WQ0009477_Renewal (Application)_20200612

State of North Carolina
Department of Environmental Quality
Division of Water Resources
WATER QUALITY REGIONAL OPERATIONS SECTION
NON -DISCHARGE APPLICATION REVIEW REQUEST FORM
Divlslon.of Water Resources
June 18, 2020
To: FRO-WQROS: Trent Allen / Mark Brantley
From: Poonam Giri, Water Quality.Permitting Section - Non=Discharge Branch
Permit Number: WQ0009417
Permit Type: Distribution of Residual Solids (503 Exempt)
Applicant: Cascades Tissue Group - North Carolina, A Division of Cascades Holding US Inc. Project Type: Renewal
Owner Type: Organization Owner in BIMS? Yes
Facility Name: Rockingham FiberClay Distribution Program Facility in BIMS? Yes
Signature Authority: John Quick
Address: PO Box 578, Rockingham, NC 283810
Fee Category: Non -Discharge Major .
Comments/Other. Information; [e-mail], eblack@nc:rr.com
Title:. Mill Manager
County; Richmond
Fee Amount: $0 - Renewal
Attached, you will- 'find all 'information submitted' in - support of the above -referenced application, for your 'review,
comment, and/or action. Within,45'calendar days, please take the following actions: .
® Return this form completed. Z Return a completed staff report.
❑ Attach an Attachment B for Certification. ❑ Issue an Attachment,B Certification.
When you receive this request form, please write your name and dates in the spaces below, make a copy of this sheet, and
return it to the appropriate Central Office Water Quality Permitting'Section contact person listed above.
RO-WQROS Reviewer: Date: /y 20 ZO
FORM: WQROSNDARR 09-15 Page 1 of 1

(V
Cascades
Date: Jun 12.2020
To: North Carolina Department of Environment Quality
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit.
1617 Mail Service Center
Raleigh, NC ,27699-1636
1-919-807-6464
Cascades Tissue Group — North Carolina
A Division of Cascades Holding US Inc.
805 Midway Road, P.O. Box 578, Rockingham, NC 28380 USA
Phone: [phone] Fax: [phone]
www.cascades.com * [e-mail]
From: Karen Bellamy
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
805 Midway Rd.
Rockingham, NC 28379
1-910-895-4033
RECEIVEDINCDEGIDWR
JUN 1 8 2020
Non -Discharge
Permitting Unit
Attention: NCDENR Division of Water Resources Water Quality Permitting Section Non -Discharge Permitting
Unit.
Subject: Permit Renewal — Cascades Tissue Group — North Carolina, a division of Cascades Holding US Inc.
Dear
Cascades Tissue Group — North Carolina, a Division of Cascades Holding US Inc., (Cascades Tissue Group)
looks forward to continuing the successful Cascades Soil Amendment Program and will Submit ARM Check
for Payment of $1310 , forms and analyses to support the application for the renewal of Permit No.
WQ0009477 have been included.
Cascades Tissue Group has operated the Cascades Soil Amendment Program for greater than 20 years to the
benefit of local farmers, the environment and Cascades Tissue Group. Cascades Soil Amendment Program is
also registered with the North Carolina Department of Agriculture as a Soil Additive. Farmers have received
free Soil Amendment, free delivery and free spreading and saved $20 to $30 per acre by not having to purchase
agricultural lime. In times of very low farm grain and cotton prices, the free Cascades Soil Amendment may
have saved some farm operations.
The permit renewal allows Cascades Tissue Group and the North Carolina Department of Environment and
Natural Resources - Division of Water Resources (DWR) the opportunity to improve the Cascades Soil
Amendment Program. Based on greater than 20 years of experience, operations and characteristics, selected
conditions contained in the current permit are recommended for modification or removal. These conditions are
identified in the format of the current permit and are as follows:

1. We would like to request that we increase the material days in field be increase to one cropping cycle.
We are requesting this because of the increase in the amount of rain (due to climate Change) has made it
more difficult to meet the current permit time line. Also due to all the heavy rains that we have seen from
Hurricanes in the last few year and the water table being so high.
We want to thank you for your attention to the Cascades Soil Amendment Program and we would appreciate
reviewing and discussing the draft permit prior to final issuance.
Thank You
Date:
Jo uick: Mill Manag

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 11-13 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website at:
htln: //porlcr/. nc•clenr. or�'lreh/ivy/�rps//au
General —This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T . 1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 11-13):
X Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 11-13) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
X The project name should be consistent on the plans, specifications, etc.
X The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC
02T .0106(b).
❑ If this project is for a modification of an existing permit, submit one copy of the existing permit.
X Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
X Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environment and
Natural Resources (NCDENR).
X STANDARD REVIEW — Submit the appropriate fee for all new and major modification applications as listed in the table
below.
STANDARD APPLICATION REVIEW FEES:
Facility Classification New Permit Major Modification'
Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395
Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245
- A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
X List all items included in the application package, as well as a brief description of the requested permitting action.
INSTRUCTIONS FOR FORM: DCAR 1 1-13 Page 1 of 3

D. Program Information (All Application Packages)
X Provide a narrative explaining the following:
The Cascades Program is based on the agricultural value of the lime.
X How the materials will be handled and transported from where the residuals were produced to where it will be treated.
The Cascades Biosolids will be removed from the storage pad floor and loaded with a front-end loader into dump,
tandem dump or other suitable trucks for transport to the designated field.
X How the residuals will be processed/treated (attach process flow diagram).
No further treatment or processing of the Cascades Biosolids is currently conducted or planned.
X How leachate collection will be handled.
FiberClay is placed in a covered area. Only a small amount of water is produced from the pile while in the storage area.
Water is collected and managed as part of the mill storm water program.
X Where the residuals will be stored until processed.
Cascades Biosolids will be stored in a three walled, concrete floor and metal roof storage area at the mill.
X How the final product will be distributed (packaging, bulk, etc.)
Bulk
X What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention
of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
Lime
X Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
a. The Cascades Biosolids Marketing Program will enter the 16" year. It is established and to a large degree relies on the
success of previous years. The marketing program incorporates activities for former and new farmers. Former farmers
are contacted by visit, phone and email. Most fanners in the Cascades Program area require lime every 2 — 4 years
depending on crop and management. New fanners are introduced to the Cascades Program by their neighbors, the
brochure, or truck signage advertising.
b. All of the estimated 50,000 wet tons/yr will be distributed to farms.
X Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided
to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
The Cascades Program Label, Information Sheet and UA are presented in Appendix A.
X Name and address of the person who prepared the residual that is sold or given away.
X A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
❑ A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
❑ A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
❑ Information on all applicable setbacks in accordance with 15A NCAC 021' .1 103(b).
❑ A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) NA
❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 115A
NCAC 021' .1 104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1 108(a) on the plans.
❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T . 1104(a)(2)(B), including leakage and pressure testing as appropriate.
INSTRUCTIONS FOR FORM: DCAR 11-13 Page 2 of 3

❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) NA
❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 03T
.1 104(a).
G. Environmental Assessments (May be Required — See 15A NCAC I C .0300) NA
❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 11-13 Page 3 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
The Operation and Management Plan is presented in Appendix B.
❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
❑ Submit the O&M Plan in accordance with 15A NCAC 02T . l 110 and include at a minimum:
❑ Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
❑ Maintenance schedules; may include equipment's calibration, maintenance of signs, etc.
❑ Safety measures; may include safety training program, manuals, signs, etc.
❑ Spill response plan; including control, containment, remediation, emergency contact information, etc.
❑ Inspection plan including the following information;
❑ Names and titles of personnel responsible for conducting the inspections.
❑ Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
❑ Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
❑ Sampling and monitoring plan including the following information;
❑ Names and titles of personnel responsible for conducting the sampling and monitoring.
❑ Detailed description of monitoring procedures including parameters to be monitored.
❑ Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 11-13 Page 4 of 3

State of North Carolina
DW
Department of Environment and Natural Resources
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 08-13
I. APPLICANT INFORMATION:
1. Applicant's name: Cascades Tissue Group —North Carolina, a division of Cascades Holding US Inc.
Applicant type: ❑ Individual X Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: John Quick Title: Mill Manager
Applicant's mailing address: POB 578
City: Rockingham State: NC Zip: 28380-
Telephone number: [phone] Email Address: Karen -Bellamy a.cascades.com
2. Consultant's name: Elwood Black License Number (for RE.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address: POB 3244
City: Cary State: NC Zip: 27519-
Telephone number: [phone] Email Address: [e-mail]
3. Fee submitted: 1,310 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, X renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WQ0009477
Date of most -recently issued permit: 12/7/2015
Date of most -recently certified Attachment A (if different than the permit): 12/07/2015
III. FACILITY INFORMATION:
1. Name of residuals processing facility: Cascades Tissue Group
City: Rockingham State: NC Zip: 28380 -
Coordinates: Latitude: 340 55' 46" Longitude: 79' 47' 40"
Datum: NADA 83 Level of accuracy: 1 m
Method of measurement: GPS
County where facility is located: Richmond
2. Facility contact (person familiar with residuals preparation):
Name: Karen Bellamy Title: Environmental Manager
Mailing address: POB 578
City: Rockingham State: NC Zip: 28380-
Telephone number: [phone] E-mail address: Karen [e-mail]
FORM: DCAR 11-13 Page I of 3

3. Is the residual process facility also the generator? ❑ X Yes; ❑ No
If No, please specify delivery frequency and quantity of residual to be processed:
4. Length of residuals storage at facility: 30 days (Note: the Division requires minimum 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.) Cascades has leased land for additional Storage. Old Dedicated
Site if needed for Storage Only. Never had to use it for storage.
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
X❑ other (explain); Bulk Agriculture
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials I
Amounts to be added
per 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: 26000-27000 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 26000-27000 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Stored in three -walled, concrete floor roofed bin until distributed to farm.
6. Does the facility have a stormwater management plan? X❑ Yes; ❑ No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Roof
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
IV
Residuals Source
Certification
FORM: DCAR 11-13 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
X❑ Yes ❑ No, Explain;
(Signature Authority's Name — John Quick)
(Mill Manager)
attest that this application for Cascades Tissue Group North Carolina, a division of Cascades Holding US Inc.
(Cascades Tissue Group North Carolina, a division of Cascades Holding US Inc. )
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: Date: 2
FORM: DCAR 11-13 Page 3 of 3

Facility Map

Imagery ©2020 Maxar Technologies, USDA Farm Service Agency, Map data ©2020 100 ft _ _
Fig. 1— Cascades Tissue Group — Rockingham Mill aerial map.

State of North Carolina
DW Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
X❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please
do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments
to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
X❑ For new or renewed permits, submit a separate certification for each source facility.
X❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed
modification.
X❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
X❑ For each source facility, attach the following:
X❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance
for Residuals Land Application Permits'.
X❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the
residuals are to be generated, treated, processed, and stored at the facility.
X❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
X❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
X❑ For each source facility, attach the following:
X❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this
certification.
X❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
Status Maximum Dry Tons Per Year
Facility Permit Holder Facility Name County Permit Number
Code Current ° Proposed
R Cascades Tissue Group Cascades Tissue Group Richmond WQ0009477 50,000 50,000
8 Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or X❑ Private.
Facility permit issued by: X❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Karen Bellamy -Environmental Manager
Complete mailing address: POB 578
City: Rockingham
Telephone number: (2.LO) 895-4033
4. Facility physical address: 805 Midway
City: Rockingham State: NC
Coordinates: Latitude: 34' 55' 446"
Datum: NAD83
State: NC Zip: 28380-_
E-mail address: Karen [e-mail]
Zip: 23879-
Longitude: 79° 47' 40"
Level of accuracy: lm
Method of measurement: GPS
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, X❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: X ❑ Yes ❑ No
7. Facility permitted/design flow: MGD and facility average daily flow: MGD
8. Average amount of residuals being generated at this facility 23302 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Paper
Type and volume of residuals storage (i.e., outside of residuals treatment units):
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
X❑ 40 CFR Part 503 or ❑ 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
❑ Biological X❑ Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: E3 yes XQ no.
If yes, list the number(s).
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: tj yes X0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Summit & Pace and Date of analysis: 02/08/20
Passed corrosivity test: X❑ yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: X❑ yes ❑ no. Flashpoint s': OF (> 140°F)
Passed reactivity test: X❑ yes Mno. HCN: &a mg/kg (<250) & H2S.
mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
ND
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
ND
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1, 1 -Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace and Date of analysis: 1-09-2020
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
1.3J
Cadmium
85
39
N/A
Copper
4,300
1,500
16.6
Lead
840
300
N/A
Mercury
57
17
N/A
Molybdenum
75
n/a
N/A
Nickel
420
420
1.5
Selenium
100
100
N/A
Zinc
7,500
2,800
199
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ >_ 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 42.7 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace and Date of analysis: 1-09-2020
Parameter
Result
(mg/kg)
Aluminum
N/A
Ammonia -Nitrogen
NC-2.3
Calcium
179000
Magnesium
1560
Nitrate -Nitrite Nitrogen
ND
pH (Standard Unit)
7.0
Phosphorus
N/A
Potassium
N/A
Sodium
N/A
Total Kjeldahl Nitrogen
1630
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.34
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: NA %. This
rate is a (check one): ❑ default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1") Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
NA
NA
Injection/Incorporation
NA
NA
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathoeen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
N/A❑A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T. 1106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T. I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
❑ Alternative I [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item Il. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [ 15A NCAC 02T. ] 106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.1107(a)(8)] -Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] -Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
X❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

General description of Fiber -Clay production

General description of Fiber -Clay production
The mill produces toilet tissue, paper towels and facial tissue from recycled office paper. In the
year 2019, the mill purchased approximately 40,000 tons of recycled office paper to produce
the various Cascades Tissue Group products. The Fiber -Clay is derived from the preparation
and washing of the recycled paper as the recycled paper is converted into the toilet tissue,
paper towels and facial tissue.
Office paper contains fibers that are bound together to form the sheet of paper. To make the
toilet tissue, paper towels and facial tissue, the paper binding agents that hold the fibers
together in the recycled paper office paper need to be broken to form individual fibers. This is
accomplished through beating, screening and washing processes.
First the recycled paper is introduced into large beaters that break the paper into individual
fibers. While the paper is in the beaters, large contaminants such as plastics and metal are
removed by a filter plate. The plastic and metals are removed, collected and sent to a landfill.
The remaining fiber is screened an additional two times to remove smaller contaminants. The
screenings consist of a coarse and a fine screening. Contaminants are removed, collected and
sent to a landfill.
The remaining fiber is now referred to as good fiber. It is then washed to separate the fiber
from clays, calcium carbonate and other filler components that are found in the recycled paper.
The washing process also removes some small fibers from the good fiber. The good fiber then
proceeds to the paper machine to produce the toilet paper, facial tissue, and paper towels.
The clay, calcium carbonate and small paper fibers are sent to a flotation cell. After which these
materials are screened to remove small plastic particles. Next the materials are dewatered in a
belt press to a solids content of between 36 to 50%. The dewatered material is referred to as
Fiber -Clay. It is the Fiber -Clay that Cascades Tissue Group has applied to farm land as a lime by-
product for the past 20 years.

COVER LETTER

(IV
Cascades
Date: Jun 10.2020
To: North Carolina Department of Environment Quality
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit.
1636 Mail Service Center
Raleigh, NC 27699-1636
1-919-807-6464
From: Karen Bellamy
Cascades Tissue Group — North Carolina
A Division of Cascades Holding US Inc.
805 Midway Road, P.O. Box 578, Rockingham, NC 28380 USA
Phone: [phone] Fax: [phone]
www.cascades.com * [e-mail]
Cascades Tissue Group -North Carolina, a division of Cascades Holding US Inc.
805 Midway Rd.
Rockingham, NC 28379
1-910-895-4033
Attention: NCDENR Division of Water Resources Water Quality Permitting Section Non. -Discharge Permitting
Unit.
Subject: Permit Renewal — Cascades Tissue Group — North Carolina, a division of Cascades Holding US Inc.
Dear
Cascades Tissue Group — North Carolina, a Division of Cascades Holding US Inc., (Cascades Tissue Group)
looks forward to continuing the successful Cascades Soil Amendment Program and will Submit ARM Check
for Payment of $1310 , forms and analyses to support the application for the renewal of Permit No.
WQ0009477 have been included.
Cascades Tissue Group has operated the Cascades Soil Amendment Program for greater than 20 years to the
benefit of local farmers, the environment and Cascades Tissue Group. Cascades Soil Amendment Program is
also registered with the North Carolina Department of Agriculture as a Soil Additive. Farmers have received
free Soil Amendment, free delivery and free spreading and saved $20 to $30 per acre by not having to purchase
agricultural lime. In times of very low farm grain and cotton prices, the free Cascades Soil Amendment may
have saved some farm operations.
The permit renewal allows Cascades Tissue Group and the North Carolina Department of Environment and
Natural Resources - Division of Water Resources (DWR) the opportunity to improve the Cascades Soil
Amendment Program. Based on greater than 20 years of experience, operations and characteristics, selected
conditions contained in the current permit are recommended for modification or removal. These conditions are
identified in the format of the current permit and are as follows:

1. We would like to request that we increase the material days in field be increase to one cropping cycle.
We are requesting this because of the increase in the amount of rain (due to climate Change) has made it
more difficult to meet the current permit time line. Also due to all the heavy rains that we have seen from
Hurricanes in the last few year and the water table being so high.
We want to thank you for your attention to the Cascades Soil Amendment Program and we would appreciate
reviewing and discussing the draft permit prior to final issuance.
Thank You
Jo ick: General Manager
Date: l�

Safety

Safety
Personnel associated with the Fiber -Clay Program will be informed of the need and monitored
to maintain a safe working environment. ARM, Health and Safety Director, Andrew Hendel, will
conduct safety discussions with operators and truckers. The Safety Director will update the
Regional Managers on new safety procedures by electronic notification and weekly managers
conference calls.

MAINTENANCE PLAN

Advanced Residuals Management LLC
1503 N Rocky River Road
Monroe, NC 28110
Phone: [phone] Fax: [phone]
Maintenance Plan
Advanced Residuals Management LLC is committed to maintaining all of
our equipment to the manufacturer's recommendations. All of our equipment is
regularly serviced and inspected for any problems or potential problems. This
process includes visual inspections of potential high wear areas and parts.
In addition, we check and calibrate our spreading equipment on a quarterly
basis. This is done by laying a tarp on the ground and making a pass by the tarp
while spreading. Then the material that lands on the tarp is weighed and a
calculation is used to determine if the spread rate is accurate for the residual
being applied. Please see the formula below.
Application Rate (tons/acre) = [Amount of Residuals Collected
(pounds) X 21.8] / Collection Area (square feet)

UTILIZATION AGREEMENT

Advanced Residuals Management, LLC
POB 1108, Fort Mill, SC 29716
Office: 803-639-7943, FAX:[phone], Cell: 910-712-0136
Utilization Agreement for the Land Application of FiberClay to Private Lands
I (Please print) do here by request Advanced
Residuals Management, LLC (ARM) to land apply FiberClay a registered soil additive
at agronomic rates to the below listed site(s) and field(s).
Field# GPS GPS Field size (ac)
I have received the FiberClay brochure and Information Sheet and I understand the
following:
1. By agreeing to accept the bulk Class A residuals, it is recognized that the
application of these residuals is allowed under the conditions of this agreement
including the prohibitions contained in condition 8. Land application of Class A
residuals is considered the beneficial reuse of a waste under 15A NCAC 02T.1100,
and has been deemed permitted under 15A NCAC 02T.1103(4) provided the
conditions of this agreement are met. Any action resulting in damages to surface
water or groundwater, caused by failure to follow the conditions of this agreement,
is subject to Division enforcement action;
2. Fields receiving the FiberClay and planted in corn, cotton and small grains will
require additional nitrogen in addition to the normal amounts,
3. Soil tests provide the best estimate of the FiberClay needed for the field,

4. The distribution/land application of the FiberClay shall be inaccordance with the
guidance on the FiberClay Information Sheet,
S. FiberClay shall be distributed/land applied within 60 calendar days of the date
that the last load was hauled to the farm field;
6. The application of FiberClay shall not occur within 100 ft of a public or private
water supply source and well and within 25 ft of surface waters;
7. Fields not covered in grass or a cover crop will be planted in corn, soybeans,
cotton or another crop:
8. FiberClay will not be applied to fields:
a. If the residuals are likely to adversely affect a threatened or endangered
species listed under section 4 of the Endangered Species Act or its
designated critical habitat,
b. If the application causes prolonged nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the
contravention of surface water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition
such that runoff of the residuals would occur;
e. Within the 100-year flood elevation if there is a hurricane watch, unless the
bulk residuals are injected or incorporated within a 24-hour period following a
residuals land application event;
f. During precipitation events, or within 24 hours following a rainfall event of
0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the
slope is greater then 18% for injected or incorporated bulk liquid residuals;
h. If the land does not have an established vegetative cover unless the residuals
are incorporated or injected within 24-hour period following a residuals land
application event. Any field that is in a USDA no -till program or common
corn -wheat -soybean rotation, cotton -soybean or corn rotation, and continuous
corn, soybean or cotton shall be exempted from meeting this vegetative cover
requirement;
i. If the vertical separation between the seasonal high water table and the depth
of residuals application is less than one foot;
j. If the vertical separation of bedrock and the depth of residuals application is
less than one foot;
k. If the application exceeds agronomic rates, e.g.' based on lime equivalency.
9. Farmers need to evaluate all lime, Ca and Mg materials, such as poultry litter, that
are added to the field to avoid excessive liming.

I am not aware of any threatened or endangered species listed under section 4 of
the Endangered Species Act or its designated critical habitat that would be adversely
affected.
This agreement is in affect until December 31, 2020. You have the right to end this
agreement at any time by notifying Cascades Tissue Group - North Carolina in
writing at the address listed below. Any changes in this agreement that are
necessitated by changes in the permit shall be mailed to you. If you sell the property
or if the permit is rescinded by NC Water Resources Environmental Quality, then
this agreement shall automatically terminate.
Address:
Town:
Phone #: Cell
e-mail address
Name: (please print)
NC Zip:
Date:
Signature Circle: Lessee, Land owner, sub -lessee or owner's representative
Cascades Rep. ARM Rep.

FiberClay Farmer Information/Data Sheet
1. Manufacturer: Cascades Tissue Group - North Carolina, 805 Midway Rd.,
Rockingham, NC 28379; Attn: Karen Bellamy @ 910-895-4033
2. Contractor: Advanced Residuals Management, LLC. -
POB 1108, Fort Mill, SC, 29716 ; @ 803-639-7943
3. Project Manager - Duke Goodwin @ 910-712-0136.
4. Source of FiberClay - Recycled office paper
5. FiberClay Sample Results - www.ncagr.goy/agronomi/. The report IDs are
the sample date.
6. The estimated tonnage for each field is based on an agronomic application
rate of 4 to 6 wet tons/ac which should furnish approximately one ton/ac
equivalent of lime. As an example, a 100 ac field would have 400 wet tons
spread to the field. This is approximately 20 truck loads.
7. The distribution/land application of the FiberClay shall be in accordance
with the FiberClay Information/Data Sheet.
8. Farmers are encouraged to obtain representative soil samples and analysis
to determine the lime requirement for their field.
9. The soil in the staging areas WILL BE IMPACTED and it is anticipated that
crop yields will be reduced in the staging areas. This affect can be reduced by
adding ammonia sulfate and Mn fertilizers in the appropriate amounts to the
staging area.
10. FiberClay is a calcitic type material. As such it does not contain important
amounts of magnesium. Farmers are encouraged to monitor the soil
magnesium levels with routine soil sampling and analysis and to make
necessary management decisions.
11. The FiberClay has a high carbon to nitrogen ratio due to the paper
component. Consequently, farmers need to apply an additional 15 to 25 #/ac
of nitrogen to corn, grass, cotton, small grain and other non-N fixing crops.
As an example, if you normally apply 140 #/ac of N to the conventional corn
field, you will need to add an additional 25 #/ac for a total of 165 #/ac.
12. For fields with a high lime recommendation, i.e. greater than 1.5 tons/ac, it is
recommended that the FiberClay be applied in split applications
approximately 6 months apart.
Signature Date

FIBER -CLAY SOIL ADDITIVE
Claim ... Fiber -Clay when thoroughly mixed into the soil
will result in increased biological population and root
development in acidic soils.
Directions for use ... Farmers should have soil test results
prior to the spreading of the Fiber -Clay. Delivery and
spreading will be provided by Advanced Residuals
Management (ARM). When applied to row crop fields, the
Fiber -Clay is to be incorporated into the soil by the farmer.
Hay and pasture fields that are to receive the Fiber -Clay are to
be cut or grazed prior to the spreading of the Fiber -Clay. Due
to the organic matter in the Fiber -Clay, farmers should apply
additional nitrogen either as manure or commercial fertilizer.
Production... The Fiber -Clay is produced by Cascades in
Rockingham, NC, as an industrial by-product from the
production of paper towels, facial tissue and toilet tissue that
are derived from recycled paper.
NetWeight ........................................... Bulk
Advanced Residuals Management
P.O. Box 1108
Fort Mill, SC 29716

SPILL CONTROL PLAN

r A ^ Advanced Residuals Management Ilc
P.O. Box 1108
aR Fort Mill, SC 29716
LLC �'
CASCADES TISSUE GROUP
SPILL CONTROL PLAN
IMPORTANT - This plan is to be placed in ALL residuals transport/spreading
vehicles - per NCDENR Permit No. WQ0009477
This spill control plan contains the procedures that are to be implemented in the
event of a road spill. The procedures are presented in steps numbered 1 through
15 and are presented in the order that they are to be implemented. The actual
steps and activities are printed in bold type print. In addition supplemental
information is provided for clarification of responsibilities and action items.
Step 1 - SET THE FOUR WAY EMERGENCY FLASHERS
Step 2 - DETERMINE IF THERE ARE ANY INJURIES, THE EXTENT OF
THE SPILL, AND THE CONDITION OF THE TRUCWEQUIPMENT
Step 3 - CALL FOR ASSISTANCE
If there is an injury, the driver is to call 911 immediately and report the accident.
As soon as possible the driver is to call Duke Goodwin, Project Manager at
[phone] to report the spill and request assistance. If the Project Manager
cannot be contacted, the driver is to call Bill Young, Director of Operations at
[phone]. If neither the Project manager nor the Director of Operations can
be contacted, the driver is to then call 911 for either the town, county, or state
highway patrol for traffic control assistance. If however the Project Manager,
Director of Operations, or 911 cannot be contacted, the driver is to proceed to
Step 4.
The Project Manager or Director of Operations will notify either the town, county,
or state highway patrol law enforcement and request assistance depending on
the spill circumstances. In addition the Project Manager or Director of Operations
will notify Karen Bellamy of the spill.
Step 4 - ALERT OTHER DRIVERS
Traffic warning signs are to be placed at distances of 20, 50, and 100 yards from
the spill area up and down the roadway. The traffic cones/triangles are to be
placed at the edge of the spilled fiber clay material.

Step 5 - SPILL CONTAINMENT
If the driver/operator is capable and resources are available, the driver/operator
as soon as possible is to contain the fiber clay material in the truck/equipment or
in the original spill area.
Step 6 - TRUCK REMOVAL FROM THE ROADWAY
If the truck can be safely removed from the roadway to a close safe flat area
without additional spillage or damage, then the driver/operator is to remove the
truck/equipment from the roadway.
Step 7 - TRAFFIC ASSISTANCE
From a safe position the driver/operator is to direct traffic away from the spilled
fiber clay material. If small piles that can be easily and safely removed from the
roadway are blocking traffic; stop traffic, remove the small piles and then
thoroughly brush the roadway surface.
Step 8 - INSPECT TRAFFIC SPILL WARNINGS
Check the status of the traffic warning signs. Reposition any highway traffic
warning cones/triangles that may have fallen over.
Step g - WAIT UNTIL THE FIELD SUPERINTENDENT/DIRECTOR OF
OPERATIONS ARRIVES ON SCENE
Step 10 - MANAGEMENT OF CLEAN UP
The Project Manager or Director of Operations will take charge of the cleanup
upon their arrival on scene. The Project Manager and/or Director of Operations
will mobilize the necessary staff and equipment to cleanup the spill. If the Project
Manager and/or Director of Operations has not done so already, it is at this time
he will notify Brandt Steele, general Manager of Advanced Residuals
Management.
Step 11 - PERSONNEL AND EQUIPMENT
The field crew and a frontend loader will mobilize to the spill. They will bring
shovels, rakes, and street brooms with them. Depending on the quantity of fiber
clay material spilled and the condition of the truck, an additional truck may also
be directed to the spill area. If need be, a tractor mounted with a broom
attachment, a backhoe with extended reach, and/or excavator with operators will
also be mobilized to the spill area to assist in the clean up.
Step 12 - CLEAN UP ACTIVITIES

The frontend loader will be used to remove as much as possible of the spilled
fiber clay material. The spilled fiber clay material will be loaded into a truck for
transport to a farm field or the local landfill. Next the tractor with the broom
attachment will sweep the remaining fiber clay material from the roadway and
adjacent spill areas. The sweepings will be collected into a pile and loaded with
the frontend loader into a truck for transport. If smaller particles remain on the
roadway surface after being swept, then clean dry sand will be spread onto the
roadway. The roadway will then be swept with the tractor mounted with the
broom attachment to remove the sand and the fiber clay material.
Step 13 - REPORTING
The Project Manager or Director of Operations will report the spill to the
NCDENR - Fayetteville Regional Office [phone] as soon as possible but
within 24 hours of the spill. They will notify NCDENR that a spill of fiber clay
material has occurred while in transit from the Cascade Tissue Group Facility to
the intended farm field.
Step 14 - SPILL DE -BRIEFING
Within 24 hours the Project Manager or Director of Operations will meet with
Karen Bellamy, Cascades Environmental Manager, and/or other designated mill
staff to discuss the spill. The discussions will pertain to the cause of the spill,
response actions taken by the truck driver and Project Manager and/or Director
of Operations, mobilization of the field crew and equipment, truckers and units,
police and state/local agencies or departments, clean up procedures
implemented, management of the cleanup, time to complete the cleanup, and
documentation of the clean up. In addition, a written report of the meeting will be
developed and delivered to Karen Bellamy within two days of the spill.
Step 15 - NCDENR WRITTEN REPORT
A written report will be delivered to NCDENR - Fayetteville Regional Office within
three days of the spill. The report will outline the actions taken or proposed to
limit future spills of the fiber clay material.

OPERATION PLAN

Advanced Residuals Management LLC
A P.O. Box 1108
Fort Mill, SC 29716-1108
Phone: [phone] Fax: [phone]
LLC '�
Operation Plan
Cascades Tissue Group operates an agricultural based by-product program for
the reuse of the short fibers and lime waste from the paper recycling program at
the Rockingham, NC mill. The program ORC is Karen Bellamy of Cascades
Tissue Group. The material called FiberClay is distributed to farms in southern
North Carolina. The by-product value of the FiberClay is the lime, calcium
carbonate. When applied to farm soils, the FiberClay will have a beneficial affect
similar to agricultural lime.
The FiberClay Program is permitted by the North Carolina Department of
Environment (DENR) as WQ Permit #0009477. The permit will be effective
January 1,2016 through December 31,2020. A permit renewal request will be
required six months prior to December 31,2020. It is the responsibility of
Cascades to renew the permit.
FiberClay is registered with the North Carolina Department of Agriculture as a
Soil Additive. Advanced Residuals Management (ARM) has held the registration
for 15 years. It is the responsibility of ARM to renew the Soil Additive registration
in June of each year.
For the past 15 years, ARM has provided environmental services for the
distribution and marketing of the FiberClay. ARM coordinates the farmer
marketing, agricultural monitoring, hauling and spreading. The program operates
in Union, Anson, Stanly, Montgomery, Richmond, Moore, Hoke, Scotland and
Robeson Counties. The program is staffed with field operators, truckers, a field
superintendent, a project manager, a soils consultant, and ARM managers.
Karen Bellamy has record collection and field review duties.
Farmers are selected for the FiberClay Program based on the need for lime. A
FiberClay brochure, Utilization Agreement and Soil Additive Information Sheet is
provided to all farmers interested in the FiberClay. Farmers are required to sign
and date the Utilization Agreement form prior to joining the FiberClay Program.
Farms are viewed by ARM or by an ARM subcontractor who notes the cropping
plan, location, surface water bodies, wells, FEMA 100 yr flood hazards, and
access roads. Staging areas are selected based on slope, wetness, and
distance from surface water, wells, and homes. The farm location information is

rA
transferred to Google Earth Pro to determine the approximate size of the field,
possible presence of surface water bodies and FEMA 100 year flood hazards.
Suitable farms are assigned a project number and the estimated loads are
calculated based on farm acreage, an equivalent one ton liming rate and the
estimated lime value of the FiberClay.
The ORC, backup ORC or certified laboratory technician obtains samples of the
FiberClay as required by the DENR permit. The samples are collected using
standard sampling techniques and procedures required for the selected
analyses. The samples are then delivered to a DENR certified laboratory for
analysis. If sample results are greater than permit conditions, the FiberClay is re -
sampled and the sample submitted to the certified laboratory for analysis. In
addition, the regional DENR office is notified of the sample results and the re -
sampling. If the re -sample results are greater than permit conditions, the
FiberClay is sampled again and the sample is split into three samples for
analysis at three different DENR certified laboratories. Again, the regional DENR
Office is notified of the results and the re -sampling for analysis.
Samples are also obtained as grab samples several times per week by ARM for
agricultural parameters. The samples are stored at ambient temperature and
delivered to the North Carolina Department of Agriculture — Agronomic Division
for waste analysis. The waste analysis results are used to determine the quantity
of FiberClay needed to supply an equivalent ton of agricultural lime. On the
NCDA Waste Report the lime equivalent is reported as the ALE. The waste
analysis report also contains C:N, Na and solids information which is important
for the successful use of the FiberClay.
The FiberClay is dewatered to approximately 45% solids and dropped onto a
concrete floor in a covered concrete walled storage bin at the mill. The FiberClay
remains in the bin until removed by ARM or subcontractor. Prior to removal from
the bin, the driver reviews the FiberClay for debris and determines the relative
solids content. If the FiberClay has any debris or has an abnormal solids
content, the driver notifies the field superintendent or project manager who
makes the necessary changes, if required.
ARM removes the FiberClay from the floor of the storage bin with a front-end
loader. The FiberClay is transferred to a tandem dump truck equipped with a
tarp to contain the FiberClay in the bed of the truck. Prior to leaving the loading
area, the driver inspects the loading area for spillage. Any spillage is removed
and placed back into the storage bin. The loaded truck then proceeds to the
scales to determine the loaded truck weight and the mass of FiberClay to be
delivered to the field.

III
Trucks travel routes to the farms that avoid areas prone to traffic congestion and
weight load limit bridges. In the unlikely event that an accident were to occur
while traveling to the farm, the driver is instructed to follow the spill prevention
plan. All transport vehicles contain a spill prevention plan.
Once at the farm the truck travels to the staging area and the FiberClay is
unloaded. The driver then pulls away from the pile of FiberClay and then
inspects the truck for spillage that has collected onto the truck. Any spillage is
removed from the truck and deposited into the pile.
The FiberClay is then loaded into a spreader for application to the field. The
spreader and travel speed is adjusted to spread the desired amount of FiberClay
to the field. Farmers are encouraged to have soil test results for fields. If soil
test results are available and the results indicate a need for 1 or more tons of
lime per acre, then FiberClay will be applied at the equivalent rate of 1 ton/ac. If
the lime requirement is greater than 1 ton/ac, FiberClay will be applied in one or
two additional spreads at 6 to 12 month intervals. Fields with liming
requirements of less than 1 ton/ac will be spread at the actual rate. For new
ground, the application is adjusted to 1.5 equivalent tons/ac because new ground
likely has a lime requirement of 2 to 4 tons/ac. For fields without soil test results,
only fields that have not been reported as having received lime in the past three
years will receive FiberClay. For these fields, FiberClay will be applied at the
equivalent rate of 1 ton/ac of lime.
Periodically the spreader will be calibrated in the field. Generally flat row crop
ground is selected for the calibration. A 10 ft x 10 ft tarp is placed on the ground
in the field receiving the FiberClay. Tent stakes are used to hold the tarp in
place. The FiberClay is spread onto the tarp as the spreader travels the field.
The FiberClay on the tarp is removed and placed into a 5 gal bucket. Then the
weight of the FiberClay in the bucket is determined with the aid of a bathroom
type scale. The weight in pounds is multiplied by 0.2178 to obtain units of wet
ton/ac.
Selected fields will be reviewed by the soils consultant related to agronomic
growth. In some conditions this will require discussions with the farmer. This
information will be provided to ARM.
Fields will be reviewed by the ORC, back-up ORC, ARM or the soils consultant
related to DENR permit conditions. This review will be conducted once per
month. Items reviewed will include buffers, condition of completed staging area,
spread patterns, crop, etc. If Cascades staff is not part of the review team,
information from the review will be provided to the Cascades ORC.

0
During the operation of the FiberClay Program, new techniques may become
available to Cascades or ARM that may offer improvement to the program. As
these new techniques become available, Cascades and ARM will evaluate the
merit of the new techniques and may evaluate those techniques that may benefit
the FiberClay Program. Prior to testing, Cascades will contact DENR.

aceAnalXical
www.pacelabs.com
January 23, 2020
Ms. Karen Bellamy
Cascades Tissue Group -NC
805 Midway Road
PO Box 578
Rockingham, NC 28380
RE: Project: Sludge
Pace Project No.: 92460661
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Dear Ms. Bellamy:
Enclosed are the analytical results for sample(s) received by the laboratory on January 14, 2020.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Accounts Payable, Cascades Tissue Group -NC
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 1 of 23

aceAnalytical
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Project: Sludge
Pace Project No.: 92460661
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

ljceAnalyfical'
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Project: Sludge
Pace Project No.: 92460661
Lab ID Sample ID
92460661001 Sludge Samples
92460661002 Sludge Samples
SAMPLE SUMMARY
Matrix
Date Collected
Date Received
Solid
01/09/20 08:10
01/14/20 10:08
Solid
01/14/20 08:05
01/14/20 10:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Page 3 of 23

ljceAnalytical'
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project:
Pace Project No.:
Sludge
92460661
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92460661001
Sludge Samples
EPA6010D
SH1
6
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA9045D
SMK
1
PASI-A
SM 271 OB-2011
DMN
1
PASI-A
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
KDF1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
92460661002
Sludge Samples
ASTM D2974-87
KDF
1
PASI-C
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalj cal
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ANALYTICAL RESULTS
Project: Sludge
Pace Project No.: 92460661
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: Sludge Samples Lab ID: 92460661001 Collected: 01/09/20 08:10 Received: 01/14/20 10:08 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050E
Arsenic
1.3J mg/kg 1.9
0.93
1
01/15/20 11:21
01/16/20 21:58
7440-38-2
Calcium
179000 mg/kg 372
186
20
01/15/20 11:21
01/17/20 21:55
7440-70-2
Copper
16.6 mg/kg 0.93
0.46
1
01/15/20 11:21
01/16/20 21:58
7440-50-8
Magnesium
1560 mg/kg 18.6
0.46
1
01/15/20 11:21
01/16/20 21:58
7439-95-4
Nickel
1.5 mg/kg 0.93
0.46
1
01/15/20 11:21
01/16/20 21:58
7440-02-0
Zinc
199 mg/kg 1.9
0.93
1
01/15/20 11:21
01/16/20 21:58
7440-66-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Total Solids
42.7 % 0.10
0.000010
1
01/14/20 16:24
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
57.3 % 0.10
0.10
1
01/14/20 16:14
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
7.0 Std. Units 0.10
0.10
1
01/20/20 14:38
H3
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
Plant Available Nitrogen
489 mg/kg 0.12
0.12
1
01/23/20 12:56
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
1630 mg/kg 40.0
20.0
1
01/20/2013:30
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia
ND mg/kg 2.3
2.3
1
01/21/20 10:38
01/21/20 14:19
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
1630 mg/kg 97.6
48.8
1
01/17/20 07:38
01/18/20 03:33
7727-37-9
REPORT OF LABORATORY ANALYSIS
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11ce Analytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Sludge
Pace Project No.: 92460661
Sample: Sludge Samples Lab ID: 92460661002 Collected: 01/14/20 08:05 Received: 01/14/20 10:08 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 57.6 % 0.10 0.10 1 01/14/20 16:39
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 01/23/2020 04:29 PM
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 9.1 4.5 1 01/14/20 22:46 01/15/20 00:17
ND mg/kg 9.1 4.5 1 01/14/20 22:46 01/15/20 00:17 14797-55-8
ND mg/kg 9.1 2.3 1 01/14/20 22:46 01/15/20 00:17 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 23

1�2ce Analytical
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QUALITY CONTROL DATA
Project: Sludge
Pace Project No.: 92460661
QC Batch: 519456 Analysis Method: EPA 601 OD
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Associated Lab Samples: 92460661001
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
METHOD BLANK: 2779945
Matrix:
Solid
Associated Lab Samples: 92460661001
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
0.50
01/16/20 21:19
Calcium
mg/kg
ND
10.0
5.0
01/16/20 21:19
Copper
mg/kg
ND
0.50
0.25
01/16/20 21:19
Magnesium
mg/kg
0.42J
10.0
0.25
01/16/20 21:19
Nickel
mg/kg
ND
0.50
0.25
01/16/20 21:19
Zinc
mg/kg
ND
1.0
0.50
01/16/20 21:19
LABORATORY CONTROL SAMPLE:
2779946
Parameter
Units
Arsenic
mg/kg
Calcium
mg/kg
Copper
mg/kg
Magnesium
mg/kg
Nickel
mg/kg
Zinc
mg/kg
Spike
LCS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
50
46.7
93
80-120
500
521
104
80-120
50
49.9
100
80-120
500
479
96
80-120
50
50.0
100
80-120
50
50.7
101
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2779947
2779948
MS
MSD
92460649001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
mg/kg
3.9
58
57.1
43.2
43.4
68
69
75-125
1
20 M1
Calcium
mg/kg
1260
580
571
1810
1880
95
108
75-125
4
20
Copper
mg/kg
43.6
58
57.1
102
99.6
101
98
75-125
2
20
Magnesium
mg/kg
2280
580
571
2880
2880
104
105
75-125
0
20
Nickel
mg/kg
11.8
58
57.1
61.8
61.3
86
87
75-125
1
20
Zinc
mg/kg
44.4
58
57.1
96.6
97.7
90
93
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 01/23/2020 04:29 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge
Pace Project No.: 92460661
QC Batch: 519340 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92460661001
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE DUPLICATE: 2779630
92460604001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 37.6 44.6 17 25
SAMPLE DUPLICATE: 2779631
92460661001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 57.3 57.4 0 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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11�;a'ceAnalyfical'
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QUALITY CONTROL DATA
Project: Sludge
Pace Project No.: 92460661
QC Batch: 519346 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92460661002
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
SAMPLE DUPLICATE: 2779645
92460661002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 57.6 57.6 0 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /23/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 23

11ceAnalXical'
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Project: Sludge
Pace Project No.: 92460661
QC Batch: 520147
QC Batch Method: EPA 9045D
Associated Lab Samples: 92460661001
SAMPLE DUPLICATE: 2783524
Parameter Units
pH at 25 Degrees C Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
92460408001 Dup
Result Result RPD
5.6 5.6
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Max
RPD Qualifiers
0 10 H3
SAMPLE DUPLICATE: 2783525
92460460001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 4.7 4.6 2 10 D6,H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /23/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23

0
11�;a'ce Analytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: Sludge
Pace Project No.: 92460661
QC Batch: 520287
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92460661001
METHOD BLANK: 2784091
Matrix: Solid
Associated Lab Samples: 92460661001
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed Qualifiers
Nitrogen, Ammonia mg/kg
ND 0.99
0.99 01/21/20 14:05
LABORATORY CONTROL SAMPLE: 2784092
Spike 1-CS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Nitrogen, Ammonia mg/kg
49.7 50.0 101
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2784093 2784094
MS MSD
92460129001
Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/kg 3800
58.8 58.8 6830 6360
3990 3180 90-110 7 10 M6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 11 of 23

aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge
Pace Project No.: 92460661
QC Batch: 519668 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Associated Lab Samples: 92460661001
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
METHOD BLANK: 2781024 Matrix: Solid
Associated Lab Samples: 92460661001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 25.0 01/18/20 03:18
LABORATORY CONTROL SAMPLE: 2781025
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg 1000 1040 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2781026 2781027
MS MSD
92459459001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 107 1960 2120 1620 1740 77 77 90-110 7 10 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /23/2020 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23

u
aceAnalytical
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QUALITY CONTROL DATA
Project: Sludge
Pace Project No.: 92460661
QC Batch: 519379 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92460661002
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
METHOD BLANK: 2779798
Matrix: Solid
Associated Lab Samples: 92460661002
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 4.0
2.0 01/15/20 00:15
Nitrogen, Nitrite
mg/kg
ND 4.0
1.0 01/15/20 00:15
Nitrogen, NO2 plus NO3
mg/kg
ND 4.0
2.0 01/15/20 00:15
LABORATORY CONTROL SAMPLE: 2779799
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 16.0 107 90-110
Nitrogen, Nitrite mg/kg 10 10.2 102 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 26.2 105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2779800
2779801
MS
MSD
92460661002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Nitrogen, Nitrate
mg/kg
ND
34.4
34.7
39.4
38.2
114
110
90-110
3 10 M1
Nitrogen, Nitrite
mg/kg
ND
23.1
23.1
24.4
23.8
106
103
90-110
3 10
Nitrogen, NO2 plus NO3
mg/kg
ND
57.6
57.8
63.8
62.0
110
106
90-110
3 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /23/2020 04:29 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 23

1�;a'ceAnalytical'
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Pace Analytical Services, LLC
6701 Conference Drive
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[phone]
QUALIFIERS
Project: Sludge
Pace Project No.: 92460661
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/23/2020 04:29 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 23

acmnalXical
www.pacelabs.com
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project:
Pace Project No.:
Sludge
92460661
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92460661001
Sludge Samples
EPA 3050B
519456
EPA6010D
519621
92460661001
Sludge Samples
SM 254OG-2011
519498
92460661001
Sludge Samples
ASTM D2974-87
519340
92460661002
Sludge Samples
ASTM D2974-87
519346
92460661001
Sludge Samples
EPA 9045D
520147
92460661001
Sludge Samples
SM 271 OB-2011
521025
92460661001
Sludge Samples
TKN+NO3+NO2
520292
Calculation
92460661001
Sludge Samples
EPA 350.1 Rev 2.0 1993
520287
EPA 350.1 Rev 2.0 1993
520485
Mod.
Mod.
92460661001
Sludge Samples
EPA 351.2 Rev 2.0 1993
519668
EPA 351.2 Rev 2.0 1993
520101
92460661002
Sludge Samples
EPA 353.2 Rev 2.0 1993
519379
EPA 353.2 Rev 2.0 1993
519390
Date: 01/23/2020 04:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 23

Document Name:
Document Revised: February 7, 2018
ZAnalyfital-Sample
Condition U on Recei t(SCUR)
Page 1 of 2
Document No,:
Issuing Authority:
(
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville� Raleigh❑ Mechanicsville❑
ConditionSample Client Name: WO# : 92460661
' �� ��SSt,� Project
Courier: ❑fe❑61
11111111d x ❑UPS ❑LISPS []ClientClientCommercial ace Other: 9Z
Custody Seal Present? ❑Yes No / Seals Intact? ❑Yes No
Date/Initials Person Examining Contents: �Y/-A)
Packing Material: ❑Bubble Wrap �,bbleags ❑None ❑ Other Biological Tiswe F;o en?
❑Yes ❑No /A
un ID: 92T058
Thermometer: Type of Ice: ❑Wet ❑Blue one
IR G
Cooler Temp (°C): -,2-0 - ( Correction Factor: Add/Subtract (•C) 0.0°C
Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): r.2c)
[]Samples out of temp criteria. Samples on ice, cooling process
hasbegun
USDA Regulated Soil (❑ N/A, water sample)
Did samples origipW in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Intern nally,
nYes f7ho Including Hawaii and Puerto Ricoh nYes tao
Comments/Discrepant .
Chain of Custody Present?
2fYe,
LINO
N/A
1.
Samples Arrived within Hold Time?
es
❑No
N/A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
o
N/A
3.
Rush Turn Around Time Requested?
Yes
o
❑N/A
4.
Sufficient Volume?
-. es
EINO
N/A
5.
Correct Containers Used?
-Pace Containers Used?
2<
514,
ONO
❑No
❑N/A
N/A
6.
Containers Intact?
es
ON.
N/A
7.
Dissolved analysis: Samples Field FiltereG?
Yes
2K'o
[]N/A
8.
Sample Labels Match CDC?
-Includes DateLLime/ID/Analysis Matrix:
.2"'
[]NO
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
Yes
No
/A
10.
Trip Blank Present?
Trip Blank Custod Seals Present?
[]Yes
Yes
[:]No
No
/A
/A
_
11.
COMMENTS/SAMPLE DISCREPANCY —. Field Data Required? [:]Yes ONO
/ GC►-e ,I S `ZO Sr�.gri1LC �I/ , 7�-.� /�i� 7/17 t.' S l- .1.2:14-ti .rr�%GC�
Lot 10 of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date: /
Page 16 of 23

Document Name:
Document Revised: February 7, 2018
=AnaWical '
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority'
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, LLHg
"*Bottom half of box is to list number of bottle
Project W0# d 92460661
PM: TIH Due Date: 01/28/20
CLIENT: 91-Cascades
2
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pH Adjustment og for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservailon adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot h
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 23

CHAIN -OF -CUSTODY / Analytical Request Document
911.1111sco. The Chain-of-Custodyis a LEGAL DOCUMENT. All relevant fields must be completed accurate) � m•.eetusco. � P y.
accu0n N Section a Section C
Required Client Information: Required Project Information: Invoice Information: Page ' 1 Of 1
Company: Cascades Tissue Group, Inc. Report To: Karen BellamyAttention
Address: 805 Midway Road Copy To: Company Name:
Rockingham. NC 28379
Address'.
Regulatory Agency
Email:
Purchase Order #:
Pace Quote:
Phone. [phone] Fax
Project Name: Sludge
Pace Project Manager: riek.hooks pacelabs.com,
State I Location
Requested Due Dale:
Project #:
Pace Profile #: 4729.1
NC
Requested
lysis
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COLLECTED
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SAMPLE ID SOhd
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SAMPLE CONDITIONS
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SAMPLER NAME AND SIGNATURE
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DATE Sig
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P7

Waypointo
ANALYTICAL
1 /22/2020
Pace Analytical Labs Charlotte
Tyriek Hooks
9800 Kindey Ave
Huntersville, NC, 28078
Ref: Analytical Testing
Report Number: 20-015-0002
Project Description: 92460661
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytica I.com
Dear Tyriek Hooks:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/15/2020 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
F_ to 6-7'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 19 of 23
Page 1 of 5

0
7621 Whitepine Road, Richmond, VA 23237
Waypoint. Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalocal.com
Sample Summary Table
Report Number: 20-015-0002
Client Project Description: 92460661
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
70166
92460661
Solids
70166
92460661
Solids
70166
92460661
Solids
70166
92460661
Solids
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
O1/09/2020 08:10 01/15/2020
01/09/2020 08:10 01/15/2020
O1/09/2020 08:10 01/15/2020
O1/09/2020 08:10 01/15/2020
SM-2540G WP MTN
SM-4500-NH3C-TKN WP MTN
AOAC 955.01 WP MTN
Page 2 of 5
Page 20 of 23

(2)WayPnt.
7621
-7 Road, Richmond,
Main 804-743-9401 0Fax
ain 80
27 -6446
804-271-6446
A ALYTICAL
www.waypointanalytical.com
11769
Pace Analytical Labs Charlotte
Tyriek Hooks
Project
92460661
Report Date : 01/22/2020
9800 Kindey Ave
Information :
Received : 01/15/2020
Huntersville , NC 28078
Pam« m� 6ewr
Pauric McGroary
Report Number: 20-015-0002
REPORT OFANALYSIS
Agronomist
Lab No : 70166
Matrix: Solids
Sample ID : 92460661
Sampled: 1/9/2020 8:10
Test
Results
Units
MQL
DF
Date / Time By Analytical
Analyzed Method
Moisture
56.5
%
0.010
1
01/16/20 16:20 ADM SM-2540G
Calcium Carbonate Equivalent
43.7
% - dry
0.1
1
01/22/20 08:57 DXT AOAC 955.01
C/N RATIO
5o
Ratio
0
1
01/16/20 16:20 CALCULATION
Test
Results
Units
MQL
DF
Date / Time By Analytical
Analyzed Method
Total Solids
43.5
%
0.010
1
01/16/20 16:20 ADM SM-2540G
Total Volatile Solids
50.8
%
0.010
1
01/16/20 16:20 ADM SM-2540G
Total Kjeldahl Nitrogen
5910
mg/Kg - dry
575
1
01/21/20 12:00 JPJ >M-4500-NH3C-TKP
Carbon (TOC)
29.5
%
0.010
1
01/16/20 16:20 CALCULATION
Qualifiers/ DF Dilution Factor L Limit Exceeded
Definitions MQL Method Quantitation Limit
Page 21 of 23
Page 3 of 5

Waypoint.(D
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 11769
Customer Name: Pace Analytical Labs Charlotte
Report Number: 20-015-0002
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
F
I
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
0 Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
High concentration container (48 hr) Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments:
0Yes I* No
Signature: lBrandi Watson I Date & Time: 1/15/2020 12:49:30
Page 4 of 5
Page 22 of 23

Chain of Custody
PAST Charlotte Laboratory
Workorder: 92460661
Workorder Name: Sludge
IhlllIIIIIIIII111hIIIIININIIII111111IF1�11111111111 °5-�2
Pace Anal"nual Labs Cha,11,11, 12 48 33
92460661
aceAnalytical
www, paceiabs.com
ested By: 1/28/2020
Report / Invoice To .
Subcontract To
Reqnested Analysis
Tyriek Hooks
Pace Analytical Charlotte
rU 11� ArO�V, l a, P.O.
9800 Kincey Ave Suite 100
J
Huntersville, NC 28078
Phone[phone]
"gyp
Email: [e-mail]
r17
State of Sample Origin: NC
SC
Preserved Containers
Collect
Item
Sample ID =
DateTme
Lab ID
Matrix
LAB USE ONLY
1
Sludge Sarrp�e-�
1/9:2020 08 10
92460661001
Solid
X
2
3
4
5
Comments
Transfers
Released By
Date/Time
Received By
Dateffirne
, :C-f.f tt/({ 5Cu351 %i>l S}vi C. / T%tivj
itI TUS� G/V '�501 LrI(/C/1
1
2
Croo
3
Cooler Temperature on Receipt
°C
Custod Seal Y or N
Received on Ice Y or N
Samples Intact Y or N
Tuesday. Janu:3ry 14, 2020 4 21 A0 PM
w
FMT-ALL-C-002rev.00 241Vlarch2009 Pag6 23-ofl23 1
Page 5 of 5

Chemical Analysis

SUMM111
Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, sNr Cuyahoga Falls, Ohio 44223
AnalyMcal Laboratories TEL: [phone] FAX: [phone]
Website: htty://www.settek.com
February 21, 2020
Karen Bellamy
Cascades Tissue Group - North Carolina Inc
805 Midway Road
Rockingham, NC 28379
TEL: [phone]
FAX: [phone]
RE: Waste Characterization
Dear Karen Bellamy: Order No.: 20020508
Summit Environmental Technologies, Inc. received I sample(s) on 2/8/2020 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Holly Florea
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0I08, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP
CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 010, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah
OH00923201 I - 1, Virginia VELAP 9456, Washington C891
Page 1 of 36

U MM I Summit Environmental Technologies, Inc. N
3310Win St. CaseaI'Pai1Ve
ENVIRONMENTAL TECHNOLOGIES. INC Cuyahoga Falls, Ohio 44223 wok 20020508
Anatyr�caf Laboraror)es TEL: [phone] FAX: [phone]
Website: htto://www.settek.com Date: 2/21/2020
CLIENT: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization
WorkOrder Narrative:
This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical
Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler
Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
20020508-OOIA TCLP-SVOC_8270E: Possible low bias for Hexachloroethane due to low recovery in
LCS-42030.
Original
Page 2 of 36

MM' NI Summit Environmental Technologies, Inc. W O rk0 rd e r
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Sample Summary
AnalyNcal taboratones TEL: [phone] FAX.- [phone] WO#: 20020508
Website: httn://www.settek.com 21-Feb-20
CLIENT': Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
20020508-001 Sludge 2n12020 8:00:00 AM 2/8/2020 8:21:00 AM Sludge
Page 3 of 36

r
Summ,,,
Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECIMOLt1G1FS, INC. Cuyahoga Falls, Ohio 44223
Ai71NVr%coi Laboratories TEL: [phone] FAX: [phone]
Website: http://www.settek.com
WO#:
20020508
Date Reported:
2/21/2020
Company:
Cascades Tissue Group - North Carolina I
Address:
805 Midway Road
Rockingham NC 28379
Received:
2/8/2020
Project#:
Waste Characteri
TCLP Metals Analysis (SW1311/6010)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge
001
2/7/2020
TCLP Arsenic(As)
0.500
ND mg/L
Sludge
EPA 6010
1
5.00
2/13/2020
EAM
D
Sludge
001
2/7/2020
TCLP Barium(Ba)
5.00
ND mg/L
Sludge
EPA 6010
1
100
2/13/2020
EAM
D
Sludge
001
2/7/2020
TCLP Cadmium(Cd)
0.100
ND mg/L
Sludge
EPA 6010
1
1.00
2/13/2020
EAM
D
Sludge
001
2/7/2020
TCLP Chromium(Cr)
0.200
ND mg/L
Sludge
EPA 6010
1
5.00
2/13/2020
EAM
D
Sludge
001
2/7/2020
TCLP Lead(Pb)
0.500
ND mg/L
Sludge
EPA 6010
1
5.00
2/13/2020
EAM
D
Sludge
001
2/7/2020
TCLP Selenium(Se)
0.0500
ND mg/L
Sludge
EPA 6010
1
1.00
2/13/2020
EAM
D
Sludge
001
2/7/2020
TCLP Silver(Ag)
0.500
ND mg/L
Sludge
EPA 6010
1
5.00
2/13/2020
EAM
D
TCLP Mercury Analysis (SW1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Sludge 001 2/7/2020 TCLP Mercury 0.00200 ND mg/L Sludge EPA 7470 A 1 0.200 2/17/2020 MJM
TCLP Pesticides Analysis (SW1311/8081)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Sludge
001
2/7/2020
Chlordane, total
0.125
ND mg/L
Sludge
EPA 8081E
5
0.0300
2/15/2020
SEK
Sludge
001
2/7/2020
Toxaphene
0.250
ND mg/L
Sludge
EPA 8081 B
5
0.500
2/15/2020
SEK
Sludge
001
2/7/2020
Endrin
0.0125
ND mg/L
Sludge
EPA 8081B
5
0.0200
2/15/2020
SEK
Sludge
001
2/7/2020
gamma-BHC
0.0125
ND mg/L
Sludge
EPA 8081E
5
0.400
2/15/2020
SEK
Sludge
001
2/7/2020
Heptachlor
0.0125
ND mg/L
Sludge
EPA 8081 B
5
0.00800
2/15/2020
SEK
Sludge
001
2/7/2020
Heptachlor epoxide
0.0125
ND mg/L
Sludge
EPA 8081 B
5
0.00800
2/15/2020
SEK
Sludge
001
2/7/2020
Methoxychlor
0.0125
ND mg/L
Sludge
EPA 8081B
5
10.0
2/15/2020
SEK
Sludge
001
2/7/2020
Surr: TCMX
10-119
55.1 %Rec
Sludge
EPA 8081E
5
2/15/2020
SEK
Sludge
001
2/7/2020
Surr: DCB
10-119
84.8 %Rec
Sludge
EPA 8081 B
5
2/15/2020
SEK
Page 4 of 36

Summit Environmental Technologies, Inc. WO#: 20020508
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported: 2/21/2020
TEL: [phone] FAX.- [phone] Company: Cascades Tissue Group - North Carolina 1
Website: http://Www.settek.com Address: 805 Midway Road
Rockingham NC 28379
Received: 2/8/2020
Project#: Waste Characteri
TCLP Volatiles Analysis
Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst
Sludge
001
2/7/2020
1,1-Dichloroethene
0.100
ND mg/L
Sludge
EPA 8260D
100
0.700
2/13/2020
MES
Sludge
001
2/7/2020
1,2-Dichloroethane
0.100
ND mg/L
Sludge
EPA 8260D
100
0.500
2/13/2020
MES
Sludge
001
2/7/2020
MEK
2.00
ND mg/L
Sludge
EPA 8260D
100
200
2/13/2020
MES
Sludge
001
2/7/2020
Benzene
0.100
ND mg/L
Sludge
EPA 8260D
100
0.500
2/13/2020
MES
Sludge
001
2/7/2020
Carbon tetrachloride
0.100
ND mg/L
Sludge
EPA 8260D
100
0.500
2/13/2020
MES
Sludge
001
2/7/2020
Chlorobenzene
1.00
ND mg/L
Sludge
EPA 8260D
100
100
2/13/2020
MES
Sludge
001
2/7/2020
Chloroform
0.100
ND mg/L
Sludge
EPA 8260D
100
6.00
2/13/2020
MES
Sludge
001
2/7/2020
Tetrachloroethene
0.100
ND mg/L
Sludge
EPA 8260D
100
0.700
2/13/2020
MES
Sludge
001
2/7/2020
Trichloroethene
0.100
ND mg/L
Sludge
EPA 8260D
100
0.500
2/13/2020
MES
Sludge
001
2/7/2020
Vinyl chloride
0.0500
ND mg/L
Sludge
EPA 8260D
100
0.200
2/13/2020
MES
Sludge
001
2/7/2020
Surr: 4-
70-130
93.7 %Rec
Sludge
EPA 8260D
100
2/13/2020
MES
Bromofluorobenzene
Sludge
001
2/7/2020
Surr:
70-130
98.8 %Rec
Sludge
EPA 8260D
100
2/13/2020
MES
Dibromofluorom ethane
Sludge
001
2/7/2020
Surr: Toluene-d8
70-130
98.8 %Rec
Sludge
EPA 8260D
100
2/13/2020
MES
TCLP Semi-Volatiles Analysis (SW1311/8270)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge
001
2/7/2020
1,4-Dichlorobenzene
0.200
ND mg/L
Sludge
EPA 8270E
2
7.50
2/14/2020
SFG
Sludge
001
2/7/2020
2,4,5-Trichlorophenol
0.500
ND mg/L
Sludge
EPA 8270E
2
400
2/14/2020
SFG
Sludge
001
2/7/2020
2,4,6-Trichlorophenol
0.500
ND mg/L
Sludge
EPA 8270E
2
2.00
2/14/2020
SFG
Sludge
001
2/7/2020
2,4-Dinitrotoluene
0.100
ND mg/L
Sludge
EPA 8270E
2
0.130
2/14/2020
SFG
Sludge
001
2/7/2020
Cresols, Total
10.0
ND mg/L
Sludge
EPA 8270E
2
200
2/14/2020
SFG
Sludge
001
2/7/2020
Hexachloro-1,3-
0.0400
ND mg/L
Sludge
EPA 8270E
2
0.500
2/14/2020
SFG
butadiene
Sludge
001
2/7/2020
Hexachlorobenzene
0.100
ND mg/L
Sludge
EPA 8270E
2
0.130
2/14/2020
SFG
Sludge
001
2/7/2020
Hexachloroethane
0.200
ND mg/L
Sludge
EPA 8270E
2
3.00
2/14/2020
SFG
Sludge
001
2/7/2020
Nitrobenzene
0.200
ND mg/L
Sludge
EPA 8270E
2
2.00
2/14/2020
SFG
Sludge
001
2/7/2020
Pentachlorophenol
0.500
ND mg/L
Sludge
EPA 8270E
2
100
2/14/2020
SFG
Sludge
001
2/7/2020
Pyridine
0.500
ND mg/L
Sludge
EPA 8270E
2
5.00
2/14/2020
SFG
Sludge
001
2/7/2020
Surr: 2-Fluorophenol
10-109
70.5 %Rec
Sludge
EPA 8270E
2
2/14/2020
SFG
Sludge
001
2/7/2020
Surr: Phenol-d6
10-109
75.6 %Rec
Sludge
EPA 8270E
2
2/14/2020
SFG
Sludge
001
2/7/2020
Surr: Nitrobenzene-
19-120
72.2 %Rec
Sludge
EPA 8270E
2
2/14/2020
SFG
d5
Sludge
001
2/7/2020
Surr: 2,4,6-
10-120
93.5 %Rec
Sludge
EPA 8270E
2
2/14/2020
SFG
Tribromophenol
Sludge
001
2/7/2020
Surr: 2-
22-117
67.2 %Rec
Sludge
EPA 8270E
2
2/14/2020
SFG
Fluorobiphenyl
Sludge
001
2/7/2020
Surr: p-Terphenyl-
34-116
91.1 %Rec
Sludge
EPA 8270E
2
2/14/2020
SFG
d14
Page 5 of 36

su
Summit Environmental Technologies, Inc.
WO#:
20020508
mm' ll
ENVIRONMENTAL TECHNOLOGIES, !NC,
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported:
2/21/2020
Analytical Laboratories TEL: [phone] FAX.- [phone]
Company:
Cascades Tissue Group - North Carolina I
Website: http://www.settek.com
Address:
805 Midway Road
Rockingham NC 28379
Received:
2/8/2020
Project#:
Waste Characteri
TCLP Herbicides by EPA 8321B
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method DF RegLvl Run Analyst
Sludge
001
2/7/2020
2,4-13
0.500
0.600 mg/L
Sludge
EPA 8321B
50
10.0 2/13/2020
BJH
Sludge
001
2/7/2020
2,4,5-TP
0.500
ND mg/L
Sludge
EPA 8321B
50
1.00 2/13/2020
BJH
Sludge
001
2/7/2020
Surr: DCAA
70-130
98.7 %Rec
Sludge
EPA 8321E
50
2/13/2020
BJH
Page 6 of 36

Summit Environmental Technologies, Inc.
3310 Win St.
SUMMIT
Analytical Report
ENVIRONMENTAL TECHNOLOGIFi, iNC
Cuyahoga Falls, Ohio 44223
(consolidated)
A%VyNcal Laborafoncs TEL: [phone] FAX: [phone]
WO#: 20020508
Wehsite: ham://www.settek.com
Date Reported: 2/21/2020
CLIENT: Cascades Tissue Group - North Carolina Inc Collection Date:
2/7/2020 8:00:00 AM
Project: Waste Characterization
Lab ID: 20020508-001
Matrix:
SLUDGE
Client Sample ID: Sludge
Analyses Result
PQL Qua[ Units
DF Date Analyzed
RCI-SOLID-W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.446 mg/Kg
1 2/19/2020 10:33:00 AM
RCI-SOLID-W/ IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
mm/sec
1 2/10/2020 1:00:00 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9045D
Analyst: VVK
PH (SW9045D)
pH 7.3
s.u.@20.00
1 2/10/2020 4:22:07 PM
RCI-SOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1 2/19/2020 10:33:00 AM
Qualifiers: H Holding times for preparation or analysis exceeded
ND Not Detected
R RPD outside accepted recovery limits
W Sample container temperature is out of lint as specified at testcode
M Manual Integration used to determine area response
PL Permit Limit
RL Reporting Detection Lint
Original
Page 7 of 36

SUMMIT Summit Environmental Technologies, St. QC SUMMARY REPORT
3310 10 Win St.
ENVIRONMENTAL TECHNOLOGIES, :Nf Cuyahoga Falls, Ohio 44223
Arraly rical Laboratones TEL: [phone] FAX: [phone] WO#: 20020508
Wehsite: http://www.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization Batchll): 41983
Sample ID: MB-41983
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 2/11/2020
RunNo: 109311
client ID: PBS
Batch ID: 41983
TestNo: SW8260 SW1311M
Analysis Date: 2/12/2020
SegNo: 2626133
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
i,i-uicmoroetnene
ND
0.0500
1,2-Dichloroethane
ND
0.0500
MEK
ND
1.00
Benzene
ND
0.0500
Carbon tetrachloride
ND
0.0500
Chlorobenzene
ND
0.500
Chloroform
ND
0.0500
Tetrachloroethene
ND
0.0500
Trichloroethene
ND
0.0500
Vinyl chloride
ND
0.0200
Surr: 4-Bromofluorobenzene
459
Surr: Dibromofluoromethane
500
Surr: Toluene-d8
497
500.0 91.8 70 130
500.0 100 70 130
500.0 99.3 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 8 of 36

SUMMIN
3310 WiSummit EnvironmentalTechno,10Win St. Inc.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGIE , . '
Cuyahoga Falls, Ohio 44223
Ar7atyfical Caboratorios
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
BatchID: 42013
Sample ID: MB-42013
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/13/2020
RunNo: 109289
client ID: PBS
Batch ID: 42013
TestNo: SW6010D SW3010A
Analysis Date: 2/13/2020
SegNo: 2626427
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowt-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1 �-Lr Mrsemc(tis)
NU
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-42013
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/13/2020
RunNo: 109289
:lient ID: LCSS
Batch ID: 42013
TestNo: SW6010D SW3010A
Analysis Date: 2/13/2020
SegNo: 2626428
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
i Ucr mrsenic(t+s)
2.11
0.500
2.000
0
105
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
111
80
120
TCLP Cadmium(Cd)
1.96
0.100
2.000
0
98.2
80
120
TCLP Chromium(Cr)
2.06
0.200
2.000
0
103
80
120
TCLP Lead(Pb)
2.14
0.500
2.000
0
107
80
120
TCLP Selenium(Se)
2.05
0.0500
2.000
0
103
80
120
TCLP Silver(Ag)
2.25
0.500
2.000
0
113
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 9 of 36

SIUMM11T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENV1nONMENTAL T[CHNOLOCIFS `
Cuyahoga Falls, Ohio 44223
Ansryrieaf Laboratories
TEL: [phone] FAX. [phone]
WO#: 20020508
Website: htto://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Waste Characterization
BatchID: 42013
Sample ID: TCLP BLANK 2/12/2
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/13/2020
RunNo: 109289
:lient ID: PBS
Batch ID: 42013
TestNo: SW6010D SW3010A
Analysis Date: 2/13/2020
SegNo: 2626429
>nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1 ULP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
iample ID: 20020509-001AMS
SampType: MS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/13/2020
RunNo: 109289
;lient ID: BatchQC
Batch ID: 42013
TestNo: SW6010D SW3010A
Analysis Date: 2/13/2020
SegNo: 2626438
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
I ULF ArsenlC(AS)
2.16
0.500
2.000
0
108
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.2736
81.2
70
130
TCLP Cadmium(Cd)
1.75
0.100
2.000
0.002100
87.5
70
130
TCLP Chromium(Cr)
1.84
0.200
2.000
0.008900
91.8
70
130
TCLP Lead(Pb)
1.80
0.500
2.000
0.009000
89.8
70
130
TCLP Selenium(Se)
2.11
0.0500
2.000
0
105
70
130
TCLP Silver(Ag)
1.98
0.500
2.000
0.007300
98.7
70
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 10 of 36

SUMM'11-
Summit Environmental Technologies, Inc..Ooq
33/0 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGIF, S
Cuyahoga Falls, Ohio 44223
a,_
Analyrical Laboratoripc
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Waste Characterization
BatchID: 42013
Sample ID: 20020509-001AMSD
SampType: MSD
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 2/13/2020
RunNo: 109289
Client ID: Batch=
Batch ID: 42013
TestNo: SW6010D SW3010A
Analysis Date: 2/13/2020
SegNo: 2626439
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.14
0.500
2.000
0
107
70
130
2.156
0.698 20
TCLP Barium(Ba)
ND
5.00
2.000
0.2736
80.5
70
130
0
0 20
TCLP Cadmium(Cd)
1.76
0.100
2.000
0.002100
87.6
70
130
1.753
0.114 20
TCLP Chromium(Cr)
1.84
0.200
2.000
0.008900
91.4
70
130
1.844
0.435 20
TCLP Lead(Pb)
1.80
0.500
2.000
0.009000
89.6
70
130
1.805
0.166 20
TCLP Selenium(Se)
2.09
0.0500
2.000
0
105
70
130
2.108
0.762 20
TCLP Silver(Ag)
1.96
0.500
2.000
0.007300
97.7
70
130
1.982
1.07 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analN
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 11 of 36

S u mow 111
Summit Environmental Technologies, St.
3310 /0 Win Sr.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGiFS. 'Nr
Analytical Laboratornei:
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
Batch[D: 42030
Sample ID: MB-42030
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 2/13/2020
RunNo: 109407
Client ID: PBS
Batch ID: 42030
TestNo: SW8270 SW3510C
Analysis Date: 2/14/2020
SegNo: 2629241
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Uichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0,630
Surr: Phenol-d6
0.674
Surr: Nitrobenzene-d5
0.696
Surr: 2,4,6-Tribromophenol
0.863
Surr: 2-Fluorobiphenyl
0.683
Surr: p-Terphenyl-d14
0.992
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
1.000
63.0
10
109
1.000
67.4
10
109
1.000
69.6
19
120
1.000
86.3
10
120
1.000
68.3
22
117
1.000
99.2
34
116
E Value above quantitation range H Holding times for preparation or anah
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 12 of 36

SUMM111-
Summit Environmental Technologies, Inc.
3310 Win St
DO7� T
Q!'� SUMMARY
Tlf, /ilf, /f A l� �7 REPORT
C S V 1�' MAR 1 RE R 1
ENVIR©NMEN7AL TECHNOLOG -
Cuyahoga Falls, Ohio 44223
Ana?Ytical (abnrator/eg
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: htto://wwm,.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
BatchID: 42030
Sample ID: LCS-42030
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 2/13/2020
RunNo: 109407
Client ID: LCSS
Batch ID: 42030
TestNo: SW8270 SW3510C
Analysis Date: 2/14/2020
SegNo: 2629242
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.345
0.100
0.8000
0
43.1
36.4
130
2,4,5-Trichlorophenol
0.819
0.250
0.8000
0
102
31.7
132
2,4,6-Trich lorophenol
0.811
0.250
0.8000
0
101
31.1
133
2,4-Dinitrotoluene
0.843
0.0500
0.8000
0
105
43.3
130
o-Cresol
0.579
0.250
0.8000
0
72.4
32.9
130
Cresols, Total
ND
5.00
1.600
0
76.1
31.7
130
Hexachloro-1,3-butadiene
0.374
0.0200
0.8000
0
46.8
31.4
130
Hexachlorobenzene
0.644
0.0500
0.8000
0
80.6
43.1
130
Hexachloroethane
0.279
0.100
0.8000
0
34.9
36.5
130
Nitrobenzene
0.528
0.100
0.8000
0
66.0
39.5
130
Pentachlorophenol
0.675
0.250
0.8000
0
84A
34
130
Pyridine
0.503
0.250
0.8000
0
62.8
10
130
Surr: 2-Fluorophenol
0.659
1.000
65.9
17.1
130
Surr: Phenol-d6
0.709
1.000
70.9
10
130
Surr: Nitrobenzene-d5
0.698
1.000
69.8
32.6
130
Surr: 2,4,6-Tribromophenol
0.981
1.000
98.1
4.43
130
Surr: 2-Fluorobiphenyl
0.731
1.000
73.1
41.8
130
Surr: p-Terphenyl-d14
0.950
1.000
95.0
36.4
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
S
Original
Page 13 of 36

summur
Summit Environmental Technologies, St.
3310 /0 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGIES, `NC
Analytical Laboratories
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://Www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Waste Characterization
BatchlD: 42030
Sample ID: 20020505-001AMS
SampType: MS
TestCode: SVOC-BNA T Units: mg/L
Prep Date: 2/13/2020
RunNo: 109407
Client ID: Batch=
Batch ID: 42030
TestNo: SW8270 SW3510C
Analysis Date: 2/14/2020
SegNo: 2629245
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.536
0.200
0.8000
0
67.0
33.8
126
2,4,5-Trichlorophenol
1.03
0.500
0.8000
0
129
28.7
144
2,4,6-Trichlorophenol
0.988
0.500
0.8000
0
124
12.8
153
2,4-Dinitrotoluene
1.04
0.100
0.8000
0
129
20.4
155
o-Cresol
0.825
0.500
0.8000
0
103
10
148
Cresols, Total
ND
10.0
1.600
0
106
10
148
Hexachloro-1,3-butadiene
0.472
0.0400
0.8000
0
59.0
29
126
Hexachloro benzene
0.774
0.100
0.8000
0
96.8
33.7
134
Hexachloroethane
0.418
0.200
0.8000
0
52.3
32.8
132
Nitrobenzene
0.740
0.200
0.8000
0
92.5
20
158
Pentachlorophenol
0.705
0.500
0.8000
0
88.1
10
176
Pyridine
0.672
0.500
0.8000
0
84.0
10
130
Surr:2-Fluorophenol
0.958
1.000
95.8
3.39
130
Surr: Phenol-d6
0.991
1.000
99.1
5
130
Surr: Nitrobenzene-d5
0.972
1.000
97.2
14.5
154
Surr: 2,4,6-Tribromophenol
1.16
1.000
116
19.5
130
Surr:2-Fluorobiphenyl
0.894
1.000
89.4
34.4
130
Surr: p-Terphenyl-dl4
1.11
1.000
ill
8.86
156
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantization limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anaIN
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 14 of 36

summill Summit Environmental Technologies, Inc. 3310 Win St. QC SUMMARY REPORT
1
ENVIRONMENTAL rECHN0LC ; Cuyahoga Falls, Ohio 44223
Anzt ticat Laboratories WO#: 20020508
} TEL: [phone] FAX.• [phone]
Website: http://www.settek.c2m 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization BatchID: 42030
Sample ID: 20020505-001AMSD
SampType: MSD
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 2/13/2020
RunNo: 109407
client ID: BatchQC
Batch ID: 42030
TestNo: SW8270 SW3510C
Analysis Date: 2/14/2020
SegNo: 2629246
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qua[
1,4-Dichlorobenzene
0.322
0.200
0.8000
0
40.3
33.8
126
0.5360
49.8
30 R
2,4,5-Trich lorophenol
0.859
0.500
0.8000
0
107
28.7
144
1.030
18.0
30
2,4,6-Trichlorophenol
0.859
0.500
0.8000
0
107
12.8
153
0.9884
14.0
30
2,4-Dinitrotoluene
0.852
0.100
0.8000
0
106
20.4
155
1.036
19.5
30
o-Cresol
0.596
0.500
0.8000
0
74.6
10
148
0.8252
32.2
30 R
Cresols, Total
ND
10.0
1.600
0
79.4
10
148
0
0
30
Hexachloro-1,3-butadiene
0.336
0.0400
0.8000
0
42.1
29
126
0.4716
33.5
30 R
Hexachlorobenzene
0.652
0.100
0.8000
0
81.6
33.7
134
0.7744
17.1
30
Hexachloroethane
0.280
0.200
0.8000
0
35.0
32.8
132
0.4184
39.5
30 R
Nitrobenzene
0.563
0.200
0.8000
0
70.4
20
158
0.7396
27.1
30
Pentachlorophenol
0.616
0.500
0.8000
0
77.0
10
176
0.7048
13.5
30
Pyridine
ND
0.500
0.8000
0
51.3
10
130
0.6720
200
30 R
Surr:2-Fluorophenol
0.630
1.000
63.0
3.39
130
0
Surr: Phenol-d6
0.730
1.000
73.0
10
130
0
Surr: Nitrobenzene-d5
0.754
1.000
75.4
14.5
154
0
Surr: 2,4,6-Tribromophenol
0.975
1.000
97.5
19.5
130
0
Surr: 2-Fluorobiphenyl
0.751
1.000
75.1
34.4
130
0
Surr: p-Terphenyl-d14
0.909
1.000
90.9
8.86
156
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 15 of 36

summill
3310 Win StSummit Environmental Technologies, St. .
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOG - , . '
Cuyahoga Falls, Ohio 44223
Anatyricat Laboratories
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
Batchll): 42055
Sample ID: MB-42055
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: PBS
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2630910
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
CLP Mercury ND 0.00200
Sample ID: LCS-42055
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: LCSS
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2630911
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
CLP Mercury 0.00390 0.00200 0.00400 0 97.5 80 120
Sample ID: TCLP BLANK 2-13-2
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: PBS
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2631230
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
CLP Mercury ND 0.00200
Sample ID: 20020549-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: BatchQC
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2631241
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00450 0.00200
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
0.00400 0 112 75
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
125
H Holding times for preparation or anal}
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 16 of 36

SUMM111
Summit Environmental Technologies, St.
3310 /0 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGIES
Cuyahoga Falls, Ohio 44223
Ar+alyneat Laboraro, �c
TEL: [phone] FAX.- [phone]
WO#: 20020508
Website: htto://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
Batchll): 42055
;ample ID: 20020549-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 211712020
RunNo: 109429
:lient ID: BatchQC
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2631241
malyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 20020549-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: BatchQC
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2631242
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
ULr mercury 0.00421 0.00200 0.00400 0 105 75 125 0.00450 6.66 20
Sample ID: MB2-42055
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: PBS
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2631244
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
ULF Mercury ND 0.00200
Sample ID: TCLP BLANK 2-14-2
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: PBS
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2631250
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
t,Lr- mercury NU 0.00200
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anaIN
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 17 of 36

SUMMIT Summit Environmental TechnolWSt. QC SUMMARY REPORT
331010 Win St.
ENVIRONMENTAL TECHNOLOGIFS, NC: Cuyahoga Falls, Ohio 44223
Anal yricai Laborajcrlpf WO#: 20020508
1 TEL: [phone] FAX.- [phone]
Website: httn://www.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization BatchlD• 42055
Sample ID: M63-42055
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 2/17/2020
RunNo: 109429
Client ID: PBS
Batch ID: 42055
TestNo: SW7470A SW7470A
Analysis Date: 2/17/2020
SegNo: 2631265
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
t,Lr mercury
ND 0.00200
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal}
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 18 of 36

summiat
Summit Environmental TechnolWSt. QC SUMMARY REPORT
331010 Win St.
ENVIRONMENTAL TECHNOt OGIES, iNC Cuyahoga Falls, Ohio 44223
Anal c I Laboraronas TEL: [phone] FAX. [phone] WO#: 20020.508
yr, .a
Website: htto://www.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization BatchID: R109137
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@20.4C
Prep Date:
RunNo: 109137
client ID: LCSS
Batch ID: R109137
TestNo: SW9045D
Analysis Date: 2/10/2020
SegNo: 2616622
4nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Hight-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 90 110
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
Page 19 of 36
H Holding times for preparation or anal}
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original

summior Summit Environmental TechnolWSt. QC SUMMARY REPORT
331010 Win St.
ENVIRONMENTAL tE-CHNOL0G7FS, ,NC Cuyahoga Falls, Ohio 44223 WO#: 20020508
Ar?3 4INCal Laboratories TEL: [phone] FAX.- [phone]
Website: huv:llwww.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization BatchlD: R109137
;ample ID: LCS-R109137
SampType: LCS
TestCode: pH_Oil(9045 Units: s.u.@20.5C
Prep Date:
RunNo: 109137
;lient ID: LCSW
Batch ID: R109137
TestNo: SW9045D
Analysis Date: 2/10/2020
SegNo: 2616511
knalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 90 110
;ample ID: 20020536-001ADUP
SampType: DUP
TestCode: pH_011(9045 Units: s.u.@20.5C
Prep Date:
RunNo: 109137
;lient ID: Batch=
Batch ID: R109137
TestNo: SW9045D
Analysis Date: 2/10/2020
SegNo: 2616516
\nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 6.8 0 0 6.7 0.4 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 20 of 36

SUMMIT Summit Environmental TechnoloWinStInc. QC SUMMARY REPORT
33/0Win St.
ENVIRONMENTAL rECHNOLOGiES, INC Cuyahoga Falls, Ohio 44223
Analyrlcal Laboratones TEL: [phone] FAX.- [phone] WO#: 20020508
Website: httn://www.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization Batchll): R109137
Sample ID: CHECK 7
SampType: LCS
TestCode: pH_NPWI450 Units: s.u.@22.00
Prep Date:
RunNo: 109137
7,lient ID: LCSW
Batch ID: R109137
TestNo: SW9045D
Analysis Date: 2/10/2020
SegNo: 2616783
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 99.9 98.6 101.4
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal;
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 36

summill
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOG -q I.-
t3nateGC.af Laboratories
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
BatchlD: R109180
Sample ID: LCS-R109180
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
Client ID: LCSS
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619308
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 8.02 7.240 0 111 70 130
Sample ID: 20020386-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
Client ID: Batch=
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619310
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
ample ID: 20020006-001ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
lient ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619312
nalyte
Result
PQL SPK value SPK Ref Val '%REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability non-flammable 0 0 20
Sample ID: 20020006-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
Client ID: Batch=
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619314
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 0.380
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
0.4000 5.13 20
H Holding times for preparation or anal}
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 22 of 36

Summ i l
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL rECHNOLOGIFS
Analyrxat Laboratories
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Waste Characterization
BatchID: R109180
iample ID: 20020006-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
;lient ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619314
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
iample ID: 20020006-002ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
;lient ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619315
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 0.430 0.4000 7.23 20
iample ID: 20020006-003ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
;lient ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619317
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability , not propagate 0 0 20
iample ID: 20020006-003ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
,lient ID: Batch=
Batch ID: R109180
TestNo: SWI030
Analysis Date: 2/10/2020
SegNo: 2619318
knalyte
Result
PQL SPK value SPK Ref Val
'%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
Qualifiers:
not propagate
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
0
0 20
H Holding times for preparation or anal}
MC Value is below Minimum Compound
PL Permit Limit Original
S Spike Recovery outside accepted reco
Page 23 of 36

SUMM1
Summit Environmental Technologies, Inc.ffl 3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL rcCHNOLOG!ES, N-
4na1Yt,cal Labnrllones
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: httn://Www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Waste Characterization
BatchID: R109180
ample ID: 20020006-004ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
lient ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619320
nalyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability 3.23 2.830 13.2 20
ample ID: 20020006-004ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
lient ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619321
nalyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qua]
Ignitability 3.09 2.830 8.78 20
Sample ID: 20020006-005ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
Client ID: Batch=
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619323
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Ignitability non-flammable 0 0 20
Sample ID: 20020293-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo:
109180
Client ID: Batch=
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo:
2619325
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD
RPDLimit Qual
Ignitability 4.46
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
5.190 15.1
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
20
Original
Page 24 of 36

S U MM 111-
33/0 Win StSummit Environmental Technologies, St. .
QC SUMMARY REPORT
ENVIRONMENTAL. TECHNOLOGIES. ^•
Cuyahoga Falls, Ohio 44223
Anaivrical Laboratories
TEL: [phone] FAX.- [phone]
WO#: 20020508
Website: http://Www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
BatchlD: R109180
#ample ID: 20020293-002ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
client ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619325
\nalyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
iample ID: 20020293-002ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mmisec
Prep Date:
RunNo: 109180
:lient ID: Batch=
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619326
knalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Jmtaowry 4.48 5.190 14.7 20
iample ID: 20020507-001ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
,lient ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619328
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qua[
grutamuty , not propagate 0 0 20
Sample ID: 20020507-001ATRIP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
'Bent ID: BatchQC
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619329
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
gmtaminy , not propagate 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anah
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 25 of 36

summilt
Summit Environmental TechnolWSt. QC SUMMARY REPORT
3310/0 Win St.
ENVInONMENTAL TECHNOLOGIES, iNC Cuyahoga Falls, Ohio 44223
Analyfical Laboratories TEL: [phone] FAX. [phone] WO#: 20020508
Website: httv:llwww.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization Batchll): R109180
Sample ID: 20020508-001ADUP
SampType: DUP
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 109180
client ID: Sludge
Batch ID: R109180
TestNo: SW1030
Analysis Date: 2/10/2020
SegNo: 2619331
analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit Highl-imit RPD Ref Val
%RPD RPDLimit Qua[
gnitability non-flammable 0 0 20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal3
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 26 of 36

SUMMIEF 3310 Win StSummit Environmental Technologies, St. QC SUMMARY REPORT
.
ENVIRONMENTAL TECHNOLOGIFS, ;NC Cuyahoga Falls, Ohio 44223
Analytical Laboralanes TEL: [phone] FAX.- [phone] WO#: 20020508
Website: httn://www.settekcom 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization Batchll): R109.573
mple ID: 20021049-007AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 109573
ant ID: BatchQC
Batch ID: R109573
TestNo: SW9014
Analysis Date: 2/19/2020
SegNo: 2637160
alyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500 10.00 0 0 81.6 122 S
Sample ID: 20021049-007AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 109573
Client ID: BatchQC
Batch ID: R109573
TestNo: SW9014
Analysis Date: 2/19/2020
SegNo: 2637161
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
3nlae, Reactive ND 0.495 10.00 0 0 81.6 122 0 0 5 S
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal}
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 27 of 36

summur
Summit Environmental Technologies, Inc. 33/0 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOL.OGiFS, ,NC
Anntyrfcal Laboratories
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://Wivw.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North
Carolina Inc
Project:
Waste Characterization
BatchlD: R109573
mple ID: Blank
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 109573
ant ID: PBW
Batch ID: R109573
TestNo: SW9014
Analysis Date: 2/19/2020
SegNo: 2637134
alyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.485
Sample ID: LCS
SampType: LCS
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 109573
Client ID: LCSW
Batch ID: R109573
TestNo: SW9014
Analysis Date: 2/19/2020
SegNo: 2637135
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 9.52 0.490 10.00 0 95.2 85 115
Sample ID: RI -Check
SampType: RLC
TestCode: Cyanide,Rea Units: mg/L
Prep Date:
RunNo: 109573
Client ID: BatchQC
Batch ID: R109573
TestNo: SW9014
Analysis Date: 2/19/2020
SegNo: 2637137
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Snide, Reactive
ND 0.485 0.5000 0 74.8 50 150
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 28 of 36

summi
Summit Environmental Technologies, Inc. 33/0 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGiFS . '
Cuyahoga Falls, Ohio 44223
Anaiyflcaf taboratonos
TEL: [phone] FAX.- [phone]
WO#: 20020508
Website: http://www.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Waste Characterization
BatchlD: R109591
Sample ID: 20021049-007AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 109591
Client ID: BatchQC
Batch ID: R109591
TestNo: SW9034
Analysis Date: 2/19/2020
SegNo: 2638334
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4530 25.0 4800 0 94.4 80 120
Sample ID: 20021049-007AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 109591
Client ID: BatchQC
Batch ID: R109591
TestNo: SW9034
Analysis Date: 2/19/2020
SegNo: 2638335
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4560 25.0 4800 0 95.0 80 120 4530 0.660 30
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 29 of 36

summill
Summit Environmental Technologies, Inc. 3310 Win St.
QC SUMMARY REPORT
ENVIRONMENTAL TECHNOLOGirS
Cuyahoga Falls, Ohio 44223
AMilyticat Laboratorles
TEL: [phone] FAX: [phone]
WO#: 20020508
Website: http://m,ww.settek.com
21-Feb-20
Client:
Cascades Tissue Group - North Carolina Inc
Project:
Waste Characterization
BatchlD: R109591
Sample ID: MB-11109591
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 109591
:lient ID: PBW
Batch ID: R109591
TestNo: SW9034
Analysis Date: 2/19/2020
SegNo: 2638284
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
iunioe, Heactive ND 25.0
iample ID: LCS-R109591
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 109591
;lient ID: LCSW
Batch ID: R109591
TestNo: SW9034
Analysis Date: 2/19/2020
SegNo: 2638285
\nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
iultide, Reactive 4660 25.0 4800 0 97.1 85 115
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 30 of 36

SUMM101
Summit Environmental Technologies, In. Qualifiers and Acronyms
3310 Win S
"0"1 ENVIRONMENTAL TFCHNOLOGIFS, .NC Cuyahoga Falls, Ohio4421 WO#: 20020508
AnalyNeal Laborarorie� TEL: [phone] FAX.- (330) 253-446
Website: httn://www.settek.co Date: 2/21/2020
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB, or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 31 of 36

SUMMIT Summit Environments! Technologies. St. DATES REPORT
3310 /0 Win St.
ENVIRONMENTAL TECHNOLOGIES, wC Cuyahoga Falls, Ohio 44223
fi r7alyrlcal Laboratorles TEL: [phone] FAX.- [phone] WO#: 20020508
Website: hulp:llwww.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc
Project: Waste Characterization
Sample ID Client Sample ID Collection Date Matrix Test Name Leachate Date Prep Date Analysis Date
20020508-00 1 A Sludge 2n/2020 8:00:00 AM Sludge Ignitability of Solids (SW-846: 1030) 2/10/2020 1:00:00 PM
pH (SW9045D) 2/10/2020 4:22:07 PM
Reactive Cyanide (9014/7.3.3.2)-Solid 2/19/2020 10:33:00 AM
Reactive Sulfide (9034)/7.3.4.2 2/19/2020 10:33:00 AM
TCLP Herbicides by EPA 8321B 2/11/2020 5:00:00 PM 2/13/2020 5:36:00 AM
TCLP Mercury Analysis (SW1311/7472/11/2020 5:00:00 PM 2/17/2020 9:00:00 AM 2/17/2020 2:08:00 PM
TCLP Metals Analysis (SW1311/6010'2/11/2020 5:00:00 PM 2/13/2020 8:50:00 AM 2/13/2020 2:43:06 PM
TCLP Pesticides Analysis (SW1311/8C2/11/2020 5:00:00 PM 2/12/2020 9:45:00 AM 2/15/2020 3:12:00 AM
TCLP Semi-Volatiles Analysis 2/11/2020 5:00:00 PM 2/13/2020 10:30.00 AM 2/14/2020 10:19:00 PM
(SW 1311 /8270)
TCLP Volatiles Analysis 2/11/2020 5:00:00 PM 2/13/2020 12:38:00 AM
Original
Page 32 of 36

summlir
Summit Environmental Technologies, Inc. Accreditation Program
3310Win St. Anal teS Report
ENVInONMENTAL TECHNOLOGIFS, ;NC Cuyahoga Falls, Ohio 44223 Y p
ARalyrcaf Laboratories TEL: [phone] FAX.- [phone] WO#: 20020508
Website: httn://www.settek.com 21-Feb-20
Client: Cascades Tissue Group - North Carolina Inc State: NW
Project: Waste Characterization Program Name: NC_WW_SCM
Sample ID !Matrix
Test Name
Analyte
Status
20020508-001 A Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321 B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321 B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW 1311 /6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW 1311 /6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW 1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW 1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW 1311 /8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW 1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW 1311 /8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW 1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW 1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW 1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW 1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Original # 1
Page 33 of 36

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�'t Summit Environmental Technologies, Inc.
S U M3310 Win St.
TjENVIRONMENTA.LTE-CHNOLOG71-- . Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Anaryrical Laboratories TEL: [phone] FAX: [phone]
Website: http://Www.settek.com
Client Name: CAS-NC-28379 Work Order Number: 20020508 RcptNo: 1
Logged by: Jacqueline Rasile
Completed By: Jacqueline Rasile
Reviewed By: Holly Florea
Chain of Custody
1. Is Chain of Custody complete?
2. How was the sample delivered?
Log In
3. Coolers are present?
2/8/2020 8:21:00 AM
2/9/2020 12:48:40 PM
2/11/2020 11:40:21 AM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0° C to 6.0°C
7, Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
Summit
Yes
Yes❑
Yes ❑
Signed By
Yes
Yes U
Yes
Yes❑
Yes
Yes ❑
Yes ❑
Yes ❑
Yes W
Yes
Yes ❑d
Yes d❑
Yes ❑
No ❑ Not Present ❑
No ❑ NA ❑
No ❑
No ❑ Not Present k
No ❑ NA ❑
No ❑ NA ❑
No ❑
No ❑
No ❑
No d❑ NA ❑
No ❑ No VOA Vials
No
No ❑
No
❑
No
❑
No
❑
No ❑ NA ❑d
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No Temp °C I Condition Seal Intact Seal No Seal Date Signed E
1 1.4 Good Not Present
--
2 11.5 1 Good. Not Present
Page 36 of 36

Barber, Jim
From:
Sent:
To:
Subject:
Attachments:
Trent Allen
Fayetteville Regional Supervisor.
Division of Water Resources
910 433 3336 office
Trent.Allen@ncdenr:eov
225 Green Street — Suite 714
Fayetteville, NC 28301
Allen, Trent
Thursday, June 18, 2020 2:36 PM
Barber, Jim
FW: [STAFF REPORT REQUEST] WQ0009477 - Rockingham FiberClay Distribution
Program Renewal Application.
WQ0009477 WSROSNDARR 200618.pdf
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed
to third parties
From: Thornburg, Nathaniel
Sent: Thursday, June 18, 2020 2:23 PM
To: Williams, Kendall <[e-mail]>
Cc: Giri, Poonam a <[e-mail]>; Allen, Trent <tren"[e-mail]>; Brantley, Mark
<[e-mail]>
Subject: [STAFF REPORT REQUEST] WQ0009477 - Rockingham FiberClay Distribution Program Renewal Application
RO Supervisors — Please assign this project to one of your staff for review.
APPLICATION LINK: https:Hedocs.deg.nc.gov/WaterResources/DocView.aspx?id=1217278&searchid=f8e981c9--0986-
41bd-bfbc-764d6c56f940&dbid=0&repo=WaterResources
Kendall,
Please process the subject application received June 18,2020 in BIMS.
I've included the RO review request form for your use. I also included the Applicant email addresses in the comment
section of RO review request form.
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Please copy the RO, Reviewer, and myself on the acknowledgement letter that you send to the Applicant.
Thank you,
Nathaniel D. Thornburg
Branch Chief
Non -Discharge Branch
Department of Environmental Quality
919 707 3653 office
[e-mail].
512 N.. Salisbury St.
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Email correspondence to and from this address is subject: to the
North Carolina Public Records Law'and may be disclosed to third'parties.
2