HomeMy WebLinkAboutWQ0001861_Monitoring - 02-2020_20200318SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT,OFENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -IN FORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
�
1617 MAIL, SERVICE CENTER,RALEIGH, NC 27699-1617 Phone: (919) 733-3221
Please Print ClearlyT
FACILITY INFORMATIOnN or Type
PERMIT Number: Expiration Date:
A /
Facility Name: \s-ttser.1/ e
M
Non -Discharge W 0, IWO I Wd U I C
Permit Name (if different):
NPDES Other
Facility Address: l S 1 gacKL't Keftd
_
TYPE OF PERMITTED OPERATION BEING MONITORED
IKLagoon ❑ Remediation: Infiltration Gallery
NC Z RY5 % County t"5 it X
ci,ti, s)nl?(zit')
❑ Spray Field ❑ Remediation:
Contact Person: A41r. 9-9"Ill r- VAWA N
Telephone#: 900 - 6y% 7278
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled: 3
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): M w" 2
Date sample collected: Z - 2% `20
FIELD ANALYSES
WAS
Well Depth: IL4 ft.
Well Diameter: Z in.
pH S tek_unniits Temp. �6•�/ °C
DRY at
Depth to Water Level: .SZ ft. below measuring point
Screened Interval: to
ZI_y
ft. Spec. Cond. µMhos
time of
__&_ft.
sampling,
Measuring Point is 1• i ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling: 19 gallons
Appearance
here: ElSamples
for metals were collected unfiltered: EYES El NO
and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: Z-Z 8 , 2•2!_ 140 ;•2.2 O
p
Laboratory Name: TA(-e "4s
Certification No. In
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
MES
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/I
Zn -Zinc mg/I
Coliform: MF Total /100ml Phosphorus:
(Note: Use MPN method for highly turbid samples)L
Total as P
mg/I
R�
G '
'
Orthophosphate nifl mg/I
Other (Specify Compounds and ConcentA&2u5it292AW
Dissolved Solids: Total su 000 al
Al - Aluminum
mg/I
pH (when analyzed) units
Ba - Barium
mg/I
T mg/I
Ca - Calcium
mg/I
m S AS :yp
Chlor g/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils c mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
P g/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate G�'Jr9Gr30G mg/I
Hg - Mercury
mg/I
Report Attached? � Yes (1) El No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC Z A/ D method # 67d0 A
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Permittee (or AuthorizA ^�Me and Title - Please print or type
GW-59 Rev.1/2007
Signature of Permittee (or Authorized Aqent)
_Il
(Date)
el IMAM enoen nni VrI I nlAl 134PPP nMl V
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
TY INFORMATION Please Print Clearly or Type
Name: Grtwy Poole v4gme-k¢ 4w.4.q
Name (if different):
Address: 151 &&t Vkw- Qswj
(Sk.el) NC z e`!S l County
(Slate) (zip)
IContact Person: e"'.01 a Telephone#: M!O- 6Y/-7i71
Well Location/Site Name: No. of wells to be sampled: 3_
:SOURCES'
OCESSING.UNIT
9-1617' Phone: (919)733-3221
PERMIT Number: Expiration Date:
Non -Discharge WfA 111100 1^1 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): /M w- 3
Date sample collected: 2.27` 2b
FIELD ANALYSED�:
WAS
Well Depth:
Weil Diameter: min,
pH S-2L unTts4 Temp. % y y °C
DRY at
time of
_V
Depth to Water Level: —!ft. below measuring point
Screened Interval: ft. to t7 ft.
Spec. Cond. µMhos
sampling,
Measuring Point is 2-1 ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling: 6 gallons
Appearance
here: ❑
Samoles for metals were collected unfiltered: DYES ❑ NO
and field acidified: ❑YES ❑ NO
LHCSVKHIVKT IIVFVKIVIHIIVIV
Date sample analyzed: 2-2 #� Y-?!�
1-1- ; 'L-?D
Laboratory Name:
Aft G�f
Certification No. '�c
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Zn -Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
b-Ii7 mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 01?0 7- L
All - Aluminum
—mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
mg/I
Ca - Calcium
mg/I
ND
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? 19 Yes (1) ❑ No (0)
62ob B
Specific Conductance
µMhos
K - Potassium
mg/I
VOC method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L vVt, Kerllovd) io
t;W-5a Kev. wzuut
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: 1
Permit Name (if different):
Facility Address: is
SUBMIT FORM ON YELLOW PAPER ONLY
NC Z W5/ County
ICiiy( (siatr:) (ZIP)
itact Person: A,. RVW~: e, 11*vILN Telephone#:
II Location/Site Name: No. of wells to be sampled:
]EPARTMENT,OF ENVIRONMENT & NATURAL RESOURCES
71VISION"OF WATER QUALITY -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221
PERMIT Number: Expiration Date:
Non -Discharge IAVbw Ifil UIC
NPDES Other
'PE OF PERMITTED OPERATION BEING MONITORED
71 Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): -M tv--y Date sample collected:
Well Depth: Z2.& ft. Well Diameter: 2 in.
Depth to Water Level: s•(, g p �, 6
p ft. below measuring point Screened Interval: ft. to2?• ft.
Measuring Point is Z • 1 ft. above land surface Relative M.P. Elevation: ft.
Volume of water pumped/bailed before sampling: _gallons
Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO
FIELD ANALYSEtS�:
pH j;_U_f its
Sec. Cond.
p
Odor
Appearance
Temp. S-s °C
µ Mhos
If WELL
WAS
DRY at
time of
sampling,
check
here: ❑
LABORATORY INFORMATION
Date sample analyzed: Z.Zy. - 2 -Zl. ; -1 , 4 -2 -20
p
LaboratoryName: PA[f
�+r5
Certification No. 3 �S
PARAMETERS NOTE: Values should r fl ct d olved and colloidal
concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead
mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mg/1
Zn - Zinc
mg/I
Coliform: MF Total /100ml Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
410L
Orthophosphate mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total IZI Qsrlt
Al -Aluminum
mg/I
pH (when analyzed) units
Ba - Barium
mg/I
TOC mg/I
Ca - Calcium
mg/I
J&A5,
Chloride mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/1
Cu - Copper
mg/I
ORGANICS: (by GC,
GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mg/I
Report Attached?
K Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/1
VOC : JV0
method # IDp 6
Total Ammonia mg/I
Mg - Magnesium
mg/I
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Ferm(ttee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.1/2007
Siqnature of
(Date)
GW-59A COMPLIANCE REPORT FORM Permit 000 161 41
(Submit one each monitoring period with G6i=59 forms-)
1
Enter date monitoring results were due.( •Io Iv) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
NO
iF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office forguidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided belov✓:
X
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES" list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO". monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subiect the permittee to a Notice of Violation
fines, and/or penalties.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the Information submitted r►�thIs
report (Compliance Report,GW-59A} Is, true and complete to the"best of my knowledge
Cif WAI- 3 -13-zo
Signature of Permittee (or Authorized Agent) Date
CW-59A 12/8/2003
q
eAnalytical
Center for Testing &Innovation
ANALYTICAL REPORT
March 05, 2020
F 7C
I qS
Soil & Env. Consultants - Raleigh, NC
[Cn]
Sample Delivery Group: L1193924
Samples Received: 02/28/2020
FSr
Project Number: GW-1 1061-200
Description: Groundwater Job #1061
E
Report To: Mr. Don Wells
1E
8412 Falls of Neuse Road, Suite 104
Al
Raleigh, NC 27615-3543
FSCI
Entire Report Reviewed By
Jason Romer
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/20 13:37 1 of 23
v
' TABLE OF CONTENTS ONE LAB. NATIONWIDE.
Cp: Cover Page
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
MW-2A L1193924-01
5
MW-3 L1193924-02
7
MW-4A L1193924-03
9
TRIP BLANK L1193924-04
11
Qc: Quality Control Summary
13
Gravimetric Analysis by Method 2540 C-2011
13
Wet Chemistry by Method 4500P E-2011
14
Wet Chemistry by Method 5540 C-2011
15
Volatile Organic Compounds (GC/MS) by Method 6200E-2011
16
GI: Glossary of Terms
21
Al: Accreditations & Locations
22
Sc: Sample Chain of Custody
23
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 2 of 23
V
'
SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
Collected by
Collected date/time
Received datettime
MW-2A L1193924-01 GW
Don Wells
02/27/2011:45
02/2812009:00
'' .
Ci-
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
i
date/time
date/time
z
TC
6ravimetric Analysis b Method 2540 C-2011
Y Y
WG1435699
1
03/01/20 09:29
03/01/2010:35
TH Mt. Juliet, TN
Wet Chemistry by Method 4500P E-2011
WG1435688
1
02/28/2015:20
02/28/2015:20
JIC Mt. Juliet, TN
Wet Chemistry by Method 5540 C-2011
WG1435925
1
02/28/2016:48
02/29/2012:11
MSP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
WG1436994
1
03/02/20 21:26
03/02/20 21:26
ADM Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
WG1438158
1
03/04/20 23:28
03/04/20 23:28
ACG Mt. Juliet, TN
Fn
Collected by
Collected date/time
Received date/time
MW-3 L1193924-02 GW
Don Wells
02/27/2011:15
02/28/2009:00
Fr
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
FC
date/time
date/time
6ravimetric Analysis by Method 2540 C-2011
WG1435699
1
03/01/20 09:29
03/01/2010:35
TH Mt. Juliet, TN
Wet Chemistry by Method 4500P E-2011
WG1435688
1
02/28/2015:21
02/28/2015:21
JIC Mt. Juliet, TN
G
Wet Chemistry by Method 5540 C-2011
WG1435925
1
02/28/2016:48
02/29/2012:14
MSP Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
WG1436994
1
03/02/20 21:46
03/02/20 21:46
ADM Mt. Juliet, TN
V AI
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
WG1438158
1
03/04/20 23:47
03/04/20 23:47
ACG Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
FC
MW-4A L1193924-03 GW
Don wells
02/2712012:10
02/28/2009:00
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
6ravimetric Analysis by Method 2540 C-2011
WG1435699
1 03/01/20 09:29
03/01/2010:35
TH
Mt. Juliet, TN
Wet Chemistry by Method 4500P E-2011
WG1435688
1 02/28/2015:22
02/28/2015:22
JIC
Mt. Juliet, TN
Wet Chemistry by Method 5540 C-2011
WG1435925
1 02/28/2016:48
02/29/2012:16
MSP
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
WG1436994
1 03/02/20 22:05
03/02/20 22:05
ADM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
WG1438158
1 03/05/20 00:07
03/05/20 00:07
ACG
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
TRIP BLANK L1193924-04 GW
Don wells
02/27/2000:00
02/28/2009:00
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 62006-2011
WG1436994
1 03/02/20 20:47
03/02/20 20:47
ADM
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200E-2011
WG1438158
1 03/05/20 00:26
03/05/20 00:26
ACG
Mt. Juliet, TN
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 3 of 23
i
' CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
C.0
!_
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
FTChave
been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
rss]
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Fr
FC1
Rl
Jason Romer
CAI
Project Manager
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 4 of 23
MW-2A SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 02/27/20 11:45 L1193924
Gravimetric Analysis by Method 2540 C-2011
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Dissolved Solids
86000
10000
1
03/01/202010:35
W61435699
;-': 71
Wet Chemistry by Method 4500P E-2011
Ss
I
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte
ug/1
ug/I
date / time
Fn
Phosphate,Ortho
ND
25.0
1
02/28/202015:20
WG1435688
Wet Chemistry by Method 5540 C-2011
Result Qualifier
RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Q C
MBAS
ND
100
1
02/29/202012:11
WG1435925
F,
Volatile Organic Compounds (GC/MS) by Method
620OB-2011
Result Qualifier
RDL
Dilution
Analysis
Batch
AI
Analyte
ug/I
ug/I
date / time
Acetone
ND J4
50.0
1
03/02/2020 21:26
WG1436994
Acrolein
ND
50.0
1
03/02/2020 21:26
WG1436994
I q
Acrylonitrile
ND J4
10.0
1
03/02/2020 21:26
WG1436994
Benzene
ND
1.00
1
03/02/2020 21:26
WG1436994
Bromobenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
Bromodichloromethane
ND
1.00
1
03/02/2020 21:26
WG1436994
Bromoform
ND
1.00
1
03/02/2020 21:26
WG1436994
Bromomethane
ND
5.00
1
03/02/2020 21:26
WG1436994
n-Butylbenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
sec-Butylbenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
tert-Butylbenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
Carbon tetrachloride
ND
1.00
1
03/02/2020 21:26
WG1436994
Chlorobenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
Chlorodibromomethane
ND
1.00
1
03/02/2020 21:26
WG1436994
Chloroethane
ND
5.00
1
03/02/2020 21:26
WG1436994
Chloroform
ND
5.00
1
03/02/2020 21:26
WG1436994
Chloromethane
ND
2.50
1
03/02/2020 21:26
WG1436994
2-Chlorotoluene
ND
1.00
1
03/04/2020 23:28
WG1438158
4-Chlorotoluene
ND
1.00
1
03/02/2020 21:26
WG1436994
1,2-Dibromo-3-Chloropropane
ND
5.00
1
03/02/2020 21:26
WG1436994
1,2-Dibromoethane
ND
1.00
1
03/02/2020 21:26
WG1436994
Dibromomethane
ND
1.00
1
03/02/2020 21:26
WG1436994
1,2-Dichlorobenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
1,3-Dichlorobenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
1,4-Dichlorobenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
Dichlorodifluoromethane
ND
5.00
1
03/02/2020 21:26
WG1436994
1,1-Dichloroethane
ND
1.00
1
03/02/2020 21:26
WG1436994
1,2-Dichloroethane
ND
1.00
1
03/02/2020 21:26
WG1436994
1,1-Dichloroethene
ND
1.00
1
03/02/2020 21:26
WG1436994
cis4,2-Dichloroethene
ND
1.00
1
03/02/2020 21:26
WG1436994
trans-1,2-Dichloroethene
ND
1.00
1
03/02/2020 21:26
WG1436994
1,2-Dichloropropane
ND
1.00
1
03/02/2020 21:26
WG1436994
1,1-Dichloropropene
ND
1.00
1
03/02/2020 21:26
WG1436994
1,3-Dichloropropane
ND
1.00
1
03/02/2020 21:26
WG1436994
2,2-Dichloropropane
ND
1.00
1
03/02/2020 21:26
WG1436994
Di -isopropyl ether
ND
1.00
1
03/02/2020 21:26
WG1436994
Ethylbenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
Hexachloro-1,3-butadiene
ND
1.00
1
03/02/2020 21:26
WG1436994
Isopropylbenzene
ND
1.00
1
03/02/2020 21:26
WG1436994
ACCOUNT: PROJECT: SDG: DATEITIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 5 of 23
' MW-2A
SAMPLE RESULTS - 01
ONE LAB. NATIONWIDE.
Collected date/time: 02/27/20 11:45
L1193924
Volatile Organic Compounds
(GUMS) by Method 620OB-2011
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
ug4
ug/I
date / time
p-Isopropyltoluene
ND
1.00 1
03/02/2020 21:26
WG1436994
2-Butanone (MEK)
ND
10.0 1
03/02/2020 21:26
WG1436994
F
Methylene Chloride
ND
5.00 1
03/02/2020 21:26
WG1436994
4-Methyl-2-pentanone (MIBK)
ND
10.0 1
03/02/2020 21:26
WG1436994
FSS
Methyl tert-butyl ether
ND
1.00 1
03/02/2020 21:26
WG1436994
Naphthalene
ND
5.00 1
03/02/2020 21:26
WG1436994
FCn]
n-Propylbenzene
ND
1.00 1
03/04/2020 23:28
WG1438158
Styrene
ND
1.00 1
03/02/2020 21:26
WG1436994
1,1,1,2-Tetrachloroethane
ND
1.00 1
03/02/2020 21:26
WG1436994
1,1,2,2-Tetrachloroethane
ND
1.00 1
03/02/2020 21:26
WG1436994
Tetrachloroethene
ND
1.00 1
03102/202021:26
WG1436994
FC1
Toluene
ND
1.00 1
03/02/2020 21:26
WG1436994
1,2,3-Trichlorobenzene
ND
1.00 1
03/02/2020 21:26
WG1436994
1,2,4-Trichlorobenzene
ND
1.00 1
03/021202021:26
WG1436994
G�
1,1,1-Trichloroethane
ND
1.00 1
03/02/2020 21:26
WG1436994
1,1,2-Trichloroethane
ND
1.00 1
03/02/2020 21:26
WG1436994
Trichloroethene
ND
1.00 1
03/02/2020 21:26
WG1436994
Trichlorofluoromethane
ND
5.00 1
03/02/2020 21:26
WG1436994
1,2,3-Trichloropropane
ND
2.50 1
03/02/2020 21:26
WG1436994
SC
1,2,4-Trimethylbenzene
ND
1.00 1
03/02/2020 21:26
WG1436994
1,3,5-Trimethylbenzene
ND
1.00 1
03/04/2020 23:28
WG1438158
Vinyl chloride
ND
1.00 1
03/02/2020 21:26
WG1436994
o-Xylene
ND
1.00 1
03/02/2020 21:26
WG1436994
m&p-Xylenes
ND
2.00 1
03/02/2020 21:26
WG1436994
(S) Toluene-d8
105
80.0-120
0310212020 2116
WG1436994
(S) Toluene-d8
101
80.0-120
0310412020 23:28
WG1438158
(S) 4-Bromofluorobenzene
97.8
77.0-126
0310212020 21:26
WG1436994
(S) 4-Bromofluorobenzene
100
77.0-126
0310412020 23:18
WG1438158
(S)1,2-Dichloroethane-d4
109
70.0-130
031021202021.26
WG1436994
(S)1,2-Dichloroethane-d4
112
70.0-130
0310412020 23:28
WG1438158
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 6 of 23
c
MW-3 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 02/27/20 11:15 L1193924
Gravimetric Analysis by Method 2540 C-2011
Resuft Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Dissolved Solids 94000
10000 1
03101/202010:35
WG1435699
Wet Chemistry by Method 4500P E-2011
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
Phosphate,Ortho ND
25.0 1
02/28/202015:21
WG1435688
Wet Chemistry by Method 5540 C-2011
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte ug/I
ug/I
date / time
MBAS ND
100 1
02/29/202012:14
WG1435925
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Analyte
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromod ichlorometha ne
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorod ibromometha ne
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropa ne
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
D ichlorod ifluorometha ne
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
H exachloro-1,3-butadie ne
Isopropylbenzene
Result
Qualifier RDL
ug/I
ug/I
ND
J4 50.0
ND
50.0
ND
J4 10.0
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
5.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
5.00
ND
5.00
ND
2.50
ND
1.00
ND
1.00
ND
5.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
5.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
ND
1.00
Dilution Analysis
date / time
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/04/2020 23:47
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
1 03/02/2020 21:46
Batch
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1438158
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
WG1436994
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 7 of 23
' MW-3 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 02/27/20 11:15 L1193924
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Result
Qualifier RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
p-Isopropyltoluene
ND
1.00
1
03/02/2020 21:46
WG1436994
2-Butanone (MEK)
ND
10.0
1
03/02/2020 21:46
WG1436994
Methylene Chloride
ND
5.00
1
03/02/2020 21:46
WG1436994
4-Methyl-2-pentanone (MIBK)
ND
10.0
1
03/02/2020 21:46
WG1436994
Methyl tert-butyl ether
ND
1.00
1
03/02/2020 21:46
WG1436994
Naphthalene
ND
5.00
1
03/02/2020 21:46
WG1436994
n-Propylbenzene
ND
1.00
1
03/04/2020 23:47
WG1438158
Styrene
ND
1.00
1
03/02/2020 21:46
WG1436994
1,1,1,2-Tetrachloroethane
ND
1.00
1
03/02/2020 21:46
WG1436994
1,1,2,2-Tetrachloroethane
ND
1.00
1
03/02/2020 21:46
WG1436994
Tetrachloroethene
ND
1.00
1
03/02/2020 21:46
WG1436994
Toluene
ND
1.00
1
03/02/2020 21:46
WG1436994
1,2,3-Trichlorobenzene
ND
1.00
1
03/02/2020 21:46
WG1436994
1,2,4-Trichlorobenzene
ND
1.00
1
03/02/2020 21:46
WG1436994
1,1,1-Trichloroethane
ND
1.00
1
03/02/2020 21:46
WG1436994
1,1,2-Trichloroethane
ND
1.00
1
03/02/2020 21:46
WG1436994
Trichloroethene
ND
1.00
1
03/02/2020 21:46
WG1436994
Trichlorofluoromethane
ND
5.00
1
03/02/2020 21:46
WG1436994
1,2,3-Trichloropropane
ND
2.50
1
03/02/2020 21:46
WG1436994
1,2,4-Trimethylbenzene
ND
1.00
1
03/02/2020 21:46
WG1436994
1,3,5-Trimethylbenzene
ND
1.00
1
03/04/2020 23:47
WG1438158
Vinyl chloride
ND
1.00
1
03/02/2020 21:46
WG1436994
o-Xylene
ND
1.00
1
03/02/2020 21:46
WG1436994
m&p-Xylenes
ND
2.00
1
03/02/2020 21:46
WG1436994
(S)Toluene-d8
103
80.0-120
031021202021.46
WG1436994
(S) Toluene-d8
101
80.0-120
0310412020 23:47
WG1438158
(S) 4-Bromofluorobenzene
96.9
77.0-126
0310212020 21.46
WG1436994
(S) 4-Bromofluorobenzene
98.8
77.0-126
0310412020 23:47
WG1438158
(S)1,2-Dichloroethone-d4
109
70.0-130
031021202021:46
WG1436994
(S)1,2-Dichloroethone-d4
ill
70.0-130
0310412020 23:47
WG1438158
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 8 of 23
' M W-4A
SAMPLE RESULTS - 03
ONE LAB. NATIONWIDE.
Collected date/time: 02/27/20 12:10
L1193924
Gravimetric Analysis by Method 2540 C-2011
---,
Result Qualifier
RDL Dilution
Analysis
Batch
Cp
Analyte
ug/I
ug/1
date / time
z
Dissolved Solids
123000
10000 1
03/01/202010:35
WG1435699
TC
Wet Chemistry by Method 4500P E-2011
E
Result QualifierRDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Fn
Phosphate,Ortho
ND
25.0 1
02/28/202015:22
WG1435688
Wet Chemistry by Method 5540 C-2011
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte
ugA
ugA
date / time
E
MBAS
ND J6
100 1
02/29/202012:16
WG1435925
�GI
Volatile Organic Compounds
(GC/MS) by Method
620OB-2011
Result Qualifier
RDL Dilution
Analysis
Batch
Analyte
ugA
ug/I
date / time
AI
Acetone
ND J4
50.0 1
03/02/2020 22:05
WG1436994
9
Acrolein
ND
50.0 1
03/02/2020 22:05
WG1436994
SC
Acrylonitrile
ND J4
10.0 1
03/02/2020 22:05
WG1436994
Benzene
ND
1.00 1
03/02/2020 22:05
WG1436994
Bromobenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
Bromodichloromethane
ND
1.00 1
03/02/2020 22:05
WG1436994
Bromoform
ND
1.00 1
03/02/2020 22:05
WG1436994
Bromomethane
ND
5.00 1
03/02/2020 22:05
WG1436994
n-Butylbenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
sec-Butylbenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
tert-Butylbenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
Carbon tetrachloride
ND
1.00 1
03/02/2020 22:05
WG1436994
Chlorobenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
Chlorodibromomethane
ND
1.00 1
03/02/2020 22:05
WG1436994
Chloroethane
ND
5.00 1
03/02/2020 22:05
WG1436994
Chloroform
ND
5.00 1
03/02/2020 22:05
WG1436994
Chloromethane
ND
2.50 1
03/02/2020 22:05
WG1436994
2-Chlorotoluene
ND
1.00 1
03/05/2020 00:07
WG1438158
4-Chlorotoluene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,2-Dibromo-3-Chloropropane
ND
5.00 1
03/02/2020 22:05
WG1436994
1,2-Dibromoethane
ND
1.00 1
03/02/2020 22:05
WG1436994
Dibromomethane
ND
1.00 1
03/02/2020 22:05
WG1436994
1,2-Dichlorobenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,3-Dichlorobenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,4-Dichlorobenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
Dichlorodifluoromethane
ND
5.00 1
03/02/2020 22:05
WG1436994
1,1-Dichloroethane
ND
1.00 1
03/02/2020 22:05
WG1436994
1,2-Dichloroethane
ND
1.00 1
03/02/2020 22:05
WG1436994
1,1-Dichloroethene
ND
1.00 1
03/02/2020 22:05
WG1436994
cis-1,2-Dichloroethene
ND
1.00 1
03/02/2020 22:05
WG1436994
trans4,2-Dichloroethene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,2-Dichloropropane
ND
1.00 1
03/02/2020 22:05
WG1436994
1,1-Dichloropropene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,3-Dichloropropane
ND
1.00 1
03/02/2020 22:05
WG1436994
2,2-Dichloropropane
ND
1.00 1
03/02/2020 22:05
WG1436994
Di -Isopropyl ether
ND
1.00 1
03/02/2020 22:05
WG1436994
Ethylbenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
Hexachloro-1,3-butadiene
ND
1.00 1
03/02/2020 22:05
WG1436994
Isopropylbenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC
GW-11061-200
L1193924
03/05/2013:37 9 of 23
lb
# MW-4A
SAMPLE RESULTS - 03
ONE LAB. NATIONWIDE. *
Collected date/time: 02/27/20 12:10
L1193924
Volatile Organic Compounds
(GUMS) by Method 620OB-2011
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
p-Isopropyltoluene
ND
1.00 1
03/02/2020 22:05
WG1436994
2-Butanone (MEK)
ND
10.0 1
03/02/2020 22:05
WG1436994
Methylene Chloride
ND
5.00 1
03/02/2020 22:05
WG1436994
4-Methyl-2-pe nta none (MIBK)
ND
10.0 1
03/02/2020 22:05
WG1436994
E
Methyl tert-butyl ether
ND
1.00 1
03/02/2020 22:05
WG1436994
Naphthalene
ND
5.00 1
03/02/2020 22:05
WG1436994
[Cn]
n-Propylbenzene
ND
1.00 1
03/05/2020 00:07
WG1438158
Styrene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,1,1,2-Tetrachloroethane
ND
1.00 1
03/02/2020 22:05
WG1436994
1,1,2,2-Tetrachloroethane
ND
1.00 1
03/02/2020 22:05
WG1436994
Tetrachloroethene
ND
1.00 1
03/02/2020 22:05
WG1436994
rQC1
Toluene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,2,3-Trichlorobenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
FGI
1,2,4-Trichlorobenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,1,1-Trichloroethane
ND
1.00 1
03/02/2020 22:05
WG1436994
1,1,2-Trichloroethane
ND
1.00 1
03/02/2020 22:05
WG1436994
QAI
Trichloroethene
ND
1.00 1
03/02/2020 22:05
WG1436994
Trichlorofluoromethane
ND
5.00 1
03/02/2020 22:05
WG1436994
1,2,3-Trichloropropane
ND
2.50 1
03/02/2020 22:05
WG1436994
FC
1,2,4-Trimethylbenzene
ND
1.00 1
03/02/2020 22:05
WG1436994
1,3,5-Trimethylbenzene
ND
1.00 1
03/05/2020 00:07
WG1438158
Vinyl chloride
ND
1.00 1
03/02/2020 22:05
WG1436994
o-Xylene
ND
1.00 1
03/02/2020 22:05
WG1436994
m&p-Xylenes
ND
2.00 1
03/02/2020 22:05
WG1436994
(S)Toluene-d8
105
80.0-120
031021202022.05
WG1436994
(S) Toluene-d8
102
80.0-120
0310512020 00.07
WG1438158
(S) 4-Bromofluorobenzene
98.8
77.0-126
0310212020 21:05
WG1436994
(S) 4-Bromofluorobenzene
103
77.0-126
0310512020 00:07
WG1438158
(S)1,2-Dichloroethane-0
108
70.0-130
031021202022:05
WG1436994
(S)1,1-Dichloroethane-d4
113
70.0-130
031051202000.07
WG1438158
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 03/05/2013:37 10 of 23
' TRIP BLANK SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE.
Collected date/time: 02/27/20 00:00 L1193924
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
ResuR
Qualifier RDL
Dilution
Analysis
Batch
Analyte
ug/I
ug/I
date / time
Acetone
ND
J4 50.0
1
03/02/2020 20:47
WG1436994
T
Acrolein
ND
50.0
1
03/02/2020 20:47
WG1436994
Acrylonitrile
ND
J4 10.0
1
03/021202020:47
WG1436994
3SS]
Benzene
ND
1.00
1
03/02/2020 20:47
WG1436994
Bromobenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
Bromodichloromethane
ND
1.00
1
03/021202020:47
WG1436994
Cn
Bromoform
ND
1.00
1
03/02/2020 20:47
WG1436994
Bromomethane
ND
5.00
1
03/02/2020 20:47
WG1436994
n-Butylbenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
sec-Butylbenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
tert-Butylbenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
Carbon tetrachloride
ND
1.00
1
03/02/2020 20:47
WG1436994
Chlorobenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
GI
Chlorodibromomethane
ND
1.00
1
03/02/2020 20:47
WG1436994
Chloroethane
ND
5.00
1
03/02/2020 20:47
WG1436994
Chloroform
ND
5.00
1
03/02/2020 20:47
WG1436994
Chloromethane
ND
2.50
1
03/02/2020 20:47
WG1436994
2-Chlorotoluene
ND
1.00
1
03/05/202000:26
WG1438158
SC
4-Chlorotoluene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,2-Dibromo-3-Chloropropane
ND
5.00
1
03/02/202020:47
WG1436994
1,2-Dibromoethane
ND
1.00
1
03/02/2020 20:47
WG1436994
Dibromomethane
ND
1.00
1
03/02/2020 20:47
WG1436994
1,2-Dichlorobenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,3-Dichlorobenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,4-Dichlorobenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
Dichlorodifluoromethane
ND
5.00
1
03/02/2020 20:47
WG1436994
1,1-Dichloroethane
ND
1.00
1
03/02/2020 20:47
WG1436994
1,2-Dichloroethane
ND
1.00
1
03/02/2020 20:47
WG1436994
1,1-Dichloroethene
ND
1.00
1
03/02/2020 20:47
WG1436994
cis-1,2-Dichloroethene
ND
1.00
1
03/02/2020 20:47
WG1436994
trans-1,2-Dichloroethene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,2-Dichloropropane
ND
1.00
1
03/02/2020 20:47
WG1436994
1,1-Dichloropropene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,3-Dichloropropane
ND
1.00
1
03/02/2020 20:47
WG1436994
2,2-Dichloropropane
ND
1.00
1
03/02/2020 20:47
WG1436994
DI -Isopropyl ether
ND
1.00
1
03/02/2020 20:47
WG1436994
Ethylbenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
Hexachloro-1,3-butadiene
ND
1.00
1
03/02/2020 20:47
WG1436994
Isopropylbenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
p-Isopropyltoluene
ND
1.00
1
03/02/2020 20:47
WG1436994
2-Butanone (MEK)
ND
10.0
1
03/02/2020 20:47
WG1436994
Methylene Chloride
ND
5.00
1
03/02/2020 20:47
WG1436994
4-Methyl-2-pentanone (MIBK)
ND
10.0
1
03/02/2020 20:47
WG1436994
Methyl tert-butyl ether
ND
1.00
1
03/02/2020 20:47
WG1436994
Naphthalene
ND
5.00
1
03/02/2020 20:47
WG1436994
n-Propylbenzene
ND
1.00
1
03/05/202000:26
WG1438158
Styrene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,1,1,2-Tetrachloroethane
ND
1.00
1
03/02/2020 20:47
WG1436994
1,1,2,2-Tetrachloroethane
ND
1.00
1
03/02/2020 20:47
WG1436994
Tetrachloroethene
ND
1.00
1
03/02/2020 20:47
WG1436994
Toluene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,2,3-Trichlorobenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,2,4-Trichlorobenzene
ND
1.00
1
03/02/2020 20:47
WG1436994
1,1,1-Trichloroethane
ND
1.00
1
03/02/2020 20:47
WG1436994
1,1,2-Trichloroethane
ND
1.00
1
03/02/2020 20:47
WG1436994
Trichloroethene
ND
1.00
1
03/02/2020 20:47
WG1436994
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 11 of 23
` TRIP BLANK SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE.
Collected date/time: 02/27/20 00:00 L1193924
Volatile Organic Compounds (GUMS) by Method 6200E-2011
Analyte
Trichlorofluoromethane
1,2,3-Trich loropropa ne
1,2,4-Trimethylbe nzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
m&p-Xylenes
(S) Toluene-d8
(S) Toluene-d8
(S) 4-Bromot7uorobenzene
(S) 4-Bromof7uorobenzene
(S)1,2-Dichloroethone-d4
(S)1,1-Dichloroethone-d4
Result
Qualifier. RDL
Dilution
Analysis
Batch
ug/I
ug/I
date / time
ND
5.00
1
03/02/2020 20:47
WG1436994
ND
2.50
1
03/02/2020 20:47
WG1436994
ND
1.00
1
03/02/2020 20:47
WG1436994
ND
1.00
1
03/05/2020 00:26
WG1438159
ND
1.00
1
03/02/2020 20:47
WG1436994
ND
1.00
1
03/02/2020 20:47
WG1436994
ND
2.00
1
03/02/2020 20:47
WG1436994
104
80.0-120
031021202020.47
WG1436994
101
80.0-120
0310512020 00:26
WG1438158
98.5
77.0-126
031OZ2020 20.47
WG1436994
100
77.0-126
0310512020 00.26
WG1438158
109
70.0-130
0310212020 20.47
WG1436994
ill
70.0-130
0310512020 00:26
WG1438158
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 12 of 23
WG1435699
Gravimetric Analysis by Method 2540 C-2011
Method Blank (MB)
(MB) R3504533-1 03/01/2010:35
MB Result
Analyte ug/I
Dissolved Solids U
MB Qualifier MB MDL MB ROL
ug/I ug/I
2820 10000
L1193940-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
1-1193924-01,02,03
(OS) L1193940-01 03/01/2010:35 • (DUP) R3504533-3 03/01/2010:35
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Dissolved Solids 1090000 1160000 1 6.25 J3 5
Laboratory Control Sample (LCS)
(LCS) R3504533-2 03/01/2010:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
Dissolved Solids 8800000 8410000 95.6 85.0-115
ONE LAB. NATIONWIDE. *-
9
Sc
ACCOUNT: PROJECT: SDG:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924
DATE/TIME:
03/05/20 13:37
PAGE:
13 of 23
WG1435688 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. a"
Wet Chemistry by Method 4500P E-2011 11193924-01,02,03
Methnd Rlank (MR)
(MB) R3504033-1 02/28/2015:19
MB Result
Analyte ug/I
Phosphate,Ortho U
MB Qualifier MB MDL MB RDL
ug/1 ug/1
9.00 25.0
L1193893-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1193893-01 02/28/2016:07 • (DUP) R3504033-5 02/28/2016:26
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
Phosphate,Ortho 73400 73500 100 0.161 20
Laboratory Control Sample (LCS)
(LCS) R3504033-2 02/28/2015:19
Spike Amount LCSResult LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
Phosphate,Ortho 245 254 104 85.0-115
L1193924-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1193924-03 02/28/2015:22 • (MS) R3504033-3 02/28/2015:22 • (MSD) R3504033-4 02/28/2015:22
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/I ug/I ug/I ug/I % % % %
Phosphate,Ortho 500 ND 504 518 101 104 1 80.0-120 2.74 20
ACCOUNT: PROJECT: SDG:
Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924
DATEMME:
03/0512013:37
PAGE:
14 of 23
WG1435925 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.'
Wet Chemistry by Method 5540 C-2011 1-1193924-01,02,03
e
Method Blank (MB)
(MB) R3504190-1 02/29/20 12:01
MB Result
Analyte ug/I
MBAS U
MB Qualifier MB MDL MB ROL
ug/I ug/I
19.0 100
L1193924-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1193924-01 02/29/2012:11 • (DUP) R3504190-3 02/29/2012:12
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/I ug/I % %
MBAS ND 33.0 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3504190-2 02/29/2012:04
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
MBAS 1000 997 99.7 85.0-115
L1193924-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1193924-03 02/29/2012:16 • (MS) R3504190-4 02/29/2012:17 • (MSD) R3504190-5 02/29/20 12:19
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte ug/I ug/I ug/I ug/I % % % %
MBAS 1000 ND 691 739 65.7 70.5 1 85.0-115 16 J6 6.71
RPD Limits
20
ACCOUNT: PROJECT: SDG:
Soil & Env. Consultants- Raleigh, NC GW-1 1061-200 L1193924
DATE/TIME:
03/05/20 13:37
PAGE:
15 of 23
WG1436994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. *- ,
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Method Blank (MB)
(MB) R3505370-3 03/02/20 19:01
MB Result
Analyte
Ug/I
Acetone
U
Acrolein
U
Acrylonitrile
U
Benzene
U
Bromobenzene
U
Bromodichloromethane
U
Bromoform
U
Bromomethane
U
n-Butylbenzene
U
sec-Butylbenzene
U
tert-Butylbenzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chlorodibromomethane
U
Chloroethane
U
Chloroform
U
Chloromethane
U
4-Chlorotoluene
U
1,2-Dibromo-3-Chloropropane
U
1,2-Dibromoethane
U
Dibromomethane
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
Dichlorodifluoromethane
U
1,1-Dichloroethane
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
cis-1,2-Dichloroethene
U
trans-1,2-Dichloroethene
U
1,2-Dichloropropane
U
1,1-Dichloropropene
U
1,3-Dichloropropane
U
2,2-Dichloropropane
U
Di -isopropyl ether
U
Ethylbenzene
U
Hexachloro-1,3-butadiene
U
Isopropylbenzene
U
p-Isopropyltoluene
U
2-Butanone (MEK)
U
L1193924-01,02,03,04
MB Qualifier MB MDL
MB RDL
ug/I
ug/I
nc
10.0
50.0
8.87
50.0
3
SS
1.87
10.0
0.331
1.00
0.352
1.00
FC
0.380
1.00
0.469
1.00
Fr
0.866
5.00
0.361
1.00
0.365
1.00
01
0.399
1.00
0.379
1.00
E
0.348
1.00
0.327
1.00
0.453
5.00
0.324
5.00
0.276
2.50
e
SC
0.351
1.00
1.33
5.00
0.381
1.00
0.346
1.00
0.349
1.00
0.220
1.00
0.274
1.00
0.551
5.00
0.259
1.00
0.361
1.00
0.398
1.00
0.260
1.00
0.396
1.00
0.306
1.00
0.352
1.00
0.366
1.00
0.321
1.00
0.320
1.00
0.384
1.00
0.256
1.00
0.326
1.00
0.350
1.00
3.93
10.0
w
ACCOUNT: PROJECT: SDG:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924
DATEITIME:
03/05/2013:37
PAGE:
16 of 23
WG1436994
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS)
by Method 6200E-2011
L1193924-01,02,03,04
F
Method Blank (MB)
(MB) R3505370-3 03/02/20 19:01
MB Result
MB Qualifier MB MDL
MB RDL
Analyte Ug/I
Ug/I
Ug/l
Ec
Methylene Chloride U
1.00
5.00
4-Methyl-2-pentanone (MIBK) U
2.14
10.0
FS
Methyl tert-butyl ether U
0.367
1.00
Naphthalene U
1.00
5.00
Styrene U
0,307
1.00
[qn
1,1,1,2-Tetrachloroethane U
0.385
1.00
1,1,2,2-Tetrachloroethane U
0.130
1.00
FirTetrachloroethene
U
0.372
1.00
Toluene U
0.412
1.00
1,2,3-Trichlorobenzene U
0.230
1.00
�
1,2,4-Trichlorobenzene U
0.355
1.00
1,1,1-Trichloroethane U
0.319
1.00
2G1
1,1,2-Trichloroethane U
0.383
1.00
Trichloroethene U
0.398
1.00
s
Trichlorofluoromethane U
1.20
5.00
Ai
1,2,3-Tdchloropropane U
0.807
2.50
1,2,4-Trimethylbenzene U
0.373
1.00
e
Sc
Vinyl chloride U
0.259
1.00
o-Xylene U
0.341
1.00
m&p-Xylenes U
0.719
2.00
(S) Toluene-d8 104
80.0-120
(S) 4-Bromoiluorobenzene 96.1
77.0-126
(S)1,2-Dichloroethone-d4 108
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3505370-1 03/02/2017:43 • (LCSD) R3505370-2 03/02/2018:03
Spike Amount
LCS Result
LCSD Result
LCS Rec. LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
Ug/I
%
%
%
%
%
Acetone
25.0
49.9
48.0
200
192
19.0-160
J4 J4 3.88
27
Acrolein
25.0
19.9
19.7
79.6
78.8
10.0-160
1.01
26
Acrylonitrile
25.0
46.7
46.4
187
186
55.0-149
J4 J4 0.644
20
Benzene
5.00
4.53
4.56
90.6
91.2
70.0-123
0,660
20
Bromobenzene
5.00
3.85
3.85
77.0
77.0
73.0-121
0.000
20
Bromodichloromethane
5.00
4.49
4.51
89.8
90.2
75.0-120
0.444
20
Bromoform
5.00
5.03
5.05
101
101
68.0-132
0.397
20
Bromomethane
5.00
4.80
4.57
96.0
91.4
10.0-160
4.91
25
n-Butylbenzene
5.00
4.73
4.66
94.6
93.2
73.0-125
1.49
20
sec-Butylbenzene
5.00
4.14
4.08
82.8
81.6
75.0-125
1.46
20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC
GW-11061-200
L1193924
03/05/2013:37 17 of 23
WG1436994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.'
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1193924-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3505370-1 03/02/20 17:43 • (LCSD) R3505370-2 03/02/2018:03
Spike Amount
LCS ResuR
LCSD Result
LCS Rec. LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
ug/I
ug/I
ug/I
%
%
%
%
%
tert-Butylbenzene
5.00
3.93
3.82
78.6
76.4
76.0-124
2.84
20
Carbon tetrachloride
5.00
4.73
4.64
94.6
92.8
68.0-126
1.92
20
Chlorobenzene
5.00
4.71
4.71
94.2
94.2
80.0-121
0.000
20
Chlorodibromomethane
5.00
4.72
4.95
94.4
99.0
77.0-125
4.76
20
Chloroethane
5.00
4.73
4.59
94.6
91.8
47.0-150
3.00
20
Chloroform
5.00
4.62
4.56
92.4
91.2
73.0-120
1.31
20
Chloromethane
5.00
5.46
5.06
109
101
41.0-142
7.60
20
4-Chlorotoluene
5.00
3.81
3.87
76.2
77.4
75.0-122
1.56
20
1,2-Dibromo-3-Chloropropane
5.00
5.93
5.62
119
112
58.0-134
5.37
20
1,2-Dibromoethane
5.00
4.99
5.13
99.8
103
80.0422
2.77
20
Dibromomethane
5.00
5.07
5.01
101
100
80.0-120
1.19
20
1,2-Dichlorobenzene
5.00
5.00
4.98
100
99.6
79.0-121
0.401
20
1,3-Dichlorobenzene
5.00
4.67
4.59
93.4
91.8
79.0-120
1.73
20
1,4-Dichlorobenzene
5.00
4.72
4.73
94.4
94.6
79.0-120
0.212
20
Dichlorodifluoromethane
5.00
4.52
4.45
90.4
89.0
51.0-149
1.56
20
1,1-Dichloroethane
5.00
4.89
4.59
97.8
91.8
70.0-126
6.33
20
1,2-Dichloroethane
5.00
5.06
5.10
101
102
70.0-128
0.787
20
1,1-Dichloroethene
5.00
4.34
4.30
86.8
86.0
71.0-124
0.926
20
cis-1,2-Dichloroethene
5.00
4.79
4.72
95.8
94.4
73.0-120
1.47
20
trans4,2-Dichloroethene
5.00
4.49
4.43
89.8
88.6
73.0-120
1.35
20
1,2-Dichloropropane
5.00
5.12
5.15
102
103
77.0-125
0.584
20
1,1-Dichloropropene
5.00
4.63
4.58
92.6
91.6
74.0-126
1.09
20
1,3-Dichloropropane
5.00
5.04
5.16
101
103
80.0-120
2.35
20
2,2-Dichloropropane
5.00
4.02
3.88
80.4
77.6
58.0-130
3.54
20
Di -isopropyl ether
5.00
5.04
4.97
101
99.4
58.0-138
1.40
20
Ethylbenzene
5.00
4.61
4.74
92.2
94.8
79.0-123
2.78
20
Hexachloro4,3-butadiene
5.00
4.32
4.31
86.4
86.2
54.0-138
0.232
20
Isopropylbenzene
5.00
4.60
4.54
92.0
90.8
76.0-127
1.31
20
p-Isopropyltoluene
5.00
4.28
4.16
85.6
83.2
76.0-125
2.84
20
2-Butanone (MEK)
25.0
38.6
39.3
154
157
44.0-160
1.80
20
Methylene Chloride
5.00
4.83
4.72
96.6
94.4
67.0-120
2.30
20
4-Methyl-2-pentanone (MIBK)
25.0
30.8
31.1
123
124
68.0-142
0.969
20
Methyl tert-butyl ether
5.00
4.95
5.08
99.0
102
68.0-125
2.59
20
Naphthalene
5.00
5.19
5.19
104
104
54.0-135
0.000
20
Styrene
5.00
4.62
4.64
92.4
92.8
73.0-130
0.432
20
1,1,1,2-Tetrachloroethane
5.00
4.59
4.64
91.8
92.8
75.0-125
1.08
20
1,1,2,2-Tetrachloroethane
5.00
4.10
4.28
82.0
85.6
65.0-130
4.30
20
Tetrachloroethene
5.00
4.61
4.69
92.2
93.8
72.0-132
1.72
20
Toluene
5.00
4.60
4.59
92.0
91.8
79.0-120
0.218
20
1,2,3-Ticchoorobenzene
5.00
4.63
4.65
92.6
93.0
50.0-138
0.431
20
ACCOUNT:
PROJECT:
SDG:
DATEITIME:
Soil & Env. Consultants - Raleigh,
NC
GW-11061-200
L1193924
03/05/2013:37
PAGE:
18of23
WG1436994 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. `
Volatile Organic Compounds (GC/MS) by Method 6200E-2011 L1193924-01,02,03,04
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3505370-1 03/02/20 17:43 • (LCSD) R3505370-2 03/02/20 18:03
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
ug/I
%
%
%
1,2,4-Trichlorobenzene
5.00
4.79
4.79
95.8
95.8
57.0-137
1,1,1-Trichloroethane
5.00
4.45
4.37
89.0
87.4
73.0-124
1,1,2-Trichloroethane
5.00
4.97
5.05
99.4
101
80.0-120
Trichloroethene
5.00
4.69
4.40
93.8
88.0
78.0-124
Trichlorofluoromethane
5.00
4.37
4.28
87.4
85.6
59.0-147
1,2,3-Trichloropropane
5.00
4.64
4.59
92.8
91.8
73.0-130
1,2,4-Trimethylbenzene
5.00
4.15
4.12
83.0
82.4
76.0-121
Vinyl chloride
5.00
5.18
5.06
104
101
67.0-131
o-Xylene
5.00
4.62
4.63
92.4
92.6
80.0-122
m&p-Xylenes
10.0
9.40
9.37
94.0
93.7
80.0-122
(S Toluene -dB
102
102
80.0-120
(S 4-Bromotluorobenzene
100
98.4
77.0-126
(S)1,2-Dichloroethone-d4
112
ill
70.0-130
LCSD Qualifier RPD
RPD Limits
0.000
20
1.81
20
1.60
20
6.38
20
2.08
20
1.08
20
0.726
20
2.34
20
0.216
20
0.320
20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 03/05/2013:37 19 of 23
WG1438158
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Method Blank (MB)
QUALITY
CONTROL SUMMARY
L1193924-01,02,03,04
ONE LAB. NATIONWIDE."
(MB) R3505497-2 03/04/20 21:31
MB Result MB Qualifier
MB MDL
MB RDL
Analyte ug/I
ug/I
ug/1
ITC]
2-Chlorotoluene U
0.375
1.00
n-Propylbenzene U
0.349
1.00
3
SS
1,3,5-Trimethylbenzene U
0.387
1.00
(S) Toluene-d8 103
80.0-120
(S)4-Bromofluorobenzene 104
77.0-126
Rn
(S)1,2-Dichloroethane-d4 110
70.0-130
SSr
Laboratory Control Sample (LCS) • Laboratory
Control
Sample
Duplicate (LCSD)
(LCS) R3505497-1 03/04/20 19:44 • (LCSD) R3505497-3 03/04/20 22:49
Spike Amount LCS Result
Analyte ug/I ug/I
LCSD Result
ug/I
LCS Rec.
%
LCSD Rec.
%
Rec. Limits LCS Qualifier LCSD Qualifier
%
RPD
%
RPD Limits
%
GI
2-Chlorotoluene 5.00 4.43
4.52
88.6
90.4
76.0-123
2.01
20
n-Propylbenzene 5.00 4.39
4.43
87.8
88.6
77.0-124
0.907
20
3AI
1,3,5-Trimethylbenzene 5.00 4.51
4.67
90.2
93.4
76.0-122
3.49
20
(S) Toluene -dB
97.9
99.2
80.0-120
(S) 4-Bromofluorobenzene
104
101
77.0-126
FSC
(S)1,2-Dich/oroethane-d4
112
ill
70.0-130
ACCOUNT: PROJECT: SDG:
Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924
DATE/TIME:
03/05/2013:37
PAGE:
20 of 23
GLOSSARY OF TERMS
ONE LAB. NATIONWIDE. #
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) -Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or'BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-1 1061-200 L1193924 03/05/2013:37 21 of 23
ACCREDITATIONS & LOCATIONS
ONE LAB. NATIONWIDE.
Pace National Is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratodes in our Industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing 1 Cc
turnaround time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. j
' Not all certifications held by the laboratory are applicable to the results reported in the attached report —
Accreditation is onty applicable to the test methods specified on each scope of accreditation held by Pace National. FT
State Accreditations `-_..
Alabama 40660 Nebraska NEOS-15-05 PS
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975 Fn
Arkansas 88-0469 New Jersey—NELAP TNO02
California 2932 New Mexico' n/a
Colorado TN00003 New York 11742 Fr
Connecticut PH 0197 North Carolina Env375
Florida E87487 North Carolina' DW21704
Georgia NELAP North Carolina' 41
6
Georgia' 923 North Dakota R-140 CSC
Idaho TN00003 Ohio—VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002 F
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LA000356
Kentucky'" 90010 South Carolina 84004
Kentucky 2 16 South Dakota n/a
Louisiana A130792 Tennessee " 2006
Louisiana' LA180010 Texas T104704245-18-15 Fc
Maine TN0002 Texas' LABO152
Maryland 324 Utah TN00003
Massachusetts M-TNO03 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A21-A
Third Party Federal Accreditations
A21-A— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A21-A— ISO 170251461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
' Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity 'Chemical/Microbiological 'Mold 'Wastewater Na Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Soil & Env. Consultants - Raleigh, NC GW-11061-200 L1193924 03/05/2013:37 22 of 23
Billing Information:
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Mr. Don Wells
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