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HomeMy WebLinkAboutWQ0001861_Monitoring - 02-2020_20200318SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT,OFENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -IN FORMATION PROCESSING UNIT COMPLIANCE REPORT FORM � 1617 MAIL, SERVICE CENTER,RALEIGH, NC 27699-1617 Phone: (919) 733-3221 Please Print ClearlyT FACILITY INFORMATIOnN or Type PERMIT Number: Expiration Date: A / Facility Name: \s-ttser.1/ e M Non -Discharge W 0, IWO I Wd U I C Permit Name (if different): NPDES Other Facility Address: l S 1 gacKL't Keftd _ TYPE OF PERMITTED OPERATION BEING MONITORED IKLagoon ❑ Remediation: Infiltration Gallery NC Z RY5 % County t"5 it X ci,ti, s)nl?(zit') ❑ Spray Field ❑ Remediation: Contact Person: A41r. 9-9"Ill r- VAWA N Telephone#: 900 - 6y% 7278 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): M w" 2 Date sample collected: Z - 2% `20 FIELD ANALYSES WAS Well Depth: IL4 ft. Well Diameter: Z in. pH S tek_unniits Temp. �6•�/ °C DRY at Depth to Water Level: .SZ ft. below measuring point Screened Interval: to ZI_y ft. Spec. Cond. µMhos time of __&_ft. sampling, Measuring Point is 1• i ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 19 gallons Appearance here: ElSamples for metals were collected unfiltered: EYES El NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Z-Z 8 , 2•2!_ 140 ;•2.2 O p Laboratory Name: TA(-e "4s Certification No. In PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I MES Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Zn -Zinc mg/I Coliform: MF Total /100ml Phosphorus: (Note: Use MPN method for highly turbid samples)L Total as P mg/I R� G ' ' Orthophosphate nifl mg/I Other (Specify Compounds and ConcentA&2u5it292AW Dissolved Solids: Total su 000 al Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I T mg/I Ca - Calcium mg/I m S AS :yp Chlor g/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils c mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) P g/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate G�'Jr9Gr30G mg/I Hg - Mercury mg/I Report Attached? � Yes (1) El No (0) Specific Conductance µMhos K - Potassium mg/I VOC Z A/ D method # 67d0 A Total Ammonia mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or AuthorizA ^�Me and Title - Please print or type GW-59 Rev.1/2007 Signature of Permittee (or Authorized Aqent) _Il (Date) el IMAM enoen nni VrI I nlAl 134PPP nMl V UNDWATER QUALITY MONITORING: PLIANCE REPORT FORM TY INFORMATION Please Print Clearly or Type Name: Grtwy Poole v4gme-k¢ 4w.4.q Name (if different): Address: 151 &&t Vkw- Qswj (Sk.el) NC z e`!S l County (Slate) (zip) IContact Person: e"'.01 a Telephone#: M!O- 6Y/-7i71 Well Location/Site Name: No. of wells to be sampled: 3_ :SOURCES' OCESSING.UNIT 9-1617' Phone: (919)733-3221 PERMIT Number: Expiration Date: Non -Discharge WfA 111100 1^1 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL SAMPLING INFORMATION WELL ID NUMBER (from Permit): /M w- 3 Date sample collected: 2.27` 2b FIELD ANALYSED�: WAS Well Depth: Weil Diameter: min, pH S-2L unTts4 Temp. % y y °C DRY at time of _V Depth to Water Level: —!ft. below measuring point Screened Interval: ft. to t7 ft. Spec. Cond. µMhos sampling, Measuring Point is 2-1 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 6 gallons Appearance here: ❑ Samoles for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑YES ❑ NO LHCSVKHIVKT IIVFVKIVIHIIVIV Date sample analyzed: 2-2 #� Y-?!� 1-1- ; 'L-?D Laboratory Name: Aft G�f Certification No. '�c PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Zn -Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate b-Ii7 mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 01?0 7- L All - Aluminum —mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I ND Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? 19 Yes (1) ❑ No (0) 62ob B Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L vVt, Kerllovd) io t;W-5a Kev. wzuut ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: 1 Permit Name (if different): Facility Address: is SUBMIT FORM ON YELLOW PAPER ONLY NC Z W5/ County ICiiy( (siatr:) (ZIP) itact Person: A,. RVW~: e, 11*vILN Telephone#: II Location/Site Name: No. of wells to be sampled: ]EPARTMENT,OF ENVIRONMENT & NATURAL RESOURCES 71VISION"OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 PERMIT Number: Expiration Date: Non -Discharge IAVbw Ifil UIC NPDES Other 'PE OF PERMITTED OPERATION BEING MONITORED 71 Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): -M tv--y Date sample collected: Well Depth: Z2.& ft. Well Diameter: 2 in. Depth to Water Level: s•(, g p �, 6 p ft. below measuring point Screened Interval: ft. to2?• ft. Measuring Point is Z • 1 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: _gallons Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO FIELD ANALYSEtS�: pH j;_U_f its Sec. Cond. p Odor Appearance Temp. S-s °C µ Mhos If WELL WAS DRY at time of sampling, check here: ❑ LABORATORY INFORMATION Date sample analyzed: Z.Zy. - 2 -Zl. ; -1 , 4 -2 -20 p LaboratoryName: PA[f �+r5 Certification No. 3 �S PARAMETERS NOTE: Values should r fl ct d olved and colloidal concentrations. COD mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/1 Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) 410L Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total IZI Qsrlt Al -Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC mg/I Ca - Calcium mg/I J&A5, Chloride mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/1 Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? K Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/1 VOC : JV0 method # IDp 6 Total Ammonia mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Ferm(ttee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.1/2007 Siqnature of (Date) GW-59A COMPLIANCE REPORT FORM Permit 000 161 41 (Submit one each monitoring period with G6i=59 forms-) 1 Enter date monitoring results were due.( •Io Iv) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO iF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office forguidance. X 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided belov✓: X 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES" list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO". monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subiect the permittee to a Notice of Violation fines, and/or penalties. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the Information submitted r►�thIs report (Compliance Report,GW-59A} Is, true and complete to the"best of my knowledge Cif WAI- 3 -13-zo Signature of Permittee (or Authorized Agent) Date CW-59A 12/8/2003 q eAnalytical Center for Testing &Innovation ANALYTICAL REPORT March 05, 2020 F 7C I qS Soil & Env. Consultants - Raleigh, NC [Cn] Sample Delivery Group: L1193924 Samples Received: 02/28/2020 FSr Project Number: GW-1 1061-200 Description: Groundwater Job #1061 E Report To: Mr. Don Wells 1E 8412 Falls of Neuse Road, Suite 104 Al Raleigh, NC 27615-3543 FSCI Entire Report Reviewed By Jason Romer Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/20 13:37 1 of 23 v ' TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 MW-2A L1193924-01 5 MW-3 L1193924-02 7 MW-4A L1193924-03 9 TRIP BLANK L1193924-04 11 Qc: Quality Control Summary 13 Gravimetric Analysis by Method 2540 C-2011 13 Wet Chemistry by Method 4500P E-2011 14 Wet Chemistry by Method 5540 C-2011 15 Volatile Organic Compounds (GC/MS) by Method 6200E-2011 16 GI: Glossary of Terms 21 Al: Accreditations & Locations 22 Sc: Sample Chain of Custody 23 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 2 of 23 V ' SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received datettime MW-2A L1193924-01 GW Don Wells 02/27/2011:45 02/2812009:00 '' . Ci- Method Batch Dilution Preparation Analysis Analyst Location i date/time date/time z TC 6ravimetric Analysis b Method 2540 C-2011 Y Y WG1435699 1 03/01/20 09:29 03/01/2010:35 TH Mt. Juliet, TN Wet Chemistry by Method 4500P E-2011 WG1435688 1 02/28/2015:20 02/28/2015:20 JIC Mt. Juliet, TN Wet Chemistry by Method 5540 C-2011 WG1435925 1 02/28/2016:48 02/29/2012:11 MSP Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 620OB-2011 WG1436994 1 03/02/20 21:26 03/02/20 21:26 ADM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 620OB-2011 WG1438158 1 03/04/20 23:28 03/04/20 23:28 ACG Mt. Juliet, TN Fn Collected by Collected date/time Received date/time MW-3 L1193924-02 GW Don Wells 02/27/2011:15 02/28/2009:00 Fr Method Batch Dilution Preparation Analysis Analyst Location FC date/time date/time 6ravimetric Analysis by Method 2540 C-2011 WG1435699 1 03/01/20 09:29 03/01/2010:35 TH Mt. Juliet, TN Wet Chemistry by Method 4500P E-2011 WG1435688 1 02/28/2015:21 02/28/2015:21 JIC Mt. Juliet, TN G Wet Chemistry by Method 5540 C-2011 WG1435925 1 02/28/2016:48 02/29/2012:14 MSP Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 620OB-2011 WG1436994 1 03/02/20 21:46 03/02/20 21:46 ADM Mt. Juliet, TN V AI Volatile Organic Compounds (GC/MS) by Method 620OB-2011 WG1438158 1 03/04/20 23:47 03/04/20 23:47 ACG Mt. Juliet, TN Collected by Collected date/time Received date/time FC MW-4A L1193924-03 GW Don wells 02/2712012:10 02/28/2009:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time 6ravimetric Analysis by Method 2540 C-2011 WG1435699 1 03/01/20 09:29 03/01/2010:35 TH Mt. Juliet, TN Wet Chemistry by Method 4500P E-2011 WG1435688 1 02/28/2015:22 02/28/2015:22 JIC Mt. Juliet, TN Wet Chemistry by Method 5540 C-2011 WG1435925 1 02/28/2016:48 02/29/2012:16 MSP Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 620OB-2011 WG1436994 1 03/02/20 22:05 03/02/20 22:05 ADM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 620OB-2011 WG1438158 1 03/05/20 00:07 03/05/20 00:07 ACG Mt. Juliet, TN Collected by Collected date/time Received date/time TRIP BLANK L1193924-04 GW Don wells 02/27/2000:00 02/28/2009:00 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time Volatile Organic Compounds (GC/MS) by Method 62006-2011 WG1436994 1 03/02/20 20:47 03/02/20 20:47 ADM Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 6200E-2011 WG1438158 1 03/05/20 00:26 03/05/20 00:26 ACG Mt. Juliet, TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 3 of 23 i ' CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the C.0 !_ appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my rss] knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. Fr FC1 Rl Jason Romer CAI Project Manager FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 4 of 23 MW-2A SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 02/27/20 11:45 L1193924 Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Dissolved Solids 86000 10000 1 03/01/202010:35 W61435699 ;-': 71 Wet Chemistry by Method 4500P E-2011 Ss I Result Qualifier RDL Dilution Analysis Batch Analyte ug/1 ug/I date / time Fn Phosphate,Ortho ND 25.0 1 02/28/202015:20 WG1435688 Wet Chemistry by Method 5540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Q C MBAS ND 100 1 02/29/202012:11 WG1435925 F, Volatile Organic Compounds (GC/MS) by Method 620OB-2011 Result Qualifier RDL Dilution Analysis Batch AI Analyte ug/I ug/I date / time Acetone ND J4 50.0 1 03/02/2020 21:26 WG1436994 Acrolein ND 50.0 1 03/02/2020 21:26 WG1436994 I q Acrylonitrile ND J4 10.0 1 03/02/2020 21:26 WG1436994 Benzene ND 1.00 1 03/02/2020 21:26 WG1436994 Bromobenzene ND 1.00 1 03/02/2020 21:26 WG1436994 Bromodichloromethane ND 1.00 1 03/02/2020 21:26 WG1436994 Bromoform ND 1.00 1 03/02/2020 21:26 WG1436994 Bromomethane ND 5.00 1 03/02/2020 21:26 WG1436994 n-Butylbenzene ND 1.00 1 03/02/2020 21:26 WG1436994 sec-Butylbenzene ND 1.00 1 03/02/2020 21:26 WG1436994 tert-Butylbenzene ND 1.00 1 03/02/2020 21:26 WG1436994 Carbon tetrachloride ND 1.00 1 03/02/2020 21:26 WG1436994 Chlorobenzene ND 1.00 1 03/02/2020 21:26 WG1436994 Chlorodibromomethane ND 1.00 1 03/02/2020 21:26 WG1436994 Chloroethane ND 5.00 1 03/02/2020 21:26 WG1436994 Chloroform ND 5.00 1 03/02/2020 21:26 WG1436994 Chloromethane ND 2.50 1 03/02/2020 21:26 WG1436994 2-Chlorotoluene ND 1.00 1 03/04/2020 23:28 WG1438158 4-Chlorotoluene ND 1.00 1 03/02/2020 21:26 WG1436994 1,2-Dibromo-3-Chloropropane ND 5.00 1 03/02/2020 21:26 WG1436994 1,2-Dibromoethane ND 1.00 1 03/02/2020 21:26 WG1436994 Dibromomethane ND 1.00 1 03/02/2020 21:26 WG1436994 1,2-Dichlorobenzene ND 1.00 1 03/02/2020 21:26 WG1436994 1,3-Dichlorobenzene ND 1.00 1 03/02/2020 21:26 WG1436994 1,4-Dichlorobenzene ND 1.00 1 03/02/2020 21:26 WG1436994 Dichlorodifluoromethane ND 5.00 1 03/02/2020 21:26 WG1436994 1,1-Dichloroethane ND 1.00 1 03/02/2020 21:26 WG1436994 1,2-Dichloroethane ND 1.00 1 03/02/2020 21:26 WG1436994 1,1-Dichloroethene ND 1.00 1 03/02/2020 21:26 WG1436994 cis4,2-Dichloroethene ND 1.00 1 03/02/2020 21:26 WG1436994 trans-1,2-Dichloroethene ND 1.00 1 03/02/2020 21:26 WG1436994 1,2-Dichloropropane ND 1.00 1 03/02/2020 21:26 WG1436994 1,1-Dichloropropene ND 1.00 1 03/02/2020 21:26 WG1436994 1,3-Dichloropropane ND 1.00 1 03/02/2020 21:26 WG1436994 2,2-Dichloropropane ND 1.00 1 03/02/2020 21:26 WG1436994 Di -isopropyl ether ND 1.00 1 03/02/2020 21:26 WG1436994 Ethylbenzene ND 1.00 1 03/02/2020 21:26 WG1436994 Hexachloro-1,3-butadiene ND 1.00 1 03/02/2020 21:26 WG1436994 Isopropylbenzene ND 1.00 1 03/02/2020 21:26 WG1436994 ACCOUNT: PROJECT: SDG: DATEITIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 5 of 23 ' MW-2A SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 02/27/20 11:45 L1193924 Volatile Organic Compounds (GUMS) by Method 620OB-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug4 ug/I date / time p-Isopropyltoluene ND 1.00 1 03/02/2020 21:26 WG1436994 2-Butanone (MEK) ND 10.0 1 03/02/2020 21:26 WG1436994 F Methylene Chloride ND 5.00 1 03/02/2020 21:26 WG1436994 4-Methyl-2-pentanone (MIBK) ND 10.0 1 03/02/2020 21:26 WG1436994 FSS Methyl tert-butyl ether ND 1.00 1 03/02/2020 21:26 WG1436994 Naphthalene ND 5.00 1 03/02/2020 21:26 WG1436994 FCn] n-Propylbenzene ND 1.00 1 03/04/2020 23:28 WG1438158 Styrene ND 1.00 1 03/02/2020 21:26 WG1436994 1,1,1,2-Tetrachloroethane ND 1.00 1 03/02/2020 21:26 WG1436994 1,1,2,2-Tetrachloroethane ND 1.00 1 03/02/2020 21:26 WG1436994 Tetrachloroethene ND 1.00 1 03102/202021:26 WG1436994 FC1 Toluene ND 1.00 1 03/02/2020 21:26 WG1436994 1,2,3-Trichlorobenzene ND 1.00 1 03/02/2020 21:26 WG1436994 1,2,4-Trichlorobenzene ND 1.00 1 03/021202021:26 WG1436994 G� 1,1,1-Trichloroethane ND 1.00 1 03/02/2020 21:26 WG1436994 1,1,2-Trichloroethane ND 1.00 1 03/02/2020 21:26 WG1436994 Trichloroethene ND 1.00 1 03/02/2020 21:26 WG1436994 Trichlorofluoromethane ND 5.00 1 03/02/2020 21:26 WG1436994 1,2,3-Trichloropropane ND 2.50 1 03/02/2020 21:26 WG1436994 SC 1,2,4-Trimethylbenzene ND 1.00 1 03/02/2020 21:26 WG1436994 1,3,5-Trimethylbenzene ND 1.00 1 03/04/2020 23:28 WG1438158 Vinyl chloride ND 1.00 1 03/02/2020 21:26 WG1436994 o-Xylene ND 1.00 1 03/02/2020 21:26 WG1436994 m&p-Xylenes ND 2.00 1 03/02/2020 21:26 WG1436994 (S) Toluene-d8 105 80.0-120 0310212020 2116 WG1436994 (S) Toluene-d8 101 80.0-120 0310412020 23:28 WG1438158 (S) 4-Bromofluorobenzene 97.8 77.0-126 0310212020 21:26 WG1436994 (S) 4-Bromofluorobenzene 100 77.0-126 0310412020 23:18 WG1438158 (S)1,2-Dichloroethane-d4 109 70.0-130 031021202021.26 WG1436994 (S)1,2-Dichloroethane-d4 112 70.0-130 0310412020 23:28 WG1438158 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 6 of 23 c MW-3 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 02/27/20 11:15 L1193924 Gravimetric Analysis by Method 2540 C-2011 Resuft Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Dissolved Solids 94000 10000 1 03101/202010:35 WG1435699 Wet Chemistry by Method 4500P E-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Phosphate,Ortho ND 25.0 1 02/28/202015:21 WG1435688 Wet Chemistry by Method 5540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time MBAS ND 100 1 02/29/202012:14 WG1435925 Volatile Organic Compounds (GC/MS) by Method 620OB-2011 Analyte Acetone Acrolein Acrylonitrile Benzene Bromobenzene Bromod ichlorometha ne Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chlorod ibromometha ne Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-Chloropropa ne 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene D ichlorod ifluorometha ne 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,1-Dichloropropene 1,3-Dichloropropane 2,2-Dichloropropane Di -isopropyl ether Ethylbenzene H exachloro-1,3-butadie ne Isopropylbenzene Result Qualifier RDL ug/I ug/I ND J4 50.0 ND 50.0 ND J4 10.0 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 5.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 5.00 ND 5.00 ND 2.50 ND 1.00 ND 1.00 ND 5.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 5.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 ND 1.00 Dilution Analysis date / time 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/04/2020 23:47 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 1 03/02/2020 21:46 Batch WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1438158 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 WG1436994 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 7 of 23 ' MW-3 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 02/27/20 11:15 L1193924 Volatile Organic Compounds (GC/MS) by Method 620OB-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time p-Isopropyltoluene ND 1.00 1 03/02/2020 21:46 WG1436994 2-Butanone (MEK) ND 10.0 1 03/02/2020 21:46 WG1436994 Methylene Chloride ND 5.00 1 03/02/2020 21:46 WG1436994 4-Methyl-2-pentanone (MIBK) ND 10.0 1 03/02/2020 21:46 WG1436994 Methyl tert-butyl ether ND 1.00 1 03/02/2020 21:46 WG1436994 Naphthalene ND 5.00 1 03/02/2020 21:46 WG1436994 n-Propylbenzene ND 1.00 1 03/04/2020 23:47 WG1438158 Styrene ND 1.00 1 03/02/2020 21:46 WG1436994 1,1,1,2-Tetrachloroethane ND 1.00 1 03/02/2020 21:46 WG1436994 1,1,2,2-Tetrachloroethane ND 1.00 1 03/02/2020 21:46 WG1436994 Tetrachloroethene ND 1.00 1 03/02/2020 21:46 WG1436994 Toluene ND 1.00 1 03/02/2020 21:46 WG1436994 1,2,3-Trichlorobenzene ND 1.00 1 03/02/2020 21:46 WG1436994 1,2,4-Trichlorobenzene ND 1.00 1 03/02/2020 21:46 WG1436994 1,1,1-Trichloroethane ND 1.00 1 03/02/2020 21:46 WG1436994 1,1,2-Trichloroethane ND 1.00 1 03/02/2020 21:46 WG1436994 Trichloroethene ND 1.00 1 03/02/2020 21:46 WG1436994 Trichlorofluoromethane ND 5.00 1 03/02/2020 21:46 WG1436994 1,2,3-Trichloropropane ND 2.50 1 03/02/2020 21:46 WG1436994 1,2,4-Trimethylbenzene ND 1.00 1 03/02/2020 21:46 WG1436994 1,3,5-Trimethylbenzene ND 1.00 1 03/04/2020 23:47 WG1438158 Vinyl chloride ND 1.00 1 03/02/2020 21:46 WG1436994 o-Xylene ND 1.00 1 03/02/2020 21:46 WG1436994 m&p-Xylenes ND 2.00 1 03/02/2020 21:46 WG1436994 (S)Toluene-d8 103 80.0-120 031021202021.46 WG1436994 (S) Toluene-d8 101 80.0-120 0310412020 23:47 WG1438158 (S) 4-Bromofluorobenzene 96.9 77.0-126 0310212020 21.46 WG1436994 (S) 4-Bromofluorobenzene 98.8 77.0-126 0310412020 23:47 WG1438158 (S)1,2-Dichloroethone-d4 109 70.0-130 031021202021:46 WG1436994 (S)1,2-Dichloroethone-d4 ill 70.0-130 0310412020 23:47 WG1438158 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 8 of 23 ' M W-4A SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 02/27/20 12:10 L1193924 Gravimetric Analysis by Method 2540 C-2011 ---, Result Qualifier RDL Dilution Analysis Batch Cp Analyte ug/I ug/1 date / time z Dissolved Solids 123000 10000 1 03/01/202010:35 WG1435699 TC Wet Chemistry by Method 4500P E-2011 E Result QualifierRDL Dilution Analysis Batch Analyte ug/I ug/I date / time Fn Phosphate,Ortho ND 25.0 1 02/28/202015:22 WG1435688 Wet Chemistry by Method 5540 C-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ugA ugA date / time E MBAS ND J6 100 1 02/29/202012:16 WG1435925 �GI Volatile Organic Compounds (GC/MS) by Method 620OB-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ugA ug/I date / time AI Acetone ND J4 50.0 1 03/02/2020 22:05 WG1436994 9 Acrolein ND 50.0 1 03/02/2020 22:05 WG1436994 SC Acrylonitrile ND J4 10.0 1 03/02/2020 22:05 WG1436994 Benzene ND 1.00 1 03/02/2020 22:05 WG1436994 Bromobenzene ND 1.00 1 03/02/2020 22:05 WG1436994 Bromodichloromethane ND 1.00 1 03/02/2020 22:05 WG1436994 Bromoform ND 1.00 1 03/02/2020 22:05 WG1436994 Bromomethane ND 5.00 1 03/02/2020 22:05 WG1436994 n-Butylbenzene ND 1.00 1 03/02/2020 22:05 WG1436994 sec-Butylbenzene ND 1.00 1 03/02/2020 22:05 WG1436994 tert-Butylbenzene ND 1.00 1 03/02/2020 22:05 WG1436994 Carbon tetrachloride ND 1.00 1 03/02/2020 22:05 WG1436994 Chlorobenzene ND 1.00 1 03/02/2020 22:05 WG1436994 Chlorodibromomethane ND 1.00 1 03/02/2020 22:05 WG1436994 Chloroethane ND 5.00 1 03/02/2020 22:05 WG1436994 Chloroform ND 5.00 1 03/02/2020 22:05 WG1436994 Chloromethane ND 2.50 1 03/02/2020 22:05 WG1436994 2-Chlorotoluene ND 1.00 1 03/05/2020 00:07 WG1438158 4-Chlorotoluene ND 1.00 1 03/02/2020 22:05 WG1436994 1,2-Dibromo-3-Chloropropane ND 5.00 1 03/02/2020 22:05 WG1436994 1,2-Dibromoethane ND 1.00 1 03/02/2020 22:05 WG1436994 Dibromomethane ND 1.00 1 03/02/2020 22:05 WG1436994 1,2-Dichlorobenzene ND 1.00 1 03/02/2020 22:05 WG1436994 1,3-Dichlorobenzene ND 1.00 1 03/02/2020 22:05 WG1436994 1,4-Dichlorobenzene ND 1.00 1 03/02/2020 22:05 WG1436994 Dichlorodifluoromethane ND 5.00 1 03/02/2020 22:05 WG1436994 1,1-Dichloroethane ND 1.00 1 03/02/2020 22:05 WG1436994 1,2-Dichloroethane ND 1.00 1 03/02/2020 22:05 WG1436994 1,1-Dichloroethene ND 1.00 1 03/02/2020 22:05 WG1436994 cis-1,2-Dichloroethene ND 1.00 1 03/02/2020 22:05 WG1436994 trans4,2-Dichloroethene ND 1.00 1 03/02/2020 22:05 WG1436994 1,2-Dichloropropane ND 1.00 1 03/02/2020 22:05 WG1436994 1,1-Dichloropropene ND 1.00 1 03/02/2020 22:05 WG1436994 1,3-Dichloropropane ND 1.00 1 03/02/2020 22:05 WG1436994 2,2-Dichloropropane ND 1.00 1 03/02/2020 22:05 WG1436994 Di -Isopropyl ether ND 1.00 1 03/02/2020 22:05 WG1436994 Ethylbenzene ND 1.00 1 03/02/2020 22:05 WG1436994 Hexachloro-1,3-butadiene ND 1.00 1 03/02/2020 22:05 WG1436994 Isopropylbenzene ND 1.00 1 03/02/2020 22:05 WG1436994 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 9 of 23 lb # MW-4A SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. * Collected date/time: 02/27/20 12:10 L1193924 Volatile Organic Compounds (GUMS) by Method 620OB-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time p-Isopropyltoluene ND 1.00 1 03/02/2020 22:05 WG1436994 2-Butanone (MEK) ND 10.0 1 03/02/2020 22:05 WG1436994 Methylene Chloride ND 5.00 1 03/02/2020 22:05 WG1436994 4-Methyl-2-pe nta none (MIBK) ND 10.0 1 03/02/2020 22:05 WG1436994 E Methyl tert-butyl ether ND 1.00 1 03/02/2020 22:05 WG1436994 Naphthalene ND 5.00 1 03/02/2020 22:05 WG1436994 [Cn] n-Propylbenzene ND 1.00 1 03/05/2020 00:07 WG1438158 Styrene ND 1.00 1 03/02/2020 22:05 WG1436994 1,1,1,2-Tetrachloroethane ND 1.00 1 03/02/2020 22:05 WG1436994 1,1,2,2-Tetrachloroethane ND 1.00 1 03/02/2020 22:05 WG1436994 Tetrachloroethene ND 1.00 1 03/02/2020 22:05 WG1436994 rQC1 Toluene ND 1.00 1 03/02/2020 22:05 WG1436994 1,2,3-Trichlorobenzene ND 1.00 1 03/02/2020 22:05 WG1436994 FGI 1,2,4-Trichlorobenzene ND 1.00 1 03/02/2020 22:05 WG1436994 1,1,1-Trichloroethane ND 1.00 1 03/02/2020 22:05 WG1436994 1,1,2-Trichloroethane ND 1.00 1 03/02/2020 22:05 WG1436994 QAI Trichloroethene ND 1.00 1 03/02/2020 22:05 WG1436994 Trichlorofluoromethane ND 5.00 1 03/02/2020 22:05 WG1436994 1,2,3-Trichloropropane ND 2.50 1 03/02/2020 22:05 WG1436994 FC 1,2,4-Trimethylbenzene ND 1.00 1 03/02/2020 22:05 WG1436994 1,3,5-Trimethylbenzene ND 1.00 1 03/05/2020 00:07 WG1438158 Vinyl chloride ND 1.00 1 03/02/2020 22:05 WG1436994 o-Xylene ND 1.00 1 03/02/2020 22:05 WG1436994 m&p-Xylenes ND 2.00 1 03/02/2020 22:05 WG1436994 (S)Toluene-d8 105 80.0-120 031021202022.05 WG1436994 (S) Toluene-d8 102 80.0-120 0310512020 00.07 WG1438158 (S) 4-Bromofluorobenzene 98.8 77.0-126 0310212020 21:05 WG1436994 (S) 4-Bromofluorobenzene 103 77.0-126 0310512020 00:07 WG1438158 (S)1,2-Dichloroethane-0 108 70.0-130 031021202022:05 WG1436994 (S)1,1-Dichloroethane-d4 113 70.0-130 031051202000.07 WG1438158 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 03/05/2013:37 10 of 23 ' TRIP BLANK SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 02/27/20 00:00 L1193924 Volatile Organic Compounds (GC/MS) by Method 620OB-2011 ResuR Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acetone ND J4 50.0 1 03/02/2020 20:47 WG1436994 T Acrolein ND 50.0 1 03/02/2020 20:47 WG1436994 Acrylonitrile ND J4 10.0 1 03/021202020:47 WG1436994 3SS] Benzene ND 1.00 1 03/02/2020 20:47 WG1436994 Bromobenzene ND 1.00 1 03/02/2020 20:47 WG1436994 Bromodichloromethane ND 1.00 1 03/021202020:47 WG1436994 Cn Bromoform ND 1.00 1 03/02/2020 20:47 WG1436994 Bromomethane ND 5.00 1 03/02/2020 20:47 WG1436994 n-Butylbenzene ND 1.00 1 03/02/2020 20:47 WG1436994 sec-Butylbenzene ND 1.00 1 03/02/2020 20:47 WG1436994 tert-Butylbenzene ND 1.00 1 03/02/2020 20:47 WG1436994 Carbon tetrachloride ND 1.00 1 03/02/2020 20:47 WG1436994 Chlorobenzene ND 1.00 1 03/02/2020 20:47 WG1436994 GI Chlorodibromomethane ND 1.00 1 03/02/2020 20:47 WG1436994 Chloroethane ND 5.00 1 03/02/2020 20:47 WG1436994 Chloroform ND 5.00 1 03/02/2020 20:47 WG1436994 Chloromethane ND 2.50 1 03/02/2020 20:47 WG1436994 2-Chlorotoluene ND 1.00 1 03/05/202000:26 WG1438158 SC 4-Chlorotoluene ND 1.00 1 03/02/2020 20:47 WG1436994 1,2-Dibromo-3-Chloropropane ND 5.00 1 03/02/202020:47 WG1436994 1,2-Dibromoethane ND 1.00 1 03/02/2020 20:47 WG1436994 Dibromomethane ND 1.00 1 03/02/2020 20:47 WG1436994 1,2-Dichlorobenzene ND 1.00 1 03/02/2020 20:47 WG1436994 1,3-Dichlorobenzene ND 1.00 1 03/02/2020 20:47 WG1436994 1,4-Dichlorobenzene ND 1.00 1 03/02/2020 20:47 WG1436994 Dichlorodifluoromethane ND 5.00 1 03/02/2020 20:47 WG1436994 1,1-Dichloroethane ND 1.00 1 03/02/2020 20:47 WG1436994 1,2-Dichloroethane ND 1.00 1 03/02/2020 20:47 WG1436994 1,1-Dichloroethene ND 1.00 1 03/02/2020 20:47 WG1436994 cis-1,2-Dichloroethene ND 1.00 1 03/02/2020 20:47 WG1436994 trans-1,2-Dichloroethene ND 1.00 1 03/02/2020 20:47 WG1436994 1,2-Dichloropropane ND 1.00 1 03/02/2020 20:47 WG1436994 1,1-Dichloropropene ND 1.00 1 03/02/2020 20:47 WG1436994 1,3-Dichloropropane ND 1.00 1 03/02/2020 20:47 WG1436994 2,2-Dichloropropane ND 1.00 1 03/02/2020 20:47 WG1436994 DI -Isopropyl ether ND 1.00 1 03/02/2020 20:47 WG1436994 Ethylbenzene ND 1.00 1 03/02/2020 20:47 WG1436994 Hexachloro-1,3-butadiene ND 1.00 1 03/02/2020 20:47 WG1436994 Isopropylbenzene ND 1.00 1 03/02/2020 20:47 WG1436994 p-Isopropyltoluene ND 1.00 1 03/02/2020 20:47 WG1436994 2-Butanone (MEK) ND 10.0 1 03/02/2020 20:47 WG1436994 Methylene Chloride ND 5.00 1 03/02/2020 20:47 WG1436994 4-Methyl-2-pentanone (MIBK) ND 10.0 1 03/02/2020 20:47 WG1436994 Methyl tert-butyl ether ND 1.00 1 03/02/2020 20:47 WG1436994 Naphthalene ND 5.00 1 03/02/2020 20:47 WG1436994 n-Propylbenzene ND 1.00 1 03/05/202000:26 WG1438158 Styrene ND 1.00 1 03/02/2020 20:47 WG1436994 1,1,1,2-Tetrachloroethane ND 1.00 1 03/02/2020 20:47 WG1436994 1,1,2,2-Tetrachloroethane ND 1.00 1 03/02/2020 20:47 WG1436994 Tetrachloroethene ND 1.00 1 03/02/2020 20:47 WG1436994 Toluene ND 1.00 1 03/02/2020 20:47 WG1436994 1,2,3-Trichlorobenzene ND 1.00 1 03/02/2020 20:47 WG1436994 1,2,4-Trichlorobenzene ND 1.00 1 03/02/2020 20:47 WG1436994 1,1,1-Trichloroethane ND 1.00 1 03/02/2020 20:47 WG1436994 1,1,2-Trichloroethane ND 1.00 1 03/02/2020 20:47 WG1436994 Trichloroethene ND 1.00 1 03/02/2020 20:47 WG1436994 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 11 of 23 ` TRIP BLANK SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 02/27/20 00:00 L1193924 Volatile Organic Compounds (GUMS) by Method 6200E-2011 Analyte Trichlorofluoromethane 1,2,3-Trich loropropa ne 1,2,4-Trimethylbe nzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene m&p-Xylenes (S) Toluene-d8 (S) Toluene-d8 (S) 4-Bromot7uorobenzene (S) 4-Bromof7uorobenzene (S)1,2-Dichloroethone-d4 (S)1,1-Dichloroethone-d4 Result Qualifier. RDL Dilution Analysis Batch ug/I ug/I date / time ND 5.00 1 03/02/2020 20:47 WG1436994 ND 2.50 1 03/02/2020 20:47 WG1436994 ND 1.00 1 03/02/2020 20:47 WG1436994 ND 1.00 1 03/05/2020 00:26 WG1438159 ND 1.00 1 03/02/2020 20:47 WG1436994 ND 1.00 1 03/02/2020 20:47 WG1436994 ND 2.00 1 03/02/2020 20:47 WG1436994 104 80.0-120 031021202020.47 WG1436994 101 80.0-120 0310512020 00:26 WG1438158 98.5 77.0-126 031OZ2020 20.47 WG1436994 100 77.0-126 0310512020 00.26 WG1438158 109 70.0-130 0310212020 20.47 WG1436994 ill 70.0-130 0310512020 00:26 WG1438158 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 12 of 23 WG1435699 Gravimetric Analysis by Method 2540 C-2011 Method Blank (MB) (MB) R3504533-1 03/01/2010:35 MB Result Analyte ug/I Dissolved Solids U MB Qualifier MB MDL MB ROL ug/I ug/I 2820 10000 L1193940-01 Original Sample (OS) • Duplicate (DUP) QUALITY CONTROL SUMMARY 1-1193924-01,02,03 (OS) L1193940-01 03/01/2010:35 • (DUP) R3504533-3 03/01/2010:35 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ug/I ug/I % % Dissolved Solids 1090000 1160000 1 6.25 J3 5 Laboratory Control Sample (LCS) (LCS) R3504533-2 03/01/2010:35 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I % % Dissolved Solids 8800000 8410000 95.6 85.0-115 ONE LAB. NATIONWIDE. *- 9 Sc ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 DATE/TIME: 03/05/20 13:37 PAGE: 13 of 23 WG1435688 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. a" Wet Chemistry by Method 4500P E-2011 11193924-01,02,03 Methnd Rlank (MR) (MB) R3504033-1 02/28/2015:19 MB Result Analyte ug/I Phosphate,Ortho U MB Qualifier MB MDL MB RDL ug/1 ug/1 9.00 25.0 L1193893-01 Original Sample (OS) • Duplicate (DUP) (OS) L1193893-01 02/28/2016:07 • (DUP) R3504033-5 02/28/2016:26 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ug/I ug/I % % Phosphate,Ortho 73400 73500 100 0.161 20 Laboratory Control Sample (LCS) (LCS) R3504033-2 02/28/2015:19 Spike Amount LCSResult LCS Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I % % Phosphate,Ortho 245 254 104 85.0-115 L1193924-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1193924-03 02/28/2015:22 • (MS) R3504033-3 02/28/2015:22 • (MSD) R3504033-4 02/28/2015:22 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I ug/I % % % % Phosphate,Ortho 500 ND 504 518 101 104 1 80.0-120 2.74 20 ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 DATEMME: 03/0512013:37 PAGE: 14 of 23 WG1435925 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.' Wet Chemistry by Method 5540 C-2011 1-1193924-01,02,03 e Method Blank (MB) (MB) R3504190-1 02/29/20 12:01 MB Result Analyte ug/I MBAS U MB Qualifier MB MDL MB ROL ug/I ug/I 19.0 100 L1193924-01 Original Sample (OS) • Duplicate (DUP) (OS) L1193924-01 02/29/2012:11 • (DUP) R3504190-3 02/29/2012:12 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ug/I ug/I % % MBAS ND 33.0 1 0.000 20 Laboratory Control Sample (LCS) (LCS) R3504190-2 02/29/2012:04 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I % % MBAS 1000 997 99.7 85.0-115 L1193924-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1193924-03 02/29/2012:16 • (MS) R3504190-4 02/29/2012:17 • (MSD) R3504190-5 02/29/20 12:19 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte ug/I ug/I ug/I ug/I % % % % MBAS 1000 ND 691 739 65.7 70.5 1 85.0-115 16 J6 6.71 RPD Limits 20 ACCOUNT: PROJECT: SDG: Soil & Env. Consultants- Raleigh, NC GW-1 1061-200 L1193924 DATE/TIME: 03/05/20 13:37 PAGE: 15 of 23 WG1436994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. *- , Volatile Organic Compounds (GC/MS) by Method 620OB-2011 Method Blank (MB) (MB) R3505370-3 03/02/20 19:01 MB Result Analyte Ug/I Acetone U Acrolein U Acrylonitrile U Benzene U Bromobenzene U Bromodichloromethane U Bromoform U Bromomethane U n-Butylbenzene U sec-Butylbenzene U tert-Butylbenzene U Carbon tetrachloride U Chlorobenzene U Chlorodibromomethane U Chloroethane U Chloroform U Chloromethane U 4-Chlorotoluene U 1,2-Dibromo-3-Chloropropane U 1,2-Dibromoethane U Dibromomethane U 1,2-Dichlorobenzene U 1,3-Dichlorobenzene U 1,4-Dichlorobenzene U Dichlorodifluoromethane U 1,1-Dichloroethane U 1,2-Dichloroethane U 1,1-Dichloroethene U cis-1,2-Dichloroethene U trans-1,2-Dichloroethene U 1,2-Dichloropropane U 1,1-Dichloropropene U 1,3-Dichloropropane U 2,2-Dichloropropane U Di -isopropyl ether U Ethylbenzene U Hexachloro-1,3-butadiene U Isopropylbenzene U p-Isopropyltoluene U 2-Butanone (MEK) U L1193924-01,02,03,04 MB Qualifier MB MDL MB RDL ug/I ug/I nc 10.0 50.0 8.87 50.0 3 SS 1.87 10.0 0.331 1.00 0.352 1.00 FC 0.380 1.00 0.469 1.00 Fr 0.866 5.00 0.361 1.00 0.365 1.00 01 0.399 1.00 0.379 1.00 E 0.348 1.00 0.327 1.00 0.453 5.00 0.324 5.00 0.276 2.50 e SC 0.351 1.00 1.33 5.00 0.381 1.00 0.346 1.00 0.349 1.00 0.220 1.00 0.274 1.00 0.551 5.00 0.259 1.00 0.361 1.00 0.398 1.00 0.260 1.00 0.396 1.00 0.306 1.00 0.352 1.00 0.366 1.00 0.321 1.00 0.320 1.00 0.384 1.00 0.256 1.00 0.326 1.00 0.350 1.00 3.93 10.0 w ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 DATEITIME: 03/05/2013:37 PAGE: 16 of 23 WG1436994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 6200E-2011 L1193924-01,02,03,04 F Method Blank (MB) (MB) R3505370-3 03/02/20 19:01 MB Result MB Qualifier MB MDL MB RDL Analyte Ug/I Ug/I Ug/l Ec Methylene Chloride U 1.00 5.00 4-Methyl-2-pentanone (MIBK) U 2.14 10.0 FS Methyl tert-butyl ether U 0.367 1.00 Naphthalene U 1.00 5.00 Styrene U 0,307 1.00 [qn 1,1,1,2-Tetrachloroethane U 0.385 1.00 1,1,2,2-Tetrachloroethane U 0.130 1.00 FirTetrachloroethene U 0.372 1.00 Toluene U 0.412 1.00 1,2,3-Trichlorobenzene U 0.230 1.00 � 1,2,4-Trichlorobenzene U 0.355 1.00 1,1,1-Trichloroethane U 0.319 1.00 2G1 1,1,2-Trichloroethane U 0.383 1.00 Trichloroethene U 0.398 1.00 s Trichlorofluoromethane U 1.20 5.00 Ai 1,2,3-Tdchloropropane U 0.807 2.50 1,2,4-Trimethylbenzene U 0.373 1.00 e Sc Vinyl chloride U 0.259 1.00 o-Xylene U 0.341 1.00 m&p-Xylenes U 0.719 2.00 (S) Toluene-d8 104 80.0-120 (S) 4-Bromoiluorobenzene 96.1 77.0-126 (S)1,2-Dichloroethone-d4 108 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3505370-1 03/02/2017:43 • (LCSD) R3505370-2 03/02/2018:03 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I Ug/I % % % % % Acetone 25.0 49.9 48.0 200 192 19.0-160 J4 J4 3.88 27 Acrolein 25.0 19.9 19.7 79.6 78.8 10.0-160 1.01 26 Acrylonitrile 25.0 46.7 46.4 187 186 55.0-149 J4 J4 0.644 20 Benzene 5.00 4.53 4.56 90.6 91.2 70.0-123 0,660 20 Bromobenzene 5.00 3.85 3.85 77.0 77.0 73.0-121 0.000 20 Bromodichloromethane 5.00 4.49 4.51 89.8 90.2 75.0-120 0.444 20 Bromoform 5.00 5.03 5.05 101 101 68.0-132 0.397 20 Bromomethane 5.00 4.80 4.57 96.0 91.4 10.0-160 4.91 25 n-Butylbenzene 5.00 4.73 4.66 94.6 93.2 73.0-125 1.49 20 sec-Butylbenzene 5.00 4.14 4.08 82.8 81.6 75.0-125 1.46 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 17 of 23 WG1436994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.' Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1193924-01,02,03,04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3505370-1 03/02/20 17:43 • (LCSD) R3505370-2 03/02/2018:03 Spike Amount LCS ResuR LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % tert-Butylbenzene 5.00 3.93 3.82 78.6 76.4 76.0-124 2.84 20 Carbon tetrachloride 5.00 4.73 4.64 94.6 92.8 68.0-126 1.92 20 Chlorobenzene 5.00 4.71 4.71 94.2 94.2 80.0-121 0.000 20 Chlorodibromomethane 5.00 4.72 4.95 94.4 99.0 77.0-125 4.76 20 Chloroethane 5.00 4.73 4.59 94.6 91.8 47.0-150 3.00 20 Chloroform 5.00 4.62 4.56 92.4 91.2 73.0-120 1.31 20 Chloromethane 5.00 5.46 5.06 109 101 41.0-142 7.60 20 4-Chlorotoluene 5.00 3.81 3.87 76.2 77.4 75.0-122 1.56 20 1,2-Dibromo-3-Chloropropane 5.00 5.93 5.62 119 112 58.0-134 5.37 20 1,2-Dibromoethane 5.00 4.99 5.13 99.8 103 80.0422 2.77 20 Dibromomethane 5.00 5.07 5.01 101 100 80.0-120 1.19 20 1,2-Dichlorobenzene 5.00 5.00 4.98 100 99.6 79.0-121 0.401 20 1,3-Dichlorobenzene 5.00 4.67 4.59 93.4 91.8 79.0-120 1.73 20 1,4-Dichlorobenzene 5.00 4.72 4.73 94.4 94.6 79.0-120 0.212 20 Dichlorodifluoromethane 5.00 4.52 4.45 90.4 89.0 51.0-149 1.56 20 1,1-Dichloroethane 5.00 4.89 4.59 97.8 91.8 70.0-126 6.33 20 1,2-Dichloroethane 5.00 5.06 5.10 101 102 70.0-128 0.787 20 1,1-Dichloroethene 5.00 4.34 4.30 86.8 86.0 71.0-124 0.926 20 cis-1,2-Dichloroethene 5.00 4.79 4.72 95.8 94.4 73.0-120 1.47 20 trans4,2-Dichloroethene 5.00 4.49 4.43 89.8 88.6 73.0-120 1.35 20 1,2-Dichloropropane 5.00 5.12 5.15 102 103 77.0-125 0.584 20 1,1-Dichloropropene 5.00 4.63 4.58 92.6 91.6 74.0-126 1.09 20 1,3-Dichloropropane 5.00 5.04 5.16 101 103 80.0-120 2.35 20 2,2-Dichloropropane 5.00 4.02 3.88 80.4 77.6 58.0-130 3.54 20 Di -isopropyl ether 5.00 5.04 4.97 101 99.4 58.0-138 1.40 20 Ethylbenzene 5.00 4.61 4.74 92.2 94.8 79.0-123 2.78 20 Hexachloro4,3-butadiene 5.00 4.32 4.31 86.4 86.2 54.0-138 0.232 20 Isopropylbenzene 5.00 4.60 4.54 92.0 90.8 76.0-127 1.31 20 p-Isopropyltoluene 5.00 4.28 4.16 85.6 83.2 76.0-125 2.84 20 2-Butanone (MEK) 25.0 38.6 39.3 154 157 44.0-160 1.80 20 Methylene Chloride 5.00 4.83 4.72 96.6 94.4 67.0-120 2.30 20 4-Methyl-2-pentanone (MIBK) 25.0 30.8 31.1 123 124 68.0-142 0.969 20 Methyl tert-butyl ether 5.00 4.95 5.08 99.0 102 68.0-125 2.59 20 Naphthalene 5.00 5.19 5.19 104 104 54.0-135 0.000 20 Styrene 5.00 4.62 4.64 92.4 92.8 73.0-130 0.432 20 1,1,1,2-Tetrachloroethane 5.00 4.59 4.64 91.8 92.8 75.0-125 1.08 20 1,1,2,2-Tetrachloroethane 5.00 4.10 4.28 82.0 85.6 65.0-130 4.30 20 Tetrachloroethene 5.00 4.61 4.69 92.2 93.8 72.0-132 1.72 20 Toluene 5.00 4.60 4.59 92.0 91.8 79.0-120 0.218 20 1,2,3-Ticchoorobenzene 5.00 4.63 4.65 92.6 93.0 50.0-138 0.431 20 ACCOUNT: PROJECT: SDG: DATEITIME: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 PAGE: 18of23 WG1436994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. ` Volatile Organic Compounds (GC/MS) by Method 6200E-2011 L1193924-01,02,03,04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3505370-1 03/02/20 17:43 • (LCSD) R3505370-2 03/02/20 18:03 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I ug/I % % % 1,2,4-Trichlorobenzene 5.00 4.79 4.79 95.8 95.8 57.0-137 1,1,1-Trichloroethane 5.00 4.45 4.37 89.0 87.4 73.0-124 1,1,2-Trichloroethane 5.00 4.97 5.05 99.4 101 80.0-120 Trichloroethene 5.00 4.69 4.40 93.8 88.0 78.0-124 Trichlorofluoromethane 5.00 4.37 4.28 87.4 85.6 59.0-147 1,2,3-Trichloropropane 5.00 4.64 4.59 92.8 91.8 73.0-130 1,2,4-Trimethylbenzene 5.00 4.15 4.12 83.0 82.4 76.0-121 Vinyl chloride 5.00 5.18 5.06 104 101 67.0-131 o-Xylene 5.00 4.62 4.63 92.4 92.6 80.0-122 m&p-Xylenes 10.0 9.40 9.37 94.0 93.7 80.0-122 (S Toluene -dB 102 102 80.0-120 (S 4-Bromotluorobenzene 100 98.4 77.0-126 (S)1,2-Dichloroethone-d4 112 ill 70.0-130 LCSD Qualifier RPD RPD Limits 0.000 20 1.81 20 1.60 20 6.38 20 2.08 20 1.08 20 0.726 20 2.34 20 0.216 20 0.320 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 03/05/2013:37 19 of 23 WG1438158 Volatile Organic Compounds (GC/MS) by Method 620OB-2011 Method Blank (MB) QUALITY CONTROL SUMMARY L1193924-01,02,03,04 ONE LAB. NATIONWIDE." (MB) R3505497-2 03/04/20 21:31 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/1 ITC] 2-Chlorotoluene U 0.375 1.00 n-Propylbenzene U 0.349 1.00 3 SS 1,3,5-Trimethylbenzene U 0.387 1.00 (S) Toluene-d8 103 80.0-120 (S)4-Bromofluorobenzene 104 77.0-126 Rn (S)1,2-Dichloroethane-d4 110 70.0-130 SSr Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3505497-1 03/04/20 19:44 • (LCSD) R3505497-3 03/04/20 22:49 Spike Amount LCS Result Analyte ug/I ug/I LCSD Result ug/I LCS Rec. % LCSD Rec. % Rec. Limits LCS Qualifier LCSD Qualifier % RPD % RPD Limits % GI 2-Chlorotoluene 5.00 4.43 4.52 88.6 90.4 76.0-123 2.01 20 n-Propylbenzene 5.00 4.39 4.43 87.8 88.6 77.0-124 0.907 20 3AI 1,3,5-Trimethylbenzene 5.00 4.51 4.67 90.2 93.4 76.0-122 3.49 20 (S) Toluene -dB 97.9 99.2 80.0-120 (S) 4-Bromofluorobenzene 104 101 77.0-126 FSC (S)1,2-Dich/oroethane-d4 112 ill 70.0-130 ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 DATE/TIME: 03/05/2013:37 PAGE: 20 of 23 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. # Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) -Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or'BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 03/05/2013:37 21 of 23 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National Is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratodes in our Industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing 1 Cc turnaround time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. j ' Not all certifications held by the laboratory are applicable to the results reported in the attached report — Accreditation is onty applicable to the test methods specified on each scope of accreditation held by Pace National. FT State Accreditations `-_.. Alabama 40660 Nebraska NEOS-15-05 PS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZ0612 New Hampshire 2975 Fn Arkansas 88-0469 New Jersey—NELAP TNO02 California 2932 New Mexico' n/a Colorado TN00003 New York 11742 Fr Connecticut PH 0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 6 Georgia' 923 North Dakota R-140 CSC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 F Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky'" 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee " 2006 Louisiana' LA180010 Texas T104704245-18-15 Fc Maine TN0002 Texas' LABO152 Maryland 324 Utah TN00003 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A21-A Third Party Federal Accreditations A21-A— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A21-A— ISO 170251461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 ' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity 'Chemical/Microbiological 'Mold 'Wastewater Na Accreditation not applicable Our Locations Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. �"ems WA CA t„1T NO J rnE > OR MN T 1D SD T vw,NY VW MI T, 1 T NE IA ( T PA T lT T UT T ♦ IL I[Ti KY VA? ` <� iv CA T CO KS N10 T - yf VAT TAZ NM OK AR T 1 l T sc MI. �. — S HGA �f T Tx T LA fT� o AK FL V� ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 22 of 23 Billing Information: A ialvsls/Container / Preser ative Chain of Custody Page T.f ;Soil & Env. Consultants - Raleigh, NC attn: Don Wells PfCS 8412 Falls of Neuse Road Chk , aceAr7al IC2/• rJarb�er c.r,>d r,,,i„;uro R ienn,2nM 8412 Falls of Neuse Road, Suite 104 Suite 104 Raleigh, NC 27615-3543 Raleigh, NC 27615-3543 v 12a65Lebanon Rd Report to: Email To: dwells@sandec.com Mr. Don Wells d z LJ Y m Mount Juliet, TN 37122 Phone: 615-758-5858 Phone:800-767.5959 Fax 615-758-5859 Project City/State Please Circle: Description: Groundwater Job #1061 Collected: PT MT CT ET O _ U = SDG p i z Phone 919-846-5900 Client Project # Lab Project # GW-11061-200 SOILENV-JOBI061 � Fax: 919 846-9467 N i �E in (N y Q E Tab Acctnum:SOILENV Collected by (print): Site/Facility ID # P.O. # QoM We GIS a `0 Z LL p i c Template:T4885 Collected by (signature)): Rush? (Lab MUST Be Notified) Quote q Q C� Prelogin: P743430 A l7� _ Same Day _ rive Day _Next Day _ 5 Day (Rad Only) Date Results Needed Q Z a p a PM: 633 -Pam Langford Immediately Two Day �10Day (RadOnly) iNo. � ►- PB: �frf Packed on Ice N _ Y' _Three Day `o( L�btA 4 0 o o shipped via: FedEX Ground Sample ID p Comp/Grab /Grab p Matrix " De th P Date Time ntrs mc ui Q N to r"! RemarAs Sample a (lab only) > > MW-2A GW 2-Z�-Zfl S 4 X X X -ra/ MW-3 GW Z-27-2a f 4 X X X Ii GW 2 27-2 a Z�l (7 4 X X X d3 TRIP BLANK GW I 1 _ . X `Matrix:Remarks: pH Temp samn4e Receipt Check3rist WC Seal Present/Intact: P Y SS -Soil AIR -Air F- Fitter _N COC signedlAccurate: �Y _N GW •Groundwater B- Bioassay Flow Other Bottles arrive intact: _ZY _N WW - WasteWater .r Correct bottles used: Y t1 DW- Drinking Water Samples returned via: Sufficient volume sent: �r AtJ If Applicable OT -Other _ _ _ Tracking UPS FedEx Courier y//;/� # lui (U VOA Zero Headspace: /t _N Prese Yvation Correct/Checked: Yr^_N RAD Screen <0.5 mR/hr: Relinquah nature Date: Time: Received by: (Signature) Trip Blank Received: y o �'/ C f J t eoH BR —. Relinquished by: (Signature) Date: Time: Received by: (Signature) Temp: °C Bottles Received: If preservation required by Login: Date/Tlme Relinquished by: (Signature) Date: Time: Received for lab by: ign t Dat Time: Hold: Conditiopq fj NCF J 1 /