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HomeMy WebLinkAboutNCS000295_MONITORING INFO_20190103STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. DOC TYPE ❑FINAL PERMIT MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER r� U7 DOI � DOC DATE ❑ V YYYYMMDD JACKSON PAPER MANUFACTURING December 28, 2018 NCI)EQ, Division of Water Resources, Information Processing Unit Attn: Central Filcs/cDMR 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RECEIVED CD RE: Discharge Monitoring Report NPDES Permit No. NCS000295 JAN 0 3 2019 .Jackson Paper Manufacturing Compan.-'ENT AL FILES D1NR SEC?JON Dear Division of Water Resources: Please find enclosed Discharge Monitoring Reports for Jackson Paper Manufacturing Company NPDES Permit No. NCS000295 for reporting period starting October 1, 2018 and ending December 31, 2018. 1Zesults from samples taken on December 14, 2018 from Outfall 002 and 003 show no henchmark cxcecdances. There was an insufficient amount of'discharge from Outfall 001 and Outf:Ell 004 to sample during this rain event. Subsequently, we look samples fi-om Outfall 001 and Outfall 004 during the next rain event on December 20, 2018 and have enclosed the discharge monitoring report. rlThcre were no exceedances at Outfall 004. There were benchmark cxcecdances at Outfall 001 for TSS and COD. Outfall 001 is located at a catch basin in the middle of the facility's front parking lot. The basin collects runoff from the employee and visitor parking areas, roof drains from the office building, and delivery truck loading/unloading docks. Portions of West Main Street, located cast of the facility, slopes towards the facility so that stormwater from this section of roadway runs tOwards Outfall 001. In response to the TSS benchmark cxcecdances, we conducted a stormwater management inspection of the facility on 12/28/18. We have identified possible causes Of the benchmark value cxcecdances. We believe the exceedanecs are primarily a result of'run-on f-ronh West Main Street. Also, a patch of grass along the curb at the loading dock was torn up and muddy due to trucks driving over the curb and into the grass. We will consider our options and select feasible controls to improve this situation, such as making the curb more visible and filling in the area with gravel. I certify that based on information and belief formed from reasonable inquiry, the statements and information in the document are true, acctn-ate, and complete. NORTH CAROLINA'S LARGEST RECYCLED PAPER PRODUCER 152 WA' MAIN STRi WD PO Bux 6670 Sven, NC 28779 -FEE. (828) 586-5534 FAX (828) 586-6755 ]'lease contact Kiesha Bridges at (828)586-5534 Ext. 226 if you have any questions or need any additional information. Sincerely, Carr "fyi dall Vice -President Operations Jackson I'aher Manulacturulg C01111MIly EnclOSLII'C: Storm«fater Discharge Monitoring Report cc: JPIMC File Stormoater Discharge Outfall (SDO) Monitoring Report Permit Number NCS000295 Facility Name: Jackson Paper Manufacturing Company Person Collecting Samples. Kiesha Bridges Certified Laboratory: Pace Analytical Services. LLC Project p 92410854 Samples Collected During Calendar Year: 2018 (']his monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) Countv: Jackson Ph ne NO. (828)536-5534 Pxt. ??6 (SIGNATURE01,PEILNIH .EORDESTGNFE) By this signature, I certify that this report is accurate and cumplete to the best of my knosN [edge. Oil and Grease Turhidit}' TSS pH COI) Benchmark 15 Not Required 50 (6-9) 120 Outfall Date Sampled Result rn 11 Benchmark Excecdance YIN Result ma L Benchmark Exceedance }7N Result Benchmark Exceed. nce YIN Result m g/L Benchmark Exceedance YIN 002 12/1412018 12:45 m ND No ND No 7.1 No ND No �0312/14/2018 1:15 m ND No 10.3 No 7A No 51.9 No ND: Not defected of or above adjusted reporting limit Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Yes x No Niensureable Storm Event? Yes D.23 Storm Event Characteristics: Date: December 14, 2018 Total event -precipitation (inches}: 10.23 - - Duration of storm event: 1.5 hours Drainage Area Mail Original and one copy to: IV Division of Water Quality 1,77 Attn: Central Files 77,101 1617 Mail Service Center 1,478 Raleigh, North Carolina 27699-1617 1T,254 I II 111 Area (acres) Area isf) volume (cf) 1.69 73,616 1,411 5.43 236,531 4,534 20,45 990,802 17,074 Estimated -volume of discharge sampled: '..Volume (gal) Time Since last rain event: 3 days 10,554 33,911, . 127,711, " 1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines aP,.r violations."� 17-1 IT (Signature of Perm' ee) (Date 6 (�IaneAnalXiba( www.Pacefabs.mm December 21, 2018 Kiesha Bridges Jackson Paper Mfg. Co. 152 West Main St. Sylva, NC 28779 RE: Project: Stormwater 4th Qtr 12114 Pace Project No.: 92410854 Pace Analytical Services, LLC 2.225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Dear Kiesha Bridges: Enclosed are the analytical results for sample(s) received by the laboratory on December 14, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures cc: Kelsha Bridges, Jackson Paper Mfg. Co. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 O aceAnalytical wnw.pa dab&COm Project: Stormwater 4th Qtr 12114 Pace Project No.: 9241C854 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 FloridalNELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNFLAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 (�IaceAnalytical" WWW..pacelabs.Com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 2226 Riverside dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: Stormwater 41h Qtr 12114 92410854 Analyzes Lab ID Sample ID Method Analysts Reported Laboratory 92410854001 OUTFALL # 2 EPA 1664B JMS 1 PASI-C SM 2540D-2011 CEH 1 PASI-A EPA9040C SMK 1 PASI-A SM 5220D-2011 GC 1 PASI-A 92410854002 OUTFALL # 3 EPA 16643 JMS 1 PASI-C SM 2540D-2011 CEH 1 PASI-A EPA 9040C SMK 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 (�IaneAnalytibale www acewcom ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 Project: Slormwater 41h Qtr 12114 Pace Project No.: 92410854 Sample: OUTFALL # 2 Lab ID: 92410854001 Collected: 12/14/18 12:45 Received: 12/14/18 15:01 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 4.8 1 12/20/18 04:52 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids ND mg)L 2.5 1 12/15/18 07:50 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C. 7.1 Std. Units 0.10 1 12/17/18 17:02 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand ND mg/L 25.0 1 12/18118 16:50 12/19/18 16:59 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/21/2018 06:36 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalytical wwwpacehiftc mm ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 4lh Qtr 12/14 1} Pace Project No.: 92410854 1 "15 ptr Sample: OUTFALL # 3 Lab ID: 92410854002 Collected: 12/14/18 42.45 Received: 12/14/18 15:01 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mglL 4,8 1 12/20/18 04:53 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 761al Suspended Solids 10.3 mglL 2.5 1 12/15/18 07:51 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.4 Std. Units 0.10 1 12/17/18 17:05 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 51.9 mg/L 25.0 1 12/18/18 16:50 12/19/18 16:59 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date' 12/21/2018 06:35 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical www.pwdabs.com QUALITY CONTROL DATA Project: Stormwaler 4th Qtr 12114 Pace Project No.: 92410854 QC Batch: 448699 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92410854001, 92410854002 METHOD BLANK: 2457606 Matrix: Water Associated Lab Samples: 92410854001, 92410854002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg1L ND 4.8 1212011804A2 Pace Analytical Services, LI-C 2225 Riverside Dr. Asheville, NC 28804 (828)254a 176 LABORATORY CONTROL SAMPLE: 2457607 Spike LCS 1-CS. % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/1- 19.2 18.8 98 64-132 MATRIX SPIKE SAMPLE: 2457608 35436943002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualiflers Total Petroleum Hydrocarbons mg1L 5.OU 20 22.8 96 64-132 Results presented an this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 12/21/2018 06:36 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 aceAnalytical w"..paeelabs.cam QUALITY CONTROL DATA Project: Stormwater 41;11 Qtr 12114 Pace Project No.: 92410854 QC Batch: 447795 Analysis Method: SM 2540D-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92410854001,92410854002 METHOD BLANK: 2453569 Matrix: Water Associated Lab Samples: 92410854001, 92410854002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mglL ND 2.5 12/15/18 07:48 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, INC 26604 (82B)254-7176 LABORATORY CONTROL SAMPLE: 2453570 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mglL 251 232 92 90-110 SAMPLE DUPLICATE: 2453571 92410686001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 6.6 7.6 14 D6 SAMPLE DUPLICATE: 2453572 92410626001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/2112018 06:36 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 (�5a'cieAnalyticalo wwwpacelabs.mm QUALITY CONTROL DATA Project: Stormwater 4th Qtr 12114 Pace Project No.: 92410854 QC Batch: 447964 Analysis Method: EPA 90400 QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92410854001, 92410854002 SAMPLE DUPLICATE: 2454019 92410732001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 8.2 8.3 0 H3 SAMPLE DUPLICATE: 2454020 Parameter pH at 25 Degrees C 92410894007 Dup Units Result Result Std. Units 9.2 9.2 RPD Qualifiers 0 H3 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12121/2018 06:36 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 laneAnalytical" „nnvpacewaWm QUALITY CONTROL DATA Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, 128804 (828)254-7176 Project: Stormwater 41h Otr 12114 Pace Project No.: 92410854 QC. Batch: 448376 Analysis Method: SM 5220D-2011 QC Bach Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92410854001,92410854002 METHOD BLANK: 2456034 Matrix: Water Associated Lab Samples: 92410854001,92410854002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand rnglL ND 25.0 12/19/18 16:58 LABORATORY CONTROL SAMALE: 2456035 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 747 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2456036 2456037 MS MSD 92410047001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec e/ Rec Limits RPD Qual Chemical Oxygen Demand mg1L 7370 100 100 786C 7610 481 241 90-110 3 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2456038 2456039 MS MSD 92410845005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL 35.0 100 100 134 139 99 103 90-110 4 R1 Results presented an this page are in the units Ind lcated by the "Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/21/2018 06:36 PM without the written consent of Pace Analytical Services, Ll Page 9 of 14 laceAnalytical" www.pacelabs.c+om QUALIFIERS Project: Stormwater 41h Qtr 12114 Pace Project 1 92410854 DEFINITIONS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, i 2BB04 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. Ml - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LC5{D} - Laboratory Control Sample (Duplicate) Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is Ti accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full. Date: 12121 /2018 06:36 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 aceAnalytical W"Pacelab&wn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Storrnwater 41h Qtr 12114 Pace Project No.: 92410854 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (628)254-7176 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92410854001 OUTFALL # 2 EPA 1664B 448699 92410854002 OUTFALL # 3 EPA 1664B 448699 92410854001 OUTFALL # 2 SM 2540D-2011 447795 92410854002 OUTFALL # 3 SM 2540D-2011 447795 92410854001 OUTFALL # 2 EPA 9040C 447964 92410854002 OUTFALL # 3 EPA 9040C 447964 92410854001 OUTFALL # 2 SM 5220D-2011 44837E SM 5220D-2011 92410854002 OUTFALL # 3 SM 5220D-2011 448376 SM 5220D-2011 Date: 12121/2018 06:36 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Hatch 448596 448596 Page 11 of 14 Document Name: Document Revised: February 7, 2018 " Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No,: Issuing Authority: C£'fil7alJ1�lCc7j� F-CAR-CS-033-Rev.06 Pace Carolinas Qual'sty office Laboratory receiving sa pies: Asheville? Eden[] Greenwood ❑ Huntersville❑ Raleigh❑ Mechanicsville[] Client Name: f� Now, -,Project q Courier: ❑F dx ❑UPS ❑lisps lient ❑ Commercial ❑Pace ❑Other: Custody Seal Present? ',lyes ❑No Seals Intact? ❑Yes ❑No Packing Material: ❑Bubble Wrap ❑Bubble Bags Plone ❑ Other Thermometer- IR Gun ID: f c7� Type of Ice: lkvet ❑Blue Cooler eT mp ('C): , s- Correction Factor: Add/Subtract ('Q Cooler Temp Corrected (('Xarantlne C): b USDA Regulated SollN/A, seater sample) Did samples originate' zone within the United States: CA, NY, or SC (check maps)? nYes nNo WO#:92410854 62410654 I II IIIII II II III Date/Initials Person Examining Contentst—El9 Biological Tissue Frozen? ❑Yes ❑No []N/A ❑None Temp should be above freezing to 6'C ❑Samples out of tern periterla. Sampleson ice, cooling process has begun Did samples originate from a foreign source (intern ationaSly, inriud'm¢ Hawaii and Puerto RICDI? nyes nND Comments/Discrepancy: Chain of Custody Present? Yes ❑No N/A 1. Samples Arrived within Hold Time? 2 Yes ONO N/A 2. Short Hold Time Analysis (472 hr.)? ❑Yes VINP ONJA 3. Rush Turn Around Time Requested? 0 Yes D N/A 4. Sufficient Volume? Yes ❑No N/A S. CWeCtContainers Used? -Pace Containers Used? �es Yes ONO ONO ❑N/A N/A 6. Containers intact? es [:]No 0 N/A 7. Dissolved analysis: Samples Field Filtered? Des ONO N/A B. Sample Labels Match COC? -Includes Date/Time/ID/Analysis rvlatrix: Yes 1 []No ❑N/A 9. Headspace in VOA Vials (55-6mm)? ❑Yes ONO N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? Oyes ❑Yes ❑No N/A ONO N/A 11, COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Reviews Field Data Required? []Yes []NO Lot ID of split containers: Date/Time: Date: f ,Z 17/V Date: ;y ,1 ' ✓ Page 12 of 14 fJ' ftehiafytica!} Document Name: Sample Condition Upon Receipt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box Is to list number of bottle Project # WOE : 92410854 PM; CDl Due Date: 12/20/18 CLIENT: 93—Jackson P dE _ 2 a Z C > u a E 0 a CO z ro Ca > u ii E o 7 a m ? -o Z c > v a c 7 a m < ? v D is `a T a a m x v N N a E LM yr a m n V O = u N a E 2 a to z o 2 0 a < Z N v N a CO iv S O `� z r E n 6 Q. m a v a j m a En a z a c 7 - t7 Q tJ 2 m` t7 Q z a a C 9 C E o m l7 Q � v v O iv S v ,Ni 0 ¢ v O ✓� N ' E E o ml7 0 Q a z P 4 J E o a rrn7 l7 4 < z u x ¢ > of 0 0 �- vi eNa z > E 0 > G Z e > e G > Z v 0 m < > E L7 O z on o 4 « m -> O > a Z z j « n S 7 y _ro G. N vat a n i w m E CD0 N e6i� — a m M Z Z rs E ran ra v .n C � a QE $ 4 ¢ > o c E l'7 > z A ro v c5, c ? E a Q 0 1 2-7 ` i X/NN\ L 3 +\� \ \11-1 a �� -�\\ NN 144�\ N\ \N\ I 6 7 R 9 10 11 -N 12 Tl�N\N N \NN I I pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot ff Note: Whenever there is a discrepancy affecting Hart Carolina compliance samples, a copy of this form will 6e sent to the North Carolina DEHNR Certification Office (Le. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 13 of 14 PaceAnalytrcal" CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain-af-CuslDdy Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Paget of Section A Section 6 Section C Required Client Information; Required Prajed Information: Invoice Information: Attention: Repon To: 2193138 c ,t eS AddrCopy �t,702A To: Company Name: REGULATORY AGENCY S IJa ,tlG g 9 Address: F NPDES F GROUNDWATER i^ DRINKINGWATER f UST j- RCRA F OTHER Em o: Purchase e 0LC!vSa er. Order No.: D8[p5 Pace Ovote Reti gnu,: P Su r� Pr FiS;�� e5t Name: �-pt j Pace wolan Site Location d. S R(o S S 3 �1 l0 3 3 �"prr%� W0. 'eF T'Y I.tana9cr. STATE: Requested Qua at AY: P Project Number: Patl° PAOfA' b• f ( O P lease- ex <d fG Requested Analysis Filtered (YIN) Section O Malrik Cocos Required Client W rmalion MATRIX I CODE - 9 - 0 COLLECTED Preservatjves z Y Drinking Wrier OW n = Water WT $ L1 rrzrnacutE courosrtc o )-- rod it W:rrnr WW Pod Pruct P m 0 GNWGIUl1 J Z } Soillsotid SL p SAMPLE ID - Q W m a 0 Wpe W (A-Z.0-91:) Air AR p w a Z M F Sample IDs MUST BE UNIQUE Tissue TS O L) (L H dt H L U Other OT � LL n0p to -EC I N 7� 4( t) � S GI ~ rn DATE TIME GATE TIME _ _ _ z Z `2 O ,.ay IY Paco Project Na-! Lab I.D. 1 2 0 0 .�� to 410 Id: LIT H1 ✓ v r 3 I 3J., Co 1-)114 I:t ✓ A V1, V1/ q - 5 6 7 8 9 to it 12 ADDfTIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME gCCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS ,� «Q1102"I �, iy I.So ! r PR SAMPLER NAME AND SIGNATURE o ORIGINAL 2 PRINT Name of SAMPLER: o U Z SIGNATURE of SAMPLER: MNVOt)mld it U y f 1.4-lvu Now: By Sig" MY form you are wcepusg Paco s NET 30 day payment terms and agreeing w Lne dtarq¢ or 1.5% per =156 for arty nvottxs rwi path y &- 36Z ys. F-ALL-0-020rev.07, 15-May-2007 Stormwaler Discharge Outfall (SDO) Monitoring Report Permit Number NCS000295 Facility Name: Jackson Paner Manufacturing Compam• Person Collecting Samples: Kiesha Bridges Certified Laboratorc: Pace Analytical Services. LLC Project # 92411690 Samples Collected During Calendar Year: 2018 (This monitoring report shall be received by the Disision no later than 30 days from the dale the facility receives the sampling results from the laboratory.) Counh': Jackson Ph to NO. 828 586 534 Ext. 226 il�C;IATuRF OF PER\ F. Olt DFSIGNEE) By this signature. I certify that this report is accurate and complete to the hest of my kno+sledge. Oil and Grease Turhiditc I'SS pH COD Benchmark 1s Not Required 50 (6-9) 120 Outfall Dale Sampled Result m,_,L Benchmark Exceedance YIN Result m.11. Benchmark Eaceedance YIN Result Benchmark Ezceedanee YIN Result mall Benchmark Fsecedancc TIN 001 12/20/2018 II:15 m ND No IS1.0 Yes 6.5 No 132.0 Yes 004 121'0/2018 11:30am ND NO 49.0 No 6.6 No 37.0 No ND: Not detected at or above adjusted reporting limit Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _Yes x No Nleasureable Storm Vvent' Yes 0.8 Storm Event Characteristics: Date: December 20, 2018 Total event precipitation,(inch es): 0.80" Duration of storm event: - 24 hours Drainage Area Mail Original and one copy to: Iv Division of Water Quality 1.77 Attn: Central Files 77,101 1617 Mail Service Center 5,140 Raleigh, North Carolina 27699-1617 39,448: l u nl Area (acres) Area (sf) volume (Cf) 1.69 73,616 4,908 5.43 236,531 15,769 20.45 990,802 59,387 Estimated volume of discharge sampled: Volume (gal) Time since last rain event: 3 days 36,710 _ 117,950 444,213 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonmentfo kn i vlolations." Jz Z� (Signature of Per tee) (Dat ) (�IaoAnalXidal' ww.pacefab&c= December 27, 2018 Kiesha Bridges Jackson Paper Mfg. Co. 152 West Main St. Sylva, NC 28779 RE: Project: Stormwater 4th Qtr 12120 Pace Project No.: 92411690 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (628)254-7176 Dear Kiesha Bridges: Enclosed are the analytical results for sample(s) received by the laboratory on December 20, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com (828)254-7176 Project Manager Enclosures cc: Keisha Bridges, Jackson Paper Mfg, Co. PURFQ� TNl Oe AS�� REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 Pace Analytical Services, LLC laceAnalyticale 2225 Ashevillee,,Riverside 28804C www..pacdabs.com (828)254-7176 CERTIFICATIONS Project: Storrnwater 4th Ctr 12120 Pace Project No.: 92411690 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certif cation #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 Pace Analytical Services, LLC aceAnalyfrcal6 27Riverside Asheville, NC 2R80404 A wwwpacelsb&cam (828)254-7176 SAMPLE ANALYTE COUNT Project: Stormwater 4th Otr 12120 Pace Project No.: 92411690 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92411690001 OUTFALL 1 EPA 1664B JMS 1 PASI-C SM 2540D-2011 CRV 1 PASI-A EPA9040C SMK 1 PAS! -A SM 5220D-2011 GC 1 PASI-A 92411690002 OUTFALL 4 EPA 1664E JMS 1 PASI-C SM 254OD-2011 CRV 1 PASI-A EPA 9040C SMK 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 (�IaceAnalXicalo wnvwpacelsbacom ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28504 (828)254-7176 Project: Starmwater 4th Qtr 12120 Pace Project No.: 92411690 Sample: OUTFALL 1 Lab ID: 92414690001 Collected: 12/20/18 11:15 Received: 12/20/18 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mglL 5.0 1 12/22/1804:05 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 181 mg1L 35.7 1 12/21/18 16:38 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.5 Std. Units 0.10 1 12/27/18 11:16 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 132 mglL 25.0 1 12/20/18 19:00 12121/18 22:17 REPORT OF LABORATORY ANALYSIS This report shaI[ not be reproduced, except in Full, Date: 12/27/2018 06:32 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 lacieAnalyticalo www.pacdabsaorn ANALYTICAL RESULTS Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Stormwater 4th Qtr 12120 Pace Project No.: 92411690 Sample: OUTFALL 4 Lab ID: 92411690002 Collected: 12120118 11:30 Received: 12120/18 13:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 5GT-HEM, TPH Anatytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mglL 5.0 1 12122/18 04:06 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 49.0 mglL 12.5 1 12/21/18 16:38 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.6 Std. Units 0.10 1 12127/18 11:18 H3 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 37.0 mglL 25.0 1 12/20118 19:00 12/21/18 22:18 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/201 B 06:32 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 laneAnalyfical* www.pacelab&cam QUALITY CONTROL DATA Project: Stormwater 41h Qtr 12120 Pace Project No.: 92411690 QC Balch: 449295 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92411690001, 92411690002 METHOD BLANK: 2460420 Matrix: Water Associated Lab Samples: 92411690001, 92411690002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg1L ND 4.8 12/22/18 03:52 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2460421 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg1L 19.2 22.4 117 64-132 MATRIX SPIKE SAMPLE: 2460422 92411073001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mglL ND 19.2 21.4 110 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in lull, Date: 12/27/2018 06:32 PM without the written can sent of Pace Analytical Services, LLC. Page 6 of 14 • aceftlytical www.pacela88.eGm QUALITY CONTROL DATA Project: Stormwater 4th Qtr 12120 Pace Project No,: 92411690 QC Batch: 449199 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92411690001, 92411690002 METHOD BLANK: 2459984 Associated Lab Samples: 02411690001, 92411690002 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2459985 Parameter Units Total Suspended Solids mglL Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7175 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 12/21/18 16:34 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 246 98 90-110 SAMPLE DUPLICATE: 2459986 92411680004 Dup Parameter Units Result Result Total Suspended Solids ni ND ND SAMPLE DUPLICATE: 2459987 92411736001 Dup Parameter Units Result Result Total Suspended Solids mg1L 57.0 66.0 RP❑ Qualifiers RPD Qualifiers 15 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 12/27/2018 06:32 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 (�IaceAnalyticalo www.paceJahs.aom QUALITY CONTROL DATA Project: Stormwater 4th Qtr 12120 Pace Project No.: 92411690 QC Batch: 449381 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92411690001, 92411690002 SAMPLE DUPLICATE: 2460745 92411981001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 5.8 5.7 2 H3 SAMPLE DUPLICATE: 2460763 Parameter pH at 25 Degrees C 92411800001 Dup Units Result Result Std. Units 6.2 6.1 RPD Qualifiers 1 H3 Pace Analytical Services, LLC 2225 Riverside dr. Asheville, NC 25804 (828)254-7176 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2018 06:32 PM without the written consent of Pace Analytical Services, LLC, Page 8 of 14 (�IaceAnalyfical" wwwpacelabsu=n QUALITY CONTROL DATA Project: Stormwater 4th Qtr 12/20 Pace Project No.: 92411690 QC Batch: 448931 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92411690001, 92411690002 METHOD BLANK: 2458946 Matrix: Water Associated Lab Samples: 92411690001,92411690002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mWL ND 25.0 12/21/18 22:15 Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE: 2458947 Spike LC5 LCS % Rec Parameter Units Conc. Result % Rec Limits Qualiflers Chemical Oxygen Demand mg1L 750 762 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2458948 2458949 MS MSD 92411168001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL 576 100 100 651 669 74 93 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2458950 2458951 MS MSD 92411790001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 848 100 100 944 934 95 86 90-110 1 M1 Results presented on thls page are In the units indicated by the "units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/27/2018 06:32 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 s ace Analytical www.pacelabs.cam QUALIFIERS Project: Stormwater 4th Qtr 12120 Pace Project No.: 92411690 DEFINITIONS Pace Analytical Services, LLC 2225 Riverside Dr, Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit, TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL- Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenyihydrazine decomposes to and cannot he separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. W Sample was received or analysis requested beyond the recognized method holding time. M 1 Matrix spike recovery exceeded QC Limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This repadshall not he reproduced, except in full, Date: 12/27/2018 06:32 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 aceAnalytical. wwwpacela6sm n QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: Stormwater 41h Qtr 12120 92411690 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92411690001 OUTFALLI EPA1664B 449295 92411690002 OUTFALL 4 EPA 1664B 449295 92411690001 OUTFALL 1 SM 2540D-2011 449199 92411690002 OUTFALL 4 SM 254OD-2011 449109 92411690001 OUTFALL 1 EPA 9040C 449381 92411690002 OUTFALL 4 EPA 9040C 449381 92411690001 OUTFALL 1 SM 5220D-2011 448931 SM 52200-2011 449268 92411690002 OUTFALL 4 SM 5220D-2011 448931 SM 5220D-2011 449268 Date: 12/27/2018 06:32 PM REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 2eAnalytical' Document Name: Sample Condition Upon Receipt(SCUR) Document Revised: February 7, 2018 Page 1 of 2 Document No.: F-CAR-CS-033-Rev.06 Issuing Authority: Pace Carolinas quality Office Laboratory receiving sapnples: Asheville [] Eden[] Greenwood ❑ Huntersvil(e❑ Raleigh❑ Mechanicsville[] Clie It Name: PrDjec WO# : 92411694 Courier: ❑F x ❑UP ❑USPS j II Client ❑ Commercial ❑Pace ❑other: 92411690 + Custody Seal Present? Yes D Seals Intact? ElYes [:]No Date/initials Person Examining contents: Packing Material: ❑Bubble Wrap ETBubble Bags ❑None ❑ other Biological Tissue Frozen? Thermometer: f? -y Type of Ice: [ et ❑IR Gun ID: 21 []Blue❑None []Yes❑No [K/A Cooler Temp ('C): ?,n Correction Factor: Add/Subtract('C) � /"� Cooler Temp corrected ('C): _�� � Temp should be above freezing to 6'C []Samples out of temp criteria. Samples on ice, cooling process USDA Regulated Soil Q-1q/A, water sample) has begun Did samples originate in a quarantine zone %vithin the United States: CA, NY, or SC (check F lyoq FlNn maps)? Did samples originate from a foreign source (internationally, includino Hanaii and Puerto Ricol? nYes ❑No Comments/Discrepa ncy: Chain of Custody Present? es El No ❑N/A 1. Samples Arrived within Hold Time? e<es []No El NIA 2. Short Bold Time Analysis (02 hr.)? ❑Yes Bh'a []N/A 3. Rush Turn Around Time Requested? EJ�es No ❑N/A 4. Sufficient Volume? [Yes ❑No [I N/A 5. Correct Containers Used? -Pace Containers Used? QYes Qves ❑No ❑N/A ❑No ❑N/A 6. Containers Intact? OYcs. [:]No ENIA 7. Dissolved analysis: Samples 'Mcl Filtered? ❑Yes ❑No O /A B. Sample labels Match COC? -Includes Date/Time/ID/Analysis / Elves Matrix: r No N/A [:]NO 9. Headspace in VOA Vials (>S•6mm)? [-]Yes No N/A 10. Trip Biank Present? Trip Bank Custody Seals Present? ❑Yes ElYes ❑f!o [:)No N/A N/A 11, COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes [:]No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: / r ZL-- Date: yr� Page 12 of 14 CU m w O a a 3 n v ra a m 2 w c 0 h a n Q a r, C Ln n v rt m rD � rt = r— O 00 m c Oa � e a � to m C w v C. a (A � 2 A � � N A 3 C m a, R V n a „ 2 w c A N r o Etemtl zzzzzz 1 z BP4U-125 mL Plastic Unpreserved {N MU-250 mL Plastic Unpreserved (N/A) BP2U.500 mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) BP4S-125 mL Plastic H2SO4 (pH < 2) (Cl.) 8P3W250 mL plastic MM03 (PH < 2) SP4Z-125 mL Plastic ZN Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (pH > 12) (Cl-) WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) (CI-) AGSM-1 liter Amber HCI {pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (Cl-) AG1S-1 liter Amber H2504 (pH < 2) zxxz AG3S-250 mt Amber H2SO4 (pH < 2) AMA{DG3A)-250 mL Amber NH4C1 (N/A)(CI-) DG9H-40 mL VOA HCI (NIA) VG9T-40 mL VOA Na2S203 (N/A) VG9U-n0 mL VOA Unp (NIA) DG9P-40 mL VOA H3PO4 (N/Al VOAX (6 vials per kit)-5035 kit IN/A) V/GI( (3 vials per kit)-VPH/Gas kit (N/A) SP5T-125 mL Sterile Plastic (N/A --lab) SP2T-250 mL Sterile Plastic (N/A — lab) MA-250 mL Plastic (NH2)2SO4 (9.3-9.7) AGOU-100 mL Amber Unpreserved vials (N/A) VSGU-20 mL Scintillation vials (NIA) DG50-40 ml.Amber Unpreserved vials (NIA) ►? PaceAnalytical' CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Page: of 4 Section A Section B Secdon C Required Client Infornolion: Required Project Information: InvoKe WOrrnalton: Report TO ALLendon: Cz k 2193139 ri er . . Ili e s CL ,; dra :W C Copy �10L S i. TO: Company Name: REGULATORY AGENCY 5,11 VOL, NC a $ -2, :� q Address. NPDES I— GROUNDWATER r DRINKING WATER UST !� ftCRA !— OTHER Purchase MA Order No.: d` Pace pods rt e5 a ernL,+ Rnlorenco: ?h Fax: Project 519 553 y (031 331LJ Name rJ rmuio-+re 94" Q�r Pa Proia<r I, anaq r: Site Location srArE; Ro u : od ue baterTAT: PrajotlNumber: B`d peoaP-W.X: t i 5Af' Requested Analysis Filtered (YIN) Section D Matrix Codes Required Cimrt khbrmdion MATRIX fCOOE u IL O COLLECTED Preservatives i OdrkIfY.9 Walnr DW water 0 " $ U ZO VVT Waste water WW m composrTE cn� rtE Z Pro SOWSolid St ; c7 O 1-0 SAMPLE ID Oil OL _ U y a d m wipe wP (o-Z, 0-91 : j Air AR w a z r o Samplo IOs MUST BE UNIQUE T6sw TS O U 4• w` F W 4nn U Other OT x u a lu a Z O u- N �' O O O O U) o c L °i N O ~ N c rn n N M Z Z t y I' GATE TIME bATE 71ME x 2 = O [-J Ix Pace Project NoJ Lab I.D. 1 W� �7 lz-f z- 11: 1$a v A I -Oat z 6 alzo lik.-30em V, V1 ll,/ V1 I I I I I 1 oaZ 3 4 5 6 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 1h, 33a 2.0 T s Epp IL,Lq S C-i fLum ORIGINAL SAMPLER NAMEANDSIGNATURE O z m PRINT Name of SAMPLER: Kie h G4 ri Gf f.1S ' Y -a- Z SIGNATURE of SAMPLER: ! (MMlDb1 . - J bATE Siprwd 1 a 1� �! g F = 82 E. r N -ImpxwW Nola: By si j mg thm Ir:m yw we woept:rg Pace's NET 30 day payment terms arid agrednp 10 lase aharc d 1.5% per month fff-q W Mces Mt Pale -am 30 days. F-ALL-Q-020rev.07. 15-May-2007