22
(5)Decochlorob/phenyl 76.2 8Z5 10.0-144
(5)Tetrochbro-m-xylene 80.9 84.2 10.0-135
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 19 of 28
WG1428898 QUALITY CONTROL SUMMARY ONE LAB NATIONWIDE. SI
Polychlorinated Biphenyls(GC)by Method EPA-608.3 Ltt89390.01,02
Method Blank(MB)
(MB)R3500482-2 02/17/20 07:09 Cp
MB Result MB Qualifier MB MDL MB RDL
Analyte mgA mg/1 mg/I TC
PCB 1260 U 0.000120 0.000500
PCB 1016 U 0.000100 0.000500 3
SS
PCB 1221 U 0.0000730 0.000500
PCB 1232 U 0.0000420 0.000500 4
PCB 1242 U 0.0000470 0.000500 Cn
PCB 1248 U 0.0000860 0.000500
PCB 1254 U 0.0000470 0.000500 SrS
(S)Decochloroblphenyl 86.2 10.0-144
(5)Telrachloro-m-xylene 103 10.0-135
III
Laboratory Control Sample(LCS) 7GI
(LCS)R3500482-1 02/17/20 06:55
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier Al_
Analyte mgA mg4 % %
PCB 1260 0.00250 0.00247 98.8 8.00-140
•
PCB 1016 0.00250 0.00315 126 50.0-140 SC
(5)Decachloroblphenyl 69.2 10.0-144
(5)Telrochloro-m-xylene 94.0 10.0-135
L1189247-01 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD)
(OS)L1189247-01 02/17/20 08:33•(MS)R3500482-3 02/17/20 08:47•(MSD)R3500482-4 02/17/20 09:01
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/1 mg/1 mgA mg/1 % % % % %
PCB 1260 0.00250 ND. 0.00282 0.00321 113 128 1 8.00-140 12.9 38
PCB 1016 0.00250 ND 0.00564 0.00630 226 252 1 50.0-140 J5 P J5 P 11.1 36
(5)Decachloroblphenyl 815 79.5 10.0-144
(5)Tetrachloro-m-xylene 109 104 10.0-135
ACCOUNT: PROJECT: SOS: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 14:13 20 of 28
WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. It
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L118 9 3 90-01,02
Method Blank(MB)
(MB)R3501438-2 02/19/20 23:46 Cp
MB Result MB Qualifier MB MDL MB RDL
2
Analyte mg/1 mg/I mg/1 Tc
Acenaphthene U 0.000316 0.00100
Acenaphthylene U 0.000309 0.00100 3
SS
Anthracene U 0.000291 0.00100
Benzldine U 0.00432 0.0100 4
Benzo(ajanthracene U 0.0000975 0.00100 Cn
8enzo(b)fluoranthene U 0.0000896 0.00100
Benzo(k)fluoranthene U 0.000355 0.00100 5Sr
Benzo(g,h,i)perylene U 0.000161 0.00100
Benzo(ajpyrene U 0.000340 0.00100 •
81s(2-chlorethoxy)methane U 0.000329 0.0100IIII
Bis(2-chloroethyl)ether U 0.00162 0.0100
2,2-0xybis(1-Chloropropane) U 0.000445 0.0100
GI
4-Bromophenyl-phenylether U 0.000335 0.0100
2-Chloronaphthalene U 0.000330 0.00100
,
4-Chlorophenyl-phenylether U 0.000303 0.0100 Al
Chrysene U 0.000332 0.00100
Dibenz(a,h)anthracene U 0.000279 0.00100 SC
3,3-Dichlorobenzidine U 0.00202 0.0100
2.4-Dinitrotoluene U 0.00165 0.0100
2,6-Dinitrotoluene U 0.000279 0.0100
Fluoranthene U 0.000310 0.00100
Fluorene U 0.000323 0.00100
Hexachlorobenzene U 0.000341 0.00100
Hexachloro-1,3-butadiene U 0.000329 0.0100
Hexachlorocyclopentadiene U 0.00233 0.0100
Hexachloroethane U 0.000365 0.0100
Indeno(1,2,3-cd)pyrene U 0.000279 0.00100
Isophorone U 0.000272 0.0100
Naphthalene U 0.000372 0.00100
Nitrobenzene U 0.000367 0.0100
n-Nitrosodimethylamine U 0.00126 0.0100
n-Nitrosodiphenylamine U 0.00119 0.0100
n-Nitrosodi-n-propylamine U 0.000403 0.0100
Phenanthrene U 0.000366 0.00100
Benzylbutyl phthalate U 0.000275 0.00300
Bis)2ethylhexyl)phthalate U 0.000709 0.00300
Dl-n-butyl phthalate U 0.000266 0.00300
Diethyl phthalate U 0.000282 0.00300
Dimethyl phthalate U 0.000283 0.00300
Di-n-octyl phthalate U 0.000278 0.00300
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 21 of 28
WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. ilk
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L118 9 3 90-01,02
Method Blank(MB)
(MB)R3501438-2 02/19/20 23:46 Cp
MB Result MB Qualifier MB MDL MB RDL
Analyte mgA mgA mg/1 2Tc
Pyrene U 0.000330 0.00100
1,2.4-Trichlorobenzene U 0.000355 0.0100 3Ss
4-Chloro-3-methylphenol U 0.000263 0.0100
2-Chorophenol U 0.000283 0.0100 4
2,4-Dichlorophenol U 0.000284 0.0100 Cn
2,4-Dimethylphenol U 0.000624 0.0100
4,6-Dinitro-2-methylphenol U 0.00262 0.0100 5
Sr
2,4-Dinitrophenol U 0.00325 0.0100
2-Nitrophenol U 0.000320 0.0100
4-Nitrophenol U 0.00201 0.0100IIII
Pentachlorophenol U 0.000313 0.0100
Phenol U 0.000334 0.0100 7G1
2,4,6-Trlchlorophenol U 0.000297 0.0100
Azobenzene U 0.000318 0.0100 3
(5)2-Fluorophenol 42.1 10.0-120 Al
(5)Phenol-d5 26.6 8.00-424
(5)Nitro benzene-d5 60.9 15.0-314 Sc9
(5)2-Fluorobiphenyl 70.6 22.0-127
(5)24,6-Tribromophenol 685 10.0-153
(S)p-Terphenyl-d14 83.1 29.0-141
Laboratory Control Sample(LCS)
(LCS)83501438-1 02/19/20 23:26
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mgA mg/ % %
Acenaphthene 0.0500 0.0382 76.4 47.0-145
Acenaphthylene 0.0500 0.0406 81.2 33.0-145
Anthracene 0.0500 0.0391 78.2 27.0-133
Benzldine 0.100 0.0244 24.4 1.00-120
Benzo(a)anthracene 0.0500 0.0413 82.6 33.0-143
Benzo(b)fluoranthene 0.0500 0.0439 87.8 24.0-159
Benzo(k)Buoranthene 0.0500 0.0408 81.6 11.0-162
Benzo(g,h,i)perylene 0.0500 0.0390 78.0 1.00-219
Benzo(a)pyrene 0.0500 0.0433 86.6 17.0-163
Bis(2-chlorethoxy)methane 0.0500 0.0335 67.0 1.00-219
Bis(2-chloroethyl)ether 0.0500 0.0381 76.2 33.0-185
2,2-0lrybis(1-Chloropropane) 0.0500 0.0358 71.6 36.0-166
4-Bromophenyl-phenylether 0.0500 0.0398 79.6 53.0-127
ACCOUNT: PROJECT: MG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 14:13 22 of 28
WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 12189390-01,02
Laboratory Control Sample(LCS)
(LCS)93501438-1 02/19/20 23:26 Cp
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier 2
Analyte mgA mgA % % Tc
2-Chloronaphthalene 0.0500 0.0369 73.8 60.0-120
4-Chlorophenyl-phenylether 0.0500 0.0405 81.0 25.0-158 'SS
Chrysene 0.0500 0.0395 79.0 17.0-168
Dibenz(a,h)anthracene 0.0500 0.0411 82.2 1.00-227
3,3-Dichlorobenzidine 0.100 0.0800 80.0 1.00-262111
2.4-Dinitrotoluene 0.0500 0.0436 87.2 39.0-139
2,6-Dlnitrotoluene 0.0500 0.0420 84.0 50.0-158 5Sr
Fluoranthene 0.0500 0.0421 84.2 26.0-137
Fluorene 0.0500 0.0402 80.4 59.0-121
Hexachlorobenzene 0.0500 0.0398 79.6 1.00-152III
Hexachloro-1,3-butadiene 0.0500 0.0323 64.6 24.0-120
Hexachlorocyclopentadlene 0.0500 0.0275 55.0 10.0-120 2Gl
Hexachloroethane 0.0500 0.0335 67.0 40.0-120
Indeno(1,2,3-cd)pyrene 0.0500 0.0403 80.6 1.00-171 a
Isophorone 0.0500 0.0358 71.6 21.0-196 Al
Naphthalene 0.0500 0,0330 66.0 21.0-133
Nitrobenzene 0.0500 0.0332 66.4 35.0-180 9
SC
n-Nitrosodimethylamine 0.0500 0.0252 50.4 10.0-120
n-Nitrosodiphenylamine 0.0500 0.0392 78.4 44.0-120
n-Nitrosodi-n-propylamine 0.0500 0.0401 80.2 1.00-230
Phenanthrene 0.0500 0.0396 79.2 54.0-120
Benzylbutyl phthalate 0.0500 0.0438 87.6 1.00-152
Bis(2ethylhexyl)phthalate 0.0500 0.0430 86.0 8.00-158
Di-n-butyl phthalate 0.0500 0.0439 87.8 1.00-120
Diethyl phthalate 0.0500 0.0432 86.4 1.00-120
Dimethyl phthalate 0.0500 0.0412 82.4 1.00-120
Di-n-octyl phthalate 0.0500 0.0425 85.0 4.00-146
Pyrene 0.0500 0.0418 83.6 52.0-120
1,2,4-Trlchlorobenzene 0.0500 0.0323 64.6 44.0-142
4-Chloro-3-methylphenol 0.0500 0.0341 68.2 22.0-147
2-Chlorophenol 0.0500 0.0334 66.8 23.0-134
14-Dichlorophenol 0.0500 0.0343 68.6 39.0-135
2,4-Dlmethylphenol 0.0500 0.0349 69.8 32.0-120
4,6-Dinitro-2-methylphenol 0.0500 0.0428 85.6 1.00-181
2.4-Dinitrophenol 0.0500 0.0436 87.2 1.00-191
2-Nitrophenol 0.0500 0.0354 70.8 29.0-182
4-Nitrophenol 0.0500 0.0170 34.0 1.00-132
Pentachlorophenol 0.0500 0.0491 98.2 14.0-176
Phenol 0.0500 0.0152 30.4 5.00-120
2,4,6-Trichlorophenol 0.0500 0.0382 76.4 37.0-144
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/201413 23 of 28
WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. Ilk
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L1189390-01,02
Laboratory Control Sample(LCS)
(LCS)R3501438-1 02/19/20 23:26 Cp
Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier
Analyte mg/1 mg/I % % �Tc
Azobenzene 0.0500 0.0412 82.4 37.0-125
(5)2-Fluorophenol 46.3 10.0-120
SS
(S)Phenol-d5 29.3 8.00-424
(S)Nitrobenzene-d5 569 15.0-314 4
(5)2-Fluorobiphenyl 76.3 22.0-127 Cn
(5)2,4,6-Tribromophenol 78.0 10.0-153
(S)p-Terphenyl-d14 84.6 29.0-141
Sr
L1189427-05 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD) 11111
(OS)L1189427-05 02/20/20 00:47•(MS)R3501438-3 02/20/20 01:08•(MSD)R3501438-4 02/20/20 01:28
7
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits GI
Analyte mg/I mg/I mg/I mg/I % % % % %
Acenaphthene 0.0500 ND 0.0355 0.0382 71.0 76.4 1 47.0-145 7.33 48 JAI
Acenaphthylene 0.0500 ND 0.0381 0.0413 76.2 82.6 1 33.0-145 8.06 74
Anthracene 0.0500 ND 0.0384 0.0397 76.8 79.4 1 27.0-133 3.33 66
8enzidine 0.100 ND 0.0597 0.0224 59.7 22.4 1 1.00-120 J3 90.9 40 -SC
Benzo(a)anthracene 0.0500 ND 0.0406 0.0424 81.2 84.8 1 33.0-143 4.34 53
Benzo(b)Buoranthene 0.0500 ND 0.0423 0.0428 84.6 85.6 1 24.0-159 1.18 71
Benzo(k)Buoranthene 0.0500 ND 0.0394 0.0411 78.8 82.2 1 11.0-162 4.22 63
Benzo(g.h,i)perylene 0.0500 ND 0.0380 0.0399 76.0 79.8 1 1.00-219 4.88 97
Benzo(a)pyrene 0.0500 ND 0.0422 0.0436 84.4 87.2 1 17.0-163 3.26 72
Bis(2-chlorethox)r)methane 0.0500 ND 0.0314 0.0331 62.8 66.2 1 33.0-184 5.27 54
Bis(2-chloroethyl)ether 0.0500 ND 0.0353 0.0366 70.6 73.2 1 12.0-158 3.62 108
2,2-Oxybis(1-Chloropropane) 0.0500 ND 0.0334 0.0343 66.8 68.6 1 36.0-166 2.66 76
4-Bromophenyl-phenylether 0.0500 ND 0.0385 0.0398 77.0 79.6 1 53.0-127 3.32 43
2-Chloronaphthalene 0.0500 ND 0.0348 0.0385 69.6 77.0 1 60.0-120 10.1 24
4-Chlorophenyl-phenylether 0.0500 ND 0.0375 0.0407 75.0 81.4 1 25.0-158 8.18 61
Chrysene 0.0500 ND 0.0379 0.0398 75.8 79.6 1 17.0-168 4.89 87
Dibenz(a,h)anthracene 0.0500 ND 0.0394 0.0418 78.8 83.6 1 1.00-227 5.91 126
3,3-Dichlorobenzidine 0.100 ND 0.0792 0.0813 79.2 81.3 1 1.00-262 2.62 108
2.4-Dinitrotoluene 0.0500 ND 0.0416 0.0448 83.2 89.6 1 39.0-139 7.41 42
2,6-Dinitrotoluene 0.0500 ND 0.0394 0.0424 78.8 84.8 1 50.0-158 7.33 48
1,2-Diphenylhydrazine 0.0500 ND 0.0392 0.0413 78.4 82.6 1 18.0-156 5.22 34
Fluoranthene 0.0500 ND 0.0415 0.0428 83.0 85.6 1 26.0-137 3.08 66
Fluorene 0.0500 ND 0.0376 0.0409 75.2 81.8 1 59.0-121 8.41 38
Hexachlorobenzene 0.0500 ND 0.0382 0.0400 76.4 80.0 1 1.00-152 4.60 55
Hexachloro-1,3-butadiene 0.0500 ND 0.0322 0.0339 64.4 67.8 1 24.0-120 5.14 62
Hexachlorocyclopentadiene 0.0500 ND 0.0277 0.0301 55.4 60.2 1 10.0-146 8.30 34
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 14:13 24 of 28
WG1429926 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. .110
Semi Volatile Organic Compounds (GC/MS)by Method 625.1 L1189390.01,02
L1189427-05 Original Sample(OS)•Matrix Spike(MS)•Matrix Spike Duplicate(MSD)
(OS)L1189427-05 02/20/20 00:47•(MS)R3501438-3 02/20/20 01:08•(MSD)R3501438-4 02/20/20 01:28 Cp
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits
.Analyte mgll mgll mg/1 mg9 % % % % % Tc
Hexachloroethane 0.0500 ND 0.0335 0.0345 67.0 69.0 1 40.0-120 2.94 52
Indeno(1,2,3-cd)pyrene 0.0500 ND 0.0391 0.0407 78.2 81.4 1 1.00-171 4.01 99 3
SS
Isophorone 0.0500 ND 0.0334 0.0353 66.8 70.6 1 21.0-196 5.53 93
Naphthalene 0.0500 ND 0.0313 0.0331 62.6 66.2 1 21.0-133 5.59 65 4
Nitrobenzene 0.0500 ND 0.0319 0.0337 63.8 67.4 1 35.0-180 5.49 62 Cn
n-Nltrosodimethylamine 0.0500 ND 0.0256 0.0260 51.2 52.0 1 10.0-120 1.55 40
n-Nltrosodiphenylamine 0.0500 ND 0.0378 0.0391 75.6 78.2 1 16.0-160 3.38 28 s
Sr
n-Nitrosodi-n-propylamine 0.0500 ND 0.0360 0.0382 72.0 76.4 1 1.00-230 5.93 87
Phenanthrene 0.0500 ND 0.0392 0.0403 78.4 80.6 1 54.0-120 2.77 39
Benzylbutyl phthalate 0.0500 ND 0.0422 0.0434 84.4 86.8 1 1.00-152 2.80 60Fl
Bis(2-ethylhexy)phthalate 0.0500 ND 0.0408 0.0420 81.6 84.0 1 8.00-158 2.90 82
Dl-n-butyl phthalate 0.0500 ND 0.0428 0.0433 85.6 86.6 1 1.00-120 1.16 47
Diethyl phthalate 0.0500 ND 0.0405 0.0426 81.0 85.2 1 1.00-120 5.05 100 CI
Dimethyl phthalate 0.0500 ND 0.0391 0.0410 78.2 82.0 1 1.00-120 4.74 183 a
Di-n-octyl phthalate 0.0500 ND 0.0406 0.0425 81.2 85.0 1 4.00-146 4.57 69 Al
Pyrene 0.0500 ND 0.0406 0.0412 81.2 82.4 1 52.0-120 1.47 49
1,2,4-Trlchlorobenzene 0.0500 ND 0.0316 0.0329 63.2 65.8 1 44.0-142 4.03 50 9Sc
4-Chloro-3-methylphenol 0.0500 ND 0.0322 0.0337 64.4 67.4 1 22.0-147 4.55 73
2-Chlorophenol 0.0500 ND 0.0326 0.0343 65.2 68.6 1 23.0-134 5.08 61
2,4-Dichlorophenol 0.0500 ND 0.0326 0.0344 65.2 68.8 1 39.0-135 5.37 50
2,4-Dimethylphenol 0.0500 ND 0.0334 0.0360 66.8 72.0 1 32.0-120 7.49 58
4,6-Dinitro-2-methylphenol 0.0500 ND 0.0423 0.0442 84.6 88.4 1 1.00-181 4.39 203
2.4-Dinitrophenol 0.0500 ND 0.0423 0.0455 84.6 91.0 1 1.00-191 7.29 132
2-N6rophenol 0.0500 ND 0.0334 0.0353 66.8 70.6 1 29.0-182 5.53 55
4-Nltrophenol 0.0500 ND 0.0178 0.0187 35.6 37.4 1 1.00-132 4.93 131
Pentachlorophenol 0.0500 ND 0.0476 0.0494 95.2 98.8 1 14.0-176 3.71 86
Phenol 0.0500 ND 0.0154 0.0162 30.8 32.4 1 5.00-120 5.06 64
2,4,6-Trichlorophenol 0.0500 ND 0.0368 0.0401 73.6 80.2 1 37.0-144 8.58 58
(S)2-Fluorophenol 45.7 49.4 10.0-120
(5)Phenol-d5 30.0 315 8.00-424
(5)Nitrobenzene-6 53.1 56.7 15.0-314
(S)2-Fluorobipheny/ 712 78.1 22.0-127
(5)2,4,6-Tribromophenol 76.5 81.0 10.0-153
(S)p-Terphenyl-d14 82.6 83.5 29.0-141
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/20 14:73 25 of 28
GLOSSARY OF TERMS ONE LAB.NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not Cp
intended as a comprehensive explanation,and if you have additional questions please contact your project representative.
z
Results Disclaimer-Information that may be provided by the customer,and contained within this report,include Permit Limits,Project Name, TC
Sample ID,Sample Matrix,Sample Preservation,Field Blanks,Field Spikes,Field Duplicates,On-Site Data,Sampling Collection Dates/Times,and
Sampling Location.Results relate to the accuracy of this information provided,and as the samples are received.
3
Abbreviations and Definitions Ss
MDL Method Detection Limit.
4
ND Not detected at the Reporting Limit(or MDL where applicable). Cn
RDL Reported Detection Limit.
Rec. Recovery. -
Sr
RPD Relative Percent Difference.
SDG Sample Delivery Group.
Surrogate(Surrogate Standard)-Analytes added to every blank,sample,Laboratory Control Sample/Duplicate and Qc
(S) Matrix Spike/Duplicate;used to evaluate analytical efficiency by measuring recovery.Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit(or MDL where applicable). GI
Analyte The name of the particular compound or analysis performed.Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material,the sample preparation volume or weight values differ from the Al
Dilution standard,or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report,the sample may be diluted for analysis.If a value different than 1 is used in this field,the
result reported has already been corrected for this factor.
These are the target%recovery ranges or%difference value that the laboratory has historically determined as normal SC
Limits for the method and analyte being reported.Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference(RPD)from a quality control
sample.The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported.If a Qualifier is present,a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result(corrected for any sample specific characteristics)reported for your sample.If there was
no measurable result returned for a specific analyte,the result in this column may state"ND"(Not Detected)or"BDL"
Result (Below Detectable Levels).The information in the results column should always be accompanied by either an MDL
(Method Detection Limit)or RDL(Reporting Detection Limit)that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results,including a discussion of any non-conformances to protocol
Case Narrative(Cn) observed either at sample receipt by the laboratory from the field or during the analytical process.If present,there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
• This section of the report includes the results of the laboratory quality control analyses required by procedure or
Quality Control
Summary(Qc) analytical methods to assist in evaluating the validity of the results reported for your samples.These analyses are not
being performed on your samples typically,but on laboratory generated material.
This is the document created in the field when your samples were initially collected.This is used to verify the time and
Sample Chain of date of collection,the person collecting the samples,and the analyses that the laboratory is requested to perform.This
Custody(Sc) chain of custody also documents all persons(excluding commercial shippers)that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples.These results are provided
Sample Results(Sr) by sample ID and are separated by the analyses performed on each sample.The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary(Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID,including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable;the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J5 The sample matrix interfered with the ability to make any accurate determination;spike value is high.
P RPD between the primary and confirmatory analysis exceeded 40%.
P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 26 of 28
ACCREDITATIONS & LOCATIONS ONE LAB.NATIONWIDE. 40
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location.One phone call,one point of contact,one laboratory.No other lab is as
accessible or prepared to handle your needs throughout the country.Our capacity and capability from our single location laboratory is comparable to the collective totals of the network 1
laboratories in our industry.The most significant benefit to our one location design is the design of our laboratory campus.The model is conducive to accelerated productivity,decreasing C p
turn-around time,and preventing cross contamination,thus protecting sample integrity.Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
"Not all certifications held by the laboratory are applicable to the results reported in the attached report.
•Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. 2
Tc
State Accreditations
3
Alabama 40660 Nebraska NE-OS-15-05 SS
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
4
Arkansas 88-0469 New Jersey—NELAP TN002 Cn
California 2932 New Mexico' n/a
Colorado TN00003 New York 11742
5
Connecticut PH-0197 North Carolina Env375 Sr
Florida E87487 North Carolina' DW21704
Georgia NELAP North Carolina' 41
6
Georgia' 923 North Dakota R-140 Qc
Idaho TN00003 Ohio—VAP CL0069
Illinois 200008 Oklahoma 9915
7
Indiana C-TN-01 Oregon TN200002 GI
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LA000356
Kentucky'6 90010 South Carolina 84004 Al
Kentucky 2 16 South Dakota n/a
Louisiana A130792 Tennessee'` 2006
l
Louisiana' LA180010 Texas T10 47 0 4 2 4 5-18-15 SC
Maine TN0002 Texas LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA
Third Party Federal Accreditations
A2LA—ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA—ISO 17025 5 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
'Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity `Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies.If you would like assistance from one of our support offices,please contact
our main office.Pace National performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Eaton Corporation 28091-R L1189390 02/20/2014:13 27 of 28
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