NCS000391_MONITORING INFO_20200121

Flo
STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
(SIC S V o U
l�
DOC TYPE
❑FINAL PERMIT
A MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
p Juao of �
YYYYMMDD

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000391 SAMPLES COLLECTED DURING CALENDAR YEAR: 2019
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME The Goodvear Tire & Rubber Co.
PERSON COLLECTING SAMPLE(S) Eliiah Herrington
CERTIFIED LABORATORY(S) Microbac Favetteville Division Lab # 11
Part A: Specific Monitoring Requirements (Tier 2 Sampling Event for Zinc)
COUNTY Cumberland
PHONE NO. (_910_) 630-5678
FSIG
NATURE OF PERMITTEE OR DESIGNEE
QUIRED ON PAGE 2.
Outfalt
No.
Date
Sample
Collected
50050
Total
Flow (if app.)
Total
Rainfall
COD, Total
Oil & Grease
Total
Suspended
Solids
Zinc, Total
Thiram
pH, Field
mo/dd/ r
MG
inches
M /I
M /i
M /l
M /I
M 11
S.U.
001
12/18/19
0.3
0.339
6.62
002
!A
cu
L
4 r►�I► �„ ...
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes _X_no
(if yes. complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements NIA
Outfall
Date
50050
00556
00530
00400
Total Flow
Total
Oil & Grease
Non -polar
Total
pH
New Motor
No.
Sample
Collected
(if applicable)
Rainfall
(if appl.)
O&G/TPH
Suspended
Oil Usage
(Method 1664
Solids
SGT-HEM), if
appl.
mo/dd/ -r
MG
inches
m /l
m /l
unit
galimo
Form SWU-247
Page l of 2

STORM EVENT CHARACTERISTICS:
Date 12/18/19
Total Event Precipitation (inches): 0.3
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable —see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh; North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permittee)
l-/a, ze
(Date)
Form S W U-24 7
Page 2 of 2

VMICROBAC@
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9L0370
Project Description
Stormwater Samples - Monthly
For:
Mr. Carlton Williams
Goodyear Tire and Rubber Co.
6650 Ramsey Street
Fayetteville, NC 28311
-� r-o- 1
Administration
Brittany Smith
Friday, January 3, 2020
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further
assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report. Analytical results are
reported on a'as received' basis unless specified otherwise. Analytical results for solids with units ending in (dry) are reported
on a dry weight basis. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be
reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the
samples analyzed as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p j www.microbac.com
Page 1 of 7

6)MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9L0370
Goodyear Tire and Rubber Co. Project Name: Stormwater Samples - Monthly
Mr. Carlton Williams Project 1 PO Number: 8239420885(2019)
6650 Ramsey Street Received: 121i812019
Fayetteville, NC 28311 Reported: 01 /03/2020
Case Narrative
Field pH (by client): 01- 6.62 02-6.5
Sample Summary Report
Sample Name
Laboratory ID
Client Matrix
Sample Type Sample Begin
Outfall #1, Grab
K91-0370-01
Aqueous
Grab
Outfall #2, Grab
K9L0370-02
Aqueous
Grab
Sample Taken Lab Received
12/17/19 09:25 12/18/19 14:40
12/17/19 09:30 12/18/19 14:40
Page 2 of 7

�MICROBAC`
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9L0370
4nalytical Testing Parameters
Client Sample ID: Outfall #1, Grab
Sample Matrix: Aqueous Collected By: Client
Lab Sample ID: K91-0370-01 Collection Date: 12/17/2019 9:25
Wet Chemistry
Result
MDL RL
Units
J�
Dilution Note
Prepared Analyzed
Analyst
Method: EPA 1664 Rev. B
Oil & Grease (HEM)
<5.0
5.0
mg1L
1
12/24119 0900
TBM
Method: SM 2540 D-2011
Total Suspended Solids
<4.17
4.17
mglL
1
12/19/19 1103
MT
Method: SM 4500 H+8-2011
pH at 25 °C
6.9
1.0
S.U.
1 H
12119l19 1321
CLB
Method: SM 5220 D-2011
COD, Total
64.4
10.0
mg1L
1
12/19/19 0911
MT
Metals
Result
MDL RL
Units
Dilution Note
Prepared Analyzed
Analyst
Method: Metals AqueouslEPA 200.7 Rev 4A 1994
Zinc
0.339
0.005
mglL
1
01/02/20 1320 01/02/20 1320
FAY
Client Sample ID: Outfall #2, Grab
Sample Matrix: Aqueous Collected By; Client
Lab Sample ID: K91-0370-02 Collection Date: 12/17/2019 9:30
Wet Chemistry
Result
MDL RL
Units
Dilution Note
Prepared Analyzed
Analyst
Method: EPA 1664 Rev. B
Oil & Grease (HEM)
<5.0
5.0
mg1L
1
12/24/19 0900
TBM
Method: SM 2540 D-2011
Total Suspended Solids
<4.17
4,17
mg1L
1
12119/19 1103
MT
Method: SM 4500 H+B-2011
pH at 25 °C
6.4
1.0
S.U.
1 H
12119/19 1321
CLB
Method: SM 5220 D-2011
COD, Total
47.4
10.0
mg1L
1
12/19/19 0911
MT
Metals
Result
MDL RL
Units
Dilution Note
Prepared Analyzed
Analyst
Method: Metals Aqueous/EPA 200.7 Rev 4.4 1994
Zinc
0.033
0.005
mglL
1
01/02/20 1324 01/02120 1324
FAY
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 7

VM'I.CROBACO
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9L0370
Batch Quality Control Summary: Microbac Laboratories, Inc. - Fayetteville
Wet Chemistry
Spike Source %REC RPD
Result RL Units Level Result %REC Limits RPD Limit Notes
Batch KL91908 - Wet Chem Aqueous - SM 5220 D-2011
Blank (KL91908-BLK1)
Prepared &Analyzed: 12/19/2019
COD, Total
<10.0
10.0
mg1L
Blank (KL91908-BLK2)
Prepared & Analyzed: 1211912019
COD, Total
<10.0
10.0
mglL
Blank (KL91908-BLK3)
Prepared & Analyzed: 12/19/2019
--. _...-- ----- .... ------ ---- -. _ _ .-._.Y.._....-_.._._--- -------
COD, Total
<10.0
10.0
mg/L
LCS (KL91908-BS1)
Prepared &Analyzed: 12/19/2019
COD, Total
493
10.0
mg1L 500 99 90-110
Duplicate (KL91908-DUP1)
Source: 1<91-0350-01
Prepared &Analyzed: 12/19/2019
COD, Total
29.4
10.0
mglL 31.4 7 20
Duplicat---
--------------------------------------
COD, Total
46.4
-.-
10.0
mg1L 48.4 4 20
Matrix Spike (KL91908-MSi)
Source: K9L035M1
Prepared & Analyzed: 12/19/2019
COD, Total
52.4
10.0
mg1L 25.0 31.4 84 80-120
Matrix Spike (KL91908-MS2)
Source: K9L0367-01
Prepared & Analyzed: 12/1912019
COD, Total
69.4
10.0
mg1L 25.0 48.4 84 80-120
Batch KL91921 - Wet Chem Aqueous - SM 2540 D-2011
Blank (KL9i921-BLK1)
Prepared &Analyzed: 1211912019
Total Suspended Solids <2.50
2.50 mg1L
Blank (KL91921-BLK2)
Prepared & Analyzed: 12/19/2019
Total Suspended Solids <2.50
2.50 mg/L
Blank (KL91921-BLK3)
Prepared & Analyzed: 12/19/2019
Total Suspended Solids
<2.50
2.50
mg/L
Blank (KL91921-BLK4)
Prepared & Analyzed: 12/1912019
Total Suspended Solids
<2.50
2.50
m IL
LCS (KL91921-BSi)
Prepared & Analyzed: 12/19/2019
Total Suspended Solids
29.6
2.50
mg1L 31.0 95 94.5-105.4
Duplicate (KL91921-DUP1)
Source: KSL036MI
Prepared & Analyzed: 12/19/2019
Total Suspended Solids
558
2.50
mg1L 548 2 10
Duplicate (KL91921-DUP2)
Source: K91-0368-01
Prepared &Analyzed: 12/19/2019
Total Suspended Solids
70.7
2.50
mg/L 72.7 3 10
Duplicate (KL91921-DUP3)
Source: K91-0403-03
Prepared & Analyzed: 1211912019
Total Suspended Solids
18.0
2,50
mg1L 18.0 0 10
Batch KL92409 - Wet Chem Aqueous - EPA 1664 Rev. B
Blank (KL92409-BLK1)
Prepared & Ana lyzed: 12/24/2019
Oil & Grease (HEM)
<5.0
5.0
mg1L
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 7

()MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9L0370
Spike Source
%REC
RPD
Wet Chemistry Result
RL
Units Level Result %REC
Limits RPD
Limit Notes
Batch KL92409 - Wet Chem Aqueous - EPA 1664 Rev. B
LCS (KL92409-BSI)
Prepared & Analyzed: 12/24/2019
Oil & Grease (HEM) 34.3
5.0
mglL 40.8 84
83-101
Matrix Spike (KL92409-MS1) Source: K91-0368-01
Prepared & Analyzed: 12/24/2019
Oil & Grease (HEM) 39.0
5.0
mglL 45.3 3.4 78
78-114
Spike Source
%REC
RPD
Metals Result
RL
Units Level Result %REC
Limits RPD
Limit Notes
Batch KA00016 - Metals Aqueous - EPA 200.7 Rev 4.4 1994
Blank (KA00016-BLK1)
Prepared & Analyzed: 01/02/2020
Zinc -
<0.010
0.010
mg1L-
Blank (KA00016-BLK2)
Prepared & Analyzed: 01/02/2020
Zinc
<0.010
0.010
mg1L
LCS (KA00016-BSI)
Prepared &Analyzed: 01/02/2020
Zinc
0.241
0.010
mg1L 0.250 96
85-115
LCS (KA00016-BS2)
Prepared &Analyzed: 01/02/2020
Zinc
0.228
0.010
mg1L 0.250 91
85-115
LCS (KA00016-BS3)
Prepared & Analyzed: 01/02/2020
Zinc
0.249
0.010
mg1L 0.250 100
85-115
LCS (KA00016-BS4)
Prepared & Analyzed: 01/02/2020
Zinc
0.243
0.010
mg1L 0.250 97
85-115
Duplicate (KA00016-DUP3)
Source: K91-0382-02
Prepared &Analyzed: 01/02/2020
Zinc
0.032
0.005
mg1L 0.032
2 10
Matrix Spike (KA00016-MS1)
Source: K9L0337-01
Prepared & Analyzed: 01/02/2020
Zinc
0.298
0.005
mglL 0.250 0.017 112
70-130-
Matrix Spike (KA00016-MS2)
Source: K91-0381-02
Prepared & Analyzed: 01102/2020
Zinc
0.283
0.005
mglL 0.250 0.045 95
70-130
Matrix Spike (KA00016-MS3)
Source: K91.0382-02
Prepared & Analyzed: 01/0212020
Zinc
0.271
0.005
mglL 0.250 0.032 96
70-130
Matrix Spike Dup (KA00016-MSD1)
Source: KSL0337-01
Prepared & Analyzed: 01/02/2020
Zinc
0.255
0.005
mglL 0.250 0.017 95
70-130
15 30
Matrix Spike Dup (KA00016-MSD2)
Source: K91-0381-02
Prepared & Analyzed: 01/02/2020
Zinc
0.284
0.005
mg1L 0.250 0.045 95
70-130
0.5 30
Matrix Spike Dup (KA00016-MS03)
Source: K9L0382-02
Prepared & Analyzed: 01/02/2020
Zinc
0.278
0.005
mg1L 0.250 0.032 98
70-130
3 30
Reference (KA00016-SRM1)
Prepared &Analyzed: 01/02/2020
Zinc
1.97
0.010
mg1L 2.00 99
95-105
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 7

�VMICROBAC®
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K9L637Q
Definitions
H: Analyte was prepared andlor analyzed outside of the analytical
method holding time
mg1L: Milligrams per Liter
RL: Reporting limit
RPD: Relative Percent Difference
S.U.: Standard Units
Cooler Receipt Log
Cooler ID: Default Cooler
Temp: 4.6°C
Cooler Inspection Checklist
Ice Present or not required?
Yes
Shipping containers sealed or not required?
Yes
Custody seals intact or not required?
Yes
Chain of Custody (COC) Present?
Yes
COC includes customer information?
Yes
Relinquished and received signature on COC?
Yes
Sample collector identified on COC?
Yes
Sample type identified on COC?
Yes
Correct type of Containers•Received
Yes
Correct number of containers listed on COC?
Yes
Containers Intact?
Yes
COC includes requested analyses?
Yes
Enough sample volume for indicated tests received?
Yes
Sample labels match COC (Name, Date & Time?)
Yes
Samples arrived within hold time?
Yes
Correct preservatives on COC or not required?
Yes
Chemical preservations checked or not required?
Yes
Preservation checks meet method requirements?
Yes
VOA vials have zero headspace, or not recd.?
Yes
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
North Carolina DENR NPDES
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted. n
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated Brittany Smith
in the footnote are present and an authorized signature is included. Administration
Reported: 01/0312020 20:42
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 0f 7

�1
V
Fayetteville Division 2592 Hope Mills Road -- Fayetteville, NC 28306 (910) 864-19201864-87'
CHAIN OF CUSTODY RECORD
1111111, fillillillillillill
PAGE 1 OF 1
CLIENTNAME -&ADDRESS: Po#
Goodyear Tire and Rubber Corhpany
6650 Ramsey Street
Fayetteville, NC 28311
PROJECT/LOCATION:
Goodyear - fa etteville
#
OF
B
O
T
T
L
E
S
TYPE OF
ANALYSIS
PRESERVATION CODE
rn
C7
0
N
CODE: A =. None,
B = HN031(pHc2) + <4°C
C H2504,(pH<2) t <4'C
D =,NaOH + <4°C
E =. ZN: Acetate +:<4°C
F =' HCI
_
CONTACT PERSON:
Elijah Herrington
PHONE:
910-630 -5678
SAMPLER: CUS —'
_
DATE! �+SETHOD OF SHIPMENT:
LAB ID #
SAMPLE TYPE
TIME
COMP
GRAB
pHJ
D.O.
TEMP'C
CHLORINE
outfall # 1
Stormwater
*DATE
f.
' 2
x
x
x
x
x
x
Outfal #2
Stormwater
l�
3
x
x
x
x
x
x
Relinquished by:
Date
Time
RCcci y: { [gnat
Date
Time
Gri1� 1
r
z
,Z- 8 1
S-50
Relinq ed b
3
Date
jZ19-1q
Time
R Ived by: tSignature
4eceiVed4
Date
l Gl
Time , �Q
rt
Relinquished by:
Date
Time
by: {Signature)
Date
Time
b
8
Comments or Special Hazards:
REVIEWED
Page 7 of 7