NC0022217_Fact Sheet_20200624

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
DENR / DWR / NPDES
EXPEDITED FACT SHEET - NPDES PERMIT RENEWAL
NPDES Permit NCO022217
Permit Writer: Joe R. Corporon, P.G. 18Jun2020 we
Facility Information
Facility Name
Motiva Enterprises, LLC
Applicant
Motiva Enterprises — Raleigh Terminal
Contact
Kenneth Watson (919-3628341); [[e-mail]]
Applicant Address
2232 Ten Ten Road, Apex 27539-8115
Facility Address
Same
Permitted Flow (MGD)
Not limited
Type of Waste
Stormwater held in proximity to above -ground storage tanks (ASTs)
containing fuel hydrocarbons >Imillion gallons.
Facility Class
I County
Wake
Facility Status
Renewal
I Regional Office
RRO
Stream Characteristics
Receiving Stream
UT to Middle Creek,
Neuse River Basin
Stream Classification
C; NSW
Stream Segment
27-43-15-(1)
Drainage basin
Neuse
Summer 7Q10 (cfs)
0.0
Subbasin
03-04-03
Winter 7Q10 (cfs)
0.0
Use Support?
NSW
30Q2 (cfs)
0.0
303(d) Listed?
No
Average Flow (cfs)
0.0
State Grid
E23NE
IWC (%) mi
100
USGS Topo Quad
Apex, NC
Facility Summaly — Because this facility stores hydrocarbon fuels at the ground surface in
quantities exceeding one (1) million gallons, it is specifically excluded from coverage under North
Carolina Stormwater Regulations, and therefore historically has been permitted under an
individual NPDES permit.
This facility's holding pond [secondary containment] confines stormwater and tank restoration
wastewaters potentially contaminated with fuel -hydrocarbons. The pond is equipped with a gravity
drain controlled by a hand -operated valve, normally closed. This controlled discharge constitutes a
point source discharge to the environment. Holding areas receive discharges from both bermed
areas [AST dikes] and stormwater runoff from a truck -loading rack. A portion of the loading rack
discharge is separated [oil -water separator], then containerized and shipped offsite for recycling.
There have been no significant changes in facility operations since last renewal. This renewal
reflects adjustments required of updated Permitting Guidance only.
WET Testing — This permit requires Acute Whole Effluent Toxicity (WET) testing using Fathead
Minnow (Pimephales promelas), 24-hr definitive, LC-50 >100% [TAE6C]. Since last renewal
(April 2008) the Permittee reports all WET testing as "PASS" in 6 of 6 samples at Outfall 001.
Acute WET testing monitoring frequency was relaxed to Annual prior to the previous permit cycle
— no changes recommended.
Fact Sheet
Renewal 2020 -- NPDES Permit NCO022217
Page 1 of 2

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SUMMARY OF FLOW (MGD) — Jan2016-May2019:
• Outfall 001
Max
Ave
Min
Discharges (n)
^
• 2016
0.420
0.191
0.21
17
0 2017
0.378
0.189
0.21
13
0 2018
0.336
0.185
0.42
16
• 2019
0.336
0.225
0.063
14 [thru May]
Outfall 001 — WET & Reasonable Potential Analysis (RPA) — Not Conducted Because:
• BTEX not detected n = 31
• MTBE not detected n = 26
• Naphthalene not detected n = 31
• Oil & Grease n = 31 Ave = 5.07 mg/L Max = 5.9 mg/L
• WET [TAE6C] Pass n = 4 Annual
The Division finalized permitting strategy for the Neuse River Basin (2013), currently classified
nutrient sensitive waters (NSW). Considering this facility's SIC Code [5171 ] and its minimal
flow (< 0.050 MGD, not limited), the Permittee is exempt under State Regulation NCAC 02B
.0508, i.e., is not required to monitor for nitrogen (TN) and phosphorus (TP).
Renewal Summary
1. in accord with Petroleum Bulk Storage Guidance (2005), relaxed monitoring
for BTEX, MTBE, Naphthalene, and Oil & Grease from Monthly to
Quarterly based on analytical results reported as "not detected;"
2. added regulatory citations appropriate to each permit Section;
3. updated WET —testing page [Section A. (2.)];
4. updated facility description and Vicinity Map;
5. Updated text detailing eDMR requirements.
Fact Sheet
Renewal -- NPDES NC0022217
Page 2 of 2

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit Number NCO022217
Program Category
NPDES WW
Permit Type
Industrial Process & Commercial Wastewater Discharge
Primary Reviewer
joe.corporon
Coastal SW Rule
Permitted Flow
Facilit
Central Files: APS SWP
09/05/13
Permit Tracking Slip
Status Project Type
In draft Renewal
Version Permit Classification
Individual
Permit Contact Affiliation
Nicola A. Ellis
2232 Ten Ten Rd
Apex NC 27502
Facility Name Major/Minor Region
Apex Terminal Minor Raleigh
Location Address County
2232 Ten Ten Rd Wake
Apex NC 27502 Facility Contact Affiliation
Owner
Owner Name
Owner Type
Motiva Enterprises LLC
Non -Government
Owner Affiliation
Jill J. Norman
Engineer Environmental
1717 - 61 st Ave N
Nashville TN 37209
Dates/Events
Scheduled
Orig Issue App Received Draft Initiated Issuance
Public Notice Issue Effective Expiration
12/31 /79 10/19/12 09/05/13
Regulated Activities
Requested/Received Events
Groundwater remediation
Region comments on draft requested
Leather and leather products manufacture
Region comments on draft received
Outfall 001
Waterbody Name Stream Index Number Current Class Subbasin
Middle Creek 27-43-15-(1) C;NSW 03-04-03

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Waxer Resources
ENVIRONMENTAL QUALITY
October 24, 2017
Scott Dilling, Complex Manager
Motiva Enterprises LLC
410 Tom Sadler Rd
Charlotte, NC 28214
Subject: Permit Renewal
Application No. NCO022217
Apex Terminal
Wake County
Dear Applicant:
ROY COOPER
Gowemar
MICHAEL S. REGAN
secretary
S. JAY ZIMMERMAN
lfmor
The Water Quality Permitting Section acknowledges the October 23, 2017 receipt of your permit renewal application
and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 15OB-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit.
The permit writer will contact you if additional information is required to complete your permit renewal. Please respond
in a timely manner to requests for additional information necessary to allow a complete review of the application and
renewal of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq. nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
.J�SincereYdfk
Wren Td
Administrative Assistant
Water Quality Permitting Section
cc: Central Files w/application(RRO)
ec: WQPS Laserfiche File w/application
State of North Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919-807-6300

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
MOTIVA
ENTERPRISES LLC
October 23, 2017
John Hennessy
512 N. Salisbury Street (9th Floor -Archdale Bldg)
Raleigh, NC 27604
Phone: [phone]
RE: NPDES Minor Industrial Permit Renewal Application
Motiva Enterprises, LLC Apex Terminal
Permit No. NCO022217
Dear Mr. Hennessy,
Please find included with this cover letter, Motiva's NPDES minor industrial permit renewal
application for our bulk terminal in Apex, North Carolina. Our current permit expires on April
30, 2018. This application is being submitted more than 180 days prior to expiration of the
permit as required.
This application is not requesting any modification to the current design of our NPDES storm
water and wastewater system and includes the following:
• Application Form —Short Form C
• Attachment I —Topographical Map and Process Flow Diagram
• Attachment II — Detailed Sampling Results August 2014 - August 2017
If you have any questions, please contact Kristine Pelt at [phone] or
[e-mail].
Very Ury�yo ,
D. Scott Dilling
Complex Manager
Enclosures
cc: Kristine Pelt (electronic)
file 550-03
RECEIVEMCDEQ/M
OCT 2 3 2017
Water Quality
Permitting Section

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
Mail the complete application to:
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
1. Contact Information:
Owner Name
Facility Name
Mailing Address
City
State / Zip Code
Telephone Number
Fax Number
e-mail Address
NPDES Permit Number INCO022217
Please print or type.
Motiva Enterprises LLC
Motiva Enterprises LLC - Raleigh Terminal
2232 Ten Ten Road
Apex
NC 27539-8115
[phone]
Kristine. Pelt@Motiva. Com
2. Location of facility producing discharge:
Check here if same as above
Street Address or State Road
City
State / Zip Code
County
Wake
3. Operator Information:
Name of the firm, consultant or other entity that operates the facility (Note that this is not referring to the
Operator in Responsible Charge or ORC)
Name Motiva Enterprises LLC
Mailing Address
City
State / Zip Code
Telephone Number
Fax Number
2232 Ten Ten Road
Apex
NC 27539-8115
[phone]
Page 1 of 4 C-MI 10/08

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
4. Ownership Status:
Federal ❑
State ❑
Private
S. Standard Industrial Classification (SIC) code(s): 5171
6. Number of employees_
Public ❑
7. Describe the treatment system List all installed waste treatment components with capacities,
describe the processes that generate wastewaters If the space proinded is not sufficient attach a
separate sheet of paper with the system description
An oil -water separator (OWS) receives water from the truck loading rack. Water from the OWS
is routed to a 10,000-gallon tank in the tank dike area. The tank is equipped with a
hydrocarbon sensor and level control. A figure is included in Attachment I.
8. Is facility covered under federal effluent limitation guidelines? No ® Yes ❑
If yes, specify the category?
9. Principal product(s) produced: No products are produced. The facility is a bulk terminal for
gasoline, petroleum distillates and ethanol.
Principal raw material(s) consumed: No raw materials are consumed. The facility is a bulk
terminal for gasoline, petroleum distillates and ethanol.
Briefly describe the manufacturing process(es):
The facility is a bulk distribution terminal for gasoline, petroleum distillates and ethanol. It does not
produce, manufacture or consume products or raw materials. Gasoline and distillates are received via
pipeline which are then stored in above ground tanks. Ethanol is received via tank truck. All products
are loaded out via tanker truck through the terminal's loading rack.
10. Amount of principal product produced or raw material consumed
Mist specific amounts consumed and/or units of production over the last three years)
Product Produced or Raw Material
Consumed
(AVERAGE)
Product Produced or Raw Material
Consumed
(PEAK)
per Day
500,000 gallons product distributed
607,500 gallons product distributed
per Month
15,000,000 gallons product distributed
18,220,000 gallons product distributed
per Year
183,000,000 gallons product distributed
194,200,000 gallons product distributed
11. Frequency of discharge: Continuous ❑ Intermittent
If intermittent:
Days per week discharge occurs: 7* Duration: 24*
* Discharge is intermittent and is determined by local rainfall amounts
Page 2 of 4 C-MI 10/08

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
12. Types of wastewater discharged to surface waters only
Discharge
Flow
GALLONS PER DAY)
Sanitary - monthly average
Not Applicable
Utility water, etc - monthly average
Not Applicable
Process water - monthly average
Not Applicable
Stormwater - monthly average
181,000 (dependent upon rainfall; last 3-year average)
Other - monthly average
Explain-
Not Applicable
Monthly Average
181,000
total discharge (all types)
13. Number of separate discharge points: 1 Outfall Identification number(s) 001
14. Name of receiving stream(s) (Provide a map showing the exact location of each outfall, including
latitude and longitude):
Unnamed tributary to Middle Creek within the Neuse River Basin. Latitude 35 42' 57"N, Longitude
78 48' 56"W Refer to Attachment I
15. Effluent Data [for new or proposed discharges]
Provide data for the parameters listed Temperature and pH shall be grab samples, for all other parameters 24-hour
composite sampling shall be used If more than one analysis is reported, report daily maxzmum and monthly
average If only one analysis is reported, report as daily maximum
NOTE: Permittees requesting renewal should complete the table ONLY for the parameters
currently monitored. Summarize the past 3 years of effluent data.
Parameter
Daily
Maximum
Monthly
Average
Units of
Measurement
Biochemical Oxygen Demand (BOD5)
Not required to be monitored under current permit. See
Attachment II for last 3 years of monitoring data.
Chemical Oxygen Demand (COD)
Total Organic Carbon
Total Suspended Solids
27.4
8.2
mg/l
Ammonia as N
Not required to be monitored under current permit See
Attachment II for last 3 years of monitoring data.
Temperature (Summer)
Temperature (Winter)
pH
Fecal Coliform (If sanitary waste is
present)
Total Residual Chlorine (if chlorine is
used)
Page 3 of 4 C-MI 10108

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial
Minor industrial, manufacturing and commercial facilities.
16. List all permits, construction approvals and/or applications (check all that apply and provide permit
numbers or check none if not applicable):
Type Permit Number Type Permit Number
Hazardous Waste (RCRA)
UIC (SDWA)
NPDES
PSD (CAA)
10571U.
WI0500057
NCO022217
None
Non -attainment program (CAA) None
NESHAPS (CAA) None
Ocean Dumping (MPRSA) None
Dredge or fill (Section 404 or CWA) None
Other - Air Quality Permit 0451ORIS
17. List any chemicals that may be discharged (Please list and explain source and potential
amounts )
None in addition to the compounds being sampled and analyzed.
18. Is this facility located on Indian country? (check one)
Yes ❑ No
19. Applicant Certification
I certify that I am familiar with the information contained in the application and that to the
best of my knowledge and belief such information is true, complete, and accurate.
Li 60r1rL_" M'0 _M 6.['1L__
Printed name of Person Signing Title
of Applicant
/ 0 /-Z-5/ 2.z� {7
Date
North Carolina General Statute 1143---21&6�b)(2) provides that Any person who knowingly makes any false
statement representation, or certification in any application, record, report, plan, or other document files or required
to be maintained under Article 21 or regulations of the Environmental Management Commission implementing that
Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method
required to be operated or maintained under Article 21 or regulations of the Environmental Management
Commission implementing that Article, shall be guilty of a misdemeanor punishable by a fine not to exceed $25,000,
or by imprisonment not to exceed six months, or by both (18 U S C Section 1001 provides a punishment by a fine
of not more than $25,000 or imprisonment not more than 5 years, or both, for a similar offense)
Page 4 of 4 C-MI 10/08

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Attachment I
Figures
Topographical Map
Oil Water Separator Process Flow Diagram

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
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i � '�_�
»1►� i�
�I
,fir
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�IIIIII�1��^,\Ijl r�l�R, •
q
l� �/�
d.
'r
IKNU� -
0 0.3 0.6 09 1 2 1.5 km M.
G
0 0.2 04 06 09 1mi
WLFL-TV (Raleigh), USGS Apex (NC) Quadrangle
Projection is UTM Zone 17 NAD83 Datum
AA=-6.715
G=1.276
Motiva Enterprises Raleigh Terminal Outfal) 001

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Motiva Enterprises LLC
Apex Terminal
NPDES Permit NCO022217
Loading Rack
Stormwater
Recovered
Product Sent Offsite
SPCC Tank 10,000 gal
Water Tank
Containment Pond
Outfall 001
Unnamed Tributary to Middle Creek
Tank Farm
Stormwater
(Diked Area)

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Attachment II
Detailed Sampling Results
August 2014 - August 2017

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Detailed Sampling Results
August 2014 - August 2017
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month
Day
Year
Parameter
Value
Units
8
11
2017
00070 - Turbidity
5.2
ntu
6
22
2017
00070 - Turbidity
6.4
ntu
5
30
2017
00070 - Turbidity
6
ntu
4
3
2017
00070 - Turbidity
4.5
ntu
1
10
2017
00070 - Turbidity
2.7
ntu
10
12
2016
00070 - Turbidity
4.8
ntu
9
28
2016
00070 - Turbidity
5.6
ntu
8
23
2016
00070 - Turbidity
5.4
ntu
7
6
2016
00070 - Turbidity
1.31
ntu
5
2
2016
00070 - Turbidity
4.4
ntu
2
9
2016
00070 - Turbidity
7.8
ntu
1
6
2016
00070 - Turbidity
4.2
ntu
11
4
2015
00070 - Turbidity
6.7
ntu
10
5
2015
00070 - Turbidity
8.4
ntu
8
12
2015
00070 - Turbidity
7.4
ntu
7
17
2015
00070 - Turbidity
17
ntu
6
29
2015
00070 - Turbidity
6.6
ntu
4
6
2015
00070 - Turbidity
11
ntu
3
13
2015
00070 - Turbidity
15
ntu
1
6
2015
00070 - Turbidity
9.9
ntu
12
4
2014
00070 - Turbidity
7.1
ntu
10
21
2014
00070 - Turbidity
7.8
ntu
9
15
2014
00070 - Turbidity
5
ntu
8
17
2014
00070 - Turbidity
8.2
ntu
8
11
2017
00556 - Oil & Grease
<5
m /I
6
22
2017
00556 - Oil & Grease
<5
m /1
5
30
2017
00556 - Oil & Grease
<5
m /1
4
3
2017
00556 - Oil & Grease
<5
m /I
1
10
2017
00556 - Oil & Grease
<5
m /I
10
12
2016
00556 - Oil & Grease
<5
m /I
9
28
2016
00556 - Oil & Grease
<5
m /1
8
23
2016
00556 - Oil & Grease
<5
m /l
7
6
2016
00556 - Oil & Grease
<5
m /I
5
2
2016
00556 - Oil & Grease
5.9
m /I
2
9
2016
00556 - Oil & Grease
<5
m /I
1
6
2016
00556 - Oil & Grease
<5
m /1
11
4
2015
00556 - Oil & Grease
<5
m /1
10
5
2015
00556 - Oil & Grease
<5
m /I
8
12
2015
00556 - Oil & Grease
<5
m /I
7
17
2015
00556 - Oil & Grease
<5
m /I
6
29
2015
00556 - Oil & Grease
<5
m /I
4
6
2015
00556 - Oil & Grease
5.3
m /I
3
13
2015
00556 - Oil & Grease
<5
m /I
1
6
2015
00556 - Oil & Grease
<5
m /I
12
4
2014
100556 - Oil & Grease
<5
m /I
10
21
2014
100556 - Oil & Grease
<5
Mg/1
Page 1 of 6

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Detailed Sampling Results
August 2014 - August 2017
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month
Day
Year
Parameter
Value
Units
9
15
2014
00556 - Oil & Grease
<5
m /I
8
17
2014
00556 - Oil & Grease
<5
m /I
8
11
2017
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
6
22
2017
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
5
30
2017
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
4
3
2017
22417 - Methyl Tert-But I Ether MTBE
<2
u /1
1
10
2017
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /1
10
12
2016
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
7
6
2016
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
5
2
2016
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
2
9
2016
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
1
6
2016
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
11
4
2015
22417 - Methyl Tert-But I Ether MTBE
<2
u /I
10
5
2015
22417 - Methyl Tert-But I Ether MTBE
<0.5
u /I
8
12
2015
22417 - Methyl Tert-But I Ether MTBE
<2
u /I
7
17
2015
22417 - Methyl Tert-But I Ether MTBE
<2
u /I
6
29
2015
22417 - Methyl Tert-But I Ether MTBE
<2
u /I
4
6
2015
22417 - Methyl Tert-But I Ether MTBE
<2
u /1
1
6
2015
22417 - Methyl Tert-But I Ether MTBE
<2
u /1
10
21
2014
22417 - Methyl Tert-But I Ether MTBE
<2
u /I
8
11
2017
34010 - Toluene
<0.25
u /I
6
22
2017
34010 - Toluene
<0.25
u /I
5
30
2017
34010 - Toluene
<0.25
u /I
4
3
2017
34010 - Toluene
<1
u /I
1
10
2017
34010 - Toluene
<0.25
u /I
10
12
2016
34010 - Toluene
<0.25
u /I
9
28
2016
34010 - Toluene
<0.25
u /1
8
23
2016
34010 - Toluene
<0.25
u /I
7
6
2016
34010 - Toluene
<0.25
u /I
5
2
2016
34010 - Toluene
<0.25
u /l
2
9
2016
34010 - Toluene
<0.25
u /I
1
6
2016
34010 - Toluene
<0.25
u /1
11
4
2015
34010 - Toluene
<1
u /I
10
5
2015
34010 - Toluene
<0.25
u /I
8
12
2015
34010 - Toluene
<1
/I
7
17
2015
34010 - Toluene
<1
/1
6
29
2015
34010 - Toluene
<1
/I
ru
4
6
2015
34010 - Toluene
<1
/I
3
13
2015
34010 - Toluene
<1
/I
1
6
2015
34010 - Toluene
<1
u /I
12
4
2014
34010 - Toluene
<1
u /I
10
21
2014
34010 - Toluene
<1
u /I
9
15
2014
34010 - Toluene
<1
u /I
8
17
2014
34010 - Toluene
<1
u /I
8
11
2017
34030 - Benzene
<0.125
u /I
6
22
2017
34030 - Benzene
<0.125
u /I
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DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Detailed Sampling Results
August 2014 - August 2017
Motiva Enterprises, LLC
Apex, NC
Permit No. NCO022217
Month
Day
Year
Parameter
Value
Units
5
30
2017
34030 - Benzene
<0.125
u /I
4
3
2017
34030 - Benzene
<1
u /I
1
10
2017
34030 - Benzene
<0.125
u /l
10
12
2016
34030 - Benzene
<0.125
u /I
9
28
2016
34030 - Benzene
<0.125
u /1
8
23
2016
34030 - Benzene
<0.125
u /I
7
6
2016
34030 - Benzene
<0.125
u /I
5
2
2016
34030 - Benzene
<0.125
u /1
2
9
2016
34030 - Benzene
<0.125
u /I
1
6
2016
34030 - Benzene
<0.125
u /I
11
4
2015
34030 - Benzene
<1
u /I
10
5
2015
34030 - Benzene
<0.125
u /I
8
12
2015
34030 - Benzene
<1
u /I
7
17
2015
34030 - Benzene
<1
u /I
6
29
2015
34030-Benzene
<1
u /I
4
6
2015
34030-Benzene
<1
u /I
3
13
2015
34030 - Benzene
<1
u /I
1
6
2015
34030 - Benzene
<1
u /I
12
4
2014
34030 - Benzene
<1
u /I
10
21
2014
34030 - Benzene
<1
u /I
9
15
2014
34030 - Benzene
<1
u /I
8
17
2014
34030 - Benzene
<1
u /I
8
11
2017
34371 - Eth (benzene
<0.25
u /I
6
22
2017
34371 - Eth (benzene
<0.25
u /1
5
30
2017
34371 - Eth (benzene
<0.25
u /l
4
3
2017
34371 - Eth (benzene
<1
u /I
1
10
2017
34371 - Eth (benzene
<0.25
u /I
10
12
2016
34371 - Eth (benzene
<0.25
u /I
9
28
2016
34371 - Eth (benzene
<0.25
u /I
8
23
2016
34371 - Eth (benzene
<0.25
u /1
7
6
2016
34371 - Eth (benzene
<0.25
u /I
5
2
2016
34371 - Eth (benzene
<0.25
u /I
2
9
2016
34371 - Eth (benzene
<0.25
u /I
1
6
2016
34371 - Eth (benzene
<0.25
u /I
11
4
2015
34371 - Eth (benzene
<1
u /I
10
5
2015
34371 - Eth (benzene
<0.25
u /I
8
12
2015
34371 - Eth (benzene
<1
u /I
7
17
2015
34371 - Eth (benzene
<1
u /1
6
29
2015
34371 - Eth (benzene
<1
u /I
4
6
2015
34371 - Eth (benzene
<1
u /1
3
13
2015
34371 - Eth (benzene
<1
u /I
1
6
2015
34371 - Eth (benzene
<1
u /I
12
4
2014
34371 - Eth (benzene
<1
u /I
10
21
2014
34371 - Eth (benzene
<1
u /I
9
15
2014
34371 - Eth (benzene
<1
u /I
8
17
2014
34371 - Eth (benzene
<1
u /I
Page 3 of 6

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Detailed Sampling Results
August 2014 - August 2017
Motiva Enterprises, LLC
Apex, NC
Permit No. NCO022217
Month
Day
Year
Parameter
Value
Units
8
11
2017
34696 - Naphthalene
<0.2
u /I
6
22
2017
34696 - Naphthalene
<0.2
u /I
5
30
2017
34696 - Naphthalene
<0.2
u /I
4 1
3
2017
34696 - Naphthalene
<1
u /I
1
10
2017
34696 - Naphthalene
<0.2
u /I
10
12
2016
34696 - Naphthalene
<0.2
u /I
9
28
2016
34696 - Naphthalene
<0.2
u /1
8
23
2016
34696 - Naphthalene
<0.2
u /I
7
6
2016
34696 - Naphthalene
<0.2
u /I
5
2
2016
34696 - Naphthalene
<0.2
u /I
2
9
2016
34696 - Naphthalene
<0.2
u /I
1
6
2016
34696 - Naphthalene
<0.2
u /I
11
4
2015
34696 - Naphthalene
<1
u /1
10
5
2015
34696 - Naphthalene
<0.2
u /I
8
12
2015
34696 - Naphthalene
<1
u /I
7
17
2015
34696 - Naphthalene
<1
u /1
6
29
2015
34696 - Naphthalene
<1
u /I
4
6
2015
34696 - Naphthalene
<1
u /I
3
13
2015
34696 - Naphthalene
<1
u /I
1
6
2015
34696 - Naphthalene
<1
u /I
12
4
2014
34696 - Naphthalene
<1
u /I
10
21
1 2014
34696 - Naphthalene
<1
u /I
9
15
2014
34696 - Naphthalene
<1
u /I
8
17
2014
34696 - Naphthalene
<1
u /I
8
11
2017
50050 - Flow, in conduit or thru treatment plant
0.168
m d
6
19
2017
50050 - Flow, in conduit or thru treatment plant
0.126
m d
6
22
2017
50050 - Flow, in conduit or thru treatment plant
0.126
m d
5
26
2017
50050 - Flow, in conduit or thru treatment plant
0.21
m d
5
30
2017
50050 - Flow, in conduit or thru treatment plant
0.021
mad
4
3
2017
50050 - Flow, in conduit or thru treatment plant
0.189
mcid
4
25
2017
50050 - Flow, in conduit or thru treatment plant
0.378
mad
4
26
2017
50050 - Flow, in conduit or thru treatment plant
0.147
m d
1
10
2017
50050 - Flow, in conduit or thru treatment plant
0.294
m d
1
31
2017
50050: Flow, in conduit or thru treatment plant
0.126
m d
10
8
2016
50050 - Flow, in conduit or thru treatment plant
0.42
m d
10
9
2016
50050 - Flow, in conduit or thru treatment plant
0.189
m d
10
12
2016
50050 - Flow, in conduit or thru treatment plant
0.042
m d
9
20
2016
50050 - Flow, in conduit or thru treatment plant
0.21
m d
9
21
2016
50050 - Flow, in conduit or thru treatment plant
0.021
m d
9
28
2016
50050 - Flow, in conduit or thru treatment plant
0.168
m d
8
10
2016
50050 - Flow, in conduit or thru treatment plant
0.126
m d
8
23
2016
50050 - Flow, in conduit or thru treatment plant
0.042
m d
7
6
2016
50050 - Flow, in conduit or thru treatment plant
0.252
mad
7
18
2016
50050 - Flow, in conduit or thru treatment plant
0.42
m d
5
2
2016
50050 - Flow, in conduit or thru treatment plant
0.294
m d
5
10
2016
50050 - Flow, in conduit or thru treatment plant
0.105
m d
Page 4 of 6

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Detailed Sampling Results
August 2014 - August 2017
Motiva Enterprises, LLC
Apex, NC
Permit No. NCO022217
Month
Day
Year
Parameter
Value
Units
5
11
2016
50050 - Flow, in conduit or thru treatment plant
0.0945
m d
5
31
2016
50050 - Flow, in conduit or thru treatment plant
0.21
m d
2
9
2016
50050 - Flow, in conduit or thru treatment plant
0.278
m d
2
29
2016
50050 - Flow, in conduit or thru treatment plant
0.084
m d
1
6
2016
50050 - Flow, in conduit or thru treatment plant
0.294
m d
11
2
2015
50050 - Flow, in conduit or thru treatment plant
0.126
m d
11
4
2015
50050 - Flow, in conduit or thru treatment plant
0.315
m d
11
20
2015
50050 - Flow, in conduit or thru treatment plant
0.336
m d
10
1
2015
50050 - Flow, in conduit or thru treatment plant
0.126
m d
10
5
2015
50050 - Flow, in conduit or thru treatment plant
0.105
m d
8
12
2015
50050 - Flow, in conduit or thru treatment plant
0.147
m d
8
24
2015
50050 - Flow, in conduit or thru treatment plant
0.042
mad
8
25
2015
50050 - Flow, in conduit or thru treatment plant
0.126
mad
7
15
2015
50050 - Flow, in conduit or thru treatment plant
0.126
m d
7
17
2015
50050 - Flow, in conduit or thru treatment plant
0.126
m d
6
26
2015
50050 - Flow, in conduit or thru treatment plant
0.42
m d
6
29
2015
50050 - Flow, in conduit or thru treatment plant
0.441
m d
4
6
2015
50050 - Flow, in conduit or thru treatment plant
0.126
m d
4
10
2015
50050 - Flow, in conduit or thru treatment plant
0.357
m d
3
9
2015
50050 - Flow, in conduit or thru treatment plant
0.147
m d
3
13
2015
50050 - Flow, in conduit or thru treatment plant
0.001
m d
3
17
2015
50050 - Flow, in conduit or thru treatment plant
0.063
m d
1
6
2015
50050 - Flow, in conduit or thru treatment plant
0.12
m d
1
20
2015
50050 - Flow, in conduit or thru treatment plant
0.21
m d
1
21
2015
50050 - Flow, in conduit or thru treatment plant
0.168
m d
12
4
2014
50050 - Flow, in conduit or thru treatment plant
0.126
m d
12
26
2014
50050 - Flow, in conduit or thru treatment plant
0.21
m d
10
21
2014
50050 - Flow, in conduit or thru treatment plant
0.105
m d
9
11
2014
50050 - Flow, in conduit or thru treatment plant
0.231
m d
9
15
2014
50050 - Flow, in conduit or thru treatment plant
0.105
m d
9
29
2014
50050 - Flow, in conduit or thru treatment plant
0.084
m d
8
17
2014
50050 - Flow, in conduit or thru treatment plant
0.042
m d
8
18
2014
50050: Flow, in conduit or thru treatment plant
0.105
m d
8
26
2014
50050 - Flow, in conduit or thru treatment plant
0.105jmg8
11
2017
81551 - X lene mix of m+o+
<0.56
22
2017
81551 - X lene mix of m+o+
<0.55
30
2017
81551 - X lene mix of m+o+
<0.54
3
2017
81551 - X lene mix of m+o+
<1
1
10
2017
81551 - X lene mix of m+o+
<0.5
u /I
10
12
2016
81551 - X lene mix of m+o+
<0.5
u /I
9
28
2016
81551 - X lene mix of m+o+
<0.5
u /I
8
23
2016
81551 - X lene mix of m+o+
<0.5
u /I
7
6
2016
81551 - X lene mix of m+o+
<0.5
u /I
5
2
2016
81551 - X lene mix of m+o+
<0.5
u /I
2
9
2016
81551 - X lene mix of m+o+
<0.5
u /I
1
6
2016
181551 - X lene mix of m+o+
<0.5
u /I
Page 5 of 6

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Detailed Sampling Results
August 2014 - August 2017
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month
Day
Year
Parameter
Value
Units
11
4
2015
81551 - X lene mix of m+o+
<1
u /I
10
5
2015
81551 - X lene mix of m+o+
<0.5
u /I
8
12
2015
81551 - X lene mix of m+o+
<1
u /I
7
17 1
2015
81551 - X lene mix of m+o+
<1.1
u /l
6
29
2015
81551 - X lene mix of m+o+
<1
u /1
4
6
2015
81551 - X lene mix of m+o+
<1
u /l
3
13
2015
81551 - X lene mix of m+o+
<1
u /l
1
6
2015
81551 - X lene mix of m+o+
<1
u /l
12
4
2014
81551 - X lene mix of m+o+
<1
u /I
10
21
2014
81551 - X lene mix of m+o+
<1
u /I
9
15
2014
81551 - X lene mix of m+o+
<1
u /I
8
17
2014
81551 - X lene mix of m+o+
<1
u /I
8
11
2017
CO530 - Solids, Total Suspended - Concentration
27.4
m /I
6
22
2017
CO530 - Solids, Total Suspended - Concentration
5.4
m /l
5
30
2017
CO530 - Solids, Total Suspended - Concentration
8.2
m /l
4
3
2017
CO530 - Solids, Total Suspended - Concentration
4.8
m /l
1
10
2017
CO530 - Solids, Total Suspended - Concentration
2
m /I
10
12
2016
CO530 - Solids, Total Suspended - Concentration
3.8
m /I
9
28
2016
CO530 - Solids, Total Suspended - Concentration
14.8
m /l
8
23
2016
CO530 - Solids, Total Suspended - Concentration
8.6
m /l
7
6
2016
CO530 - Solids, Total Suspended - Concentration
5.78
m /l
5
2
2016
CO530 - Solids, Total Suspended - Concentration
6.2
m /l
2
9
2016
CO530 - Solids, Total Suspended - Concentration
5.67
m /I
1
6
2016
CO530 - Solids, Total Suspended - Concentration
3
m /I
11
4
2015
CO530 - Solids, Total Suspended - Concentration
4.75
m /l
10
5
2015
CO530 - Solids, Total Suspended - Concentration
4
m /l
8
12
2015
CO530 - Solids, Total Suspended - Concentration
9.6
m /I
7
17
2015
CO530 - Solids, Total Suspended - Concentration
11.7
m /I
6
29
2015
CO530 - Solids, Total Suspended - Concentration
7.3
m /I
4
6
2015
CO530 - Solids, Total Suspended - Concentration
6
m /l
3
13
2015
CO530 - Solids, Total Suspended - Concentration
10
m /I
1
6
2015
CO530 - Solids, Total Suspended - Concentration
5.6
m /I
12
4
2014
CO530 - Solids, Total Suspended - Concentration
4
m /I
10
21
2014
CO530 - Solids, Total Suspended - Concentration
24
m /I
9
15
2014
CO530 - Solids, Total Suspended - Concentration
8
m /I
8
17
2014
CO530 - Solids, Total Suspended - Concentration
7.3
m /l
1
10
2017
TAE6C - LC50 Static 24hr Acute Pime hales
>100%
percent
2
9
2016
TAE6C - LC50 Static 24hr Acute Pime hales
>100%
percent
4
6
2015
1 TAE6C - LC50 Static 24hr Acute Pime hales
>100%
percent
Data is shown for all months with recorded flows sufficient for smapling.
Page 6 of 6

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
ROY COOPER
Governor
MICHAEL S. REGAN
Serretnry
LINDA CULPEPPER
Environmental Qua:, t
December 10, 2019
Motiva Enterprises, LLC
Attn: John Herman
223E Ten -Ten Road
Apex, NC 27539
Subject: Compliance Evaluation Inspection
Motiva Raleigh (Apex) Terminal
NPDES Permit NC0022217
Wake County
Dear Mr. Herman:
On December 10, 2019, Stephanie Goss of the Raleigh Regional Office (RRO) conducted a
compliance evaluation inspection at the Motiva Raleigh Terminal site in Apex. The assistance of
Kristine Pelt and yourself during the inspection was greatly appreciated. The following
observations were made:
• The permit expired on April 30, 2018; however, the Division of Water Resources Water
Quality Permitting Section acknowledged that on October 23, 2017 receipt of the permit
renewal application was received.
• Motiva Enterprises, LLC is permitted to discharge stormwater wastewater from the Raleigh
Terminal located in Apex into an unnamed tributary of Middle Creek, a Class C-Nutrient
Sensitive Waters in the Neuse River Basin.
• Stormwater'wastewater is collected into a retention pond and discharged through an effluent
pipe at the outfall as needed. The outfall was closed and locked; therefore, no discharge was
occurring during the time of the inspection.
• The facility looked well maintained, clean and the benn surrounding the facility was in good
condition.
• A review of discharge monitoring report (DMR) data for the period January 2017 through
October 2019 showed all required monitoring was performed.
• A cursory review of laboratory and DMR data for June 2018 and April 2019 showed
consistent reporting of results.
�\ 1, rrifr (,.e,rIitiA IJ, I,jr r¢rrII of Eli-- u or i tv rn I a I (?u.iGiy - I)rvi•,i In ,if Wain; Rt:vIII; tc%
_ ��� R.r�ric}IoRrtiinu,�lU•`firi S,ii7OIS,u;rl;iPiYc i;tE,•:yh.iinFrft(-,ut�lin.i�li+U')

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
If you have questions concerning this report, please contact Stephanie Goss at 919-791-4256 or
via e-mail at stephanie.gossirEncdenr.gov.
Sincerely,
ZL-) � -_ ��� � �
Scott Vinson, Regional Supervisor
Water Quality Regional Operations Section
Raleigh Regional Office
Division of Water Resources, NCDEQ
cc; RRO, SWP
Charles Weaver
?IP-1up

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
United ~tares Cnwronmental Prate to Agency
Form Approved
EPA Washington D C 204_C
OMB No 204G-0057
Water Compliance Inspection Report
Approval expires8-31 98
Section A- National Data System Coding (i e , PCS)
Transaction Code NPDES yr mo:day nspe_tion Type
inspector Fat Type
1 U 2 15 1 3 I NCO022217 I11 12 19: 12 10 17 18 I� t
191 s 1 201
1
�I
211 L I f I I I l I I I I I I_I_._I I I I I I I I I I I I I I I I I I I
I I I I f6
.I
Inspection Work Days Facility Self -Monitoring Evaluation Rating B1 OA
,I -I
Reserved- .....----- .
67 701 LJ I 71 Lj 72 1 �, 1 731 I 174
LJ I I I
75III JLJ80
Section B Facility Data
Name and Location of Facility Inspected ;For Industrial Users discharging to POTW also injude E--try Time Date
Permit Effechve Date
POTW name and NPDES oermil Number)
17 OOAM 19.12110
1112101
Apex Terminal
2232 Ten Ten Rd Exit Time Date
permit Expiration Date
Apex NC 27502 'sA 45AM 1911210
18/04/30
Name(s) of Onsite Representative(sifT'Iles(sj:Phone and Fax Numbers)
Other Facility Data
X
Not RequiredlORC1919-807-6353;
Name Address of Responsible Official/Ti0elPhone and Fax N: mber
Contacted
Nicola A Ellis,2232 Ten Ten Rd Apex NC 275021.`919-387-5764:
No
Section C: Areas Evaluated During Inspection (Check only those areas evaluated)
Permit N Flow Measurement Operations 8 Maintenance 0 Records/Reports
Self -Monitoring Program N Facility Site Review Effluent/Receiving Waters N Laboratory
Section D: Summary of FindinglCommenls (Attach additional sheets of narrative and checklists as necessary)
(See attachment summary)
Name(s) and Signature(s) of Inspector(s) AgencylOfficelPhone and Fax Numbers
Date
Stephanie Goss DWWRRO WO1919-791-42001
� ..&3-
talt',
Signature of Management O A Reviewer Agency/OfficelPhone and Fax Numbers
Date
LIAT �11111
IL/1,1ry
EPA Form 3560-3 (Rev 9-94) Previous editions are obsolete
Page#

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
NPIDES yrlmolday Inspection Type
31 NCO022217 {11 12 191 2110 17 18 ICI
Section D: Summary of Finding/Comments (Attach additional sheets of narrative and checklists as necessary)
PwP#

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit: NCO022217 Owner -Facility: Apex Terminal
Inspectlon Date: 12110f2o19 Inspection Type: Compliance Evaluation
Operations_& Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ❑ ❑ ❑
Does the facility analyze process control parameters for ex MLSS MCRT Settleable ❑ ❑
Solids, pH, DO, Sludge ,fudge, and other that are applicable?
Comment:
Permit
Yes No NA NE
(If the present permit expires in 6 months or less) Has the permittee submitted a new
M
❑
❑
application?
Is the facility as described in the permit?
❑
❑
❑
# Are there any special conditions for the permit?
❑
❑
0
❑
Is access to the plant site restricted to the general public?
❑
❑
❑
Is the inspector granted access to all areas for inspection?
❑
❑
❑
Comment:
Lagoons
Yes No NA NE
Type of lagoons?
# Number of lagoons in operation at time of visit?
t
Are lagoons operated in?
# Is a re -circulation line present?
❑
❑
0
❑
Is lagoon free of excessive floating materials?
0
❑
❑
❑
# Are baffles between ponds or effluent baffles adjustable?
❑
❑
M
❑
Are dike slopes dear of woody vegetation?
❑
❑
❑
Are weeds controlled around the edge of the lagoon?
❑
❑
❑
Are dikes free of seepage?
❑
❑
❑
Are dikes free of erosion?
❑
❑
❑
Are dikes free of burrowing animals?
❑
❑
❑
# Has the sludge blanket in the lagoon (s) been measured periodically in multiple
❑
❑
M
❑
locations?
# If excessive algae is present, has barley straw been used to help control the growth?
❑
❑
M
❑
Is the lagoon surface free of weeds?
❑
❑
❑
Is the lagoon free of short circuiting?
❑
❑
❑
Comment:

DocuSlgn Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
.y .. --y
Year
Parameter
UOM
Value
Modifier
.....
a
NCO022217
Motiva Enterprises LLC - P
1
6
2016
00070 - Turbidity
ntu
4.2
NCO022217
Motiva Enterprises LLC - P
2
9
2016
00070 - Turbidity
ntu
7.8
NCO022217
Motiva Enterprises LLC - P
5
2
2016
00070 - Turbidity
ntu
4.4
NCO022217
Motiva Enterprises LLC - P
7
6
2016
00070 - Turbidity
ntu
1.31
NCO022217
Motiva Enterprises LLC - P
8
23
2016
00070 - Turbidity
ntu
5.4
NCO022217
Motiva Enterprises LLC - P
9
28
2016
00070 - Turbidity
ntu
5.6
NCO022217
Motiva Enterprises LLC - P
10
12
2016
00070 - Turbidity
ntu
4.8
NCO022217
Motiva Enterprises LLC - P
1
10
2017
00070 - Turbidity
ntu
2.7
NCO022217
Motiva Enterprises LLC - P
4
3
2017
00070 - Turbidity
ntu
4.5
NCO022217
Motiva Enterprises LLC - P
5
30
2017
00070 - Turbidity
ntu
6
NCO022217
Motiva Enterprises LLC - P
6
22
2017
00070 - Turbidity
ntu
6.4
NCO022217
Motiva Enterprises LLC - P
8
11
2017
00070 - Turbidity
ntu
5.2
NCO022217
Motiva Enterprises LLC - P
9
8
2017
00070 - Turbidity
ntu
3.2
NCO022217
Motiva Enterprises LLC - P
12
14
2017
00070 - Turbidity
ntu
3
NCO022217
Motiva Enterprises LLC - P
2
5
2018
00070 - Turbidity
ntu
7.2
NCO022217
Motiva Enterprises LLC - P
3
26
2018
00070 - Turbidity
ntu
6.5
NCO022217
Motiva Enterprises LLC - P
6
21
2018
00070 - Turbidity
ntu
3.7
NCO022217
Motiva Enterprises LLC - P
7
30
2018
00070 - Turbidity
ntu
2.8
NCO022217
Motiva Enterprises LLC - P
9
11
2018
00070 - Turbidity
ntu
2.3
NCO022217
Motiva Enterprises LLC - P
10
25
2018
00070 - Turbidity
ntu
4.8
NCO022217
Motiva Enterprises LLC - P
11
19
2018
00070 - Turbidity
ntu
5.9
NCO022217
Motiva Enterprises LLC - P
12
18
2018
00070 - Turbidity
ntu
6.9
NCO022217
Motiva Enterprises LLC - P
2
12
2019
00070 - Turbidity
ntu
5.3
NCO022217
Motiva Enterprises LLC - P
4
4
2019
00070 - Turbidity
ntu
4.1
NCO022217
Motiva Enterprises LLC - P
6
13
2019
00070 - Turbidity
ntu
5.7
NCO022217
Motiva Enterprises LLC - P
8
8
2019
00070 - Turbidity
ntu
5.6
NCO022217
Motiva Enterprises LLC - P
11
20
2019
00070 - Turbidity
ntu
2.3
NCO022217
Motiva Enterprises LLC - P
12
19
2019
00070 - Turbidity
ntu
16
NCO022217
Motiva Enterprises LLC - P
1
10
2020
00070 - Turbidity
ntu
11
NCO022217
Motiva Enterprises LLC - P
2
13
2020
00070 - Turbidity
ntu
7
NCO022217
Motiva Enterprises LLC - P
5
6
2020
00070 - Turbidity
ntu
5.8
NCO022217
Motiva Enterprises LLC - P
1
6
2016
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
9
2016
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
2
2016
00556 - Oil & Grease
mg/I
5.9
NCO022217
Motiva Enterprises LLC - P
7
6
2016
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
23
2016
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
28
2016
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
12
2016
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2017
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
3
2017
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
30
2017
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
22
2017
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
11
2017
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
8
2017
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
14
2017
00556 - Oil & Grease
mg/I
5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
5
2018
00556 - Oil & Grease
mg/I
5
LESSTHAN

DocuSlg` Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
2018
00556 -Oil &Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
21
2018
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
7
30
2018
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
9
11
2018
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
10
25
2018
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
11
19
2018
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
18
2018
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
12
2019
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
4
4
2019
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
13
2019
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
8
8
2019
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
11
20
2019
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
19
2019
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
1
10
2020
00556 - Oil & Grease
mg/I
5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
13
2020
00556 - Oil & Grease
mg/I
5.6
NC0022217
Motiva Enterprises LLC - P
5
6
2020
00556 - Oil & Grease
mg/I
5.7
NC0022217
Motiva Enterprises LLC - P
1
6
2016
22417 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
9
2016
22418 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
5
2
2016
22419 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
7
6
2016
22420 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
10
12
2016
22421 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
1
10
2017
22422 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
4
3
2017
22423 - MTBE
ug/I
2
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
5
30
2017
22424 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
22
2017
22425 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
8
11
2017
22426 - MTBE
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
9
8
2017
22427 - MTBE
ug/I
2
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
14
2017
22428 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
5
2018
22429 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
21
2018
22430 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
7
30
2018
22431 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
10
25
2018
22432 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
11
19
2018
22433 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
18
2018
22434 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
12
2019
22435 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
4
4
2019
22436 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
13
2019
22437 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
11
20
2019
22438 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
19
2019
22439 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
1
10
2020
22440 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
13
2020
22441 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
5
6
2020
22442 - MTBE
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
1
6
2016
34010 - Toluene
ug/I
0.25
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
9
2016
34010 - Toluene
ug/I
0.25
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
5
2
2016
34010 - Toluene
ug/I
0.25
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
7
6
2016
34010 - Toluene
ug/I
0.25
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
8
23
2016
34010 - Toluene
ug/I
0.25
LESSTHAN

DocuSigEnvelope n EnvelID: F00435A5- YFA2-4D47-AFE2-734BB9D7EEAC `
2016
34010 -Toluene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
12
2016
34010 - Toluene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2017
34010 - Toluene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
3
2017
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
30
2017
34010 - Toluene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
22
2017
34010 - Toluene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
11
2017
34010 - Toluene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
8
2017
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
14
2017
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
5
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
3
26
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
21
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
30
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
30
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
25
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
19
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
18
2018
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
12
2019
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
4
2019
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
13
2019
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
8
2019
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
20
2019
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
19
2019
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2020
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
13
2020
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
6
2020
34010 - Toluene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
6
2016
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
9
2016
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
2
2016
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
6
2016
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
23
2016
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
28
2016
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
12
2016
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2017
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
3
2017
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
30
2017
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
22
2017
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
11
2017
34030 - Benzene
ug/I
0.125
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
8
2017
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
14
2017
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
5
2018
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
3
26
2018
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
21
2018
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
30
2018
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
30
2018
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
25
2018
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
19
2018
34030 - Benzene
ug/I
1
LESSTHAN

DocuSigEnvelope n EnvelID: F00435A5- YFA2-4D47-AFE2-734BB9D7EEAC `
2018
34030 -Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
12
2019
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
4
2019
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
13
2019
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
8
2019
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
20
2019
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
19
2019
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2020
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
13
2020
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
6
2020
34030 - Benzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
6
2016
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
9
2016
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
2
2016
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
6
2016
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
23
2016
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
28
2016
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
12
2016
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2017
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
3
2017
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
30
2017
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
22
2017
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
11
2017
34371 - Ethylbenzene
ug/I
0.25
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
8
2017
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
14
2017
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
5
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
3
26
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
21
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
30
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
30
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
25
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
19
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
18
2018
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
12
2019
34371 - Ethylbenzene
ug/I
0.4
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
4
2019
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
13
2019
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
8
2019
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
20
2019
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
19
2019
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2020
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
13
2020
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
6
2020
34371 - Ethylbenzene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
6
2016
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
9
2016
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
2
2016
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
6
2016
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
23
2016
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
28
2016
34696 - Naphthalene
ug/I
0.2
LESSTHAN

DocuSlg` Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
2016
34696 -Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2017
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
3
2017
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
30
2017
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
22
2017
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
11
2017
34696 - Naphthalene
ug/I
0.2
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
8
2017
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
14
2017
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
5
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
3
26
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
21
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
30
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
9
30
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
10
25
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
19
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
18
2018
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
12
2019
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
4
4
2019
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
6
13
2019
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
8
8
2019
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
11
20
2019
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
12
19
2019
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
10
2020
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
13
2020
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
6
2020
34696 - Naphthalene
ug/I
1
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
1
6
2016
50050 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
2
9
2016
50051 - Flow
mgd
0.278
NCO022217
Motiva Enterprises LLC - P
2
29
2016
50052 - Flow
mgd
0.084
NCO022217
Motiva Enterprises LLC - P
5
2
2016
50053 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
5
10
2016
50054 - Flow
mgd
0.105
NCO022217
Motiva Enterprises LLC - P
5
11
2016
50055 - Flow
mgd
0.0945
NCO022217
Motiva Enterprises LLC - P
5
31
2016
50056 - Flow
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
7
6
2016
50057 - Flow
mgd
0.252
NCO022217
Motiva Enterprises LLC - P
7
18
2016
50058 - Flow
mgd
0.42
NCO022217
Motiva Enterprises LLC - P
8
10
2016
50059 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
8
23
2016
50060 - Flow
mgd
0.042
NCO022217
Motiva Enterprises LLC - P
9
20
2016
50061 - Flow
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
9
21
2016
50062 - Flow
mgd
0.021
NCO022217
Motiva Enterprises LLC - P
9
28
2016
50063 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
10
8
2016
50064 - Flow
mgd
0.42
NCO022217
Motiva Enterprises LLC - P
10
9
2016
50065 - Flow
mgd
0.189
NCO022217
Motiva Enterprises LLC - P
10
12
2016
50066 - Flow
mgd
0.042
NCO022217
Motiva Enterprises LLC - P
1
10
2017
50067 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
1
31
2017
50068 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
4
3
2017
50069 - Flow
mgd
0.189
NCO022217
Motiva Enterprises LLC - P
4
25
2017
50070 - Flow
mgd
0.378
NCO022217
Motiva Enterprises LLC - P
4
26
2017
50071 - Flow
mgd
0.147

DocuSigEnvelope n EnvelID: F00435A5- YFA2-4D47-AFE2-734BB9D7EEAC `
2017
50072 - FIOW
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
5
30
2017
50073 - Flow
mgd
0.021
NCO022217
Motiva Enterprises LLC - P
6
19
2017
50074 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
6
22
2017
50075 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
8
11
2017
50076 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
9
8
2017
50077 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
12
11
2017
50078 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
12
14
2017
50079 - Flow
mgd
0.252
NCO022217
Motiva Enterprises LLC - P
2
5
2018
50080 - Flow
mgd
0.252
NCO022217
Motiva Enterprises LLC - P
3
20
2018
50081 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
3
26
2018
50082 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
6
21
2018
50083 - Flow
mgd
0.042
NCO022217
Motiva Enterprises LLC - P
7
16
2018
50084 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
7
24
2018
50085 - Flow
mgd
0.252
NCO022217
Motiva Enterprises LLC - P
7
30
2018
50086 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
9
11
2018
50087 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
9
13
2018
50088 - Flow
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
9
19
2018
50089 - Flow
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
9
30
2018
50090 - Flow
mgd
0.042
NCO022217
Motiva Enterprises LLC - P
10
9
2018
50091 - Flow
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
10
25
2018
50092 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
11
19
2018
50093 - Flow
mgd
0.336
NCO022217
Motiva Enterprises LLC - P
12
18
2018
50094 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
12
31
2018
50095 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
2
12
2019
50096 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
2
18
2019
50097 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
2
21
2019
50098 - Flow
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
2
22
2019
50099 - Flow
mgd
0.126
NCO022217
Motiva Enterprises LLC - P
2
24
2019
50100 - Flow
mgd
0.189
NCO022217
Motiva Enterprises LLC - P
4
4
2019
50101 - Flow
mgd
0.084
NCO022217
Motiva Enterprises LLC - P
4
9
2019
50102 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
4
18
2019
50103 - Flow
mgd
0.336
NCO022217
Motiva Enterprises LLC - P
6
8
2019
50104 - Flow
mgd
0.063
NCO022217
Motiva Enterprises LLC - P
6
13
2019
50105 - Flow
mgd
0.336
NCO022217
Motiva Enterprises LLC - P
8
8
2019
50106 - Flow
mgd
0.231
NCO022217
Motiva Enterprises LLC - P
8
31
2019
50107 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
11
20
2019
50108 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
12
19
2019
50109 - Flow
mgd
0.231
NCO022217
Motiva Enterprises LLC - P
1
10
2020
50110 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
1
29
2020
50111 - Flow
mgd
0.168
NCO022217
Motiva Enterprises LLC - P
2
13
2020
50112 - Flow
mgd
0.294
NCO022217
Motiva Enterprises LLC - P
5
6
2020
50113 - Flow
mgd
0.21
NCO022217
Motiva Enterprises LLC - P
5
27
2020
50114 - Flow
mgd
0.336
NCO022217
Motiva Enterprises LLC - P
1
6
2016
81551 - Xylenes
ug/I
0.5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
2
9
2016
81551 - Xylenes
ug/I
0.5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
5
2
2016
81551 - Xylenes
ug/I
0.5
LESSTHAN
NCO022217
Motiva Enterprises LLC - P
7
6
2016
81551 - Xylenes
ug/I
0.5
LESSTHAN

DocuSlgEnvelope n EnvelID: F00435A5- YFA2-4D47-AFE2-734BB9D7EEAC `
2016
81551 -Xylenes
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
9
28
2016
81551 - Xylenes
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
10
12
2016
81551 - Xylenes
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
1
10
2017
81551 - Xylenes
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
4
3
2017
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
5
30
2017
81551 - Xylenes
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
22
2017
81551 - Xylenes
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
8
11
2017
81551 - Xylenes
ug/I
0.5
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
9
8
2017
81551 - Xylenes
ug/I
2
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
14
2017
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
5
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
3
26
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
21
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
7
30
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
9
30
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
10
25
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
11
19
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
18
2018
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
12
2019
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
4
4
2019
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
6
13
2019
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
8
8
2019
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
11
20
2019
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
12
19
2019
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
1
10
2020
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
2
13
2020
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
5
6
2020
81551 - Xylenes
ug/I
1
LESSTHAN
NC0022217
Motiva Enterprises LLC - P
1
6
2016
CO530 - TSS
mg/I
3
NC0022217
Motiva Enterprises LLC - P
2
9
2016
CO530 - TSS
mg/I
5.67
NC0022217
Motiva Enterprises LLC - P
5
2
2016
CO530 - TSS
mg/I
6.2
NC0022217
Motiva Enterprises LLC - P
7
6
2016
CO530 - TSS
mg/I
5.78
NC0022217
Motiva Enterprises LLC - P
8
23
2016
CO530 - TSS
mg/I
8.6
NC0022217
Motiva Enterprises LLC - P
9
28
2016
CO530 - TSS
mg/I
14.8
NC0022217
Motiva Enterprises LLC - P
10
12
2016
CO530 - TSS
mg/I
3.8
NC0022217
Motiva Enterprises LLC - P
1
10
2017
CO530 - TSS
mg/I
2
NC0022217
Motiva Enterprises LLC - P
4
3
2017
CO530 - TSS
mg/I
4.8
NC0022217
Motiva Enterprises LLC - P
5
30
2017
CO530 - TSS
mg/I
8.2
NC0022217
Motiva Enterprises LLC - P
6
22
2017
CO530 - TSS
mg/I
5.4
NC0022217
Motiva Enterprises LLC - P
8
11
2017
CO530 - TSS
mg/I
27.4
NC0022217
Motiva Enterprises LLC - P
9
8
2017
CO530 - TSS
mg/I
6.7
NC0022217
Motiva Enterprises LLC - P
12
14
2017
CO530 - TSS
mg/I
1.08
NC0022217
Motiva Enterprises LLC - P
2
5
2018
CO530 - TSS
mg/I
2.17
NC0022217
Motiva Enterprises LLC - P
3
26
2018
CO530 - TSS
mg/I
3.17
NC0022217
Motiva Enterprises LLC - P
6
21
2018
CO530 - TSS
mg/I
33.4
NC0022217
Motiva Enterprises LLC - P
7
30
2018
CO530 - TSS
mg/I
3
NC0022217
Motiva Enterprises LLC - P
9
11
2018
CO530 - TSS
mg/I
3
NC0022217
Motiva Enterprises LLC - P
10
25
2018
CO530 - TSS
mg/I
4.17

DocuSlgEnvelope n EnvelID: F00435A5- YFA2-4D47-AFE2-734BB9D7EEAC `
2018
CO530 -TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
12
18
2018
CO530 - TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
2
12
2019
CO530 - TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
4
4
2019
CO530 - TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
6
13
2019
CO530 - TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
8
8
2019
CO530 - TSS
mg/I
5.33
NC0022217
Motiva Enterprises LLC - P
11
20
2019
CO530 - TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
12
19
2019
CO530 - TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
1
10
2020
CO530 - TSS
mg/I
4.17
NC0022217
Motiva Enterprises LLC - P
2
13
2020
CO530 - TSS
mg/I
2.56
NC0022217
Motiva Enterprises LLC - P
5
6
2020
CO530 - TSS
mg/I
2.95
NC0022217
Motiva Enterprises LLC - P
2
9
2016
TAE6C - LC50 Static
percent
100
NC0022217
Motiva Enterprises LLC - P
1
10
2017
TAE6C - LC50 Static
percent
100
NC0022217
Motiva Enterprises LLC - P
4
4
2019
TAE6C - LC50 Static
percent
100
NC0022217
Motiva Enterprises LLC - P
5
6
2020
TAE6C - LC50 Static
percent
100
LESSTHAN
LESSTHAN
LESSTHAN
LESSTHAN
LESSTHAN
LESSTHAN
LESSTHAN
LESSTHAN
GRATRTHN
GRATRTHN
GRATRTHN
GRATRTHN

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
corrected - assumed NOT less than

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
4
NC®ENR
North Carolina Department of Environment and Natura
Division of Water Resources
Pat McCrory
Governor
Kenneth Watson, Complex Manager
Motiva Enterprises, LLC
2232 Ten Ten Road
Apex, North Carolina 27539-8115
Dear Mr. Watson:
Water Quality Programs
Thomas A. Reeder
Director
November 8, 2013
Resources
John E. Skvarla, III
Secretary
Subject: Issuance of NPDES Permit NCO022217
Motiva Raleigh Terminal
2232 Ten Ten Road, Apex
Wake County
The Division of Water Resources (the Division or DWR) hereby issues the attached NPDES permit for the
subject facility. This permit is issued pursuant to the requirements of North Carolina General Statute 143-
215.1 and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection
Agency dated October 15, 2007, or as subsequently amended.
IMplementing Electronic Discharge Monitoring Reports (eDMRs). Please be advised that the Division
will implement an electronic Discharge Monitoring Report (eDMR) program, in accord with pending
requirements by the Enviromnental Protection Agency (EPA). We have included the details required to
implement the eDMR program in this issuance final [see permit Special Condition A. (3.)].
Proposed federal regulations require electronic submittal of all DMRs and specify that, if North Carolina
does not establish a program to receive such submittals, Permittees must then submit eDMRs directly to
EPA. For information on eDMRs, registering for eDMR submittal, and obtaining an eDMR user
account, please visit DWR's webpage:
http://poital.nedei-ir.org/AATeb/wg/admin/bog/l*p-Lt/edmr.
For information on EPA's proposed NPDES Electronic Reporting Rule, please visit EPA's website:
http://www2.epa.gov/compliance/proposed-npdes-electronic-reporting rule
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: [phone] FAX: [phone]
Internet: www.ncwaterquality.org
An Equal Opportunity 1 Affirmative Action Employer

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Mr. Kenneth Watson
NC0022217 Renewal 2013
p. 2
Summary of Changes to the Previous Permit.
1. For renewal, DWR has updated your facility -description (Supplement to Cover Sheet);
updated the Vicinity Map, revised the WET -testing page [Section A. (2.)], and added
parameter codes to the effluent table [Section A. (1.)] for your convenience.
2. EPA Test Methods 624 and 625 — Per your request, DWR has discontinued monitoring by
Methods 624 and 625 based on parameters not detected above test- method practical
quantitation levels (PQLs) over the past permit cycle.
3. Total Nitrogen (TN) and Total Phosphorus (TP) — The Division has finalized its 2013
permitting strategy for the Neuse River Basin, a basin currently classified nutrient sensitii>e
}voters (NSW). Considering this facility's existing analytical database, its episodic minimal
flow (< 0.050 MGD, not limited), and SIC Code [5171], Motiva is exempt under State
Regulation NCAC 02B .0508, and is no longer required to monitor effluent nitrogen and
phosphorus. DWR has therefore discontinued monitoring; removed previous permit Special
Condition and related footnotes.
4. Oil and Grease (O&G). Due to the requirement to sample "during discharge" at the
designated outfall, DWR has removed the table footnote [Section A. (1.)] requiring a
"quiescent zone" for sampling O&G as this sampling practice has been questioned as "non-
operational."
5. In accord with Bulk Storage Strategy 2005, relaxed MTBE monitoring from Monthly to
Quarterly based on "not detected."
6. Finally, we have added monitoring for Naphthalene [code 34696] to detect the presence of diesel
fuel in the effluent.
If any parts, measurement frequencies, or sampling requirements contained in this permit are
unacceptable, you have the right to an adjudicatory hearing, upon written request submitted within thirty
(30) days after receiving this letter. Your request must take the form of a written petition conforming to
Chapter 150B of North Carolina General Statutes, and you must file it with the Office of Administrative
Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such a demand is
made, this permit shall remain final and binding.
This permit is not transferable except after notifying the Division of Water Resources. The Division may
require permit modification, or revocation and re -issuance. Please note that this permit does not affect
your legal obligation to obtain other permits required by the Division of Water Resources, the Division
of Land Resources, the Coastal Area Management Act, or other federal or local governments.

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Mr. Kenneth Watson
NCO022217 Renewal 2013
p. 3
If you have questions, or if we can be of further service, please contact Joe R. Corporon L.G. ROC at
[ioe.corporon e ncdenr.gov] or call his direct line [phone].
Respectfully,
, � q. - i"- -.fl
f— Thomas A. Reeder
Enclosure: NPDES Permit NCO022217 (Issuance Final)
hc: Central files
RRO/SWPS Supervisor, Danny Smith
NPDES Program Files
ec: ATU, Susan Meadows
DWR/RRO, Mitch Hayes
Motiva Enterprises, LLC, Kenneth Watson (Complex Manager) [[e-mail]]

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit NCO022217
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER RESOURCES
PERMIT
TO DISCHARGE STORMWATER/WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
(NPRES)
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Motiva Enterprises, LLC
is hereby authorized to discharge stormwater/wastewater from an outfall located at the
Raleigh Terminal
2232 Ten Ten Road, Apex
Wake County
to receiving waters designated as an unnamed tributary of Middle Creels within the Neuse River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I,
II, III and IV hereof.
This permit shall become effective December 1, 2013.
This permit and authorization to discharge shall expire at midnight on April 3 0, 2018.
Signed this day November 8, 2013.
_ Thomas A. Reeder, Director
Division of Water Resources
By Authority of the Environmental Management Commission
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DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit NCO022217
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing this number is no longer effective.
Therefore, the exclusive authority to operate and discharge from this facility arises under the permit
conditions, requirements, terms, and provisions described herein.
Motiva Enterprises, LLC
is hereby authorized to:
1. continue to operate a Surface -Water Pollution Control System managing stormwater and
related petroleum -contact water held in proximity to above -ground storage tanks (ASTs) and
appurtenant piping for the distribution of hydrocarbon fuels, petroleum distillates, and ethanol
[surface bulk -storage exceeding one (1) million gallons], the System consisting of
• truck -loading rack with stormwater runoff containment [petroleum -contact
water, containerized and recycled offsite];
• earthen berms [dikes] surrounding ASTs [secondary -containment areas]
• runoff -containment pond
• gravity drain piping with discharge sample point and gate valve, hand -
operated, normally closed
located at the Motiva Raleigh Terminal, 2232 Ten Ten Road, Apex; and
2. discharge from said treatment works via Outfall 001, located on the attached map, to an
unnamed tributary (UT) to Middle Creek [Stream Segment 17-43-15-(1)], a waterbody
currently classified C; NSW within Subbasin 03-04-03 of the Neuse River Basin.
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DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit NCO022217
PART I
A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
Beginning upon the effective date and lasting until permit expiration, the Permittee is authorized to
discharge treated wastewater/stormwater from Outfall 001. Such discharges shall be limited and
monitored) by the Permittee as specified below:
EFFLUENT
CHARACTERISTICS
(Parameter Codes)
LIMITS
MONITORING REQUIREMENTS
1
Monthly
Average
Daily
Maximum-—'
Measurement
Frequency
Sample
Type
Sample
Location
Flow 2
50050
Episodic
2
Effluent
Total Suspended Solids
C0530
45.0 mg/L
Monthly
Grab
Effluent
Turbidity
00076
Monthly
Grab
Effluent
Oil and Grease 3
00556
Monthly
Grab
Effluent
Benzene 3
34030
Monthly
Grab
Effluent
Toluene
34010
Monthly
Grab
Effluent
Eth lbenzene
34371
Monthly
Grab
Effluent
X lene 3
81551
Monthly
Grab
Effluent
Naphthalene 3
34696
Monthly
Grab
Effluent
MTBE 3
22417
Quarterly
Grab
Effluent
WET Testing 4
TAE6C
Annually 4
Grab
Effluent
Footnotes:
1. No later than 90 days from the permit effective date, begin submitting discharge Monitoring
Reports electronically using NCDWR's eDMR application system. See Special Conditions A. (3.
2. Flow — If no flow occurs within a given month, the Permittee shall submit a monthly
Discharge Monitoring Report (DMR) indicating "No flow" or "No Discharge." Flow shall be
monitored with each discharge event, and may be monitored in one of four ways:
a. measure flow continuously;
b. Rational Method -- calculate flow based on total rainfall per unit area,
including built -on area draining to the outfall;
c, estimate flow at 20-minute intervals during the entire discharge event; or
d. report flow based on discharge pump logs.
3. Samples to be collected concurrently with WET -Test sampling.
4. Whole Effluent Toxicity (WET) Testing — Acute WET testing has been relaxed from Quarterly to
Annually based on past compliance. Testing will continue Annually provided that the Permittee
maintains WET -test results showing "pass" [LC50 > 100%] for each annual event. If WET -test
results show "fail" [LC50 < 100%] the sampling frequency shall immediately increase to
Quarterly in accord with Section A. (2.), and the Permittee shall not regain eligibility for annual
testing frequency except after five (5) consecutive calendar quarters showing "Pass."
Conditions:
1. The Permittee shall discharge no floating solids or foam.
2. The Permittee shall discharge no tank solids, tank bottom water, or tank rag layer.
3. Following hydrostatic tank testing, the Permittee shall discharge no tank (or pipe) contents with
concentrations of benzene exceeding 1.19 µg/L or toluene greater than 11 µg/L.
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DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit NCO022217
A. (2.) ACUTE TOXICITY MONITORING - LIMITED (ANNUAL)
ACUTE TOXICITY MONITORING (EPISODIC)
Petroleum Bulk Storage
The Permittee shall conduct quarterly acute toxicity tests [except when relaxed to Annual monitoring]
using protocols defined as definitive in E.P.A. Document EPA/600/4-90/027 entitled "Methods for
Measuring the Acute Toxicity of Effluents to Freshwater and Marine Organisms." The monitoring shall
be performed as a Fathead Minnow (Pimephales promelas) 24-hour static test. Effluent samples for self -
monitoring purposes must be obtained below all waste treatment. The tests will be performed on a
discharge event during each quarter (January -March, April -June, July -September, October -
December), except when relaxed to Annual monitoring.
Should there be no discharge [no flow] from the facility during a quarter in which toxicity monitoring is
required, the Permittee will complete the information located at the top of the aquatic toxicity (AT) test
form indicating the facility name, permit number, pipe number, county, and the month/year of the report
with the notation of "No Flow" in the comment area of the form. The report shall be submitted to the
Environmental Sciences Section at the address cited below.
The parameter code for this test is TAE6C. All toxicity testing results required as part of this permit
condition will be entered on the Effluent Discharge Form (MR-1) for the month in which it was
performed, using the appropriate parameter code. Additionally, DWR Form AT-1 (original) is to be sent
to the following address:
Attention: North Carolina Division of Water Resources
Environmental Sciences Section
1621 Mail Service Center
Raleigh, N.C. 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later
than 30 days after the end of the reporting period for which the report is made.
Test data shall be complete and accurate and include all supporting chemical/physical measurements
performed in association with the toxicity tests, as well as all dose/response data. Total residual chlorine
of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of
the waste stream.
Should any test data from either these monitoring requirements or tests performed by the North Carolina
Division of Water Resources indicate potential impacts to the receiving stream, this permit may be re-
opened and modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control
organism survival and appropriate environmental controls, shall constitute an invalid test and will
require immediate follow-up testing to be completed no later than the last day of the month following the
month of the initial monitoring.
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DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit NCO022217
A (3.) ELECTRONIC REPORTING - DISCHARGE MONITORING REPORTS
Proposed federal regulations require electronic submittal of all discharge monitoring reports (DMRs)
and specify that, if a state does not establish a system to receive such submittals, then Permittees must
submit DMRs electronically to the Environmental Protection Agency (EPA). The Division intends to
adopted and implement these regulations in 2013.
NOTE: This special condition supplements or supersedes the following sections within Part II of this
permit (Standard Conditionsfor NPDES Permits):
• Section B. (11.) Signatory Requirements
• Section D. (2.) Reporting
• Section D. (6.) Records Retention
• Section E. (5.) Monitoring Reports
1. Reporting [Supersedes Part H, Section D. (2.) and Section E. (5.) (a)1
Beginning no later than 90 days from the effective date of this permit, the Permittee shall begin
reporting discharge monitoring data electronically using the NC DWR's Electronic Discharge
Monitoring Report (eDMR) internet application.
Monitoring results obtained during the previous month(s) shall be summarized for each month and
submitted electronically using eDMR. The eDMR system allows permitted facilities to enter
monitoring data and submit DMRs electronically using the internet. Until such time that the state's
eDMR application is compliant with EPA's Cross -Media Electronic Reporting Regulation
(CROMERR), Permittees will be required to submit all discharge monitoring data to the state
electronically using eDMR and will be required to complete the eDMR submission by printing,
signing, and submitting one signed original and a copy of the computer printed eDMR to the
following address:
NC DENR / DWR / Information Processing Unit
ATTENTION: Central Files / eDMR
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
If a Permittee is unable to use the eDMR system due to a demonstrated hardship or due to the facility
being physically located in an area where less than 10 percent of the households have broadband
access, then a temporary waiver from the NPDES electronic reporting requirements may be granted
and discharge monitoring data may be submitted on paper DMR forms (MR 1, 1. 1, 2, 3) or
alternative forms approved by the Director. Duplicate signed copies shall be submitted to the
mailing address above.
Requests for temporary waivers from the NPDES electronic reporting requirements must be
submitted in writing to the Division for written approval at least sixty (60) days prior to the date the
facility would be required under this permit to begin using eDMR. Temporary waivers shall be valid
for twelve (12) months and shall thereupon expire. At such time, DMRs shall be submitted
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DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
Permit NC0022217
electronically to the Division unless the Permittee re -applies for and is granted a new temporary
waiver by the Division.
Information on eDMR and application for a temporary waiver from the NPDES electronic reporting
requirements is found on the following web page:
http://portal.ncdenr. org/web/wg/admin/bog/ipu/edmr
Regardless of the submission method, the first DMR is due on the last day of the month following
the issuance of the permit or in the case of a new facility, on the last day of the month following the
commencement of discharge.
2. Si2natory Requirements [Supplements Part II, Section B. (11.) (b) and supersedes Section B. (11.) (d)1
All eDMRs submitted to the permit issuing authority shall be signed by a person described in Part Il,
Section B. (I 1.)(a) or by a duly authorized representative of that person as described in Part Il,
Section B. (I 1.)(b). A person, and not a position, must be delegated signatory authority for eDMR
reporting purposes.
For eDMR submissions, the person signing and submitting the DMR must obtain an eDMR user
account and login credentials to access the eDMR system. For more information on North
Carolina's eDMR system, registering for eDMR and obtaining an eDMR user account, please visit
the following web page:
http://pol-tal.nedenr.org/web/wq/admin/bog/l*pu/edmr
Certification. Any person submitting an electronic DMR using the state's eDMR system shall make the
following certification [40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL
BE ACCEPTED:
"I certify, under penalty of law, that this document and all attachments were prepared tinder my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the information,
the information submitted is, to the best of my knowledge and belief, trite, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations. "
3. Records Retention [Supplements Part H, Section D. (6.)]
The Permittee shall retain records of all Discharge Monitoring Reports, including eDMR submissions. These
records or copies shall be maintained for a period of at least 3 years front the date of the report. This period
may be extended by request of the Director at any time [40 CFR 122.41].
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DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC
n
I°Y
Motiva Enterprises,
LLC
Raleigh Terminal
State Grid/Quad: E23NE / Apex, NC Sub -Basin:
03-04-03
Permitted Flow: Episodic -- not limited Stream Class:
C; NSW
Stream Segment: 27-43-15-(1) HUC:
03020201
Receiving Stream: UT to Middle Creek Drainage Basin: Neuse River
Approximate Facility
Boundary
l T.—
Facility�-
Location
not to scale
NPDES Permit NCO022217
North
Wake County

DocuSign Envelope ID: F00435A5-CFA2-4D47-AFE2-734BB9D7EEAC