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Home My WebLink AboutNCS000373_COMPLETE FILE - HISTORICAL_20200128Mf E�. , -- • -• ---STORMWATER DIVISION CODING -SHEET - ..., ....,,;_ RESCISSIONS ------------ PERMIT N0. N � S DC) -,>-73 DOCTYPE 1� COMPLETE FILE- HISTORICAL DATE OF RESCISSION ❑ YYYYMMDD STORiMWA"TER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit ,Number NCS 000373 FACILITY NAME _Michelin Aircraft Tire Company. PERSON COLLECTING SAMPLE(S) Chris Crisler CERTIFIED LABORATORY(S) Pace Analytical Lab # PASI-C Pace Analytical_ _ Lab # PASI-A Part A: Specific ,Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2020 ("This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Stanly PHONE NO. 7( Q4 ) 474-7777 SIGNATURE OF PERM ITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall No. Date Sample Collected 50050 Total Flow if a Total Rainfall Oil &Grease pH COD ��oo l.. ` 1.% rn mo/ddl -r MG inches 117q I L to '+ SDO1 117120 NIA .10 D 6.49 D ` SDO 2 117120 NIA .10 ND 7.31 40.3 t'L NTRA Roof above cu 117120 NIA .10 ND 6.74 31.1 uV'vFi , F '7n� Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ()yes ®no (if yes, complete Part B) Part B: Vehicle Maintenance Activity MonitoringRe uirements Outfall No. Date Sample; "" Collected 50050 00556 00530 00400. Total Flow `' (if applicable)' Total' Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH-. (Method 1664 SGT-HEM); if appl. Total Suspended Solids pH New Motor Oil Usage. mo/dd/vr MG inches mg/1 m /l unit gal/mo Form SWU-247. last revised 61121 015 Pa<ae 1 of STORM EVENT CHARACTERISTICS: Date 1 /7/2020 Total Event Precipitation (inches): A 0 inches Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) iMail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 0� C4� A;;2L 1 /23/20 (Signature of Pe it e) (Date) Form SWU-247. Iasi revised 611 12015 Page 2 of 2 aceAnalytical www.pacalab3.com January 22, 2020 Chris Crisler Michelin Aircraft Tire Co LLC 40584 S Stanly School Rd Norwood, NC 28128 RE: Project: Winter 2020 Sample Pace Project No.: 92459914 Dear Chris Crisler: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 09, 2020. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, VC9(. fP�"rk-,�� Amanda Payne amanda.payne@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Heather Ashby, Michelin Aircraft Tire Co LLC REPORT OF LABORATORY ANALYSIS This report shah not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 12 lacieAnalyfical"' www.pacete6a. am Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Nuntersville, NC 28078 (704)B75-9092 CERTIFICATIONS Project: Winter 2020 Sample Pace Project No.: 92459914 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Nuntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E8764B Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 12 acmnalytical www.paceletrs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersviiVe, NC 28078 (704)875-9092 Project: Pace Project No.: Winter 2020 Sample 92459914 Analytes Lab ID Sample I❑ Method Analysts Reported Laboratory 92459914001 SDO #1 EPA 1664B HH 1 PASI-C FPA 2003 Rev 4A 1994 IDS 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92459914002 SDO #2 EPA 1664E HH 1 PASI-C EPA 200.7 Rev 4.4 1994 DS 1 PASI-A SM 5220D-2011 MDW 1 PASI-A 92459914003 Roof Above Curing EPA 200.7 Rev 4.4 1994 IDS 1 PASI-A SM 5220D-2011 MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 12 laceAnalyfical" MMM.48CW3h&C0M ANALYTICAL RESULTS Project: Winter 2020 Sample Pace Project No.: 92459914 Pace Analytical Servicos, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: SDO #1 Lab ID: 92459914001 Collected: 01/07/20 11:00 Received: 01/09/20 09:13 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg1L 10.2 1 01/21/20 16:19 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Zinc 62.7 ug/L 10.0 1 01/14/20 01:31 01/15/20 17:25 7440-66-6 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 01/14/20 20:05 01115/20 00:45 Sample: SDO #2 Lab ID: 92459914002 Collected: 01/07/20 10:53 Received: 01/09/20 09:13 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 10A 1 01/21/20 16:20 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Zinc 210 ug1L 10.0 1 01/14/20 01:31 01/15120 17:28 7440-66-6 52200 COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 40.3 mg/L 25.0 1 01/14120 20:05 01/15/20 00:45 Sample: Roof Above Curing Lab ID; 92459914003 Collected: 01/07/20 11:10 Received: 01/09/20 09:13 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Zinc 242 ug/L 10.0 1 01/14/20 01:31 01/15/20 17:31 7440-66-6 52200 COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 31.1 mg1L 25.0 1 01/14/20 20:05 01115/20 00:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01122/2020 08:31 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 12 aceAnalytrcal e +wtvw.pacelabli,c m QUALITY CONTROL DATA Project: Winter 2020 Sampie Pace Project No.: 92459914 QC Batch: 520571 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92459914001, 92459914002 METHOD BLANK: 2785369 Matrix: Water Associated Lab Samples: 92459914001, 92459914002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mglL ND 5.0 01121/20 16:12 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)575-9092 LABORATORY CONTROL SAMPLE: 2785370 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oii and Grease mglL 40 36.8 92 78-114 MATRIX SPIKE SAMPLE: 2785371 2627985003 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mglL ND 38.5 27.4 71 78-114 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/22/2020 08:31 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 12 (�Ia'neAnalj4icaf' WWW.pacelabs.corn QUALITY CONTROL DATA Project: Winter 2020 Sample Pace Project No.: 92459914 QC Balch: 519121 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 2007 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92459914001, 92459914002, 92459914003 METHOD BLANK: 2778740 Matrix: Water Associated Lab Samples: 92459914001, 92459914002, 92459914003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Zinc ug/L NO 10.0 0111512018:41 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2778741 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Zinc ug/L 500 442 88 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2778742 MS 92459859001 Spike Parameter Units Result Conc. Zinc ug/L 67.3 500 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2778744 MS 92459904001 Spike Parameter Units Result Conc. Zinc ug/L 0.065 500 mg1L 2778743 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % ReC % Rec Limits RPD 500 538 552 94 97 70-130 3 2778745 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 585 553 104 98 70-130 6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01122/2020 08:31 AM without the written consent of Pace Analytical Services, LLC, Quat Qual Page 6 of 12 aceAnalytical tt wK.Pacelabs.c= QUALITY CONTROL DATA Project: Winter 2020 Sample Pace Project No.: 92459914 QC Batch: 519129 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples. 92459914001, 92459914002, 92459914003 Pace Analytical Services, I.LC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 METHOD BLANK: 2778780 Matrix: Water Associated Lab Samples: 92459914001, 92459914002, 92459914003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mglL ND 25.0 01/15/20 00:35 LABORATORY CONTROL SAMPLE: 2778781 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 753 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2778782 2778783 MS MSD 92460296001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 3840 100 100 4050 3990 203 146 90-110 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2778784 2778785 MS MSD 2627316002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Resuft % Rec % Rec Limits RPD Qual Chemical Oxygen Demand Ing/L 83.8 100 100 185 244 101 161 90-110 28 M1,R1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /22/2020 08:31 AM without the written consent of Pace Analytical Services, L-C. Page 7 of 12 laneAnalyfical' WWW.paeellbs.cam QUALIFIERS Project: Winter 2020 Sample Pace Project No.: 92459914 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Hun:ersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and Was for a specific analyte in a specific matrix. S. - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 C h loroethyl vinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. W_I:Id:7Vti1ZTr*9 PAS1-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /22/2020 08:31 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 12 (�IaclMnalXical* trmr.patalabs.tom QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Winter 2020 Sample 92459914 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92459914001 SDO #1 EPA 1664B 520571 92459914002 SDO #2 EPA 1664B 520571 92459914001 SDO #1 EPA 200.7 Rev 4.4 1994 519121 EPA 200.7 Rev 4.4 1994 519137 92459914002 SDO #2 EPA 200.7 Rev 4.4 1994 519121 EPA 200.7 Rev 4.4 1994 519137 92459914003 Roof Above Curing EPA 200.7 Rev 4.4 1994 519121 EPA 200.7 Rev 4.4 1994 519137 92459914001 SDO #1 SM 5220D-2011 519129 SM 5220D-2011 519383 92459914002 SDO #2 SM 5220D-2011 519129 SM 5220D-2011 519383 92459914003 Roof Above Curing SM 5220D-2011 519129 SM 52201)-2011 519383 Date: 01/22/2020 08:31 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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