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Home My WebLink AboutNCS000533_COMPLETE FILE - HISTORICAL_20190326STORMWATER DIVISION CODING SHEET RESCISSIONS . PERMIT NO.. N DOC TYPE COMPLETE FILE'- HISTORICAL DATE OF RESCISSION p � � l l 03 c) YYYYMMDD STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. NCGNE DOC TYPE ❑ HISTORICAL FILE DOC DATE ❑ YYYYMMDD e April 30, 2018 Division of'Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: March 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the March 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalis SW001, SWO02, SWO05, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x101 or rward@silar.com. Regards, 4'�Y, 6joi Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com RECEIVED MAR 2 6 2019 L: EN' RAL FILES DVVR SECT10,11 Silar, LLC - STORM WATER SAMPLING REPORT Certificate orCoverage No-: NCS000533 Columbus County, North Carolhta Pcrstrrute] Collccrmg Szu�la: G. Ward _-- _ _ _ _ �� jj Cct iSed Laborataria: Eavhnslmw'trl Chemists I.ab ID: % 1 T 3alntiona lac. LAUD: 37_ ANALYTICAI. RESM.TS 00530 00310 003t0 00610 W625 00630 00665 77U5 50060 71=0 01042 01092 01053 01031 00556 a"" 00300 TAA3B TOW T&td TOW TOW Tana! Non -Polar Acute Dale 1'9.9 BOD COD MUTK1Y NQ3+tV07 PbwpSmna OdNMnd TRC El�mloe FarmeNdgda tiper p Lde Maaaaaere d O$G Loadx. pH D.O. To Ootlall andddyr e/1 ra melt -0 nw mgl mgl 1 ragl manmg0 Raom09 mtYl W rrrg3 rag! r-rG wgl LCSO 001-NlarWhse "Iti8 0 0 0 0 0 0 0 0 0- 0 0 0 0 0 0 0 0 0 002 - Lab Weir 3131118 0 0 0 0 0 0 0 1 0 0 0 1 0 0 0 1 0 0 0 0 0 005 -Siia Weir V31118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 010 MOB 0 0 0 0. 0 0 0- 0 0 0 0 0 0 0 0 0 0 0 005 Upst MI -I 0 0 oo5 Dowmb=o 351, 0 0 STORM EVEM CNAStACTERISTICS Total Evens Prodpitation (ins.): N1A Petrtrii Sxnpling Period.-= Note: M:L duplicate copies ta: Division of water Quality Watar Quality Section Ann- Ca1Lxl ]Fia 1617 Ma>Y Scr%ice Center Raklgh, NC 27699-1617 By this signature, I cel* this report is accurate and complete to the bat of my lntowlc*. ALP y 1� tgaat0ra of Perrnitt c or Designee Date + r ( Y 5A v— Name and i-dle Company Information S17ar, LLC 333 Neila Eddy Rand Rivgftood, NC 28456 (910) 655.42I2 EXT. 100 Personnel Collecting Samples: G. Ward CerkW Laborz=cs: Euvuomnadal Chemttta ;Environmcrna] Toting Sahttiam, Inc. ANALYTICAL RESULTS Silar, LI.0 — STORM WATER SAMPLING REPORT Certiticate of CoverageNo.: NCS000533 Cniumbua County, North Caraiirm Lab ID: 94 Lab ID: - 37 60530 00310 00340 00610 oncxs 00630 0"65 77581 50060 01012 0l092 01055 Olast OOSS6 tIW00 00300 TAA3B Tan] Tan1 Total lard Total Non -Polar Acute Date TSS ROD COD NH3 TKN NO3iM2 Pbnp' Metband TRC fkzambw ;11U3 Fwbyde GpperLos Llagapee t-md Odic pH AA. Tom 0Wfa11 mddd!7r mri mrJ1 mpll m@tl mpjt mg71 mkt mil mil myi .ql m8/1 1489 r.o. see+] 1.C50 ow-SiloWhse 3J31118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - Lb Weir Y31118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Silar Weir 3/31/18 0 0 0 0 0 0 0 0 1 0 1 0 0 0 F 0 0 0 0 0 0 0 010 3131118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 003 tlp6>Tea7n 1131118 WOD 0 0 005Dowmmb V31/18 0 0 STORM EVELYI CIIARACTFRISTICS Mall duplicate copies to: Division of Water Quality Total Evan Precipitation (in5.):F NIA Water Qoaw Section Attn: Car" Fdcz Permit Sampling Petiod: 1617 Alad Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify this report is accurate and complete to the beat of my knowledge. Company Informatlon Aliq-A�— S Sam, ILC U 333 Veils Eddy Road tgnaturu of Perrnittee or Designee Date Riegelwood, NC 28456 (910)655-4212 _ EXT. 100 Print Name and Tick March 1, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: February 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the February 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for OutfatIs SW001, SWO02, SW005, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x 101 or rward@silar.com. Regards, Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com RECEIVED MAR 2 6 2019 ;END-Q\L FILE` OVVR SECTION Silar, LLC - STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists - -- - — Lab ID: 94 -- - P.nvironmental Testing Solutions, Inc. Lab ID: 37 i ANALYTICAL RESULTS 00530 00310 00340 00610 00625 00630 00665 77885 50060 71890 01042 01092 61055 01051 00556 9D400 00300 TAA39 Total Tote! Total Total Total Non -Polar Acute Date TSS ROD COD N713 TKN NO3+NO2 Phorpharus Methanol TRC He:9mine Formaldehyde Copper Zinc ,hlangartere Lead O&G pit D.O. Tax. Outtall mdddlyr mgll rng/t mgfl mgll mgfi mg/l cowl mg/1 mg(I tngA mgn -10 mgA UW mgfl mg11 Ca mg/1 LC50 001-St7ar Whse 2R8118 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - fah We 2R8118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Silar Weir 2129119 0 0 0 0 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 O10 zn8118 0 0 0 0 0 0 0 a 0 0 0 a o a a a o a 005 upstream 7l2&fs o a 005 Downstream 2128lI8 a 0 STORM EVENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): NIA Water Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this si re, I certify this report is accurate and complete to the best of my knowledgc. ` � 1 Company Information iL Sitar, C G�/C�GJ 333 Neils Eddy Road titre of Permit/tee or Designee ate Riegelwood, NC 78456 (910) 655-4212 Pnnt Name and Title EXT. 100 Personnel Collecting Samples: G. R'ard Certified laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ANALYTICAL RF,SULTS Silar, LLC — STORM RATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina lab M: 94 Lab ID: 37 00530 00310 00340 00610 00625 00630 00665 77885 50060 71880 01042 01092 01055 01051 00556 004001 00300 'I'lw Moral Total Total Total Total Non -Polar Acute Dale 'M ROIL COD N1I3 'I'KN NO3+NO2 Phosphorus Methanol TRC llexamine Furmaldehvile Copper Zinc Mangan— Lead O&G pll D.O. lox. Outtall molddhr mgll MWI mgti mgll mgrl mwl MWI MWI mgn mgn tngll mgfl mg/l mgA mglt MWI a.u. mgrl I.C50 0o1-Sitar Whse 2128118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - lab Weir M8118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - soar Weir 2i28118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 2I28118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 Upstream 2l28116 0 D 005 Downstream 2l28118 0 0 STORM EN'FN I' CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): NIA Water Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Service Center Raleigh, NC 27699-1617 Note CFRTIFICATION STATE'%lF1T lly this si alure. I certify this mporl is accurate and complete to the best of my knowledge. f �( Company Information Sitar, LLC 333 Neils Eddy Road alurc of Permit= or Designee ate Riegelwood, NC 28456 (910)655-4212 EXT. 100 Print Name and Tide January 31, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: January 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the .January 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for OutfalIs SWOO1, SWO02, SWO05, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 a101 or rward@silar.com. Regards, RECEIVED Gina Ward MAR. 2 6 2019 Environmental health and Safety CENTRAL FILES Silar Laboratories DVIR -S� p(910)-655-4212 ext.101-�r101``! f (910-655-8201) rward@silar.com s am Tke-g- T-) Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ANALYTICAL RESULTS Sitar, LLC — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab tt): 94 Lab tt): 37 00530 00310 00340 00610 00625 00630 00665 77885 50060 71880 01042 01092 01055 01051 00556F10 00300 TAA313 Total Total Total Total Total Non -Polar Acute Dale 7S5 ROD COD NH3 TK.ti \'03+�'02 Phosphorus ?lethanol 7RC Recamine FormaldeMde Copper Zinc A[angenese hrad O&Gpit U.O. TO%. Outfall molddl7r mpJ] mpJl mp,/I mg11 mgll mgJE mgll m8ll mgll mpJl mgll mgll mg11 mga mgll m�Jl MWI 1.C50 001-Sitar R7sse 11311I8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - Lab Weu 11311I8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Silar Weir 1131l18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 1131118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 Upstream 1131lIS 0 005 Downstream 1131l18 0 STORM EVE,Vr CIIARACTERISTICS Mail duplicate copies to: Division of Water Quakily Total Event Precipitation (ins.): N!A Water Quality Section Attn: Central Files Permit Sampling Period: = 1617 ),fail Service Center Raleigh, NC 27699-1617 Note: CERTI FICATION STATFNIENT lay this signature, I certify this report is accurate and complete to the best of my knowledge. j 3 r Company Information Sitar, LLC 0 I 333 Neils Eddy Road Signature of Perminee or Designee to ' Kicgebvood, \TC 28456 (910)655-4212 Print Name and Tile lI XT. 100 Silar, LLC—STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Personnel Collecting Samples: G_Ward Certified Laboratories: Envirorunental ChemistsT Lab ID: 94 I TEnvironmental Testing Solutions, Inc. Lab ID: _37 J. ANALYTICAL RESULTS 0053D 00310 00340 00610 00625 00630 00665 1 77885 50060 71880 01042 01092 D1055 01051 00556 00400 00300 TAA3$ TOW Total Total Talal Total Non -Polar Acute Date TSs ROD COD NH3 TKN NO3+NO2 Phosphorus Methanol TRC Hexamine Formaldehyde Copper TJae Manasme Lead O&G pH D.O. Tox. Ovtfall mo/ddlyr mg/1 mgn -0 mall mgA mall MO mg/i mgfl mg/l mgn mall mg/I MCA mall mg/1 La. mgA LC50 00l-Silas Whw U31118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002-Lab Weir inin8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Silar Weir 1131/18 0 0 0 1 0 D 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 W1118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 005 Upstream 1/31118 0 0 005 Downstream 1131118 0 0 STORM EVENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): r--N—/—A7 Water Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Service Center Raleigh, NC 27699-I617 Note: CERTIFICATION STATEMENT 13y this signature, I certify this report is accurate and complete to the best of my knowledge. r Company Information Silas, Lt.c f 333 Neils Eddy Road Signature of Permittee or Designcc ale Riegelwood, NC 28456 i (910)655-4212 EXT. 100 Print Name and Title July 22, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: June 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the June 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for OutfalIs SWOO1, SWO02, SWO05, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x101 or rward@silar.com. Regards, REC E I E D �) MAR. 2 6 2019 DVIR SECTION Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental 'testing Sohnions, Inc ANALVHCAL RESUI; tS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab [Di 37 00530 00310 00340 M10 00625 00630 00665 77885 50060 71880 01042 01092 01055 01051 00556 00300 TAA3B Total Total Total Total Total Non -Polar Acute Date TSS ROD COD NH3 TKN NO3+N'02 Phnspharos \telhannl TRC 1[esamine t-'ormaldehrde Copper 'zinc NanCaoese Lead O&C. ;00400 pit U.O. Tox. Outfatl molddl.r mgA m.-A mg, mgll mgA mRA mgA .%A mgA mgA mgA mg/l mg/l mrA meA mgA s.u, -0 LC50 00)-Silar Witse 6120f18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002-Lab Weir W2ons 1 26.2 1 25 1 166 4.0 L2.2 312 28 <5 0 <10 19%P8 0.034 0,280 0.026 <0.010 <5 822 0 005-Silar Weir 6120118 13.6 28 194 3,8 104 3.24 0.19 <5 0 <10 1270Pg 0.093 .441 0.139 <0.010 <5 7,98 0 0 010 0,120115 0 0 0 0 0 0 u 0 0 0 D 0 0 0 0 0 0 U 005 Upstream E6/20118005 Dowmstream 20113 0 0 STORM EVENT C1IARACTERISTWS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins,): 0.4 Water Quality Section Attn: Central Files Permit Sampling Period: 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT' By this signature, I eeriiR, this report is accurate and complete to the best of my knowledge. Company Information Sitar, LLC ja 333 Neils Edd%, Road lgnature of Permittee or Designee We Riegehsood, NC 28456 (910) 655-4212 r lrn I /)/ K/7Q Print Name and Title EXT. 100 Personnel Collecting Samples: G. Ward Certified Laboratories, Emvironmemal Chemists Environmental Testing Solutions, Inc. ANALYTICAL RESULTS Silar, LLC—STORM WATER SAMPLING REPORT Certificate of Coxerage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 00530 00310 00340 006t0 00625 00630 00665 77885 500-60 71880 01042 01092 01055 01051 00556 40300 TAA36 Ourfall Pale molddi r TSS mpA BOD m-A COD mpA N113 m.A TKN mp11 NO3+NO2 mgll 'ro[al phosphorus mgA Methanol mg/l TAC mph Ite.amine mp,4 Farmaldehsde nog/1 Total Capper mg'l Total Zinc Mtn 7ot.l \l..22n mVA Total Lead .0 Non -Polar O&C. mgfl U,O, mpJl Acute Tox, LC50 001-5i11r Whse 6120/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002-Lab weir 6120118 26.2 25 166 4,0 12.2 3.12 .28 <5 0 <to 1990u& 0.034 0.280 0026 <0.ot0 <5 ]7.98 0 005 - Silo Weir 6120118 13.6 28 194 3.8 104 3.24 0,19 15 0 <10 t 270 p g 0.098 A41 0139 <0.010 <5 0 0 UIU 005 Upstream 005 Downstream �i'20118 61201180 6120118 0 0 U ll U 0 U U 0 0 0 U U U U 0 0 U 0 STORM EVEN'r CHARACTERISTICS Mail duplicate copies to: Division of Water Qualily Total i;vent Precipitation (ins.): 0.4 Water Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By [his signature, 1 certify this report is accurate and complete to the best of my knowledge_ Company Information \ /I T Silar, I.LC fX,] 333 Neils Eddy Road SignahTr_e of Per-mittee or Designee ale Riegelwood, NC 28456 (910) 655-4212 Pri—M Name and Title EXT_ 100 5 April 30, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: April 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the April 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under PermitNCS000533 for Outfalls SWOO1, SWO02, SWO05, and SWO10. If you have any questions regarding this submittal, 1 can be contacted at (910) 655-4212 x101 or rward@silar.com. Regards, /�O 0. Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com RECEIVED MAR 2 6 2019 ;:EN-)-RAL FILI C CVVR SE:CTIO- 1 Pcmomcl Collecting Samples: G. Ward . Certified Lzbomwries: Environmental Chemisie NtviMstmentai Testing Soiufi m i e. ANALYTICAL RESULTS Sitar, Id.0 —STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 OOS30 00110 00340 00610 1 00625 00630 00665 771185 So060 71920 01042 01092 01055 01051 005S6 00401 003D0 TAA3B Total Total Total TOW TOW Nan -Polar Acute Datr T33 80D COP Nli] T1Q1 tY03+K02 Plro4lrorur it4elhand THC Heamine For,oaldehyde Capper zincMac_Lead 0'(;pH D.O. Toa- Oarfall mdddlyr m0q mg/! my1 -VI-0 + 40 mg/l m07 "A mrfl MCC mN M&4 q0 rerpfl my/1 s.a. m;n LCSo wl-silerwhsO 4wIS 0 a 0 0 0 0 0 0 0 0 0 0 0 Q O 0 Q p 002- Lab Weir Awls 0 0 0 0 a 0 0 0 0 0 0 0 0 0 0 0 0 Q 005-Sitar Wcir 4wi8 a 0 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 4r3WI8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 UpwCam 4WI8 0 0 a03 Powmumn 4i3N10 p O STORM EVENT CIIARACTERiSTICS Mail duplicate copies to: Division of Water Quality Total L cm Precipitation (ms.):F_N1_Aj Water Quality SWAM Attn: Central Files Permit Sampling Period:� 1617 Mail Service CcnttT Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify this report is accurate and complete to the best of my knowledgc. Company Information Sitar, LLC ( J a 333 Neils Eddy Road tgnatirre of Pc mirtce or Designee etc Riegelwood, NC 28456 (910) 6$5-4212 EAT, 100 Print Name and T. Silar, LLC—STORM WATER SAMPL=REPORT Certilicsre of Coverage No.: NCS000533 Columfurs CounlN North Carolina Persatmd C.,ollxting Samples: G. Ward CutdiW Labatsaoriea: i ilzr mncd>al Chemise J Lab ID: 94 :Ervb sWTesting Schuions,hr— _ Lab ID: ANALYTICAL RFSMTS 00510 00310 00360 00610 00623 006I0 00665 77M 50060 711130 01062 Olm Gloss 01051 00556 oNo0 00300 TAA3B Toot TOW Total ialat Tow Mon -Polar Acute Done T33 BOIL COD PW TIDY NO"03 FWuplamw ?ddhasnt TRC 1laamtn Farmalilft Ceppw zinc bf-g ne Lead O&G pH D.O. Tor. Oatfalt ondddryr 1w awl col melt rna/l 1130 mG9 me K410 radl >Rd1av To -0 elm mA7 LC50 OolSihrwhse 4wis 0 0 a a a D 0 0 a 01 0 0 0 a a 0 0 0 002 . Lab WdF er3a7S a 0 0 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 0 a vas-sihrweir 45WIS a 0 v 0 0 0 a o I o 0 0 a v 0 0 a a a v 010 _ 0 O ..0 O _ 0_ 0 0 8 005 Up wM0 A OOS Downstream O 0 STORM EVENT CHARACTERISTICS Total Exert Precipitation (ma.): WA Permit Sampling Pe iod:= Note: M I duplicate copies to: Dicsaioo of ivatcr Qwday Water Quality Section Attn: Central Film 1617 Mail Service Ceruer R&W3, NC 27699-1617 By this sigmiutr, I cvufy this report is aectuam and complete to the best of my Faawlcdge- J c- , it tgnartue ofPeamiaw or Designee ate �Lffr Print Name and T' e Company Information Saar, LLC 333 Neils Eddy Road Riegelwood, NC 29456 (910) 655-4212 EXT. 100 June 14, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: May 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the May 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SW001, SW002, SW005, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x101 or rward@silar.com. Regards, e �tz 4 Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com Personnel Collecting Samples: G. Ward Certified Laboralories: Environmental Chemists Environmemal Testing Solutions, Inc. ANALN-TICAL Rl•.SltiLTS Silar, LLC—STORM WATER SAMPLING REPORT Certificate of Coveruge No.: NCS1i00533 Columbus Counly, North Carolina Lab ID. 94 Lab Ill: 37 00530 00310 00340 00610 00625 00630 00665 778" 50060 71980 01042 01092 01055 01051 00556 00400 00300 TAA31f 'ratal Total 'Total Total Total Non -Polar Acute Dafe 'rss ROD COD N113 TKN SO;+NO2 Phosphorus Meth-11 TRC Ilexamine Formaldehyde Copper Zinc Alsngancse Lead O&c(: pit D.O. Tox. Ouffall molddlvr mgA -10 -9A -0 mo me l mgA mg+l -ZA mgA mgll ino mgA mgil mgil mgfl mCA LC50 001-Sitar Whse 512511E 21.2 8 53 2.7 1 0.71 0.36 c5 0 <25 6520 0.015 0.147 0)l$ <0.010 <5 7.8 0 002 - Lab Weir 5125118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005-Sitar Weir 5125118 50 20 74 21 <0.5 0.37 023 <5 0 Q5 2870 0.108 0,397 0.037 c0010 <5 8.26 0 0 Oto 3125118 IM, to 36 22 1.0 U.46 U.61 <5 U <25 7590 0.025 0.341 0.018 <UAIU 15 8.3 0 005 Upsumm 5125118 E1125/18 0 0 005 Dounsu or 0 0 STORM EVENT CHARACTERISTICS \tail duplicate copies to: Division of Water Quality Total Evens Precipitation (ins.): OA2 Water Quality Section Alin_ CenIial Files Permit Sampling Period: 1617 Mail Sen'ice Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT alure, I certify this report is accurate and complete to the best of my knowledge, ©wl_ Company Information p{ J u Sitar. oils 333 Neils F.ddq Road Signature of Permittee or Designee ate Riegelwood, NC 28456 (910) 655-4212 07' ExT.loo Print Name and Title Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Fm•ironmental Testing Solutions, Inc. ANALVHCAL RESIJI:rS Silar, LLC—STORM wATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 00530 00310 00340 00610 00625 00630 00665 77385 50060 71880 01042 01092 01055 01051 00156 ootoo 00300 TAA3B outran Dale molddlyr T5s man BOD man COD m-4 NH3 mg4 Tl(N' mgA NO3+NO2 mgll i'o[al Phosphorus Mg/1 Methanol mpA TRC -0 Be-raioe mg4 Formaldehyde man Ta1a1 Copper mglt Total Zinc mgA Taal Styaoane,e m'4 Total Lead mg4 Non -Polar O&G Mtn p1E S.U. mg4 Acute I.C50 001-Silar Whse 5125YIS 21,2 8 53 2,7 1 0.71 0.36 <5 0 <25 6520 0.015 0.147 0.019 <0.010 <5 7.8 0 002 - lab Weir 5125118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 -Silar Weir 5I25113 50 W 74 21 10.5 0.37 0.23 <5 0 <25 2870 0.108 0.397 0.037 .0 ULO <5 8.26 0 0 010 005 Upstream 005 Downstream SR5118 5125118 5725118 1 _ l0 36 2,2 1,0 0.41, 0_61 <5 0 <25 2590 0_025 U.341 0.016 <U,OIU a5 8.3 0 0 0 0 0 STORM EVENTC11ARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Fvent Precipitation (ins.): F 0 42 Water Quality Section Alm Central Files Permit Sampling Period: 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certifg this report is accurate and complete to the best of my knowledge. Company- Information � Sitar, LLC 333 Neils Eddy Road St azure of Petmittee or Designee ate Ricgehwod, NC 28456 (910) 655-4212 EXT, 100 Pnm Name and Title IL Aug 13, 2018 Division of Enemy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RL: July 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the July 2019 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SWOOI, SW002, SWO05, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x101 or rward@silar.com. Regards, MAR 2 6 2019 u�r1R S CT O1`1} Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com Personnel Collecting Samples: G. Ward Certified Laboratories: Emrironmental Chemists Environmental Testing Solutions, Inc. ANALYTICAL RESULTS Silar, LLC—STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 00530 00310 00340 00610 00625 00630 o0b6s 77995 50060 71880 01042 01092 01055 01051 00556 00400 00300 TAA313 Total Total Total Total Total Non -Polar Acute Date TSS HOD COD N113 TKN NO3+NO2 Phosphorus Methanol TRC Hexamine Formaldehyde Capper 7lmc hbaaanese Lead O$G pit D.O. Tox. Ontfall mo/ddlyr mgll mgli m I mWI mg/l mgn mg/1 mg/I mgA mg/1 mg/l mg/I mgll > mgp mgll S.U. mgfl LCSO 001-Silar Whse 7/31/18 0 0 0 0 0 0 0 D 0 0 0 D 0 0 0 0 0 0 D02 - Lab Weir 7/31/18 0 0 0 0 0 0 0 0 D 0 0 0 0 0 0 0 0 0 005-Sft Weir 7M/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 7/31119 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 D05 Upstream 7/31/18 0 0 005 Downstream 7/31118 0 0 STORM EVFNTT CHARACTERISTICS Mall duplicate copies to: Division of Water Quality Tots! Event Precipitation (ins.): NIA Water Quality Section Attn: Central Files Permit Sampling Period: 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify this deport is accurate and complete to the best of my knowledge. y I� Ii Company Information Sitar, LLC 4al 333 Neils Eddy Road ignature of Perrhittee or Designee Riegelwood, NC 28456 (910)655-4212 EXT. 100 Print Name and Title Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ANALYTICAL RESULTS Silar, LLC — STORN4 WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab 1& 94 Lab ID: 37 00530 00310 00340 00610 006251 00630 00"s 77885 50060 1 71990 01042 01092 01055 01051 B 1 00556 00400 00309 TAcute Outrall Date TSS mo/dd/yr mg/I BOD mg/1 COD mg/I N113 mg/I TKN mvi NO3+NO2 mg/I Total Phosphorus MO merhanot mg/I TRC mg/l Htmmlm nto Formaldehyde mgll Tool Copper mwi Total TOW Zinc h"wese mg/I nw-4 Too! Lead MWI Non -Polar Oa4G pll D.O. UWA s.u. mgn LC50 001-Silar Wl s 7/31/19 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 ❑ 0 0 002 - Lab Weir 7131/18 0 0 0 0 0 0 ❑ 0 0 0 0 1. 0 0 0 0 0 0 D 005 - Sitar Weir 7/31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 0 O10 OOSUpstream Downstream 7131/1 00 0 0 0 0 0 0 0 0 0 0 p 0 0 0 0 0 8 0 D �7�131BDOS 0 STORM EVENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins-): N/A Water Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Service Center Ralelgh NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify thiss rt is accurate and complete to the best of my knowledge. / "Q C�� Company Information Silar, I.LC t S 333 Neils Eddy Road ilgtature of Petmittec or Designee at Riegelwood, NC 28456 (910) 655-4212 EXT. ]DO Print Name and Title Oct 8, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: August 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the August 2018 Discharge Monitoring Report (DMR) for Sitar Laboratories under Permit NCS000533 for Outfalls SW001, SW002, SW005, and SW010. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x101 or rward a silar.com. Regards, Gina Ward Environmental Health and Safety Sitar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com FI\/E MAR 2 6 2019 QVIRISECT; ME',') Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Fnvirontncntal Testing Solutions, Inc. ANALYTICAL RESULTS Silar, LLC—STORM WATER SAMPLING REPORT Certificate of Coverage No,; NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 00530 00310 00340 00610 00625 00630 00665 77885 50060 71880 01042 01092 01055 01051 00556 00400 tm300 TAA3R Twat 'total TOW Total Total Non -Polar Acute _ Date 'FSS ROD COD NH3 TKN NO3+NO2 Phosphorus .Methanol TRC Hevamine F'Ormaldeh5de Copper Zinc ]tangAnm 1-end O&G pH D.O. 1,01. Outfall mOldd/5 mgA mg1l mgA MO mg9 mgfl mgA mg4 mgA m%A mgl mgA .10 men mgA mgA 3- mg/1 LC50 001-Soar R'hse 8128118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 p 002 -tab Weir SY28118 144 64 561 5,9 71.9 3.38 2.39 <5 0 200 <50p g 0.114 0.586 0.063 '0010 <5 8.39 0 005 - Silar Weir 8128118 145 54 466 5,8 39,6 141 4.32 4 0.00264 121 <50g g 0.32 0.3_13 1.13 <0.01 <5 8.72 0 0 Uiu 8119.2 27 209 6.4 31.ti 1.35 1.03 <5 000111 72,3 <500e UU65 093b 0.038 <0.01 �5 8 to 0 005 Upsa— �SQA8118W5 Doenstream 0 0 S"rOItM EN'E\"I'Ci1,1RAC-I-ERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.}: 0.32 Water Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I cenify this report is accurate and complete to the best of my knowledge. Company Information 1 Q Sitar, LLC ,zj l j 333 Neils Eddy Road gnature of Permittee or Designee D le RiegclwoM, NC 28456 (910) 655-4212 rnn FXT. too Print Name and Title Personnel Collecting Samples: G. Ward Certified laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ANALVIACAL RESULTS Silar, LLC—STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 00530 00310 00340 00610 00625 00630 00665 77885 SOG60 71880 01042 01092 01055 01051 00556 00400 fT03UU TAA3B 0.117.11 Hate mofdJl.r TSS mgA BU❑ mgA CUD mgll SH3 mgA 'I'fiN mgJt SOS+\'U2 mg11 Total Phosphorus mgA Verhanol tog/1 '1'RC mg,A Hezamene milli Formaldrh.de mgA Total Copprr mgA Total 7inr mgA Total .51aoRane.e mgA Total Lend mgA Non -Polar O&G mgll P I s.u. D.O. mgA Acule 7bx. LC50 001-Silar Whse 8/28118 0 0 0 0 0 0 0 0 0 0 0 0 0 a a 0 0 0 W - Lab Wefr 8128118 144 64 561 5-9 71.9 3.38 2,39 �5 0 200 <50µg 0.114 0,586 0.063 <0.010 <5 8.39 0 005 - Sitar Weir 8128118 145 54 466 5.8 39.6 1.41 4.32 a5 0.00264 121 z50µ g 0.32 0.323 1.13 <0.01 a5 8.72 0 0 Wo 005 Upstream 005 Downstream 6126118 8 ER/8 19.2 27 209 6.4 31.6 1.35 1.63 a5 0.00111 72.3 <SUµg p,U85 U.936 0,U38 <O,UI s5 8.16 D 0 0 0 0 STORM EVENT C1IARACITRIS77CS Total Event Precipitation (ins.): = Permit Sampling Period: Note: \fail duplicate copies to: CERTIFICATION STATEMENT 13%. this signature, I certifc this epos is accurate and complete to the best of my knowledge. /17]1 azure o ermittee or Designee to nm Name and Title Division of Water Quality Water Quality Section Alin- Central Files 16t7 Mail Service Center Raleigh, NC 27699-1617 Cornpany Information Sitar, I.LC 333 Neils Eddy Road Riegelwood, NC 28456 (910) 655-4212 EXT. I00 Oct 10, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: September 2018 Discharge Monitoring Report To Whom It May Concern: I nclosed are two copies of the September 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SWOO1, SWO02, SWO05, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 s101 or rward a silar.com. Regards, dn� Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com REC'EI ED MAR 2 6 2019 CENTRAL FILE'.' DAP/R SECTIOI I Personnel Collecting Samples: G. Ward Certified Laboratories: Envirotunental Chemists Environmental Testing Solutions, Inc. ANALYTICAL RESULTS Sitar, LLC — STORM WATER SAMPLING REPOR'r Cet tificate or Co. crage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab iD: 37 00530 00310 00340 00610 00625 00630 00665 77885 50060 71890 01012 0109E 01055 01051 00556 00300 TAA3R Total Tolml Total Total Total Non -Polar ,\cute Date 785 BOD COD N113 TKN NO3+NO2 Phosphorus Mrlhanol THC Hexamine Formaldehyde Copper 7.Inr Martgsnese Lead O&G ;0(1400 p11 D.O. Tov Oulfall molddlyr mgll mgll mgll mgll mg11 mgll rnp11 MWI mp11 mgll MF)i MWI mgli m&1 mp11 mgll S.U. mp11 LC50 001-Silar %k ue 9139JI8 0 0 0 0 0 0 0 0 0 D 0 0 0 0 0 0 0 0 002 - Lab Weir 9130118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Sitar Weir 9130118 0 0 0 0 0 0 0 0 0 0 0 0 D 0 0 0 D 0 0 010 9.j3011B 0 0 0 0 0 0 0 0 0 v 0 0 0 0 0 0 0 0 005 Upstream W30/18 0 0 D05 Downstream 0130/16 0 0 SCORAI EVENT CHARACTERISTICS Mail duplicate copies to: Uidsion of Water Quality Total Event Precipitation (ins.): \!A Waler Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Scrnice Center Raleigh, NC 27699-1617 Note CERTIFICATION STATE\tE.N r By this signature, I cc this eporl is accurate and complete to the best of my knowledge. Company Information Sitar, , LI-LC 333 Neils IiddyRoad Signature of Penance or Designee ll to Riegelwood, NC 28456 (910)655-4212 EXT. 100 Tint Name and'I'iile Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ANALYTICAL RESULTS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 00530 OD310 00340 OD610 OD625 00630 00665 77885 50060 71890 01042 01092 01055 01051 00556 00400 TAA3B Total Total Total Total Total Non -Polar Acute Date TSS BOD COD NH3 TKY NO3+NO2 Phosphorus Methanol TRC Hexunine Formaldehyde Copper Zinc Manganese Lad O&G pH Toz. Outtall ma/ddlyr mg/1 ma11 mgn mg/1 mgn mg/l mg/l mg/I mail mg11 mail UWA mgfl can mgll mg/l s.a JDO. LC50 001-SilasWhse 9r"18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 00 002 - Lab Weir 9130/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 00 005 - Silar Weir 9130118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 D 0 0 0 010 9/30/19 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 D 0 0 005 Upstream 9/3(Vk8 0 0 005 Downstream 9/30✓18 0 0 STORM EVENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): NIA Water Quality Section Attn: Central Files Permit Sampling Period:= 1617 Mail Service Center Raleigi4 NC 27699-1617 Nate: CERTIFICATION STATEMENT By this signahtre, I cc this port is accurate and complete to the best of my knowledge. ,. Company Information Sitar, Ld.0 333 Neils Eddy Road Signaatttre of Pennittec Or Designee Dete RiegelwoodNC 28456 (910)655-4212 EXT. 100 'ISTint Name and Title Nov 05, 2018 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: October 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the October 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SW001, SW002, SW005, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x101 or rward@silar.com. Regards, d,2""3/)CC_,j Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com RECEIVED MAR 2 B 2019 CENTRAL FILE,:, DIP/R SECTIOtl Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ANAI.vf-ICAL RESUhrs Silar, TAX — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab m: 94 lab ID: 37 00530 00310 00340 00610 00625 00630 00665 77885 50060 719210 01042 (1109E 01055 01051 00556 004011 00300 TAA3I Total Total Total Toll Total Noll -Polar Acute Date TSS HOD COD tiE13 i-hT' \'O1+102 Phosphorus Methanol TIiC Hezamine Formaldehyde Copper Zinc .1[anganese Lend O&G pll D.O. Tox. Ou11e11 molddlpr MR1 mg/1 MWI mg/I mgll MWI M?)l mgft mgll mpfl mglt mgfl mgll mgt mg11 mg11 S.U. mgJl I,C50 001-Sitar Whse 10/31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - tab Weir 10/31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 -Sitar Wen 10/31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 16J31118 0 0 0 0 0 0 0 0 0 p 0 0 0 0 D 0 0 0 005 Upsueam 10/31/19 0 0 005 Downstream 10/31/18 0 0 STORM F,\'E\ 1' CltARACTF;RIs•r1Cs Mail duplicate copies to: Dixision of Rater Quality Total Event Precipitation (ins.): NIA Rater Quality Section Ann: Central Files Permit Sampling Period: 1617 A4ail Senirc Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATENiENT By this signature. I certify this report is accurate and complete to the best of my knowledge. /1 p� Company Information Sitar,, Ll- LI_C 333 \oils Faddy Road tgnature of Permiltee or Designee 1 ate Riegehvood, NC 28456 (910)655-4212 EXT. iDo Print Namc and Title r Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Enviromnental Testing Solution-, Inc. ANALYTICAL RESULTS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina La61D: 94 Lab ID: 37 00530 00310 00340 00630 00625 00630 00665 1 77885 50060 7188D 01842 01092 01055 01051 00556 00100 00300 TAA3B Torah Total Taut Taw Total Non -Polar Acute Date TSS iIOD COD N113 TiOV NO3+3NO2 PhaspMrua Methanol TRC Hexamine Formaldehyde Copper 71nc Manan4w Lad O&G pH D.O. Tex. Outfall mNddlyr mWrl mrA mg/l MWI mgll mg/l M&4 mg/l mg/l mg/1 mgli My] mgfo men mgll mgll S.U. mgtl LC50 001-52= Whu 10131/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - Lab Weir 10/31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 003-May Weir Joni/is 0 0 0 1 0 1 D 0 0 D 0 0 0 0 0 0 0 0 0 0 0 010 10(31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Upstream F 10/31/18 0 0 ownstream 10/31/19 0 0 STORM EVENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): NIA Water Quality Section Attn: Central Files Permit Sampling Period: C� 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify this report is accurate and complete to the best of my knowledge. I Company information Sitar, LLC 333 Neils Eddy Road tgnature of Pcrmiliee or Designee Bate, Riegelwood, NC 28456 (910)655-4212 G. , 11-J 4 � I EXT. 100 Print Name and Tidc —� je Dec 12, 2018 Division of' Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: November 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the November 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SWO01, SWO02, SWO05, and SWO10. If you have any questions regarding this submittal, 1 can be contacted at (910) 655-4212 x 101 or rward@si lar.corn. Regards, �4 0, �tLj Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext,101 f (910-655-8201) rward@silar.com REC'EI ED MAR 2 6 Z019 CENTNL FILE:, DP-IR SECT1O"-1 Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ,10;AIXTICAL RESULTS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus Counts, North Carolina Lab ID; 94 Lab ID; 37 00530 00310 60340 00610 00625 00630 00665 77885 50060 71890 01042 01092 01055 01051 00556 1104410 00300 T.L13f3 Oatfall Date mo/dtUsr TSS mgII 130D MWI COD MV)I MI3 mg11 -1'KN- 7%03+NO2 mg11 mgll Total Phosphorus mgll Methanol mgfl TRC mp,11 "examine Mgt] Formaldehyde mgll Total Copper mgll Total Zinc mgA Total Mangane- mg,l Total lead MWI Non -Polar O&G mg/l pll S.U. D.O. MWI Acute Tox. LC50 001-SdarNNJSc 11/30118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - Lab Weir 1 1/30118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Silas Weir I1130JI8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 010 005lipsVcam 005 Dokmstream 1113 EJE 0 a 0 0 0 0 0 0 0 0 0 0 0 0 0 0 D 0 D 0 STORU F%,FNi-CILIRA.C-rER[sr1CS Mail duplicate copies to: Di,,ision of Water Quahtv Total Bl nt Precipitation (ins.): \!A Water Quality Section Attn: Central Piles Permit Sampling Periodr= 1617 \lail Ser%ice Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify this report is accurate and complete to the best of my knowledge Company Information Sitar, LLC 333 Veils Eddy Road Signature of Permittec or Designee I le Riegelwood, NC 29456 (910)655-4212 /J1 FXY 101) Print lame and Title Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. — ANALYTICAL RESULTS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 O05J0 00310 00340 00610 00625 00630 00665 77US 50060 71880 OIG42 01"2 01055 1 0105E 00556 00400 00300 TAA3B Ootfall Date TSS molddlyr mgll BOD m811 COD mg/l NM mgR TICN NOJ+NO2 mrA m8A Total Phwphorm mg/l Methanol mg4 TRC mgA Hexamine mgll Formaldehyde mg/1 Total Total Copper Zinc -0 mg/l Total M.Ranese M94 Total Lead myfl Non -Polar O&G mg/l pH W.U. A.O. mgJl Acute To%. 11050 001-Sdar Whse I ir"18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002-Lab Weir IIf30lIs 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Sitar Weir I I l30118 0 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 005 Upstream 005 Domrstream 1101118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 11/30/18 0 11130/IH 0 0 0 0 STORM EVENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): FTN-171 Water Quality Section Attn: Central Files Permit Sampling Period: = 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify this report is accurate and complete to the best of my knowledge. ` %'W,2r Signature of Permittee or Designee Company Information Soar, LLC 333 Neils Eddy Road Riegelwood, NC 28456 r., ez (910) 655-4212 EXT. 100 Print Name and Title r t Dee 31, 2018 Division of' Energy, (minerals, Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RE: December 2018 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the December 2018 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SWOO1, SW002, SW005. and SW010. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 s101 or rward a silar.corn. Regards, Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com RECEIVED MAR 2 6 2019 CEN1TROAL FILES DV-/R SECTION Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc ANALYTICAL RESULT'S Silar, LLC — STORM WATER SAAfPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab ID: 94 Lab ID: 37 00530 00310 00340 00610 00625 00630 00665 77885 500611 718811 01042 01092 01055 01051 00556 00400 00300 TAA3R Total Total Total Total Total Non -Polar Acute Date i'Ss OOD COO M13 TKN N'03+Y02 Phosphorus Methanol TRC llexamine Formaldehyde Copper Zinc Mananese Lead O&G pH D.O. "fox. Outfall molddlSr mg11 mg/l mall mg11 mall mgll mg/I mall mg11 mgll mall mall mgll MCI mall mgll S.U. mall LC50 001-Silas Wlue 12/31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - Lab Weir 12/31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Silar Weir 1 ULS 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 12/31118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005Upstream 12131118 0 0 005 Da%n tream 11131I18�M 0 0 STORM EVENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): h'IA Water Quality Section Alin: Central Files Permit Sampling Period:= 1617 ,\tali Sersice Center Raleigh, NC 27699-1617 Note: CERTIFICATION S7 ATE1fE\--1' By this signature, I certilIy ' report is accurate and complete to the best of my knowledge. Company information ff„/] Sitar, LLC of 333 teifs L'dd)' Road Signature of Perrnittee or Designee Da a Riegelwood, NC 28456 (910)655-4212 EXT. 100 IfnJj"V �/LQ t fame and'fitic Personnel Collecting Samples: G. Ward Certified laboratories: Emironmental Chemists Environmental Testing Solutions, Inc. ANALI'TICAL RESULTS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of Cox crage No.: NCS000533 Columbus County, North Carolina Lab Ill: 94 lab Ill: 37 00530 00310 00340 00610 00625 00630 00665 77885 50060 71880 01042 01092 01055 01051 00556 004010 Total Total Total Tour Total Non -Polar Acute Date 1SS BOD COD N113 TKN NO3+NO2 Phosphorus Methanol 7RC llcxamtne Formaldehyde Copper 'Lint Manganese Lead O&G pH Tox. Outlall molddl}r mgfl mgfl -RI, mgfl mwl mgn mgfl mgft mgn mgfl MWI cowl MWI and mgll howl s.u. joTAAJIB I.C50 001-Star Whse 1201118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - Lab Weir 17J31/18 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Sitar Weir 12/31118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 . 0 0 DIO 17J31118 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 Upstream 12/31/18 0 0 005Downsueazn 12f3If18 0 0 STORM EYENf CHARACTERISTICS Mail duplicate copies to: Division of Rater Quality Total Event Precipitation (ins.): N!A Water Quality Section Ann! Central Files Permit Sampling Period:= 1617 Mail Sersice Center Raleigh, NC 27699-1617 Note; CERTIFICATION STATEMENT By this signature, I certify this report is accurate and complete to the best of my knolwledge. L I l Company Information Silar, LLC !2 f 333 Neils Eddy Road Signature of Pernutice or Designee D to Riegelwood, NC 28456 (910) 655-4212 EXT. 100 (681� ✓ 1 Print Name and Title Jan 31, 2019 llivision of lrnergy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RI: January 2019 Discharge Monitoring Report To Whom It May Concern: Enclosed are two copies of the January 2019 Discharge Monitoring Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SW001, SWO02, SWO05, and SWO10. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x101 or rward a silar.com. Regards, �e4, zV J- Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com RECEIVED MAR 2 $ 2019 CENTS AL FILES DWR SECTIOI"1 Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. A-NALYTICAI. RFSULTS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of CoNcrage No.: NCS000533 Columbus Counh, North Carolina Lab ID: 94 Lab ID: 37 00530 011310 00340 00610 00625 00630 00665 77885 50060 71990 01042 01092 01055 01051 00556 00400 00300 TWIT Total Total Total Toth Total Non -Polar Acute Date 1'Ss ROD COD NH3 TKN NO3+NO2 Phosphorus \lethanal TRC Hexamine Formaldeh3de Copper Zinc A1sng nese Lead OSG pEI D.o. Tux. Outfall molddl3r mgll mg/l mg11 MWI mgll mg/I MWI mgll mg/I mg/l mg/1 mgll mgfl mg1 MWI mgll U. mg11 LC50 001-Silas Wlue 1/31/19 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002-Lab Weir 1/31/19 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Sitar Weir 1131119 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 010 1/31/19 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 O05llpstream 0 0 005 Domislreatn�1""Lq 119 0 0 STORNI SPENT CHARACTERISTICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.): N°1A Water Quality Section Attn: Central Files Permit Sampling Period: 1617 Mail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION S'1'ATEMENT By this signature, I certify this report ' accurate and complete to the best of my knowledge. ' 1 Company Information Silar, LI-C 333 Neils Eddy Road Signature of Pernutlee or Designee )ate Riegelwood, NC 26456 (910)4555-4212 I /"/C.r'la Yl FAT. 100 Print Name and Titic Personnel Collecting Samples: G. Ward Certified Laboratories: Environmental Chemists Environmcntal Testing Solutions, Inc. ANALYTICAL RESULTS Silar, LLC — STORM WATER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab 1D: 94 Lab ®: 37 00530 00310 00340 00610 0625 00630 00665 77885 50060 71880 01042 01092 01055 01051 00556 00400 00300 TAA313 Total Total Total Tntd Total non -Polar Acute Date TSS BOB I COD N113 TKti NO3+NO2 Phosphorus Methanol TRC lleaamine Formaldehyde Copper Zinc Alsngsnesr Lead O&G pil D.O. Toy. Outlall maiddlyr mWI MWI Mwl me/I mg/l mgll MWI mgll MWI MVI MWI MWI mg11 met mR11 mg71 S.U. mg/l LC50 001-Silar R'hse 1/31119 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 002 - Lab Weir 1131/19 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 005 - Uar Weir V31119 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 0 0 0 010 1/31119 0 0 0 0 0 0 0 0 0 D 0 0 0 0 0 0 0 0 005 Upstream 1131119 0 0 005 Downstream 1131119 0 0 S•I.OPM EYE\ f CIIARACTERISTICS Mail duplicate copies to: Division of Water Quality Total ►went Precipitation (ins.): NIA Water Quality Section Attn: Central Files Permit Sampling Period: 1617 Mail Service Center Raleigh, NC 27699-1617 Note CERTIFICATION STAIFEMEN'T By this signature, I certify this report is accurate and complete to the best of my knowledge. _ Company Informaliau r Sitar, LLC 333 Neils Eddy Road azure of Permiltee or Designee f A. Riegelwood, NC 29456 (910) 655-4212 EX'f. l00 'ice % f A Print Name and Title 1 Mar 4, 2019 Division of Energy, Minerals, & Land Resources ATTN: Central Files 1617 Mail Service Center Raleigh, NC 27699- l 617 RE: February 2019 Discharge Monitoring; Report To Whom It May Concern: Enclosed are two copies of the February 2019 Discharge Monitoring; Report (DMR) for Silar Laboratories under Permit NCS000533 for Outfalls SW001, SW002, SW005, and SW010. If you have any questions regarding this submittal, I can be contacted at (910) 655-4212 x 101 or rward@silar.com. Regards, fl Ci Gina Ward Environmental Health and Safety Silar Laboratories p(910)-655-4212 ext.101 f (910-655-8201) rward@silar.com RECEIVED MAR 2 6 2019 CENTRAL FILES DVVR SECTION Personnel Collecting Samples: P. $usovne Certified Laboratories: Environmental Chemists Environmental Testing Solutions, Inc. ANALYTICAL RESULTS Silar, LLC — STORM W.11TER SAMPLING REPORT Certificate of Coverage No.: NCS000533 Columbus County, North Carolina Lab In: 94 Lab 117: 37 00530 00310 00340 00610 00625 00630 00665 77885 50060 71680 01042 01092 01055 01051 00556 00400 00300 TAA313 Ootfall Date mdddlrr TSS mpfl ROD mrJt COD mpJi M13 mgJt TKN Mg/1- \03+,NO2 mgll Total Phosphoru. mgJl Methanol mgll TRC mpJl llexamine mgll Formaldehyde m mpJl Total Copper mpJl Total 7Anc mpJl Toul sse ng2m mg7 Total Lead mgll Non -Polar O&G MOSM..W. pH D.D. Acute Tox. I.C50 001-Siluwhse 02/11/19 5.4 2 40 0.5 1.-, O.t3 0.30 <5 0,032 05 0[32 0.005 0,035 0.018 <0.01 <5 7.60 NA O07 - 1.ab Weir 02111/19 84 76 174 4.6 14.4 0,43 0.26 <5 0 <25 2.86 0.049 0.352 0.040 <0,01 <5 8.33 NA 005 - Situ Wtir OVI 1/19 40.5 14 93 3.1 7.3 0.42 0.17 <5 0 <25 1.24 0.052 0.416 0.025 <0.01 <5 6.08 NA NA 010 O2l1U19 22,6 >37 124 3.4 7.6 0.28 0.12 <5 0 <25 L61 0029 0,486 0,033 <0OT <5 B.I6 NA Up the Hill (004) 005 Upstream 005 Pom"newil 02/11119 02111/09 NA NA NA NA NA NA NA 01 NA NA NA NA NA NA NA NA NA NA NA NA I NA NA NA STORM EVENT CHARACTF,RiS'rICS Mail duplicate copies to: Division of Water Quality Total Event Precipitation (ins.):FT4-4-1 Rater Quality Section Attn: Central Files Permit Sampling Period: 1617 Nfail Service Center Raleigh, NC 27699-1617 Note: CERTIFICATION STATEMENT By this signature, I certify this repon is accurate and complete to the best of my knowledge. Company Information Silar, LLC `f 1 333 Neils 1, dd%' Road tgnature of Permittee or Designee Date Riegelwood, NC 28456 (910)655-4212 6;'n 4 W4 � � Print Name and Title GJC//� E.XT. 100 I/ �