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HomeMy WebLinkAboutNCS000370_COMPLETE FILE - HISTORICAL_20191204-- -----STORMWATER DIVISION CODINGSHEET- RESCISSIONS. PERMIT NO. DOC TYPE COMPLETE FILE -HISTORICAL DATE OF RESCISSION El WYYMMDD November 22, 2019 North Carolina Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 BRIDGESTONE AMERICAS TIRE OPERATIONS, LLC Wilson Plant P.O. Box 1139 Wilson, North Carolina 27894-1139 RECEIVED DEC, 04 2019 ct--" , + ., ,L- r' i i-fry Dlh/r SECTION Re: Storm water Sampling Year 10, Period 1 Analytical Results Dear Sir or Madam: The BATO-Wilson facility operates under National Pollutant Discharge Elimination System (NPDES) permit number NCS000370. The permit requires semi-annual quantitative sampling of storm water at the facility's two outfalls. The outfalls are named by their geographic locations, South and East. Please find the analytical results and Storm Water Outfall Discharge Monitoring Reports for the Sampling Year 10 Period 1 for the South and East outfalls in the Attachment. The samples were collected on November 11, 2019. The analytical results were received from the laboratory via electronic mail at BATO Wilson on November 21, 2019. As required, the original and one copy are enclosed. If you have any questions concerning this report, please contact Tausha Fanslau at (252) 246-7485, Sincerely, 4_ll Norrod Plant Manager BATO — Wilson Plant cc: BATO Wilson Environmental Department p:\My Documents\Water-Stormwater\Files19 STORNIWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS 000370 FACILITY NAME Bridgestone Americas Tire Operations, LLC PERSON COLLECTING SAMPLE(S) Tausha Fanslau CERTIFIED LABORATORY(S) Pace Analytical Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 2019 (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Wilson PHONE NO ( 252_)246-7485 SIGNATURE OF PER.MITTEE OR DESIGNEE REQUIRED ON PAGE 2. Outfall _. No Date Sample Collected. Total 'Flo�r�(if aAp+) Total Raka 11 ZINC ; {t) , _ COD TSS., -6 TRH - y KPH , a "' 'm6/ddlvr�' . 1VIG , -`. inches _ 11 /Lt MaIL-R East 11/12/2019 0.47 0.0246 <25 4.7 < 5 6.4 South 11/12/2019 0.47 0.154 <25 48.5 5.0 6.2 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Ouifall Date - 50 500-�,� ;00556 :�,;; _QU530 ' -No 5 Sam le F- Sa A [Total?FIoH- _ -_Total`s.' $Oily& Greas` a �Nori polar ' "Total ; " ;p H ` 1 ' ' 6 1 1\ew 1liotor Cord; if a Ii aC ble '(z Pp �..� ,Rainfall 3 ( �f�a I: } &GITPH !Nuspended=� .� r � �UiFusage z :" ,�.: :. - y Epp s�,u� s�Iethod1664 f 9Solids ,r r k r>� SGT-HEM), if 7 r a.,�_ hr' .inchEii4 iri/1 ..ml ._ i.n cat/ o� Form SWU-247, last revised 21212012 Pagel of 2 STORM EVENT CHARACTERISTICS: Date 11/12/2019 Total Event Precipitation (inches): 0.47 Event Duration (hours): 4.0 (only if applicable — see permit.) (if more than one storm event was sampled) Mail Original and one coAy to: Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh. North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee) fl�� (Date) Form SWU-247, last revised 21212012 Page 2 of 2 aceAnalXical® (�www.pacelehe.com November 21, 2019 Tausha Fanslau Bridgestone Americas 3001 Firestone Parkway Wilson, NC 27893 RE: Project: Stormwater Sampling Pace Project No.: 92453778 Dear Tausha Fanslau: Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 14, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Amanda Payne amanda.payne@pacelabs.com (704)875-9092 Project Manager Endosures REPORT OF LABORATORY ANALYSIS This repot shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 1 of 15 acmnalyii{cal www.pacdtbt.com CERTIFICATIONS Project: Stormwater Sampling Pace Project No.: 92453778 Pace Analytical Services Charlotte Pace Analytical Services, LLC 9800 KincoyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 9800 Kincey Ave. Ste 100. Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87048 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalytical WWW.pacalabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 KirceyAve. Suite too HuntersvOle, NC 28078 (704)875-9092 Project: Pace Project No.: Stormwater Sampling 92453778 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92453778001 SOUTH EPA 1664E HH 1 PASI-C EPA 200.7 Rev 4A 1994 KQ 1 PASI-A SM 254OD-2011 CJL 1 PASI-A EPA 9040C ECH 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92453778002 EAST EPA 16649 HH 1 PASI-C EPA 200.7 Rev 4.4 1994 KQ 1 PASI-A SM 254OD-2011 CJL 1 PASI-A EPA9040C ECH 1 PASI-A SM 522OD-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 15 lacieAnalyfical wvrw.pacalaha.ca I ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Sampling Pace Project No.: 92453778 Sample: SOUTH Lab ID: 92453778001 Collected: 11/12/19 13:10 Received: 11/14/19 09:04 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons 5.0 mglL 4.8 1 11/20/19 15:17 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4A 1994 Zinc 154 uglL 10.0 1 11/16/19 12:39 11/18/19 06:29 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 48.5 mglL 12.5 1 11/18/19 18:56 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.2 Std, Units 0.10 1 11/17/19 14:50 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mglL 25.0 1 11/19/19 16:37 11/19/19 23:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/21/2019 08:20 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 15 (�Ia'neAnalyticale xrru.prlc1lab3X= ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Stormwater Sampling Pace Project No.: 92453778 Sample: EAST Lab ID: 92453778002 Collected: 11/12/19 13:30 Received: 11/14/19 09:04 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 4.8 1 11/20/19 16:17 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4A 1994 Zinc 24.6 uglL 10.0 1 11/16/19 12:39 11/18/19 06:33 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 4.7 mg/L 2.5 1 11/18/19 18:57 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.4 Std. Units 0.10 1 11/17/19 14:55 H3 52200 COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 11/19/19 16:37 11/19/19 23:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/21/2019 08:20 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 15 to aceAnalytical xr+P.pacil,111 .cons QUALITY CONTROL DATA Project: Stormwater Sampling Pace Project No.: 92453778 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 OC Batch: 510729 - Analysis Method: EPA 1664E QC Batch Method: EPA 16646 Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92453778001, 92453778002 LABORATORY CONTROL SAMPLE: 2739945 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 22.1 110 64-132 MATRIX SPIKE SAMPLE: 2739946 35510490004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 51.4 19.6 88.9 192 64-132 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/2112019 08:20 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 15 IeAnalytical www.pacidibi am Project: Stormwater Sampling Pace Project No.: 92453778 QC Batch: 509903 QC Batch Method: EPA 200.7 Rev 4.4 1994 Associated Lab Samples: 92453778001, 92453778002 METHOD BLANK: 2736512 Associated Lab Samples: 92453778001, 92453778002 Parameter Units Zinc uglL LABORATORY CONTROL SAMPLE: 2736513 Parameter Units Zinc uglL Pace Analytical Services, LLG 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 10.0 11/18/19 05:07 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 500 478 96 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2736514 2736515 MS MSD 92452973001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Zinc uglL 153 500 500 619 640 93 97 70-130 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2736516 2736517 MS MSD 92453397008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Zinc uglL 0.23 500 500 ' 733 715 101 98 70-130 2 mg/L Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/21/2019 0820 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 15 aceAnalytical wwrr.paedrtbs.citrs QUALITY CONTROL DATA Project: Sturmwater Sampling Pace Project No.: 92453778 QC Batch: 510251 Analysis Method: SM 2540D•2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92453778001, 92453778002 METHOD BLANK: 2737978 Matrix: Water Associated Lab Samples: 92453778001, 92453778002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 11/18/19 18:51 Pace Analytical Services, LLG 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2737979 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 234 94 90-110 SAMPLE DUPLICATE: 2737980 92453632001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 44.9 51.7 14 SAMPLE DUPLICATE: 2737981 92453776004 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 40.2 39.4 2 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/2112019 08:20 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 15 (�15'neAnalyficalo www.pacttlah.com QUALITY CONTROL DATA Project: Stormwater Sampling Pace Project No.: 92453778 QC Batch: 509994 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92453778001, 92453778002 SAMPLE DUPLICATE: 2736835 92452727001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 7.9 7.7 2 H3 SAMPLE DUPLICATE: 2736836 Parameter pH at 25 Degrees C 92453279001 Dup Units Result Result Std, Units 5.9 5.4 RPD Qualifiers 8 H3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/21/2019 08:20 AM without the written consent of Pace Analytical Services, LI-C. Page 9 of 15 Pace Analytical Services, LLC aeeAnalytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 xww•P+tuatss.ton (704)875-9092 QUALITY CONTROL DATA Project: Stormwater Sampling Pace Project No.: 92453778 QC Batch: 510477 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 52201) COD Associated Lab Samples: 92453778001, 92453778002 METHOD BLANK: 2738904 Matrix: Water Associated Lab Samples: 92453778001, 92453778002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L ND 25.0 11/19/19 23:16 LABORATORY CONTROL SAMPLE: 2736905 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mglL 750 757 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738906 2738907 MS MSD 92453323001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL ND 100 100 106 103 143 101 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738908 2738909 MS MSD 92453776001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 327 100 100 444 444 118 118 90-110 0 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11121l2019 08:20 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 15 aceAnalyticalm www.pscdsbs,com QUALIFIERS Project: Stormwater Sampling Pace Project No.: 92453778 I014SI:iifro] :l-'3 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)B75-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260, N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. Mi Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in Full, Date: 11121 /2019 08:20 AM without the written consent of Pace Analytical Services, I.I.C. Page 11 of 15 laceAnalytical. www.pacalahs.cara QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Sampling Pace Project No.: 92453778 Lab ID Sample ID QC Batch Method QC Batch 92453778001 SOUTH EPA 1664B 510729 92453778002 EAST EPA1664B 510729 92453778001 SOUTH EPA 200.7 Rev 4.4 1994 509903 92453778002 EAST EPA 200.7 Rev 4.4 1994 509903 92453778001 SOUTH SM 254OD-2011 510251 92453778002 EAST SM 254OD-2011 510251 92453770001 SOUTH EPA 9040C 509994 92453778002 EAST EPA 9040C 509994 92453778001 SOUTH SM 5220D-2011 510477 92453778002 EAST SM 5220D-2011 510477 Date: 11121/2019 08:20 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Analytical Method Batch EPA 200.7 Rev 4.4 1994 509934 EPA 200.7 Rev 4A 1994 509934 SM 5220D-2011 SM 5220D-2011 510531 510531 Page 12 of 15 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Rece�tjscuiiij Page 1 of 2 Document No.: Issuing Authority: uii+$r4fl$�jCA� F-CAR-a-033-Rev.06 Pace Caroilnas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh !f Meechanicsville❑ • Client Name: i b110V 02453778 78 . PraJect Af• Courier: Fed Ex UPS us PS — CNent ! 1110iI! ❑ Commercial JDPace [Others ' 92483778 Custody SeatPresent7 ❑Yes �ZNo• sealslntact7 []Yes QW, Date/initla Is Person Examining Contents: W II / /4 Packing Material: []Bubble Wrap • ❑Bubble Bag_ s Z]None ❑ other Biological Tissue Frozen? Thermometer, ❑Yes ❑No ZN/A AIR Gun iD: gr M� Type of ice: AWat []Blue ONana Cooler Temp rQ 0.3 Correction Fact u ) _ C Temp should be above freezing to 6'C Cooler Temp Corrected ('C): ' 0.3 Qsamples out of temp criteria. Samples on Ice, cooling process has begun USDA Regulated Soil (® N/A, water sample) Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Yes No Did samples originate from a foreign source (internationally, Ineludlfw Hawn II and Puorm RIcn1? MYes FlNo, Comments/Discrepant Present? Yes No N/a 1.rrived within Hold Time? Y. No NIA 2- Eofrustodyustody Time A,tal ls <72. hr.)? es No N/A 3. Around Tlme Re uested? Yes No NIA 4. Valume7 Yes Ma N A 5. ntainers Used?JYes ontainers Used? es ❑Nn EINo ❑N/A N/A 6. Containers Intact? 14Yes oNo N/A 7. Dissolved analysis: Sam les Field Filtered? QYei Na XqLA 6: Sample Labels Match COC? includes Date/Time/ID/Analysis Matrix: Wes [:]No []NIA 9. Heads ace In VOA Vials (>S-6mm)? QYes. Na gNJA 10. Trip Blank Present? . Trip Blank Custody Seals Present? E]Yes OYes ❑No No /A /A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No Lot ID of split containers: CUENTNOTiFICATION/RESOLUTION - — Person contacted: Date/Time: Project Manager SCURF Review: Project Manager SRF Review: Date:, I 1 { 4i 11� + _ Data: I Page 13 of 15 • I1 6 7 8 10 12 Document Name, Document Revised: February 7, 2018 An,h�� sample Condition Upon Remlpt(SCUR) Page 1 of 2 ! - Ce�a1ICa� Document No.: Issuing Authority: F CAR-CS-033-Rev.06 Pace Carolinas Qua(4 Office "Check mark top half of box If pH and/or dechlorination Is verified and within the acceptance range for preservation samples: Exceptions: VOA, Collform, TOC, Ofl and Grease, DROJW15 (water) DOC, Lift "Bottom half of box Is to list number of bot tie rr= 924537�78�: Project � ; wo PM: AP' Due Date: '11Y21/I8 CLIENT: 92-BFUSA V _z a4 �L i° 2 m z c r c Z z ° a Q z, 2s v g�� rg pp r a 1�� 2ry 4 �� o u u V � y u .G ? T `� E JZ N 61 2 j, L G u ' z S q 91 e a. 06 n a. F9 u7 ry pp 9. ,� j ❑ O ? > a Pt E d. n o E E E E a a E E E E E E E e v E g $ mI�wtl _ rn 0 d 3 4 a 6 a 3 i? l9 l7 t7 C�7 L l7 m m m CO m in m do •\ i i t PH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH span receipt Date presarvation adjusted Time preservation adjusted Amount of Proservativa added int p Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form WIN tie sent to the North Carolina DEHNR Certtticatlon Uttke (Le. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 14 of 15 ■ Jp CHAIN -OF -CUSTODY ! Analytical Request Document o The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must he completed a rately. Ln 5ec:ioo a 1 sections Section C M Requir4d Calm* 4110MQrien: RagrArad Frayed beanTadierk kwoioe inloetrntioa: P e : 1 Qf 1 d ,CWPeI . aridpWom Americas RePDrtToc TaushaFarsstau Address: 3001 Fireswm Pmkway Copy To: Wilson, HC 27893 Emslt; ccM Purchase Order it 'Phcnc 252y246-7485 Fac Prciw Narm. st mrimm er Regxstad Due DOm. Prapa A 2 'rramcr CODE C Dftt:o wr am� Wage WT $ rf wae.ry * ww y2 SAMPLE ID ° a s °a START O V C One haracW Per boa. VW" WP pr M PA 5arrrple Ws> bo iffftT"W is as LU '= DATE T SOUT, uuTi, EAST yyT l>.�i5 1. 0-1 x o _ crt w O � 2 END d-i g '� IL z O1 omo � T = = Z Z 6 $ o IXF O .t! l". II��II>iJ1KLEMlFWYCj 7i///////= �"�—RfMlLfiRECRIM � EL.wa�� '':: a—�x��cs:::.;�c:rr:�..._;-:?•�.==e:::�;•;� izw�: ��r."3ri+!? ^�x''.� <�'.P,1''+"�"i�::'=�Yi?:� r c PW" Macn or S"PLER: LL` �Ci i.L�TtCi 1� �Yl S a h e o. St[3MAWRE d SWP DATE Signed: e z z z .,�_O ftjf�il�i ��Y fig, T>