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NCG240019_MONITORING INFO_20181115
mzo STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. DOC TYPE ❑HISTORICAL FILE ie' MONITORING REPORTS DOC DATE ❑ gD I � (I J 5 YYYYMMDD Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 11/13/2018 CERTIFICATE OF COVERAGE NO. NCG240019 SAMPLE COLLECTION YEAR 2018 FACILITY NAME Mecklenburg County Compost CentralJnewj SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec COUNTY Mecklenburg County _ Ilk /C n or ® Monthlyl_October (month} PERSON COLLECTING SAMPLES Khaliem Adams i1RECE DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA LABORATORY: Pace Analytical Services Lab Cert. # 92 NOV 15 Z018 ❑Zero -flow []Water Supply ❑SA Comments on sample collection or analysis: [—]Other CEN-TRAL FILE.? UV_VK SL`a I luN Part A: Stormwater Benchmarks and Monitoring Results Total event rainfall 10.20 in or ❑ No discharge this period3 Date Sample Colle Collected' (mo/ cted' Outfall No. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 11/5/2018 1 11.2 121 6000 3.3 1.0 0.0053 ¢0.0050 0.011 6.9 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an qn-site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 4The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Date Sample Collected' (mo/dd/yr) Outfali No. pH TPH using method 1564A SGT-HEM TSS Total Rainfall' Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/1-4 - - 11/5/2018 1 6.9 <5.0 11.2 0.20 75 gal/month Footnotes from Part A also apply to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART It SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail on original and one cony of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina period in the case o "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." prat wr-ofd�r ittee) rmit Date: 10/1/2011-9/30/2016 l ze (Date Last Revised 12/02/11 Page 2 of 2 aceAnalytical wwwpacelabs.mm November 12, 2018 Darren Steinhiiber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNUNELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste p.CCRFO TNl REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 laneAnalytical "pacelabs.cam Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 Pace Analytical services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification 113s 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNEIAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 aceAnalytical www.pacelabs.cam SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 2 92405896 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92405896001 OUTFALL 1 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 CRV 1 PASI-A EPA9040C SMK 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A SM 5220D-2011 GC 1 PASI-A 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 aceAnalXifcal www.pawlabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersvllie, NC 2807B (704)875-9092 Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 Sample: OUTFALL 1 Lab ID: 92405896001 Collected: 11/05/18 10:11 Received: 11/05/18 10:50 Matrix; Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 4.8 1 11109/18 05:17 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper 0.0053 mg1L 0.0050 1 11/06/18 05:44 11/08/18 23:24 7440-50-8 Lead ND mg1L 0.0050 1 11/06/18 05:44 11/08/18 23:24 7439-92-1 Zinc 0.01i mg1L 0.010 1 11/06/18 05:44 11108/18 23:24 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 6000 CFU1100 mL 1.0 1 11/05/18 13:19 11106/18 13:02 u2 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 11.2 mg1L 6.7 1 11107/18 18:54 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 6.9 Std. Units 0.10 1 11/06/18 13:53 H3 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 3.3 mg1L 0.52 1 11/12/18 10:14 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 3.3 mg1L 0.50 1 11/07/18 02:05 11/08/18 00:57 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg1L 0.020 1 11/07/18 10:19 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 1.0 mg1L 0.050 1 11/06/18 22:42 11/07/18 20:43 7723-14-0 52200 COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 121 mg1L 25.0 1 11/08/18 19:11 11/09/18 00:04 REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, ❑ate: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnalXical wwwpact fabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 441313 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92405896001 METHOD BLANK: 2423463 Associated Lab Samples: 92405896001 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 11/09/18 04:58 Pace analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2423464 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 20.9 108 64-132 MATRIX SPIKE SAMPLE: 2423465 92405876001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.2 21.7 113 64-132 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 aceAnalytrcal www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 440463 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92405896001 METHOD BLANK: 2419374 Matrix: Water Associated Lab Samples: 92405896001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mglL NO 0.0050 11/08/18 23:12 Lead mglL ND 0.0050 11/08/18 23:12 Zinc mglL NO 0.010 11/08/18 23:12 LABORATORY CONTROL SAMPLE: 2419375 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mglL 5 0,50 100 85-115 Lead mglL .5 OA7 94 85-115 Zinc mglL .5 OA7 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419376 2419377 MS MSD 92405896001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mglL 0.0053 .5 .5 0.52 0.52 103 103 70-130 0 Lead mg1L ND .5 .5 0.49 0.48 98 97 70-130 1 Zinc mglL O.D11 .5 .5 0.50 0,50 98 98 70-13D 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419378 2419379 MS MSD 92405904001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mglL ND .5 .5 1 0.51 102 103 70-130 1 Lead mglL ND .5 .5 0.48 0.48 96 97 70-130 1 Zinc mg/L 0.014 .5 .5 0.50 0.50 97 97 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 113 aceAnalX cal www.pacelebs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 440382 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Associated Lab Samples: 92405896001 METHOD ELAN!(: 2419100 Matrix: Water Associated Lab Samples: 92405896001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Colifofms CFU1100 mL ND 1.0 11/06/18 13:02 SAMPLE DUPLICATE: 2419101 Parameter Fecal Coliforms 92405900001 Dup Units Result Result RPD Qualifiers CFU1100 mL 6000 600 164 D6,u2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC, Page 7 of 18 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 440962 Analysis Method: SM 25400-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92405896001 METHOD BLANK: 2421859 Associated Lab Samples: 92405896001 Parameter Units Total Suspended Solids mglL LABORATORY CONTROL SAMPLE: 2421860 Parameter Units Total Suspended Solids mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 11/0711818:48 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 250 100 90-110 SAMPLE DUPLICATE: 2421861 92405854001 Dup Parameter Units Result Result Total Suspended Solids mglL ND 8.0 SAMPLE DUPLICATE: 2421862 92406039001 Dup Parameter Units Result Result Total Suspended Solids mglL 410 412 RPD Qualifiers RPD Qualifiers 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 aceAnalytical www.parelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 440509 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Associated Lab Samples: 92405896001 SAMPLE DUPLICATE: 2419615 92405971001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.4 6.3 1 H3 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 1111212018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnalX cal www pacelabs.com QUALITY CONTROL DATA ,Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 440741 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92405896001 METHOD BLANK: 2420774 Matrix: Water Associated Lab Samples: 92405896001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mglL ND 0.50 11/08/18 00:50 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 2420775 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mglL 10 10.8 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2420776 2420777 MS MSD 92405942001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L ND 10 10 11.3 11.6 112 115 90-110 2 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2420778 2420779 MS MSD 92406101001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldaht, Total mg/L 44.0 10 10 56.4 55.8 123 118 90-110 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 ace Analytical ww+.pamiabs.corn Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 440551 QC Batch Method: EPA 353.2 Rev 2.0 1993 Associated Lab Samples: 92405896001 METHOD BLANK: 2419688 Associated Lab Samples: 92405896001 Parameter Units Nitrogen, NO2 plus NO3 mg/L QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 11/07/18 09:47 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2419689 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg1L 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419690 2419691 MS MSD 92405400004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.44 2.5 2.5 2.5 2.6 82 87 75-125 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419692 2419693 MS MSD 92405400005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 my/L 0,41 2.5 2.5 2.3 2.4 76 81 75-125 4 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Pagel 1 of 18 (�IaceAnalytical www.paceiabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 440709 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 924{15896001 METHOD BLANK: 2420683 Matrix: Water Associated Lab Samples: 92405896001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 11107/1820:33 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntorsviile, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2420684 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2420685 2420686 MS MSD 92405874001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.026J 2.5 2.5 2.6 2.7 104 105 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2420687 2420688 MS MSD 92405923001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 20.1 2.5 2.5 22.6 22.6 100 100 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 1 B aceAnalytrcal wwwpacalabs.cam QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 QC Batch: 441148 Analysis Method: SM 5220D-2011 QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92405896001 METHOD BLANK: 2422559 Associated Lab Samples: 92405896001 Parameter Units Chemical oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2422560 Parameter Units Chemical oxygen Demand mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 11/09/18 00:04 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 757 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422561 2422562 MS MSD 92406236003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 107 100 100 216 216 109 109 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422563 2422564 MS MSD 92405876001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mglL ND 100 100 130 133 113 116 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 Pace Analytical Services, LLC aceAna,(X ca! 9800 Kincey Ave. Suits100 HunlersviEle, NC 28078078 www.pat,Wabs.com (704 )875-9092 QUALIFIERS Project: COMPOST CENTRAL 2 Pace Project No.: 92405896 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/12/2018 10:17 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 acmnalytical wwwpamlabs.c m QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 2 92405896 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92405896001 OUTFALL 1 EPA1664B 441313 92405896001 OUTFALL 1 EPA 200.7 Rev 4.4 1994 440463 EPA 200.7 Rev 4.4 1994 440492 92405896001 OUTFALL 1 SM 9222D-2006 440382 SM 9222D-2006 440383 92405896001 OUTFALL 1 SM 254OD-2011 440962 92405896001 OUTFALL1 EPA 9040C 440509 92405896001 OUTFALL 1 TKN*NO3+NO2 441718 Calculation 92405896001 OUTFALL 1 EPA 351.2 Rev 2.0 1993 440741 EPA 351.2 Rev 2.0 1993 440986 92405896001 OUTFALL 1 EPA 353.2 Rev 2.0 1993 440551 92405896001 OUTFALL 1 EPA 365.1 Rev 2.0 1993 440709 EPA 365.1 Rev 2.0 1993 440751 92405896001 OUTFALL 1 SM 5220D-2011 441148 SM 5220D-2011 441293 Date: 11/12/2018 10:17 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 15 of 18 Document Name: Document Revised: February 7, 2019 ;OlceAnal fCa�n Sam leCondition Upon Recei t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033•Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Client Name: r-c Courier: ❑Fed Ex ❑UPS ❑USPS ❑ Commercial ❑Pace ❑Other. Custody Seal Present? ❑Yes No Seals Intact? []Yes HuntersvllleZ Ralelgh❑ Mechanicsville[] Pr jest #: W P # : 92405896 JClient 11 �11�I EI �I ll� 1 I111i 9240SBEIS Date/1nitleisPerson ExaminingContents:r'-�" Packing Material: ❑Bubble Wrap ❑Bubble Bags a None ❑ Other Biological Tissue Frozen? Thermometer ❑Yes ❑NO [31 /A Type of lee: et ❑Blue ❑None IR Gun ID; �" Cooler Temp l'Cl: (J, / Correction Factor: Add/Subtract ('C)-1 - Temp % p should be above freezing to VC Cooler Temp Corrected I ): ❑5amples out of temp criteria. Samples on ice, waling process has begun USDA Regulated Soll ([5�'N/A, water sampie) Did samples on ate in a quarantine zone within the United States. CA, NY, or SC {check maps)? old sarnplesoriginate from a foreign source (internationally, FlYes I1lNn includlne Hawaii and Puerto RIcDI? ayes OWr No Comments/Discrepancy: Chain of Custody Present? J�Yes ❑No N A 1, Samples Arrived within Hold Time? O(e []Na ❑N/A 2. Short Hold Time Analysis IO2 hr.)? Yes No ❑NJA 3, S Rush Turn Around Time Requested? Oyes o ❑N/A 4. Sufficient Volume] es []No ❑N/A S. C_orrect Conlairiers.Used? -Pace Containers Used? Yes b Yes ❑Na ❑ND ❑N/A ❑N/A 6. Containers Intact? , Yes ND _QN1A 7, Dissolved analysts: Sam tes Field Filtered? ❑ves Cl No . N/A B. Sample Labels Match COC? -includes Date/Time/ID/Analysis Matrix: Yes ❑No ❑NJA 9. I �yw_ o i 1-7 Heads ace in VOA Vials (>5.6mm)? Oyes 0N2 2rll 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑Yes ONo ❑No ❑N//A fu/A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? [:]Yes [—]No LOT lu 01 split Containers: CLIENT NOTIFICATION/RE50LUTION Person Contacted: Date/Time: Prolect Manager SCURF Review. Dale: 11,� Project Manager SRF Review: Date: u j— Page 16 of 18 Document Name: Document Revised: February 7, 2018 —. ace Analytical" Sample Condition Upon Recel tISCUR) Pa e 1 of Z Document No.: Issuing Authority: r F-CAR-CS-033-Rev,06 Pace Carolinas Quality Office 'Check mark top half of box If pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions, VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom-haifof-box is -to -list -number -of bottle- --- Project # WQ# , 924Q5896 PN: NW13 Due Date: 11 2 11 /! 8 CLIENT: 92-NECK CO _ n ypv - Z > z Y 2 i' 2y vl x ?' u z a z ZALO z Z cl o Q Q Q T O a Z V1 O _ c c c a N O N tJ a D r� E V y Z v 0 V7 a '� '" C O a G 7 7 C 2 2 Z N Z 9 C U N 2 Q ) 2 3 A a a d a = O a O O O C m us d < 4 a a 4 E a a < a ry > > > Ci in W m o ° e c E vvi a ° `m o r� E E E g 9 n E o E E 0 Ny Ny n 0 2 O,~-1 U� N 06 Ci O Q r'1 N V7 r1 N ,Ny U • w .. .y S. N ,NJ, nl 0 Y W VE d st ][ r r a 7 A. u a m a o�, a a a 3 .. l7 ,�• l7 m l7 t7 t7 t7 a, l7 at t9 a U a+ rs a O y cn a N a m a m 17 in t7 o _ m m m m m m a a a a a a a s > v, a 1 In /Jm ! 9 YNN NZ- \N I 2 3 1 1 \\NN \'7T 4 6 X \\\N \\\I 7 g 9 10 C 11 12 pH Adjustment Log for Preserved Samples Sample 10 Type of Preservative pH upon fecelpt Date preservatlon adjusted Time preservation adjusted Amount of preservative added Lot# Note: wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office Il.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 17 of 18 116 CHAIN -OF -CUSTODY tf Analytical Request Document Ce A d1 The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accura Section A Section 6 Section C Required Client Information: Required Project Information: Invoice Information: Company: Nlecklenourp County Solid Waste Reporl To: Khaliem Adams Attention: Address: 2145 Sutge Ave. Copy To: Company Name, Crixiotte, NC 25208 Address: Regbiawy A enc Email: Fha[iem, atlams mccklenbwpcount pDY Purchase Order 0: Pace Quote, Phone (980)314-3856 Fax Project Name: Compost Central 2 Paco Project Managen mauti w.lxainard(dipacetabs,cam, Slate r Location Requested Due Date: Proiecl 0: Pace Profile Nt 3207-1 I NC Requested Ana[ sis Filtered Y1N t^ -ITRIA CGOE DincA9 Wald UW w,t« wr Yra:rr W.I. Ww aLodur v SAMPLE ID oyd5ob6 a� One Character per box. WuPe WP (A-Z D-91. -i 01" 07 Sample Ids must be unique T-- Ts - - 3 r w o x 4 a zi 0 U m u v n � q rn COLLECTED z w V 4 a r N w z z O O _ Preservatives _Z } START END C N z Z s- U D z -•% O N h m a Q N _ m O m Y ^' J d IS Lout ¢ c- O v p O y L�✓�f `.-� DATE TIME DATE TIME { C� IEl�/�i L h IR I p I XIA I I I I I I I I Lr�l 2 3" 4 5` �7 8 _ I 9 AID i1 'r -�:y. :r•'ADOmONf1L CDMI.SF.NTS,-. ��': .. ` ,-r, REc3NCU15�HED BYIAFFluAT10N ,- DATE-_;' i.�TME- ACCEPTED BY f AFFILIATION DATE-„` - T3FRE. SAtdPI-E CONgmONS- . 't � C 'l1 E-%l /7C�� i t IC, r✓ � [, :J t� �� - J � • uf/ � � - L ' L it � C �I.-' ( C7 � 03 cc ro m 0 �L Environmentol Quality Stormwater .Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling oul lhis form, please visil littl)s://deci.tic.cov/about/divisionslever<w-mineral-land- resourceslenergy-mineral-land-penniIslstormNvater permitslnj2des-industrial-sw#tabb4 Permit No.: NIC16, nor * 0 01�1�1 or Certificate of Covera =e No.: NICIGI %IIIJ 0I�I�I Facility Name: t rCLao) County: l Ij Phone No. C 70 3 — 170 9— Inspector: Y'+ It Date of inspection: 0 1g Time of Inspection: Q 4 0 Total Event Precipitation (inches): 0 ' a 0 All permits require qualitative monitoring to be performed during a `'measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted silc Outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the perinittee obtains approval from the local DEML IZ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permitlee or Designee) 1. Outfall Description: n : 0� Outfall No. Structure (pipe, ditch, etc.): Y e V Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: hC4 t yMI, Cie Mk*k-o,-kA Page I of SWl]-242, Last modified 0712812017 2. Color: Describe the color of the lisch4rge using (light, medium, dark) as descriptors: 9 cz4LW — 3. Odor: Describe ny distinct odors that the disch chlorine odor, etc.): t, 0 dA S f,(' is colors (red, brown, blue, etc.) and tint own +0 1iah�- brawn may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no solids and 5 is the surface covered with floating solids: Cl 2 3 4 5 C. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where l is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the storm.water discharge? O Yes � No. S. Is there an oil sheen in the stormwater discharge? OYes c'3 No, (' 9. Is there evidence of erosion or deposition at the oudall'? O Yes 40. 10. Other Obvious Indicators of Storm�,�j�ater, Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 CHAIN -OF -CUSTODY 1 Analytical Request Document .� The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be enmpleted accurately. i Section A Section 5 Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company: Mecklenburg County Solid Waste Report TO: Khaliem Adams Attention: Address, 2145 Suttle Ave. Copy To: Company Name; Charlotte. NC 28208 Address: Email: khaliem,adams@mecklent)urgcnunlync.gov Purchase Order #: Pace Quote: Phone: (980)314-3856 Fax Project Name: Compost Central 2 Pace Project Manager: malthew.brainard acelabs.com. i'S{ M =: State 1 G1c'atiori't s "0` :�•: Requested Due Date: Project #: Pace Profile #: 3207-1 NC s:.S?R nested"Anal Es Fltered- !N 2�i �r 11'3R4 ��.'k"' � ; KATR1X CODE 0 COLLECTED � Preservatives rem N rkin" Wata Dw 3 Watc WS Waste warn WW.0 Proaucr P U 0 ❑ z SAMPLE ID So'lvs.w SL oL 7 START END U n �N4 w r c One Character per box. wiwPs m a z m w c o ft (A•2;0-91 -) ar ax timer ❑p O i ~ w ~ ¢ Z m m k�= I. ZE g° ._ = o- U Sample Ids must be unique P q T sue s i X TIAIET111 w O v O e ir0i U 2 U 0v a W K a a a U O © c p N ''� 2 U = m uHi m i° m t t C� 71 A P o = m 0. O m rn DATE TIME w +t _ _ = z Z O 24 +1 r 5l 11N I8 �I N6 11 L I I I I I L I - r^v.� ._� :....... �...} r'd4 'ryyr" - i ADDITIONAi COMMEt1T5y`�. .,, - '.:eL�tn_vi RELINQUISHED %Y'AI •++3'ri-::..F �u.Yt!e-SAL -- eY,f AFflLIATtON� .,�.u4 SL DATE - 4�'. TIME^ACCEPTED Mioc..: _-., 1i"#R'ssc-r �.�-X. �y.4'Yd� BYf AFFILEATIDN�,x-� �+'p-'.;=ZEM1F�:ITCA Y'S OA .T1ME`� �e'� SAAiSPLE CONDITIONS °e,giSctF�� �w'�-.� t�3% 9�� il6ha (lem Adar-s{t s lose. J - ti-Q-tY toy Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 10/22/2018 CERTIFICATE OF COVERAGE NO. NCG240019 FACILITY NAME Mecklenburg County Compost Central (new) COUNTY Meck lenburg Count PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services_ Lab Cert. # 92 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ® Monthly' October (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑water Supply [—]SA RE CIE-IVED ❑Other Part A: Stormwater Benchmarks and Monitoring Results ��,';, Total event rainfall 2.0 in or ❑ No discharge this period3 Date Sample . Collected' (mo/dd/yr) Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc PH Parameter benchmarks =__> 100 mg/L" 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 10/12/2018 1 11.9 131 6000 3.1 0.81 0.0050 <0.0050 0.010 6.7 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM TSS Total Rainfall' Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L" - - 10/12/2018 1 6.7 <4.8 11.9 2.0 75 gal/month Footnotes from Part A also apply to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one coon of this DMR. includina all "No Discharae" reoorts. within 30 days of receipt of the lab results for at end of monitoring Period in the case of "No Discharae" reoorts! to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICA►!ON FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." c ?2 (Date) it Elate: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 13 1 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out thisform, please visit littps://deg,nc.l4ov/about/divisions/erterey-mineral-1,,ind- resources/energy-mineral-land-permitslstorni pater-pennits(npdes-industrial-sw#tab-4 Permit No.: NICIG al l 0I 1-01& or Certificate of Coverage No.: NICIG/4j/Q/(?lZl j Facility Name: /I// (',C f jL'�1'D Cll�l� County: IVI ICf� C)L,4 Inspector: Ct /f t Date of Inspection: �D �G a U Time of Inspection: Phone No. I( 70 416 J 7 r 1 "Total Event Precipitation (inches): �?t 0 MGAX1j All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply ifthe permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office, By this signature, I certify that this report is accurate and complete to the best of my knowledge: - I % n (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. Structure (pipe, ditch.. etc.): how-, �u � pe-4- Receiving Stream: D4scribe the industrial activities that occur within the outfall drainage area: f � 1209+jOq / 1I (7, Imo,, C I!L � t � f tom'! 0--r-.O/ Page I of 2 S Wt1-242, fast modified 07/28/2017 2. Color: Describe the color of the disc (light, medium, dark) as descriptors: using basic colors (red, brown, blue, etc.) and tint I„ I. , 3. Odor: Describe 1 `S dis in t odors th the di chlorine odor, etc_): may have (i.e., smells strongly of oil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids ill the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? 0/Yes O No. 8. is there an oil sheen in the stormwater discharge? 0Yes G%'No. 9. Is there evidence of erosion or deposition at the outfall? O Yes Q/No. 0 10. Other Obvious Indicators of Stormwater Pollution: List and describe No Ohe4- i m(lii:dio Dote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may he indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, last modified 07/28/2017 aceAnalytical www.paceJabs.com October 18, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 12, 2018, The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew. brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste pGCRF�� 3'NI REPORT OF LABORATORY ANALYSIS This report shad not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 Pace Analytical Services, LLC aceAnalytrcal 9800 KinceyAve. Suite100 Huntersville, NC 28078078 wwwpacelabs.ocm (704)875-9092 CERTIFICATIONS Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersvitle, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification lDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 aceAnalytical www.pacelabs.c= SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 26073 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 2 92403209 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92403209001 OUTFALL 001 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 SH1 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 CEH 1 PASI-A EPA 9040C RLO 1 PASI-A TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 GC 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuli, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 aceAnalytrcal" , wWw.pBoelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 Sample: OUTFALL 001 Lab ID: 92403209001 Collected: 10/12/18 08:11 Received: 10/12/18 08:59 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 4.8 1 10/17/18 01:51 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 2007 Rev 4.4 1994 Copper 0.01i mg1L 0.0050 1 10113/1813:45 1011411819:27 7440-50-8 Lead ND mg1L 0.0050 1 10/13/1813:45 1011411819:27 7439-92-1 Zinc D.010 mg/L 0.010 1 10/1311813:45 10/14/1819:27 7440.66-6 M12110 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 6000 CFU1100 mL 1.0 1 10/12/18 15:53 10113/18 17:13 D6,u2 2540D Total Suspended Solids Analytical Method: SM 254OD-2011 Total Suspended Solids 11.9 mg/L 6.9 1 10/16/18 02:39 9040 pH Analytical Method: EPA9040C pH at 25 Degrees C 6.7 Sid. Units 0,10 1 10/16/18 05:36 H3 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 3.1 mg/L 0.52 1 10/18/18 14:54 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 3.1 mg/L 0.50 1 10/14/18 14:41 10/16/18 01:13 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg/L 0.020 1 10/17118 10:37 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.81 mg/L 0.050 1 10/16/18 19:DD 10/17/18 01:26 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 131 mg/L 25.0 1 10/15118 20:00 10/16118 20:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:57 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnalytical wwwpacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436564 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92403209001 METHOD BLANK: 2401908 Matrix: Water Associated Lab Samples: 92403209001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg1L ND 4.8 10/17/18 01:42 LABORATORY CONTROL SAMPLE: 2401909 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 2D.1 104 64-132 MATRIX SPIKE SAMPLE: 2401910 35423403002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 4.8U 19.2 21.4 111 64-132 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:57 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 I eAnalytical w w.pacelabs.aom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436114 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA200.7 Rev4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92403209001 Pace Analytical Services, LLC 9B00 Kincey Ave. Suite 100 Hunlersviile, NC 28078 (704)875-9092 METHOD BLANK: 2399B09 Matrix: Water Associated Lab Samples: 92403209001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg1L ND 0.0050 10/1411818746 Lead mg1L ND 0.0050 10114/1818:46 Zinc mg1L ND 0.010 10/14/1818:46 LABORATORY CONTROL SAMPLE: 2399810 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper mg1L .5 0.52 103 85-115 Lead mg1L 5 0.49 98 85-115 Zinc mg1L .5 0.49 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399811 2399812 MS MSD 92403064001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 2.6 .5 .5 3.1 3.2 82 105 70-130 4 Lead mg/L 0.0050 .5 .5 0.52 0.53 102 106 70-130 3 Zinc mg/L 1.7 .5 .5 2.3 2.3 104 122 70-130 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2399813 2399814 MS MSD 92403281001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Copper mg/L 8.9 ug/L .5 .5 0,53 0.54 105 106 70-130 1 Lead mg/L ND .5 .5 0,51 0,51 101 101 70-130 0 Zinc mg/L 33.9 .5 .5 0.55 0.55 104 104 70-130 0 ug/L Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2048 02:57 PM without the written consent of Pace Analytical Services, LLC, Page 6 of 18 I eAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436043 Analysis Method: SM 9222D-2006 QC Batch Method: SM 9222D-2006 Analysis Description: 9222D Fecal Coliform(MF) - CHT Associated Lab Samples: 92403209001 METHOD BLANK: 2399587 Matrix: Water Associated Lab Samples: 92403209001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 10/13/18 17:13 SAMPLE DUPLICATE: 23995BB 92403209001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFUI100 mL 6000 600 164 D6,u2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 2BO78 (704)875-9092 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/11312018 02:57 PM without the written consent of Pace AnalyScal Services, LLC. Page 7 of 18 lacieAnayical wwwpacelabs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436341 Analysis Method: SM 254OD-2011 QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92403209001 METHOD BLANK: 2400752 Associated Lab Samples: 92403209001 Parameter Units Total Suspended Solids mg[L LABORATORY CONTROL SAMPLE: 2400753 Parameter units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2400754 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2400755 Parameter Total Suspended Solids Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 10116118 02:36 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 251 246 98 90-110 92403318001 Dup Result Result RPD Qualifiers 2440 2140 13 D6 92402710007 Dup Units Result Result mg/L ND ND RPD Qualifiers Results presented on this page are In the units indicated by the"Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10118/2018 02:57 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 (�IacieAnalj&al www.pacelabs.com Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436345 QC Batch Method: EPA 9040C Associated Lab Samples. 92403209001 SAMPLE DUPLICATE: 2400761 Parameter Units pH at 25 Degrees C Std. Units SAMPLE DUPLICATE: 2400762 Parameter pH at 25 Degrees C QUALITY CONTROL DATA Analysis Method: EPA 9040C Analysis Description: 9040 pH 92403054001 Dup Result Result RPD Qualifiers 7.3 7.3 0 H3 92403281002 Dup Units Result Result Std. Units 6.3 6.3 RPD Qualifiers 1 H3 Pace Analytical Services, LLC 9800 Kinsey Ave. Suite 100 Hunlersville, NC 28078 (704)875.9092 Results presented on this page are In the units Indicated by the" Units" column except wtiere an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:57 PM without the written consent of Pace Analytical Services, LLC, Page 9 of 18 aceAnalytical wwrw.pacelabs.cam Pro;ect: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436148 QC Batch Method: EPA 351.2 Rev 2.0 1993 Associated Lab Samples: 92403209001 METHOD BLANK: 2399875 Associated Lab Samples: 92403209001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 2399876 Parameter Units Nitrogen, Kjeldahl, Total mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 10/16/18 00:56 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 9.4 94 90-110 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2399877 2399878 MS MSD 92402844001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.1 10 10 9.7 10.9 86 98 90-110 11 M1,R1 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2399879 2399880 MS MSD 92403137001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L 4.8 10 10 15,5 15.6 107 109 90-110 1 Results presented on this page are in the units indicated by the"1lnits" column except where an alternate unit Is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:57 PM without the wr tten consent of Pace Analytical Services, LLC. Page 10 of 18 (:"a'ne Analytical wwwpamiabs.com Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436373 OC Batch Method: EPA 353.2 Rev 2.0 1993 Associated Lab Samples: 92403209001 METHOD BLANK: 2400847 Associated Lab Samples: 92403209001 Parameter Units Nitrogen, NO2 plus NO3 mglL LABORATORY CONTROL SAMPLE: 2400848 Parameter Units Nitrogen, NO2 plus NO3 mglL Pace Analytical Services, LLC 9800 Kircey Ave. Suite 100 Hurtersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 10/17/18 10:15 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400849 2400850 MS MSD 92402332002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 4,0 2.5 2.5 6.0 6.0 82 81 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 2400851 2400852 MS MSD 92402419001 Spike Spike MS MSD M5 MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.24 2.5 2.5 1.6 1.6 55 55 75-125 1 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10I1812018 02:57 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalytical www.pacalabs.com Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436494 QC Batch Method: EPA 365.1 Rev 2.0 1993 Associated Laic Samples: 92403209001 METHOD BLANK: 2401745 Associated Lab Samples: 92403209001 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE: 2401746 Parameter Units Phosphorus mglL Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 10/17/18 01:13 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.6 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2401747 2401748 MS MSD 92403453001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg1L ND 2.5 2.5 2.6 2.5 103 102 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2401749 2401750 MS MSD 92403209001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.81 2.5 2,5 3.5 3.4 108 105 90-110 2 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:57 PM without the written consent of Pace Analytical services, LLC. Page 12 of 18 aceAnalytical www.parslabs.cam QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 QC Batch: 436319 Analysis Method: SM 5220D-2011 QC Balch Method: SM 5220D-2011 Analysis Description: 5220D COD Associated Lab Samples: 92403209001 METHOD BLANK: 2400688 Matrix: Water Associated Lab Samples: 92403209001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mglL ND 25.0 10/16/18 20:08 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2400689 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 751 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400690 2400691 MS MSD 92403094001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Chemical Oxygen Demand mglL 69.8 100 100 209 190 140 121 90-110 9 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2400692 2400693 MS MSD 92403287002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua! Chemical Oxygen Demand mglL 27.2 100 100 157 148 130 121 90-110 5 M1,R1 Results presented on this page are in the units indicated by the"Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/18/2018 02:57 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 Pace Analytical Services, LLC Iace na(�lyti cal 9800 4 ncey Ave. Suite 100 H Hunter5ville, NC 28078 wwwpamfabs.com (704)875-9092 QUALIFIERS Project: COMPOST CENTRAL 2 Pace Project No.: 92403209 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyle in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SV11846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NEt AC Institute, LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: I W18/2018 02:57 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 aceAnalytical www.pamlabs.carn QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLG 9800 K( ncey Ave, Suite 100 Huntersville, NC 28078 (704)875.9092 Project: Pace Project No.: COMPOST CENTRAL 2 92403209 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92403209001 OUTFALL 001 EPA 1664B 436564 92403209001 OUTFALL 001 EPA 200.7 Rev 4.4 1994 436114 EPA 200.7 Rev 4.4 1994 436138 92403209001 OUTFALL 001 SM 9222D-2006 436043 SM 9222D-2006 436044 92403209001 OUTFALL 001 SM 25400-2011 436341 92403209001 OUTFALL 001 EPA 9040C 436345 92403209001 OUTFALL 001 TKN+NO3+NO2 437006 Catculation 92403209001 OUTFALL 001 EPA 351.2 Rev 2.0 1993 436148 EPA 351.2 Rev 2.0 1993 436330 92403209001 OUTFALL 001 EPA 353.2 Rev 2.0 1993 436373 92403209001 OUTFALL 001 EPA 365.1 Rev 2.0 1993 436494 EPA 365.1 Rev 2.0 1993 436541 92403209001 OUTFALL 001 SM 5220D-2011 436319 SM 5220D-2011 436532 Date: 10/18/2018 02:57 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 Document Name: Document Revised: February 7, 2018 h — JceAMAGal— Sample Condition Upon Recet t(SCUR) Page 1 of 2 NM:- issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville-[ Raleigh❑ Mechaanicsville❑ Client Narn : Ari0 ; 92403209 I �� q Project; 1{/IIH ` Courier: ❑Fed Ex ,VDun `❑L}USPS} � '�Crl,nt III Q I J1 I III I1��� ❑ Commercial ❑Pace ❑Other: 111I �, 92403209 Custody Seat Present? [-]Yes/ No Seals Intact? []YesQNo Date/Initials Person Examinfgg Came Parking Material: ❑Bubble wrap ClOubble Bags ❑None ❑ other Thermometer: un ID: 92TO45 Type of ice -wet ❑Blue q Cooler Temp ('Cir Correction Factor: Add/Subtract )'Ci {j Cooler Temp Corrected ('C): USDA Regulated Soil .�Q N/A, water sample) Did samples orginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? 11Yes fflrzo Biological Tissue Frozen? [:]Yes❑No [-]N/A [:]None Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on Ire, cooling process hasbegun Did samples originate from a foreign source {intrer�nationally, includtAQ Hawaii and Puerto RicoP f `iYes C-INO Cam ments/0lscre ancy: Chain of Custody Present? ❑vas QUO []N/A 1. Samples Arrived within Hold Time?©yei ❑No N/A 2. Short Hold Time Anal sis (a72 hr.)? s jwes ONO []NIA 3. Rush Turn Around Time Requested? Yes - o ❑N/A 4. Sufficient Volume? t Yes No ❑N/A 5. Correct Containers Used? \❑'yeses ONO ❑NIA 6. -Pace Containers Used? C[jYds ❑No ❑NIA Containers Intact? b Yes Div,, 7, Dissolved analysis: Samples Field filtered? ❑Yes ONO ��N/'�A �DN]A B. Sample Labels Match CDC? i�i� ❑Na ©NIA 9. -�� � ! � -IncludesDate/Time/ID/Analyshs Matrix: 1! Headspace in VOA Vials (55.6mml? Dyes, ` No []lf A 10. Trip Blank Present? ❑Ycs'-j] O ❑N/A 11. Trip Blank Custody Seals Present? ❑Yes No ❑N/A COMMENTS/SAMPLE DISCREPANCY Lot ID of split Containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? ❑Yes ❑No Page 16 of 18 r CHAIN -OF -CUSTODY 1 Analytical Request Document �.:. 1 - The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section a Section C i Requlmd Client Information: Required Project Information: Invoice Information: Page 1 Of 1 ReportTo: Khaliem AdnmS Attention: j Copy To: Company Name: Company: Merklenhurq County Solid Waste Address: 2145 Suttle Ave. Charlotte, NC 28208 Address; - �"Regulztory Agancyw . ..• Email: kAaliern.adarnsipmecklenbur nt nc qov Purchase Order p: Paco Quote: I Phone: (960)314-3856 Fax Project Name: Compost Central 2 Pace Project Manager, n%alLhew.brainard@pacelabs.com. 7- =state I Location Requested Due Date: Project #: Pace Profile p; 3207-1 NC I R ueatod Ana! Is Flllered 1N 'x' yA x gopE u COLLECTED z Preservatives Y_ - a n orv,. w", wain �v wrw e 3 v W.: w.:n w w � z p O V } SAMPLE ID a u START END o !m x a, _ ¢ F J C One Character per box. wlp. WP W w w O •} Go tA'Z, 0-91.v-, or u Sample leis must be unique in:v TS x w o r ON q m- ca z v ii a o ca z c� O f �If�%iJf ~ DATE TIME DATE TIME = 2 = O 1 I - 979`7 +c%/ X1 OY 'XIXI I I (�Ut r-ri.err 3. 4-4 5 6 -7 s�-. I I ,9� t f.;hy Y`7 yet :i:Y ADDfTTONAL'•GOMIAENTS� c_e ..,ip��''-(.'. �s•'� re "''•REiJNGU15HFA 8Yf AF}lLthTIDN b ;=} %.r'flAT£�i `s »'vy`..T1ME r�'�-� -i BYl��LL1A7iON Sy fib' �i+:q DATE r: �- �i[11E••: -,T- �i'!9AMPLNII DONS EtO • J..r1-Scsv"s .-4. rr.�.. _ -xt,. .:fc t�:_ .Tr1.:y, wFi- w.:-wrcr-r-n-..M^ ..r�r.rcw:-� �r. _�:�� •.c.., t'��E"-+,''ACCEPTED !! x: .d. :/ - .3�. n,F�' .�i-.y:'i - .I- Y t l -- 0 Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 8/1/2018 CERTIFICATE OF COVERAGE NO. NCG240019 FACILITY NAME Mecklenburg County Compost Central (new) COUNTY Mecklenburg County PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 92 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ❑ Jan -March ❑ April -June ® July -Sept ❑ Oct -Dec or ❑ Monthly' _ _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA RECE 'EQZero-flow ❑Water Supply ❑SA AUG 0 $ 2018❑Other CENTRAL FILES DWR SECTION Total event rainfall z 0.34 in or ❑ No discharge this period Date Sample Collected' (mo/dd/yr) Outfall No. TSS COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L° 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 07/24/2018 1 16.4 137 6000 4.0 0.83 <0.0050 <0.0050 0.010 7.7 ' Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part ts: vehicle nnaintenance Area Ivlonitoring Kesults: only Tor Taclllues averaging > 5.5 gal or new mot Date Sample Collected' (mo/dd/yr) - Outfall No. - pH T TPH using method 1664A SGT-HEM TS5 Total Rainfall' Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L' - - 07/24/2018 1 7.7 <5.0 16.4 0.34 75 gal/month Footnotes from Part A also annlv to this Part B FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. or oil/month. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Marl an oriainal and one cony of this DMR. includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." rre bi( 4rmitteej (Date)' Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 Emvironmenlat Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance onfilling out Ihisforin, please vi.sil httl2s://dN.iie.eov/aboti /divisioiis/eneri�,Y-mine resources/ener�,gy-m i neral-1and- permits/stormwater-perm its/npdes-ind ustri al-sw4tab-4 Permit No.: N/C/. Facility Name: County: A LU 101&I/ or Cer�ilicate of Coverage No Phone No. a/YlIj/a/1/I/ -770 <— Inspector: n QU I 1 -(:�r r/ Date of Inspection 0 Time of Inspection: "Total Frvent Precipitation (inches): Q' 3 I All permits require qualitative nnonitoring to be performed during a `measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site Outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply i f the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. j Structure (pipe, ditch, etc.): �� P-C, Receiving Stream: Describe the industrial activities that occur within the outfall drainage area:Spy d- Page 1 of 2 SWU-242, fast mod ified07/28/2017 2. Color: Describe the color of th`e dischargeru�sing basic color (red. brown, blue, etc.) and tint (light, medium, dark) as descriptors: U �rV 40- A+ l I 3. Odor: Describe any distinct odI hat t]h di chlorine odor, etc.): o od.,IEV, may have (i.e., smells strongly of oil, weak t. Clarity: Choose the number which best describes the clarity of the discharge, where l is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stonrwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: (D 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 2 3 4 5 7. 8. 9. Is there any foam in the stormwater discharge? O Yes is there an oil sheen in the stormwater discharge? OYes Is there evidence of erosion or deposition at the outfall? O Yes to. Other Obvious Indicatorso fStormwater Pollution: List and describe No dVet,�wr- CP" No. o Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, last modified 07/2812017 aceAnalytical www.pacafabs.aam August 01, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 2 Pace Project No.: 92392987 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, incerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Mecienburg County Solid Waste REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 acmnalytical www.pacwlabs.wm Project: Compost Central 2 Pace Project No.: 92392987 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huwersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170029 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E8764B Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 FloridaMELAP Certification #: E87627 Kentucky UST Certification #: 84 VirginiaNELAP Cer3ification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 9903DD01 VirginiafVELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 113 aceAnalytrcal www.pacafabs.com SAMPLE ANALYTE COUNT Project: Compost Central 2 Pace Project No.: 92392987 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NG 28078 {704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92392987001 Outfall 1 EPA 166413 JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 IDS 3 PASI-A SM 9222D-2006 KDF 1 PASI-C SM 254OD-2011 CRV 1 PASI-A EPA 9040C MDW 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 Rev 2.0 1993 BRJ 1 PASI-A EPA 353.2 Rev 2.0 1993 DMN 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A SM 5220D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 3 of 18 (�IaceAnalytical wwwpacelabs.00m ANALYTICAL RESULTS Pace analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersOle, NC 2807B (704)875-9092 Project: Compost Central 2 Pace Project No.: 92392987 Sample: Outfall 1 Lab ID: 92392987001 Collected: 07/24/18 08:56 Received: 07/24/18 09:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg1L 5.0 1 07/26/18 03:28 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Copper ND mg/L 0.0050 1 07125/18 04:00 07125/18 14:13 7440-50-8 Lead ND mg/L 0.0050 1 07/25/18 04:00 07125/18 14:13 7439-92-1 Zinc ND mg/L 0.010 1 07/25/18 04:00 07125/18 14:13 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 922217-2006 Preparation Method: SM 9222D-2006 Fecal Coliforms 6000 CFU1100 mL 1.0 1 07/24/18 15:15 07/25118 13:19 u2 2540D Total Suspended Solids Analytical Method: SM 2540D-2011 Total Suspended Solids 16.4 mg1L 10.0 1 07/26/18 21:55 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.7 Std. Units 0.10 1 07/25/18 04:20 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 4.0 mg1L 0.52 1 08/01/18 08:52 351.2 Total Kjeldahl Nitrogen Anatytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 4.0 mg1L 0.50 1 07/25/18 05:18 07/28/18 00:31 7727-37-9 353.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 ND mg/L 0.020 1 07/31/18 12:05 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 0.83 mglL 0.050 1 07/25/18 15:52 07/27/18 03:04 7723-14-0 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 137 mg/L 25.0 1 07125/18 23:52 07/26/18 18:29 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/01 /201 B 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 19 acmnaiXical wwwpacelabs.com QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 421183 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Associated Lab Samples: 92392987001 METHOD BLANK: 2332713 Associated Lab Samples: 92392987001 Parameter Units Total Petroleum Hydrocarbons mg/L LABORATORY CONTROL SAMPLE: 2332714 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (7D4)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 4.8 07/26/18 03:13 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 19.2 19.5 101 64-132 MATRIX SPIKE SAMPLE: 2332715 35405365007 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 5.OU 20 19.1 96 64-132 Resutts presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08101/2018 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 m ace Analytical mmpacelabs.com Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 420878 QC Batch Method: EPA 200.7 Rev 4.4 1991 Associated Lab Samples: 92392987001 METHOD BLANK: 2331472 Associated Lab Samples: 92392987001 Parameter Copper Lead Zinc QUALITY CONTROL DATA Analysis Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Units Result Limit Analyzed mg/L ND 0.0050 0712511813:51 mg1L ND 0.0050 07I2511813:51 mg/L N❑ 0.010 07/2611819:11 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 2331473 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg1L 5 0.48 97 85-115 Lead mg1L .5 0,44 89 85-115 Zinc mglL .5 0.44 88 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2331476 2331477 MS MSD 92393008001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg1L 5.3 ug1L .5 .5 0.48 0.49 95 97 70-130 2 Lead mg1L ND .5 .5 0.44 0.45 88 90 70-130 2 Zinc mg1L 24.4 .5 .5 0.46 0,47 87 89 70-130 3 ug1L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2331482 2331483 MS MSD 92392929001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Copper mg/L ND .5 .5 0.49 0.49 97 97 70-130 0 Lead mg/L ND .5 .5 0.43 0.43 85 86 70-130 1 Zinc mg/L 0.021 .5 .5 0.45 0.45 85 86 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/0112018 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 ace Analytical www.pawlabs.com Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 421070 QC Batch Method: SM 9222D-2006 Associated Lab Samples: 92392987001 METHOD BLANK: 2332201 Associated Lab Samples: 92392987001 Parameter Units Fecal Coliforms CFU1100 mL SAMPLE DUPLICATE: 2332202 Parameter Units Fecal Coliforms CFU1100 mL QUALITY CONTROL DATA Analysis Method: SM 922213-2006 Analysis Description: 9222D Fecal Cofiform(MF) - CHT Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 07/25/1813:19 92393066003 Dup Result Result RPD Qualifiers 22.0 30.0 31 D6,u1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 08/01/2D18 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 (�aceAnalytical www.paceliibs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9B00 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 421415 Analysis Method: SM 254OD-2011 QC Batch Method: SM 2540D-2011 Analysts Description: 2540D Total Suspended Solids Associated Lab Samples: 92392987001 METHOD BLANK: 2333858 Matrix: Water Associated Lab Samples: 92392987001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Tota4 Suspended Solids mg1L ND 2.5 07/26/18 21:51 LABORATORY CONTROL SAMPLE: 2333859 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/l_ 250 246 98 90-110 SAMPLE DUPLICATE: 2333860 92393019001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 25.2 25.9 3 SAMPLE DUPLICATE: 2333861 92393204002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mglL 39.2 46.6 17 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/01/201 B 08:53 AM without the written consent of Pace Analytical Services, LLC. Page B of 18 (�IaneAnalytrcaI wrvwpacerabs.com Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 420875 QC Batch Method: EPA 9040C Associated Lab Samples: 92392987001 SAMPLE DUPLICATE: 2331458 Parameter Units pH at 25 Degrees C Std. Units SAMPLE DUPLICATE; 2331459 Parameter pH at 25 Degrees C QUALITY CONTROL DATA Analysis Method: EPA 9040C Analysis Description: 9040 pH 92393132004 Dup Result Result RPD Qualifiers 7.4 7A 4 H6 92393132002 Dup Units Result Result Std. Units 7.2 6.5 RPD Qualifiers 10 D6,H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/01/2018 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnalytrcal MM..paoel8bs.com QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 420880 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Associated Lab Samples: 92392987001 METHOD BLANK: 2331484 Matrix: Water Associated Lab Samples: 92392987001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0,50 07/28118 00:26 Pace Analytical Services, LLC 9500 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2331485 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.2 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2331486 2331487 MS MSD 92392223001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L ND 10 10 10.7 10.4 104 101 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2331488 2331489 MS MSD 92393100002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.1 10 10 10.0 9.9 89 88 90-110 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 0810112018 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 lacmnaiXicall' wwwpacolabs.com QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 421985 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92392987001 METHOD BLANK: 2336152 Matrix: Water Associated Lab Samples: 92392987001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg1L ND 0.020 07/31/18 10:45 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875.9092 LABORATORY CONTROL SAMPLE: 2336153 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mglL 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2336154 2336155 MS MSD 92392939005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 1.2 2.5 2.5 3.6 3.6 97 95 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2336156 2336157 MS MSD 92392939006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L ND 2.5 2.5 2.4 2.4 96 97 75-125 1 Results presented on this page are In the units Indicated by the" Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 08/01/2018 08:53 AM without the written consent of Pace Analytical Services, LLC, Page 11 of 18 (�IacieAnalyfical" wwwpac9labs-ow Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 421019 QC Batch Method: EPA 365.1 Rev 2.0 1993 Associated Lab Samples: 92392987001 METHOD BLANK: 2331956 Associated Lab Samples: 92392987001 Parameter Units Phosphorus mg/L QUALITY CONTROL DATA Analysis Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 07/27/18 02:48 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2331957 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg1L 2.5 2.6 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2331958 2331959 MS MSD 92392939003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg1L 0.052 2.5 2.5 2.7 2.7 107 107 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2331960 2331961 MS MSD 92392939013 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Quat Phosphorus mg/L ND 2.5 2.5 2.8 2.7 112 107 90-110 4 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/01/2018 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 (�IaceAnalytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 2 Pace Project No.: 92392987 QC Batch: 421157 Analysis Method: SM 5220D-2011 QC Batch Method: SM 522DD-2011 Analysis Description: 5220D COD Associated Lab Samples: 92392987001 METHOD BLANK: 2332621 Matrix: Water Associated Lab Samples: 92392987001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg1L ND 25.0 07/26/18 18:28 LABORATORY CONTROL SAMPLE: 2332622 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 744 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2332623 2332624 MS MSD 92392923001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 100 100 125 137 106 118 90-110 9 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2332625 2332626 MS MSD 92393100001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 39.7 100 100 162 153 122 113 90-110 6 M1,R1 Results presented on this page are In the units Indicated by the "units" column except where an alternate unit Is presented to the right of the result. Date: 08/01/2018 08:53 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 18 aceAnalytical wvmpacerabscom QUALIFIERS Project: Compost Central 2 Pace Project No.: 92392987 DEFINITIONS Pace Analytical Services, LLG 9800 Kinsey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Dup€icate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and Cannot be Separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD va?ue was outside control limits. u1 Results based upon colony counts outside acceptable range. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/01/2018 08:53 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 4 27 2018 CERTIFICATE OF COVERAGE NO. NCG240019 FACILITY NAME Mecklenburg County Compost Central (new) COUNTY Mecklenburg County PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 92 Comments on sample collection or analysis: SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ❑ Jan -March ® April -June ❑ July -Sept ❑ Oct -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW [—]Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA RECEi /ED ❑Other MAY 0 3 2018 CEN'rkAL FILES Part A: Stormwater Benchmarks and Monitoring Results DWR SECTION Total event rainfall 2 0.80in or ❑ No discharge this period' Date Sample Colle Collected' (mo/ cted Outfall No. 755 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks ===> 100 mg/L' 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 4/17/2018 1 25.4 77.0 6000 2.5 0.44 0.0051 <0.0050 0.012 7.3 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit ©ate: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part rj: vehicle iviaintenance Area iviorntoring Results: only for Tacilitles averaging > 55 gal OT new mot Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM TSS Total Rainfall' Check if No Flow This Period Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L4 - - 4/17/2018 1 7.3 <5.0 25.4 0.80 75 gal/month Footnotes from Part A also aooly to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART If SECTION B. or oil/month. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ® NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one coov of this DMR. includina all "No Dischorae" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Dischorae" reoorts) to: Division of Water Quality Attw DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significaWpryhalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Sign Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 2 of 2 aceAnalytical w6m acelabs.mm April 25, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on April 17, 2018, The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste pCCgg�� a; TN[ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 Pace Analytical Services, LLC ® 9800 Kincey Ave. Suite 100 Huntersville, NC 2807$ (�IacVimna wwwpocul©bs.com (704)875-9092 CERTIFICATIONS Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 FforidalNELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NCO30 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 laceAnalytical W-6wpacalabs.aam SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: COMPOST CENTRAL 2 92381218 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92381218001 OUTFALL 001 EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASI-A SM 92221) KDF 1 PASI-C SM 2540D EJJ 1 PASI-A EPA 9040 RLO 1 PASI-A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA 353.2 DMN 1 PASI-A EPA 365.1 MDW 1 PASI-A SM 52201) MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 acmnalyfical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersOle, NC 28078' (704)875-9092 Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 Sample: OUTFALL 001 Lab ID: 92381218001 Collected: 04/17/18 15:50 Received: 04/17/18 17:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mi 5.0 1 04/20/18 04:46 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0=51 mg/L 0.0050 1 04/19/18 00:45 04/21/18 17:43 7440-50-8 Lead ND ni 0.0050 1 04/19/18 00:45 04/21/18 17:43 7439-92-1 Zinc 0.012 mg/L 0.010 1 04/19/18 00:45 04/21/18 17:43 7440-66-6 MSIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 6000 CFU1100 mL 1.0 1 04/17/18 18:16 u2 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 25.4 mg1L 7.1 1 04/19/18 19:16 9040 pH Analytical Method: EPA 9040 pH 7.3 Slid. Units 0.10 1 04/18/18 04:11 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 2.5 mglL 0.52 1 04/24/18 12:07 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 2.5 ni 0.50 1 04/21/18 09:02 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 ND ni 0.020 1 04/20/18 14:03 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 0.44 ni 0.050 1 04/18/18 22:47 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 77.0 ni 25.0 1 04/25/18 00:32 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 18 (�IaceAnalytical" www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 2807e (704)875-9092 Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 407080 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92381218001 METHOD BLANK: 2258850 Associated Lab Samples: 92381218001 Parameter Units Total Petroleum Hydrocarbons mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 04120/18 04:34 LABORATORY CONTROL SAMPLE: 2258851 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 19.2 19.7 103 64-132 MATRIX SPIKE SAMPLE: 2258852 92381487001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 19.2 19.5 99 64-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 (�IaceAnalytical" www.pacelahs.com QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 406887 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92381218001 METHOD BLANK: 2257498 Matrix: Water Associated Lab Samples: 92381218001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 04/21/1816:29 Lead mg/L ND 0.0050 04121I1816:29 Zinc mg/L ND 0.010 04/2111816:29 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Humersviile, NC 28079 (704)875-9092 LABORATORY CONTROL SAMPLE: 2257499 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L .5 0.49 99 85-115 Lead mglL .5 0.45 90 85-115 Zinc mg/L .5 0.44 89 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2257500 2257501 MS MSD 92381014001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND 5 .5 0.47 0,45 94 89 70-130 6 Lead mg/L ND .5 .5 0.45 0.42 89 84 70-130 6 Zinc mg/L ND .5 .5 0.44 0.42 89 83 70-130 6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2257502 2257503 MS MSD 92381014011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND .5 .5 0.45 0.47 90 95 70-130 5 Lead mg/L ND 5 .5 0.42 0.44 83 88 70-130 5 Zinc mg/L 15.4 .5 .5 0.43 0.45 82 87 70-130 5 ug/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 (�IacieAnalytical ww.pacelabs.c= QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 406841 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 92221) MBIO Fecal Coliform - CHT Associated Lab Samples: 92381218001 METHOD BLANK: 2257339 Matrix: Water Associated Lab Samples: 92381218001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 04/17/18 18:16 SAMPLE DUPLICATE: 2257340 Parameter Fecal Coliforms 923812180D1 Dup Units Result Result CFU1100 mL 6000 600 RPD Qualifiers 164 u2 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Hunlersville, NC 28076 (704)875.9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 (�IaceAnalytical wwwpacefabs com Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 407018 QC Batch Method: SM 2540D Associated Lab Samples: 92381218001 METHOD BLANK: 2258531 Associated Lab Samples: 92381218001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 2258532 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2258533 Parameter Total Suspended Solids SAMPLE DUPLICATE: 2258534 Parameter Total Suspended Solids Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 04119/1819:13 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 266 106 90-110 Units 92381126002 Result Dup Result mg1L ND ND Units 92381434002 Result Dup Result mg1L 19.0 18.3 RPD Qualifiers RPD Qualifiers 4 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04125/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 18 aoAnalytical mvwpacelab&=n QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 406703 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92381218001 SAMPLE DUPLICATE: 2256493 92381218001 Dup Parameter Units Result Result RPD Qualifiers pH Std. Units 7.3 7.3 0 H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 (�IacieAnalytical wwrw pacelabs.mm QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 406946 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92381218001 METHOD BLANK: 2257874 Matrix: Water Associated Lab Samples: 92381218001 Blank Reporting Parameter Units Result limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 04/21/18 08:51 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2257875 Spike 1-CS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg1L 10 9.8 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2257876 2257877 MS MSD 92380280002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 34.9 10 10 87.0 86.8 521 519 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2257878 2257879 MS MSD 92380434001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RP❑ Qua) Nitrogen, Kjeldahl, Total mg/L 8.9 10 10 20.0 20.5 110 116 90-110 3 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/2512018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 aoAnalytrcal wwwpacelabs.aom QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 407097 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92381218001 METHOD BLANK: 2258887 Associated Lab Samples: 9238121 B001 Parameter Units Nitrogen, NO2 plus NO3 mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 0412011813:31 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9D92 LABORATORY CONTROL SAMPLE: 22588BB Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mglL 2.5 2.5 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2258889 2258890 MS MSD 92381012013 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 0.052 2.5 2.5 2.6 2.6 102 102 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2258891 2258892 MS MSD 92381012014 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 0.021 2.5 2.5 2.5 2.5 100 101 75-125 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 laneAnaVical" wwwpacelabs.com Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 406861 QC Batch Method: EPA 365.1 Associated Lab Samples: 92381218001 METHOD BLANK: 2257403 Associated Lab Samples: 92381218001 Parameter Units Phosphorus mg1L LABORATORY CONTROL SAMPLE: 2257404 Parameter Units Phosphorus mglL Pace Analytical Services, LLC 9800 KinceyAve, Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 04/18/18 22:44 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2257405 2257406 MS MSD 92381218001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.44 2,5 2.5 3.0 3.0 101 101 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 aceAnalytrcal tnvw.pacelabs.aam i QUALITY CONTROL DATA Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 QC Batch: 407727 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92381218001 METHOD BLANK: 2262419 Associated Lab Samples: 92381218001 Parameter Units Chemical Oxygen Demand mg/L LABORATORY CONTROL SAMPLE: 2262420 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HuntersvHl e, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 04/25/18 00:32 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 750 757 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2262421 2262422 MS MSD 92381197001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L ND 1DO 100 21J 26.0 12 17 90-110 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2262423 2262424 MS MSD 92381193001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result ale Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 4870 100 100 4850 4820 -20 -56 90-110 1 M1 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 lacmnalXical" www.pacelabs.m n QUALIFIERS Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPO - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anaiytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/25/2018 06:23 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 lacmnalXical wwwpacwlabs.cmn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: COMPOST CENTRAL 2 Pace Project No.: 92381218 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92381218001 OUTFALL 001 EPA 1664B 407080 92381218001 OUTFALL 001 EPA 200.7 406887 EPA 200.7 92381218001 OUTFALL 001 SM 92220 406841 92381218001 OUTFALL 001 SM 2540D 407018 92381218001 OUTFALL 001 EPA 9040 406703 92381218001 OUTFALL 001 TKN+NO3+NO2 407663 Calculation 92381218001 OUTFALL 001 EPA 351.2 406946 92381218001 OUTFALL 001 EPA 353.2 407097 92381218001 OUTFALL 001 EPA 365.1 406861 92381218001 OUTFALL 001 SM 5220D 407727 Date: 04/25/2018 06:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 407014 Page 15 of 18 Document Name: Document Revised: February 7, 2018 aceAnalytical v Sample Condition Upon Recelpi(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR•CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ "untersvit 4e Ralelgh❑ Mechanicsville❑ Client Name: Project � WO : 92381218 � r U Courler: Fed Ex ❑UPS Q sps vJ � Iient I Ile I I III I I (I I II ❑ Commercial ❑Pace ❑Qther: 92361218 Custody Seal Present? ❑Yes 'PIG Seals intoct? Oyes (R`0 1 1 �1 `"1 l Daro/Initials Person tixamin ng Ca e Packing Material: ❑Bubble Wrap ❑Bubble Bags QnNone ❑ Other TFrermo afar• Gun1D: 92TO36 Type of tea: CoWet [:]Blue C Cooler Temp ('C): rrection Factor: Add/Subtract ('C) +0, j Cooler Temp Corrected ('CI: USDA Regulated Soil N/A, water sample] Did samples originate in quarantine zone within the United States: CA, NY, or SC (check maps)? Fiyes FlNo Biol gi I Tissue Frozen? []Hone ❑Yes No [-]N/A Temp ouid be above freezing to 6'C mples out of temp criteria. Samples on ice, coaling process as begun Did samples originate from a foreign source ' ter tlonaRy, indudlnit Hawall and Puerto Rim)? r lYes M. Comments/Dlscre ancy; Chain of Custody Present? es No N A 1, Samples Arrived within Hold Time? s CINU N/A 2. Short Hold Time Analysls (<72 hr.)? es ❑N/A 3, Rush Turn Around Time Requested? Yes rEFNQ QN/A Q, Sufficient Volume? � s No N/A 5. Correct Containers Used? -Pace Containers Used? r s s ❑N. No ❑N/A ❑N A 6. Containers Intact? Eaps No N/A 7. Dissolved analysis: Samples Field Filtered? Yes ❑NU ❑N/A a. Sample Lapels Match COC? �es -Includes Date/Time/ID/Analysis Malrlx: ❑Na N/A 4. Heads ate in VIDA Vials >5.6mml? Dyes []No OtftVA 10. Trip Blank Present? ❑Yes Trip Blank Custody Seals Present? ❑Yes ❑ . No N/A ,i/A 11. COMMENTS/SAMPLE DISCREPANCY 1, Lot ID of split contalnem CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes []No Person contacted: Date/Tlme: Project Manager SCURF Review: Date; Project Manager SRF Review: Date: �T- . Page 16 of 18 document Name: Document Revised: February 7, 2018 y Sample Condition upon ReceiptjSCUR} Page 1 of 2 Document No.: issuing Authority: aCBAR81ytlCal F-CAR-CS-033-Retr,06 Pace Carolinas Quality Office `Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DROIBOIS (water) DOC, LLHS "Bottom half of box is to list number of bottle Project # W®# : 92381218 PM: MWB Due Date: 04/24/18 CLIENT: 92-DECK CO _ zz L n c 7 IL E A. Z a c 7 0. E 3 m z? L n c a EVJ 3 m Oi a� c a 7 Q. N x $ yr = u� 0. m N xa 4 z z A a 2 m Z H ?q d xx a m n x 2 a IJ m '-: C a c aEE d N l7 d c 0 A ¢ r;-1 l? a ym a c = � E r M l7 a a .Ni L7 a v M e,�� l7 d _ E d E �s5 t7 a 2 x d > E T l7 o M i z d O J Oi U y ? a 7 C O E a 0 y? O a x 4 O E IL M L7 a Z 1 Y ? _ ? y 9 a 9 a 9! d N E vt '� a y y J E d •1n n z a E 4 m QQ M j E l7 a > C c = c E 7y > a 7 d a E4 1 2 N \J\N \\N\� \N\� I 4 i\\� I I \N\ \N\ 6 7 NN B 9 N I \d\NN N N 10 N N 11 —\M\ 12 �s \NN pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Caroline DEHNR Certification Office {i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. —�- Page 17 of 18 ;G,2wAM 4it-:?1 CHAIN -OF -CUSTODY 1 Analytical Request Document .. The Chain -of -Custody is a LEGAL DOCUMENT, All relevant fields must be completed accurately. Section A Section 8 Section C Required Client Information: Required Project Information; Invoica Information: Pa e 1 Of f Comr- ^fr Mecklenburg County Salad Waste Report To: Khali— Adams Attention: Address: 2145 Suttle Ave. Copy To: Company Name. Charlotla, NC 28206 res5: - - Regulatory Agency Email: krtalfem.adams ecklerburgcountync.gov Purchase Order it: Pace Quote: Phcrm: (990)344-3&56 Fa■ Prajecl Name. Compost Central 2 Paw Project Manager. mallhawbrainam pacelabs.com, ' ' State r Location ' Requested Due Date: Project M Pace Profile p3207-1 NC - Ro uasted An IysJs Fillerad IN - t Trlu cone 0 COLLECTED 2 Preservatives >- amkingwme, Ow wAtr V!T n 3 V D m W-t. wmt'-- P'ee— P SAMPLE ID i O T a a r� START F D One Character per box. Wipe WP w w g z m `o (A-Z 0-9 1 -} �" na nrr or C o a - = n U # Sample Ids must be unique n P q >.�t zs u ac r � � z o O °c rd M _ o o _ N DATE TIME DATE TIME =1 2 = _ z z O tom- g +� a LL IL r 2 44 14r -a 1l2 --- -t, Ss•,ysy r. ^pp01TiONAL COMMENTS,�?�- �:; >.RELINOUSSt[FA BY rAFFrL1ATION E6 CEPT8Y=pFFlL4oT'tOrJ ,:�. CAL UfnS f / 1102 Co f,. Environmentai Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguiclance onfilling out thisfornt, please Wsil httLi0/deg.nc.tgovlabout/divisions/energy- ill ineral-land- resources/energy-minera I-1and- perm its/storm water-perin its/npdes-ind ustrial-sw#tab-4 Permit No.: NICI-�I o l�lOV / d/ / or Certifi Facility Name: County: Inspector: Date of inspection: `Time of Inspection: "total Event Precipitation (inches): 0 - 20 NICIGIiI ua4 lbll All permits require qualitative monitoring to be performed during a "measurable storm event." (new) A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior, The 72-1101.11- storm interval does not apply ifthe permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local D1rMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Ptt � Z �� r vP r Outfall No. j _ Structure (pipe, ditch, etc.): Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Page I of 2 SWU-242, last modified 07/29/2017 2. Color: Describe the color of the discharge using11basic colors (red, brown, blue, etc.) and tint (light medium dark) as descriptors; _ tfV brO W n 3. Odor: Describe ny distir ct odors iat he di chlorine odor, etc.): Q ow a P la - may have (i.e., smells strongly ofoil, weak 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: l D 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: l 0 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: I 2 3 4 5 7. Is there any foam in the stormwater discharge? (dYes O No. Y e rY 8. Is there an oil sheen in the stormwater discharge? OYes WNO. N 0 9. Is there evidence of erosion or deposition at the outfall? O Yes VN, No 10. Other Obvious Indicators of Storm -water Pollution: List and describe No O 4IV-,r' de e G -�o r s Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWO-242, Last modified 07/28/2017 0 MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste February 2, 2018 (� f Central Files RECEIVED NCDENR / DWQ FEB 0 8 2Q18 1617 Mail Service Center Raleigh, North Carolina 27699-1617 CENTRAL FILES DWR SECTION Attention: Central Files Subject: Discharge Monitoring Report Mecklenburg County Compost Central (new) — Certificate of Coverage No. NCG240019 Dear Central Files: Please find enclosed the Discharge Monitoring Report, January 2018, for Mecklenburg County Compost Central (new), a Type I facility located at 140 Valleydale Road, North Carolina. If you have any questions, please contact me at 704-634-7705 or by email at khaliem.adams a,mecklenbur gcg ountync.ov Sincerely, . V'4"It� 1&1"� Khaliem Adams Solid Waste Environmental Specialist Enclosed: 2018 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte. North Carolina 28208 www, wipeoutwaste. com Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 2/2/2018 CERTIFICATE OF COVERAGE NO. NCG240019 FACILITY NAME Mecklenburg County Compost Central (new) COUNTY Mecklenburg County PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 92 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2018 SAMPLE QUARTER ® Jan -March ❑ April -June ❑ July -Sept ❑ Oct -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero -flow ❑Water supply [:)SA ❑Other Total event rainfall 10.23 in or ❑ No discharge this period' Date Sample Collected) (mo/dd/yr) Outfall No. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks =__> 100 mg/L4 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 01/23/2018 1 36.0 114 115 2.4 0.57 0.0061 <0.005 0.011 6.9 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 3 For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. 'The TS5 benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Fart w vehicle ivialnTenance Area IVIOnitoring Kesuiu: only Tor Tacimies averaging > 55 gal OT new moi Date Sample Collected' (mo/dd/yr) Outtall No. pH TPH using method 1664A SGT-HEM T55 Total Rainfall' Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L4 - - 01/23/2018 1 6.9 1 <5.0 36.0 0.23 75 gal/month Footnotes from Part A also annly to this Part B or oil/month. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ®NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an oriainal and one copv of this DMR. includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharae" reports) to. - Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there arq significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature 60ermiAee) (Date) Permit Dane: 10/1/2011-9/30/2016 Last Revised 12/02/11 / Page 2 of 2 aceAnalytrcal wwwpaoslabs.00m February 01, 2018 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Compost Central 2 Pace Project No.: 92370468 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on January 23, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Khaliem Adams, Meclenburg County Solid Waste A�RFO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical services, LLC. Page 1 of 18 acmnalyfical www.pacelabs.corn CERTIFICATIONS Project: Compost Central 2 Pace Project No.: 92370468 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 KinceyAve, Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida]NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 VrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 FloridalNELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, without the written consent 0 Pace Analytical Services, LLC. Page 2 of 18 (�IacleAnalytical® w%w.pacelab&= SAMPLE ANALYTE COUNT Project: Compost Central 2 Pace Project No.: 92370468 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analyses Reported Laboratory 92370468001 Outfall 1 EPA 16643 JMS 1 PASI-C EPA200.7 SH1 3 PASI•A SM 9222D KDF 1 PASI-C SM 2540D MJP 1 PASI-A EPA 9040 KMM 1 PASI-A TKN+NQ3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA 353.2 CJH1 1 PAS1-A EPA 365.1 AES2 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 Pace Analytical Services, LLC (� IacieAnalXical ® 9800Huntersv Ile, NC1280778 www.pacelabs.com (744)875-9092 ANALYTICAL RESULTS Project: Compost Central 2 Pace Project No.: 92370468 Sample: Outfall 1 Lab ID: 92370468001 Collected: 01/23/18 12:51 Received: 01/23/18 13:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mglL 5.0 1 01/25/18 04:34 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper 0.0061 mglL 0.0050 1 01/24/18 06:30 01/26/18 17:43 7440-50-8 Lead ND mglL 0.0050 1 01/24/18 06:30 01/26/18 17:43 7439-92-1 Zinc 0.011 mglL 0,010 1 01/24/18 06:30 01/26/18 17:43 7440-66-6 M1310 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 115 CFU1100 mL 1.0 1 01/23/18 14:19 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 36.0 mglL 16.7 1 01/25/18 07:58 9040 pH Analytical Method: EPA 9040 pH 6.9 Sid. Units 0,10 1 01126/1802:46 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 2.4 mg/l_ 0.52 1 01/29/18 11:45 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 2.3 mglL 0.50 1 01/27/18 00:01 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 ND mglL 0.020 1 01/26/18 03:43 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 0.57 mglL 0.050 1 01/25/1811:32 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 114 mglL 25.0 1 01/31/18 20:21 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 02:40 PM without the written consent of Pace Analytical Services, LLC Page 4 of 18 aceAnalytical www.Pacelabs.00m QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 2 Pace Project No.: 92370468 QC Batch: 395430 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 SGT-HEM, TPH Associated Lab Samples: 92370468001 METHOD BLANK: 2192127 Matrix: Water Associated Lab Samples: 92370468001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 01/25/18 04:26 LABORATORY CONTROL SAMPLE: 2192128 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 19.9 100 64-132 MATRIX SPIKE SAMPLE: 2192129 92370070001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 19.1 96 64-132 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/0112018 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 laneAnalyfical' tnvw.pacelab&cem QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 9237046B QC Batch: 395226 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 9237046B001 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersviiie, NC 28078 (704)875-9092 METHOD BLANK: 2191003 Matrix: Water Associated Lab Samples: 92370468001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Copper mg/L ND 0.0050 01I2611815:55 Lead mg/L ND 0.0050 01/2611815:55 Zinc mg1L NO 0.010 01/2611815:58 LABORATORY CONTROL SAMPLE: 2191004 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Capper m91L 5 0.50 101 85-115 Lead mg/L .5 0.49 98 85-115 Zinc mg1L .5 0.49 97 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2191005 2191006 MS MSD 92370282001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 251 .5 .5 0.73 0.76 97 101 70-130 3 ug/L Lead mg/L ND .5 .5 0.45 0.46 85 89 70-130 4 Zinc mg/L 3460 .5 .5 3.6 3.5 37 18 70-130 3 M6 ug1L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2191007 2191008 MS MSD 92370429001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 7.8 ug/L .5 .5 0.50 0.52 99 102 70-130 3 Lead mg1L ND .5 .5 0.50 0.51 99 101 70-130 2 Zinc mg1L 23.4 .5 .5 0,52 0.53 100 102 70-130 2 ug1L Results presented on this page are In the units indicated 4y the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/0112018 02:40 PM without the written consent of Pace AnaYytical Services, LLC. Page 6 of 18 aceAnalytical wiiwpacelabs.carn QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92370468 QC Batch: 395321 Analysis Method: SM 9222D QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - CHT Associated Lab Samples: 92370468001 METHOD BLANK: 2191457 Matrix: Water Associated Lab Samples: 92370468001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL ND 1.0 01/23/18 14:19 SAMPLE DUPLICATE: 2191458 92370468001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU1100 mL 115 130 12 u1 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAnalytrcal wwwpacerabs.corn Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92370468 QC Batch: 395442 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92370468001 METHOD BLANK: 2192160 Associated Lab Samples: 92370468001 Parameter Units Total Suspended Solids mg1L LABORATORY CONTROL SAMPLE: 2192161 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 01/25/18 07:53 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 252 101 90-110 SAMPLE DUPLICATE: 2192162 92370354009 Dup Parameter Units Result Result Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 2192163 92370435001 Dup Parameter Units Result Result Total Suspended Solids mg1L ND ND RPD Qualifiers RPD Qualifiers Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02101/2018 02:40 PM without the written consent of Pace Analytical Services, LI-C. Page 8 of 18 aceAnalytrcal Mvwpacela6s.=n QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 2 Pace Project No.: 9237046E QC Batch; 395594 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples. 92370468001 t SAMPLE DUPLICATE: 2193066 Parameter pH 92370341001 Dup Units Result Result RPD Qualifiers Std. Units 7.2 7.2 0 H6 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 02/01 /2018 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 lacmnalytical" www,Pacglabs mm Project: Compost Central 2 Pace Project No.: 92370468 QC Batch: 395424 QC Batch Method: EPA 351.2 Associated Lab Samples: 92370468001 METHOD BLANK: 2192094 Associated Lab Samples: 92370468001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 2192095 Parameter Units Nitrogen, Kjeldahl, Total mg1L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 351.2 Analysis Description: 351.2 TKN Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0,50 01/27/18 00:38 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 9.0 90 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2192096 2192097 MS MSD 92370316002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.9 10 10 11.8 11.5 99 96 90-110 3 MATRIX SPIKE & MATRIX SPIKE DUPLICATE; 2192098 2192099 MS MSD 92370740002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mglL 2.6 10 10 12.2 11.1 95 85 90-110 9 M1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 laneAnalytical" Pace Analytical Services, LLC 9800 Kincey Ave. Suite1 OD Hunlersville, NC 28078078 www.pacclabs.cwn (704)875-9092 QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92370468 QC Batch: 395585 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92370468001 METHOD BLANK: 2193036 Matrix: Water Associated Lab Samples: 92370468001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg1L ND 0.020 01/26/18 03:26 LABORATORY CONTROL SAMPLE: 2193037 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg1L 2.5 2.4 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2193038 2193039 MS MSD 92370354011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.3 2.3 93 93 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2193040 2193041 MS MSD 92370230001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 0.20 2.5 2.5 2.4 2.4 88 88 75-125 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02101 /2018 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalytica!® wwwpacetabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Compost Central 2 Pace Project No.: 92370468 QC Batch: 395386 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92370468001 METHOD BLANK: 2191976 Matrix: Water Associated Lab Samples: 92370468001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg1L ND 0,050 01/25/1811:27 LABORATORY CONTROL SAMPLE: 2191977 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.6 104 90.110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2191978 2191979 MS MSD 92370354016 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 103 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2191980 2191981 MS MSD 92370497007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0,14 2,5 2.5 2.8 2.7 105 104 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in futt, Date: 02101 /2018 02A0 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 (�IaneAnalytical w"pacelabs.com QUALITY CONTROL DATA Project: Compost Central 2 Pace Project No.: 92370468 QC Batch: 396112 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description; 5220D COD Associated Lab Samples: 92370468001 METHOD BLANK: 2196020 Associated Lab Samples: 92370468001 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Stank Reporting Result Limit Analyzed Qualifiers ND 25.0 01/31/18 20:21 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LA130RATORY CONTROL SAMPLE: 2196021 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 753 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2196022 2196023 MS MSD 92370468001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 114 100 100 220 223 106 109 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2196024 2196025 MS MSD 92370760001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 4490 100 100 5050 5160 560 672 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02101 /2018 02AQ PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 (�IaceAnalyfical* wuavpacelabsoom QUALIFIERS Project: Compost Central 2 Pace Project No.: 9237046E DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. POL - Practical Ouantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. u1 Results based upon colony counts outside acceptable range. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/0112018 02:40 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 (�Iacmnalytical Wimpacelabs.omn QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Compost Central 2 Pace Project No.: 92370468 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92370468001 Outfall 1 EPA 1664B 395430 92370468001 Outfall 1 EPA 200.7 395226 EPA 200.7 92370468001 Outfall 1 SM 9222D 395321 92370468001 Outfall f SM 25400 395442 92370468001 Outfall 1 EPA 9040 395594 92370468001 Outfall1 TKN+NO3+NO2 395859 Calculation 92370468001 Outfall 1 EPA 351.2 395424 92370468001 Outfall 1 EPA 353.2 395585 92370468001 Outfall 1 EPA 365.1 395386 92370468001 Outfall 1 SM 5220D 396112 Date: 02/01/2018 02:40 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 395243 Page 15 of 18 Document Name: Document Revised: August 4, 2017 Sample Condition Upon Recei t{SCUR) Page 1 of 2 Document No.: { issuing Authority: aceAnalytreal F-CAR-CS-033-Rev.04 Pace Quafty Office Laboratory receiving satrapies: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑ UM Client Name: WO# . 9Z3?046$ f Prole Lr�z/ct s#: __—_— - Courier: ❑Fed Ew ❑UPS ❑Client commercial ❑ Other:/ 92370468 Custody Seal Present? ❑Yes ❑No Seals Intact? ❑Yes No C r 2 y Date/tnitlals Person Examining Contents: Packing Material: ❑Bubble Wrap []Bubble Bags None ❑ Other Biological Tissue F ozen? ❑�N/A Thermo mre-t�er: T— ! / �,� IR Gun ID: I I kt1let ❑Blue Type of ce: ❑Yes ❑�to ❑None Correction Factor: Cooler Temp Corrected ('C): 7 Tem should be above freezing to 6'C Samples Samples Ice, out of temp criteria. on cooling process USDA Regulated Soil.( dN/A, Water samplel Did samples arigNl� In a quarantine zone within the United States: CA, NY, or SC (check maps)? Myes n has begun ma ' Did samples originate from a foreign source (intety, including Hawaii and Puerto Ricol? Flyes FfNo Comments/Discrepancy: Chain of Custody Present? Yes No N/A 1. Samples Arrived within Hold Time? es No N/A 2. Short Hold Time Analysis 02 hr.)? es ON. ❑N/A 3. Rush Turn Around Time Requested? yes ONo N/A 4. Suffi Cie rat volume? lLlOyes ❑No ON/. 5. Correct Containers Used? ONO ❑N/A 6. -Pace Containers Used? �es 2Yes No N/A Containers Intact? EfYe, 01. N/A 7. Dissolved analysis: Samples Field Filtered? QYes No N/A 8. Sample Labels Match CDC? ves ON. ❑N/A s. / -Includes Date/Time/ID/Analysis Matrix: w Headspace in VOA Vials (>5-6mm)? ❑yes ❑Np ErNI, 10. Trip Blank Present? ❑Yes No ❑NJA 11. Trip Blank Custody Seals Present? Oyes ❑No EfNIA CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comment0ample Discrepancy: Date/Prne: Field Data Required? ❑Yes ❑No Lot ID of split containers: Project Manager SCURF Review: Date: , ' a I l f i ly' igf Project Manager SRF Review: b Date: � �I—r� Note: Whenever there is a discrepancy affecting North Carolina compliance Samples, a copy of this form will be sent to the North Carolina DCHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers? Page 16 of 18 0 a 3 v v 1 n n v C W C n, b Q- O P C LA rs e eD r- 0 O a � a c O � m � a M V+ fC � C 3 (D w d Q � � � i9 a1 it CL � ,O o' Ip a Ln D 3 n v m � n m e b_ t rs a_ a N O Item+t ZZZZAZZZZZZZ MU-325 mL Plastic Unpreserved (N/A) (Cf-) BP3U-250 mL Ptastic Unpreserved (N/A) BPZU-500 ml. Plastic Unpreserved IN/A) SP1U-3 liter Plastic Unpreserved (N/A) BP45-125 mL Plastic H2504 (pH < 2) (CI-1 B 3N-2S0 mL plastic HNO3 (pH < 2) BP42-125 mL Plastic ZN Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH IpH > 12) (Cl-) WGFU-Wide-mouthed Glass jar Unpreserved AG1U-1 liter Amber Unpreserved (N/A) ICI-) AGIM-) liter Amber HCl (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (CI-) AG2S-1 liter Amber H2SO4 (PH, 2) AG3S-250 mL Amber H2SO4 (pH < 2) AWA(DG3A)-250 mi Amber NH4Cl (N/A)(CI-) DG9H.40 ml VOA HCI (N/A) VG9T-40 mL VOA Na25203 INN VG5U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOAN (6 vials per kit)-S035 kit (N/A) V/GK (3wials per kit)-VPH/Gas kit (N/A) 5P5T-125 m1 Sterile Plastic IN/A — lab) ` SP2T.250 mL Sterile Plastic (N/A — lab) BP3A-250 mL Plastic (NH2)2504 (9.3-9.7) Cubitainrr VSGU-20 mL Scintillation vials (N/A) GN 'm M 1 =r .0. fb = n �o CL 3 ar ly 0 x �, ut CL er at � t7 'Cr '6 ? S rO m p' x &n 'L N S O Crm O n x W n � R � a z m � -Ow 7 0 Cr Q .��. a � � S u+ O 7 d R a 7 r 3 M Z 3 —i z9g: w N 1 3 m 0 7 O C) f0 0 1'f t9 O r 41 O r GO tb CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a. LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page : 1 Of 1 Company Mer-kienbLarg Counly SOW Waste Report To; Darren Steinhilber Attention: Address: 2145 Suttle Ave Copy To: Company Name: Charlotte, NC 28208 Address: - .x., REgulatory Agoncyl rs Email: daren.sleinhiiber@rnockler�urgco�rt am Purchase Order a_ Pace Quote: Plmne; (7D4)33fi-0447 Fax Project Name; Co m Central 2 Pace Project Manager. mmithL w,Lrainard pace Labs com. State 1 t_ocation:". = y •1'- Requemed Due Date: Project A: Paco Profile R. 3207-1 NC Requested Anal gala Fllierad Y!N IMTRlx CCDe s COLLECTED = Preservatives a pnn.gw.lN IhV Wain WT a V 4 U Wa[In W.I. WW v P C D _ SAMPLE ID Psoari P ° a i ty a START END O V One Character per box_ Wt" WP n z ca w G o 4 (A-Z, 0-9 1. .I ann aT u r 2 rt o }. F o o .oi Sample Ids erwst be uni4ue Tnw Ty J J p m O '/7%� 3 NTQATETIMEjI DATE TIME __= z z o r r r n v_ rt t u ( V�l/� j tall -W• IO�I T. /? �3: rs" >+s 1 P '8' <.16 _ =.12 ADUmONAL'CQNMENT r, '��";r_'p C'� -Z? -RELJNgU1SFiFD BYlAFF1LIAT7QN -� DAiE �.+,k pCCEPTEDBY l AFF3UATGPJTIME :••4t•SAMPLE CONDfT1ON9��` r, .� i i' v ,V. G� lip•" G.S I `7 f1 7.. 1- ti SAMPLER NAME AN_D SIGNATURE ';- ll' of M LER: / ! � " m S - RE of AIAPLER: 1 ✓ D/yTE IQ j a a m u u 2 a p 2 m 2 En C} m rn m a_ Fnviro=enral Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling oul this fibrin, please visit littps://deg.nc.gov/about/divisiga /ene,rgy-mi,nerallland- resources/eneney-mineral-land-permits/storinwater-permits/npdes-industrial-swgtab-4 Permit No.: NIC&aIAID l O10/ 01 orNificate of Coverage No.: NIC/G/alAl D / /111p1 Facility Name:_ ��I��6u,(�� U I_�d�l'ilIJ�ST I C/I�i��t�l 1 n�ti County: JVW [1T\ Inspector: Date of Inspection Time of Inspection rif, " Total Event Precipitation (inches): 1 U Phone No. Ali permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall escription: �/ j Outfall No. Structure (pipe, ditch, etc.): pl' {� ` U Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Page 1 of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the disc] rge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: C 3. Odor: Describe any distinct odo�rrs�that the di barge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): NO n r# n �� i +( - ''p 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stonrwater discharge, where l is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? W Yes O No. J 8. is there an oil sheen in the stormwater discharge? OYes VN0. / ►► 9. Is there evidence of erosion or deposition at the outfall? O Yes V10. 10. Other Obvious Indicators of Stormf�w_ate�r Pollution: list and describe A �I t Yl � G�XJG eGk, r`5 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 5WU-242, last modified 0728/2017 MECKLENBURG COUNTY Land Use & Environmental Services Agency Solid Waste November 9, 2017 Central Files NCDI?Q / DEMLR 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Central Files RECEIVED NOV 27 Z017 CENTRAL FILES UWR SECTION Subject: Discharge Monitoring Report Mecklenburg County Compost Central (new) — Certificate of' Coverage No`.,NCG240019 t Dear Central Files: Please hind enclosed the Discharge Monitoring Report, October -December 2017, For the Mecklenburg County Compost Central (new), a barge Type I facility located at 140 Valleydale Road in Charlotte, North Carolina. If YOU have any questions, please contact me at 704-634-7705 or by email at Khaliem.adams a,mecklenbur Tcg�ync.ggy Sincerely, Khaliem Adams Solid Waste Environmental Specialist }Inclosed: 2017 DMR PEOPLE • PRIDE PROGRESS • PARTNERSHIP 2145 Suttle Avenue Charlotte, North Carolina 282028 mm.wipeoutwastc.cum Environmental Qua7lty Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit https://(ieg.nc.gov/al)out/divisions/energy-mineral-land- resources/cnergy-mineral-land-permits/stormwater-perniits/npdes-industrial-sw#tab-4 q Permit No.: NICI_I_I_I_I_I_I_I or Certificate of Coverage No.: NIC/G/ c71�I OI�1 I Facility Name: f County: lilt e (k� Inspector: 14 A a (: Date of Inspection: Time of Inspection: Phone No. Total Event Precipitation (inches): of - I lylc'ryJ ro-TA All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) 1. Outfall Description: Outfall No. 1 Structure (pipe, ditch, etc.): P' e Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Pagel of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color oft ei discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: r W fl f 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,l weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5-is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no solids and 5 is extremely muddy: 16 2 3 4 5 7. Is there any foam in the stormwater discharge? k DYe 0 No. 8. Is there an oil sheen in the stormwater discharge? 0Yes (� N�. 9. Is there evidence of erosion or deposition at the outfall? O Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 9WU-242, isst modified 07/28/2017 Quarterly Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG240000 Date submitted 11/09/17 CERTIFICATE OF COVERAGE NO. NCGi240016 FACILITY NAME _Mecklenburg County Compost Central (new) COUNTY Mecklenbure Countv PERSON COLLECTING SAMPLES Khaliem Adams LABORATORY: Pace Analytical Services Lab Cert. # 12 Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2017 SAMPLE QUARTER ❑ Jan -March ❑ April -June ❑ July -Sept ® Oct -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA ❑Zero -flow ❑Water Supply ❑SA ❑Other Total event rainfall z 2.1 in or ❑ No discharge this period' Date Sample Colle Collected' [ma/ cted' Outfall No. T55 COD Fecal coliform Total nitrogen Total phosphorus Total copper Total lead Total zinc pH Parameter benchmarks __> 100 mg/La 120 mg/L 1000 col./100 mL 30 mg/L 2 mg/L 0.010 mg/L 0.075 mg/L 0.126 mg/L 6-9 10/24/17 1 19.0 56.0 >6000 1.4 0.35 <0.005 <0.005 <0.10 7.1 1 Monthly sampling (instead of quarterly) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. a For sampling periods with no discharge, you must still submit this discharge monitoring report with a checkmark here. °The TSS benchmark value is 100 mg/L; except when discharging to ORW, HQW, Trout, and PNA waters in which case the benchmark is 50 mg/L. Permit Date: 10/1/2011-9/30/2016 Last Revised 12/02/11 Page 1 of 2 Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new motor oil/month. Date Sample Collected' (mo/dd/yr) Outfall No. pH TPH using method 1664A SGT-HEM T55 Total Rainfall' Check if No Flow This Period' Average New Motor Oil Usage 6-9 15 mg/L 100 mg/L' - - 10/24/17 1 7.1 1 <5.0 19.0 2.1 1 75 gal/month Footnotes from Part A also apply to this Part B FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Teresa Bradford Mail an original and one copy of this DMR, includina all "No Discharae" reports, within 30 days of receipt of the lab results for at end of monitorina period in the case of "No Discharae" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure-that.qualified.personnel. properly. gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and-b-elief,-true,-accurate,-and-complete- am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." i;fr0/l/2011-9/30/2016 P.ytee) !e: (Date) Last Revised.12/02/11' Page 2 of 2 0 aceAnalytical www.paceraea.com October 31, 2017 Darren Steinhilber Mecklenburg County Solid Waste 2145 Suttle Ave Charlotte, NC 28208 RE: Project: Central Compost 2-Valleydale Pace Project No.: 92360297 Dear Darren Steinhilber: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 24, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs. com (704)875-9092 Project Manager Enclosures PCB REPORT OF LABORATORY ANALYSIS V This report shall not be reproduced, except in full, 9A�without the written consent of Pace Analytical Services, LLC. Page i of 18 aceAnalytical� www.pacpiahs =n Project: Central Compost 2-Valleydale Pace Project No.: 92360297 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 LouisianalNELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification M M-NC030 VirginiafVELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville. NC 28078 (704)875-9092 Page 2 of 18 aceAnalytrcal" www.pacalabac= I " SAMPLE ANALYTE COUNT Project: Central Compost 2-Valleydale Pace Project No.: 92360297 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample I❑ Method Analysts Analytes Reported Laboratory 92360297001 Outfall 001 EPA 1664E JMS 1 PASI-C EPA200.7 SH1 3 PASi-A SM 9222D KDF 1 PASI-C SM 2540D WC 1 PAS I -A EPA 9040 ECH 1 PAS I -A TKN+NO3+NO2 Calculation EWS 1 PASI-A EPA 351.2 BRJ 1 PASI-A EPA353.2 CJH1 1 PASI-A EPA 365+1 MDW 1 PASI-A SM 5220D NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Anatytical Services, LLC. Page 3 of 18 _ aceAnalytical` wwwpacelabu.com ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Central Compost 2-Valleydale Pace Project No.: 92360297 Sample: Outfall 001 Lab ID: 92360297001 Collected: 10/24/17 10:59 Received: 10/24/17 11:59 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT HEM, TPH Analytical Method: EPA 1654B Total Petroleum Hydrocarbons NO mg1L 5.0 1 10126/17 03:25 200.7 MET ICP Analytical Method: EPA 2007 Preparation Method: EPA 200.7 Copper NO mglL 0.0050 1 10/26/17 15:40 10/27/17 23:03 7440-50-8 Lead NO mg11- 0,0050 1 10/26/17 15:40 10/27/17 23:03 7439-92-1 Zinc NO mg1L 0.010 1 10/26/17 15A0 10/27/17 23:03 7440-66-6 MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D Fecal Coliforms 6000 CFU1100 mL 1.0 1 10/24/17 14:31 u2. 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 19.0 mg1L 12.5 1 10125/17 20:35 9040 pH Analytical Method: EPA 9040 pH 7.1 Sid. Units 0.10 1 10/25/17 17:12 H6 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Total Nitrogen 1.4 mg1L 0.12 1 10/31/17 11:15 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 1.4 mglL 0.50 1 10/31/17 00:14 7727-37-9 353.2 Nitrogen, N021NO3 pros. Analytical Method: EPA 353.2 Nitrogen, NO2 plus NO3 NO mg1L 0,020 1 10126117 04:00 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 0.35 mglL 0.050 1 10/27/17 21:24 7723-14-0 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 56.0 mglL 25.0 1 10/25/17 19:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 IaaAnalyticai wwwpacelebs.com Project: Central Compost 2-Valleydale Pace Project No.: 92360297 QC Batch: 384025 QC Batch Method: EPA 1664B Associated Lab Samples: 92360297001 METHOD BLANK: 2128406 Associated Lab Samples: 92360297001 Parameter Units Total Petroleum Hydrocarbons. mg1L LABORATORY CONTROL SAMPLE: 2128407 Parameter Units Total Petroleum Hydrocarbons mg/L Pace Analytical Services, LLC 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 SGT HEM, TPH Matrix; Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 10/26/17 03:16 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 19.5 98 64-132 MATRIX SPIKE SAMPLE: 2128408 92359385001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 19.2 96 64-132 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right or the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 18 _ aceAnalytical wwwpacelabs.com QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92360297 QC Batch: 384115 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92360297001 METHOD BLANK: 2128861 Associated Lab Samples: 92360297001 Parameter Units Copper mg1L Lead mg/L Zinc mg/L Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 10/27/17 21:28 ND 0.0050 10/27/17 21:28 NO 0.010 10127/17 21:28 Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Hunlersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2128862 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L .5 0.48 96 85-115 Lead mg1L .5 0.47 94 85-115 Zinc mg1L .5 0.47 94 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128863 2128864 MS MSD 92359340006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 376 .5 .5 0.85 0.86 94 98 70-130 2 ug/L Lead mg1L ND .5 .5 0.44 0.45 88 90 70-130 2 Zinc mg1L 243 .5 .5 0,69 0.70 90 92 70-130 2 ug/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128865 2128866 MS MSD 92360049003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L NO .5 .5 0,49 0.49 97 97 70-130 0 Lead mg1L NO .5 .5 0.48 0.47 95 95 70-130 1 Zinc mg/L 65.5 .5 .5 0.55 0,54 96 96 70-130 0 ug/L Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 18 a-eAnalytical. www,pacelabitbrrr Project: Central Compost 2-Valleydale Pace Project No.: 92360297 OC Balch: 383899 QC Batch Method: SM 9222D Associated Lab Samples: 92360297001 METHOD BLANK: 2127681 Associated Lab Samples: 92360297001 Parameter Units Fecal Coliforms CFU11 OD mL SAMPLE DUPLICATE: 2127682 Parameter Units Fecal Coliforms CFU1100 mL QUALITY CONTROL DATA Analysis Method: SM 92220 Analysis Description: 9222D MBIO Fecal Cotiform - CHT Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 10/24/17 14:31 92360297001 Dup Result Result RPD Qualifiers 6000 600 164 u2 Pace Analytical Services, LLC 9800 Kincey Ave Suite 100 Huntersville, NC 28078 (704)e75-9092 Results presented on this page are In the units indicated by tha "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 Pace Analytical Services, LLC Iane*lalXical' 980U Kincey Ave. Suite100 Huntersville, NC 28078078 WNW.pacelabamm (704)875-9092 QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92360297 QC Batch: 383996 Analysis Method: SM 25400 QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92360297001 METHOD BLANK: 2128309 Matrix: Water Associated Lab Samples: 92360297001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L N❑ 2.5 10/25/17 20:31 LABORATORY CONTROL. SAMPLE; 2128310 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 240 96 90.110 SAMPLE DUPLICATE: 2128311 92360395002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 34.8 35.6 2 SAMPLE DUPLICATE: 2128312 92360491005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L ND ND Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in M, Date: 10/31 /2017 04:31 PM without the written consent of Pace Analytical Services, LLC, Page 8 of 18 aceAnalytical � www,pdt:elabs.corh QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92360297 QC Batch: 383907 Analysis Method: EPA 9040 QC Batch Method: EPA 9040 Analysis Description: 9040 pH Associated Lab Samples: 92360297001 SAMPLE DUPLICATE: 2127731 92360352001 Dup Parameter Units Result Result RPD Qualifiers pH Std. Units 6.9 6.9 0 H6 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 aceAnalyiical www,pacelabs.twm QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92360297 QC Batch: 384087 Analysis Method: EPA 351.2 QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN Associated Lab Samples: 92360297001 METHOD BLANK: 2128641 Matrix: Water Associated Lab Samples: 92360297001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/31/17 00:07 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2128542 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.5 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128643 2128644 MS MSD 92360211002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.4 10 10 9.5 9.6 81 82 90-110 1 M1 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10131 /2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 (�IapeAnalytical wwwpacelabs.com QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92360297 QC Batch: 383886 Analysis Method: EPA 353.2 QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved Associated Lab Samples: 92360297001 METHOD BLANK: 2127546 Associated Lab Samples: 92360297001 Parameter Units Nitrogen, NO2 plus NO3 mg/L LABORATORY CONTROL SAMPLE: 2127548 Parameter Units Nitrogen, NO2 plus NO3 mg1L Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 10126/17 03:43 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127549 2127550 MS MSD 92359886002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 0.25 2.5 2.5 2.B 2.8 101 101 75-125 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127551 2127552 MS MSD 92359566001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.29 2.5 2.5 2.7 2.6 95 94 75-125 0 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC, Page 11 of 18 lan eAnalytical wwwpacolab&com QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92360297 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 384014 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92360297001 METHOD BLANK: 2128363 Matrix: Water Associated Lab Samples: 92360297001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 10/27/17 21:19 LABORATORY CONTROL SAMPLE: 2128364 Spike LCS LCS % Rec Parameter units Cone. Result % Rec Limits Qualifiers Phosphorus mg1L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128365 2128366 MS MSD 92360015001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 14.3 2.5 2.5 15.0 17.2 25 115 90-110 14 M6,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128367 2128368 MS MSD 92360469001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RP❑ Qual Phosphorus mg/L 0.37 2.5 2.5 3.0 3.0 107 106 90-110 1 Results presented on this page are in the units Indicated by the "units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not he reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 (�IaceAnaWical � www.pacelaL.i.cam QUALITY CONTROL DATA Project: Central Compost 2-Valleydale Pace Project No.: 92360297 QC Batch; 383806 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92360297001 METHOD BLANK: 2127238 Matrix: Water Associated Lab Samples: 92360297001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 10/25/17 19:16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huatersvilie, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2127239 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg1L 750 755 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127240 2127241 MS MSD 92360015004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc, Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 169 750 750 861 868 92 93 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2127242 2127243 MS MSD 92359510005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg1L 47.0 750 750 739 748 92 93 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date; 10/31/2017 04:31 PM without the written consent or Pace Analytical Services, LLC. Page 13 of 18 aceAnalytical e WWW;acefabscarrr QUALIFIERS Project: Central Compost 2-Valleydale Pace Project No.: 92360297 DEFINITIONS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrotein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H6 Analysis initiated outside of the 15 minute EPA required holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. u2 Colonies are too numerous to count. Actual result may be greater than reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/31/2017 04:31 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 aceAnalytrcal* wwwpacelatu.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Central Compost 2-Valleydale Pace Project No.: 92360297 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersviile, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92360297001 Outfall 001 EPA 1664B 384025 92360297001 Outfall 001 EPA 200.7 384115 EPA 200.7 92360297001 Outfall 001 SM 9222D 383899 92360297001 Outfall 001 SM 2540D 383996 92360297001 Outfall 001 EPA 9040 383907 92360297001 Outfall 001 TKN+NO3+NO2 384653 Calculation 92360297001 Outfall 001 EPA 351.2 384087 92360297001 Outfall 001 EPA 353.2 383886 923602970DI Outfall 001 EPA 365A 384014 92360297001 Outfall 001 SM 5220❑ 383808 Date: 10/31/2017 04:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 384336 Page 15 of 18 Document Name: Document Revised: August 4, 2017 Sample Condition Upon Rete€ t(SCUR) Page 1 of 2 Document No.: Issuing Authority: . r af;eAnaVical f F-CAR•CS-033•Rev.04 Pace Quality Office Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersvll Ratetgh❑ Mechanicsville[] Client Name: ! WO# 92360297 r IffI �I Courler. ❑Fed Ex ❑UPS ❑USPS 4B nt I II� III I I� II �I ❑ Commercial ❑Pace ❑Other: i 9z3613!97 Custody Seal Present? ❑Yes "E� o� Seals Intact? ❑Yes 8176— Date/tnitlals Person Examining Content rE . "2- % Packing Material: ❑Bubble Wrap JE�ubble Hags ❑None ❑ other Biological Tissue Frozen? Thermometer: _i_7u ❑yes [:]No fNTN � •-wet ©91ue ❑atone 'Erlt Gun ID: Type of Ice: Correction Factor: Cooler Temp Corrected ('C): Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated SotrY'Q'N/A, water sample] Did samples oLgiaate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internationally, Ivor Nn inelvdinv Hawaii and Puprtn Rlrni, ny,.. ' F-9I'ro Commen is/Discrepancy: Chain of Custody Present? No N/A 1. Samples Arrived within Hold Time? es QN0 N/A 2. Short Hold Time Analysis <72 hr.)? Dyes .Q*d ❑N/A 1 3. Rush Turn Around Time Requested? ❑Yes wt! ONJA 4, Sufficient Volume? �es ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? - 1-Y;, ON. No ❑N/A FNIA 6, Containers Intact? _4afes ONo ❑N/A 7. Dissolved analysis: Samples Field Filtered? Dyes A` 8h Sample Labels Match COC? -Includes Date/Time/ID/Analysls Matrix: -,12rirs ❑No ❑N/A 9. Heads ace in VOA Vials I>S•bmmj? ❑Yes ONO ,®tska" 1.0, Trip Blank Present? Trip Blank Custody Seals Present? Oyes ches ❑No ONO caw&, OwA-1 L1. ' CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comments/Sample Discrepancy: Lot 10 of split containers: Date/Time: Field Data Required? UYes UNo Project Manager SCURF Review: 4M.2 Date: [ of 1r1 I i _ Project Manager SRF Review: �� Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certif€catlon Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 16 of 18 T v Co <o V O a I 3 n 0 K O v' n b n S v a -n O. C r^ fl m a r! ro � � A O a 3 mj m c �a � A � O eD tA 3 M m 9 CL IL 4^ M " Cu n ' � a a tp 3 %A 3 a C a R 9 a� S m c m 0 1p co rh N A N .- nemN BP4U-12S mt Plastic Unpreserved IN/A) (CI-) 8P3U-250 mL Plastic Unpreserved (N/A) 8P2U.500 mL Plastic Unpreserved (N/A) SP1U-1 liter Plastic Unpreserved (N/A) SP4S.125 mi-Plaslk H2504 (pH < 2) JCI-) BP3N.250 mL plastic HNO3 (pH < 2) S -125 mL Plastic 2N Acetate & NaOH (�g) BR4C-125mL Plastic NaOH (pH-Y2) (CI-) wGFu-wide-mouthed Glass jar Unpreserved AG1U-1 Ilter Amber Unpreserved (N/A) (CI-) z z z zzzzi?<.. AG1H-1 Titer Amber HCl (pH < 2) AG31.1-250 mt. Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber H2504 (pH < 21 AGM-250 mL Amber H2504 (pH < 2) AG3A[i1G3A(-250 mL Amber NH4CI (N/A)(CI-) DG9H40 mL VOA HCI (N/A) VG9T-40 mL V0A Na25203 (N/A) VG91JA0 mL VOA Unp (N/A) OGSP-40 rnL V0A H3PO4 IN/A) VOAR (6 vials per kit)-S035 kit (N/A) V/GK 13 vials per kitFVPH/Gas kit (N/A) SP5T-375 rnLStcrile Plastic (N/A— lab) SPIT-250 mi.5terilePlastiC (N/A —lab) SP3A-250 mL Plastic (NH2)2504 (93-9.7) Cubitairw VSGU-20 mL Scintillation vials (N/Aj GN fD A 0 3 w Q. 3 .► _ an CLCU 0 3 -0 \ Cr S T ci tf x 3 cnn (] Cr 0 N 3 Cr n N a L D10 � Cr CL 0 It rn vt 0 m' T � � R Q n n v a b A C W .T r.r p Z w 0 2 = b m o w 3 m m A � O r1 m � � a at r 3 • Nrn N n I] ra c 0 w q w x N CLw C1 ? n O M n 1 O m y a r* iV ti A � o W Co CHAIN -OF -CUSTODY 1 Analytical Request Document Z�Zwvclr Ttie Chaln-of-Custody is.i LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project tnlonnation: Invoice Information: Page: t of 1 Company: Mecklenbn County Solid Waste Report To; barren Sleinhilbet Atlantiari' Address' 2145 Suttle Ave Copy To; Company Name: - Charlotte. NC28208 Address: —_- "Regil Email' daren.sleinhilber ,Mecklenbu CWn ev Pur-haso Order#; Paco Quote: Pnone: 704-57s-1537 FeK Project Name: Central Compost 2 - Valle ale Paca Protect Manauer. matthevi.hralnafd ACQIabS.LOm Requested Due Date: Project K; Pace Profile a: 32D7-1 NC RequestedAneE sll Filtered YIN s. rt'; ..:.[ •''"`-'"x " T"" r'"r^ "" f `� �� COLLECTED 7 Preservatives }:`.. `-".�s-i• ormuny wsAn OW wwR wt o u O W.T. Warn ww W pp�n P SAMPLE ID ot START END F ¢ F� z One Character per box. woe Vir 0-9 ana or Z w - >m r° 1 y +� � e Ids must b Semple ids must 6a unique Tcsw rs x j U „ � O o � ,� : � � cam. � a L 7Q, 0).L'�� r a O c y � z w O o '$ m nY. DATE RATE v+ _ = o Zit r u �. I- O u tr •'�1 i ITIME tl '.� 1TIME V Outfall00t VYT 5t� t[) S 1?�i x x x x Ix x x >a- ;Y1. �^- e " y yA17F)m01iAL t;OMMENT9 v r °" a` B t+.:R>ilniaulsNeoer,rFlLutTaaN` a~ _x - �,._ „� �- gY,, AFF Il.%ATION � 9�A�PLE GRNOyTIa� ^�. - a _.. - _-�.,:_.�_�._' i . . "'ar_ - ✓ f"Gk':e-a. 4.s ��:>.zrax.r.a. �;-;.•, .. .j:� _ .>-CCEPTEO _ r. t..'" a„ k; 011, c- I J �� fC II. C jK t-/,'!J y C Adf v t 7 IL i 5AfdPLER NAEIE_AND SIGNATUREI ^•''. --•: �^� x'!r sssa z`a ° c . >.. w•. PRINT Nama of SAMPLER: i SIGNATURE or SAMPLER:` DATE Signed: j�� wOff f to 0 00 aceAnalXical www.pacafabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Compost Central 2 92392987 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92392987001 Outfall 1 EPA 1664B 421183 92392987001 Outfall 1 EPA 200.7 Rev 4.4 1994 420878 EPA 200.7 Rev 4.4 1994 420907 92392987001 Outfall 1 SM 9222D-2006 421070 SM 9222D-2006 421072 92392987001 Outfall 1 SM 2540D-2011 421415 92392987001 Outfall 1 EPA 9040C 420875 92392987001 Outfall1 TKN+NO3+NO2 422285 Calculation 92392987001 Outfall 1 EPA 351,2 Rev 2,0 1993 420880 EPA 351.2 Rev 2.0 1993 421828 92392987001 Outfall 1 EPA 353.2 Rev 2.0 1993 421985 92392987001 Outfall 1 EPA 365.1 Rev 2.0 1993 421019 EPA 365.1 Rev 2.0 1993 421706 92392987001 Outfall 1 SM 5220D-2011 421157 SM 5220D-2011 421348 Date: D810112018 08:53 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 18 Document Name: Document Revised: Februar/ 7, 2018 aceAnalyticalA Sample Condition Upon Recei t(SCUR Page 1 of Z Document No.: Issuing Authority: F-CAR•CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: _ Asheville ❑ Eden[] Greenwood ❑ Huntersville-El----'- Raleigh❑ Mechanicsville[] Client Name: WO : 92392987 Courier: Fed x ❑UP ❑LISPSQlent ❑ Commercial ❑Pace ❑Other: 114 `111BB iii 1111 ! Rf 1111 111 .82392987— — Custody Seal Present? Oyes ❑ Seals Intact? ❑Yes pNo-- � Date/Initials Pusan Esamfning [ontents '%—d Packing Material: ❑Bubble Wrap 43rubble Bags []None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes ❑No—Q*tA--"- �GUn iD: 92T040 Type of Ice: et ©slue []None Cooler Temp ('C): j4, qCorrection Factor: Add/5ubtract ('C) +0.4 Cooler Temp Corrected ('C): Temp should be above freezing to 6'C ❑Samples out of temp criteria. Samples on Ice, tooling process hasbegurs USDA Regulated Soil tEMT, water sample) Did Samples on i e in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally, nyes No Inciudina Hawail and Puerto Rico)? f 1Yes 17-1810-- [ammeets/Discrepancy: Chain of Custody Present? Yes No N/A 1. Samples Arrived within Hold Time? es ❑No ❑N/A 2. , Short Hold Time Anai sis <72 hr.l? cs ' No N/ Rush Turn Around Time Re uested7 ❑Yes No N/A 4. Sufficient Volume? ei ❑NO ❑N/A 5. Correct Containers Used? -Pace Containers Used? es es [IN. No ❑N/A ❑N/A 6. Containers Intact? ONO ❑N/A 7, Dissolved analysis: Samples Field Filtered? ❑yes o ❑N/A B. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: ;akf' [:)No ❑N/A 9. Headspace in VOA Vials (55-6mm)7 Dyes No /A 10. Trip Blank Present? TripBlank Custody Seals Present? [DYES Dyes ❑No ONO ❑ A 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Field Data Required? []Yes ONO Lot ID of split containers; Date: 711 Date: Page 16 of 18 D 7 0 ro ti 0 m a 0 v m S K• m s 0 7 rs' � n � n n. o p� = N ra 9 n ro w � d r— o aq7 m Oa n ro W, H 3 ro m a � Q e 9 � Cu A n � a c rp 3 a c d 0 a 19 n c n 0 ._ Item# 9P41J-125 mL Plastic Unpreserved (NIA) (CH 8133U-250 mL Plastic Unpreserved (N/A) OP2U-500 ml. Plastic Unpreserved (N/A) 6P1U-1 titer Plastic Unpreserved (NIA) 9P4S-125 mL Plastic H2504 (pit < 2) {CI-) PM-2SO mL plastic HNO3 (pH < 21 BM-125 mL Plastic ZN Acetate & NaOH (>9) BP4C-125 mL Plastic NaOH (pH > 12) (Cl-) WGFU-Wide-mouthed Glass jar Unpreserved AG 1U-1 liter Amster Unpreserved (NIA) (CI-) AG1H-1 Ilter Amber HCI (pH < 2) AG3U.250 ml. Amber Unpreserved (N/A) (CI-) AG1S-1 liter Amber H2504 (pH < 2) AG35-250 mL Amber H25O4 (pl i < 2) AG3A(DG3A}-250 ml-Amber NH4C7 (N/A)(CI-) D69W40 mL VOA HCI (N/A) VG9T-40 mL VOA Na2S2O3 (N/A( VG9U-40 mL VOA Unp (N/A) DG9P-40 mL VOA H3PO4 (N/A) VOAK (6 vials per kit)-5035 kit (N/A) V/GK 13 vials per kit)-VPH/Gas kit (N/A) SP5T-125 mL Sterile Plastic (N/A —lab) SM-250 mL Sterile Plastic (N/A — lab) BP3A-250 mL Plastic (NH2)25O4 (9.3-93) AGOU-100 mt Amber Unpreserved vials (N/A) VSGU-20 mL Scinillialion vials MA) 11G9U-40 ml Amber Unpreserved vials tN/A) • T N C t m m ob -gym 0 °y y L x 3 O � r .. 0 -M S Cr 5, W 0 3 ,. x , =r �. H 0 M 0 n r 0 p In, G w A x fi C a d f�D N rp 6r O 3 L �. CI CM O Cr mo o. o o a m n _ 10 v m r~aftl O 1 v c � 0 R O o � = 3 tW O W n+ \ r qD O C) zu (A) CD NJ w/y� CW V 00 Section A Reeulred Client Int—lion- Section 8 Ranuired Praiect Information: CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. section C Invoke Information: Paae - t Of 1 Company: Mecklenburg CoumX Solid Waste Report To: Khaliem Adams Attention Address: 2145 SultleAve. Copy To: Company Name: Charlotte, NC 2e2De Address: Email khaliem.a r;xY-k$e raync vy Purchase Order tr: PaceOuole. Phone: (980)314-e55 Fax Project Name: Compost Central Pars Project Manager. rnalthew.brainard ceiabs.com, =�'-= �' �•..-r :: i;SStste 1 Locatlon " '_s-�t-.zr� Requested Due Date: Project M: Pace Profile F: 3207-1 NC uealed Analysis Filtered M - 2' COLLECTED Preservatives _ } - MATRlx CODE o Z ix m Ormkne Watm ON wue, wT 9 U W warts Wafer WVu RotlU[l P SAMPLE ID o.�b s� u 8 START END @' F, Z Y Q �i 0 } m One Character per box wtpo w'P _ _ 2' 2R # (A-4 D-9I, -) 012e, oT Sample Ids must be unique T.— Ts x ¢ a TDATETTME w R. `p U m < 0 O =O O y g m' R b •. J7 1 W N a Z� 2 is _rsB DATE TIME s= x = z i O _ v" N Yi- IXIi V--1 0`� -91 JYJX A Il _ram �3u rar4r 5 �� ' .6, •� 8; 9 "`' 3 .��,ADl1rTfONAL'WMMENTK �-t-�•. 3�a���.�+�? „!K?�i-_�r,��-�..�:� -tr ;�� �L, f]ATExb' x -`_-A � ,�?_ _ 'X-'�;•.' k�, yTIME�_ F�':. GONO1TlON5.a.it _ --i t - P i,NJQ�V',,� li GZ � 00