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WQ0035049_Monitoring - 05-2020_20200626
PENDER COUNTY UTILITIES Kenneth Keel, PE, Director ,•�%�T 605 E. Fremont Street P C U P.O. Box 995 —d- County Utilities m ,hd,oQa;;,y Burgaw, NC 28425 Phone - 910.259.1570 Fax - 910.259.1579 June 26, 2020 RE: Maple Hill WWTF Permit # WQ0035049 NDMR & NDAR-1 submittal Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Three copies of the following documents are enclosed for the subject facility: • May 2020, NDMR & NDAR-1 submittal Thank you. Sincerely, kc�f - 1Vq Kenneth P. Keel, PE Director Cc: Chris Pickett, MH_WWTF Superintendent File FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page_1_of _4_ Permit No.: WQ0035049 Facility Name: Maple Hill WWTF County: Pender Month: May Year: 2020 Did irrigation occur Field Name: 1 Field Name: 2 Field Name: 3 Field Name: 4 at this facility? Area (acres): 1.72 Area (acres): 1.72 Area (acres): 1.72 Area [acres): 1.72 Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Bermuda d YES ❑ NO Hourly Rate (In): 0.41 Hourly Rate (In): 0.41 Hourly Rabe (In): 041 Hourly Rate (In): 0.41 Annual Rate (in): 2971 Annual Rabe (in): 29.71 Annual Rate (in): 29.71 Annual Rate (in): 29.71 Weather Freeboard Field Irrigated? p YES ❑ NO Field Irrigated? 21 YES ❑ NO Field Irrigated? I] YES ❑ No Field Irrigated? El YES ❑ NO m E o m o m 16�p it �: N Q m a ax E o► k`C �'C� m w m m o, E � b Em fg E $ � Oi � �y E �C 7.0 C ' m m� ?�C 7t'C a m ~� 1a � _ a �a ~'E 7� a a _ ° 3-a �a ~ O E � x3 a- E m �a ~'E E a - 0 a J _ � OF In ft ft gal min in In gal I min In in gal min In in gal min In In 1 PC 60 0.8 4.7 2 3 41 C 73 0 1 4.7 51 R 58 0.2 1 4.7 6 CL 61 1 4.7 7 C 56 0 4.7 8 C 53 0 4.7 9 10 11 C 67 0 4.7 12 C 52 0 4.7 396 20 0.01 0.01 395 1 20 0,01 0.01 394 20 0.01 001 13 CL 63 0 4.7 14 CL 69 0 4.7 15 C 73 0 4.7 16 17 18 CL 76 0.5 4.7 1 395 20 0.01 0.01 19 R 69 0.2 4.7 201 CL 62 0.1 4.7 21 R 66 6 4.8 22 C 72 1 A 4.8 23 24 C 77 0.2 4.8 387 30 0.01 0.01 389 30 0.01 0.01 390 30 0.01 0.01 390 30 0.01 0.01 25CL 68 0 4.8 261 CL 71 0 4.8 367 20 0.01 0.01 372 20 0.01 0.01 366 20 0.01 0.01 368 20 0.01 0.01 271 CL 75 0 4.7 28 CL 78 0 4.7 365 30 0.01 0.01 369 30 0.01 0.01 1 370 30 0.01 0.01 364 30 0.01 0.01 29 PC 79 0 4.7 30 31 Monthly Loading: 1.515 0.03 1,525 0.03 1,520 0.03 1,517 0.03 10.34 U Month Floating Total (in): 10.76 10.54 10 4$ FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _2- of _44 Permit No.: W00036049 Facility Name: Maple Hill WWTF County: Pender IMonth: May Year: 2020 Did irrigation occur Field Name: 5 Field Name: 6 Field Name: 7 Field Name: 8 at this facility? Area (acres): 172 Area (acres): 1.72 Area (acres): 1 74 Area (acres): 1.71 Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Bermuda 21 YES ❑ NO Hourly Rate (in): 0.41 Hourly Rate (In): 0.41 Hourly Rate (In): 0.41 Hourly Rate (In): 0.41 Annual Rate (In): 2971 Annual Rate (in): 29.71 Annual Rate (In): 2971 Annual Rate (In): 29.71 Weather Freeboard Field Irrigated? p YES p NO Field Irrigated? 0 YES ❑ NO Field Irrigated? 21 YE5 ❑ NO Field Irrigated? Rl YES ❑ NO m lu o im�pp m ° ' a W E pp 0i 0i � E� C 0 E�6 p 01 Ol �i C 3 y` C E C E �+ Oi 4. C 7 T C L ?,a m W 3a �a °� a�x� 3a Em �a ~ ,�� Ens ° x443 �g EW �a ~ Ey _�- Ee ° x ° ° °'= '.� E°� g J r 9 a � a us g OF In ft ft gal min In In gal min in in gal min In in j gal min In in 1 PC 60 0.8 4.7 2 3 4 C 73 0 4.7 376 20 0.01 0.01 376 20 0.01 0.01 373 20 0.01 0.01 5 R 58 0.2 4.7 6 CL 61 1 4.7 7 C 56 0 4.7 a C 53 0 4.7 9 10 III C 67 0 4.7 12 C 52 0 4.7 13 CL 63 0 4.7 14 CL 69 0 4.7 15 C 73 0 4.7 16 17 16 CL 76 0.5 4.7 400 20 0.01 0.01 409 20 0.01 0.01 406 20 0.01 0.01 395 20 0.01 0.01 19 R 69 1 0.2 1 4.7 20 CL 62 0.1 4.7 21 R 66 6 4.8 22 C 72 1.1 4.8 23 241 C 77 0.2 4.8 403 30 0.01 0.01 410 30 0.01 0.01 25 CL 68 0 4.8 407 30 0.01 0.01 397 1 3D 0.01 0.01 26 CL 71 0 4.8 376 1 20 0.01 0.01 385 20 0.01 0.01 27 CL 75 0 4.7 380 20 1 001 0.01 368 20 0.01 0.01 2a CL 78 0 4.7 1 378 30 0.01 0.01 380 30 0.01 0.01 29 PC 79 0 4.7 379 30 0.01 001 364 30 0.01 0.01 30 31 Monthly Loading: 1,557 0.03 1,960 0.04 1,948 0.04 1,897 0.04 12 Month Floating Total (in): 10.36 10.42 1 D 32 10.23 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _3^ of _4_ Permit No.: WQ0035049 Did irrigation occur at this facility? El YES ❑ NO 0 Weather Freeboard Facility Name: MAPLE HILLWWTF Field Name: 9 Field Name: 10 County: Pe der Month: May Field Name: 11 Field Name: Year: 2020 Area (acres): 175 Area (acres): 1.77 Area (acres): 172 Area (acres): Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Hourly Rate (In): 0.41 Hourly Rate (In): 0.41 Hourly Rate (In): 0.41 Hourly Rate (In): Annual Rate (in): Field irrigated? 29.71 Rl YEs ❑ No Annual Rate (in): Field Irrigated? 29.71 El YES ❑ NO Annual Rate (In): Field Irrigated? 2971 21 YES ❑ NO Annual Rate (In): Field Irrigated? ❑ YES ❑ NO a v m l9 a is a E Q rh u a 16V m �= A �a_ E, F= re E rA E �'S o m a p a �a E oa m� p m E m �._ E �� o 2_ m a_ o c a �a as F �_ O E rA �'._ E v M�� m E m �-- C a as 'g m}S E gm _ ~ :A ,,c -- � E E 3v o �_� OF In ft $ gal miry I in in gal min in I in gal min in in gal I min in I In 1 2 PC 60 0.8 4.7 3 4 C 73 0 4.7 365 20 0.01 0,01 374 20 0.01 0,01 346 20 0.01 OA1 5 6 R CL 58 61 0.2 1 4.7 4.7 7 C 56 0 4.7 81 9 C 53 1 0 1 4.7 10 11 C 67 0 4.7 12 C 52 0 4.7 13 CL 63 0 4.7 14 151 CL C 69 73 0 0 4.7 4.7 16 17 18 19 CL R 76 69 0.5 0.2 4.7 4.7 401 20 0.01 0.01 397 20 0.01 1 0.01 373 20 0.01 0.01 20 CL 62 0.1 4.7 211 R 66 6 4.8 221 23 C 1 72 1.1 4.8 24 25 26 C CL CL 77 68 71 0.2 0 0 4.8 4.8 4.8 408 30 0.01 0.01 403 30 0,01 1 0.01 379 30 001 0.01 27 CL 75 0 4.7 378 1 20 0.01 1 0.01 377 20 0.01 0.01 354 20 0.01 0.01 28 CL 78 0 4.7 29 PC 79 0 4.7 383 30 0.01 0.01 1 380 1 30 0.01 0.01 356 30 0.01 0.01 30 r��12Monthly Loading: Month Floating Total pn): 1,935 0.04 10,42 1,931 0.04 %37 9,808 0.04 10.20 0 0.00 FORM. NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page_4 of_4_ Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? ❑+ Compliant ❑ Non -Compliant p Compliant ❑ Non -Compliant 21 Compliant ❑ Non -Compliant 0 Compliant ❑ Non -Compliant 21 Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective aulU11k0j %ORV&I. nROIAI GUMMU1 lar 01 rOOW rl Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: JAMES PROCTOR Permittee: Pender County Utilities Certification No.: 29132 Signing Official. Kenneth Keel Grade: WW-SI Phone Number: 910-259-1570 Signing Official's Title: Director Has the ORC changed since the previous NDAR-1? ❑ Yes ❑1 No Phone Number: 910-259-1570 Permit Exp.: 3/31/21 Signature Date Signature Date By this signature. I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty or law, that this document and all attachments were prepared under my direction or supervlslon In accordance with a system designed to assure that all qualified personnel property gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the irtarmatlon, the Information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDMR 10-13 NOWDISCHARGE MONITORING REPORT (NDMR) Page _1_of_2_ Permit No.: WQ0035049 Facility Name: Maple Hill WWTF County. Pender Month: May Year: 2020 PPI: 001 Flow Measuring Point: Rl Inffuent ❑ Effluent ❑ No flaw generated Parameter Monitoring Point: ❑ Influent 0 Effluent 17 Groundwater Lowering ❑ Surface water Parameter Code 50050 00400 00310 00530 00610 00620 00625 31616 00600 00665 00940 70300 i a E �~ O E$ HN a0 0 a in O �a C W c ~ o co c E E Q x grm ��' ~Y LLV m 1 o �L p P a $ V die 9 � N d0 24-hr hrs GPD su mg/L mg/L mg/L mg/L mg1L #1100 mL mglL mg/L mg/L m L 1 09:30 4 10,347 7.8 2 12,234 3 12,871 4 09:15 5 10,662 8 5 09:00 5 12,623 7.9 61 10:00 4 22,886 7.9 7 10:00 4 12,387 7.9 8 09:30 4 11,423 7.8 9 11,723 10 14,612 11 09:15 5 6,331 7.8 121 09:00 6 5,676 7.7 4 <2.5 34 0.31 5.5 >2420 5.57 6.33 13 09:00 4 7,968 7.9 14 09:45 5 11,823 7.8 15 09:00 4 10,744 7.8 >2420 16 11,432 17 1 12,818 181 09:30 5 12,865 7.8 19 09:45 5 12,900 7.8 20 09:45 5 22,399 7.7 21 09:45 4 95,544 7.8 22 09:45 4 10,549 7.7 23 1 11,021 241 08:00 4 4,330 25 08:00 4 4,774 7.7 26 09:30 5 3,866 7.5 27 09:30 5 3,959 7.5 28 09:15 4 3,531 10 <1 MPN 1100 29 09:30 4 3,855 7.6 301 4,528 311 4,783 Average: 12,816 4.00 0.00 3.40 0.31 5,50 1.00 5.57 6.33 Daily Maximum: 95,544 10.00 4.00 2.50 3.40 0.31 1 5.50 #VALUEI 5.57 6.33 Daily Minimum: 3,531 7.50 4,00 2.50 3.40 0.31 5.50 #VALUEI 557 6.33 Sampling Type: Recorder Grab Composite Composite Composite Composite Composite Grab Composite Grab Composite Composite Monthly Avg. Limit: 42,000 nla 30 30 15 n/a We 200 n/a n/a nIa nla Daily Limit: nla a to 9 n/a n/a n/a nla n/a n/a We We n/a nla Sample Frequency: 1 Confl;Zs 5XWK Weekly Weekly Weekly Weekly Weekly Weekly Monthly Montly 3XYR 3XYR FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page 2_ of 2_ Name: Name: Sampling Person(s) Samples were collected by the Certified Laboratory Certified laboratories Name: Environmental Chemists, Inc. Name: Jay Baker Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant 17 Nan-Gompllant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective taxen. Htiacn aaamonai sneers it reason for being non compliant UV system was not operating correctly.The date 5 / 12 /2020 and 5 / 1512020. 1 thought the system needed cleaning so Its in the numbers were the same so I replaced the bulbs. I had the system resampled again on 5/28/2020 and was in compliance. my Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Christopher K. Pickett Permittse: Pender County Utilities Certification No.: 995432 Signing Official: Kenneth Keel Grade: WW2 Phone Number: 910-259-1570 Signing Official's Title: Director Feb ❑ Yes O No Phone Number. 910-259-1570 Permit Expiration: 3/31/2021 Signature Date Signature Date By this signature, I certify that this report Is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualltled personnel property gathered and evaluated the information submitted. Based an my Inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Information, Including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 :envirrochem] ANALYTICAL & CONSULTING CHEMISTS EnvironmentalChemists, ineo 6602 Wnidmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 710 $ow'sertown Road, Manteo, NC 27954 . 252.473.5702Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@a environmentaichemismcom Pender County Utility Operations Date of Report: May 21, 2020 Post Office Box 995 Customer PO #: Burgaw NC 28425 Customer ID: 08100095 Attention: Kurt Lonander Report #: 2020-07797 Project ID: Maple Hill WWTP Lab ID Sample ID: Collect Datefrime Matrix Sampled by 20-19177 Site: Effluent 5/12/2020 9:10 AM Water Walker Diab Test Method Results Date Analyzed Ammonia Nitrogen EPA 35©.1 3.4 mg/L 06/20/2020 Total Kjeldahl Nitrogen (TKN) EPA 351.2 5.5 mg/L 05/20/2020 Residue Suspended (TSS) SM 2540 f] <2.5 mg/L 05/13/2020 BO❑ SM 5210 B 4 mg/L 05/12/2020 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.24 mg/L 05/12/2020 Nitrate+Nitrite-Nitrogen EPA 353.2 0.55 mg/L 05/15/2020 Nitrate Nitrogen subtmcuon Method 0.31 mg/L 05121/2020 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-19178 Site: Effluent - Grab 5112/2020 9.12 AM Water Walker Dian Test Method Results Date Analyzed Fecal Coliform kraaor colifen-9 e >2420 MPN1100ml 05/12/2020 Temperature SM 2550 f3 15.9 C 05/12/2020 pH SM 4600 H B 8.4 units 05/12/2020 Total Phosphorus SM 4500 P F 6.33 mg/L 05/19/2020 Comment: Reviewed by: Report #_: 2020-07797 pane 1 of i Dace _ F I Ze7 t;acHICY Yana: ��' - C p NS t nalyst Y'r Y Permit NpH - Calibration Tune Cal Buffer 4 0 s u. Cat Buffer 10 0 s.u. Check Buffer 7 0 S.U. Comments ' p H check bur'Ter must read within t 0. I pH units of the butTer's true value. 4 so buffer Lot#/: Ricca 22QI791I ZaQ 7 so buffer Lord/ _ R 28os7 7ao 10 su buffer Loth-_ Rim 1203A44 EULLO 0 Sample location sarriple Collection Sample Analysis PH Result I A Post -analysis Bttt%r Time* I Time* 1 s u I r hock vst.. a.. Commencs/Data Quahf'urs r ---?-Oq ► Post analysts buffer check is required when performing analyses at multiple sampling locations and must be withnt t 0 l units of the buffer's true value W pH values in pH units (i.e., s-u.). Record all data to the maraca 0 01 s u. and report to the nearest o. I s.u. Total Residual Chlorine (TRC) Reference Method., SM 4500 CI-G201 t: Hach 8l67 W- Pl�e circle icabie Method Instrument 1D: Daily CWk 5tanda d Restilt Check Sid. standartiTime k s Sample7 Sample ;what Nudynng L� CoTime Analysis 1L or Comments/Data Qtaalifirn WY%L or mg/L a m,dtiniw eit"I Analyzed Time Time Ng/C or mg/1. rRC Daily Check Standard true value pWL or mg/L acceptance raw- g/L or mg/L C: heck standards mast recover within t E0% of the check standard's true value %nmtal Calibration Curve Verification Date: Reagent Blank Value: (Whets appficable..Analyze and document a reagent blank when standards. sample dilutions or PT Samples are prepared} Disaalw:d Oxygen (DO) Calibration/ Calibratiatrvanable Mew reading •Post-analysiscalibratiott Venfcation verification (when necessary) or % efficiency Comitrenrs Time Barometric after calibration Theoretical Calculated Temperature pTessure Value m Value mRll a '�a...arwrf I se this row when performing a',rritletattoa instead of Sample Location Sainpie Collection Sample Analysis DO reading Time mg/L Comments/Dam Qualifiers • When performing analyses at multiple locations, the meter must be remiibrated at each site before analysis or a post -analysis calibration venticauon must be performed. •.anil�le is measured dtrectly :n the ,[warn .andior onsire. erril% ?irnc }naly ud unvld Fe ,&carded a idi a crate that the,= urn ineasureci art hill t7r itmneljaarel� Temperature Iteference Method: SM 2550 B-20l0 instrument In- 1 Sample "Sample Temperature Sample Location ; Collection r Analysis Ic Ti— i r; e . _1 i IN. 1L ! K,46 i � f aunple is rneasutett djr�ctlt an rlre NIteim amlior Oil t;tr• gJ11% rii:ie an.tltccJ Nonual Verification Date 1,2020 Field Personnel Now. CommenEwDiata Qualifiers r,rura; - w nh _t nnae that tia,V .UC riicastrral in situ sr Rev 07i2019 ' p H check bur'Ter must read within t 0. I pH units of the butTer's true value. 4 so buffer Lot#/: Ricca 22QI791I ZaQ 7 so buffer Lord/ _ R 28os7 7ao 10 su buffer Loth-_ Rim 1203A44 EULLO 0 Sample location sarriple Collection Sample Analysis PH Result I A Post -analysis Bttt%r Time* I Time* 1 s u I r hock vst.. a.. Commencs/Data Quahf'urs r ---?-Oq ► Post analysts buffer check is required when performing analyses at multiple sampling locations and must be withnt t 0 l units of the buffer's true value W pH values in pH units (i.e., s-u.). Record all data to the maraca 0 01 s u. and report to the nearest o. I s.u. Total Residual Chlorine (TRC) Reference Method., SM 4500 CI-G201 t: Hach 8l67 W- Pl�e circle icabie Method Instrument 1D: Daily CWk 5tanda d Restilt Check Sid. standartiTime k s Sample7 Sample ;what Nudynng L� CoTime Analysis 1L or Comments/Data Qtaalifirn WY%L or mg/L a m,dtiniw eit"I Analyzed Time Time Ng/C or mg/1. rRC Daily Check Standard true value pWL or mg/L acceptance raw- g/L or mg/L C: heck standards mast recover within t E0% of the check standard's true value %nmtal Calibration Curve Verification Date: Reagent Blank Value: (Whets appficable..Analyze and document a reagent blank when standards. sample dilutions or PT Samples are prepared} Disaalw:d Oxygen (DO) Calibration/ Calibratiatrvanable Mew reading •Post-analysiscalibratiott Venfcation verification (when necessary) or % efficiency Comitrenrs Time Barometric after calibration Theoretical Calculated Temperature pTessure Value m Value mRll a '�a...arwrf I se this row when performing a',rritletattoa instead of Sample Location Sainpie Collection Sample Analysis DO reading Time mg/L Comments/Dam Qualifiers • When performing analyses at multiple locations, the meter must be remiibrated at each site before analysis or a post -analysis calibration venticauon must be performed. •.anil�le is measured dtrectly :n the ,[warn .andior onsire. erril% ?irnc }naly ud unvld Fe ,&carded a idi a crate that the,= urn ineasureci art hill t7r itmneljaarel� Temperature Iteference Method: SM 2550 B-20l0 instrument In- 1 Sample "Sample Temperature Sample Location ; Collection r Analysis Ic Ti— i r; e . _1 i IN. 1L ! K,46 i � f aunple is rneasutett djr�ctlt an rlre NIteim amlior Oil t;tr• gJ11% rii:ie an.tltccJ Nonual Verification Date 1,2020 Field Personnel Now. CommenEwDiata Qualifiers r,rura; - w nh _t nnae that tia,V .UC riicastrral in situ sr Rev 07i2019 Environmental Chemist, Inc. Wilmington, NC Lab #94 6602 VVinrtmil! lha. Wilmington, NC 284C Sample R ceipt [checklist 91U.792.0222 Clien: �t� L}ate.5_ II Report Number Q—�"� �Cl 7 Receipt of sample. Delivered C7 YES ❑ No © YI:S ❑ UP5 ❑ FedEx ❑ Other ❑ N/A 1. Were custody seals present on the col ND N/A � 2. if custody seals were present, were they intact/unbroken' i OriginaI temperature upon receipt •C How temperature taken: Sorrected tent ❑ Temperature gunk. Qerature upon receip- 'C IR Gun ID: Thomas Traceable 5/N 192511657 Against Bottles 13 YES [) No IR Gun Correction Factor `C: 0[t 3 If temperature of YES © No cooler exceeded VC, was Project M r. 4_ Were proper custody8 /4A notified' YES ❑ NO procedures (relinquished/received) followed% 5 Were sample ID s listed YES ❑ NO on the C0C3 1 6. Were samples ID's listed YES ❑ NO on sample 7. Were collection date and YES ❑ NO time Iis ed on the CDC? 8. Were tests to be Performed YES ❑ NO listed on11111111 the COC? 9. Did samples arrive in proper YES ❑ NO containers for each test? 10. Did samples arrive YES ❑ NO in good condition for each test? 11. Was adequate sample YES © NO volume available? 12. Were samples received YES © NO within proper balding time for requested 7 13. Were acid preserved tests i YES ❑ NO ❑ YES ❑ samples received at a pH of <27 * I 14. Were cyanide samples received at a NO YES 0 ND pH >12? 15. Were sulfide samples received at a PH 3,9? © YES Q No © 16. Were NH3 KN P MC / henot received at a chlorine residual of i7• Were Sulfide C snide YES © No received at a chlorine residual of 18 Were orthophosphate samples fi#iered in the field within 15 minutes? TBacte stiles are pH checked at time of analysis and recorded on the benchsheet Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchshee;. r.Sarnple(s) nple Preservaition: {Must be completed for any Y sample(s) incorrectly preserved or with headspace) ddin were received incorrectlypreserved and were adjusted accordingly g Icircle one):e of r Hi5C3, HNO3 HCl Preserved p enervation: If more than one preservative is needed, notate in comments Note: Not+ty customer servile ,m rnediateiy for incorreciiy Pre scry d sanV*s. obtain a belor� notify the state lab if directed new sample or to anah'xcd by the customer, Whe Volatiles Sample{5j was r►otified, date and time were reteivari .ui.i,. �__ COMMEIWTS: -4r--vvc m® m Is cp Q mto V "u !C . (D � 3 0 or O t! L� V Semple CompoaNe s7 c) G) 0 0 0 0 0 l7 G7 0 n 0 n or Gray u G7 'G C? _u fi3 t) zJ -a Container (P or G) a V m V Chlorine I� L.K�� ■■ S Id w tk* NUMBER in n X X NONE m c NCL x A ► MCM M :e M45 I! � NNW C a NAOR x TF10 z 11 OTHM -n 0 z CD 3 0) G Q o CL _ [n o w [n � z o m N -pm a C m to F20, ANALYTICAL & CONSULTING CHEMISTS Pender County Utility Operations Post Office Box 995 Burgaw NC 28425 Attention: Kurt Lonander Environmental Chemists, Inc® 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com environmentalchemists.corn Date of Report: May 18, 2020 Customer PO #: Customer ID: 08100095 Report #: 2020-08109 Project ID: Maple Hill WWTP Lab ID Sample ID: Collect DatelTime Matrix Sampled by 20-19957 Site: Effluent - Grab 5/15/2020 8:50 AM Water Walker Diab Test Method Results Date Analyzed Fecal Coliform Idexx Cortet-1a >2420 MPN/100m1 05115/2020 Comment: Reviewed by: Report*:, 2020-08109 pana I nf I Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 910.392,0223 Sample Receipt Checklist Client: _Per)) d � { . l 1 l' pate: j 3 Report ,� Number: Receipt of sample: © Delivered UPS ❑ FedEx Q Other C] YES N/A I. Were custody seals present on the cooler? 13YES 113 NO N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt ---�' Corrected temperature upon receipt How temperature taken: © Temperature Blank Against Bottles IR Gun 10: Thomas Traceable S/N 192511657 ill Gun Correction Factor'C: 0.0 © YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified? YE5 © NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO S. Were sample ID's listed on the COC? Jf YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7, Were collection date and time listed on the COU JX YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO— 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YE5 ❑ NO 11. Was adequate sample volume available?' X YES ❑ NO 12, Were samples received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2? • ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? © YES © NO 1S. Were sulfide samples received at a pH >9? 13 YES d YES ❑ NO ❑ 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? •� ❑ YES NO © 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? NO 18. Were orthophosphate samples filtered in the field within 15 minutes? ' TOCNolatiles are pH checked at time of analysis and recorded on the benchsheet. *' Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO, HNO3 HCl NaOH Time of preservation: If more than one preservative is needed. notate in comments below Note: !Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: OOC. QA.002 m m o � 4 � n � o a s C� 0 e � a 38"w* Type 0000000000000000 compoom o. Grab S Cwrtalner (P or O} G) Chkwhw PH of 6olth A � 14UMBER NONE HCL H29O4 m $ NNW m i NAOH TM � FILTERED Z ID . • OTHER t� si m m � C) ze M t/1 r4 Ei m 0 10 "o Z O m o 0 Z z 3 M M h I If m O A Z G O O 1 7 m z ZZ z �t 10 D m �x s M Z x X D S o N O to m m m g [) za la'a r Z 0 ,Fppwpw,— Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environnsentalchemists.corn Pander County Utility Operations Post Office Box 995 Burgaw NC 28425 Attention: Chris Pickett, ORC Date of Report: Jun 01, 2020 Customer PO #: Customer ID: 08100095 Report #: 2020-08752 Project ID: Maple Hill WWTP Lab ID Sample ID: Collect Daterrime Matrix Sampled by 20-21585 Site: Effluent - Grab 5/28/2020 12:50 PM Water jcb/envirochem Test Method Results Date Analyzed Fecal Coliform IdemColflen-18 <1 MPN/100ml 05/28/2020 Comment: �'_�.� Reviewed by: '`�a'� ......_ Report #:: 202MB752 Pegg 1 of 1 Environmental Chemist, Inc., Wilmington, NC Lab ##94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client: PEKiD*- Q. DateA a Report Numbe 0 - d 8-) Receipt of sample'. Delivered UPS ❑ FedEx ❑ Other ❑ ❑ YES 113 NO N/A 1. Were custody seals resent on the cooler? ❑ YES 10 NO N/A 2. If custody seals were present, were they intact/unbroken? Original tem rature u an receipt J 'C Corrected temperature upon receipt °C How temperature taken: ❑ Temperature Blank Against Bottles I Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0 ❑ YES ❑ NO 3. if temperature of cooler exceeded VC, was Pro' et M r./QA notified? OIL YES ❑ NO 4. Were pMUr custody procedures (relin uished/received) followed? Vr YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the CDC? YES ❑ NO S. Were tests to be performed listed on the COC? Xf YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in lood condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were sam les received within proper holding time for requested tests? © YES ❑ NO 13. Were acid preserved samples received at a EH of <27 ❑ YES ❑ NO 14. Were cyanide samples received at a W >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >97 ❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? " ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Voiatiies are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded an the benchsheet. nple Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) nple(s) were received incorrectly preserved and were adjusted accordingly adding (circle one): H2SO4 HNO3 HC1 NaOH Ye of preservation: if more than one preservative is needed, notate in comments below e: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or fy the state lab if directed to analyzed by the customer. Who was notified, date and time: latiles Sample(s) were received with headspace COMMENTS: 00C. QA.002 n m m a � x � O w � z W � m 3 � D � r o � � a � SBmpie Type G) C) G) n G) C) G) 0 G) C) G) C) G) 0 G) C) Gomposke 3 I Grob G) tJ 0 G) Tt G) -M G) -u G) Zt G) -0 Container ip or G) y Chlonne MVIL o � PH of battle a LAB IQ NUMBER NONE HCL H2sO,4 m, m $ HNO3 M NAOH THiO Q FILTERED Z OTHER i D iy* C � b ! IM 0 r m C7 0 z a z G? a_ z Q n C Q m zz �C O A Z T 9rn g Z O wmq z Z �r v 0 C)m m Op V� z • m z 0 len7vi •och m] ANALYTICAL & CONSULTING CHEMISTS Environmental emists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Ponder County Utility Operations Date of Report: Jun 01, 2020 Post Office Box 995 Customer PO #: Burgaw NC 28425 Customer ID: 08100095 Attention: Chris Pickett, ORC Report #: 2020-08757 Project ID: Maple Hill WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 20-21590 Site: Effluent - Grab 5/28/2020 1:00 PM Water jcb/enwirochem Test Fecal Coliform Comment: Reviewed by: method ldexx Colilert-18 Results Date Analyzed <1 MPN/100ml 05/28/2020 Report #:: 2020-08767 Pace 1 of 1 Environmental Chemist, Inc., Wilmington, NC Lab ##94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client: l CD • Date h<5 aZ 0 Report Number 0 - a $� Receipt of sample: Delivered UPS ❑ FedEx ❑ Other CO ❑ YES 10 NO N/A 1. Were custody seals Eresent on the cooler? ❑ YES 10 NO Q N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected tem erasure u on receipt °C How temperature taken: ❑ Temperature Blank Against Bottles IR Gun ID: Thomas Traceable S/N 192.511657 IR Gun Correction Factor °C: 0.0 ❑ YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project M r./qA notified? Vk YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples 10's listed on sample containers? YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑7 NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were sam les received within proper holding time for requested tests? ❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <27' ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? ❑ YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES 10 NO 118. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. *' Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: if more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 I -A O 0 m m V n V �r 0 a a 3 � E � b 1 O � = m z o =� . a Sample Type 00 G) 0(7) n G) 0 G) 0G) 0 G) 0 G) 0 C alt6 ar Grab Gofftalner S (P or 6) � Chloflffe v m Ga mg/ t PH of bottle LAS ID O NUMBER # m $ I { NONE HCL ct 3 i H2304 ! k HNO3 In g NAOH y Y TWO O6 FILTERED Z OTHER c G z jP r r 9 1 ra p m Q c � a m f c v 90 3 up ur Z n a m z E O "�z m m z r n x m Y• r�rA VS z 0