NCS000315_MONITORING INFO_20200122

M-12/0
STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
/"VC
DOC TYPE
❑FINAL PERMIT
MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ ji,- w 0
YYYYMMDD

dp UnivarSolutions
.January 9, 2020
NC DEQ
Division of Energy Mineral and Land Resources
Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Semi -Annual Storm Water Sampling Results for 2019 Period 2
Univar Solutions USA Inc.
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
To Whom It May Concern:
JA N 2 2 2020
b `c;L-C
�J SrZ
Univar Solutions USA Inc. conducted the semi-annual analytical monitoring event for 2019 Period
2 at the facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, !North
Carolina, on December 17, 2019, as prescribed in the National Pollutant Discharge Elimination
System (NPDES) stormwater permit (NCS000315). Per the requirements, the stormwater sample
was collected from the storm water discharge outfall (SDO) 001 during a measurable storm event
that consisted of 1,5 inches of total rainfall, as measured by the onsite rain gauge. The previous
measurable storm event was at least 72 hours prior.
Enclosed is one signed original and one signed copy of the Discharge Monitoring Report (DMR)
for the 2019 Period 2 sampling event. The permittee recorded the required qualitative monitoring
observations on the SDO Qualitative Monitoring Report form, which will be retained on site.
Should you have any questions or require additional information, please contact me at 704-391-
6877.
Sincerely,
Univar Solutions USA Inc.
r
Timothy Nightwine
Facility Manager
Enclosure
cc: Ana Mauricio, Univar Solutions
Univar Solutions 1 3 Waterway Square Place, Suite ioo0 1 The Woodlands, Texas 77380 1 USA

STORMWAITH DISCIIARGE QUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000315
FACILITY NAME Univar Solutions USA inc.
PERSON COLLECTING SAMPLE(S) Jeff Strickland, Anlea Group
CERTIFIED LABORATORY(S) EuroTins TestAmerica U, b g 269
Lab 4
Part A: Specific -Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2019
(This monitoring report shall he received by the Division no later than 30 days front
the date the facility receives the sampling results from the laboratory.)
COUNTY Mecklenbur
PRONE NO. 7(_ 04_ ) 391-6877
SIGNATURE OF PERMITTEE OR DESIGNEI:
REQUIRED ON PAGE 2.
----------
----------
----------
----------
----------
----------
----------
----------
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Dyes r@no
(ifycs. complete Part B)
Part U: Vehicle Maintenance Activitv Monitorin! Requirements
Outlall
No.
Date
Sample
Collected
50050
00556
100530
00401)
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non-pular
O&G/TPli
(,Method 1(A4
SGT-III?M), if
at 1.
Total
Suspended
Solids
pll
New Ntutor
Oil usage
moldEXr
MG
inehcs
Um/l
nt n
unit
allmo
Form SWU-247, Iasi revised 611212015
Page I of 2

STORM EVENT CHARACTERISTICS:
Date 12/17/19
Total Event Precipitation (inches): 1.5
Event Duration (hours): (only if applicable —set permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Evcnt Duration (hours): (only ifapplicable--see permit.)
Mail Original and one copy to:
Division of Energy Mineral and Land Resources
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or, supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. (lased on my inquiry of the person
or persons who manage the system, or (hose persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."_; 7�0�; -7, e�
l�
(Signature Pern uee) (Dale)
Form SWU-247, lusr revised 611212015
Page 2 ol''_

I. Outfall Description:
Outfall No. SDO 001 Structure (pipe, ditch, etc.): Pipe
Receiving Stream: City of Charlotte MS4 and Stewart's Creek
Describe the industrial activities that occur within the outfail drainage area:. Located_near_truck
containment area. but accepts drainage from operational areas near truck scale, parking, and near
hazardous waste storage areas
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Clear, no significant tint or additional discoloration
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.):_ TheEee was no odor associated with the outfall discharge.
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
O2 3 4 S
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and S is the surface covered with floating solids:
O2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
O2 3 4 S
7. Is there any foam in the stormwater discharge? ❑ Yes ® No
8. is there an oil sheen in the stormwater discharge? ❑ Yes ® No.
9. is there evidence of erosion or deposition at the outfail? ❑ Yes ® No.
1.0. Other Obvious Indicators of Stormwater Pollution:
List and describe:_ There were no obvious indicators of stormwater pollution during the
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017 -revised by EHS Support 03/27/19

Environmental
Quality
Stormwater Discharge Outfall (SDO)
Semi -Annual Qualitative Monitoring Report
Forguidance on filling out this form, please visit htt(.nc,gov�about/divisions/energy-mineral-land-
resourceslenergy-mineral-land ep rmits/stormwater ep rmitsjnndes-industrial-sw#tab-4
Permit No.: 3 /I/ 5/
Facility Name: Univar Solutions
County: Mecklenburg _
Inspector Name, Title, and Company: _Mr. Jeff Strickland. Staff Professional, Anteil Group
Phone No. 704-324-7033
Date and Time of Inspection:___1.2117/2019 HAS
Attach photograph ofoutfall.
Total Event Precipitation (inches): 1,5 (source is on -site rain gauge).
Sample Location: SDO 001
Time of Sample Collection:] _ 09:15
Field Parameter for pH: 7,Q7r H
Analytical Monitoring Requirements: TSS. COD. pH
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DEMLR Regional Office.
By this signature, I certify that this report is accurate jand complete to the best of my knowledge:
[S
ittee or Designee]
' Grab samples shall be collected within first 30 minutes of discharge.
Pagel of 2
SWU-242, Last modified 07/28/2017 -revised by EHS Support 03/27/19

1. Outfall Description:
Outfall No.� SDO 001 Structure (pipe, ditch, etc.): Pipe
Receiving Stream: City of Charlotte MS4 and Stewar_t's_Cr_e-gk
Describe the industrial activities that occur within the outfall drainage area: Located near truck
containment area but accepts drainage from operational areas near truck scale, Parking, and near
hazardous waste storage areas
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Clear, no significant tint or additional discoloration
3, Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weals chlorine odor, etc.); There was no odor associated with the outfall discharge.
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
0 2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
O2 3 4 5
5. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
O2 3 4 5
7. Is there any foam in the stormwater discharge? ❑ Yes ® No.
8. is there an oil sheen in the stormwater discharge? ❑ Yes ® No.
9. Is there evidence of erosion or deposition at the outfall? ❑ Yes ® No.
10. Other Obvious indicators of Stormwater Pollution:
List and describe: There were no obvious indicators of 5torrnwater pollution -during the
sampling event.
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017 -revised by EHS Support 03/27/19

10
Location zJ5L f,—j C- . rEk pate 0- 7Z/q
Project / Client
y
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61

Tisri-
nor -
M@-B ©ueea C1i1 t�r3ue
Charlailke, 8C 28280
Phone: [phone] Fax:
t�
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C
Chain of Custody Record 2 5 5 4 a. u TestAmenca
I44
THE LEADER IN ENVIRONMENTAL tES7l14G l
TestAmerica Laboratories, Inc. 1
Regulatory Program: ❑Dw ❑NPDES ❑RCRA ❑Other: TAL-8210(0713)
- Client Contact
Project Manager: r;,. ?
Site Contact: ••`` i .r_ _4 _
H
Date: j } i f f `I
COC No:
Company Name: G 11 1 „ _,,,,,,—}
Tel/Fax: ZT710 _T-," ZJ _ ! �T y 7
Lab Contact: r
Carrier.
I of ! COCs
Analysis Turnaround Time
i
o
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,�
Z
}
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``"
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Sampler:
iCity/State/Zip: V) _ _ ` ''_ (f_ ' i I,
❑ CALENDAR DAYS ❑ WORKING DAYS
For Lab Use only:
Walk-in Client:
Lab Sampling:
?hone: 4 q
TAT it different from Below
❑ 2 weeks
©,_ I week
❑ 2 days
❑ Iday
Fax'.
Project Name: hf
site: s . v' Cr
Job 1 SDG No.:
PC#
1
i
.4
Sample Identification
Sample
Date
Sample
Time
Sample
IC�ComA. ' Type
GwGmb)
Matrix
F or
cant"
Sample Specific Notes:
J _
•-
t
k
Preservation Used: 1= Ice, 2= HCl; 3-- H2SO4; 4=HNO3; 5=NaOH; 6= Other
Li
i
Possible Hazard Identification:
.Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the
Comments Section if the lab is to dispose of the sample.
Sample Disposal (A tee may be assessed if samples are retained longer than 1 month)
❑ Retum to Client QDisposal by Lab ❑ Archive for Months
IQNcn-Hazard ❑ Flammable ❑ Skln Irritant ❑ Poison 8 ❑ Unknown
,Special Instructions/QC Requirements & Comments:
.J 1 / i _ �! i �: �✓':.y � r-:.. _mil r
1
f
Custody Seals intact: ❑ Yes 0 No Custody Seal No.: CODlEI Tamp. (C); ObS d.
linquished by Company: Datemme: Received by:
— !
eiinquished by: r" 11 1 � �t 1
Com a ' -rr:?: f/S[ - -)(I\ �i�l! t 1
'— p Company., Date/Time: Received by:
2elinquished by: Company: Date/Time: Received in Laboratory by:
f
COh'd. Therm 10 No.: r
r
Company,,
P y Date/Time: t
Company: Datemme:
Compan Y Date/Time:

urofins
Environment Testing
TestAmerica
ANALYTICAL REPORT
Eurofins TestAmerica, Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-178425-1
Client Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
For:
EHS Support, LLC
30475 Middle Creek Circle
Daphne, Alabama 36527
Attn: Amy Bauer
Authorized for release by:
11712020 3:54:45 PM
Sheila Hoffman, Project Manager II
[phone]
[e-mail]
Designee for
Jerry Lanier, Project Manager 1
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TN! requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: EHS Support, LLC Laboratory Job ID: 680-178425-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3
Sample Summary .........................................
4
Method Summary ...........................................
5
Definitions/Glossary.......................................
6
Detection Summary ........................................
7
Client Sample Results ......................................
8
QC Sample Results ........................................
9
QC Association Summary ...................................
11
Lab Chronicle ............................................
12
Chain of Custody ..........................................
13
Receipt Checklists .........................................
14
Certification Summary .......................................
15
Eurofins TestAnnerica, Savannah
Page 2 of 15 1/7/2020

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Job ID: 680-178425-1
Laboratory: Eurofins TestAmerica, Savannah
Narrative
Case Narrative
CASE NARRATIVE
Client: EHS Support, LLC
Project: Nexeo - Charlotte, N.C. (Outfall 001)
Report Number: 680-178425-1
R]
Job ID: 680-178425-1 .
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 12/1812019'. the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.9 C.
TOTAL. SUSPENDED SOLIDS
Sample SDO-001 (680-178425-1) was analyzed for total suspended solids in accordance with SM 25400. The samples were analyzed on
12/24/2019,
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHEMICAL OXYGEN DEMAND
Sample SDO-001 (680-178425-1) was analyzed for chemical oxygen demand in accordance with SM 52200. The samples were analyzed
on 12/30/2019.
Chemical Oxygen Demand failed the recovery criteria low for the MS of sample SDO-001 MS (680-178425-1) in batch 680-602675.
Refer to the QC report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample SDO-001 (680-178425-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were analyzed on
01 /0612020.
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins TestAnnerica, Savannah
Page 3 of 15 1/7/2020

Sample Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
680-178425-1 SDO-001 GW 12/17/19 09:15 12/18/19 10:20
Job ID: 680-178425-1
Eurofins TestAnnerica, Savannah
Page 4 of 15 1/7/2020

Method Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Method Method Description
SM 2540D Solids, Total Suspended (TSS)
SM 4500 H+ B pH
SM 5220D COD
Protocol References:
SM = "Standard Methods For The Examination Of Water And Wastewater'
Protocol
SM
SM
SM
Job ID: 680-178425-1
Laboratory
TAL SAV
TAL SAV
TAL SAV
RI
0
Laboratory References:
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins TestAmerica, Savannah
Page 5 of 15 1/7/2020

Definitions/Glossary
Client: EHS Support, LLC Job I❑: 680-178425-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Qualifiers
General Chemistry
Qualifier Qualifier Description
Fl MS and/or MSD Recovery is outside acceptance limits.
i Field parameter with a holding time of 15 minutes. Test performed by laboratory at dienYs request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
o Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDIDOE}
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
Di Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DOD/DOE)
LCQ Limit of Quantization (DoD1DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin!
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
POL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting -imit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
Ti Toxicity Equivalent Quotient (Dioxin)
Eurofins TestAmerica, Savannah
Page 6 of 15 1 /7/2020

Detection Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: SDO-001
Analyte Result Qualifier
pH 6.9 HF
Temperature 21.1 HF
Chemical Oxygen Demand 11 F1
This Detection Summary does not include radiochemical test results.
NONE
10
NONE Unit
su
Degrees C
mg1L
M
Job ID: 680-178425-1
Lab Sample ID: 680-178425-1
FE
Dil Fac D Method
Prep Type
t
1 SM 4500 11+ D
Tota1/NA
1 SM 4500 H+ B
t SM 5220D
TotalINA
TotalINA
i
Eurofins TestAmerica, Savannah
Page 7of15
1/7/2020

Client Sample Results
Client: EHS Support, LLC
ProjecVSite: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: SDO-001
Date Collected: 12/ 17119 09:15
Date Received: 12/18119 10:20
HI
Job ID: 680-178425-1
'r
Lab Sample ID: 680-178425-1
Matrix: GW
General Chemistry
Analyte
Result Qualifier
NONE
NONE Unit
D Prepared Analyzed
Oil Fac
pH
6.9 HF
SU
—
01/06/20 20:05
1
Temperature
21.1 HF
Degrees C
01/06/20 20:05
1
Analyte
Result Qualifier
RL
MOIL Unit
D Prepared Analyzed
Dil Fac
Chemical Oxygen Demand
11 I'll10
mg1L
12130l19 20:39
1
Analyte
Result Qualifier
RL
RL Unit
D Prepared Analyzed
Oil Fac
-
Total Suspended Solids
<2.0
2.0
mg/L
12/24/19 12:59
1
?`
FC
Eurofins TestAmerica, Savannah
Page 8 of 15 1/7/2020

QC Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.G. (Outfall 001)
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-60199911
Matrix: Water
Analysis Batch: 601999
MB MB
Analyte Result Qualifier RL RL Unit
Total Suspended Solids
Lab Sample ID: LCS 680-60199912
Matrix. Water
Analysis Batch: 601999
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-60199913
Matrix: Water
Analysis Batch: 601999
Analyte
Total Suspended Solids
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-603001134
Matrix: Water
Analysis Batch: 603001
Analyte
Lab Sample ID: LCS 680-60300115
Matrix: Water
Analysis Batch: 603001
Analyte
Method: SM 5220D - COD
Lab Sample ID: MB 680-60267513
Matrix: Water
Analysis Batch: 602675
Analyte
Chemical Oxygen Demand
Lab Sample ID: LCS 680-60267514
Matrix: Water
Analysis Batch: 602675
Analyte
Chemical Oxygen Demand
<1.0
1.0 mg/L
Fq�
Job ID: 680-178425-1
I� 1
Client Sample ID: Method Blank
'
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
r
12124119 12:59 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit ❑ %Rec Limits
0
50.0 54.0
mg/L 108 80- 120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCS❑ %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
_ jI
50.0 53.0 mglL 106 80 _ 120 2 25 --
1�4
Client Sample ID: Lab Control Sample
Prep Type: TOtal1NA
Spike
Added
LCS LCS
Result Qualifier
Unit
%Rec.
❑ %Rec Limits
7,01
7.2
SU
103 63 - 158
Client Sample ID: Lab Control Sample
Prep Type: TotaIINA
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit
❑ % Rec Limits
7.01
7.1
SU
101 63-158
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
a10 10 mg1L 12/30119 20 39 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
50.0 50.9 mg/L 102 90 - 110
Eurofins TestAmerica, Savannah
Page 9 of 15 1/7/2020

QC Sample Results
Client: EHS Support, LLC
ProjectlSite: Nexeo - Charlotte, N,C. (Outfall 001 )
Method: SM 5220D - COD (Continued)
Lab Sample ID: 680-178425-1 MS
Matrix: GW
Analysis Batch: 602675
Sample
Sample
Spike
MS MS
Anatyte
Result
Qualifier
Added
Result Qualifier Unit
Chemical Oxygen Demand
11
F1
50.0
53.3 F1 mglL
Lab Sample ID: 680-178425-1 MSD
Matrix: GW
Analysis Batch: 602675
Sample
Sample
Spike
MSD MSD
Analyte
Result
Qualifier
Added
Result Qualifier Unit
Chemical Oxygen Demand 11 F1 50.0 57.2
Page 10 of 15
mg/L
IT I
Job ID: 680-178425-1
Client Sample ID: SDO-001
-
Prep Type: T Total/NA
'
%ReC.
D %Rec Limits
84 90 _ 110
7 {
� i; I
Client Sample ID: SDO-001
r;
Prep Type: Total/NA
- -
%Rec. RPD
D %Rec Limits RPD Limit
92 90 _ 110 7 30
Eurofins TestAmerica, Savannah
1/7/2020

QC Association Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
General Chemistry
Analysis Batch: 601999
Lab Sample ID
Client Sample ID
680-178425-1
S D O-001
MB 680-601999/1
Method Blank
LCS 680-601999/2
Lab Control Sample
LCSD 680-601999/3
Lab Control Sample Dup
Analysis Batch: 602675
Lab Sample ID
Client Sample ID
680-178425-1
SOO-001
MB 680-60267513
Method Blank
LCS 68MO2675/4
Lab Control Sample
680-178425-1 MS
SDO-001
680-178425-1 MSD
SOO-001
Analysis Batch: 603001
Lab Sample ID
Client Sample ID
680-178425-1
S D O-001
LCS 680-603001/34
Lab Contro! Sample
LCS 680-603001/5
Lab Control Sample
Prep Type
Matrix
Method
Total/NA
GW
SM 2540D
Total/NA
Water
SM 2540
TotalINA
Water
SM 2540D
TotalINA
Water
SM 2540
Prep Type
Matrix
Method
Total/NA
GW
SM 5220
TotalINA
Water
SM 5220
Total/NA
Water
SM 5220
Total/NA
GW
SM 5220
TotalINA
GW
SM 5220
D
,lob ID: 680-178425-1
i
Prep Batch
D
D
Prep Batch
D
D
D
.
Prep Type Matrix Method Prep Batch
TotalINA GW SM 4500 H+ B
i
Total/NA Water SM 4500 H+ B
Total/NA Water SM 4500 H+ B
Page 11 of 15
Eurofins TestAmerica, Savannah
1/7/2020

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: SDO-001
Date Collected: 12/17/19 0915
Date Received: 12118119 10:20
Batch Batch
Prep Type Type Method Run
Total/NA Analysis SM 2540❑
Instrument ID: NOEQUIP
Tota11NA Analysis SM 4500 H+ B
Instrument ID: MANTECH
TctallNA Analysis SM 5220D
Instrument ID: SP07
Lab Chronicle
Job ID: 680-178425-1
Dil initial
Factor Amount
1 500 mL
1
1 2 mL
Lab Sample ID: 680-178425-1
Matrix: GW
u
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
❑
1000 mL
601999
12/24/19 12:59
MCL
TAL SAV
603001
01106120 20:05
JER
TAL SAV
2 mL
602675
12130119 20;39
TB
TAL SAV
0
Laboratory References: Ln
TAL SAV = Eurofins TestAmerica, Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]a5s M
Page 12 of 15
Eurofins TestAnnerica, Savannah
1/7/2020

TestAmerica Charlotte
2938-0 Queen City ©rive
Charlotte, KC 28280
Phone: 704.392.t264 Fax:
f }}}} t�(^�.�q Chain of Custody Record
�I"1t�.�'���ilP ��V
Regulatory Program: ❑lyv 7Npm f jaCrw Fjother:
2 5 5 3� 10 TestAmedc a
flit LEADER IN VWRONMENTAL TILVING
TestAmerica Laboratories, Inc.
TAL•8210107131
Client Contact
Project Manager; /��,
Site Contact: A,, «k�
Date: f
COC No:
Company Name: J' S t-
TellFax: y r
Lab Contact: r
Carrier:
_j_ of COCs
Address: , _ .tea Ale
Analysis Turnaround Time
Z
y
e
a
rn
,�
Y
o
0
2
L
a
O5
V
iY
i
d
Sampler;
CllylstalelZ€p:. 1Jc v L -k • r'1 ILi
❑ CALE. MAR DAYS J vrCRKING DAYS
For Lab Use Only:
Walk-€n Client;
Lab Sampling;
Phone: - 3 "
TAT it d.f:ment from Below
[] 2 wects
{5{f t WacF.
❑ 2 days
[] t day
Fax:
Project Name: S
Sue: ��- �. (�
Job! SDG No.:
P 0 0
Sample Identification
Sample
Date
Sample
Time
Sample
Type
tc cC p.
G•er=nF
Matrlx
Cent.
Sample SpecificNotes:
.SDU-Jo 1
iz r
v
G
3
N
680-17BA25 Chain of Custody
Preservation,Usedr An Ica, 2= HCI;'3=_H2SO4; '4=HH01; SnNaOH;'6=_Other,
Possible Hazard Identification:
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in she
Comments Section if the lab is to dispose of the sample.
Samplo Disposal { A fee may be assessed it samples are retained longer than 1 month)
t
❑ Retum to Gerft i isoesal by tdb a Ar[hive for Months
� ,:7n•lia:azd [; Ilamma'9e Lj Skin Irritant ❑ Potson 5 Lj funknenrt
Special Instructions/CC Requirements & Comments:
Custody Seals Intact: [J Yes r-1 ,140
Custody Seal No.: Cooler Temp. (C): bs'd; Corr'd: Therm ID No.:
Relingwshed.hy: / 7
Com any:
Dateffime:
Recl�-v by;
Company;
Date irn
;
Relln r
Company:
Dal !FT' fe:
Ills
Received by:
Company:
Dat €— :
Relinquished by;
Camvany:
Dal/Time.
Received in aborat ry by:
��- �.�
Company: /
I f •r�J
Dah"Mrne:
f L� 1 61 j `} i o��
CD
N
CD

Login Sample Receipt Checklist
43 j
Client: EHS Support, LLC
Job Number: 680-178425-1
L
Login Number: 178425
List Source: Eurofins TestAmerica, Savannah
List Number: 1
Creator: Weston, Pamela
Question
Answer Comment
F91
Radioactivity wasn't checked or is <1= background as measured by a survey
N/A
f
meter.
I
The cooler's custody seal, if present, is intact.
True
Samplecustodycustody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
❑
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
NIA
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection datellimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation verified.
NIA
There is sufficient vol. for all requested analyses, incl. any requested
True
MSlMSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (114").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
Eurofins TestAmerica, Savannah
Page 14 of 15 1/7/2020

Accreditation/Certification Summary
Client: EHS Support, LLC Job ID: 680-178425-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Laboratory: Eurofins TestAmerica, Savannah
The accreditationslcertifications listed below are applicable to this report.
Authority
LNorth Carolina (WW1SVV)
Program Identification Number Expiration Date
State Program 269 12-31-20
Eurofins TestAmerica, Savannah
f�
m
Page 15 of 15 1/7/2020